data_lty2277_0m _audit_creation_date 2017-04-13 _audit_creation_method ; Olex2 1.2 (compiled 2017.03.28 svn.r3405 for OlexSys, GUI svn.r5335) ; _shelx_SHELXL_version_number '2014/7' _publ_contact_author_address ? _publ_contact_author_email ? _publ_contact_author_id_orcid ? _publ_contact_author_name '' _publ_contact_author_phone ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety '0.5(C96 H24 Gd16 N12 O96), 1(O)' _chemical_formula_sum 'C48 H12 Gd8 N6 O49' _chemical_formula_weight 2714.64 _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Gd' 'Gd' -8.8380 11.9157 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'cubic' _space_group_IT_number 225 _space_group_name_H-M_alt 'F m -3 m' _space_group_name_Hall '-F 4 2 3' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z' '-x, y, -z' 'x, -y, -z' 'z, x, y' 'z, -x, -y' '-z, -x, y' '-z, x, -y' 'y, z, x' '-y, z, -x' 'y, -z, -x' '-y, -z, x' 'y, x, -z' '-y, -x, -z' 'y, -x, z' '-y, x, z' 'x, z, -y' '-x, z, y' '-x, -z, -y' 'x, -z, y' 'z, y, -x' 'z, -y, x' '-z, y, x' '-z, -y, -x' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' '-x, y+1/2, -z+1/2' 'x, -y+1/2, -z+1/2' 'z, x+1/2, y+1/2' 'z, -x+1/2, -y+1/2' '-z, -x+1/2, y+1/2' '-z, x+1/2, -y+1/2' 'y, z+1/2, x+1/2' '-y, z+1/2, -x+1/2' 'y, -z+1/2, -x+1/2' '-y, -z+1/2, x+1/2' 'y, x+1/2, -z+1/2' '-y, -x+1/2, -z+1/2' 'y, -x+1/2, z+1/2' '-y, x+1/2, z+1/2' 'x, z+1/2, -y+1/2' '-x, z+1/2, y+1/2' '-x, -z+1/2, -y+1/2' 'x, -z+1/2, y+1/2' 'z, y+1/2, -x+1/2' 'z, -y+1/2, x+1/2' '-z, y+1/2, x+1/2' '-z, -y+1/2, -x+1/2' 'x+1/2, y, z+1/2' '-x+1/2, -y, z+1/2' '-x+1/2, y, -z+1/2' 'x+1/2, -y, -z+1/2' 'z+1/2, x, y+1/2' 'z+1/2, -x, -y+1/2' '-z+1/2, -x, y+1/2' '-z+1/2, x, -y+1/2' 'y+1/2, z, x+1/2' '-y+1/2, z, -x+1/2' 'y+1/2, -z, -x+1/2' '-y+1/2, -z, x+1/2' 'y+1/2, x, -z+1/2' '-y+1/2, -x, -z+1/2' 'y+1/2, -x, z+1/2' '-y+1/2, x, z+1/2' 'x+1/2, z, -y+1/2' '-x+1/2, z, y+1/2' '-x+1/2, -z, -y+1/2' 'x+1/2, -z, y+1/2' 'z+1/2, y, -x+1/2' 'z+1/2, -y, x+1/2' '-z+1/2, y, x+1/2' '-z+1/2, -y, -x+1/2' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z' '-x+1/2, y+1/2, -z' 'x+1/2, -y+1/2, -z' 'z+1/2, x+1/2, y' 'z+1/2, -x+1/2, -y' '-z+1/2, -x+1/2, y' '-z+1/2, x+1/2, -y' 'y+1/2, z+1/2, x' '-y+1/2, z+1/2, -x' 'y+1/2, -z+1/2, -x' '-y+1/2, -z+1/2, x' 'y+1/2, x+1/2, -z' '-y+1/2, -x+1/2, -z' 'y+1/2, -x+1/2, z' '-y+1/2, x+1/2, z' 'x+1/2, z+1/2, -y' '-x+1/2, z+1/2, y' '-x+1/2, -z+1/2, -y' 'x+1/2, -z+1/2, y' 'z+1/2, y+1/2, -x' 'z+1/2, -y+1/2, x' '-z+1/2, y+1/2, x' '-z+1/2, -y+1/2, -x' '-x, -y, -z' 'x, y, -z' 'x, -y, z' '-x, y, z' '-z, -x, -y' '-z, x, y' 'z, x, -y' 'z, -x, y' '-y, -z, -x' 'y, -z, x' '-y, z, x' 'y, z, -x' '-y, -x, z' 'y, x, z' '-y, x, -z' 'y, -x, -z' '-x, -z, y' 'x, -z, -y' 'x, z, y' '-x, z, -y' '-z, -y, x' '-z, y, -x' 'z, -y, -x' 'z, y, x' '-x, -y+1/2, -z+1/2' 'x, y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' '-x, y+1/2, z+1/2' '-z, -x+1/2, -y+1/2' '-z, x+1/2, y+1/2' 'z, x+1/2, -y+1/2' 'z, -x+1/2, y+1/2' '-y, -z+1/2, -x+1/2' 'y, -z+1/2, x+1/2' '-y, z+1/2, x+1/2' 'y, z+1/2, -x+1/2' '-y, -x+1/2, z+1/2' 'y, x+1/2, z+1/2' '-y, x+1/2, -z+1/2' 'y, -x+1/2, -z+1/2' '-x, -z+1/2, y+1/2' 'x, -z+1/2, -y+1/2' 'x, z+1/2, y+1/2' '-x, z+1/2, -y+1/2' '-z, -y+1/2, x+1/2' '-z, y+1/2, -x+1/2' 'z, -y+1/2, -x+1/2' 'z, y+1/2, x+1/2' '-x+1/2, -y, -z+1/2' 'x+1/2, y, -z+1/2' 'x+1/2, -y, z+1/2' '-x+1/2, y, z+1/2' '-z+1/2, -x, -y+1/2' '-z+1/2, x, y+1/2' 'z+1/2, x, -y+1/2' 'z+1/2, -x, y+1/2' '-y+1/2, -z, -x+1/2' 'y+1/2, -z, x+1/2' '-y+1/2, z, x+1/2' 'y+1/2, z, -x+1/2' '-y+1/2, -x, z+1/2' 'y+1/2, x, z+1/2' '-y+1/2, x, -z+1/2' 'y+1/2, -x, -z+1/2' '-x+1/2, -z, y+1/2' 'x+1/2, -z, -y+1/2' 'x+1/2, z, y+1/2' '-x+1/2, z, -y+1/2' '-z+1/2, -y, x+1/2' '-z+1/2, y, -x+1/2' 'z+1/2, -y, -x+1/2' 'z+1/2, y, x+1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, y+1/2, -z' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z' '-z+1/2, -x+1/2, -y' '-z+1/2, x+1/2, y' 'z+1/2, x+1/2, -y' 'z+1/2, -x+1/2, y' '-y+1/2, -z+1/2, -x' 'y+1/2, -z+1/2, x' '-y+1/2, z+1/2, x' 'y+1/2, z+1/2, -x' '-y+1/2, -x+1/2, z' 'y+1/2, x+1/2, z' '-y+1/2, x+1/2, -z' 'y+1/2, -x+1/2, -z' '-x+1/2, -z+1/2, y' 'x+1/2, -z+1/2, -y' 'x+1/2, z+1/2, y' '-x+1/2, z+1/2, -y' '-z+1/2, -y+1/2, x' '-z+1/2, y+1/2, -x' 'z+1/2, -y+1/2, -x' 'z+1/2, y+1/2, x' _cell_length_a 27.860(3) _cell_length_b 27.860(3) _cell_length_c 27.860(3) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 21623(7) _cell_formula_units_Z 4 _cell_measurement_reflns_used 9899 _cell_measurement_temperature 240 _cell_measurement_theta_max 65.230 _cell_measurement_theta_min 2.748 _shelx_estimated_absorpt_T_max 0.299 _shelx_estimated_absorpt_T_min 0.143 _exptl_absorpt_coefficient_mu 15.913 _exptl_absorpt_correction_T_max 0.207 _exptl_absorpt_correction_T_min 0.107 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ? _exptl_absorpt_special_details ? _exptl_crystal_colour 'clear colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 0.834 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description 'block' _exptl_crystal_F_000 4984 _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.1 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0894 _diffrn_reflns_av_unetI/netI 0.0184 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 32 _diffrn_reflns_limit_h_min -23 _diffrn_reflns_limit_k_max 32 _diffrn_reflns_limit_k_min -27 _diffrn_reflns_limit_l_max 32 _diffrn_reflns_limit_l_min -31 _diffrn_reflns_number 36398 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 65.184 _diffrn_reflns_theta_max 65.184 _diffrn_reflns_theta_min 2.747 _diffrn_ambient_temperature 240.01 _diffrn_detector 'CCD area detector' _diffrn_detector_area_resol_mean 8 _diffrn_detector_type 'APEX II CCD' _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device_type 'Bruker X8 Prospector Ultra' _diffrn_measurement_method ? _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_source 'IMuS micro-focus source' _diffrn_source_target Cu _diffrn_standards_number ? _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 768 _reflns_number_total 991 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'SAINT v8.34A (Bruker, 2013)' _computing_data_collection ? _computing_data_reduction 'SAINT v8.34A (Bruker, 2013)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _refine_diff_density_max 1.202 _refine_diff_density_min -1.177 _refine_diff_density_rms 0.215 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.164 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 43 _refine_ls_number_reflns 991 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0850 _refine_ls_R_factor_gt 0.0668 _refine_ls_restrained_S_all 1.164 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1518P)^2^+373.4749P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2306 _refine_ls_wR_factor_ref 0.2550 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All N(H,H) groups 2. Others Fixed Sof: N1(0.125) H1A(0.125) H1B(0.125) O4S(0.16667) 3.a X=CH2 refined with riding coordinates: N1(H1A,H1B) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Gd1 Gd 0.20141(2) 0.29859(2) 0.29859(2) 0.0382(6) Uani 1 6 d S T P . . O2 O 0.2152(3) 0.2152(3) 0.2848(3) 0.041(3) Uani 1 6 d S T P . . O3S O 0.1504(3) 0.3496(3) 0.3496(3) 0.081(5) Uani 1 6 d S T P . . O1 O 0.2218(3) 0.2782(3) 0.3749(4) 0.177(10) Uani 1 2 d S T P . . C1 C 0.2500 0.2500 0.3972(8) 0.16(2) Uani 1 4 d S T P . . C2 C 0.2500 0.2500 0.4499(7) 0.138(16) Uani 1 4 d S T P . . C3 C 0.2808(5) 0.2192(5) 0.4760(6) 0.144(11) Uani 1 2 d S T P . . N1 N 0.3126(15) 0.1874(15) 0.4556(17) 0.12(3) Uani 0.25 2 d S T P . . H1A H 0.3305 0.1695 0.4737 0.149 Uiso 0.25 2 calc RS T P . . H1B H 0.3147 0.1853 0.4245 0.149 Uiso 0.25 2 calc RS T P . . O5S O 0.5000 0.5000 0.5000 0.36(10) Uiso 1 48 d S T P . . O4S O 0.1449(13) 0.2458(14) 0.3551(13) 0.119(16) Uani 0.3333 2 d S T P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Gd1 0.0382(6) 0.0382(6) 0.0382(6) -0.0041(2) 0.0041(2) 0.0041(2) O2 0.041(3) 0.041(3) 0.041(3) 0.002(3) 0.002(3) -0.002(3) O3S 0.081(5) 0.081(5) 0.081(5) -0.017(5) 0.017(5) 0.017(5) O1 0.249(15) 0.249(15) 0.033(5) 0.000(4) 0.000(4) 0.188(17) C1 0.23(3) 0.23(3) 0.034(12) 0.000 0.000 0.17(3) C2 0.19(3) 0.19(3) 0.025(10) 0.000 0.000 0.13(3) C3 0.196(17) 0.196(17) 0.041(9) 0.000(6) 0.000(6) 0.13(2) N1 0.18(4) 0.18(4) 0.02(3) 0.012(17) -0.012(17) 0.10(5) O4S 0.13(2) 0.09(3) 0.13(2) 0.02(2) -0.05(3) -0.02(2) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Gd1 Gd1 3.8290(17) 74 ? Gd1 Gd1 3.8290(17) 28 ? Gd1 O2 2.386(5) . ? Gd1 O2 2.386(5) 28 ? Gd1 O2 2.386(5) 74 ? Gd1 O3S 2.460(17) . ? Gd1 O1 2.273(11) 79 ? Gd1 O1 2.273(11) . ? Gd1 O1 2.273(11) 58 ? Gd1 O4S 2.67(5) 79 ? Gd1 O4S 2.67(5) 58 ? Gd1 O4S 2.67(5) . ? O2 Gd1 2.386(5) 28 ? O2 Gd1 2.386(5) 74 ? O1 C1 1.273(15) . ? C1 O1 1.272(15) 74 ? C1 C2 1.47(3) . ? C2 C3 1.42(2) . ? C2 C3 1.42(2) 74 ? C3 C3 1.34(3) 98_556 ? C3 N1 1.37(6) . ? N1 H1A 0.8700 . ? N1 H1B 0.8700 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Gd1 Gd1 Gd1 60.0 28 74 ? O2 Gd1 Gd1 36.63(16) 74 74 ? O2 Gd1 Gd1 36.63(16) . 28 ? O2 Gd1 Gd1 36.63(16) 28 28 ? O2 Gd1 Gd1 76.8(3) 74 28 ? O2 Gd1 Gd1 76.8(3) 28 74 ? O2 Gd1 Gd1 36.63(16) . 74 ? O2 Gd1 O2 70.1(5) . 28 ? O2 Gd1 O2 70.1(5) . 74 ? O2 Gd1 O2 70.1(5) 28 74 ? O2 Gd1 O3S 138.4(3) 74 . ? O2 Gd1 O3S 138.4(3) . . ? O2 Gd1 O3S 138.4(3) 28 . ? O2 Gd1 O4S 69.7(10) 28 79 ? O2 Gd1 O4S 125.5(7) . 58 ? O2 Gd1 O4S 125.5(7) 74 . ? O2 Gd1 O4S 125.5(7) . 79 ? O2 Gd1 O4S 125.5(7) 28 58 ? O2 Gd1 O4S 125.5(7) 74 79 ? O2 Gd1 O4S 69.7(10) . . ? O2 Gd1 O4S 69.7(10) 74 58 ? O2 Gd1 O4S 125.5(7) 28 . ? O3S Gd1 Gd1 144.735(1) . 74 ? O3S Gd1 Gd1 144.7 . 28 ? O3S Gd1 O4S 68.7(10) . 79 ? O3S Gd1 O4S 68.7(10) . . ? O3S Gd1 O4S 68.7(10) . 58 ? O1 Gd1 Gd1 119.0(3) 79 74 ? O1 Gd1 Gd1 119.0(3) 58 28 ? O1 Gd1 Gd1 69.3(3) . 74 ? O1 Gd1 Gd1 69.3(3) 79 28 ? O1 Gd1 Gd1 119.0(3) . 28 ? O1 Gd1 Gd1 119.0(3) 58 74 ? O1 Gd1 O2 82.3(3) . . ? O1 Gd1 O2 82.3(3) . 74 ? O1 Gd1 O2 146.1(4) 79 74 ? O1 Gd1 O2 82.3(3) 79 . ? O1 Gd1 O2 146.1(5) 58 . ? O1 Gd1 O2 82.3(3) 58 28 ? O1 Gd1 O2 82.3(3) 79 28 ? O1 Gd1 O2 146.1(5) . 28 ? O1 Gd1 O2 82.3(3) 58 74 ? O1 Gd1 O3S 75.5(3) 79 . ? O1 Gd1 O3S 75.5(3) 58 . ? O1 Gd1 O3S 75.5(3) . . ? O1 Gd1 O1 113.9(3) 79 58 ? O1 Gd1 O1 113.9(3) 79 . ? O1 Gd1 O1 113.9(3) 58 . ? O1 Gd1 O4S 57.18(11) 58 58 ? O1 Gd1 O4S 144.2(10) . 79 ? O1 Gd1 O4S 57.18(11) . 58 ? O1 Gd1 O4S 57.18(11) 79 . ? O1 Gd1 O4S 57.18(11) 58 79 ? O1 Gd1 O4S 144.2(10) 79 58 ? O1 Gd1 O4S 57.18(11) 79 79 ? O1 Gd1 O4S 144.2(10) 58 . ? O1 Gd1 O4S 57.18(11) . . ? O4S Gd1 Gd1 91.5(8) . 28 ? O4S Gd1 Gd1 91.5(8) 79 28 ? O4S Gd1 Gd1 146.5(10) 79 74 ? O4S Gd1 Gd1 91.5(8) 58 74 ? O4S Gd1 Gd1 146.5(10) 58 28 ? O4S Gd1 Gd1 91.5(8) . 74 ? O4S Gd1 O4S 107.6(10) . 58 ? O4S Gd1 O4S 107.6(10) . 79 ? O4S Gd1 O4S 107.6(10) 58 79 ? Gd1 O2 Gd1 106.7(3) . 74 ? Gd1 O2 Gd1 106.7(3) 28 74 ? Gd1 O2 Gd1 106.7(3) . 28 ? C1 O1 Gd1 140.0(12) . . ? O1 C1 O1 121(2) 74 . ? O1 C1 C2 119.3(10) . . ? O1 C1 C2 119.3(10) 74 . ? C3 C2 C1 120.9(10) . . ? C3 C2 C1 120.9(10) 74 . ? C3 C2 C3 118(2) . 74 ? C3 C3 C2 120.9(10) 98_556 . ? C3 C3 N1 114(2) 98_556 . ? N1 C3 C2 125(2) . . ? C3 N1 H1A 120.0 . . ? C3 N1 H1B 120.0 . . ? H1A N1 H1B 120.0 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Gd1 O1 C1 O1 0.000(6) . . . 74 ? Gd1 O1 C1 C2 180.000(3) . . . . ? O1 C1 C2 C3 0.000(6) 74 . . . ? O1 C1 C2 C3 180.000(5) . . . . ? O1 C1 C2 C3 180.000(5) 74 . . 74 ? O1 C1 C2 C3 0.000(6) . . . 74 ? C1 C2 C3 C3 180.000(3) . . . 98_556 ? C1 C2 C3 N1 0.000(11) . . . . ? C3 C2 C3 C3 0.000(7) 74 . . 98_556 ? C3 C2 C3 N1 180.000(10) 74 . . . ? _shelx_res_file ; lty2277_0m.res created by SHELXL-2014/7 TITL lty2277_0m_a.res in Fm-3m REM Old TITL LTY2277_0m in Fm-3m #225 REM SHELXT solution in Fm-3m REM R1 0.141, Rweak 0.006, Alpha 0.080, Orientation as input REM Formula found by SHELXT: C56 N O32 Gd8 CELL 1.54178 27.8596 27.8596 27.8596 90 90 90 ZERR 4 0.0032 0.0032 0.0032 0 0 0 LATT 4 SYMM -X,-Y,+Z SYMM -X,+Y,-Z SYMM +X,-Y,-Z SYMM +Z,+X,+Y SYMM +Z,-X,-Y SYMM -Z,-X,+Y SYMM -Z,+X,-Y SYMM +Y,+Z,+X SYMM -Y,+Z,-X SYMM +Y,-Z,-X SYMM -Y,-Z,+X SYMM +Y,+X,-Z SYMM -Y,-X,-Z SYMM +Y,-X,+Z SYMM -Y,+X,+Z SYMM +X,+Z,-Y SYMM -X,+Z,+Y SYMM -X,-Z,-Y SYMM +X,-Z,+Y SYMM +Z,+Y,-X SYMM +Z,-Y,+X SYMM -Z,+Y,+X SYMM -Z,-Y,-X SFAC C H Gd N O UNIT 192 48 32 24 196 L.S. 100 PLAN 10 SIZE 0.1 0.2 0.2 TEMP -33.14 BOND $H LIST 6 MORE -1 CONF fmap 2 acta REM REM REM WGHT 0.151800 373.474884 FVAR 0.05003 GD1 3 0.201409 0.298591 0.298591 10.16667 0.03822 0.03822 = 0.03822 -0.00411 0.00411 0.00411 O2 5 0.215213 0.215213 0.284787 10.16667 0.04075 0.04075 = 0.04075 0.00158 0.00158 -0.00158 O3S 5 0.150431 0.349569 0.349569 10.16667 0.08062 0.08062 = 0.08062 -0.01748 0.01748 0.01748 O1 5 0.221834 0.278166 0.374881 10.50000 0.24918 0.24918 = 0.03329 0.00034 -0.00034 0.18840 C1 1 0.250000 0.250000 0.397232 10.25000 0.22894 0.22894 = 0.03426 0.00000 0.00000 0.16771 C2 1 0.250000 0.250000 0.449876 10.25000 0.19486 0.19486 = 0.02511 0.00000 0.00000 0.12592 C3 1 0.280830 0.219170 0.475986 10.50000 0.19577 0.19577 = 0.04059 -0.00036 0.00036 0.13171 N1 4 0.312562 0.187438 0.455582 10.12500 0.17504 0.17504 = 0.02209 0.01187 -0.01187 0.09681 AFIX 93 H1A 2 0.330528 0.169472 0.473738 10.12500 -1.20000 H1B 2 0.314697 0.185303 0.424500 10.12500 -1.20000 AFIX 0 O5S 5 0.500000 0.500000 0.500000 10.02083 0.35571 O4S 5 0.144935 0.245768 0.355065 10.16667 0.13367 0.08969 = 0.13367 0.01786 -0.04910 -0.01786 HKLF 4 REM lty2277_0m_a.res in Fm-3m REM R1 = 0.0668 for 768 Fo > 4sig(Fo) and 0.0850 for all 991 data REM 43 parameters refined using 0 restraints END WGHT 0.1517 373.4202 REM Highest difference peak 1.202, deepest hole -1.177, 1-sigma level 0.215 Q1 1 0.3719 0.1281 0.4569 10.50000 0.05 0.70 Q2 1 0.1527 0.1527 0.3473 10.16667 0.05 0.67 Q3 1 0.0928 0.2147 0.3978 11.00000 0.05 0.65 Q4 1 0.5000 0.0000 0.5000 10.02083 0.05 0.53 Q5 1 0.1204 0.2459 0.3880 11.00000 0.05 0.44 Q6 1 0.0812 0.2207 0.3932 11.00000 0.05 0.44 Q7 1 0.4011 0.0000 0.5000 10.12500 0.05 0.44 Q8 1 0.3746 0.5000 0.5000 10.12500 0.05 0.42 Q9 1 0.1026 0.3974 0.3974 10.16667 0.05 0.42 Q10 1 0.1593 0.1593 0.4527 10.50000 0.05 0.38 ; _shelx_res_checksum 46220 _shelx_hkl_file ; -1 -1 -1 10.10 0.90 -1 -1 -1 13.10 1.40 1 -1 1 11.80 1.50 1 1 -1 11.40 1.00 1 1 -1 12.20 1.40 1 -1 1 10.80 2.10 1 -1 1 9.70 1.10 -1 1 1 11.70 1.50 -1 1 1 12.30 1.70 1 -1 -1 14.10 1.30 1 -1 -1 13.90 1.50 1 -1 -1 11.30 0.90 -1 1 -1 9.20 0.90 -1 1 -1 8.10 1.70 -1 -1 1 11.10 1.00 -1 -1 1 11.80 1.40 -1 1 -1 8.20 1.30 1 1 1 11.80 1.00 1 1 1 13.40 1.40 -2 0 0 9346.76 445.46 -2 0 0 8979.50 444.86 0 -2 0 9042.20 445.16 0 -2 0 9999.00 445.56 0 2 0 9410.16 445.16 0 2 0 9337.17 445.36 2 0 0 9705.13 445.56 2 0 0 9294.47 444.86 2 0 0 9937.21 445.36 -2 -2 0 4439.96 210.08 -2 0 -2 3966.00 210.08 -2 0 -2 4821.52 210.28 -2 0 2 4483.05 209.98 -2 0 2 4524.95 210.08 -2 0 2 4252.97 209.68 -2 2 0 4331.67 209.68 -2 2 0 4761.62 209.78 0 -2 -2 3861.91 209.78 0 -2 -2 4737.93 210.18 0 -2 2 4442.76 209.88 0 -2 2 4179.68 210.18 0 2 -2 4345.27 209.78 0 2 -2 4541.15 210.18 0 2 2 4188.68 209.88 0 2 2 4794.42 210.18 2 0 -2 4245.48 209.78 2 0 -2 4864.91 210.08 2 0 2 4212.98 210.18 2 0 2 4879.11 210.28 2 2 0 4575.24 210.28 2 2 0 4507.45 209.68 -2 -2 -2 1106.19 58.29 -2 -2 -2 1321.67 58.69 2 -2 2 1333.77 58.59 2 2 -2 1156.68 58.29 2 2 -2 1301.87 58.69 2 -2 2 1346.97 59.19 2 -2 2 1175.68 58.29 -2 2 2 1082.69 58.79 2 -2 -2 1214.38 58.39 2 -2 -2 1199.68 58.49 2 -2 -2 1254.77 58.09 -2 2 -2 1173.98 58.19 -2 -2 2 1249.88 58.29 -2 -2 2 1283.97 58.69 2 2 2 1218.08 58.29 2 2 2 1290.67 58.69 -3 -1 -1 86.99 4.90 -3 -1 -1 101.79 5.50 3 -1 1 101.99 5.30 1 -1 3 81.39 7.90 1 1 -3 91.99 5.40 1 1 -3 93.49 6.40 1 -3 1 83.49 5.30 -3 1 1 101.39 4.90 -3 1 1 101.29 5.20 -3 1 1 90.69 5.00 -1 -3 -1 87.99 4.90 -1 -3 -1 98.89 5.30 3 -1 1 94.29 4.80 -1 3 1 90.89 4.80 -1 3 1 99.19 5.00 -1 -1 -3 80.29 5.30 -1 -1 -3 97.09 6.70 1 3 -1 100.59 5.40 3 -1 1 103.19 5.80 3 1 -1 104.59 5.50 1 3 -1 93.09 5.00 -1 -3 1 99.19 4.90 -1 3 -1 97.29 5.00 -3 -1 1 97.09 5.00 1 -3 -1 82.49 4.90 -3 1 -1 95.09 4.80 1 -1 -3 81.49 5.90 1 -1 -3 80.99 7.10 -3 -1 1 102.19 5.00 -3 -1 1 96.29 5.40 -3 1 -1 89.79 4.80 -3 1 -1 97.59 5.40 1 1 3 88.69 5.40 1 1 3 100.09 6.50 -1 -3 1 100.09 4.90 -1 -3 1 100.09 5.30 1 3 1 94.59 4.90 1 3 1 98.99 4.90 3 -1 -1 97.09 4.90 3 -1 -1 100.59 5.20 3 -1 -1 98.89 4.90 3 -1 -1 100.89 5.60 -1 3 -1 100.29 5.20 -1 -1 3 98.39 5.50 -1 -1 3 85.79 6.10 3 1 1 99.89 5.00 -3 -3 -1 348.27 16.20 3 -1 3 352.86 16.70 3 1 -3 342.57 16.40 1 3 -3 333.47 16.50 -3 -1 -3 295.77 15.80 -3 -1 -3 347.27 16.60 3 3 -1 306.77 15.50 1 3 -3 299.27 15.70 3 -1 3 311.07 15.70 -1 -3 -3 341.07 16.50 -3 1 3 323.87 15.90 -3 1 3 294.57 16.10 -3 1 3 304.07 15.60 3 3 -1 343.47 15.70 -1 3 3 307.87 16.00 -3 3 1 318.07 15.80 -1 -3 -3 283.07 15.70 -1 3 3 349.96 16.70 3 -3 1 344.47 16.10 1 -3 3 290.97 16.20 -1 3 -3 319.87 15.90 -1 -3 3 318.17 15.70 -3 -3 1 335.97 16.10 -3 1 -3 347.57 17.00 1 -3 -3 333.07 15.40 -1 -3 3 301.17 16.30 -3 -1 3 319.57 16.30 -3 -1 3 305.87 15.50 -3 3 -1 332.37 15.60 1 3 3 308.47 15.70 1 3 3 327.97 16.30 -1 3 -3 316.27 17.10 3 -1 -3 314.37 15.80 3 -1 -3 340.87 16.30 3 -1 -3 314.27 15.60 -3 1 -3 276.07 15.70 -3 -3 1 333.27 15.60 3 1 3 315.17 15.70 3 1 3 340.57 16.50 -3 3 -1 313.77 15.60 -3 -1 3 334.27 15.80 3 3 1 334.17 15.60 3 3 1 335.27 15.40 -3 -3 -3 1871.41 85.79 3 3 -3 1836.42 85.69 3 -3 3 1703.83 84.99 3 -3 3 1927.41 86.29 3 -3 3 1898.71 85.59 -3 3 -3 1705.93 84.99 3 -3 -3 1796.02 85.29 3 -3 -3 1790.72 85.39 3 -3 -3 1809.92 84.79 -3 3 -3 1672.93 84.79 -3 -3 3 1842.92 85.09 3 3 3 1716.13 85.09 -4 0 0 1332.47 63.89 0 -4 0 1332.47 63.79 0 -4 0 1473.65 64.09 0 0 -4 1232.08 64.79 0 0 -4 1261.07 65.79 0 0 4 1132.29 64.79 0 4 0 1374.46 63.79 0 4 0 1435.96 63.99 4 0 0 1446.96 63.89 4 0 0 1371.96 63.79 4 0 0 1449.15 64.39 0 4 -2 547.45 25.70 0 4 -2 515.15 25.40 0 4 2 497.15 25.20 0 4 2 561.84 25.60 2 0 -4 528.55 26.70 2 0 4 502.35 25.70 2 0 4 573.84 27.20 4 -2 0 579.04 25.20 4 -2 0 561.14 25.90 4 2 0 529.05 25.30 -2 0 4 471.45 26.40 0 -4 -2 446.36 25.20 0 -4 -2 562.74 25.70 0 -4 2 510.65 25.20 0 -4 2 510.05 25.80 0 4 -2 502.05 25.20 -4 2 0 556.74 25.20 -2 0 -4 482.75 25.90 -2 0 -4 565.54 27.30 -2 0 4 536.65 25.90 -4 2 0 565.74 25.40 -4 2 0 522.25 25.30 -4 2 0 546.55 25.10 -4 2 0 511.65 25.10 4 0 2 561.84 25.80 4 0 2 518.55 25.20 4 0 -2 562.84 25.70 4 0 -2 563.64 25.70 0 2 4 559.54 27.10 2 4 0 511.45 25.20 2 4 0 528.45 25.10 4 0 -2 513.75 25.20 0 -2 -4 512.15 25.10 0 -2 4 515.45 25.90 0 -2 4 459.75 26.90 0 2 -4 488.75 25.80 0 2 -4 526.95 27.10 0 2 4 495.45 25.80 -4 0 -2 464.25 25.10 -4 0 -2 575.74 25.90 -4 0 2 541.95 25.30 -4 0 2 557.14 25.70 -4 0 2 527.55 25.20 -2 -4 0 521.25 25.20 -2 -4 0 561.94 25.60 -2 4 0 554.44 25.30 0 -2 -4 477.25 27.40 -4 -2 -2 98.49 6.30 4 -2 2 97.39 5.80 4 -2 2 105.89 6.80 4 2 -2 104.09 6.30 2 4 -2 89.39 5.20 2 -2 4 86.89 6.50 -4 2 2 95.19 5.20 -4 2 2 97.69 5.60 -4 2 2 95.59 5.40 -2 -4 -2 97.39 6.00 2 4 -2 95.89 6.10 -2 -2 -4 101.09 7.50 2 2 -4 97.99 7.20 2 -2 4 92.29 9.50 -2 4 2 85.09 5.10 4 -2 2 91.29 4.90 -2 2 4 74.59 9.00 -2 4 -2 96.09 6.30 -2 -2 4 86.79 4.90 -2 -4 2 98.89 6.00 2 -2 -4 78.89 6.50 2 -2 -4 99.09 8.40 2 -2 -4 93.69 5.40 -4 2 -2 98.49 5.10 -2 4 -2 95.29 5.30 -2 -2 4 87.79 5.70 2 2 4 85.29 5.60 2 2 4 108.49 7.60 -2 -4 2 94.39 5.10 -4 2 -2 90.09 5.10 2 4 2 92.79 5.20 4 -2 -2 92.59 5.00 4 -2 -2 101.59 5.50 4 -2 -2 102.59 5.20 -4 -2 2 97.89 5.20 -4 2 -2 84.49 4.90 -4 2 -2 103.69 6.50 4 2 2 95.99 5.30 -4 0 -4 508.15 25.70 -4 0 4 506.75 24.60 -4 0 4 468.75 24.20 -4 4 0 501.95 24.40 -4 4 0 511.45 24.30 0 -4 -4 511.85 25.80 0 -4 4 512.15 24.70 0 4 -4 498.05 25.60 0 4 4 482.35 24.50 0 4 4 505.85 25.20 4 0 -4 521.55 25.30 4 0 4 498.65 24.50 4 4 0 512.75 24.30 4 4 0 488.15 24.10 -4 -4 -2 8.70 2.50 2 -4 4 15.80 5.10 -4 -2 -4 10.00 3.10 4 -2 4 7.30 1.70 4 2 -4 12.40 2.90 4 -4 2 9.50 2.00 -4 2 4 8.70 2.60 -4 2 4 7.00 2.70 -4 2 4 9.60 2.20 2 4 -4 11.30 2.80 2 -4 4 6.20 3.30 -2 4 4 8.30 3.40 -4 4 2 6.50 2.30 -2 -4 -4 13.10 3.00 -2 4 4 3.80 2.50 4 4 -2 11.60 2.60 2 -4 4 11.40 2.70 4 -4 2 9.00 2.60 -2 -4 4 7.30 1.90 -4 4 -2 12.80 1.90 2 -4 -4 7.40 4.20 2 -4 -4 12.60 1.70 -4 4 -2 12.70 2.00 -2 4 -4 6.30 2.30 -4 2 -4 11.10 4.20 -4 4 -2 0.30 4.10 2 4 4 8.80 1.80 4 -4 -2 9.00 1.20 -2 4 -4 9.30 4.30 -2 4 -4 8.90 1.90 4 -2 -4 13.00 2.70 4 -2 -4 9.10 2.10 -4 -2 4 8.60 1.90 -4 -2 4 10.20 1.60 4 2 4 9.80 1.90 -4 -4 2 9.20 1.70 4 4 2 9.30 1.70 -4 -4 -4 -0.30 2.80 4 4 -4 1.30 2.70 4 -4 4 -0.60 1.60 4 -4 4 -1.80 3.60 4 -4 4 0.30 3.00 -4 4 4 8.00 3.60 -4 4 -4 -1.50 1.90 -4 4 -4 0.20 1.70 4 -4 -4 3.20 2.40 4 -4 -4 0.20 1.70 -4 -4 4 -3.20 1.30 -4 4 -4 -0.60 2.60 -4 4 -4 -2.30 5.10 -4 -4 4 0.50 1.80 4 4 4 0.00 1.70 -5 -1 -1 14.80 2.70 5 1 -1 11.30 1.90 -1 -1 -5 12.80 6.30 5 -1 1 11.50 1.60 5 -1 1 14.20 3.20 -5 1 1 16.10 2.10 -5 1 1 15.20 2.20 -5 1 1 16.10 3.00 -5 1 1 13.60 2.20 -1 -5 -1 15.10 2.00 -1 -5 -1 19.10 3.30 -1 1 5 16.30 4.70 -1 5 1 9.10 1.60 1 -1 5 8.00 4.20 1 1 -5 14.10 5.30 -1 5 1 17.20 2.20 1 5 -1 13.80 2.10 -1 -5 1 20.00 2.10 -1 5 -1 13.70 2.20 -5 -1 1 14.60 2.30 -1 -1 5 7.70 3.70 1 -5 -1 11.60 1.50 -5 -1 1 13.80 2.70 1 -1 -5 3.90 5.80 -1 -5 1 12.70 2.30 -5 1 -1 9.80 1.50 1 1 5 10.40 3.30 -1 1 -5 3.00 6.40 1 5 1 18.70 2.20 1 5 1 22.60 2.70 5 -1 -1 14.40 3.10 -5 1 -1 13.00 2.60 -5 1 -1 9.80 2.10 -1 -5 1 19.50 2.00 5 1 1 11.10 1.80 5 -3 1 586.64 27.60 5 3 -1 578.64 26.90 -3 -1 -5 574.54 28.70 5 -3 1 609.44 26.50 1 -5 3 553.44 26.90 1 -5 3 501.15 27.90 1 5 -3 577.14 27.50 1 5 -3 550.54 26.90 -5 3 1 548.45 26.50 -5 3 1 555.74 26.60 -5 3 1 546.75 26.90 3 -1 5 545.05 27.30 3 1 -5 589.24 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9.50 8.10 11 13 13 9.70 5.20 11 -13 -13 -25.10 28.20 -13 13 -11 10.50 6.60 13 13 11 12.90 5.50 13 13 -13 75.89 16.20 -13 13 13 113.59 15.00 13 13 -13 73.39 22.00 13 13 -13 89.09 9.90 -13 13 -13 78.79 15.40 13 -13 -13 58.19 31.30 13 13 13 109.29 14.70 13 13 13 110.19 12.60 13 13 13 107.49 15.20 13 13 13 76.59 17.20 -14 0 0 986.20 49.50 -14 0 0 937.51 51.19 -14 0 0 998.20 49.60 0 0 -14 1078.99 56.09 0 0 14 1090.09 51.59 0 14 0 1030.00 49.80 2 0 -14 593.64 35.40 2 0 14 589.34 29.30 -2 0 14 565.34 29.40 0 14 -2 529.25 27.50 0 14 -2 426.86 29.50 0 14 2 463.65 29.30 -2 0 -14 616.74 35.10 -14 2 0 511.75 28.50 -14 2 0 544.45 27.30 -14 -2 0 530.05 27.00 -14 2 0 511.75 26.50 -14 -2 0 525.65 26.90 -14 -2 0 496.15 29.10 4 0 -14 50.99 12.70 4 0 14 77.79 10.40 0 14 4 54.19 9.70 0 14 4 60.49 6.60 0 14 -4 50.79 9.80 -14 4 0 63.59 7.30 -4 0 -14 61.09 12.50 -4 0 14 65.49 9.00 0 14 -4 61.79 6.90 -14 -4 0 54.89 7.80 -14 -4 0 59.79 6.00 -14 -4 0 58.59 6.90 6 0 14 116.49 12.00 0 14 -6 104.89 10.80 6 0 14 104.89 10.00 -6 0 -14 155.98 21.40 0 14 -6 108.69 12.50 0 14 6 117.09 7.80 0 14 6 96.99 11.80 0 14 6 110.69 11.00 -14 -6 0 104.19 8.90 -14 -6 0 97.59 13.10 -14 6 0 121.99 11.90 6 0 -14 91.09 15.30 -6 0 14 71.19 10.70 -8 0 -14 145.99 23.00 -14 8 0 192.58 16.70 8 0 14 221.98 16.00 14 -8 0 193.18 13.00 0 14 -8 213.58 11.90 0 14 -8 206.68 15.10 0 14 -8 248.48 20.50 0 14 8 220.08 12.40 0 14 8 220.98 20.20 -14 -8 0 207.58 13.40 -14 -8 0 200.68 17.60 8 0 14 210.78 14.30 0 14 8 224.98 15.30 8 0 -14 169.78 23.30 0 14 10 420.76 22.40 10 0 -14 377.16 31.80 10 0 14 431.46 23.90 0 14 10 433.06 24.20 0 14 -10 498.25 29.30 10 0 14 455.75 25.40 0 14 10 471.25 28.50 14 -10 0 376.36 28.30 0 14 -10 417.66 25.20 -14 -10 0 427.76 23.40 -14 -10 0 377.16 27.10 14 -10 0 406.36 22.60 0 -14 -10 427.16 22.00 0 14 12 375.96 25.70 12 0 -14 272.47 34.70 12 0 -14 301.47 44.40 14 -12 0 321.67 20.10 14 -12 0 284.17 26.90 0 14 12 346.67 21.90 0 14 -12 324.97 34.00 12 0 14 380.66 20.90 12 0 14 369.16 22.50 0 14 12 349.77 19.80 0 14 -12 432.26 27.30 -14 12 0 342.67 18.70 0 14 -12 368.46 23.80 0 2 14 576.54 29.50 -2 14 0 547.35 27.80 0 2 -14 572.04 35.30 -14 0 -2 513.85 27.10 -2 -14 0 532.95 28.60 -14 0 2 481.95 29.00 -14 0 2 535.25 27.60 -2 -14 0 550.44 26.90 -14 0 2 528.85 27.30 14 0 2 527.95 27.20 -14 0 -2 499.15 29.60 2 14 0 550.94 27.60 -14 0 -2 556.34 27.70 0 -2 -14 579.94 35.10 0 -2 14 572.04 29.70 -2 14 2 242.98 21.20 2 2 -14 316.97 26.20 2 14 -2 315.37 17.40 2 14 -2 284.37 21.80 -14 -2 -2 295.57 17.10 -2 -2 -14 326.37 25.90 -14 2 2 301.47 16.60 -14 2 2 277.27 18.30 -14 2 2 309.47 17.40 -2 2 14 344.67 19.50 -14 -2 -2 290.77 19.60 -2 -14 -2 322.37 16.20 2 -2 14 346.17 19.30 -14 -2 -2 290.07 16.60 2 2 -14 297.07 18.40 -2 14 -2 311.17 17.70 -14 -2 2 273.17 19.20 2 -2 -14 341.57 25.90 -14 -2 2 316.07 17.00 -14 2 -2 289.47 16.20 -2 -2 14 324.17 20.20 -14 2 -2 317.87 17.60 14 2 2 308.87 16.70 2 2 14 351.86 19.60 2 14 2 288.57 15.90 -2 2 -14 327.77 25.90 -2 -14 2 316.37 17.00 2 14 2 282.47 19.40 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14 -6 102.59 7.40 2 14 6 97.39 7.80 2 14 6 117.39 7.60 -14 6 -2 105.49 9.40 -2 14 -6 82.29 11.90 8 -2 14 171.98 14.00 -2 14 8 153.38 12.70 14 -8 2 138.09 12.60 2 -14 8 165.58 14.60 8 -2 14 151.38 12.50 2 14 -8 151.28 13.40 2 14 -8 184.48 19.20 8 2 -14 168.58 14.40 2 14 -8 139.89 15.00 -14 -8 -2 150.08 11.40 -14 -8 -2 147.39 15.90 8 2 -14 125.99 22.60 -8 2 14 147.39 16.10 -2 14 8 163.28 19.10 -2 14 8 167.58 10.10 2 14 8 148.49 10.80 8 2 14 168.68 14.60 8 2 14 160.58 11.80 2 14 8 176.38 10.30 -2 14 -8 156.68 9.70 -2 14 -8 149.29 13.50 -2 14 -8 179.88 19.90 2 14 8 191.98 13.90 -14 8 -2 170.38 15.70 2 14 8 170.18 18.10 -14 -8 2 147.99 11.50 -8 2 -14 190.68 23.90 8 -2 -14 115.39 16.80 2 -14 -8 149.88 10.00 14 8 2 168.58 11.40 -14 -8 2 159.28 11.60 -14 -8 2 137.49 15.90 10 -2 14 302.97 18.60 2 14 -10 223.78 21.20 2 14 -10 265.17 18.80 -2 14 10 273.47 15.50 10 -2 14 290.97 17.50 14 -10 2 241.88 16.30 -10 2 14 202.78 20.20 14 -10 2 248.58 22.10 10 2 -14 235.08 26.40 -14 -10 -2 251.77 16.30 -14 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18.20 7.40 -4 14 8 23.90 5.80 -8 -4 -14 9.30 12.40 8 4 -14 -2.20 11.70 4 14 -8 18.90 7.00 8 4 -14 10.80 7.60 -4 14 8 27.30 4.00 -4 14 8 20.10 10.50 -4 -14 8 17.40 6.10 14 8 4 21.30 5.10 8 4 14 18.70 7.30 4 14 8 13.30 4.80 4 14 8 20.90 9.90 -4 14 -8 30.40 4.10 -8 4 -14 36.10 8.30 4 14 8 18.20 7.40 4 -14 -8 17.20 4.70 4 14 8 30.00 4.00 -8 -4 14 8.00 7.20 -8 4 -14 21.00 12.20 -14 -8 4 20.50 5.30 -14 -8 4 19.80 5.50 -14 8 -4 25.70 8.30 8 -4 -14 5.20 11.40 8 4 14 20.00 4.90 -4 14 -8 13.10 7.40 -4 14 10 89.09 8.60 4 14 -10 86.59 10.80 10 -4 14 94.49 9.80 -10 4 14 110.49 14.50 4 14 -10 101.29 13.60 14 -10 4 109.79 18.20 10 4 -14 61.59 24.40 -4 14 10 98.59 13.40 4 14 -10 66.19 11.50 -4 14 10 108.79 8.80 10 -4 14 116.09 15.90 4 14 10 98.09 10.60 4 14 10 79.39 10.10 10 4 14 99.39 9.80 -4 14 -10 91.89 10.80 14 -10 -4 117.39 10.90 10 4 14 105.39 13.30 -10 -4 14 116.89 14.30 -10 4 -14 98.09 16.10 -14 -10 4 101.19 10.50 14 -10 -4 56.39 16.10 4 -14 -10 94.19 8.00 14 10 4 101.69 10.10 4 14 10 107.99 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918.61 51.09 3 7 -15 988.80 59.59 -15 -3 7 1014.60 51.39 3 7 15 1009.40 52.99 3 7 15 1114.69 52.39 15 3 7 1035.90 51.19 3 7 15 1002.10 51.59 -15 -3 7 1043.40 50.59 3 7 15 956.40 50.79 7 15 3 1062.49 53.19 3 -7 -15 1053.19 57.29 -7 -15 3 1052.79 50.99 -15 3 -7 1001.30 64.79 -7 15 -3 1024.30 51.39 -7 15 -3 1114.19 50.39 -3 7 -15 1106.49 59.49 7 15 3 987.10 50.59 -15 3 -7 1161.88 51.79 -7 15 5 1591.44 77.59 5 -7 15 1791.02 79.69 5 7 -15 1619.64 79.69 5 -7 15 1432.86 79.29 -5 7 15 1712.23 79.79 5 7 -15 1513.65 86.39 7 15 -5 1524.65 77.89 7 -15 5 1626.34 80.09 7 15 -5 1663.83 81.29 -15 -5 -7 1432.86 81.69 -7 -15 -5 1544.85 81.09 -5 7 15 1457.15 78.29 -5 7 15 1523.95 79.19 7 15 5 1561.54 78.09 -5 7 -15 1778.32 85.79 7 -15 -5 1627.64 77.09 -7 -15 5 1673.53 78.49 -7 15 -5 1679.63 77.79 5 7 15 1576.94 78.99 -15 -5 7 1600.04 78.69 5 7 15 1624.24 80.39 -5 7 -15 1774.42 80.69 -15 5 -7 1807.12 78.89 -15 -5 7 1644.64 77.59 7 15 5 1602.74 77.39 -7 15 -5 1558.64 78.69 7 15 5 1625.94 79.89 15 5 7 1564.44 78.49 7 15 -7 1063.79 56.79 -7 -15 -7 1113.59 60.89 7 -15 7 1145.89 59.39 7 7 -15 1120.89 58.69 -7 15 7 1170.48 56.09 7 -7 15 1027.50 57.99 7 15 -7 1192.18 60.39 -7 7 15 1214.38 58.29 -7 7 -15 1312.97 59.79 -7 15 -7 1198.98 56.29 -7 7 -15 1185.18 64.29 -7 -15 7 1159.78 57.39 7 -15 -7 1127.69 55.59 -7 15 -7 1113.49 57.49 -15 -7 7 1115.79 55.99 7 7 15 1126.89 57.49 7 15 7 1110.59 56.79 7 15 7 1173.28 58.59 15 7 7 1188.18 58.89 7 15 7 1132.69 55.99 -7 15 9 230.18 16.30 7 15 -9 178.58 25.60 7 -15 9 219.38 21.10 -7 15 9 237.78 24.60 9 -7 15 171.78 15.70 -7 15 9 227.98 13.30 7 15 -9 193.38 16.20 7 15 -9 204.48 22.20 9 7 -15 189.88 19.80 15 9 -7 277.17 34.20 7 15 9 218.48 19.50 7 -15 -9 227.48 14.50 9 -7 -15 179.08 32.60 -15 -9 7 190.08 14.30 7 15 9 216.38 13.30 -7 -15 9 198.98 16.80 -7 15 -9 220.68 17.70 -7 15 -9 254.27 28.90 -9 7 -15 285.77 20.70 7 15 9 148.89 23.10 9 7 15 198.38 14.60 11 7 -15 32.90 26.50 7 15 -11 30.20 12.70 7 15 -11 52.19 10.10 11 -7 15 45.80 8.00 11 7 -15 47.40 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9 13 74.59 16.50 9 -13 -15 35.00 35.40 -13 15 -9 96.79 13.50 15 9 13 104.09 13.90 15 9 13 82.99 10.90 9 13 15 89.79 9.90 15 -9 -13 107.79 30.70 9 13 15 110.69 27.30 9 13 15 56.79 19.50 9 13 15 59.99 10.90 -13 15 -9 93.79 14.90 13 15 9 75.99 15.80 -9 13 -15 90.79 15.60 9 13 15 81.59 10.80 15 11 -13 17.10 7.80 -11 13 15 33.00 11.20 15 -11 13 11.70 7.70 15 11 -13 12.70 28.80 15 11 -13 9.20 20.50 11 13 -15 -1.60 14.80 -13 15 11 8.40 10.70 -13 15 11 13.00 9.20 13 15 -11 0.90 19.10 11 13 -15 15.20 7.70 -11 13 15 -2.80 14.50 13 15 -11 -1.10 14.70 11 13 -15 19.80 19.30 -13 15 -11 12.90 12.30 15 11 13 33.60 8.00 11 13 15 21.20 6.60 11 13 15 20.50 7.80 11 13 15 24.80 8.80 11 13 15 4.80 15.40 11 -13 -15 -27.10 31.60 -11 13 -15 10.20 12.30 13 15 11 5.50 14.20 15 -11 -13 54.39 31.30 15 11 13 21.90 8.80 15 11 13 -1.80 14.80 -15 11 -13 21.00 11.90 -13 15 -11 23.10 7.50 15 13 -13 183.58 27.50 13 13 -15 180.88 26.70 -13 13 15 140.99 20.70 15 13 -13 213.78 16.50 -13 15 13 256.27 22.60 -13 15 13 172.68 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41.00 22 4 0 103.09 14.10 -22 -4 0 75.19 12.40 -22 4 0 101.39 14.60 0 22 -4 105.59 10.40 0 22 -4 109.99 14.20 0 22 4 118.19 11.20 0 22 4 167.58 23.30 0 22 4 126.09 16.20 0 22 4 99.89 13.40 0 22 4 64.19 13.20 4 0 -22 87.99 25.60 4 0 22 114.39 11.30 22 4 0 121.39 15.00 22 4 0 119.29 16.50 22 4 0 85.79 12.90 0 22 6 59.49 12.40 6 0 -22 39.80 25.10 6 0 22 61.99 8.00 22 6 0 54.19 9.10 22 6 0 65.19 11.40 22 6 0 65.79 12.30 22 6 0 59.09 13.30 0 22 -6 48.50 12.70 0 22 -6 91.49 15.50 0 22 6 64.29 7.90 0 22 6 90.19 15.50 0 22 6 79.69 17.10 -22 -6 0 55.39 11.10 0 22 6 27.20 13.90 0 22 -6 52.49 6.90 -22 6 0 84.19 14.00 22 8 0 430.76 31.60 22 8 0 419.46 29.60 22 8 0 446.96 28.30 8 0 -22 478.55 53.99 0 22 -8 439.76 31.20 0 22 -8 445.56 34.00 0 22 8 434.06 25.10 0 22 8 426.86 32.60 8 0 22 455.05 25.40 22 8 0 399.66 25.60 0 22 8 376.76 33.20 0 22 8 463.85 29.90 0 22 8 420.96 35.80 0 22 -10 695.53 45.60 0 22 -10 634.64 41.50 0 22 10 651.83 45.10 22 10 0 647.24 35.60 22 10 0 682.73 39.10 10 0 22 693.13 35.70 10 0 -22 716.63 63.59 22 10 0 666.83 37.70 22 10 0 634.74 40.90 0 22 10 676.93 42.10 0 22 10 658.23 39.30 0 22 10 595.04 43.10 0 22 10 640.84 35.60 22 12 0 460.25 29.70 0 22 12 486.35 33.00 22 12 0 527.05 32.60 0 22 -12 480.15 35.30 0 22 -12 491.05 44.20 22 12 0 462.15 34.10 12 0 -22 603.44 63.59 12 0 22 472.85 27.30 0 22 12 497.05 28.60 0 22 12 493.05 35.10 0 22 -12 462.45 27.40 0 22 12 472.85 30.10 0 22 12 474.95 37.80 0 22 12 481.15 39.10 14 0 22 125.79 12.40 14 0 -22 70.29 37.90 0 22 14 103.59 14.90 0 22 14 94.89 17.30 0 22 14 101.49 20.90 0 22 -14 97.29 16.70 0 22 14 92.59 11.20 0 22 14 93.29 15.20 22 14 0 97.79 14.80 22 14 0 89.99 16.40 0 22 -14 60.29 26.20 22 14 0 99.09 12.20 0 22 -16 22.30 13.70 0 -22 -16 34.50 32.70 22 16 0 31.30 15.10 0 22 16 28.20 8.80 0 22 16 21.50 13.40 16 0 -22 -35.90 38.90 16 0 22 30.40 6.60 22 16 0 15.40 9.00 0 22 16 31.00 19.20 22 16 0 5.30 12.90 0 22 -16 -27.30 25.70 0 22 16 20.10 14.60 0 22 16 6.70 7.80 0 22 -18 196.68 30.20 18 0 -22 153.68 40.60 0 22 -18 221.98 25.10 18 0 22 229.58 15.40 0 22 18 223.48 18.30 0 22 18 162.08 17.70 22 18 0 214.98 22.80 0 22 18 282.27 28.30 22 18 0 189.68 18.30 0 22 18 248.88 22.30 22 18 0 271.57 28.30 0 -22 -18 220.08 37.10 0 22 20 319.97 21.10 22 20 0 316.77 25.10 0 -22 20 357.36 35.80 20 0 -22 280.47 55.49 20 0 -22 305.37 23.70 0 22 20 365.96 29.20 22 20 0 279.27 21.00 0 22 -20 300.67 27.00 0 22 -20 327.27 39.40 0 -22 -20 328.57 47.20 0 22 20 295.17 20.60 22 20 0 399.36 31.30 0 -2 22 745.43 42.80 -22 0 -2 747.13 41.50 -22 0 2 749.82 40.70 -2 22 0 741.73 43.70 2 22 0 778.82 38.40 2 22 0 746.93 42.90 0 2 22 754.22 38.60 -2 22 0 749.53 42.00 0 -2 22 725.93 38.40 22 0 -2 729.73 41.70 22 0 -2 721.23 41.60 22 0 -2 775.42 57.79 22 0 2 688.73 41.00 -2 22 0 781.02 38.60 0 -2 -22 745.13 58.29 22 0 2 776.22 41.70 22 0 2 680.23 49.30 22 0 -2 689.53 40.60 -2 22 0 782.82 40.80 2 22 0 882.61 44.20 -22 -2 -2 452.45 29.50 -2 22 2 502.25 30.20 22 2 -2 509.65 47.00 2 22 -2 466.45 25.40 -2 -2 -22 443.56 47.20 22 2 -2 473.45 29.70 -2 22 2 491.35 32.90 22 2 -2 451.75 30.20 -2 22 2 443.96 29.40 -22 2 2 452.85 29.10 2 -2 22 475.65 25.90 22 2 -2 427.86 27.70 -2 22 2 497.45 26.00 -2 2 22 487.95 25.60 2 22 -2 427.76 30.70 2 -2 22 406.66 34.60 -2 22 -2 484.55 32.30 2 22 2 495.65 25.70 2 2 22 486.25 25.90 -2 -2 22 476.65 25.60 22 2 2 430.66 27.90 22 2 2 489.15 29.30 22 2 2 407.66 29.60 -22 -2 2 414.96 28.40 -22 2 -2 511.25 30.50 2 -2 -22 480.05 49.20 -2 22 -2 478.75 25.60 2 22 2 474.55 32.50 22 -2 -2 450.55 30.60 -2 22 -2 526.95 31.90 -2 -2 22 466.25 32.10 2 22 2 535.15 32.20 -2 22 4 76.99 12.20 -2 22 4 60.99 13.20 2 22 -4 78.29 7.60 -2 22 4 84.69 16.20 4 -2 22 74.39 8.30 2 22 -4 80.19 12.80 22 4 -2 79.99 13.60 22 4 -2 77.79 12.20 -22 -4 -2 61.49 11.80 22 4 -2 67.09 12.30 -2 22 4 64.59 7.90 -2 22 4 112.59 15.90 4 2 -22 57.29 28.40 -22 4 2 78.59 12.70 22 4 -2 67.79 9.80 22 4 -2 107.49 22.80 22 4 2 65.39 13.60 -2 22 -4 72.49 13.10 2 22 4 72.89 13.60 4 -2 -22 56.99 25.30 2 22 4 85.59 8.20 22 4 2 67.99 9.90 4 2 22 72.19 8.20 22 -4 -2 72.39 13.70 -2 22 -4 79.59 14.20 22 4 2 62.89 12.40 -4 -2 22 66.49 13.10 -22 4 -2 65.69 13.70 -22 -4 2 55.99 11.40 2 22 4 108.69 16.00 -2 22 -4 69.29 7.60 22 4 2 78.29 11.40 22 6 -2 65.29 13.10 22 6 -2 33.90 11.70 22 6 -2 41.10 8.60 -2 22 6 25.90 13.70 2 22 -6 48.90 12.10 6 -2 22 39.20 7.20 -22 -6 -2 41.80 11.50 -2 22 6 37.60 7.00 -2 22 6 63.79 14.30 -2 22 6 57.99 16.90 -2 22 6 31.50 11.40 22 6 -2 31.90 10.20 2 22 -6 39.00 6.10 6 2 -22 43.80 26.30 6 -2 -22 19.40 24.40 2 22 6 69.69 14.70 6 2 22 41.50 7.10 22 6 2 37.60 12.20 2 22 6 44.40 12.80 -22 -6 2 39.40 10.90 22 6 2 48.60 10.30 -22 6 -2 49.30 14.10 -2 22 -6 43.20 6.60 -2 22 -6 40.60 12.30 2 22 6 12.40 14.00 22 6 2 47.10 8.80 -6 -2 22 34.50 12.30 2 22 6 49.00 7.00 22 6 2 52.99 13.30 -2 22 8 364.46 21.50 22 8 -2 332.67 26.40 -2 22 8 274.77 29.70 22 8 -2 315.57 22.50 22 8 -2 323.97 27.90 8 2 -22 390.96 52.59 -2 22 8 371.96 29.00 -2 22 8 290.57 32.60 22 8 -2 329.27 25.00 -2 22 8 331.97 26.00 2 22 -8 381.96 29.40 2 22 -8 339.87 27.90 8 -2 22 353.56 21.40 -2 22 -8 340.67 27.90 22 8 2 340.17 26.90 8 -2 -22 333.47 49.99 2 22 8 363.56 29.70 2 22 8 343.17 21.10 -2 22 -8 366.16 33.60 2 22 8 310.77 27.70 22 8 2 319.57 22.10 22 8 2 362.76 24.40 8 2 22 353.76 21.20 22 8 2 313.27 28.30 2 22 8 308.47 30.00 2 22 -10 537.45 40.90 22 10 -2 538.65 30.80 2 22 -10 532.35 36.20 -2 22 10 572.24 30.50 -2 22 10 441.36 31.90 22 10 -2 510.35 33.00 22 10 -2 535.95 35.80 -2 22 10 548.55 34.00 -2 22 10 490.75 39.40 22 10 -2 563.64 33.90 -2 22 10 534.55 40.90 10 -2 22 554.44 30.20 -2 22 10 544.65 37.30 10 2 -22 650.23 62.69 22 10 2 538.15 34.70 2 22 10 520.75 30.20 22 10 2 535.45 32.10 2 22 10 574.74 38.30 10 -2 -22 573.24 60.29 22 10 2 541.55 30.20 -2 22 -10 583.34 43.20 22 10 2 522.55 36.20 2 22 10 523.55 35.10 10 2 22 563.04 30.10 2 22 10 585.94 37.50 -2 22 -10 542.75 29.90 -2 22 -10 486.55 36.10 -2 22 12 389.46 34.70 2 22 -12 352.36 30.90 22 12 -2 390.36 30.80 -2 22 12 386.16 24.40 12 -2 22 396.46 23.40 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22 -18 68.59 29.00 22 18 2 102.49 15.90 2 -22 -18 105.79 34.40 18 2 22 113.39 11.70 2 22 18 97.19 11.90 -2 22 20 229.38 25.60 20 2 -22 195.98 18.50 2 -22 20 159.48 23.20 -2 22 20 156.18 14.70 -2 -22 -20 133.29 32.30 20 2 -22 145.59 36.80 20 -2 22 191.48 13.20 22 20 -2 139.59 16.60 2 22 -20 202.58 35.40 -2 22 20 219.48 17.00 22 20 -2 225.98 27.20 22 20 -2 181.98 20.30 2 22 20 119.09 18.40 20 2 22 161.78 19.70 2 22 20 212.58 24.90 22 20 2 225.68 28.20 -2 22 -20 227.98 23.90 2 22 20 198.88 16.40 22 20 2 177.68 17.20 20 -2 -22 133.79 36.90 -2 -22 20 210.58 31.00 2 22 20 168.88 15.40 -2 22 -20 171.88 28.90 22 20 2 188.08 15.80 2 -22 -20 151.08 32.80 0 -4 22 107.89 14.70 22 0 -4 99.99 11.90 -4 22 0 121.09 14.70 -4 22 0 116.69 11.40 22 0 4 113.79 12.80 -4 22 0 109.89 13.80 -4 22 0 154.58 19.30 0 -4 22 110.19 10.90 22 0 -4 92.59 13.00 22 0 -4 125.79 14.30 -22 0 -4 103.29 14.30 0 4 22 101.39 10.60 4 22 0 108.59 10.10 22 0 4 116.19 17.30 0 -4 -22 81.39 26.10 -22 0 4 108.49 13.00 22 2 -4 80.09 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8.40 -8 22 14 55.39 15.30 8 22 -14 43.90 18.50 8 22 -14 28.40 23.80 -8 22 14 38.60 14.00 -8 22 14 53.69 18.20 -8 22 14 18.70 23.20 14 8 22 47.90 12.10 14 8 22 55.49 8.20 14 8 22 41.00 9.80 8 22 14 54.39 8.70 8 22 14 52.89 10.90 14 -8 -22 11.10 36.00 22 14 8 46.30 18.30 22 14 8 54.29 11.00 14 8 22 79.19 19.30 8 22 14 61.69 15.90 -8 22 -14 32.10 15.90 -8 22 16 28.80 13.50 16 -8 22 4.90 5.80 16 8 -22 3.00 9.80 -8 22 16 0.80 6.80 -8 22 16 -7.70 13.50 8 22 -16 16.20 23.60 -8 22 16 5.70 12.70 22 16 -8 -6.30 13.00 16 8 -22 -15.40 32.00 -8 22 16 3.30 22.40 22 16 -8 -12.70 22.80 -8 22 16 15.50 16.20 22 16 -8 2.10 15.80 16 8 22 4.80 5.80 22 16 8 15.40 17.80 8 22 16 5.00 13.10 16 8 22 41.90 18.70 16 8 22 1.40 10.40 16 -8 -22 -24.00 38.00 8 22 16 6.80 9.00 8 22 16 -4.50 6.50 22 16 8 5.80 9.20 -8 22 -16 -7.10 14.10 -8 22 18 51.49 15.20 18 8 -22 110.89 15.50 8 22 -18 72.59 23.00 22 18 -8 74.59 23.40 -8 22 18 57.89 8.70 -8 22 18 98.79 22.90 8 -22 18 83.69 11.30 18 -8 22 92.19 8.70 22 18 -8 84.09 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455.55 54.59 -10 22 2 555.24 39.80 -10 22 2 537.05 33.40 22 2 -10 565.54 35.90 22 2 -10 564.94 36.10 22 2 -10 554.84 33.70 2 10 -22 540.15 33.10 2 -10 22 588.24 41.10 -10 22 2 526.45 30.10 2 -10 22 521.45 30.10 -2 10 22 575.24 30.70 22 2 -10 586.14 60.29 -2 10 22 576.74 40.10 -10 22 2 538.65 36.40 22 2 10 504.75 33.60 2 10 22 599.44 31.00 -2 -10 22 608.84 42.60 22 -2 -10 530.15 37.60 22 -2 -10 602.84 59.49 -10 22 -2 562.64 32.00 2 10 22 499.25 31.20 2 -10 -22 525.45 59.29 2 10 22 584.94 39.20 -10 22 -2 521.85 30.10 -10 22 -2 538.35 36.20 22 2 10 583.24 50.69 22 2 10 530.25 33.70 -10 22 4 120.39 16.60 22 4 -10 116.29 16.70 -10 22 4 87.89 20.30 -10 22 4 116.69 12.90 22 4 -10 110.89 13.50 -10 22 4 97.59 14.40 -10 22 4 123.89 26.90 4 -10 22 94.69 10.40 22 4 -10 76.99 43.90 4 -10 22 111.69 18.70 22 4 -10 110.09 15.80 22 4 -10 105.99 32.90 -4 10 22 120.29 12.40 -4 10 22 115.29 18.90 4 10 -22 105.79 12.80 22 4 10 93.09 19.60 4 10 22 99.59 10.50 4 -10 -22 89.09 33.30 -10 22 -4 108.89 16.30 4 10 22 123.89 18.80 22 4 10 115.89 13.50 -10 22 -4 116.99 14.50 4 10 22 95.59 11.50 22 4 10 113.19 13.80 -4 -10 22 120.49 19.00 -10 22 -4 113.59 12.90 22 6 -10 43.90 32.40 22 6 -10 19.40 10.20 6 10 -22 17.80 9.40 -10 22 6 24.10 12.50 6 -10 22 29.90 7.80 -10 22 6 44.90 21.10 -10 22 6 26.30 7.10 -6 10 22 29.50 15.30 6 -10 22 24.80 15.90 22 6 -10 32.50 13.80 -6 10 22 25.00 6.50 22 6 -10 24.40 24.80 -10 22 6 40.80 13.30 -10 22 6 21.50 19.40 -10 22 6 16.50 12.10 10 22 -6 42.10 20.30 6 10 22 26.30 8.80 -10 22 -6 24.60 13.30 22 6 10 28.30 10.50 -10 22 -6 25.80 8.30 22 6 10 5.50 17.10 22 6 10 28.10 9.80 6 10 22 42.60 15.60 6 10 22 23.60 7.30 -6 -10 22 35.90 16.00 10 22 6 1.50 14.70 6 -10 -22 2.00 33.20 8 -10 22 358.16 32.50 8 -10 22 393.86 24.20 22 8 -10 338.27 41.50 -10 22 8 384.46 31.10 8 10 -22 373.66 25.20 8 10 -22 341.07 41.20 22 8 -10 381.76 29.60 22 8 -10 338.27 58.49 -8 10 22 374.46 32.70 -10 22 8 386.16 27.60 10 22 -8 426.46 38.30 22 8 -10 390.56 26.10 -10 22 8 381.16 38.60 8 10 -22 360.56 41.60 -10 22 8 493.05 39.60 -10 22 8 372.96 31.10 -10 22 8 359.76 23.40 -10 22 -8 355.96 31.40 -10 22 -8 363.76 24.30 22 8 10 373.66 27.10 8 10 22 335.37 24.60 8 -10 -22 392.76 61.19 22 8 10 394.76 35.70 -8 -10 22 385.46 34.00 22 8 10 371.96 25.10 8 10 22 393.46 34.80 8 10 22 404.86 23.80 8 10 22 375.76 32.50 10 22 -10 606.14 42.50 22 10 -10 612.44 47.90 -10 22 10 548.35 34.60 22 10 -10 562.34 32.50 10 -10 22 529.65 36.80 22 10 -10 548.65 35.90 10 -10 22 544.35 31.80 -10 22 10 520.35 31.50 -10 22 10 545.25 39.30 -10 22 10 549.15 38.20 10 10 -22 560.94 32.30 10 10 -22 514.45 45.70 -10 22 10 568.04 45.90 22 10 -10 462.05 66.49 -10 22 -10 588.84 40.80 10 -10 -22 591.74 64.59 10 10 22 503.75 32.30 22 10 10 609.74 32.10 10 10 22 571.14 40.60 -10 -10 22 607.04 40.80 -10 22 -10 558.24 32.50 22 10 10 550.34 41.50 10 10 22 582.54 39.40 10 10 22 558.04 33.30 22 10 10 565.04 34.40 10 10 22 585.94 31.60 -10 22 12 370.16 31.30 22 12 -10 278.37 29.10 22 12 -10 306.17 26.80 -10 22 12 274.17 25.80 10 22 -12 329.67 33.40 12 10 -22 342.07 23.00 22 12 -10 313.77 40.40 -10 22 12 382.26 34.60 10 22 -12 313.87 36.90 12 -10 22 310.27 21.10 -10 22 12 300.87 21.20 -10 22 12 275.97 28.60 -10 22 12 299.87 40.30 12 10 -22 312.27 39.30 -10 22 -12 301.97 21.90 12 10 22 334.37 24.10 12 10 22 257.57 21.60 12 10 22 301.77 30.70 12 10 22 355.56 34.30 12 10 22 337.77 20.90 22 12 10 287.77 33.40 22 12 10 306.67 23.90 -12 -10 22 295.57 31.70 -10 22 -12 312.97 31.90 12 -10 -22 333.47 63.39 -10 22 14 34.10 18.00 14 10 -22 56.79 11.00 22 14 -10 42.30 19.30 -10 22 14 46.80 13.80 22 14 -10 40.80 13.80 10 22 -14 43.30 23.20 -10 22 14 41.50 24.60 14 -10 22 61.49 8.50 22 14 -10 31.00 24.70 14 10 -22 45.10 23.30 -10 22 14 77.49 15.80 -10 22 14 34.90 8.60 -10 22 14 47.30 15.60 14 10 22 51.89 8.10 10 22 14 49.50 8.10 14 10 22 62.19 19.30 22 14 10 44.30 19.50 22 14 10 49.20 11.30 -10 22 -14 49.20 16.10 10 22 14 48.90 10.60 14 -10 -22 42.30 37.00 -14 -10 22 35.10 17.30 14 10 22 48.40 9.60 14 10 22 46.40 11.20 -10 22 16 -2.70 13.70 -10 22 16 7.80 12.20 -10 22 16 11.00 16.00 16 10 -22 2.20 22.00 22 16 -10 -20.40 23.90 16 -10 22 18.80 6.40 22 16 -10 10.90 16.70 22 16 -10 18.30 20.10 16 10 -22 18.10 9.50 -10 22 16 50.09 13.60 -10 22 16 0.80 23.40 10 22 -16 25.00 22.10 -10 22 16 2.90 6.80 10 22 16 5.80 9.10 16 10 22 25.30 18.20 16 10 22 16.40 6.00 16 10 22 2.70 9.60 16 10 22 4.70 7.80 22 16 10 2.40 18.40 10 22 16 11.00 6.60 16 -10 -22 -30.60 37.70 22 16 10 20.30 10.00 -10 22 -16 7.10 14.50 18 10 -22 173.98 14.40 22 18 -10 126.59 23.90 10 22 -18 150.68 23.60 22 18 -10 97.69 20.10 -10 22 18 151.78 24.90 -10 22 18 82.79 16.30 18 -10 22 145.99 11.80 10 -22 18 118.29 12.90 18 10 -22 96.19 36.40 18 10 -22 103.49 23.80 -10 22 18 130.89 12.40 18 10 22 112.19 14.40 18 -10 -22 127.39 41.90 10 22 18 103.39 12.10 22 18 10 141.29 20.80 18 10 22 154.58 19.90 -10 22 -18 133.29 17.50 10 22 18 129.79 15.90 22 18 10 139.69 16.30 -10 22 20 150.68 21.10 20 10 -22 175.98 30.50 -10 22 20 250.27 27.90 10 -22 20 185.18 27.60 10 -22 20 209.78 20.50 22 20 -10 203.78 23.00 10 22 -20 250.57 27.40 20 10 -22 171.88 31.40 20 10 22 266.67 26.20 20 10 22 202.68 15.00 -10 22 -20 275.37 24.00 22 20 10 231.98 24.30 22 20 10 280.67 28.80 10 22 20 216.18 17.10 20 -10 -22 172.38 35.60 22 20 10 204.58 17.60 0 12 22 482.55 29.60 0 12 22 524.55 39.30 22 0 -12 534.85 64.09 -12 22 0 467.55 39.30 22 0 12 519.25 37.40 -12 22 0 467.45 28.20 0 12 22 524.35 28.90 -12 22 0 469.45 35.00 0 -12 -22 503.95 57.39 22 0 -12 511.75 33.10 0 -12 22 533.65 41.10 -12 22 0 504.85 30.90 -2 12 22 407.26 35.00 -2 12 22 392.96 23.90 -12 22 2 383.16 23.50 2 -12 22 370.26 23.30 -2 -12 -22 348.07 52.09 22 2 -12 388.46 27.50 2 -12 22 401.36 38.00 22 2 -12 396.46 29.30 2 12 -22 358.76 45.80 -12 22 2 382.66 36.10 -12 22 2 381.56 27.20 -2 12 22 379.06 24.70 -12 22 2 368.56 30.10 -2 12 22 383.26 27.50 22 2 -12 370.86 60.29 22 2 -12 442.06 32.60 -2 -12 22 421.66 37.10 -12 22 -2 410.26 26.10 -12 22 -2 359.06 31.50 2 12 22 380.46 25.10 22 2 12 381.46 36.40 22 -2 -12 438.86 61.39 2 12 22 406.76 24.10 -12 22 -2 375.26 23.50 2 12 22 402.76 35.10 2 -12 -22 410.46 57.09 2 12 22 353.06 43.80 22 2 12 371.66 28.40 -4 12 22 68.59 13.30 -12 22 4 72.59 21.30 -12 22 4 72.59 8.90 22 4 -12 22.30 34.20 4 12 -22 65.49 23.70 -4 12 22 69.49 17.50 22 4 -12 74.39 14.80 4 -12 22 67.89 9.00 22 4 -12 83.19 16.40 -12 22 4 63.99 14.20 4 12 -22 78.39 12.10 22 4 -12 78.89 12.60 -4 12 22 72.69 8.80 4 -12 22 54.09 17.80 -12 22 4 65.49 13.10 4 12 22 62.59 10.30 -12 22 -4 76.49 10.80 4 12 22 68.49 20.40 4 12 22 75.69 10.10 4 -12 -22 58.09 33.70 22 4 12 61.89 19.30 -12 22 -4 68.09 15.00 -4 -12 22 85.19 18.70 22 4 12 64.49 12.10 22 -4 -12 136.89 36.50 4 12 22 64.89 18.30 22 4 12 69.99 12.50 -12 22 6 27.70 21.00 -12 22 6 12.40 6.80 -12 22 6 6.20 11.40 6 -12 22 14.90 16.30 22 6 -12 14.50 14.70 -6 12 22 17.90 6.30 -12 22 6 61.69 22.60 22 6 -12 -19.60 34.60 -6 12 22 11.20 15.20 22 6 -12 17.60 24.60 6 12 -22 8.00 21.50 -12 22 6 47.10 13.70 6 -12 22 28.40 7.60 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167.48 20.10 -12 -12 22 146.59 19.80 12 22 12 173.48 18.20 12 -12 -22 127.19 38.90 12 12 22 153.38 18.60 22 12 12 148.49 18.60 22 12 12 132.09 22.20 12 12 22 120.49 16.30 12 12 22 174.08 15.00 -12 22 14 16.40 13.70 12 22 -14 34.40 21.50 14 12 -22 40.70 22.20 14 12 -22 38.90 9.20 14 -12 22 30.40 7.30 -12 22 14 8.20 7.30 -12 22 14 46.00 13.20 22 14 -12 23.50 14.50 -12 22 14 32.00 12.90 -12 22 14 53.29 25.30 22 14 -12 6.50 19.80 22 14 -12 13.80 25.10 -12 22 14 38.20 18.00 14 12 22 24.20 8.60 14 12 22 52.89 18.70 14 12 22 15.30 9.40 -14 -12 22 5.40 16.30 12 22 14 28.10 10.10 -12 22 -14 24.50 14.90 14 12 22 20.80 6.70 14 -12 -22 -3.20 35.80 22 14 12 25.00 10.50 22 14 12 24.60 18.80 12 22 -16 18.50 21.20 -12 22 16 -1.50 17.80 -12 22 16 23.30 23.70 12 -22 16 2.70 8.50 -22 16 12 -27.80 19.70 -12 22 16 -11.60 12.40 16 12 -22 20.10 21.30 -12 22 16 44.40 11.50 16 12 -22 17.80 8.10 16 -12 22 14.50 6.00 22 16 -12 -12.80 22.60 22 16 -12 -1.80 18.20 16 12 22 31.10 17.50 -12 22 -16 18.00 14.30 22 16 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2 -20 86.69 38.90 -2 -20 -22 144.89 32.80 2 -20 22 177.78 29.30 -2 20 22 125.59 18.00 22 2 20 183.68 21.00 2 20 22 206.18 26.30 20 22 2 173.88 20.80 2 20 22 189.78 16.30 20 22 2 177.58 16.70 22 2 20 148.59 20.40 -2 -20 22 217.68 30.60 2 20 22 179.28 15.10 -2 20 -22 162.98 27.60 2 -20 -22 228.38 46.80 2 20 22 160.58 19.60 -4 20 22 25.10 18.10 -20 22 4 9.30 11.50 20 22 -4 27.20 15.70 -4 20 22 11.70 6.10 -4 20 22 51.39 12.80 -4 20 22 -8.60 11.90 4 -20 22 -16.60 15.60 -4 -20 -22 -11.70 29.10 4 20 -22 29.30 21.10 4 -20 22 19.70 9.30 22 4 -20 36.40 10.40 -4 -20 22 21.80 16.90 20 22 4 -10.70 12.70 20 22 4 30.80 16.70 4 20 22 30.30 17.00 4 -20 -22 29.70 30.80 22 4 20 33.70 17.40 4 20 22 18.10 8.40 -4 20 -22 -7.70 23.90 4 20 22 1.60 13.90 4 20 22 10.00 6.70 -4 20 -22 33.60 13.10 22 4 20 0.70 10.70 -6 20 22 -7.70 11.50 -6 -20 -22 -24.60 28.00 6 -20 22 19.10 6.60 6 -20 22 2.50 15.10 -20 22 6 -12.10 11.30 6 20 -22 27.30 20.70 22 6 -20 42.80 9.90 -6 20 22 10.30 5.60 -6 20 22 39.90 11.90 20 22 -6 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377.06 30.70 23 7 5 363.06 25.50 23 9 -5 104.39 16.50 23 9 -5 100.49 12.00 9 5 -23 143.69 51.69 -5 23 9 96.49 10.60 5 23 -9 97.59 21.70 23 9 -5 102.49 15.30 9 -5 23 98.69 10.40 -5 23 9 59.39 11.60 -5 23 9 132.79 17.90 -5 23 9 110.69 20.50 -5 23 9 96.79 14.20 -5 23 9 65.79 19.90 5 23 -9 138.29 23.90 9 5 -23 90.69 12.60 23 9 -5 91.39 14.90 5 23 9 127.39 13.00 23 9 5 102.69 11.50 23 9 5 93.69 16.30 -5 23 -9 83.89 16.40 9 5 23 101.79 10.20 -9 -5 23 96.89 15.80 -5 23 -9 112.89 13.30 5 23 9 95.89 16.20 9 -5 -23 92.39 32.20 23 9 5 97.19 12.80 23 9 5 86.09 16.90 5 23 9 135.19 17.90 23 11 -5 2.10 13.20 23 11 -5 -1.90 13.70 5 23 -11 -8.80 17.80 11 5 -23 5.60 10.10 -5 23 11 12.30 7.30 11 5 -23 -6.20 33.60 23 11 -5 -10.50 10.50 23 11 -5 3.00 8.30 -5 23 11 4.00 17.70 11 -5 23 10.00 6.40 -5 23 11 25.90 13.90 -5 23 11 -4.20 8.40 -5 23 11 -23.50 19.00 -5 23 11 -9.50 12.50 11 5 23 11.60 10.60 -5 23 -11 5.20 6.70 23 11 5 -1.70 9.20 23 11 5 10.20 15.00 5 23 11 2.90 6.30 11 5 23 -1.60 5.90 11 -5 -23 9.50 32.70 5 23 11 28.30 14.60 5 23 11 3.40 13.90 -5 23 -11 -1.80 13.70 5 23 11 -4.40 15.20 23 11 5 -27.90 14.30 23 11 5 3.00 8.20 13 -5 23 120.09 12.80 13 5 -23 91.99 37.80 23 13 -5 111.09 17.40 -5 23 13 96.49 19.30 13 5 -23 110.09 13.30 -5 23 13 101.19 13.20 23 13 -5 90.49 15.20 -5 23 13 69.59 21.90 5 23 -13 78.09 23.10 -5 23 13 93.39 16.40 -5 23 13 92.09 15.20 23 13 -5 74.79 13.70 -5 23 13 93.89 11.30 -5 23 -13 99.59 13.90 5 23 13 131.69 16.40 5 23 13 92.69 10.60 23 13 5 99.19 18.30 13 5 23 105.89 14.40 5 23 13 76.09 19.20 13 5 23 115.09 12.50 5 23 13 166.78 24.70 23 13 5 99.69 12.40 23 13 5 115.09 17.40 13 5 23 141.59 20.70 13 -5 -23 64.89 35.60 5 23 13 106.39 15.10 -5 23 -13 89.89 17.10 -5 23 -13 62.69 28.00 13 5 23 113.69 16.10 5 23 -15 172.48 27.30 15 5 -23 204.78 38.50 -5 23 15 176.68 25.70 23 15 -5 254.77 28.30 15 5 -23 228.38 20.40 15 -5 23 228.38 15.90 23 15 -5 190.08 21.40 -5 23 15 266.37 22.20 23 15 -5 249.88 24.20 -5 23 15 188.48 17.30 -5 23 15 208.48 31.70 -5 23 15 249.88 27.70 -5 23 15 193.18 19.00 5 23 15 235.68 26.40 15 -5 -23 227.28 41.90 23 15 5 207.98 19.20 -5 23 -15 190.48 27.40 23 15 5 262.37 29.80 15 5 23 249.28 16.20 15 5 23 220.38 21.70 5 23 15 207.98 17.50 23 15 5 264.87 27.80 5 23 15 255.07 22.30 5 23 15 211.78 19.00 -5 23 -15 131.49 33.30 5 23 15 210.68 28.60 15 5 23 284.57 30.60 5 -23 17 165.48 17.20 -5 23 17 232.58 31.00 23 17 -5 162.28 18.80 17 -5 23 181.98 13.10 17 5 -23 129.49 35.40 17 5 -23 201.48 18.30 -5 23 17 143.89 16.00 5 23 -17 130.69 25.50 -5 23 17 126.29 14.40 23 17 -5 171.58 16.70 23 17 -5 190.88 32.80 -5 23 17 162.38 18.60 23 17 -5 212.08 26.50 17 5 23 263.27 29.00 5 23 17 110.59 18.00 5 23 17 183.88 16.60 17 5 23 180.18 13.30 17 -5 -23 157.28 42.50 17 5 23 138.59 18.90 23 17 5 163.98 16.70 23 17 5 176.98 18.90 -5 23 -17 75.79 31.60 5 23 17 119.49 14.60 5 23 17 176.18 26.80 -5 23 -17 157.88 19.90 23 17 5 178.68 21.70 19 5 -23 75.29 10.80 -5 23 19 36.40 7.40 23 19 -5 65.79 17.10 19 -5 23 71.09 7.20 -5 23 19 29.70 11.80 -5 23 19 90.19 19.20 23 19 -5 63.29 21.80 5 -23 19 55.79 8.90 5 23 -19 64.09 22.20 23 19 -5 46.50 12.80 -5 -23 -19 10.20 27.60 -5 23 19 19.80 13.60 23 19 -5 52.59 10.80 19 5 -23 2.20 30.90 23 19 5 43.70 9.50 19 5 23 44.40 10.60 23 19 5 44.80 15.20 5 23 19 45.80 9.20 23 19 5 69.79 17.30 5 23 19 20.20 13.40 5 23 19 29.20 7.60 19 -5 -23 30.00 36.80 -5 23 -19 60.99 14.20 21 5 -23 -27.30 28.90 -5 -23 -21 -26.80 24.10 -5 23 21 18.50 10.50 -5 23 21 -18.10 11.20 -5 23 21 19.50 15.50 5 -23 21 -14.10 15.20 23 21 -5 -5.00 15.40 21 5 -23 16.00 8.00 23 21 -5 -4.30 8.40 5 23 -21 -5.10 19.10 -5 -23 21 -0.20 14.10 -5 23 -21 7.80 12.30 21 -5 -23 -28.80 30.10 5 23 21 -25.40 11.10 23 21 5 -4.40 7.30 21 5 23 -15.70 7.90 23 21 5 21.50 15.40 5 23 21 -1.00 6.90 23 21 5 -33.20 12.60 -7 23 1 5.40 15.10 1 -7 23 20.20 5.90 -1 7 23 10.50 5.50 -7 23 1 17.50 11.60 -7 23 1 13.10 6.20 -1 7 23 30.70 13.80 23 1 -7 16.60 11.20 1 -7 23 23.60 13.80 -1 -7 -23 16.90 27.20 -7 23 1 11.00 8.50 23 1 -7 81.89 33.40 23 1 -7 24.80 10.80 23 1 -7 -9.60 12.80 -7 23 -1 17.80 7.90 1 7 23 17.50 6.10 23 1 7 17.00 10.10 1 7 23 21.20 13.70 -7 23 -1 15.20 16.00 -7 23 -1 12.70 6.10 -7 23 -1 26.70 11.90 23 -1 -7 10.10 13.40 1 -7 -23 13.50 27.50 -1 -7 23 21.00 13.90 23 1 7 16.30 9.90 -3 7 23 207.28 15.00 23 3 -7 183.68 20.00 23 3 -7 204.48 22.70 -7 23 3 206.98 19.90 -7 23 3 209.88 26.80 3 7 -23 165.48 19.60 -3 7 23 256.67 26.80 -3 -7 -23 156.88 30.70 -7 23 3 178.38 17.50 23 3 -7 318.07 52.39 3 -7 23 222.08 26.70 -7 23 3 209.18 15.90 3 -7 23 205.68 15.80 -7 23 3 199.18 25.10 23 3 -7 182.68 18.40 3 7 23 214.68 15.70 23 3 7 200.58 19.00 23 3 7 187.88 24.20 3 -7 -23 176.18 32.90 -7 23 -3 198.58 15.30 -7 23 -3 225.78 24.60 23 -3 -7 202.68 19.30 -7 23 -3 208.68 17.10 23 3 7 210.28 20.90 -3 -7 23 196.68 27.40 3 7 23 240.88 26.30 23 3 7 207.28 19.80 -7 23 5 388.46 33.20 5 -7 23 386.46 23.10 23 5 -7 380.26 32.40 23 5 -7 356.36 26.00 -7 23 5 395.16 27.80 23 5 -7 381.86 29.60 5 -7 23 376.66 30.00 5 7 -23 324.57 25.50 -7 23 5 367.56 23.00 23 5 -7 437.66 55.29 23 5 -7 372.46 28.70 -7 23 5 384.56 29.90 -7 23 5 368.26 35.40 -5 7 23 382.86 31.50 -7 23 5 404.16 27.90 -5 7 23 368.16 25.40 -7 23 -5 368.56 22.60 5 7 23 399.36 23.00 5 -7 -23 361.36 56.19 -7 23 -5 372.06 30.50 -5 -7 23 384.06 31.90 -7 23 -5 367.26 23.80 5 7 23 397.56 31.00 7 23 5 437.36 33.10 23 5 7 384.76 30.00 23 5 7 380.66 27.10 23 5 7 361.46 33.70 7 23 5 358.16 26.30 23 5 7 346.07 25.10 7 23 -7 299.77 35.50 -7 23 7 322.47 34.10 23 7 -7 283.97 31.10 23 7 -7 335.67 52.19 -7 23 7 315.67 21.00 -7 23 7 353.66 29.20 23 7 -7 325.17 27.60 -7 23 7 295.97 25.60 23 7 -7 333.87 27.70 7 -7 23 329.67 21.10 -7 23 7 310.67 27.20 23 7 -7 300.07 23.20 7 -7 23 290.77 26.00 7 7 -23 276.67 23.30 -7 23 7 293.27 32.80 -7 7 23 312.37 29.60 23 7 7 342.27 25.00 23 7 7 333.17 28.70 -7 -7 23 342.17 31.10 23 7 7 321.07 32.10 7 -7 -23 335.07 53.79 -7 23 -7 320.07 28.80 7 7 23 320.77 20.80 -7 23 -7 334.07 21.40 7 23 7 302.07 20.10 7 23 7 304.07 30.30 7 7 23 354.36 29.20 23 7 7 315.37 22.80 23 9 -7 86.59 15.40 23 9 -7 79.19 14.90 9 -7 23 100.69 10.70 9 7 -23 80.19 12.10 -7 23 9 82.69 10.10 -7 23 9 70.09 13.80 -7 23 9 83.59 20.40 23 9 -7 75.99 17.30 -7 23 9 69.99 21.30 7 23 -9 79.89 20.80 23 9 -7 86.69 11.80 -7 23 9 65.69 15.00 -7 23 9 114.89 16.90 23 9 7 85.79 17.00 23 9 7 89.19 13.00 -7 23 -9 100.29 13.50 9 7 23 95.99 9.90 -9 -7 23 94.29 16.10 7 23 9 87.69 16.30 23 9 7 73.99 17.80 7 23 9 89.69 9.70 -7 23 -9 91.39 17.20 9 7 23 97.79 15.80 23 9 7 89.79 11.50 9 -7 -23 68.19 32.60 -7 23 11 -7.20 12.80 -7 23 11 -21.00 20.70 -7 23 11 -9.30 18.10 23 11 -7 17.10 13.50 7 23 -11 -17.00 17.70 -7 23 11 3.90 12.90 11 7 -23 9.30 9.90 -7 23 11 25.70 14.30 7 23 -11 -27.20 18.00 -7 23 11 12.00 7.10 23 11 -7 -0.30 15.30 11 -7 23 10.60 6.60 23 11 -7 -1.20 8.20 23 11 7 -1.10 8.40 -11 -7 23 -4.40 14.20 7 23 11 34.20 17.00 23 11 7 -4.60 15.60 23 11 7 -8.40 16.00 11 7 23 3.80 16.70 -7 23 -11 2.80 7.20 11 7 23 2.10 5.80 7 23 11 8.80 13.50 11 7 23 11.40 10.40 11 -7 -23 -4.50 33.60 23 11 7 -5.20 9.60 7 23 11 6.60 6.40 11 7 23 10.10 13.50 -7 23 -11 -7.60 14.10 7 23 -13 67.19 22.70 13 7 -23 120.39 17.20 23 13 -7 86.79 17.50 -7 23 13 68.49 10.20 -7 23 13 127.29 18.20 13 7 -23 88.69 34.40 -7 23 13 99.19 19.10 23 13 -7 90.79 15.10 -7 23 13 91.09 17.10 -7 23 13 64.59 23.10 13 -7 23 87.19 9.70 7 23 -13 81.89 20.10 -7 23 13 86.79 15.30 13 7 23 90.49 13.50 7 23 13 124.99 16.50 13 -7 -23 61.69 35.90 7 23 13 107.99 17.30 13 7 23 105.39 16.80 -7 23 -13 61.49 17.10 7 23 13 102.39 14.20 13 7 23 95.69 9.70 23 13 7 75.89 18.00 13 7 23 96.79 19.80 23 13 7 100.59 19.90 7 23 13 86.49 10.10 23 13 7 89.79 12.50 -7 23 -13 75.39 10.50 23 15 -7 140.09 16.80 15 -7 23 169.48 13.70 23 15 -7 148.89 19.70 -7 23 15 159.28 19.80 -7 23 15 129.29 16.60 23 15 -7 209.38 33.90 -7 23 15 136.69 19.30 15 7 -23 195.58 18.50 15 7 -23 135.09 34.60 -7 23 15 123.29 14.90 -7 23 15 148.69 24.90 7 23 -15 157.58 25.40 15 7 23 196.48 22.30 23 15 7 172.18 17.90 -7 23 -15 152.38 20.10 7 23 15 187.88 25.10 23 15 7 134.59 19.80 7 23 15 154.88 14.70 23 15 7 154.78 21.80 15 7 23 164.28 19.20 15 7 23 161.18 13.80 7 23 15 157.48 17.50 15 -7 -23 128.49 39.70 17 -7 23 118.99 11.30 -7 23 17 83.49 10.20 -7 23 17 116.79 16.70 23 17 -7 94.69 14.80 -7 23 17 116.89 14.00 7 -23 17 98.29 12.30 -7 23 17 51.39 16.30 7 23 -17 91.49 23.10 23 17 -7 103.09 24.20 23 17 -7 106.39 14.30 23 17 -7 120.99 18.80 17 7 -23 54.49 32.20 -7 23 17 140.39 23.40 17 7 -23 159.58 16.40 7 23 17 84.99 16.30 7 23 17 114.09 15.30 17 -7 -23 80.89 40.10 23 17 7 110.19 20.00 23 17 7 110.09 15.60 17 7 23 113.29 11.00 17 7 23 109.09 12.90 23 17 7 108.09 18.10 -7 23 -17 113.69 18.00 7 23 17 82.39 10.40 17 7 23 141.89 20.60 -7 23 19 18.60 6.40 -7 23 19 -3.90 13.30 19 7 -23 54.89 9.40 7 -23 19 39.00 8.30 7 23 -19 25.50 20.20 23 19 -7 34.70 17.00 23 19 -7 39.90 21.00 19 -7 23 36.20 5.80 -7 23 19 63.69 19.50 19 7 -23 -1.20 30.20 23 19 -7 46.80 11.20 19 7 23 24.80 9.10 23 19 7 62.29 17.50 7 23 19 41.70 8.80 23 19 7 10.30 15.10 19 -7 -23 -17.60 35.80 -7 23 -19 48.20 14.00 23 19 7 35.20 9.20 7 23 19 7.20 12.80 7 23 19 24.80 6.90 23 21 -7 1.00 8.90 -7 23 21 20.00 9.20 -7 23 21 23.00 15.50 21 7 -23 11.30 6.90 21 7 -23 -40.20 26.70 23 21 -7 -20.20 15.40 7 -23 21 -0.30 14.70 7 23 -21 -16.10 17.40 -7 -23 -21 -24.60 23.80 7 23 21 -26.00 10.70 21 7 23 -6.90 6.90 21 -7 -23 -3.50 29.20 -7 -23 21 2.60 13.00 23 21 7 -27.50 13.20 7 23 21 3.30 7.10 23 21 7 25.90 15.90 23 21 7 -2.60 7.60 -7 23 -21 4.90 12.10 -9 23 1 1.80 5.90 -1 9 23 2.20 5.70 1 9 -23 -16.20 10.00 23 1 -9 3.50 10.30 -9 23 1 11.80 16.90 -9 23 1 3.30 8.30 -1 -9 -23 -13.20 28.00 1 -9 23 8.50 15.20 23 1 -9 -11.20 13.80 -1 9 23 -3.60 14.00 23 1 -9 52.09 32.70 1 -9 23 -0.60 5.40 -9 23 1 0.80 11.20 23 1 -9 -4.80 11.30 1 9 23 4.70 5.80 -9 23 -1 0.70 17.40 -9 23 -1 0.90 5.80 -9 23 -1 3.60 7.70 -9 23 -1 0.40 11.40 1 9 23 -0.20 13.90 -1 -9 23 6.40 15.00 23 -1 -9 64.09 33.10 1 -9 -23 -31.60 28.90 23 -1 -9 -12.60 14.20 23 1 9 3.20 9.80 23 3 -9 55.99 13.80 -9 23 3 54.79 13.20 -9 23 3 41.40 13.30 -3 9 23 46.00 7.40 -3 -9 -23 29.00 27.60 23 3 -9 34.40 14.40 -3 9 23 54.39 15.70 23 3 -9 96.99 34.10 3 -9 23 52.69 7.80 3 -9 23 53.39 15.70 23 3 -9 52.19 11.60 -9 23 3 44.40 7.70 -9 23 3 45.10 18.30 3 9 -23 47.00 11.10 -9 23 3 33.50 10.60 -3 -9 23 62.49 16.30 -9 23 -3 44.70 13.80 3 -9 -23 34.30 30.80 23 3 9 40.10 18.00 -9 23 -3 50.89 9.30 23 3 9 62.39 11.20 -9 23 -3 57.19 8.10 3 9 23 49.70 8.20 23 3 9 47.30 11.20 3 9 23 61.99 16.10 5 -9 23 94.49 16.30 -9 23 5 98.79 10.20 -9 23 5 119.99 16.40 5 -9 23 116.19 13.00 23 5 -9 88.59 13.10 -9 23 5 103.89 14.40 -5 9 23 94.29 17.80 -9 23 5 93.39 14.70 23 5 -9 83.09 15.50 23 5 -9 104.99 16.40 -9 23 5 90.09 22.90 -9 23 5 99.69 20.50 23 5 -9 109.49 33.70 5 9 -23 90.69 12.10 23 5 -9 83.49 19.40 -5 9 23 108.29 11.70 5 9 23 118.79 18.00 9 23 5 92.09 19.40 5 9 23 96.79 10.10 23 5 9 123.79 17.70 23 5 9 106.19 16.40 -9 23 -5 114.69 14.30 -5 -9 23 105.89 17.20 5 9 23 82.89 11.50 23 5 9 97.69 19.20 23 5 9 100.29 13.20 -9 23 -5 99.69 16.40 5 -9 -23 102.29 34.20 9 23 -7 97.29 21.80 -9 23 7 105.49 16.20 -9 23 7 89.69 10.10 7 9 -23 77.39 11.80 7 -9 23 87.89 9.90 -9 23 7 84.79 15.40 -9 23 7 58.99 21.20 -9 23 7 107.29 22.10 23 7 -9 91.09 12.60 23 7 -9 76.39 19.30 -7 9 23 96.99 17.40 23 7 -9 81.09 15.30 23 7 -9 102.19 33.90 7 -9 23 75.59 14.80 23 7 -9 87.69 15.90 -9 23 7 97.49 14.30 23 7 9 92.49 13.20 7 9 23 108.39 17.50 23 7 9 93.59 17.30 7 9 23 83.39 10.70 23 7 9 121.19 17.10 -9 23 -7 91.09 11.10 -7 -9 23 78.59 17.10 7 -9 -23 67.59 34.10 -9 23 -7 94.49 16.90 9 23 7 77.99 16.60 23 7 9 98.99 19.00 7 9 23 100.79 10.60 23 9 -9 4.90 17.30 23 9 -9 17.20 9.80 -9 23 9 37.40 13.10 9 -9 23 24.10 7.40 -9 23 9 25.60 20.00 23 9 -9 21.10 24.10 -9 23 9 28.40 7.70 23 9 -9 14.30 32.00 -9 23 9 10.20 13.70 -9 23 9 35.10 13.90 -9 23 9 12.50 21.50 9 23 -9 22.60 19.30 23 9 -9 19.10 13.80 9 -9 23 5.90 12.00 9 9 -23 26.40 10.00 -9 23 -9 30.50 15.30 9 9 23 37.20 9.90 23 9 9 1.00 17.20 23 9 9 11.90 10.60 9 9 23 21.40 8.40 9 -9 -23 33.60 32.40 -9 -9 23 26.80 15.00 23 9 9 26.40 9.90 9 9 23 23.10 7.40 9 23 9 29.60 14.40 23 9 9 5.80 16.40 -9 23 -9 23.90 8.30 9 9 23 25.90 14.60 -9 23 11 18.10 13.80 23 11 -9 6.70 7.70 -9 23 11 8.70 18.80 9 23 -11 -12.60 18.10 -9 23 11 -20.90 12.80 -9 23 11 -3.20 22.20 23 11 -9 -13.00 16.80 11 -9 23 6.50 6.40 -9 23 11 -14.10 13.50 23 11 -9 18.20 13.90 11 9 -23 4.80 9.60 23 11 -9 16.80 23.40 -9 23 11 0.60 6.90 11 9 23 -8.50 13.90 -11 -9 23 10.50 14.90 -9 23 -11 -6.90 14.70 11 -9 -23 1.50 34.20 23 11 9 -7.70 16.30 23 11 9 -2.20 8.80 11 9 23 -5.40 7.80 11 9 23 12.00 6.60 -9 23 -11 -1.10 7.50 23 11 9 -3.50 10.00 9 23 11 6.80 6.40 23 11 9 -5.60 17.20 11 9 23 27.90 17.40 11 9 23 6.00 10.10 13 -9 23 30.90 7.10 9 23 -13 -5.80 20.90 -9 23 13 29.60 14.30 -9 23 13 14.80 14.10 -9 23 13 25.50 17.70 -9 23 13 3.00 13.60 -9 23 13 28.40 23.40 13 9 -23 39.70 10.50 -9 23 13 13.90 7.70 23 13 -9 4.50 16.70 23 13 -9 6.90 13.60 23 13 -9 23.50 23.10 13 9 23 11.90 14.60 23 13 9 22.00 10.50 9 23 13 24.30 7.20 13 9 23 44.50 18.10 13 -9 -23 -13.30 34.00 9 23 13 36.10 10.10 13 9 23 29.40 11.10 -9 23 -13 18.50 15.30 13 9 23 16.60 6.70 23 13 9 44.80 18.60 -9 23 15 43.60 16.80 23 15 -9 24.40 13.50 15 -9 23 51.59 7.60 -9 23 15 33.30 23.50 23 15 -9 51.69 24.00 -9 23 15 31.50 13.20 -9 23 15 78.89 15.20 9 23 -15 32.40 22.00 15 9 -23 50.99 10.60 23 15 -9 30.80 17.10 -9 23 15 30.50 14.70 -9 23 15 18.10 7.70 23 15 9 45.20 10.80 23 15 9 17.40 17.70 -9 23 -15 50.49 15.40 15 9 23 51.59 7.30 9 23 15 47.70 8.20 9 23 15 37.10 10.00 15 9 23 72.19 18.60 15 9 23 36.40 10.60 15 -9 -23 19.30 36.00 23 15 9 45.20 18.80 -9 23 17 14.70 6.70 17 9 -23 36.80 9.40 -9 23 17 36.00 22.60 9 -23 17 29.00 9.30 17 9 -23 14.80 37.00 23 17 -9 9.20 22.70 23 17 -9 32.80 15.20 23 17 -9 40.00 17.40 17 -9 23 29.50 6.10 -9 23 17 -14.10 13.20 9 23 -17 23.30 20.80 -9 23 17 66.09 13.30 -9 23 17 47.50 12.00 23 17 9 55.89 18.50 23 17 9 9.50 16.70 17 -9 -23 8.70 37.60 17 9 23 22.60 8.90 17 9 23 74.09 18.10 9 23 17 15.60 6.60 23 17 9 27.70 9.90 17 9 23 31.20 6.10 9 23 17 33.30 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23 3 155.28 14.50 -3 15 23 146.49 13.70 -3 15 23 137.09 20.00 3 -15 23 154.78 13.40 -15 23 3 152.08 19.90 3 15 -23 144.99 26.70 15 23 -3 149.19 21.30 -15 23 -3 135.09 18.90 23 3 15 167.48 21.70 3 15 23 139.69 15.80 3 15 23 151.68 14.40 -15 23 -3 133.69 16.90 3 15 23 152.58 21.60 23 3 15 137.39 21.70 3 -15 -23 139.29 35.20 3 15 23 137.29 21.50 -15 23 -3 137.19 25.10 23 -3 -15 82.49 40.70 -3 -15 23 144.19 20.80 5 -15 23 203.38 16.20 5 -15 23 185.08 28.90 5 15 -23 276.47 38.10 -5 15 23 209.78 22.20 -15 23 5 187.58 18.10 -15 23 5 219.48 27.00 23 5 -15 220.98 21.20 -15 23 5 251.97 34.80 -15 23 5 223.18 17.60 -15 23 5 225.28 23.40 23 5 -15 116.99 44.60 -5 15 23 212.98 16.00 -5 15 23 246.58 27.90 15 23 -5 237.98 27.30 5 15 23 224.58 18.20 5 15 23 241.28 17.10 -15 23 -5 169.38 28.10 -5 -15 23 251.47 31.40 23 5 15 246.68 22.50 5 15 23 209.88 29.20 5 -15 -23 209.88 39.00 5 15 23 232.18 29.60 -15 23 -5 225.78 27.60 23 -5 -15 166.98 43.10 23 5 15 182.18 23.40 -15 23 -5 213.08 18.90 -15 23 7 243.98 26.00 23 7 -15 200.68 18.40 15 23 -7 144.39 19.40 7 -15 23 151.18 14.50 7 -15 23 118.59 18.80 -15 23 7 147.29 19.50 -15 23 7 133.59 15.70 -7 15 23 144.09 19.00 -15 23 7 160.98 15.40 -7 15 23 133.89 15.80 7 15 -23 206.48 35.20 -15 23 7 135.59 26.10 -15 23 7 149.39 22.20 23 7 -15 156.48 30.40 23 -7 -15 128.19 40.40 7 -15 -23 133.09 36.20 23 7 15 141.09 22.10 -7 -15 23 174.48 28.40 7 15 23 147.49 20.40 7 15 23 177.18 16.10 -15 23 -7 167.38 21.10 -15 23 -7 161.18 16.90 7 15 23 131.09 16.00 7 15 23 167.78 14.60 23 7 15 185.38 19.80 23 7 15 146.89 18.00 23 9 -15 82.99 15.20 9 -15 23 52.29 8.00 -15 23 9 38.50 13.30 -9 15 23 44.30 12.80 23 9 -15 36.80 26.60 15 23 -9 48.40 17.10 -15 23 9 82.69 21.30 -15 23 9 46.90 15.30 9 15 -23 56.79 22.30 -15 23 9 42.80 12.80 -9 15 23 31.10 14.10 9 -15 23 10.40 14.30 -15 23 9 55.09 25.00 23 9 -15 60.49 10.10 23 9 15 43.90 10.80 23 -9 -15 28.20 35.80 23 9 15 36.20 10.50 -15 23 -9 39.70 8.70 -15 23 -9 44.40 16.60 23 9 15 29.10 18.70 9 -15 -23 20.80 32.60 9 15 23 45.30 9.10 -9 -15 23 55.69 16.50 9 15 23 40.40 15.40 9 15 23 41.20 7.60 9 15 23 34.10 9.10 23 9 15 70.09 15.20 11 15 -23 9.20 20.80 -15 23 11 7.10 25.70 11 -15 23 -12.30 11.70 15 23 -11 -18.60 17.10 -15 23 11 11.00 14.10 -15 23 11 26.90 24.70 23 11 -15 -4.70 23.90 -15 23 11 -14.30 11.70 11 -15 23 10.00 6.10 -15 23 11 1.00 11.00 11 -15 -23 -13.70 32.80 11 15 23 0.20 13.10 11 15 23 2.60 5.70 11 15 23 -4.30 6.80 11 15 23 0.90 7.60 23 11 15 -8.40 8.10 23 11 15 6.10 17.40 23 11 15 -4.00 8.90 15 23 11 -2.00 8.70 -11 -15 23 8.10 14.90 -15 23 -11 6.30 14.90 -15 23 13 90.49 12.60 15 23 -13 82.59 20.60 -15 23 13 112.59 25.40 23 13 -15 55.59 23.30 23 13 -15 64.29 21.80 13 15 -23 84.49 21.30 13 -15 23 60.09 8.00 13 15 23 51.09 9.00 -13 -15 23 59.19 16.10 15 23 13 61.09 10.50 23 13 15 54.19 18.00 -15 23 -13 74.59 16.50 13 -15 -23 82.79 33.20 23 13 15 53.09 10.10 13 15 23 57.79 7.40 15 -23 15 94.49 11.70 -15 23 15 109.89 23.90 15 15 -23 123.79 20.50 23 15 -15 118.69 22.40 23 15 -15 106.99 21.00 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311.87 28.60 -5 15 25 337.27 19.70 5 15 25 345.37 29.30 5 15 25 348.87 20.70 25 -5 -15 276.17 47.60 5 15 25 375.06 20.90 -5 -15 25 349.96 30.20 5 -15 -25 399.76 51.09 25 5 15 354.06 25.80 -15 25 -5 317.77 36.40 -15 25 -5 332.67 23.60 5 15 25 302.57 21.30 -15 25 -5 374.26 31.70 25 5 15 391.36 35.50 7 -15 25 215.38 15.40 25 7 -15 289.87 34.60 -15 25 7 247.98 34.80 -15 25 7 236.98 23.30 -7 15 25 234.88 23.40 25 7 -15 214.28 33.30 25 7 -15 285.27 19.10 -7 -15 -25 160.28 32.00 7 15 -25 266.77 34.30 -15 25 7 229.58 17.60 -15 25 7 188.48 18.00 7 -15 25 212.18 23.90 -15 25 7 236.38 27.20 -15 25 -7 267.67 29.00 7 15 25 197.18 16.70 7 15 25 256.27 25.90 25 7 15 234.68 20.70 25 7 15 267.27 31.40 -15 25 -7 225.68 18.30 -7 -15 25 254.87 27.20 -15 25 -7 219.88 28.60 7 -15 -25 270.77 48.40 25 -7 -15 183.08 41.80 7 15 25 230.48 16.80 7 15 25 243.98 16.00 9 -15 25 23.80 10.30 -15 25 9 45.90 15.20 -15 25 9 40.40 13.70 -9 15 25 35.10 11.30 25 9 -15 67.69 23.90 25 9 -15 61.69 21.70 -15 25 9 28.70 11.50 9 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37.80 3 15 27 179.18 21.90 3 15 27 156.78 12.60 3 15 27 170.88 12.30 27 3 15 157.38 19.50 27 5 -15 276.97 18.20 -15 27 5 250.87 27.60 -15 27 5 235.38 21.80 -15 27 5 275.97 31.10 -5 15 27 245.38 22.00 -5 -15 -27 252.27 40.10 5 -15 27 220.28 19.40 -5 -15 27 258.07 23.60 27 -5 -15 185.78 38.10 5 -15 -27 313.07 42.90 -15 27 -5 251.07 27.70 -15 27 -5 232.58 18.50 27 5 15 256.27 20.80 27 5 15 271.47 28.90 -15 27 -5 262.97 32.40 5 15 27 230.48 15.60 5 15 27 234.08 15.20 5 15 27 257.47 23.70 7 15 -27 159.58 25.80 -7 -15 -27 129.39 26.90 -15 27 7 146.79 19.00 -15 27 7 173.18 24.10 27 7 -15 126.29 25.60 -7 15 27 155.28 17.20 -15 27 7 134.39 18.50 -7 -15 27 169.38 20.60 27 7 15 203.78 25.70 7 -15 -27 197.78 39.00 -15 27 -7 205.48 29.80 -15 27 -7 195.88 25.70 7 15 27 148.09 11.80 27 7 15 172.98 15.80 7 15 27 180.18 20.20 -15 27 9 -1.20 13.20 27 9 -15 13.90 18.10 27 9 -15 36.10 18.90 -9 15 27 32.00 9.80 -15 27 9 68.59 20.90 9 15 -27 22.30 17.60 -9 -15 -27 9.40 22.30 -15 27 9 22.70 9.60 9 -15 -27 31.70 26.00 27 9 15 38.10 16.60 -15 27 -9 29.40 14.30 -15 27 -9 30.50 20.40 9 15 27 19.80 11.00 27 11 -15 -34.00 17.40 -15 27 11 17.60 8.10 27 11 -15 31.00 9.50 -15 27 11 31.70 18.80 27 11 15 44.70 16.00 27 11 15 14.10 8.50 11 15 27 5.50 8.60 -15 27 -11 -6.30 19.40 15 27 11 20.80 6.70 -15 27 -11 16.10 13.10 -1 17 27 8.20 10.80 1 -17 27 4.30 10.70 -17 27 1 3.60 9.00 -17 27 1 21.90 14.60 27 1 -17 17.60 9.10 -1 -17 -27 23.70 26.00 27 -1 17 -7.10 9.80 -1 17 27 8.30 14.00 -17 27 1 25.20 19.00 -17 27 -1 12.10 8.60 -1 -17 27 12.90 11.40 -17 27 -1 -12.10 18.60 1 17 27 4.90 10.90 1 -17 -27 22.70 24.80 -17 27 -1 32.40 14.90 1 17 27 10.10 4.90 27 -1 -17 20.10 9.80 27 1 17 1.40 9.60 -3 -17 -27 103.19 26.70 27 3 -17 118.39 13.70 -17 27 3 89.99 17.70 -3 17 27 89.89 12.80 -17 27 3 112.49 16.50 3 -17 27 76.99 11.60 27 3 -17 13.80 35.30 3 17 -27 92.19 18.70 27 -3 17 77.59 12.20 -17 27 3 128.59 21.40 -3 -17 27 84.39 13.10 -17 27 -3 97.19 21.10 3 -17 -27 92.49 25.30 27 3 17 98.89 11.70 3 17 27 96.59 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14 0 27.40 16.80 28 14 0 5.40 13.70 0 28 14 23.20 8.90 0 28 -14 27.90 12.80 16 0 28 6.80 8.90 0 28 16 11.00 9.20 16 0 -28 10.70 22.10 28 16 0 -4.10 12.50 28 16 0 -1.10 15.70 16 0 -28 -3.30 7.30 28 16 0 1.30 8.90 2 28 0 150.88 18.90 28 0 2 162.18 19.70 0 2 28 184.28 22.80 28 0 -2 133.99 19.00 28 0 -2 177.48 21.30 -2 28 0 141.09 20.70 0 2 28 153.18 12.40 2 28 0 138.29 13.30 -2 28 0 147.59 13.80 28 0 2 174.88 20.60 -2 28 0 170.08 25.80 -2 2 28 102.09 15.40 -2 28 2 92.69 10.00 -2 28 2 122.99 17.60 28 2 -2 89.89 17.10 28 2 -2 117.59 14.70 28 -2 2 113.79 15.30 2 28 -2 111.39 17.60 2 28 -2 98.19 11.30 2 -2 28 112.39 10.90 -2 28 2 96.09 18.60 2 2 28 114.69 11.00 2 -2 -28 105.79 32.30 28 2 2 105.49 18.00 2 28 2 98.09 9.90 2 28 2 113.09 17.10 -2 28 -2 97.09 17.50 -2 28 -2 107.19 11.90 28 2 2 106.89 14.00 2 2 28 117.89 16.00 28 -2 -2 125.89 15.60 28 -2 -2 108.99 18.10 28 4 -2 33.20 12.00 -2 28 4 22.20 16.30 4 -2 28 23.30 6.10 -4 2 28 23.40 12.40 28 4 -2 23.30 15.20 -2 28 4 38.90 14.50 -2 28 4 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-6 13.90 15.20 -6 28 6 0.10 18.90 6 6 -28 3.70 9.80 28 6 -6 -9.50 11.30 -6 28 6 -18.30 9.70 -6 28 6 11.00 14.20 6 -6 28 1.00 4.80 -6 28 6 2.50 6.20 -6 6 28 8.80 11.60 28 6 -6 -3.90 9.90 -6 28 6 -21.70 13.90 28 6 6 -20.10 15.70 28 6 6 2.70 17.20 28 6 6 4.40 10.50 28 6 6 -8.70 9.80 6 -6 -28 12.20 29.50 -6 28 -6 -2.30 15.10 6 6 28 12.90 8.40 6 6 28 6.10 13.10 -6 28 -6 1.00 15.40 6 6 28 4.10 5.50 -6 28 -6 6.20 6.90 28 8 -6 13.00 17.20 -6 28 8 3.80 6.30 -6 28 8 -6.10 11.20 28 8 -6 1.40 11.90 8 6 -28 -7.40 9.20 28 8 -6 3.10 9.00 8 -6 28 8.20 4.90 28 8 -6 28.60 15.00 -6 28 8 15.40 14.40 -6 28 8 -4.10 13.90 -6 28 8 -5.60 18.90 8 6 28 8.70 12.60 8 -6 -28 20.90 29.90 -6 28 -8 3.50 7.00 -6 28 -8 13.10 15.20 -6 28 -8 -3.10 15.90 28 8 6 11.90 10.50 28 8 6 -4.10 10.00 6 28 8 -44.50 13.30 28 8 6 -14.80 16.10 28 8 6 2.30 16.90 8 6 28 5.20 8.50 8 6 28 5.60 5.40 28 10 -6 18.10 14.40 28 10 -6 -6.50 11.30 -6 28 10 -0.10 6.40 28 10 -6 17.90 17.40 -6 28 10 11.40 14.60 28 10 -6 -15.20 19.90 -6 28 10 -10.30 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14 8 28 12.30 6.20 -8 28 -14 13.00 13.50 28 14 8 6.00 8.60 -10 28 0 150.38 17.20 -10 28 0 188.08 26.50 0 -10 28 215.28 19.30 0 10 28 200.88 23.20 -10 28 0 146.49 21.10 0 -10 -28 215.68 44.10 28 0 -10 153.88 37.30 0 10 28 152.98 12.50 28 0 -10 184.58 21.00 28 0 10 181.98 21.40 -10 28 0 163.18 19.10 -10 28 2 100.79 17.80 -10 28 2 92.99 20.10 -2 -10 -28 110.89 29.50 -10 28 2 91.39 10.00 -10 28 2 86.19 16.30 -2 10 28 108.79 10.10 28 2 -10 146.69 18.90 -10 28 2 86.09 12.40 28 -2 10 103.59 15.00 -2 10 28 114.79 16.30 2 10 28 113.09 16.60 2 -10 -28 112.19 29.60 28 -2 -10 132.19 15.80 28 2 10 143.49 20.50 28 -2 -10 110.09 34.30 -10 28 -2 113.79 18.00 -10 28 -2 86.79 11.40 -10 28 -2 107.19 19.60 -10 28 -2 113.79 17.90 -2 -10 28 151.38 18.20 2 10 28 107.29 10.70 -10 28 4 11.70 9.70 4 -10 28 20.90 5.00 28 4 -10 15.80 10.20 -10 28 4 34.60 15.10 -10 28 4 -2.70 13.80 -10 28 4 3.60 19.90 -4 10 28 17.60 12.50 -4 -10 -28 20.50 25.80 -10 28 4 18.50 6.90 28 4 10 31.30 12.00 4 10 28 23.00 5.90 -10 28 -4 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28 8 10 65.99 10.30 -10 28 -8 57.29 8.80 -10 -10 -28 59.99 24.20 28 10 -10 109.59 15.30 10 -10 28 71.09 8.10 28 10 -10 93.19 14.50 -10 28 10 90.59 20.70 -10 28 10 78.89 16.40 -10 28 10 83.19 13.00 28 10 -10 83.99 20.70 28 10 -10 87.29 22.90 28 10 10 101.29 18.10 10 -10 -28 108.59 29.40 28 10 10 106.89 16.50 10 10 28 87.09 12.20 -10 28 -10 76.79 19.70 28 10 10 68.59 11.00 10 10 28 94.69 8.90 -10 28 -10 84.19 16.60 10 10 28 101.49 13.60 -10 28 12 78.59 12.10 28 12 -10 44.20 19.90 -10 28 12 85.89 18.70 28 12 -10 58.69 13.00 -10 28 12 31.90 14.30 28 12 -10 59.19 21.10 -10 28 -12 68.39 15.10 28 12 10 66.89 17.40 10 28 12 69.99 8.80 12 10 28 74.19 11.30 12 -10 -28 82.99 29.20 12 10 28 54.09 7.20 -10 28 -12 71.89 19.40 28 12 10 60.29 14.90 28 12 10 48.50 10.00 28 0 -12 128.89 37.50 28 0 12 119.59 15.30 0 -12 28 121.79 18.40 28 0 -12 148.69 19.80 -12 28 0 104.69 15.40 0 -12 -28 108.39 29.90 0 12 28 123.99 10.50 -12 28 0 130.39 20.90 -12 28 0 117.79 18.20 -12 28 0 121.89 17.20 0 12 28 136.29 16.70 28 2 -12 74.39 12.30 28 2 -12 20.00 34.90 -2 -12 -28 92.29 28.10 -2 12 28 62.39 6.70 -2 12 28 75.19 14.10 -12 28 2 85.39 16.20 2 -12 28 74.69 10.90 28 -2 12 63.29 13.50 -12 28 2 70.09 11.20 -12 28 2 65.69 19.70 -12 28 2 46.60 15.00 2 -12 -28 87.29 28.00 2 12 28 84.59 9.10 28 -2 -12 85.19 13.70 28 -2 -12 71.99 35.10 -2 -12 28 68.69 12.40 -12 28 -2 59.69 9.80 -12 28 -2 68.19 19.10 -12 28 -2 69.49 16.50 2 12 28 72.99 14.80 28 2 12 70.39 13.20 -12 28 -2 71.59 17.70 -12 28 4 15.60 6.60 28 4 -12 8.60 9.50 -12 28 4 30.40 20.00 -4 -12 -28 22.50 25.40 -12 28 4 3.30 9.50 -12 28 4 14.90 14.30 -12 28 4 -5.50 14.40 -4 12 28 14.40 11.40 4 12 28 9.10 12.80 -4 -12 28 19.50 10.90 28 -4 -12 37.10 19.60 28 4 12 5.30 11.30 4 12 28 14.80 5.10 28 -4 -12 27.40 32.80 4 -12 -28 20.00 26.90 4 12 28 22.80 7.10 -12 28 -4 8.50 7.60 -12 28 -4 9.90 14.10 -12 28 -4 18.80 18.50 -6 12 28 4.30 10.80 28 6 -12 14.20 8.30 -12 28 6 11.00 13.90 -12 28 6 -2.00 20.10 -6 -12 -28 13.50 23.70 -12 28 6 5.20 6.10 -12 28 6 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3 55.99 18.10 7 3 29 52.29 6.90 3 29 7 63.29 15.00 7 -3 -29 71.09 28.50 3 29 7 44.40 7.40 29 7 3 72.99 12.30 29 7 3 38.30 12.00 -3 29 9 22.90 13.80 -3 29 9 2.10 6.10 -3 29 9 12.50 14.10 29 9 -3 -0.60 17.00 -3 29 9 -3.90 10.50 29 9 -3 -2.90 10.80 29 9 -3 0.50 14.20 9 3 -29 -1.10 10.10 9 -3 29 8.30 4.80 9 3 29 3.30 11.40 -3 29 -9 12.50 14.10 3 29 9 13.40 13.70 29 9 3 -6.70 10.10 3 29 9 -10.90 6.30 29 9 3 17.30 16.80 3 29 9 2.40 5.90 9 -3 -29 38.40 28.70 -3 29 -9 5.00 6.20 9 3 29 9.50 5.20 29 9 3 1.20 15.50 29 11 -3 3.50 13.80 29 11 -3 -2.00 10.50 11 3 -29 7.90 8.70 11 -3 29 14.40 4.90 -3 29 11 10.00 14.00 29 11 -3 12.60 17.30 -3 29 11 5.70 10.60 -3 29 11 7.70 6.00 11 3 29 13.20 4.90 29 11 3 26.40 16.30 3 29 11 15.70 13.60 3 29 11 0.90 8.40 3 29 11 2.20 6.50 11 3 29 5.60 10.60 11 -3 -29 35.60 28.00 29 11 3 -18.60 14.90 -3 29 -11 16.40 14.10 29 11 3 2.20 10.00 -3 29 13 56.09 11.40 29 13 -3 40.40 13.70 13 3 -29 41.90 8.60 29 13 -3 22.40 19.10 29 13 -3 41.30 11.20 -3 29 13 22.20 14.40 29 13 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7 29.20 9.90 -7 -13 -29 44.90 20.40 -13 29 7 39.00 18.80 29 7 13 49.60 16.10 7 13 29 35.90 11.00 -13 29 -7 41.70 14.70 7 13 29 26.50 5.60 7 -13 -29 56.69 24.90 -13 29 -7 31.80 17.40 -15 29 1 39.80 18.40 29 1 -15 8.10 8.30 29 -1 15 -8.20 9.60 -1 15 29 -3.30 10.10 -15 29 1 16.60 13.90 -1 -15 -29 19.00 21.50 -15 29 1 6.20 8.30 -15 29 -1 10.40 17.40 -15 29 -1 8.10 8.00 29 1 15 -5.40 9.20 1 15 29 2.30 10.40 29 -1 -15 4.50 9.00 1 -15 -29 20.70 22.10 -15 29 -1 17.70 13.70 1 15 29 6.00 4.70 -3 15 29 53.49 10.80 -15 29 3 46.40 10.20 -15 29 3 52.79 15.10 -15 29 3 65.79 19.60 -15 29 -3 44.10 17.90 3 15 29 47.30 11.80 -15 29 -3 54.49 8.60 -15 29 -3 70.99 15.00 0 0 30 283.67 23.60 0 30 0 243.88 17.90 0 30 0 273.97 28.80 30 0 0 344.37 25.30 30 0 0 380.46 28.60 30 -2 0 243.98 22.00 30 2 0 254.17 22.40 30 2 0 222.88 21.40 2 0 30 179.08 21.70 2 0 30 195.48 13.10 0 30 2 220.08 26.60 -2 0 30 180.68 20.60 0 30 -2 180.48 26.30 0 30 2 155.08 14.30 30 4 0 41.30 11.90 30 -4 0 52.39 13.00 4 0 30 27.80 12.60 0 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30 0 -4 59.59 12.90 0 4 30 36.60 12.60 -4 30 0 41.30 15.20 -4 30 0 32.00 7.90 30 0 4 53.29 13.00 0 4 30 33.60 7.50 -4 30 2 17.70 6.20 30 2 -4 24.50 15.70 30 -2 4 33.40 12.50 -4 30 2 10.30 7.60 -2 4 30 23.00 11.90 30 2 -4 18.20 11.30 -4 30 2 32.50 15.00 -2 -4 30 -5.10 10.30 -4 30 -2 21.60 7.00 30 2 4 26.70 11.90 2 4 30 7.20 11.90 -4 30 -2 29.50 14.60 30 2 4 8.80 21.20 2 4 30 21.90 5.20 2 -4 -30 53.49 25.70 30 -2 -4 17.00 12.20 30 -4 4 -3.10 11.70 -4 4 30 -2.00 10.60 -4 30 4 5.40 13.80 30 4 -4 3.30 10.00 30 4 -4 16.10 15.50 -4 30 4 1.40 5.80 4 -4 30 1.00 4.30 -4 30 4 -1.50 7.70 30 -4 -4 15.20 12.10 -4 30 -4 1.40 14.20 -4 30 -4 -2.90 6.20 4 4 30 5.50 4.60 4 4 30 -0.30 11.50 30 4 4 1.10 11.20 30 4 4 -32.30 15.60 4 -4 -30 25.40 25.40 -4 30 6 6.30 5.90 30 6 -4 -5.60 14.90 -6 4 30 14.30 13.10 6 4 -30 -9.60 10.10 -4 30 6 -2.20 8.40 6 -4 30 9.50 4.60 30 6 -4 21.20 9.50 -4 30 6 7.70 14.00 6 4 30 5.40 11.30 -4 30 -6 4.30 6.10 30 6 4 0.30 16.40 -4 30 -6 15.60 14.20 6 4 30 4.90 4.60 30 6 4 6.70 10.80 4 30 6 11.60 13.60 6 -4 -30 10.10 25.30 -4 30 8 21.60 14.20 8 4 -30 19.70 8.90 30 8 -4 10.20 10.90 -4 30 8 20.10 6.50 -4 30 8 7.30 9.40 30 8 -4 5.30 20.10 30 8 -4 -42.50 20.80 30 8 -4 -0.10 14.80 8 -4 30 23.00 5.70 -4 30 -8 14.60 6.30 30 8 4 -3.50 15.90 8 4 30 12.80 11.00 8 4 30 18.50 5.00 -4 30 -8 15.60 14.20 30 8 4 12.10 17.30 30 8 4 11.80 10.30 4 30 8 21.00 13.50 8 -4 -30 30.50 25.60 30 10 -4 -9.20 18.60 30 10 -4 24.20 14.10 30 10 -4 19.40 18.10 10 4 -30 34.40 8.90 30 10 -4 8.60 10.60 -4 30 10 19.10 9.60 -4 30 10 13.20 14.60 30 10 4 15.50 16.70 10 4 30 21.90 7.80 -4 30 -10 33.10 14.20 30 10 4 10.20 15.50 30 10 4 11.20 9.80 10 4 30 7.60 10.20 4 30 10 24.50 12.90 10 -4 -30 48.20 25.80 4 30 10 12.60 6.60 -4 30 12 24.80 9.50 30 12 -4 4.30 17.40 30 12 -4 3.80 10.00 30 12 -4 11.80 13.00 -4 30 12 -20.60 13.20 30 12 -4 20.40 17.60 12 4 -30 14.60 7.60 4 30 12 8.40 11.60 12 4 30 11.40 9.00 30 12 4 6.20 15.80 30 12 4 6.90 9.40 12 -4 -30 39.40 23.50 12 4 30 7.80 6.30 4 30 12 6.90 6.50 -4 30 -12 31.20 12.90 30 12 4 12.20 14.40 -6 30 0 24.60 6.30 30 0 -6 23.90 11.90 0 -6 -30 40.70 23.60 0 6 30 18.20 4.80 -6 30 0 23.30 7.70 -6 30 0 30.20 14.30 30 0 6 27.30 12.30 0 6 30 33.00 12.20 -2 -6 -30 28.70 35.80 30 -2 6 26.10 12.30 -6 30 2 14.80 14.10 -6 30 2 14.00 7.80 -6 30 2 13.30 6.00 -2 6 30 22.70 11.90 30 2 -6 17.60 10.80 2 6 30 20.70 12.10 30 2 6 13.80 11.60 -6 30 -2 22.30 14.20 2 -6 -30 24.90 25.10 2 6 30 16.70 5.00 30 -2 -6 27.30 11.90 -6 30 -2 10.90 6.90 30 -4 6 5.20 11.80 -6 30 4 8.30 14.00 30 4 -6 5.60 9.70 30 4 -6 24.10 15.00 -6 30 4 4.20 5.80 -6 30 4 2.60 8.00 -4 6 30 8.40 10.60 30 -4 -6 19.30 11.90 -6 30 -4 6.40 6.50 -6 30 -4 0.40 14.20 4 6 30 7.50 7.90 4 6 30 5.00 4.60 4 6 30 11.50 11.60 30 4 6 7.30 11.00 4 -6 -30 17.30 25.30 30 4 6 -6.10 17.00 -6 30 6 3.10 5.70 30 6 -6 1.90 8.70 30 6 -6 17.80 14.80 -6 30 6 -7.80 13.40 -6 30 6 -2.90 8.20 -6 6 30 1.10 9.70 30 6 -6 -21.90 26.70 -6 30 -6 10.70 13.90 30 6 6 1.50 15.50 30 6 6 3.40 10.40 6 -6 -30 19.00 25.80 6 6 30 -4.30 4.30 6 6 30 -6.00 10.80 -6 30 -6 5.10 6.40 6 6 30 3.40 7.30 30 8 -6 14.50 13.90 30 8 -6 -4.90 18.70 -6 30 8 7.30 14.60 30 8 -6 3.00 10.50 -6 30 8 5.10 8.90 8 6 30 2.10 10.50 8 -6 -30 33.90 25.90 30 8 6 18.30 16.50 30 8 6 10.30 15.50 8 6 30 6.20 7.30 30 8 6 -7.80 9.20 -6 30 -8 4.60 6.20 -6 30 -8 21.60 14.10 -6 30 10 0.70 14.20 30 10 -6 0.20 18.00 30 10 -6 20.60 10.40 10 6 -30 20.80 8.50 30 10 -6 27.80 13.60 -6 30 10 11.60 9.30 30 10 -6 21.00 17.90 30 10 6 16.70 9.50 10 6 30 22.40 7.10 -6 30 -10 22.80 14.00 30 10 6 -3.00 14.90 30 10 6 26.60 16.30 10 6 30 18.60 10.00 10 -6 -30 40.00 25.70 0 -8 -30 227.18 35.50 -8 30 0 170.38 16.80 30 0 -8 232.98 21.30 30 0 8 233.48 21.60 -8 30 0 195.88 25.20 0 8 30 212.78 21.70 -8 30 2 105.09 14.90 -2 -8 -30 126.59 24.60 -8 30 2 106.39 17.20 30 2 -8 136.39 18.00 -8 30 2 105.19 11.40 30 -2 8 127.49 15.30 -2 8 30 130.69 18.30 2 8 30 109.29 11.50 2 -8 -30 135.39 27.00 -8 30 -2 107.29 13.70 30 -2 -8 147.29 19.00 2 8 30 132.29 19.60 -8 30 -2 126.49 17.90 30 2 8 153.98 19.40 -8 30 4 21.20 14.30 -8 30 4 1.00 8.60 -4 8 30 23.30 10.70 -4 -8 -30 26.60 20.90 30 4 -8 24.50 9.70 -8 30 4 14.50 6.10 30 -4 8 21.30 12.10 30 -4 -8 30.10 11.80 4 -8 -30 29.60 25.40 4 8 30 19.00 7.10 4 8 30 23.60 11.70 -8 30 -4 17.00 14.30 30 4 8 28.80 11.20 4 8 30 19.60 7.20 -8 30 -4 14.30 6.90 -8 30 6 8.20 13.80 30 6 -8 9.70 8.10 -6 8 30 27.90 9.70 -8 30 6 6.30 9.00 -8 30 -6 26.10 13.90 6 8 30 7.90 10.70 -8 30 -6 5.60 6.60 30 6 8 12.20 9.90 30 6 8 2.70 16.90 6 8 30 7.50 7.10 6 -8 -30 22.00 25.00 30 8 -8 95.69 14.50 -8 30 8 62.39 16.00 30 8 -8 69.59 19.60 -8 30 8 66.79 11.50 8 8 30 69.69 11.70 8 8 30 65.79 8.30 -8 30 -8 85.69 11.50 30 8 8 119.49 18.00 8 -8 -30 109.49 26.10 30 8 8 109.59 16.00 -8 30 -8 81.29 15.30 30 10 -8 97.09 20.30 30 10 -8 194.78 18.90 30 10 -8 126.99 16.60 30 10 -8 123.69 20.80 -8 30 10 97.29 17.40 -8 30 10 109.29 16.50 10 -8 -30 187.58 35.80 30 10 8 132.59 18.10 -8 30 -10 159.08 22.20 30 10 8 137.29 16.20 30 10 8 99.69 14.50 10 8 30 126.49 16.00 10 8 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5 0.60 7.90 -5 9 31 17.50 8.60 31 -5 9 7.20 11.00 -9 31 5 -1.90 13.30 31 5 9 -9.60 8.20 31 -5 -9 20.00 10.30 5 -9 -31 36.70 21.90 5 9 31 10.50 5.90 5 9 31 6.30 9.70 -9 31 -5 8.10 6.30 -9 31 -5 21.70 13.30 0 0 32 205.88 19.20 0 32 0 259.97 26.40 32 0 0 267.87 21.80 32 -2 0 176.88 19.40 -2 0 32 125.59 15.40 0 32 -2 147.39 18.30 0 32 2 152.78 22.80 2 0 32 123.59 16.60 4 0 32 9.50 9.80 32 -4 0 39.40 11.60 32 4 0 36.60 15.50 0 32 4 26.70 13.20 32 4 0 37.20 9.90 0 32 4 15.60 6.40 -4 0 32 30.20 13.70 0 32 -4 26.60 13.30 0 32 6 27.50 7.20 32 6 0 25.30 15.00 6 0 32 13.00 9.30 32 -6 0 28.10 12.10 0 32 6 19.40 13.30 0 32 -6 27.60 12.80 0 -2 32 114.99 15.60 32 0 -2 172.88 18.70 -2 32 0 114.29 12.10 -2 32 0 173.38 23.70 0 2 32 123.39 16.60 -2 32 2 70.79 15.00 32 2 -2 125.49 16.60 2 -2 32 58.49 11.20 -2 2 32 81.99 11.50 32 -2 2 92.49 13.30 -2 32 2 82.99 11.30 2 2 32 74.29 11.60 -2 -2 32 78.89 10.70 32 2 2 133.29 17.10 -2 32 -2 75.99 10.50 -2 32 -2 96.29 16.60 32 -2 -2 135.79 18.00 2 32 2 78.49 15.20 -2 32 4 10.60 12.70 4 -2 32 4.90 9.20 -2 32 4 10.10 6.60 32 4 -2 28.50 9.20 32 4 -2 25.50 14.80 -4 2 32 21.30 8.70 32 -4 2 21.70 11.30 32 -4 -2 21.70 11.00 32 4 2 1.20 15.30 32 4 2 19.20 9.80 4 2 32 12.60 9.70 -2 32 -4 9.20 5.50 2 32 4 15.60 12.60 -2 32 -4 21.50 13.30 -2 32 6 15.30 7.20 32 6 -2 35.20 14.50 -2 32 6 15.50 13.70 32 -6 2 21.30 12.00 6 -2 32 15.90 9.20 6 2 32 8.30 9.40 -2 32 -6 12.70 5.40 2 32 6 18.90 12.50 -2 32 -6 21.20 12.80 32 -6 -2 26.60 10.90 32 6 2 27.60 15.10 32 0 -4 34.20 10.80 -4 32 0 30.10 14.20 0 4 32 20.60 10.30 32 0 4 17.40 11.10 -4 32 0 17.40 6.30 0 -4 32 10.30 9.00 32 -2 4 14.50 10.80 2 -4 32 -8.00 8.80 -4 32 2 10.60 13.10 -4 32 2 3.70 6.30 -2 4 32 6.20 9.10 32 2 -4 24.60 9.90 2 4 32 20.70 10.20 -2 -4 32 -1.00 8.00 -4 32 -2 4.40 13.80 32 2 4 16.30 10.70 -4 32 -2 9.00 5.80 32 -2 -4 16.20 10.60 32 -4 4 21.80 11.00 32 4 -4 14.50 8.70 4 -4 32 -12.90 8.50 -4 32 4 1.90 13.00 -4 4 32 9.20 8.50 -4 32 4 3.80 6.80 32 -4 -4 24.20 10.50 32 4 4 -36.20 18.80 32 4 4 0.70 9.60 -4 32 -4 9.00 12.80 -4 32 -4 -0.20 5.30 4 4 32 5.90 9.90 -4 32 6 -2.50 13.20 -4 32 -6 9.00 12.60 32 0 -6 36.90 10.30 32 0 6 20.20 10.80 -6 32 0 15.60 6.80 -6 32 0 34.70 14.20 0 -6 32 8.80 8.20 0 6 32 19.60 9.80 -6 32 2 17.70 13.60 32 -2 6 12.00 10.60 -2 6 32 19.60 9.10 2 -6 32 -1.00 8.40 -6 32 2 14.90 6.80 32 2 -6 21.90 9.20 32 -2 -6 27.30 10.50 -2 -6 32 8.90 8.40 2 6 32 15.60 9.50 32 2 6 21.40 10.30 -6 32 -2 34.70 14.10 2 6 32 7.10 6.20 -6 32 -2 9.80 6.00 -4 6 32 13.80 8.40 -6 32 4 8.50 13.30 -6 32 -4 6.90 12.80 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 11877 _olex2_submission_special_instructions 'No special instructions were received'