data_DS2112D _audit_creation_method SHELXL-2014/6 _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'In K S6 Sn2' _chemical_formula_weight 583.66 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'In' 'In' -0.7276 1.3100 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'K' 'K' 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Sn' 'Sn' -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system trigonal _space_group_IT_number 166 _space_group_name_H-M_alt 'R -3 m :H' _space_group_name_Hall '-R 3 2"' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' 'y, x, -z' '-x, -x+y, -z' 'x-y, -y, -z' 'x+2/3, y+1/3, z+1/3' '-y+2/3, x-y+1/3, z+1/3' '-x+y+2/3, -x+1/3, z+1/3' 'y+2/3, x+1/3, -z+1/3' '-x+2/3, -x+y+1/3, -z+1/3' 'x-y+2/3, -y+1/3, -z+1/3' 'x+1/3, y+2/3, z+2/3' '-y+1/3, x-y+2/3, z+2/3' '-x+y+1/3, -x+2/3, z+2/3' 'y+1/3, x+2/3, -z+2/3' '-x+1/3, -x+y+2/3, -z+2/3' 'x-y+1/3, -y+2/3, -z+2/3' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' '-y, -x, z' 'x, x-y, z' '-x+y, y, z' '-x+2/3, -y+1/3, -z+1/3' 'y+2/3, -x+y+1/3, -z+1/3' 'x-y+2/3, x+1/3, -z+1/3' '-y+2/3, -x+1/3, z+1/3' 'x+2/3, x-y+1/3, z+1/3' '-x+y+2/3, y+1/3, z+1/3' '-x+1/3, -y+2/3, -z+2/3' 'y+1/3, -x+y+2/3, -z+2/3' 'x-y+1/3, x+2/3, -z+2/3' '-y+1/3, -x+2/3, z+2/3' 'x+1/3, x-y+2/3, z+2/3' '-x+y+1/3, y+2/3, z+2/3' _cell_length_a 3.68030(10) _cell_length_b 3.68030(10) _cell_length_c 26.1276(16) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_volume 306.48(3) _cell_formula_units_Z 1 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 6906 _cell_measurement_theta_min 2.339 _cell_measurement_theta_max 52.142 _exptl_crystal_description sheet _exptl_crystal_colour yellow _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 3.162 _exptl_crystal_F_000 264 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.280 _exptl_crystal_size_mid 0.280 _exptl_crystal_size_min 0.120 _exptl_absorpt_coefficient_mu 7.208 _shelx_estimated_absorpt_T_min 0.237 _shelx_estimated_absorpt_T_max 0.478 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.237 _exptl_absorpt_correction_T_max 0.478 _exptl_absorpt_process_details SADABS _exptl_absorpt_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source ? _diffrn_measurement_device_type 'CCD area detector' _diffrn_measurement_method 'phi and omega scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 2654 _diffrn_reflns_av_unetI/netI 0.0138 _diffrn_reflns_av_R_equivalents 0.0383 _diffrn_reflns_limit_h_min -4 _diffrn_reflns_limit_h_max 4 _diffrn_reflns_limit_k_min -4 _diffrn_reflns_limit_k_max 4 _diffrn_reflns_limit_l_min -33 _diffrn_reflns_limit_l_max 33 _diffrn_reflns_theta_min 4.681 _diffrn_reflns_theta_max 27.864 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.992 _diffrn_measured_fraction_theta_full 0.990 _diffrn_reflns_Laue_measured_fraction_max 0.992 _diffrn_reflns_Laue_measured_fraction_full 0.990 _diffrn_reflns_point_group_measured_fraction_max 0.992 _diffrn_reflns_point_group_measured_fraction_full 0.990 _reflns_number_total 124 _reflns_number_gt 124 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Bruker SMART' _computing_cell_refinement 'Bruker SMART' _computing_data_reduction 'Bruker SAINT' _computing_structure_solution 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL-2014/6 (Sheldrick, 2014)' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0999P)^2^+2.7784P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens . _refine_ls_hydrogen_treatment undef _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 124 _refine_ls_number_parameters 13 _refine_ls_number_restraints 12 _refine_ls_R_factor_all 0.0308 _refine_ls_R_factor_gt 0.0308 _refine_ls_wR_factor_ref 0.1090 _refine_ls_wR_factor_gt 0.1090 _refine_ls_goodness_of_fit_ref 1.091 _refine_ls_restrained_S_all 1.064 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group In1 In 0.0000 0.0000 0.0000 0.0070(6) Uani 0.3332 12 d S T P A 4 Sn1 Sn 0.0000 0.0000 0.0000 0.0070(6) Uani 0.6667 12 d S T P A 4 S1 S 0.3333 0.6667 0.05544(11) 0.0085(8) Uani 1 6 d S T P A 4 K1 K -0.1667 0.6667 0.1667 0.020(7) Uani 0.06 4 d S TU P B 1 K2 K 0.0000 0.0000 0.1660(15) 0.027(7) Uani 0.0767 6 d S TU P C 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 In1 0.0021(6) 0.0021(6) 0.0167(8) 0.000 0.000 0.0011(3) Sn1 0.0021(6) 0.0021(6) 0.0167(8) 0.000 0.000 0.0011(3) S1 0.0060(10) 0.0060(10) 0.0134(13) 0.000 0.000 0.0030(5) K1 0.025(10) 0.032(10) 0.006(8) -0.003(8) -0.001(4) 0.016(5) K2 0.033(8) 0.033(8) 0.014(9) 0.000 0.000 0.017(4) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag In1 S1 2.5715(17) 19 ? In1 S1 2.5715(17) 19_665 ? In1 S1 2.5715(17) 1_445 ? In1 S1 2.5715(17) 1_545 ? In1 S1 2.5715(17) 19_565 ? In1 S1 2.5715(17) . ? S1 Sn1 2.5715(17) 1_565 ? S1 In1 2.5715(17) 1_565 ? S1 Sn1 2.5715(17) 1_665 ? S1 In1 2.5715(17) 1_665 ? K1 K1 1.84014(5) 2_565 ? K1 K1 1.84015(5) 3_455 ? K1 K1 1.84015(5) 3_465 ? K1 K1 1.84016(5) 2_675 ? K1 K1 3.18722(8) 3_565 ? K1 K1 3.18723(8) 2_665 ? K1 K1 3.18724(8) 2_575 ? K1 K1 3.18725(8) 3_355 ? K1 K1 3.68029(10) 1_565 ? K1 K1 3.68029(10) 1_455 ? K1 K1 3.68030(10) 1_445 ? K1 K1 3.68030(10) 1_665 ? K2 K2 2.1251(14) 25 ? K2 K2 2.1251(13) 25_445 ? K2 K2 2.1251(13) 25_455 ? K2 K2 3.68030(10) 1_445 ? K2 K2 3.68030(15) 1_665 ? K2 K2 3.68030(10) 1_655 ? K2 K2 3.68030(11) 1_565 ? K2 K2 3.68030(10) 1_455 ? K2 K2 3.68030(11) 1_545 ? K2 K2 4.2498(7) 25_545 ? K2 K2 4.2498(7) 25_565 ? K2 K2 4.2498(7) 25_345 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag S1 In1 S1 91.38(8) 19 19_665 ? S1 In1 S1 88.62(8) 19 1_445 ? S1 In1 S1 180.00(11) 19_665 1_445 ? S1 In1 S1 88.62(8) 19 1_545 ? S1 In1 S1 88.62(8) 19_665 1_545 ? S1 In1 S1 91.38(8) 1_445 1_545 ? S1 In1 S1 91.38(8) 19 19_565 ? S1 In1 S1 91.38(8) 19_665 19_565 ? S1 In1 S1 88.62(8) 1_445 19_565 ? S1 In1 S1 180.00(11) 1_545 19_565 ? S1 In1 S1 180.0 19 . ? S1 In1 S1 88.62(8) 19_665 . ? S1 In1 S1 91.38(8) 1_445 . ? S1 In1 S1 91.38(8) 1_545 . ? S1 In1 S1 88.62(8) 19_565 . ? Sn1 S1 In1 0.0 1_565 1_565 ? Sn1 S1 In1 91.4 1_565 . ? In1 S1 In1 91.38(8) 1_565 . ? Sn1 S1 Sn1 91.38(8) 1_565 1_665 ? In1 S1 Sn1 91.38(8) 1_565 1_665 ? In1 S1 Sn1 91.4 . 1_665 ? Sn1 S1 In1 91.4 1_565 1_665 ? In1 S1 In1 91.38(8) 1_565 1_665 ? In1 S1 In1 91.38(8) . 1_665 ? Sn1 S1 In1 0.0 1_665 1_665 ? K1 K1 K1 60.0 2_565 3_455 ? K1 K1 K1 120.0 2_565 3_465 ? K1 K1 K1 180.0 3_455 3_465 ? K1 K1 K1 180.0 2_565 2_675 ? K1 K1 K1 120.0 3_455 2_675 ? K1 K1 K1 60.0 3_465 2_675 ? K1 K1 K1 150.0 2_565 3_565 ? K1 K1 K1 90.0 3_455 3_565 ? K1 K1 K1 90.0 3_465 3_565 ? K1 K1 K1 30.0 2_675 3_565 ? K1 K1 K1 90.0 2_565 2_665 ? K1 K1 K1 30.0 3_455 2_665 ? K1 K1 K1 150.0 3_465 2_665 ? K1 K1 K1 90.0 2_675 2_665 ? K1 K1 K1 60.0 3_565 2_665 ? K1 K1 K1 90.0 2_565 2_575 ? K1 K1 K1 150.0 3_455 2_575 ? K1 K1 K1 30.0 3_465 2_575 ? K1 K1 K1 90.0 2_675 2_575 ? K1 K1 K1 120.0 3_565 2_575 ? K1 K1 K1 180.0 2_665 2_575 ? K1 K1 K1 30.0 2_565 3_355 ? K1 K1 K1 90.0 3_455 3_355 ? K1 K1 K1 90.0 3_465 3_355 ? K1 K1 K1 150.0 2_675 3_355 ? K1 K1 K1 180.0 3_565 3_355 ? K1 K1 K1 120.0 2_665 3_355 ? K1 K1 K1 60.0 2_575 3_355 ? K1 K1 K1 120.0 2_565 1_565 ? K1 K1 K1 180.0 3_455 1_565 ? K1 K1 K1 0.0 3_465 1_565 ? K1 K1 K1 60.0 2_675 1_565 ? K1 K1 K1 90.0 3_565 1_565 ? K1 K1 K1 150.0 2_665 1_565 ? K1 K1 K1 30.0 2_575 1_565 ? K1 K1 K1 90.0 3_355 1_565 ? K1 K1 K1 60.0 2_565 1_455 ? K1 K1 K1 120.0 3_455 1_455 ? K1 K1 K1 60.0 3_465 1_455 ? K1 K1 K1 120.0 2_675 1_455 ? K1 K1 K1 150.0 3_565 1_455 ? K1 K1 K1 150.0 2_665 1_455 ? K1 K1 K1 30.0 2_575 1_455 ? K1 K1 K1 30.0 3_355 1_455 ? K1 K1 K1 60.0 1_565 1_455 ? K1 K1 K1 0.0 2_565 1_445 ? K1 K1 K1 60.0 3_455 1_445 ? K1 K1 K1 120.0 3_465 1_445 ? K1 K1 K1 180.0 2_675 1_445 ? K1 K1 K1 150.0 3_565 1_445 ? K1 K1 K1 90.0 2_665 1_445 ? K1 K1 K1 90.0 2_575 1_445 ? K1 K1 K1 30.0 3_355 1_445 ? K1 K1 K1 120.0 1_565 1_445 ? K1 K1 K1 60.0 1_455 1_445 ? K1 K1 K1 180.0 2_565 1_665 ? K1 K1 K1 120.0 3_455 1_665 ? K1 K1 K1 60.0 3_465 1_665 ? K1 K1 K1 0.0 2_675 1_665 ? K1 K1 K1 30.0 3_565 1_665 ? K1 K1 K1 90.0 2_665 1_665 ? K1 K1 K1 90.0 2_575 1_665 ? K1 K1 K1 150.0 3_355 1_665 ? K1 K1 K1 60.0 1_565 1_665 ? K1 K1 K1 120.0 1_455 1_665 ? K1 K1 K1 180.0 1_445 1_665 ? K2 K2 K2 119.98(12) 25 25_445 ? K2 K2 K2 119.98(12) 25 25_455 ? K2 K2 K2 119.98(12) 25_445 25_455 ? K2 K2 K2 149.99(7) 25 1_445 ? K2 K2 K2 30.01(6) 25_445 1_445 ? K2 K2 K2 90.000(1) 25_455 1_445 ? K2 K2 K2 30.01(6) 25 1_665 ? K2 K2 K2 149.99(7) 25_445 1_665 ? K2 K2 K2 90.000(2) 25_455 1_665 ? K2 K2 K2 180.0 1_445 1_665 ? K2 K2 K2 30.01(6) 25 1_655 ? K2 K2 K2 90.000(2) 25_445 1_655 ? K2 K2 K2 149.99(7) 25_455 1_655 ? K2 K2 K2 120.000(2) 1_445 1_655 ? K2 K2 K2 60.000(1) 1_665 1_655 ? K2 K2 K2 90.000(1) 25 1_565 ? K2 K2 K2 149.99(7) 25_445 1_565 ? K2 K2 K2 30.01(6) 25_455 1_565 ? K2 K2 K2 120.000(2) 1_445 1_565 ? K2 K2 K2 60.0 1_665 1_565 ? K2 K2 K2 120.000(4) 1_655 1_565 ? K2 K2 K2 149.99(7) 25 1_455 ? K2 K2 K2 90.0 25_445 1_455 ? K2 K2 K2 30.01(6) 25_455 1_455 ? K2 K2 K2 60.0 1_445 1_455 ? K2 K2 K2 120.000(3) 1_665 1_455 ? K2 K2 K2 180.0 1_655 1_455 ? K2 K2 K2 60.000(1) 1_565 1_455 ? K2 K2 K2 90.000(1) 25 1_545 ? K2 K2 K2 30.01(6) 25_445 1_545 ? K2 K2 K2 149.99(6) 25_455 1_545 ? K2 K2 K2 60.000(1) 1_445 1_545 ? K2 K2 K2 120.000(3) 1_665 1_545 ? K2 K2 K2 60.0 1_655 1_545 ? K2 K2 K2 180.0 1_565 1_545 ? K2 K2 K2 120.000(1) 1_455 1_545 ? K2 K2 K2 59.997(14) 25 25_545 ? K2 K2 K2 59.997(14) 25_445 25_545 ? K2 K2 K2 179(3) 25_455 25_545 ? K2 K2 K2 90.0 1_445 25_545 ? K2 K2 K2 90.000(2) 1_665 25_545 ? K2 K2 K2 30.003(16) 1_655 25_545 ? K2 K2 K2 149.997(18) 1_565 25_545 ? K2 K2 K2 149.997(18) 1_455 25_545 ? K2 K2 K2 30.003(15) 1_545 25_545 ? K2 K2 K2 59.997(15) 25 25_565 ? K2 K2 K2 179(3) 25_445 25_565 ? K2 K2 K2 59.997(17) 25_455 25_565 ? K2 K2 K2 149.997(17) 1_445 25_565 ? K2 K2 K2 30.003(16) 1_665 25_565 ? K2 K2 K2 90.000(2) 1_655 25_565 ? K2 K2 K2 30.003(14) 1_565 25_565 ? K2 K2 K2 90.0 1_455 25_565 ? K2 K2 K2 149.997(18) 1_545 25_565 ? K2 K2 K2 119.99(3) 25_545 25_565 ? K2 K2 K2 179(3) 25 25_345 ? K2 K2 K2 59.997(15) 25_445 25_345 ? K2 K2 K2 59.997(14) 25_455 25_345 ? K2 K2 K2 30.003(16) 1_445 25_345 ? K2 K2 K2 149.997(18) 1_665 25_345 ? K2 K2 K2 149.997(18) 1_655 25_345 ? K2 K2 K2 90.0 1_565 25_345 ? K2 K2 K2 30.003(17) 1_455 25_345 ? K2 K2 K2 90.0 1_545 25_345 ? K2 K2 K2 119.99(3) 25_545 25_345 ? K2 K2 K2 119.99(3) 25_565 25_345 ? _refine_diff_density_max 3.000 _refine_diff_density_min -0.510 _refine_diff_density_rms 0.367 _shelxl_version_number 2014/6 _shelx_res_file ; TITL DS2112D in R-3m CELL 0.71073 3.6803 3.6803 26.1276 90.000 90.000 120.000 ZERR 1 0.0001 0.0001 0.0016 0.000 0.000 0.000 LATT 3 SYMM - Y , X - Y , Z SYMM - X + Y , - X , Z SYMM Y , X , - Z SYMM - X , - X + Y , - Z SYMM X - Y , - Y , - Z SFAC In K S Sn UNIT 1 1 6 2 OMIT -2 56 L.S. 20 ACTA BOND FMAP 2 PLAN 5 CONF eadp in1 sn1 exyz in1 sn1 size 0.28 0.28 0.12 ISOR 0.01 K1 K2 temp -173.15 WGHT 0.099900 2.778390 FVAR 0.15332 PART 4 MOLE 1 IN1 1 0.000000 0.000000 0.000000 10.02777 0.00214 0.00214 = 0.01667 0.00000 0.00000 0.00107 SN1 4 0.000000 0.000000 0.000000 10.05556 0.00214 0.00214 = 0.01667 0.00000 0.00000 0.00107 S1 3 0.333333 0.666667 0.055437 10.16667 0.00597 0.00597 = 0.01344 0.00000 0.00000 0.00298 PART 1 K1 2 -0.166667 0.666667 0.166667 10.01500 0.02542 0.03196 = 0.00588 -0.00254 -0.00127 0.01598 PART 2 K2 2 0.000000 0.000000 0.166037 10.01278 0.03317 0.03317 = 0.01400 0.00000 0.00000 0.01659 PART HKLF 4 1 -1.0000 -1.0000 0.0000 0.0000 1.0000 0.0000 0.0000 0.0000 -1.0000 REM DS2112D in R-3m REM R1 = 0.0308 for 124 Fo > 4sig(Fo) and 0.0308 for all 124 data REM 13 parameters refined using 12 restraints END WGHT 0.0562 9.8607 REM Highest difference peak 3.000, deepest hole -0.510, 1-sigma level 0.367 Q1 1 0.0000 0.0000 0.0288 10.16667 0.05 3.00 Q2 1 0.3333 0.6667 0.0301 10.16667 0.05 1.11 Q3 1 0.0000 0.0000 0.0580 10.16667 0.05 0.77 Q4 1 0.3333 0.6667 0.0805 10.16667 0.05 0.56 Q5 1 0.1677 0.3355 0.0336 10.50000 0.05 0.45 ; _shelx_res_checksum 67753 _shelx_hkl_file ; -1 -1 0 709.66 35.17 1 -2 0 698.72 34.91 2 -1 0 636.55 34.88 2 -1 0 698.88 34.96 2 -1 0 686.06 35.13 -2 1 0 672.90 34.94 -2 1 0 713.39 34.91 -2 1 0 685.42 34.88 -3 0 0 328.25 18.44 -3 0 0 335.95 18.51 -3 0 0 349.14 18.36 -3 0 0 376.40 18.12 -3 0 0 319.04 18.39 -3 0 0 329.95 18.38 3 0 0 347.22 18.37 3 0 0 366.36 18.19 3 0 0 338.60 18.39 0 -3 0 363.25 18.07 3 -3 0 367.18 18.23 3 -3 0 374.13 18.40 3 -3 0 392.18 18.38 3 -3 0 332.20 18.33 -3 3 0 388.55 18.44 -3 3 0 411.49 18.15 -3 0 0 342.64 18.14 -4 2 0 265.12 14.10 -4 2 0 265.51 14.11 -4 2 0 275.89 13.79 2 -4 0 249.24 13.93 4 -2 0 258.55 14.16 -4 2 0 252.29 14.11 4 -2 0 261.25 14.03 4 -2 0 271.27 13.79 4 -2 0 278.35 14.01 4 -2 0 252.38 13.89 4 -2 0 265.86 14.12 4 -2 0 269.86 13.96 -4 2 0 277.04 13.95 -2 -2 0 290.39 13.66 -2 -2 0 278.32 13.89 2 -4 0 293.18 13.67 -5 4 0 168.10 8.14 -4 -1 0 151.59 8.07 -1 -4 0 160.02 7.98 4 -5 0 172.73 8.10 -5 1 0 149.81 8.36 5 -1 0 149.61 8.59 -4 -1 0 150.08 8.50 -4 -1 0 147.90 8.43 -5 1 0 144.24 8.12 -5 1 0 167.88 9.03 1 -5 0 154.96 7.98 4 1 0 157.68 8.15 5 -4 0 158.69 8.15 5 -4 0 167.24 8.65 5 -4 0 162.57 8.55 5 -4 0 142.01 8.44 5 -4 0 148.72 8.78 -5 1 0 150.92 8.58 -5 1 0 149.93 8.63 5 -1 0 148.96 8.15 -5 1 0 151.39 8.07 6 -3 0 110.66 6.38 6 -3 0 110.02 6.04 -6 3 0 111.88 6.08 6 -3 0 120.77 6.69 6 -3 0 115.55 6.73 -3 -3 0 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-29 24.79 2.01 -3 -1 -29 27.15 2.05 4 -1 29 22.69 1.76 4 -1 29 24.40 2.07 4 -3 -29 26.17 2.15 -1 -3 29 23.62 1.62 -1 -3 29 22.03 1.84 -1 -3 29 25.18 2.07 1 3 -29 21.86 1.59 -4 1 -29 25.02 2.03 -4 3 29 22.23 1.58 3 -4 -29 22.95 1.58 1 -4 29 25.35 1.96 -4 1 -29 24.33 2.20 1 -4 29 20.70 1.81 1 -4 29 25.52 1.98 3 -4 -29 24.93 1.94 1 -4 29 23.39 1.61 -4 1 -29 20.15 1.60 3 -4 -29 24.34 2.08 -4 1 -29 24.62 1.96 3 1 29 22.57 1.73 -4 0 29 22.95 2.09 4 -4 29 19.35 1.89 4 0 -29 19.96 1.54 4 -4 29 19.77 1.93 4 -4 29 22.41 1.88 0 -4 -29 23.01 1.42 -4 0 29 23.34 2.31 3 -5 29 21.69 1.88 2 -5 -29 18.52 1.31 3 -5 29 15.47 1.49 -5 2 29 20.12 2.21 3 -5 29 20.53 1.82 3 -5 29 19.27 1.48 3 2 -29 18.03 1.65 -5 3 -29 16.92 1.53 -5 2 29 15.16 1.97 -5 2 29 17.90 1.46 5 -3 29 16.81 1.72 5 -2 -29 18.02 1.67 5 -3 29 19.26 1.59 5 -3 29 19.46 1.78 5 -2 -29 23.58 2.55 5 -2 -29 19.10 1.47 5 -3 29 19.21 1.99 -3 -2 29 19.98 1.84 -3 -2 29 21.50 2.03 -2 -3 -29 21.07 1.33 5 -3 29 19.60 1.89 -3 -2 29 17.79 1.43 5 -5 -29 17.21 1.94 -5 0 -29 19.56 2.04 5 0 29 17.34 2.33 5 -5 -29 18.80 2.25 -5 0 -29 18.03 1.97 -5 5 29 16.38 2.39 0 -5 29 14.39 1.46 -4 -2 -29 15.18 1.57 -2 -4 29 15.55 1.79 -4 -2 -29 15.21 1.85 6 -2 29 14.77 1.76 6 -4 -29 18.53 3.25 6 -2 29 14.23 1.60 2 -6 29 15.46 1.69 -6 2 -29 15.76 2.53 4 -6 -29 15.03 1.94 -6 2 -29 12.26 1.43 4 2 29 12.13 2.04 2 -6 29 15.96 2.27 -6 4 29 14.77 1.95 1 -6 -29 15.11 1.44 5 1 -29 16.80 2.52 1 -6 -29 12.76 1.18 5 -6 29 14.25 2.22 -6 5 -29 14.46 2.17 6 -1 -29 13.75 2.06 -5 6 -29 13.78 2.44 -1 -5 -29 12.46 1.39 -1 -5 -29 11.21 1.22 -7 4 -29 7.35 1.72 4 -7 29 11.73 2.20 -7 3 29 15.05 1.98 3 -7 -29 9.75 1.60 -3 -4 -29 10.55 1.61 7 -4 29 9.85 4.16 0 0 30 34.64 2.12 0 0 -30 36.01 2.00 0 0 30 33.63 2.03 0 0 30 36.49 2.29 0 0 30 34.94 2.39 0 0 -30 36.58 2.30 0 0 -30 37.45 2.25 0 0 -30 36.02 2.29 0 0 30 37.50 2.41 0 0 -30 34.56 2.00 0 0 30 36.18 2.10 0 0 -30 36.65 2.30 1 -2 30 18.03 1.34 1 -2 30 21.21 1.64 -1 -1 30 21.56 1.78 1 -2 30 20.04 1.46 -1 -1 -30 25.14 1.53 -2 1 -30 21.34 1.35 1 -2 -30 22.82 1.67 1 -2 -30 23.19 1.64 1 -2 -30 21.78 1.59 1 -2 30 21.98 1.63 -1 -1 -30 21.72 1.30 1 -2 30 19.42 2.00 1 -2 30 18.93 1.77 2 -1 30 19.08 1.71 -1 -1 -30 23.13 1.78 2 -1 30 17.34 1.37 2 -1 -30 18.27 1.69 -2 1 30 18.41 1.35 2 -1 -30 21.63 1.75 2 -1 -30 19.45 1.71 -1 -1 30 21.70 1.73 -1 -1 30 20.21 1.34 1 -2 30 21.82 1.43 2 -1 -30 18.34 1.77 -2 1 -30 20.78 1.70 -1 -1 -30 22.17 1.36 -1 -1 -30 22.85 1.57 2 -1 30 19.43 1.77 -1 -1 30 20.68 1.30 2 -1 30 19.72 1.54 1 -2 -30 22.87 1.35 -2 1 -30 16.53 1.59 -1 -1 30 20.76 1.47 -1 2 -30 20.43 1.29 1 -2 30 22.93 1.31 -2 1 -30 22.36 1.72 1 1 -30 21.53 1.84 -2 1 -30 20.76 1.75 -1 -1 30 22.29 1.44 2 -1 -30 20.12 1.33 2 -1 30 20.08 1.60 -1 2 30 19.58 1.30 1 1 -30 21.06 1.35 -1 -1 -30 23.76 1.60 3 -3 -30 14.57 1.67 0 -3 30 16.38 1.32 3 0 -30 19.99 2.30 -3 0 30 18.22 1.87 -3 0 30 16.98 1.75 3 -3 -30 14.92 1.56 3 0 30 21.48 1.47 0 -3 30 20.74 1.73 3 -3 30 13.23 1.54 -3 0 -30 20.76 1.83 0 -3 30 17.32 1.52 -3 3 30 15.84 1.28 0 3 -30 16.59 1.19 -3 0 30 18.85 1.75 3 -3 30 12.90 1.60 0 -3 30 19.02 1.52 -3 0 30 21.16 2.07 3 -3 -30 17.34 1.33 -3 0 30 16.90 1.23 3 0 -30 16.24 1.26 -3 0 30 18.84 1.32 -3 0 -30 19.39 1.24 4 -2 30 15.97 1.79 2 -4 30 14.23 1.36 4 -2 30 16.43 1.63 2 -4 -30 15.41 1.43 -2 -2 30 16.71 1.72 2 -4 30 16.47 1.57 2 2 30 17.23 1.34 4 -2 -30 17.79 1.96 2 -4 30 17.13 1.53 -2 4 -30 15.71 1.21 -4 2 -30 16.54 1.67 4 -2 30 15.11 1.46 -2 4 30 19.39 1.27 4 -2 30 18.14 1.59 4 -2 -30 17.59 1.78 -4 2 30 15.75 1.25 -4 2 30 15.72 1.90 -2 -2 -30 19.72 1.43 -2 -2 30 14.31 1.50 2 2 -30 15.69 1.28 4 -2 30 14.48 1.64 4 -2 30 15.88 1.37 2 -4 -30 17.56 1.58 -2 -2 30 14.63 1.19 2 -4 -30 15.56 1.14 4 -2 -30 16.31 1.28 4 -2 -30 15.22 1.42 -2 -2 30 14.00 1.54 -2 -2 -30 17.55 1.16 -2 -2 -30 19.50 1.46 2 -4 30 14.40 1.21 4 -5 30 10.37 1.25 4 -5 30 10.12 1.32 -5 1 30 10.12 1.34 -1 -4 30 10.25 1.17 -5 1 30 11.97 1.84 -5 1 30 12.75 2.06 4 -5 30 10.88 1.50 -5 1 30 14.39 2.43 4 -5 30 12.57 1.52 5 -4 -30 15.41 2.14 1 -5 -30 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