data_fxm-lww-4-cl _audit_creation_date 2017-03-14 _audit_creation_method ; Olex2 1.2 (compiled 2017.03.02 svn.r3394 for OlexSys, GUI svn.r5324) ; _shelx_SHELXL_version_number '2014/7' _publ_contact_author_address ? _publ_contact_author_email ? _publ_contact_author_id_orcid ? _publ_contact_author_name '' _publ_contact_author_phone ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C19 H25 Cl O3, 0.5(H2 O)' _chemical_formula_sum 'C19 H26 Cl O3.50' _chemical_formula_weight 345.85 _chemical_absolute_configuration ad _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'monoclinic' _space_group_IT_number 5 _space_group_name_H-M_alt 'C 1 2 1' _space_group_name_Hall 'C 2y' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' _cell_length_a 18.6435(7) _cell_length_b 6.1999(2) _cell_length_c 15.8122(6) _cell_angle_alpha 90 _cell_angle_beta 90.137(3) _cell_angle_gamma 90 _cell_volume 1827.68(11) _cell_formula_units_Z 4 _cell_measurement_reflns_used 4098 _cell_measurement_temperature 290.64(10) _cell_measurement_theta_max 71.8800 _cell_measurement_theta_min 4.7590 _shelx_estimated_absorpt_T_max ? _shelx_estimated_absorpt_T_min ? _exptl_absorpt_coefficient_mu 1.976 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.55194 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro, Agilent Technologies, Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET) (compiled Aug 13 2014,18:06:01) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _exptl_crystal_colour 'clear light colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier light _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.257 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description plate _exptl_crystal_F_000 740 _exptl_crystal_size_max 0.7 _exptl_crystal_size_mid 0.5 _exptl_crystal_size_min 0.15 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0492 _diffrn_reflns_av_unetI/netI 0.0363 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_limit_h_max 22 _diffrn_reflns_limit_h_min -22 _diffrn_reflns_limit_k_max 7 _diffrn_reflns_limit_k_min -6 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_limit_l_min -12 _diffrn_reflns_number 9541 _diffrn_reflns_point_group_measured_fraction_full 0.952 _diffrn_reflns_point_group_measured_fraction_max 0.952 _diffrn_reflns_theta_full 66.812 _diffrn_reflns_theta_max 66.812 _diffrn_reflns_theta_min 5.503 _diffrn_ambient_environment air _diffrn_ambient_temperature 290.64(10) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 15.9595 _diffrn_detector_type EosS2 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_details ; #__ type_ start__ end____ width___ exp.time_ 1 omega 17.00 105.00 1.0000 1.7700 omega____ theta____ kappa____ phi______ frames - 36.2921 38.0000 90.0000 88 #__ type_ start__ end____ width___ exp.time_ 2 omega 10.00 104.00 1.0000 1.7700 omega____ theta____ kappa____ phi______ frames - 36.2921 77.0000 -30.0000 94 #__ type_ start__ end____ width___ exp.time_ 3 omega 17.00 105.00 1.0000 1.7700 omega____ theta____ kappa____ phi______ frames - 36.2921 38.0000 150.0000 88 #__ type_ start__ end____ width___ exp.time_ 4 omega 10.00 104.00 1.0000 1.7700 omega____ theta____ kappa____ phi______ frames - 36.2921 77.0000 150.0000 94 #__ type_ start__ end____ width___ exp.time_ 5 omega 23.00 90.00 1.0000 1.7700 omega____ theta____ kappa____ phi______ frames - 36.2921 -125.0000 60.0000 67 #__ type_ start__ end____ width___ exp.time_ 6 omega 17.00 105.00 1.0000 1.7700 omega____ theta____ kappa____ phi______ frames - 36.2921 38.0000 -90.0000 88 #__ type_ start__ end____ width___ exp.time_ 7 omega -31.00 53.00 1.0000 1.7700 omega____ theta____ kappa____ phi______ frames - 36.2921 -57.0000 90.0000 84 #__ type_ start__ end____ width___ exp.time_ 8 omega 1.00 75.00 1.0000 1.7700 omega____ theta____ kappa____ phi______ frames - 36.2921 -99.0000 -180.0000 74 #__ type_ start__ end____ width___ exp.time_ 9 omega 39.00 109.00 1.0000 7.0600 omega____ theta____ kappa____ phi______ frames - 108.0000 -94.0000 90.0000 70 #__ type_ start__ end____ width___ exp.time_ 10 omega 91.00 176.00 1.0000 7.0600 omega____ theta____ kappa____ phi______ frames - 108.0000 45.0000 -60.0000 85 #__ type_ start__ end____ width___ exp.time_ 11 omega 37.00 146.00 1.0000 7.0600 omega____ theta____ kappa____ phi______ frames - 108.0000 -15.0000 -90.0000 109 #__ type_ start__ end____ width___ exp.time_ 12 omega 37.00 146.00 1.0000 7.0600 omega____ theta____ kappa____ phi______ frames - 108.0000 -15.0000 120.0000 109 #__ type_ start__ end____ width___ exp.time_ 13 omega 38.00 116.00 1.0000 7.0600 omega____ theta____ kappa____ phi______ frames - 108.0000 -111.0000 -30.0000 78 #__ type_ start__ end____ width___ exp.time_ 14 omega 40.00 98.00 1.0000 7.0600 omega____ theta____ kappa____ phi______ frames - 108.0000 -45.0000 -30.0000 58 #__ type_ start__ end____ width___ exp.time_ 15 omega 38.00 91.00 1.0000 7.0600 omega____ theta____ kappa____ phi______ frames - 108.0000 -30.0000 30.0000 53 #__ type_ start__ end____ width___ exp.time_ 16 omega 100.00 178.00 1.0000 7.0600 omega____ theta____ kappa____ phi______ frames - 108.0000 111.0000 60.0000 78 #__ type_ start__ end____ width___ exp.time_ 17 omega 39.00 109.00 1.0000 7.0600 omega____ theta____ kappa____ phi______ frames - 108.0000 -94.0000 120.0000 70 #__ type_ start__ end____ width___ exp.time_ 18 omega 38.00 91.00 1.0000 7.0600 omega____ theta____ kappa____ phi______ frames - 108.0000 -30.0000 -120.0000 53 #__ type_ start__ end____ width___ exp.time_ 19 omega 38.00 91.00 1.0000 7.0600 omega____ theta____ kappa____ phi______ frames - 108.0000 -30.0000 0.0000 53 #__ type_ start__ end____ width___ exp.time_ 20 omega 40.00 98.00 1.0000 7.0600 omega____ theta____ kappa____ phi______ frames - 108.0000 -45.0000 -180.0000 58 #__ type_ start__ end____ width___ exp.time_ 21 omega 39.00 109.00 1.0000 7.0600 omega____ theta____ kappa____ phi______ frames - 108.0000 -94.0000 -150.0000 70 #__ type_ start__ end____ width___ exp.time_ 22 omega 40.00 135.00 1.0000 7.0600 omega____ theta____ kappa____ phi______ frames - 108.0000 -77.0000 -30.0000 95 #__ type_ start__ end____ width___ exp.time_ 23 omega 40.00 98.00 1.0000 7.0600 omega____ theta____ kappa____ phi______ frames - 108.0000 -45.0000 90.0000 58 #__ type_ start__ end____ width___ exp.time_ 24 omega -31.00 53.00 1.0000 1.7700 omega____ theta____ kappa____ phi______ frames - 36.2921 -57.0000 -150.0000 84 #__ type_ start__ end____ width___ exp.time_ 25 omega 1.00 75.00 1.0000 1.7700 omega____ theta____ kappa____ phi______ frames - 36.2921 -99.0000 -30.0000 74 #__ type_ start__ end____ width___ exp.time_ 26 omega 10.00 104.00 1.0000 1.7700 omega____ theta____ kappa____ phi______ frames - 36.2921 77.0000 -90.0000 94 #__ type_ start__ end____ width___ exp.time_ 27 omega 10.00 104.00 1.0000 1.7700 omega____ theta____ kappa____ phi______ frames - 36.2921 77.0000 60.0000 94 #__ type_ start__ end____ width___ exp.time_ 28 omega -33.00 55.00 1.0000 1.7700 omega____ theta____ kappa____ phi______ frames - 36.2921 -38.0000 -90.0000 88 #__ type_ start__ end____ width___ exp.time_ 29 omega -33.00 55.00 1.0000 1.7700 omega____ theta____ kappa____ phi______ frames - 36.2921 -38.0000 0.0000 88 #__ type_ start__ end____ width___ exp.time_ 30 omega 70.00 178.00 1.0000 7.0600 omega____ theta____ kappa____ phi______ frames - 108.0000 15.0000 -180.0000 108 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'New Gemini, Dual, Cu at zero, EosS2' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_UB_11 -0.0276320000 _diffrn_orient_matrix_UB_12 -0.1846250000 _diffrn_orient_matrix_UB_13 0.0564196000 _diffrn_orient_matrix_UB_21 0.0778995000 _diffrn_orient_matrix_UB_22 -0.0668685000 _diffrn_orient_matrix_UB_23 0.0195901000 _diffrn_orient_matrix_UB_31 0.0006742000 _diffrn_orient_matrix_UB_32 0.1520823000 _diffrn_orient_matrix_UB_33 0.0769969000 _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_source 'Enhance (Cu) X-ray Source' _reflns_Friedel_coverage 0.734 _reflns_Friedel_fraction_full 0.896 _reflns_Friedel_fraction_max 0.896 _reflns_number_gt 2891 _reflns_number_total 3123 _reflns_odcompleteness_completeness 99.83 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 66.97 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement ; CrysAlisPro, Agilent Technologies, Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET) (compiled Aug 13 2014,18:06:01) ; _computing_data_collection ; CrysAlisPro, Agilent Technologies, Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET) (compiled Aug 13 2014,18:06:01) ; _computing_data_reduction ; CrysAlisPro, Agilent Technologies, Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET) (compiled Aug 13 2014,18:06:01) ; _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _refine_diff_density_max 0.304 _refine_diff_density_min -0.254 _refine_diff_density_rms 0.052 _refine_ls_abs_structure_details ; Flack x determined using 1100 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.016(16) _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.074 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 217 _refine_ls_number_reflns 3123 _refine_ls_number_restraints 1 _refine_ls_R_factor_all 0.0600 _refine_ls_R_factor_gt 0.0572 _refine_ls_restrained_S_all 1.073 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1080P)^2^+0.0910P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1533 _refine_ls_wR_factor_ref 0.1587 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups, All O(H) groups, All O(H,H) groups 2. Others Fixed Sof: H00W(0.5) H00X(0.5) 3.a Riding coordinates: O006(H00W,H00X) 3.b Ternary CH refined with riding coordinates: C005(H005), C009(H009), C00H(H00I) 3.c Secondary CH2 refined with riding coordinates: C00B(H00A,H00B), C00C(H00C,H00D), C00E(H00F,H00G), C00J(H00K,H00L) 3.d Aromatic/amide H refined with riding coordinates: C00D(H00E), C00G(H00H), C00I(H00J), C00K(H00M) 3.e Idealised Me refined as rotating group: C00M(H00N,H00O,H00P), C00N(H00Q,H00R,H00S), C00O(H00T,H00U,H00V) 3.f Idealised tetrahedral OH refined as rotating group: O002(H002) ; _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary direct _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cl01 Cl 0.43687(9) -0.0367(3) 0.88662(9) 0.1055(6) Uani 1 1 d . . . . . O002 O 0.26463(14) 0.5216(5) 0.46857(18) 0.0618(7) Uani 1 1 d . . . . . H002 H 0.2518 0.4220 0.4379 0.093 Uiso 1 1 calc GR . . . . O003 O 0.27461(18) 0.6551(5) 0.63002(19) 0.0714(8) Uani 1 1 d . . . . . O004 O 0.45322(16) 0.7442(6) 0.36773(17) 0.0665(8) Uani 1 1 d . . . . . C005 C 0.32460(17) 0.4570(6) 0.5163(2) 0.0486(7) Uani 1 1 d . . . . . H005 H 0.3333 0.3026 0.5078 0.058 Uiso 1 1 calc R . . . . O006 O 0.5000 1.0383(8) 0.5000 0.0791(13) Uani 1 2 d S T P . . H00W H 0.4885 0.9497 0.4612 0.119 Uiso 0.5 1 d R . . . . H00X H 0.5079 0.9699 0.5457 0.119 Uiso 0.5 1 d R . . . . C007 C 0.31094(18) 0.5018(6) 0.6099(2) 0.0517(8) Uani 1 1 d . . . . . C008 C 0.34507(18) 0.3655(6) 0.6761(2) 0.0506(8) Uani 1 1 d . . . . . C009 C 0.36304(18) 0.4824(6) 0.2210(2) 0.0492(7) Uani 1 1 d . . . . . H009 H 0.3202 0.4148 0.2451 0.059 Uiso 1 1 calc R . . . . C00A C 0.40464(19) 0.5765(7) 0.3964(2) 0.0526(8) Uani 1 1 d . . . . . C00B C 0.4195(2) 0.3606(7) 0.3570(2) 0.0578(9) Uani 1 1 d . . . . . H00A H 0.3807 0.2628 0.3710 0.069 Uiso 1 1 calc R . . . . H00B H 0.4633 0.3024 0.3812 0.069 Uiso 1 1 calc R . . . . C00C C 0.39071(19) 0.5846(7) 0.4899(2) 0.0550(8) Uani 1 1 d . . . . . H00C H 0.3846 0.7338 0.5069 0.066 Uiso 1 1 calc R . . . . H00D H 0.4322 0.5280 0.5196 0.066 Uiso 1 1 calc R . . . . C00D C 0.3435(2) 0.4367(8) 0.7598(2) 0.0598(9) Uani 1 1 d . . . . . H00E H 0.3224 0.5688 0.7723 0.072 Uiso 1 1 calc R . . . . C00E C 0.42738(19) 0.3703(7) 0.2610(2) 0.0552(8) Uani 1 1 d . . . . . H00F H 0.4708 0.4481 0.2467 0.066 Uiso 1 1 calc R . . . . H00G H 0.4314 0.2251 0.2387 0.066 Uiso 1 1 calc R . . . . C00F C 0.3575(2) 0.4544(7) 0.1234(2) 0.0567(8) Uani 1 1 d . . . . . C00G C 0.3778(2) 0.1683(7) 0.6585(3) 0.0607(9) Uani 1 1 d . . . . . H00H H 0.3803 0.1192 0.6030 0.073 Uiso 1 1 calc R . . . . C00H C 0.3779(2) 0.7494(7) 0.3432(2) 0.0575(9) Uani 1 1 d . . . . . H00I H 0.3486 0.8579 0.3721 0.069 Uiso 1 1 calc R . . . . C00I C 0.4063(2) 0.0461(8) 0.7230(3) 0.0677(10) Uani 1 1 d . . . . . H00J H 0.4280 -0.0857 0.7116 0.081 Uiso 1 1 calc R . . . . C00J C 0.3622(2) 0.7204(7) 0.2497(2) 0.0618(9) Uani 1 1 d . . . . . H00K H 0.3976 0.7998 0.2174 0.074 Uiso 1 1 calc R . . . . H00L H 0.3156 0.7817 0.2372 0.074 Uiso 1 1 calc R . . . . C00K C 0.3724(3) 0.3156(9) 0.8238(3) 0.0715(11) Uani 1 1 d . . . . . H00M H 0.3717 0.3650 0.8793 0.086 Uiso 1 1 calc R . . . . C00L C 0.4022(2) 0.1216(9) 0.8044(3) 0.0664(11) Uani 1 1 d . . . . . C00M C 0.4237(3) 0.5343(11) 0.0790(3) 0.0840(15) Uani 1 1 d . . . . . H00N H 0.4310 0.6840 0.0920 0.126 Uiso 1 1 calc GR . . . . H00O H 0.4179 0.5172 0.0191 0.126 Uiso 1 1 calc GR . . . . H00P H 0.4645 0.4527 0.0977 0.126 Uiso 1 1 calc GR . . . . C00N C 0.3471(3) 0.2150(10) 0.1023(3) 0.0816(13) Uani 1 1 d . . . . . H00Q H 0.3907 0.1381 0.1140 0.122 Uiso 1 1 calc GR . . . . H00R H 0.3352 0.2000 0.0435 0.122 Uiso 1 1 calc GR . . . . H00S H 0.3091 0.1571 0.1362 0.122 Uiso 1 1 calc GR . . . . C00O C 0.2917(3) 0.5757(12) 0.0898(3) 0.0957(17) Uani 1 1 d . . . . . H00T H 0.2492 0.5211 0.1166 0.143 Uiso 1 1 calc GR . . . . H00U H 0.2880 0.5552 0.0298 0.143 Uiso 1 1 calc GR . . . . H00V H 0.2966 0.7267 0.1020 0.143 Uiso 1 1 calc GR . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cl01 0.1208(10) 0.1189(13) 0.0768(8) 0.0344(8) -0.0160(7) 0.0267(9) O002 0.0605(13) 0.0620(17) 0.0628(15) -0.0050(12) -0.0141(11) -0.0008(12) O003 0.0913(18) 0.0687(19) 0.0543(15) 0.0030(13) 0.0069(13) 0.0269(16) O004 0.0767(16) 0.0722(19) 0.0507(14) -0.0008(13) 0.0030(11) -0.0217(15) C005 0.0588(16) 0.0452(17) 0.0419(16) -0.0032(14) -0.0045(12) 0.0026(14) O006 0.113(3) 0.057(2) 0.067(2) 0.000 -0.024(2) 0.000 C007 0.0582(17) 0.049(2) 0.0475(17) 0.0009(14) 0.0043(13) -0.0013(16) C008 0.0511(15) 0.054(2) 0.0466(17) 0.0038(15) 0.0033(12) -0.0040(14) C009 0.0556(15) 0.0482(18) 0.0439(17) 0.0015(14) 0.0006(12) 0.0008(15) C00A 0.0554(17) 0.057(2) 0.0456(17) -0.0029(16) -0.0008(13) -0.0073(15) C00B 0.071(2) 0.054(2) 0.0480(19) 0.0040(16) -0.0037(15) 0.0128(17) C00C 0.0602(18) 0.062(2) 0.0430(16) -0.0031(16) -0.0053(13) -0.0088(16) C00D 0.0690(19) 0.062(2) 0.0480(19) -0.0027(16) 0.0058(14) 0.0033(18) C00E 0.0621(19) 0.056(2) 0.0477(18) -0.0032(15) -0.0019(13) 0.0122(16) C00F 0.0694(19) 0.057(2) 0.0435(17) -0.0001(16) -0.0050(14) -0.0001(17) C00G 0.069(2) 0.059(2) 0.054(2) -0.0007(17) 0.0007(16) 0.0037(17) C00H 0.073(2) 0.0469(19) 0.053(2) -0.0019(15) 0.0080(15) -0.0005(16) C00I 0.070(2) 0.061(2) 0.073(3) 0.0033(19) -0.0024(18) 0.0091(18) C00J 0.086(2) 0.050(2) 0.049(2) 0.0047(16) -0.0027(17) 0.0126(19) C00K 0.081(3) 0.087(3) 0.046(2) -0.0026(19) 0.0014(17) 0.003(2) C00L 0.064(2) 0.076(3) 0.059(2) 0.020(2) -0.0034(16) 0.000(2) C00M 0.099(3) 0.105(4) 0.048(2) -0.001(2) 0.005(2) -0.021(3) C00N 0.113(4) 0.076(3) 0.055(2) -0.010(2) -0.006(2) -0.013(3) C00O 0.112(4) 0.107(4) 0.068(3) -0.011(3) -0.034(3) 0.027(3) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cl01 C00L 1.752(4) . ? O002 H002 0.8200 . ? O002 C005 1.405(4) . ? O003 C007 1.210(5) . ? O004 C00A 1.452(5) . ? O004 C00H 1.456(5) . ? C005 H005 0.9800 . ? C005 C007 1.529(4) . ? C005 C00C 1.524(5) . ? O006 H00W 0.8501 . ? O006 H00X 0.8500 . ? C007 C008 1.486(5) . ? C008 C00D 1.395(5) . ? C008 C00G 1.394(6) . ? C009 H009 0.9800 . ? C009 C00E 1.523(5) . ? C009 C00F 1.556(5) . ? C009 C00J 1.544(6) . ? C00A C00B 1.502(6) . ? C00A C00C 1.503(5) . ? C00A C00H 1.449(6) . ? C00B H00A 0.9700 . ? C00B H00B 0.9700 . ? C00B C00E 1.527(5) . ? C00C H00C 0.9700 . ? C00C H00D 0.9700 . ? C00D H00E 0.9300 . ? C00D C00K 1.370(7) . ? C00E H00F 0.9700 . ? C00E H00G 0.9700 . ? C00F C00M 1.506(6) . ? C00F C00N 1.533(7) . ? C00F C00O 1.533(6) . ? C00G H00H 0.9300 . ? C00G C00I 1.376(6) . ? C00H H00I 0.9800 . ? C00H C00J 1.517(5) . ? C00I H00J 0.9300 . ? C00I C00L 1.371(7) . ? C00J H00K 0.9700 . ? C00J H00L 0.9700 . ? C00K H00M 0.9300 . ? C00K C00L 1.360(8) . ? C00M H00N 0.9600 . ? C00M H00O 0.9600 . ? C00M H00P 0.9600 . ? C00N H00Q 0.9600 . ? C00N H00R 0.9600 . ? C00N H00S 0.9600 . ? C00O H00T 0.9600 . ? C00O H00U 0.9600 . ? C00O H00V 0.9600 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C005 O002 H002 109.5 . . ? C00A O004 C00H 59.8(2) . . ? O002 C005 H005 109.7 . . ? O002 C005 C007 109.5(3) . . ? O002 C005 C00C 110.4(3) . . ? C007 C005 H005 109.7 . . ? C00C C005 H005 109.7 . . ? C00C C005 C007 107.9(3) . . ? H00W O006 H00X 109.5 . . ? O003 C007 C005 119.4(3) . . ? O003 C007 C008 120.1(3) . . ? C008 C007 C005 120.4(3) . . ? C00D C008 C007 118.5(4) . . ? C00G C008 C007 123.0(3) . . ? C00G C008 C00D 118.5(4) . . ? C00E C009 H009 106.6 . . ? C00E C009 C00F 114.3(3) . . ? C00E C009 C00J 108.8(3) . . ? C00F C009 H009 106.6 . . ? C00J C009 H009 106.6 . . ? C00J C009 C00F 113.4(3) . . ? O004 C00A C00B 113.1(3) . . ? O004 C00A C00C 113.1(3) . . ? C00B C00A C00C 118.0(3) . . ? C00H C00A O004 60.2(3) . . ? C00H C00A C00B 118.8(3) . . ? C00H C00A C00C 119.1(3) . . ? C00A C00B H00A 108.9 . . ? C00A C00B H00B 108.9 . . ? C00A C00B C00E 113.3(3) . . ? H00A C00B H00B 107.7 . . ? C00E C00B H00A 108.9 . . ? C00E C00B H00B 108.9 . . ? C005 C00C H00C 108.9 . . ? C005 C00C H00D 108.9 . . ? C00A C00C C005 113.2(3) . . ? C00A C00C H00C 108.9 . . ? C00A C00C H00D 108.9 . . ? H00C C00C H00D 107.8 . . ? C008 C00D H00E 119.4 . . ? C00K C00D C008 121.2(4) . . ? C00K C00D H00E 119.4 . . ? C009 C00E C00B 110.7(3) . . ? C009 C00E H00F 109.5 . . ? C009 C00E H00G 109.5 . . ? C00B C00E H00F 109.5 . . ? C00B C00E H00G 109.5 . . ? H00F C00E H00G 108.1 . . ? C00M C00F C009 111.9(3) . . ? C00M C00F C00N 108.6(4) . . ? C00M C00F C00O 109.5(5) . . ? C00N C00F C009 109.4(3) . . ? C00O C00F C009 109.9(3) . . ? C00O C00F C00N 107.4(4) . . ? C008 C00G H00H 119.9 . . ? C00I C00G C008 120.2(4) . . ? C00I C00G H00H 119.9 . . ? O004 C00H H00I 115.4 . . ? O004 C00H C00J 116.1(3) . . ? C00A C00H O004 60.0(2) . . ? C00A C00H H00I 115.4 . . ? C00A C00H C00J 122.9(3) . . ? C00J C00H H00I 115.4 . . ? C00G C00I H00J 120.5 . . ? C00L C00I C00G 119.0(4) . . ? C00L C00I H00J 120.5 . . ? C009 C00J H00K 108.9 . . ? C009 C00J H00L 108.9 . . ? C00H C00J C009 113.5(3) . . ? C00H C00J H00K 108.9 . . ? C00H C00J H00L 108.9 . . ? H00K C00J H00L 107.7 . . ? C00D C00K H00M 120.7 . . ? C00L C00K C00D 118.6(4) . . ? C00L C00K H00M 120.7 . . ? C00I C00L Cl01 118.9(4) . . ? C00K C00L Cl01 118.6(4) . . ? C00K C00L C00I 122.5(4) . . ? C00F C00M H00N 109.5 . . ? C00F C00M H00O 109.5 . . ? C00F C00M H00P 109.5 . . ? H00N C00M H00O 109.5 . . ? H00N C00M H00P 109.5 . . ? H00O C00M H00P 109.5 . . ? C00F C00N H00Q 109.5 . . ? C00F C00N H00R 109.5 . . ? C00F C00N H00S 109.5 . . ? H00Q C00N H00R 109.5 . . ? H00Q C00N H00S 109.5 . . ? H00R C00N H00S 109.5 . . ? C00F C00O H00T 109.5 . . ? C00F C00O H00U 109.5 . . ? C00F C00O H00V 109.5 . . ? H00T C00O H00U 109.5 . . ? H00T C00O H00V 109.5 . . ? H00U C00O H00V 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O002 C005 C007 O003 -32.5(5) . . . . ? O002 C005 C007 C008 150.7(3) . . . . ? O002 C005 C00C C00A -53.2(4) . . . . ? O003 C007 C008 C00D -9.7(5) . . . . ? O003 C007 C008 C00G 169.4(4) . . . . ? O004 C00A C00B C00E -48.9(4) . . . . ? O004 C00A C00C C005 162.9(3) . . . . ? O004 C00A C00H C00J 103.4(4) . . . . ? O004 C00H C00J C009 81.1(4) . . . . ? C005 C007 C008 C00D 167.0(3) . . . . ? C005 C007 C008 C00G -13.9(5) . . . . ? C007 C005 C00C C00A -172.8(3) . . . . ? C007 C008 C00D C00K 178.3(4) . . . . ? C007 C008 C00G C00I -177.8(4) . . . . ? C008 C00D C00K C00L -0.9(7) . . . . ? C008 C00G C00I C00L -0.2(7) . . . . ? C00A O004 C00H C00J -114.5(4) . . . . ? C00A C00B C00E C009 -52.7(5) . . . . ? C00A C00H C00J C009 11.4(5) . . . . ? C00B C00A C00C C005 -61.7(5) . . . . ? C00B C00A C00H O004 -101.7(4) . . . . ? C00B C00A C00H C00J 1.8(5) . . . . ? C00C C005 C007 O003 87.7(4) . . . . ? C00C C005 C007 C008 -89.1(4) . . . . ? C00C C00A C00B C00E 175.8(3) . . . . ? C00C C00A C00H O004 101.5(3) . . . . ? C00C C00A C00H C00J -155.1(4) . . . . ? C00D C008 C00G C00I 1.3(6) . . . . ? C00D C00K C00L Cl01 -178.2(4) . . . . ? C00D C00K C00L C00I 2.1(7) . . . . ? C00E C009 C00F C00M -57.4(5) . . . . ? C00E C009 C00F C00N 63.0(4) . . . . ? C00E C009 C00F C00O -179.2(4) . . . . ? C00E C009 C00J C00H -43.6(4) . . . . ? C00F C009 C00E C00B -166.8(3) . . . . ? C00F C009 C00J C00H -172.1(3) . . . . ? C00G C008 C00D C00K -0.8(6) . . . . ? C00G C00I C00L Cl01 178.7(3) . . . . ? C00G C00I C00L C00K -1.6(7) . . . . ? C00H O004 C00A C00B 111.1(4) . . . . ? C00H O004 C00A C00C -111.4(4) . . . . ? C00H C00A C00B C00E 18.7(5) . . . . ? C00H C00A C00C C005 95.3(4) . . . . ? C00J C009 C00E C00B 65.3(4) . . . . ? C00J C009 C00F C00M 68.1(5) . . . . ? C00J C009 C00F C00N -171.4(4) . . . . ? C00J C009 C00F C00O -53.7(5) . . . . ? loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma _refln_scale_group_code 0 -6 5 394.488 97.7382 30 0 -6 6 251.82 79.3821 30 0 -6 7 62.5473 28.5149 30 0 -6 8 253.556 71.7454 30 0 -6 9 261.458 62.9858 11 0 -6 9 310.15 74.8623 30 0 -6 10 274.22 57.9166 11 0 -6 10 374.237 73.9118 30 0 -6 11 458.762 71.6673 30 0 -6 11 436.777 65.2931 11 0 -6 12 412.024 59.2109 30 0 -4 0 10169.8 958.205 6 0 -4 1 3477.47 557.738 6 0 -4 -1 3759.82 566.156 6 0 -4 1 3718.46 370.659 4 0 -4 2 7488.11 814.194 6 0 -4 2 6718.84 512.866 4 0 -4 -2 7363.48 768.913 6 0 -4 -3 3756.34 519.986 6 0 -4 3 3961.61 569.162 6 0 -4 3 3597.52 559.015 29 0 -4 3 3378.31 373.919 4 0 -4 -4 3724.14 498.579 6 0 -4 4 4687.1 607.255 6 0 -4 4 3843.18 417.809 4 0 -4 4 3828.33 604.017 29 0 -4 5 3198.11 412.016 4 0 -4 5 3034.74 480.699 6 0 -4 5 2881.81 516.654 29 0 -4 6 2990.05 536.928 29 0 -4 6 2833.78 460.128 6 0 -4 7 752.354 141.397 30 0 -4 7 1005.95 268.235 6 0 -4 7 1287.51 345.413 29 0 -4 7 921.632 148.469 11 0 -4 8 8249.29 459.311 30 0 -4 8 7238.45 424.551 11 0 -4 9 9022.26 478.012 30 0 -4 9 8937.97 461.31 11 0 -4 10 1773.51 191.123 11 0 -4 10 1821.13 207.394 30 0 -4 11 599.692 116.934 30 0 -4 11 557.212 104.888 11 0 -4 12 1357.24 166.136 30 0 -4 12 1323.58 159.651 14 0 -4 12 1316.93 151.636 11 0 -4 13 748.567 115.659 30 0 -4 13 715.881 113.932 14 0 -4 13 683.945 104.824 11 0 -4 14 398.276 80.0908 14 0 -4 14 298.879 70.6068 30 0 -4 14 423.45 78.667 11 0 -4 15 406.624 72.4218 14 0 -4 15 381.255 67.2733 11 0 -4 15 311.577 62.8822 30 0 -4 16 987.176 98.887 14 0 -4 16 954.712 93.692 11 0 -2 0 117072 2463.41 4 0 -2 -1 10180.9 474.808 4 0 -2 1 11157.4 487.877 4 0 -2 2 88752.8 1889.9 4 0 -2 -2 85286.6 1908.83 4 0 -2 -3 118432 2553.76 4 0 -2 -3 114961 2229.68 3 0 -2 -4 25156.8 936.2 6 0 -2 4 27546.5 1165.28 29 0 -2 4 25739.7 878.921 4 0 -2 5 48388 1758.66 29 0 -2 5 51993.8 1593.75 6 0 -2 -5 48033.2 1364.88 6 0 -2 5 53496.1 1490.22 4 0 -2 6 21598 960.576 6 0 -2 6 20742.8 1125.82 29 0 -2 7 15100.3 793.191 6 0 -2 7 16726 1037.44 29 0 -2 -8 8192.84 666.961 2 0 -2 8 8368.88 762.804 29 0 -2 9 7254.06 749.188 29 0 -2 -9 6145.3 631.525 2 0 -2 10 22922.5 1433.98 29 0 -2 -10 20673.9 1352.34 27 0 -2 11 6861.28 795.082 29 0 -2 -11 5468.97 714.826 27 0 -2 11 5405.86 323.909 11 0 -2 12 1359.48 159.26 11 0 -2 13 879.646 127.953 11 0 -2 13 870.782 140.489 22 0 -2 14 660.088 110.719 11 0 -2 14 1059.42 152.531 22 0 -2 15 313.466 76.1316 11 0 -2 15 336.309 85.6436 22 0 -2 15 476.797 98.7525 14 0 -2 16 590.596 103.496 22 0 -2 16 766.649 115.865 14 0 -2 17 807.885 112.18 14 0 -2 18 758.582 96.0075 14 0 0 3 26837.9 786.366 29 0 0 3 25109.1 806.523 28 0 0 -3 22783.7 691.301 2 0 0 3 21913.9 544.541 7 0 0 4 114310 2196.83 7 0 0 4 130338 2591.17 29 0 0 4 126216 2657.44 28 0 0 -4 120565 2461.35 2 0 0 -4 113897 2172.86 26 0 0 5 126672 2853.79 28 0 0 -5 130558 2682.38 2 0 0 5 126666 2879.75 25 0 0 5 127163 2375.51 7 0 0 5 130421 2796.12 29 0 0 6 6797.7 501.06 25 0 0 -6 5459.46 392.865 2 0 0 6 7136.67 506.965 28 0 0 -6 3296 199 26 0 0 6 6948.06 466.459 29 0 0 6 5071.16 374.24 5 0 0 6 4091.84 234.327 7 0 0 7 189261 4334.02 25 0 0 7 194321 4221.62 29 0 0 -7 201470 4151.75 2 0 0 8 227967 4991.36 25 0 0 8 211693 4791.77 29 0 0 -8 223987 4710.98 2 0 0 9 4627.5 474.515 29 0 0 -9 5131.4 472.874 2 0 0 -9 4956.91 564.136 27 0 0 9 5156.01 462.044 5 0 0 9 4539.44 497.386 25 0 0 -9 4973.73 489.356 1 0 0 10 4003.55 470.669 29 0 0 -10 4515.28 494.273 1 0 0 10 4700.88 534.855 25 0 0 -10 4644.96 587.303 27 0 0 10 5306.25 506.703 5 0 0 -11 6171.85 624.526 1 0 0 -11 5665.36 691.268 27 0 0 11 5298.21 604.481 25 0 0 11 6170.46 590.048 5 0 0 12 96.5073 52.6501 22 0 0 12 -26.5401 50.3121 25 0 0 -12 2.07204 18.3658 1 0 0 12 14.1109 32.2094 5 0 0 13 3127.33 251.414 14 0 0 13 3258.83 278.775 22 0 0 14 4031.52 311.323 22 0 0 14 3914.07 287.359 14 0 0 15 292.612 72.6 14 0 0 15 391.965 94.8954 22 0 0 16 555.593 104.929 14 0 0 16 477.368 106.276 22 0 0 17 230.505 62.085 14 0 0 17 285.879 76.5844 22 0 0 18 286.565 69.6135 22 0 0 19 83.7393 34.0514 22 0 2 0 109481 2121.26 1 0 2 0 112523 2451.75 8 0 2 -1 6942.04 294.76 27 0 2 1 6809.61 325.52 25 0 2 -1 9163.78 368.787 1 0 2 1 8237.8 449.029 8 0 2 1 8186.99 514.808 24 0 2 -1 8838.23 456.641 8 0 2 2 89057.5 1936.08 8 0 2 -2 79388.3 1681.94 27 0 2 2 92356.9 2021.02 24 0 2 2 85411.3 1847.36 25 0 2 -2 93656.8 1844.64 1 0 2 -2 86616.4 1879.51 8 0 2 3 128973 2843.35 5 0 2 3 137731 2872.69 24 0 2 -3 129796 2843.41 1 0 2 -3 126854 2752.48 8 0 2 -3 128780 2898.18 2 0 2 3 135338 2861.33 8 0 2 -3 126443 2708.88 27 0 2 3 127529 2913.42 25 0 2 4 24064.5 932.203 5 0 2 4 28320.4 973.307 24 0 2 -4 23935.6 990.112 2 0 2 4 24699.9 948.411 8 0 2 -4 21760.8 832.487 8 0 2 4 24421.3 1021.92 25 0 2 -4 26073 960.345 27 0 2 5 52848.4 1596.85 8 0 2 -5 55251 1709.58 27 0 2 5 49409.9 1566.72 5 0 2 -5 52687.1 1700.99 2 0 2 5 53443.2 1505.43 24 0 2 5 49890.7 1672.42 25 0 2 6 20938.5 883.679 24 0 2 -6 17812.1 1025.19 27 0 2 -6 22903.7 1113.48 2 0 2 6 19280.9 1010.28 25 0 2 -6 23096.1 1058.07 1 0 2 6 21998.9 1022.33 5 0 2 6 22622.4 1010.57 8 0 2 -7 16329.7 921.517 1 0 2 7 14193 886.663 25 0 2 7 14175.3 865.902 8 0 2 -7 12853 938.227 27 0 2 7 15779.6 937.003 5 0 2 -7 14116.8 933.952 2 0 2 -8 6840.12 734.438 27 0 2 8 7435.05 700.572 5 0 2 -8 7620.19 710.285 2 0 2 8 7065.05 649.238 25 0 2 -8 8623.19 694.278 1 0 2 8 9692.98 762.978 8 0 2 -9 5409.79 694.827 27 0 2 -9 6262.48 614.764 1 0 2 9 5347.17 640.651 5 0 2 -9 5943.01 647.103 2 0 2 9 5535.31 601.334 25 0 2 10 26243.1 1536.87 5 0 2 -10 25943.9 1368.36 1 0 2 -10 25075 1405.89 2 0 2 -10 21614.5 1489.94 27 0 2 10 20242.2 1265.25 25 0 2 11 7729.84 839.652 5 0 2 11 5551.19 317.93 13 0 2 -11 7115.89 726.736 1 0 2 11 5991.8 326.556 16 0 2 11 4934.84 626.291 25 0 2 -11 5738.87 769.507 27 0 2 12 1477.73 178.966 22 0 2 12 1530.48 160.923 13 0 2 13 530.799 91.7324 13 0 2 13 500.32 103.664 22 0 2 14 994.527 132.542 13 0 2 14 877.546 134.702 22 0 2 15 560.322 110.084 22 0 2 15 536.47 97.44 13 0 2 16 536.821 99.8269 22 0 2 16 711.598 104.856 13 0 2 17 926.983 113.022 13 0 2 17 652.133 101.702 22 0 2 18 997.492 103.167 13 0 2 18 715.453 95.025 22 0 4 0 11106.2 911.465 24 0 4 0 14010.9 936.128 8 0 4 -1 3908.22 492.951 8 0 4 1 3883.45 518.899 24 0 4 1 4513.96 518.976 8 0 4 -1 3596.18 515.385 24 0 4 2 7580.33 684.585 8 0 4 -2 7613.08 704.466 8 0 4 -2 7759.42 785.86 24 0 4 2 7348.52 719.328 24 0 4 3 4443.79 525.669 8 0 4 3 3548.06 491.589 24 0 4 -3 3794.57 559.52 24 0 4 -4 3377.78 559.446 24 0 4 4 3713.63 495.436 8 0 4 5 3339.77 486.035 8 0 4 -5 3649.55 624.463 24 0 4 -6 3620.24 660.514 24 0 4 6 2522.19 441.922 8 0 4 7 762.082 125.796 17 0 4 -7 681.29 124.564 23 0 4 7 870.712 135.373 9 0 4 7 805.415 117.262 21 0 4 8 8838.91 411.941 21 0 4 8 8298.33 424.252 17 0 4 -8 8163.21 419.682 12 0 4 9 7633.25 390.738 13 0 4 9 8177.29 408.753 21 0 4 -9 8202.46 419.584 12 0 4 9 8530.78 421.04 17 0 4 9 8254.25 434.891 9 0 4 10 1877.93 181.101 13 0 4 10 1735.16 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217.965 30 2 -4 9 307.017 86.2724 30 2 -4 9 316.09 80.5192 11 2 -4 10 2866.17 244.977 11 2 -4 10 3005.28 259.037 30 2 -4 11 223.252 67.5592 30 2 -4 11 203.769 55.9168 11 2 -4 11 252.04 78.6435 14 2 -4 12 -14.6262 35.2435 30 2 -4 12 10.4076 29.598 11 2 -4 12 44.2231 31.8366 14 2 -4 13 525.973 90.4477 11 2 -4 13 676.18 109.626 14 2 -4 13 608.759 103.441 30 2 -4 14 184.257 48.0043 14 2 -4 14 256.642 65.3795 30 2 -4 14 201.69 53.4037 11 2 -4 15 933.418 105.275 11 2 -4 15 957.259 110.823 14 2 -4 15 879.229 103.829 30 2 -4 16 328.002 54.2238 14 2 -4 16 288.561 51.2205 11 -2 -2 18 105 37.1768 14 -2 -2 17 104.511 41.5336 14 -2 -2 17 74.0561 33.2946 22 -2 -2 16 283.724 71.8423 22 -2 -2 16 389.29 84.1851 14 -2 -2 15 1710.41 186.301 22 -2 -2 15 1949.85 182.517 11 -2 -2 14 164.691 64.1004 22 -2 -2 14 102.57 48.4531 11 -2 -2 13 4396.61 299.706 11 -2 -2 13 4283.87 323.019 22 -2 -2 12 13549.9 598.815 22 -2 -2 12 13902.1 563.041 11 -2 -2 11 5343.91 324.584 11 -2 -2 11 4945.13 704.577 29 -2 -2 10 2020.05 433.462 29 2 -2 -10 2067.73 400.414 2 2 -2 -9 7953.04 763.785 2 -2 -2 9 9613.04 905.332 29 2 -2 -8 5416.72 561.733 2 2 -2 -8 4897.96 489.09 26 -2 -2 8 4179.86 577.832 29 2 -2 -7 10344.6 700.412 26 -2 -2 7 8310.83 756.62 29 -2 -2 6 31069.1 1447.52 29 2 -2 -6 33522.5 1325.76 26 -2 -2 5 14244.3 670.121 4 2 -2 -5 12015.5 566.161 6 -2 -2 4 21759.2 1097.33 28 2 -2 -4 22103.9 830.006 6 -2 -2 4 21965.2 802.591 4 2 -2 -3 32496.9 919.395 4 -2 -2 3 32533.2 1322.71 28 -2 -2 3 30802 831.443 25 2 -2 -2 23575.4 709.491 4 -2 -2 2 21716.3 566.26 25 2 -2 -2 28094.6 1024.1 6 -2 -2 2 26033.4 864 3 -2 -2 2 25633 852.176 4 2 -2 -1 126043 2572.67 29 2 -2 -1 128855 3035.96 6 -2 -2 1 130645 2718.46 3 2 -2 -1 131778 2569.75 4 -2 -2 0 13074.5 533.63 3 2 -2 0 10961 660.075 6 2 -2 0 11361.9 423.545 4 -2 -2 0 12459 570.045 4 -2 -2 -1 3608.93 260.621 3 2 -2 1 3196.2 211.862 4 2 -2 1 3801.75 356.115 29 -2 -2 -1 3326.2 284.592 4 2 -2 1 2904.56 334.66 6 -2 -2 -2 24519.9 878.726 4 2 -2 2 24832 755.513 4 -2 -2 -2 25641.9 788.619 3 2 -2 2 27280.9 1114.7 29 2 -2 2 28218.4 1096.68 6 -2 -2 -2 23557.1 674.089 27 2 -2 3 6364.08 381.19 26 2 -2 3 6672.31 374.66 4 -2 -2 -3 5458.65 371.683 27 -2 -2 -3 5795.49 407.192 4 2 -2 3 6306.63 531.587 29 -2 -2 -3 6098.72 363.2 3 2 -2 4 31007.4 985.65 26 -2 -2 -4 38567.7 1307.41 27 2 -2 4 45796.9 1407.35 6 2 -2 4 50162.7 1651.2 29 -2 -2 -4 38290.8 1227.14 4 -2 -2 -4 37517.3 1104.51 3 -2 -2 -5 16091.3 897.081 27 -2 -2 -5 17824.6 733.838 3 2 -2 6 4657.13 407.738 6 -2 -2 -6 3522.07 435.635 27 2 -2 6 4749.32 515.524 29 -2 -2 -7 31294.4 1483.66 27 2 -2 7 33223.1 1244.63 6 2 -2 8 8730.17 768.087 29 -2 -2 -8 7519.91 737.547 27 -2 -2 -9 3217.14 497.519 27 2 -2 9 4964.62 608.842 29 -2 -2 -10 7190.42 795.957 27 2 -2 10 7925.27 805.508 29 2 -2 11 1316.15 153.733 11 2 -2 11 1639.41 382.028 29 -2 -2 -11 1246.82 341.732 27 2 -2 11 1844.48 345.379 5 2 -2 12 1089.79 143.894 11 2 -2 12 1326.41 171.2 30 2 -2 13 10143.2 466.249 11 2 -2 13 10579.2 490.682 14 2 -2 14 173.708 58.8898 14 2 -2 14 112.211 50.9526 11 2 -2 15 153.562 57.0054 14 2 -2 16 2018.46 190.563 14 2 -2 17 37.5806 25.0493 14 2 -2 18 1308.88 125.187 14 -2 0 19 461.837 75.1627 22 -2 0 18 59.592 40.3795 22 -2 0 17 107.144 51.529 22 -2 0 16 -8.86623 28.3971 14 -2 0 16 26.6797 28.0361 22 -2 0 15 3682.06 294.516 22 -2 0 15 2022.13 206.788 14 -2 0 14 -3.93177 25.9008 22 -2 0 13 2429.52 245.747 22 2 0 -12 171.792 108.897 1 -2 0 12 252.972 88.6314 22 2 0 -12 308.461 169.507 27 -2 0 12 306.851 137.817 5 -2 0 11 4140.18 472.014 5 2 0 -11 3552.27 551.069 27 2 0 -11 3940.06 508.772 1 -2 0 11 3317.53 489.841 25 2 0 -11 4459.53 522.273 2 -2 0 10 3722.53 420.549 5 -2 0 10 4602.15 553.268 25 2 0 -10 4162.31 464.404 2 -2 0 9 10454.8 805.352 25 -2 0 9 9202.84 680.484 29 -2 0 9 9306.31 747.215 28 -2 0 9 11066.7 681.007 5 2 0 -9 10495.4 710.361 2 -2 0 8 15770.6 850.519 29 2 0 -8 19490.5 923.72 2 -2 0 8 16414.5 962.854 28 -2 0 8 19335.5 869.889 5 -2 0 8 18368 1024.89 25 -2 0 7 43661.5 1608.1 28 -2 0 7 50066.9 1453.57 5 -2 0 7 46276.3 1654.34 25 2 0 -7 49948.4 1516.57 2 -2 0 7 44879.3 1478.5 29 -2 0 6 26470.3 907.139 5 -2 0 6 21751.6 995.154 25 2 0 -6 25829.2 935.419 2 -2 0 6 21359.8 880.156 29 -2 0 6 22011.1 989.194 28 -2 0 5 43515.7 1271.86 29 -2 0 5 45067 1414.63 28 -2 0 5 44437 1387.33 25 2 0 -4 24086.9 891.975 26 -2 0 4 42606.5 1152.79 28 2 0 -3 11141.7 513.067 26 2 0 -2 7669.39 197.513 7 -2 0 2 8123.1 292.42 3 -2 0 1 9480.97 271.468 4 2 0 -1 9947.1 284.797 7 2 0 1 40235.5 800.044 5 -2 0 -1 44497.7 827.432 24 2 0 2 21116.6 566.205 5 2 0 2 21484.5 486.618 8 2 0 3 33394.6 924.268 5 -2 0 -3 34489.8 791.283 2 2 0 3 35948.3 763.992 8 2 0 4 455.06 94.6574 5 2 0 4 404.366 106.78 29 2 0 4 609.717 80.7825 6 2 0 4 644.385 106.476 7 -2 0 -4 469.545 102.736 1 2 0 4 451.146 68.4873 8 2 0 4 445.692 102.985 25 -2 0 -4 387.66 74.0651 2 2 0 5 5198.53 366.876 5 -2 0 -5 4421.43 296.081 2 2 0 5 5171.81 239.208 6 2 0 5 4215.5 373.826 29 -2 0 -5 3961.94 388.721 27 2 0 5 5402.96 327.574 7 -2 0 -5 4403.85 359.054 1 2 0 5 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265.691 14 2 0 15 1459.18 170.88 14 2 0 15 1569.51 189.112 22 2 0 16 1020.12 140.976 14 2 0 16 1180.07 158.69 22 2 0 17 257.001 69.6118 14 2 0 17 296.286 78.7444 22 2 0 18 114.529 49.9373 22 2 0 19 618.664 85.5502 22 -2 2 18 70.8717 29.8827 22 -2 2 18 167.319 43.2447 13 -2 2 17 64.9149 34.9415 13 -2 2 17 105.61 45.9841 22 -2 2 16 352.657 81.6119 22 -2 2 16 220.722 57.7608 13 -2 2 15 1997.89 199.319 22 -2 2 15 2000.48 186.154 13 -2 2 14 283.399 79.1695 22 -2 2 14 207.854 65.3053 13 -2 2 14 157.214 51.7507 21 -2 2 13 5372.88 300.582 21 -2 2 13 4857.83 309.643 16 -2 2 13 5179.75 318.667 13 -2 2 13 4375.78 315.212 22 -2 2 12 15187.4 578.219 16 -2 2 12 14480.8 565.052 13 -2 2 12 13187.8 577.541 22 -2 2 11 4662.4 644.091 5 -2 2 11 3977.16 568.543 25 -2 2 11 4268.66 279.828 13 2 2 -11 5256.43 617.767 1 -2 2 11 3789.55 288.816 22 -2 2 11 4312.26 281.43 16 -2 2 11 5309.15 302.767 21 2 2 -11 5296.47 653.143 2 2 2 -10 2740.81 458.467 2 -2 2 10 1632.39 342.381 25 2 2 -10 2333.33 387.781 1 -2 2 10 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3 9 11684.5 490.254 13 3 3 10 4622.79 291.962 13 3 3 10 4396.51 284.846 17 3 3 10 4502.85 289.036 9 3 3 11 4630.72 290.368 13 3 3 11 4475.69 286.321 17 3 3 11 4370.17 278.784 9 3 3 12 1901.94 178.614 13 3 3 12 1736 168.224 9 3 3 13 1022.9 124.322 9 3 3 13 1107.55 134.653 13 3 3 14 161.262 51.8941 13 3 3 14 99.4826 36.6031 9 3 3 15 1925.61 168.509 13 3 3 16 1152.3 125.681 13 -3 5 14 245.007 44.7088 21 -3 5 13 42.5942 24.9273 13 -3 5 13 121.863 42.5563 21 -3 5 12 1848.15 154.682 21 3 5 -12 1461.83 136.286 12 3 5 -11 1324.68 140.273 12 -3 5 11 1588.04 150.099 17 3 5 -10 1275.05 144.639 12 -3 5 10 1606.38 158.168 17 -3 5 10 1442.08 160.759 21 -3 5 9 552.023 102.525 21 -3 5 9 790.119 120.247 17 3 5 -9 687.633 111.449 12 -3 5 8 564.262 106.573 9 -3 5 8 467.739 97.2611 17 3 5 -8 393.787 88.246 12 -3 5 8 318.342 72.8585 21 -3 5 7 1261.07 155.657 21 -3 5 7 1214.58 160.51 9 -3 5 7 1217.97 163.635 17 3 5 -7 1114.67 157.518 23 3 5 -6 3371.16 277.023 23 3 5 -6 3827.63 298.958 10 -3 5 6 3735.47 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30 -4 -4 7 652.131 126.741 30 -4 -4 7 840.762 141.824 11 -4 -4 6 149.405 67.3417 11 4 -4 -6 99.4867 97.2637 26 -4 -4 6 256.672 159.588 29 -4 -4 6 196.548 73.6316 30 -4 -4 6 26.7007 42.9673 4 4 -4 -5 -46.3516 64.6091 26 -4 -4 5 -53.3847 52.9472 4 4 -4 -4 2234.41 436.583 26 -4 -4 4 2378.95 342.241 4 4 -4 -3 8715.67 875.053 26 4 -4 -3 9212.03 800.412 6 -4 -4 3 8569.63 650.005 4 4 -4 -2 8070.47 772.47 6 4 -4 -2 5958.41 712.95 26 -4 -4 2 7432.55 610.971 4 4 -4 -1 49.0136 74.3379 6 -4 -4 1 163.691 83.9551 4 4 -4 -1 73.7562 164.221 26 -4 -4 0 1049.99 236.262 4 4 -4 0 1255.98 296.586 6 4 -4 0 1427.43 310.901 26 4 -4 1 9390.13 900.245 6 -4 -4 -1 11539.6 821.124 4 4 -4 1 11157.7 885.037 26 4 -4 2 4615.49 530.016 26 4 -4 2 4299.13 598.985 6 -4 -4 -2 3872.47 482.772 4 -4 -4 -3 374.891 134.19 4 4 -4 3 808.737 254.058 6 -4 -4 -4 2215.35 370.308 4 4 -4 4 2360.92 431.11 6 4 -4 5 10846.3 923.856 6 -4 -4 -5 9319.65 795.538 4 4 -4 6 8944.8 476.769 11 4 -4 6 9970.35 528.485 30 -4 -4 -6 10308.6 859.686 4 4 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3948.48 567.941 2 -4 -2 10 3083.37 558.108 29 4 -2 -9 4221.89 583.942 2 -4 -2 9 4904.51 677.334 29 4 -2 -8 10144.1 774.261 26 -4 -2 8 8846.95 860.034 29 4 -2 -8 10198.6 817.153 2 -4 -2 8 8974.24 831.69 28 4 -2 -7 7058.4 619.121 26 -4 -2 7 5729.98 509.917 4 4 -2 -7 6272.46 586.16 2 -4 -2 7 5848.64 644.218 28 4 -2 -6 2006.22 326.725 26 -4 -2 6 1919.54 263.76 4 -4 -2 6 2035.2 362.526 28 -4 -2 5 46540.9 1408.87 4 -4 -2 5 49330 1905.38 28 -4 -2 4 4943.45 542.896 28 4 -2 -4 5330.26 392.198 6 -4 -2 4 4552.53 340.684 25 -4 -2 4 5602.14 393.342 4 4 -2 -3 15038.6 718.828 6 -4 -2 3 14765.1 910.722 28 4 -2 -3 15847.5 877.758 26 -4 -2 3 13980.8 640.523 4 -4 -2 3 14888.8 700.075 3 4 -2 -2 24185.8 972.184 6 -4 -2 2 21825.4 1082.59 28 -4 -2 2 21751.7 830.726 4 -4 -2 2 21505.3 846.449 3 4 -2 -2 20761.9 998.307 26 -4 -2 1 14466.9 652.297 3 4 -2 -1 15553.7 784.314 6 4 -2 -1 11182.5 443.653 29 -4 -2 1 10670.2 687.746 28 -4 -2 1 12956 628.493 4 4 -2 -1 15059.6 779.454 26 -4 -2 0 15173 663.823 3 -4 -2 0 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549.193 24 -7 3 4 16569.9 1116.65 24 7 3 -4 17785.9 1100.83 2 -7 3 3 6505.61 660.448 24 7 3 -3 6420.76 609.908 2 -7 3 2 11705.9 889.489 24 7 3 -2 12998.7 825.746 7 -7 3 2 11543.7 831.867 28 -7 3 1 3104.17 440.215 24 7 3 -1 2679.15 379.318 8 7 3 -1 3316.14 408.216 7 -7 3 0 16380.3 1045.18 24 7 3 0 18131.8 1010.18 8 7 3 0 18875.4 1022.54 7 -7 3 -1 3535.18 473.451 24 7 3 1 4273.24 478.695 8 7 3 1 3935.87 471.591 7 -7 3 -2 526.673 196.926 24 7 3 2 311.693 127.777 8 7 3 2 412.475 148.648 7 -7 3 -2 321.378 150.083 27 -7 3 -2 203.338 105.857 1 -7 3 -3 1083.21 269.344 24 7 3 3 1097.5 256.258 7 7 3 3 1360.86 275.87 8 -7 3 -3 1012.5 228.789 1 -7 3 -3 915.113 252.752 27 -7 3 -4 3871.65 539.887 24 7 3 4 3447.71 489.859 7 -7 3 -4 3830.36 469.459 1 -7 3 -4 3106.47 443.477 27 7 3 4 4286.6 510.615 8 -7 3 -5 7014.09 772.942 24 7 3 5 7371.55 731.808 7 -7 3 -5 7368.95 700.645 1 -7 3 -5 6386.75 666.493 27 7 3 5 8175.77 723.997 8 -7 3 -6 2178.36 455.009 24 7 3 6 3459.03 505.794 7 -7 3 -6 3263.28 505.058 1 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342.829 61.5399 21 7 5 -11 45.1175 31.7874 12 -7 5 11 43.9252 33.9488 21 -7 5 10 430.127 89.456 21 -7 5 9 379.271 83.5711 21 7 5 -9 224.149 57.6167 10 -7 5 8 927.397 128.047 21 7 5 -8 1169.7 141.116 10 -7 5 7 -21.5639 44.7693 21 7 5 -7 14.8939 24.1095 10 7 5 -6 964.224 142.204 23 -7 5 6 744.576 119.752 21 -7 5 6 781.51 126.017 20 7 5 -6 1053.18 148.272 10 7 5 -5 675.524 121.409 23 -7 5 5 724.098 116.408 21 -7 5 5 805.995 128.292 20 7 5 -5 743.658 128.903 10 7 5 -4 850.409 132.754 23 -7 5 4 853.525 123.329 21 -7 5 4 883.337 128.77 20 7 5 -4 948.656 150.563 10 7 5 -3 2787.23 248.332 23 -7 5 3 3037.14 237.304 21 -7 5 3 2927.6 236.472 20 7 5 -3 2961.05 269.905 10 7 5 -2 3127.3 264.896 23 -7 5 2 3250.1 245.855 21 -7 5 2 3365.16 253.776 20 7 5 -2 3269.57 285.572 10 7 5 -1 180.818 72.5829 23 -7 5 1 208.601 60.8058 21 7 5 -1 296.852 93.2113 10 7 5 0 2851.41 257.431 23 7 5 0 2992.48 256.149 10 -7 5 -1 1926.09 192.221 12 7 5 1 2090.13 226.853 23 7 5 1 2170.31 209.311 10 7 5 2 160.581 64.457 23 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241.534 54.7921 23 7 7 -3 156.779 36.504 21 -7 7 3 275.723 49.9511 20 7 7 -2 -13.4772 19.4314 21 -7 7 2 19.5578 13.8071 20 7 7 -1 108.472 33.6392 21 -7 7 1 186.424 48.9143 20 7 7 -1 168.653 49.9519 23 7 7 0 1420.13 141.271 23 7 7 0 1128.21 98.7165 21 7 7 1 18.0943 26.5295 23 7 7 1 8.08178 13.1969 21 -7 7 -1 59.9013 34.5325 20 7 7 2 401.474 76.8749 23 7 7 2 283.141 45.3413 21 -7 7 -2 394.818 72.3408 20 7 7 3 68.648 37.6022 23 -7 7 -3 24.2527 18.5247 20 -7 7 -4 32.6991 23.9938 20 -8 -6 10 165.013 39.2626 30 -8 -6 9 116.021 38.0943 30 -8 -6 8 110.255 39.986 30 -8 -6 7 199.372 60.4896 30 -8 -6 6 201.22 60.7458 30 -8 -6 5 1359.14 164.861 30 -8 -6 4 294.224 81.9846 30 8 -6 8 252.141 55.5904 11 8 -6 9 181.453 43.6756 11 -8 -4 15 225.658 43.8329 11 -8 -4 15 221.686 44.5548 14 -8 -4 14 84.3222 35.8617 11 -8 -4 14 13.6 16.2487 30 -8 -4 13 242.786 58.1865 11 -8 -4 13 163.712 50.4525 30 -8 -4 12 187.043 60.3777 11 -8 -4 12 142.311 53.8593 30 -8 -4 11 92.0046 45.2059 11 -8 -4 11 71.3751 40.9986 30 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628.013 118.824 11 8 -4 9 742.249 131.368 30 8 -4 10 2278.01 213.91 11 8 -4 10 2226.09 216.185 30 8 -4 11 1305.92 150.998 11 8 -4 12 375.589 74.7852 11 8 -4 13 710.535 96.0868 11 8 -4 14 489.027 73.4329 11 8 -4 15 277.546 44.2508 11 8 -4 15 299.823 51.5634 19 -8 -2 17 366.184 59.1503 22 -8 -2 17 493.598 69.0363 14 -8 -2 16 118.442 40.0018 22 -8 -2 15 566.741 102.359 22 -8 -2 15 343.205 68.7072 11 -8 -2 14 2717.84 242.403 22 -8 -2 14 2583.12 207.321 11 -8 -2 14 2202.07 240.794 18 -8 -2 13 3461.58 258.797 11 -8 -2 13 2913.26 283.314 18 -8 -2 12 4165.34 299.954 11 -8 -2 12 4619.28 370.006 18 -8 -2 11 631.188 139.824 18 -8 -2 11 561.896 113.696 11 -8 -2 10 3226.66 299.998 30 -8 -2 10 4553.81 375.777 18 -8 -2 9 2051.39 242.17 18 -8 -2 9 1447.38 194.278 30 -8 -2 9 1279.98 343.635 29 -8 -2 9 1564.76 402.365 28 8 -2 -8 12172.5 1004.6 2 -8 -2 8 10726.4 1020.49 28 8 -2 -7 3326.59 489.5 2 8 -2 -7 2824.91 537.104 26 -8 -2 7 3942.78 445.565 4 -8 -2 7 3002.29 524.383 28 8 -2 -6 3660.82 483.734 2 -8 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13629.9 875.523 6 -8 -2 -2 12572 771.013 3 8 -2 2 12889.1 818.223 29 8 -2 2 12123.4 849.165 26 -8 -2 -3 28375.8 1220.86 4 8 -2 3 34096 1421.39 6 -8 -2 -3 32583 1312.06 3 8 -2 3 31832.6 1435.71 29 8 -2 3 30039.8 1383.74 26 8 -2 4 17045.3 949.457 6 -8 -2 -4 15774 908.116 3 8 -2 4 15126.7 1028.67 29 -8 -2 -5 8409.84 673.759 4 8 -2 5 10299.5 717.989 6 -8 -2 -5 9639.03 737.871 3 8 -2 5 8623.46 837.062 29 -8 -2 -6 6294.62 618.233 4 8 -2 6 6871.78 586.689 6 -8 -2 -6 6157.8 636.71 3 8 -2 6 6486.85 763.986 29 8 -2 7 33.4156 41.7992 6 -8 -2 -7 81.0408 105.681 3 8 -2 7 265.563 157.499 29 -8 -2 -7 30.592 52.3422 4 -8 -2 -8 5493.81 664.708 4 -8 -2 -8 4662.93 626.08 3 8 -2 8 5138.95 728.889 29 8 -2 9 4834.67 574.258 7 8 -2 9 4137.51 300.891 11 8 -2 9 3975.37 300.847 30 8 -2 9 4017.3 654.747 29 8 -2 9 3768.93 314.1 14 8 -2 10 1352.3 166.414 11 8 -2 10 1179.62 177.526 14 8 -2 11 1986.82 201.712 11 8 -2 11 2130.14 236.752 14 8 -2 12 931.181 134.511 11 8 -2 12 965.444 151.577 14 8 -2 13 2661.04 239.656 14 8 -2 13 1873.36 184.54 11 8 -2 14 662.571 101.385 11 8 -2 14 497.51 100.078 14 8 -2 15 39.6321 27.7621 19 8 -2 15 46.2537 38.3944 14 8 -2 16 223.704 57.145 19 8 -2 16 261.232 61.4592 14 8 -2 17 914.255 93.082 19 8 -2 17 1116.78 109.316 14 -8 0 18 160.624 44.1515 22 -8 0 17 216.754 55.3948 22 -8 0 16 1.13175 24.3467 22 -8 0 15 588.656 116.335 22 -8 0 14 15.0327 32.987 22 -8 0 13 2229.63 259.118 18 -8 0 13 3623.21 266.254 13 -8 0 12 1743.39 230.988 18 -8 0 12 1469.29 174.349 13 -8 0 11 4074.7 292.602 16 -8 0 11 4195.74 303.41 13 8 0 -10 1220.61 296.21 2 -8 0 10 1607.28 409.628 28 -8 0 10 1616.69 402.197 25 8 0 -9 127.555 101.075 2 -8 0 9 254.225 153.581 28 -8 0 9 394.599 188.76 25 8 0 -8 11674.3 844.445 2 -8 0 8 9895.05 926.9 28 -8 0 8 10908.6 941.02 25 8 0 -7 2089.57 344.51 2 -8 0 7 1499.48 314.208 25 8 0 -7 1147.71 255.575 26 -8 0 7 1370.34 307.31 28 8 0 -6 12972 847.606 2 -8 0 6 13208.1 917.822 28 8 0 -6 11975.3 869.424 26 -8 0 6 13477.6 893.014 25 8 0 -5 28120.9 1231.7 2 -8 0 5 23399.3 970.206 3 8 0 -5 24243.2 1255.66 26 -8 0 5 24441 1210.75 28 -8 0 5 24249.5 1159.63 25 -8 0 4 23349.3 1132.68 28 8 0 -4 25400.3 1144.34 2 -8 0 4 20697.1 864.596 3 8 0 -4 19262.6 1131.14 26 -8 0 3 824.441 118.25 4 8 0 -3 1058.23 164.08 7 -8 0 3 971.251 171.748 3 8 0 -3 1003.57 205.746 2 8 0 -3 1236.12 276.378 26 8 0 -2 8707.83 499.11 7 8 0 -2 8780.66 588.7 2 -8 0 2 8194.06 492.491 3 -8 0 2 9497.52 642.579 28 8 0 -2 8655.63 673.785 26 8 0 -1 53293.7 1495.39 7 8 0 -1 55891.9 1533.33 2 -8 0 1 49265 1428.46 3 -8 0 1 49759.1 1614.11 28 8 0 -1 53757.2 1732.89 26 -8 0 0 44.438 51.728 1 -8 0 0 84.3948 52.0206 3 -8 0 0 37.5315 22.2268 4 8 0 0 118.561 84.1098 7 8 0 0 23.4699 38.7837 2 8 0 0 45.8302 92.5186 26 -8 0 0 31.0309 49.4279 28 -8 0 -1 8256.5 451.291 4 8 0 1 8901.13 410.024 2 8 0 1 9292.36 627.178 7 8 0 1 8788.09 625.419 6 -8 0 -1 9457.4 569.719 3 -8 0 -1 9220.75 590.65 1 8 0 1 8538.16 586.181 26 -8 0 -2 170.136 74.9174 4 8 0 2 207.849 116.158 7 -8 0 -2 181.145 86.6287 1 8 0 2 234.824 104.821 6 -8 0 -2 299.702 88.3301 3 8 0 2 530.432 154.399 26 -8 0 -3 14530 788.384 1 8 0 3 18865.7 969.703 7 8 0 3 18650 943.325 6 8 0 3 14795.3 853.683 29 8 0 3 15626.2 795.385 26 -8 0 -3 14282.7 768.743 3 -8 0 -3 14461.9 851.532 27 -8 0 -4 19390.7 972.12 1 8 0 4 21877.4 985.425 26 -8 0 -4 20094.9 986.698 3 8 0 4 21976.2 1120.38 29 -8 0 -4 20457.4 1067.98 27 -8 0 -5 1150.65 260.495 27 8 0 5 1502.29 278.83 7 -8 0 -5 1281.67 249.173 1 -8 0 -5 1362.59 259.983 3 8 0 5 1313.39 277.202 29 -8 0 -6 61959.5 2145.93 1 -8 0 -6 62115 2166.86 3 8 0 6 56124.4 2230.15 29 -8 0 -6 54976.6 2192.97 27 8 0 7 21650.4 1094.64 7 -8 0 -7 17045.8 1114.38 1 8 0 7 18954.7 1265.68 29 -8 0 -7 15177.6 1063.27 3 -8 0 -7 18280.4 1255.69 27 8 0 8 1398.71 279.598 7 -8 0 -8 1165.09 295.382 1 -8 0 -8 1244.18 351.766 27 -8 0 -8 1125.4 284.74 3 8 0 8 1247.81 342.976 29 -8 0 -9 190.479 132.134 1 8 0 9 54.2299 59.749 7 -8 0 -9 171.031 116.74 3 8 0 9 153.624 119.058 29 -8 0 -9 135.328 120.034 27 -8 0 -10 1533.77 361.879 3 8 0 10 960.377 160.986 22 -8 0 -10 1600.77 368.724 1 8 0 10 1228.1 170.312 14 8 0 10 773.673 271.306 29 -8 0 -10 1074.91 354.127 27 8 0 11 45.1047 48.4728 22 8 0 11 26.305 40.1864 19 8 0 11 74.7227 59.5428 14 8 0 12 9982.96 536.901 22 8 0 12 9458.47 470.952 19 8 0 12 10184.6 507.862 14 8 0 13 5926.58 391.969 22 8 0 13 6260.56 370.368 14 8 0 14 584.859 117.878 22 8 0 14 578.669 104.841 14 8 0 15 184.517 49.5027 9 8 0 15 218.314 68.4452 22 8 0 15 185.528 56.6943 14 8 0 16 591.406 102.352 22 8 0 16 593.683 95.4188 14 8 0 16 641.875 85.2751 9 8 0 17 98.2733 40.1225 22 8 0 17 104.397 34.8681 14 8 0 18 25.515 16.6427 22 -8 2 17 433.514 59.4031 13 -8 2 16 154.86 44.7919 22 -8 2 16 274.666 56.6224 13 -8 2 15 428.572 85.6221 22 -8 2 15 564.518 90.4244 16 -8 2 15 488.284 86.7306 13 -8 2 14 2813.1 237.654 22 -8 2 14 3240.86 240.425 16 -8 2 14 3144.2 238.749 13 -8 2 13 3893.9 281.556 13 -8 2 13 3310.38 218.278 21 -8 2 13 3792.35 277.946 16 -8 2 12 4375.79 312.966 13 -8 2 12 3536.64 239.582 21 -8 2 12 4448.25 315.359 16 -8 2 11 424.608 86.3584 21 -8 2 11 570.615 112.782 16 -8 2 11 579.124 121.117 13 -8 2 10 4223.16 265.606 21 -8 2 10 4241.12 322.3 16 -8 2 10 4561.37 330.985 13 -8 2 9 1694.38 196.86 13 -8 2 9 1812.01 171.979 21 -8 2 9 1727.54 202.325 16 -8 2 9 1775.04 450.2 25 -8 2 8 10344 1024.35 25 8 2 -8 11380.7 998.069 2 -8 2 7 3304.19 486.738 28 -8 2 7 3439.84 544.464 25 8 2 -7 3521.71 544.497 2 -8 2 6 3485.78 504.772 25 -8 2 6 2728.35 416.9 28 8 2 -6 3771.32 539.822 2 -8 2 5 4514.08 523.017 28 8 2 -5 4485.56 556.38 2 -8 2 5 4738.02 546.8 25 -8 2 5 4353.98 525.351 24 -8 2 4 8848.2 703.879 28 8 2 -4 10604.2 793.279 2 -8 2 4 8957.64 697.736 25 -8 2 4 9517.2 747.969 24 -8 2 3 17925.2 1022.85 24 8 2 -3 18123.5 892.718 7 -8 2 3 19690.1 1051.33 28 8 2 -3 18028.6 973.601 2 -8 2 3 17496.8 943.204 25 -8 2 2 8481.97 668.664 24 8 2 -2 8852.45 606.838 7 -8 2 2 10092.4 733.416 28 8 2 -2 9649.68 647.131 2 -8 2 2 8480.05 611.151 25 8 2 -1 52557.4 1689.18 7 8 2 -1 50735.7 1629.6 2 -8 2 0 27314 1262.77 24 -8 2 0 30583.1 1243.61 1 8 2 0 29395.7 1201.05 7 8 2 0 29460.9 1128.08 2 -8 2 0 28850.1 1370.9 27 -8 2 -1 15389.7 859.331 1 -8 2 -1 13180 851.112 24 8 2 1 15164 858.28 7 -8 2 -1 15854.1 768.014 3 -8 2 -1 13424.8 903.064 27 -8 2 -2 12975.5 850.846 24 -8 2 -2 12519.5 772.64 1 8 2 2 13742.7 853.555 7 8 2 2 13503.7 809.029 8 -8 2 -2 12270.2 708.872 3 -8 2 -2 12415.3 843.146 27 -8 2 -3 29098.9 1348.73 24 8 2 3 30300.7 1280.1 8 8 2 3 26742.7 1282.37 7 -8 2 -3 26619.9 1200.72 1 -8 2 -3 24942 1264.34 27 8 2 4 18722.5 991.102 8 -8 2 -4 16602.8 1039.47 24 8 2 4 15886.1 1006.24 7 -8 2 -4 15733.1 938.201 1 -8 2 -4 15756.1 1002.71 27 -8 2 -5 6282.54 659.018 24 8 2 5 7783.43 703.207 7 -8 2 -5 7192.65 698.823 27 -8 2 -5 7838.06 692.223 1 8 2 5 7977.12 640.236 8 8 2 6 8388.75 746.383 7 -8 2 -6 7115.95 718.05 1 -8 2 -6 7388.68 766.879 27 8 2 6 7209.58 611.329 8 -8 2 -7 172.583 119.851 1 8 2 7 136.547 86.7946 7 -8 2 -7 -37.7315 68.0223 27 8 2 8 5562.12 606.315 7 -8 2 -8 5203.15 697.33 1 -8 2 -8 5116.34 737.056 27 8 2 9 3864.68 318.613 22 -8 2 -9 3420.74 647.59 27 8 2 9 4088.61 303.844 13 8 2 9 4106.75 268.347 9 8 2 10 1272.72 185.53 22 8 2 10 1713.37 193.283 13 8 2 10 1513.27 164.924 17 8 2 10 1678.9 166.328 9 8 2 11 1970.53 226.085 22 8 2 11 2275.37 220.857 13 8 2 11 1929.33 190.808 17 8 2 11 1930.1 175.722 9 8 2 12 881.824 146.809 22 8 2 12 925.96 132.21 17 8 2 12 991.842 121.367 9 8 2 13 2236.04 221.056 22 8 2 13 2290.62 203.395 17 8 2 13 2241.27 179.487 9 8 2 14 590.303 107.079 22 8 2 14 731.127 96.283 9 8 2 15 27.0963 32.0489 22 8 2 15 0.91553 16.4774 9 8 2 16 170.248 43.361 22 8 2 16 185.669 45.3108 9 8 2 17 986.329 103.362 22 8 2 17 961.327 84.6765 9 -8 4 15 209.087 38.0464 13 -8 4 14 57.0962 25.3529 13 -8 4 13 268.167 63.141 21 -8 4 13 173.458 46.7673 13 -8 4 13 215.845 52.5522 16 -8 4 12 231.687 61.3035 21 -8 4 12 217.556 58.8434 13 -8 4 12 188.662 53.0055 16 -8 4 11 57.7298 37.8751 21 -8 4 11 68.4483 45.322 16 -8 4 11 66.569 33.2125 13 -8 4 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64909.8 2060.6 3 -9 1 -5 12010.1 847.903 1 -9 1 -5 12715.6 887.58 3 -9 1 -5 10088.5 830.509 27 9 1 6 1512.48 313.36 7 -9 1 -6 1175.48 285.341 1 -9 1 -6 819.26 254.692 27 9 1 7 4907.43 562.513 7 -9 1 -7 4364.67 588.788 1 -9 1 -7 4659.69 641.402 27 9 1 8 334.065 145.807 7 -9 1 -8 137.259 117.836 27 -9 1 -8 143.625 112.731 1 9 1 9 10860.3 561.085 22 9 1 9 12868.4 931.517 7 -9 1 -9 11299 1071.26 1 9 1 10 3177.15 296.388 22 9 1 10 3008.38 269.377 19 9 1 10 2854.28 264.078 14 9 1 11 5891.87 407.109 22 9 1 11 5757.33 377.22 14 9 1 12 11706 566.66 22 9 1 12 10645.5 510.617 14 9 1 12 11891.8 452.961 9 9 1 13 614.635 122.935 22 9 1 13 709.116 119.218 14 9 1 13 870.653 112.191 9 9 1 14 1283.77 164.903 22 9 1 14 1377.54 155.42 14 9 1 14 1656.92 151.846 9 9 1 15 283.846 72.269 22 9 1 15 316.029 67.3184 14 9 1 15 361.569 67.9806 9 9 1 16 388.602 79.2464 22 9 1 16 547.815 76.6089 9 9 1 17 108.683 36.0929 22 9 1 17 169.19 37.28 9 -9 3 16 347.961 52.6076 13 -9 3 15 693.9 88.792 13 -9 3 14 268.775 62.1889 13 -9 3 14 316.835 64.5 16 -9 3 13 811.484 107.097 21 -9 3 13 669.213 106.253 16 -9 3 13 820.14 114.497 13 -9 3 12 261.511 68.6048 21 -9 3 12 259.473 75.9986 16 -9 3 12 397.862 85.0994 13 -9 3 11 1206.07 142.572 21 -9 3 11 1197.78 158.235 16 -9 3 11 1108.43 149.87 13 -9 3 10 751.046 117.52 21 -9 3 10 673.04 122.379 16 -9 3 10 624.627 119.452 13 -9 3 9 4205.07 281.724 21 9 3 -9 3067.31 249.269 10 -9 3 9 3893.83 298.195 16 -9 3 9 3638.25 283.318 13 -9 3 8 1714.35 182.059 21 -9 3 8 1565.91 193.3 20 9 3 -8 1420.93 168.35 10 -9 3 8 1492.7 183.651 16 -9 3 8 1420.26 177.07 13 -9 3 7 1739.21 181.351 21 -9 3 7 1959.14 208.052 20 9 3 -7 1615.9 178.328 10 -9 3 7 1439.65 175.37 16 -9 3 7 1311.61 166.322 13 -9 3 6 922.15 133.536 21 -9 3 6 1118.43 151.558 20 9 3 -6 1143.77 150.502 10 9 3 -6 672.253 249.536 2 -9 3 6 1145.56 149.825 16 -9 3 6 778.399 270.306 24 -9 3 6 977.619 140.637 13 -9 3 5 356.455 165.573 24 9 3 -5 590.409 222.252 2 -9 3 4 957.144 265.341 24 9 3 -4 1041 280.912 2 9 3 -3 534.807 186.399 2 -9 3 3 612.716 209.257 24 -9 3 2 85.4018 82.5157 24 9 3 -2 102.655 79.3962 7 -9 3 2 280.794 153.856 28 9 3 -1 1758.9 337.539 8 9 3 -1 1673.67 307.836 7 -9 3 1 1690.27 355.061 28 -9 3 1 2220.1 398.927 24 -9 3 0 3834.82 526.935 24 9 3 0 3434.39 450.387 7 9 3 0 3514.12 468.652 8 -9 3 -1 21714.9 1315.32 24 9 3 1 22133.5 1222.8 8 9 3 1 22083.2 1221.94 7 -9 3 -2 2435.25 440.102 24 9 3 2 2440.91 398.529 8 9 3 2 2183.68 388.599 7 -9 3 -2 1899.51 337.03 1 -9 3 -2 2071.37 394.313 27 -9 3 -3 121.485 90.931 24 9 3 3 104.621 120.086 8 9 3 3 44.7472 56.9931 7 -9 3 -3 154.899 121.27 1 -9 3 -3 -86.2577 86.6228 27 -9 3 -4 5738.92 710.213 24 -9 3 -4 5450.5 605.525 1 9 3 4 5535.78 666.241 7 -9 3 -4 4651.42 604.294 27 9 3 4 5981.62 649.941 8 9 3 5 3116.92 499.868 7 -9 3 -5 3069.22 472.825 1 -9 3 -5 2130 421.31 27 9 3 5 3659.05 516.054 8 -9 3 -6 974.408 141.738 12 9 3 6 1176.05 287.021 8 9 3 6 792.183 256.407 7 9 3 6 951.188 142.235 17 -9 3 -6 781.184 246.217 1 9 3 6 870.493 125.746 9 -9 3 -6 877.191 275.855 27 -9 3 -7 1838.54 192.002 12 9 3 7 2052.22 202.925 17 9 3 7 1660.24 180.307 9 -9 3 -8 1236.5 155.985 12 9 3 8 1304.4 180.433 22 9 3 8 1528.49 171.01 17 9 3 8 1228.73 157.284 9 -9 3 -9 6738.56 367.277 12 9 3 9 6863.7 365.546 17 9 3 9 7020.29 380.483 9 -9 3 -10 377.043 80.7144 12 9 3 10 158.797 64.291 22 9 3 10 362.25 79.9561 17 9 3 10 262.111 66.8791 9 9 3 11 1044.09 130.97 17 9 3 11 917.327 123.23 9 9 3 12 672.287 119.472 22 9 3 12 853.918 112.909 17 9 3 12 998.202 120.977 9 9 3 13 907.192 128.616 22 9 3 13 1132.24 127.754 17 9 3 13 1104.8 119.895 9 9 3 14 1100.23 128.517 22 9 3 14 1455.98 134.194 17 9 3 14 1500.25 132.018 9 9 3 15 624.939 83.2359 22 9 3 15 833.899 88.8962 9 9 3 16 151.982 32.1347 9 -9 5 12 455.8 61.2827 21 9 5 -11 98.2114 32.0719 12 -9 5 11 85.0911 34.699 21 -9 5 10 34.083 27.2133 21 -9 5 9 -41.7089 38.8078 21 9 5 -9 -8.63596 21.6762 10 -9 5 8 95.2103 49.8389 21 9 5 -8 76.3166 35.5476 10 -9 5 7 713.988 111.293 21 -9 5 7 665.046 113.972 20 9 5 -7 886.591 120.929 10 -9 5 6 853.317 123.157 21 -9 5 6 1179.05 151.696 20 9 5 -6 923.828 132.306 10 9 5 -5 97.3386 38.1266 23 -9 5 5 34.3902 27.163 21 9 5 -5 137.514 56.3449 10 9 5 -4 1709.58 185.211 23 -9 5 4 1361.12 162.447 21 -9 5 4 2064.41 196.299 20 9 5 -4 1786.56 200.483 10 9 5 -3 576.975 104.984 23 -9 5 3 541.155 127.955 21 -9 5 3 691.097 116.981 20 9 5 -3 555.134 114.697 10 9 5 -2 142.757 56.4145 23 -9 5 2 256.65 75.2234 20 9 5 -2 217.51 67.4812 10 9 5 -1 1032.93 148.577 23 -9 5 1 1179.95 151.064 20 9 5 -1 1020.15 151.821 10 9 5 0 272.67 82.0097 23 -9 5 0 248.875 67.5654 12 -9 5 0 334.166 83.0435 20 9 5 0 286.919 78.559 10 -9 5 -1 5518.54 326.999 12 9 5 1 5279.05 358.518 23 -9 5 -1 5482.63 352.375 20 9 5 1 5541.19 342.193 10 -9 5 -2 2747.7 231.186 12 9 5 2 2561 251.099 23 -9 5 -2 2603.7 242.901 20 9 5 2 2198.21 204.357 10 -9 5 -3 640.901 113.929 12 9 5 3 436.6 104.613 23 -9 5 -3 637.916 122.325 20 9 5 3 506.08 99.888 17 9 5 4 551.641 113.173 23 -9 5 -4 551.777 108.234 12 -9 5 -4 359.239 91.2623 20 9 5 4 648.551 103.363 9 9 5 4 489.33 102.943 17 9 5 5 0.63627 28.3863 23 -9 5 -5 53.7939 51.6285 12 -9 5 -5 10.5423 38.9307 20 9 5 5 24.8124 23.1453 9 9 5 6 177.808 57.5178 23 -9 5 -6 112.265 41.9226 12 -9 5 -6 168.28 64.0123 20 9 5 6 207.305 70.9551 17 9 5 6 143.771 43.0751 9 -9 5 -7 646.102 105.657 12 9 5 7 617.75 103.285 23 9 5 7 742.393 118.693 17 9 5 7 518.025 97.4779 9 -9 5 -8 586.105 96.9497 12 9 5 8 726.742 109.896 17 9 5 8 480.484 86.6408 9 -9 5 -9 2561.84 190.685 12 9 5 9 2711.7 201.093 17 9 5 9 2351.46 200.907 9 -9 5 -10 6.48716 22.8921 12 9 5 10 -3.49834 24.7481 17 9 5 10 25.0038 28.1888 9 -9 5 -11 845.005 90.6899 12 9 5 11 955.046 99.3457 17 9 5 11 928.015 102.299 9 9 5 12 1669.5 121.334 9 9 5 12 1487.64 111.797 17 9 7 -2 74.4785 26.8341 23 9 7 -1 91.3733 34.8285 23 -9 7 1 82.2844 32.1517 20 9 7 0 201.244 48.8475 23 -9 7 0 166.635 43.2087 20 9 7 1 104.402 36.5712 23 -9 7 -1 173.967 47.1261 20 9 7 2 119.638 38.3429 23 -9 7 -2 151.858 41.5497 20 -10 -6 8 46.12 27.9609 30 -10 -6 7 51.9575 29.7377 30 -10 -6 6 91.3043 38.7083 30 -10 -6 5 108.935 49.404 30 -10 -6 4 67.8837 24.1543 30 -10 -6 3 94.6342 42.5243 30 -10 -4 14 19.096 16.6441 11 -10 -4 13 11.4275 14.5385 11 -10 -4 13 -35.6441 23.3442 30 -10 -4 12 -1.7819 24.4997 11 -10 -4 12 -4.42603 28.4425 30 -10 -4 11 397.114 81.2146 11 -10 -4 11 450.871 98.218 30 -10 -4 10 421.014 88.4776 11 -10 -4 10 379.69 92.9722 30 -10 -4 9 3200.1 251.179 11 -10 -4 9 3200.86 288.893 30 -10 -4 8 1855.24 196.555 11 -10 -4 8 1520.62 202.855 30 -10 -4 7 2463.06 234.713 11 -10 -4 7 2071.65 240.881 30 -10 -4 6 2204.42 227.979 11 -10 -4 6 1731.01 222.299 30 -10 -4 5 238.081 90.3439 30 -10 -4 5 376.412 99.6417 11 -10 -4 4 57.5695 45.3384 30 -10 -4 3 1079.2 175.11 30 -10 -4 2 2645.62 280.684 30 -10 -4 1 8567.09 523.85 30 -10 -4 0 8637.86 533.126 30 -10 -4 -1 1982.52 256.139 30 10 -4 2 5317.07 330.312 11 10 -4 3 3395.13 266.134 11 10 -4 4 353.462 87.7732 11 10 -4 5 751.61 127.831 11 10 -4 6 1566.73 191.803 11 10 -4 7 484.684 109.215 11 10 -4 8 4626.63 328.682 11 10 -4 9 359.206 85.8617 11 10 -4 10 938.695 132.223 11 10 -4 11 1486.84 155.458 11 10 -4 12 860.38 108.815 11 10 -4 12 909.919 118.7 19 10 -4 13 762.759 90.174 11 10 -4 13 814.95 101.016 19 10 -4 14 40.0668 18.0435 11 10 -4 14 68.4781 28.1708 19 -10 -2 16 563.849 78.7831 22 -10 -2 15 146.846 51.2169 22 -10 -2 15 138.305 38.8342 11 -10 -2 14 48.9654 30.7878 22 -10 -2 14 87.1449 60.1429 18 -10 -2 14 135.185 47.8962 11 -10 -2 13 205.863 90.5789 18 -10 -2 13 188.51 59.146 11 -10 -2 12 678.787 118.688 11 -10 -2 12 538.016 125.589 18 -10 -2 11 1508.09 180.781 11 -10 -2 11 1397.41 205.633 18 -10 -2 10 5050.34 402.64 18 -10 -2 9 10691.2 587.563 18 -10 -2 9 7983.35 487.145 30 -10 -2 8 2072.29 234.14 30 -10 -2 8 2308.3 266.532 18 -10 -2 7 549.172 171.65 4 -10 -2 7 711.538 145.327 18 10 -2 -7 799.515 261.565 2 -10 -2 7 812.355 283.986 28 10 -2 -7 382.541 204.534 26 10 -2 -6 1520.26 413.784 26 10 -2 -6 1565.61 347.801 2 -10 -2 6 1687.47 292.247 4 -10 -2 6 1399.75 361.212 28 -10 -2 5 3647.03 466.882 3 -10 -2 5 3149.86 529.068 28 10 -2 -5 3398.87 487.525 2 -10 -2 5 3647.33 411.938 4 10 -2 -5 3261.85 619.267 26 -10 -2 4 2355.62 369.718 3 10 -2 -4 2309.86 346.844 6 10 -2 -4 2474.04 408.347 2 -10 -2 4 1904.93 384.122 28 -10 -2 4 2006.93 293.77 4 10 -2 -4 1674.38 422.46 26 -10 -2 3 2179.09 313.357 4 -10 -2 3 2811.47 393.895 3 10 -2 -3 2987.62 395.852 6 10 -2 -3 3074.41 433.4 2 -10 -2 3 2149.17 391.673 28 10 -2 -3 1693.98 416.27 26 -10 -2 2 1498.06 260.42 4 -10 -2 2 1618.46 300.702 3 10 -2 -2 2154.19 339.756 6 10 -2 -2 2000.37 343.583 2 -10 -2 2 1903.4 352.691 28 10 -2 -2 1863.45 484.579 26 -10 -2 1 24404.2 1197.43 3 10 -2 -1 26058.7 1265.18 6 10 -2 -1 22748.6 1456.82 26 -10 -2 1 22371.1 1120.81 4 10 -2 0 25047.6 1270.17 6 -10 -2 0 22693.3 1122.24 3 10 -2 0 23603.2 1396.95 26 -10 -2 0 23025.1 1153.99 4 -10 -2 -1 253.784 123.769 4 10 -2 1 575.945 188.81 6 -10 -2 -1 377.319 141.686 3 10 -2 1 371.418 207.296 26 -10 -2 -2 2494.78 357.117 4 10 -2 2 2632.65 406.081 6 -10 -2 -2 2450.73 363.092 3 10 -2 2 1844.37 324.649 29 10 -2 2 2160.26 384.911 26 -10 -2 -3 20806.9 1112.5 4 -10 -2 -3 23056.5 1197.76 3 10 -2 3 21134.7 1234.77 29 10 -2 3 24234.3 1282.89 26 -10 -2 -4 2971.68 402.822 4 10 -2 4 4012.06 486.792 6 -10 -2 -4 3607.34 468.738 3 10 -2 4 3506.56 522.082 29 -10 -2 -5 2639.25 390.652 4 10 -2 5 3434.52 447.934 6 -10 -2 -5 3253.41 466.758 3 10 -2 5 3423.75 558.894 29 -10 -2 -6 1762.35 332.856 4 10 -2 6 2416.02 373.251 6 -10 -2 -6 2375.59 424.273 3 10 -2 6 2847.12 529.442 29 -10 -2 -7 720.49 231.574 4 10 -2 7 1086.84 260.969 7 10 -2 7 592.53 113.485 11 -10 -2 -7 809.859 256.948 3 10 -2 8 2722.24 248.358 11 10 -2 8 2184.43 238.279 14 10 -2 9 3615.13 288.291 11 10 -2 9 3218.37 297.41 14 10 -2 10 150.374 54.3504 11 10 -2 10 152.954 64.0869 14 10 -2 11 9349.16 456.99 11 10 -2 11 9529.95 509.759 14 10 -2 12 1361.33 157.49 11 10 -2 12 1330.96 174.852 14 10 -2 13 485.854 87.1275 11 10 -2 13 600.865 107.241 19 10 -2 13 572.166 107.455 14 10 -2 14 7.23642 20.4404 19 10 -2 14 28.937 29.6089 14 10 -2 15 729.231 101.598 19 10 -2 15 516.751 88.7422 14 10 -2 16 621.263 83.3733 19 10 -2 16 659.014 84.6396 14 10 -2 16 497.043 58.3531 9 -10 0 17 40.4274 27.0187 22 -10 0 16 1.27535 20.7655 22 -10 0 15 625.603 111.565 22 -10 0 14 3122.14 271.556 22 -10 0 14 1754.64 202.662 18 -10 0 13 853.176 146.162 18 -10 0 13 787.102 117.038 13 -10 0 12 3950.5 345.671 18 -10 0 12 3602.06 272.792 13 -10 0 11 3915.32 358.537 18 -10 0 11 3189.46 261.813 16 -10 0 11 3162.75 264.332 13 -10 0 10 113.258 71.3179 18 -10 0 10 -7.96368 37.3624 16 -10 0 10 52.2456 37.4048 13 -10 0 9 15490.7 1306.05 28 -10 0 9 18903.8 818.766 18 -10 0 9 14786.1 594.536 16 -10 0 9 16712.7 1309.32 25 10 0 -8 214.845 167.902 2 -10 0 8 401.506 191.949 28 -10 0 8 238.576 140.88 25 10 0 -7 44.0352 97.6894 2 -10 0 7 174.428 124.254 28 10 0 -7 -22.2492 83.1359 26 -10 0 7 -46.8354 70.8644 25 10 0 -6 17751.8 1171.47 26 10 0 -6 20593 1191.51 2 -10 0 6 19717.5 1248.96 28 -10 0 6 19293.8 1162.14 25 10 0 -5 34.3282 81.3181 26 -10 0 5 60.0374 84.615 3 10 0 -5 92.1544 124.877 2 -10 0 5 62.2412 79.978 28 -10 0 5 78.5695 101.837 25 10 0 -4 12981.8 878.666 2 10 0 -4 9452.83 846.245 26 -10 0 4 11718.5 704.927 3 -10 0 4 10822 856.488 28 -10 0 3 157.978 76.8067 3 10 0 -3 182.144 105.444 2 -10 0 3 76.1611 43.2085 28 10 0 -3 216.203 79.0411 26 10 0 -2 77.8238 48.8716 7 10 0 -2 25.4494 50.238 2 -10 0 2 103.929 75.8302 3 -10 0 2 220.245 120.972 28 10 0 -2 -46.5759 124.436 26 10 0 -1 15819.4 803.488 2 10 0 -1 16918.3 870.837 7 -10 0 1 15431.7 835.976 3 -10 0 1 15445.8 947.123 28 10 0 -1 14763.1 963 26 10 0 0 12641.6 791.245 7 -10 0 0 11949.9 731.875 3 -10 0 0 10065.2 747.393 28 10 0 0 10572.5 773.362 26 -10 0 0 10265.5 777.962 27 10 0 1 1537.74 285.891 7 -10 0 -1 1027.94 213.115 3 -10 0 -1 1310.6 251.68 1 -10 0 -1 871.107 221.468 28 -10 0 -1 752.826 203.559 27 10 0 1 1298.42 255.302 26 -10 0 -2 12147.6 654.025 4 10 0 2 16099.9 994.728 7 -10 0 -2 14088.1 829.885 3 10 0 2 15216.1 891.355 26 -10 0 -2 15534.5 958.623 27 -10 0 -2 14645.5 870.537 1 -10 0 -3 2117.82 269.121 4 10 0 3 3053.5 432.113 7 -10 0 -3 2579.04 352.624 3 -10 0 -3 1893.38 325.705 27 10 0 3 2111.95 333.531 26 -10 0 -3 2369.62 350.118 1 -10 0 -4 357.608 127.019 4 10 0 4 518.997 175.982 7 -10 0 -4 314.536 127.462 1 -10 0 -4 426.281 160.728 3 -10 0 -4 105.001 58.8639 27 10 0 4 193.159 102.718 26 -10 0 -5 21915.7 1189.82 1 -10 0 -5 21520 1198.14 3 10 0 5 19276.9 1234.04 29 -10 0 -6 9713.99 827.942 1 10 0 6 12084.9 883.989 7 -10 0 -6 10178.1 865.031 3 10 0 6 10339 941.909 29 -10 0 -6 8991.34 851.618 27 10 0 7 1345.27 286.476 7 -10 0 -7 1356.39 326.022 1 -10 0 -7 1015.73 287.433 3 10 0 7 1139.86 323.839 29 -10 0 -7 703.915 242.444 27 -10 0 -8 16285.5 1219.75 1 10 0 8 13252.7 1192.66 29 -10 0 -8 14100.6 1150.97 3 -10 0 -8 14023.8 1238.73 27 10 0 9 5966.49 411.532 22 -10 0 -9 6763.55 819.224 1 10 0 9 6677.79 404.547 19 10 0 9 6113.48 822.503 29 10 0 9 6559.69 417.437 14 -10 0 -9 5085.07 791.271 27 10 0 10 9245.23 529.084 22 10 0 10 10334.6 508.097 19 10 0 10 9906.25 523.956 14 10 0 11 7075.71 458.172 22 10 0 11 7605.6 425.187 19 10 0 11 7965.65 453.155 14 10 0 12 36.8653 19.9676 19 10 0 12 52.5274 38.9691 14 10 0 13 183.935 72.6896 22 10 0 13 284.558 74.3885 19 10 0 14 187.101 62.0667 22 10 0 14 171.928 56.008 19 10 0 14 146.11 53.1986 14 10 0 14 337.961 68.9494 9 10 0 15 116.621 40.1718 22 10 0 15 151.389 52.6273 14 10 0 15 197.178 49.3248 9 10 0 16 1394.19 142.819 22 10 0 16 1269.13 126.94 14 10 0 16 1565.43 125.88 9 10 0 17 1499.63 130.229 22 10 0 17 1535.59 120.842 14 10 0 17 1521.62 104.305 9 -10 2 16 821.175 88.1366 13 -10 2 15 172.866 50.7242 22 -10 2 15 162.943 47.2156 16 -10 2 15 200.479 52.5388 13 -10 2 14 93.2829 48.7454 22 -10 2 14 106.456 43.4282 13 -10 2 14 106.005 49.7694 16 -10 2 13 113.488 55.1915 22 -10 2 13 99.8319 39.0797 16 -10 2 13 163.84 61.2516 13 -10 2 12 831.184 143.522 22 -10 2 12 584.348 110.471 16 -10 2 12 629.6 117.426 13 -10 2 11 1408.16 145.471 21 -10 2 11 1700.53 199.742 16 -10 2 11 1682.12 199.605 13 -10 2 10 3836.62 255.586 21 -10 2 10 3453.72 305.929 20 -10 2 10 4111.72 318.403 16 -10 2 10 4158.24 321.834 13 -10 2 9 10172.8 427.752 21 -10 2 9 10239.4 513.251 16 -10 2 9 9794.86 511.574 13 -10 2 8 2264.15 194.752 21 -10 2 8 1942.69 218.446 20 10 2 -8 1870.07 187.737 10 -10 2 8 2339.79 232.563 16 -10 2 8 2365.67 237.475 13 10 2 -7 773.301 260.744 2 -10 2 7 540.624 104.696 16 -10 2 7 412.162 183.333 28 -10 2 7 448.828 205.267 25 10 2 -6 1582.59 373.372 2 -10 2 6 1474.71 335.858 28 -10 2 6 1859.59 390.633 25 -10 2 5 3607.05 533.913 28 10 2 -5 4012.51 560.504 2 -10 2 5 3445.31 507.248 25 -10 2 4 1965.3 374.515 24 -10 2 4 2118.15 390.028 28 10 2 -4 2673.31 427.464 2 -10 2 4 1912.78 350.592 25 -10 2 3 2251.77 394.748 28 10 2 -3 2381.24 370.404 2 -10 2 3 2065.9 354.296 25 -10 2 3 2032.89 364.069 24 10 2 -2 2450.47 338.191 7 -10 2 2 2573.56 419.421 28 10 2 -2 2340.93 340.633 2 -10 2 2 2399.66 355.81 25 -10 2 2 2404.81 392.974 24 -10 2 1 23178.4 1237.01 24 10 2 -1 23231.3 1123.22 7 -10 2 1 23988 1319.91 28 -10 2 0 19160.1 1129.67 24 10 2 0 20526.1 1075.59 7 -10 2 0 21953.3 1161.11 1 -10 2 -1 509.822 188.606 24 -10 2 -1 290.435 134.416 1 10 2 1 535.796 166.304 7 -10 2 -1 575.556 216.118 27 -10 2 -2 2367.41 410.5 24 10 2 2 2766.9 396.789 8 10 2 2 2873.16 424.528 7 -10 2 -2 2857.92 448.863 27 -10 2 -2 2558.74 385.846 1 -10 2 -3 20793.7 1257.61 24 -10 2 -3 22606 1202.41 1 10 2 3 23935.7 1231.42 8 10 2 3 22912.2 1307.34 7 -10 2 -3 22203.5 1137.19 3 -10 2 -3 20265.4 1242.23 27 10 2 4 2580.75 391.201 8 -10 2 -4 2863.75 423.086 1 10 2 4 2667.36 455.36 7 -10 2 -4 3005.51 426.397 3 -10 2 -4 2464.1 424.392 27 -10 2 -5 3409.26 485.952 1 10 2 5 3805.95 549.347 7 -10 2 -5 2890.23 452.608 3 -10 2 -5 2656.73 454.379 27 10 2 6 3153.91 501.56 7 -10 2 -6 2198.42 421.497 1 -10 2 -6 2923.21 481.556 3 -10 2 -6 2447.22 459.708 27 10 2 7 913.668 145.674 22 10 2 7 928.286 264.628 7 -10 2 -7 772.451 274.318 1 -10 2 -7 444.693 199.043 3 10 2 7 911.772 131.948 9 -10 2 -7 850.711 285.459 27 -10 2 -8 2092.85 196.927 12 10 2 8 2316.39 240.529 22 10 2 8 2011.68 215.144 14 10 2 8 2403.53 214.179 9 10 2 9 3478.02 306.254 22 10 2 9 3699.81 265.537 9 10 2 10 246.759 85.9659 22 10 2 10 249.454 69.6022 17 10 2 10 330.197 73.3617 9 10 2 11 9197.1 505.153 22 10 2 11 10357.2 460.681 17 10 2 11 9299.23 413.725 9 10 2 12 1607.05 196.608 22 10 2 12 1861.29 186.289 17 10 2 12 1822.79 163.463 9 10 2 13 411.366 92.1982 22 10 2 13 642.362 101 17 10 2 13 540.664 85.0291 9 10 2 14 -3.25541 20.0152 22 10 2 14 -24.3704 21.6593 17 10 2 14 -20.7032 22.9048 9 10 2 15 609.147 93.0409 22 10 2 15 678.523 84.6182 9 10 2 16 692.281 77.6139 9 10 2 16 568.308 80.9886 22 -10 4 14 -16.6992 18.9245 13 -10 4 13 20.8453 15.2303 16 -10 4 13 -16.4253 23.0592 13 -10 4 12 35.7069 35.4876 21 -10 4 12 -8.33159 23.0753 16 -10 4 12 -6.54016 19.5524 13 -10 4 11 377.696 73.0164 13 -10 4 11 529.593 85.7195 21 -10 4 11 381.865 74.7021 16 -10 4 10 339.608 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125.688 51.9544 11 11 -5 8 50.9398 33.9466 11 11 -5 9 546.958 89.8627 11 11 -5 10 1963.39 156.327 11 11 -5 11 231.16 46.5904 11 -11 -3 15 37.5829 19.8313 11 -11 -3 14 515.956 79.7743 11 -11 -3 13 854.426 113.018 11 -11 -3 12 65.5928 51.8064 18 -11 -3 12 26.2161 32.9476 11 -11 -3 12 32.8886 41.7724 30 -11 -3 11 1840.15 211.101 18 -11 -3 11 1755.29 203.003 30 -11 -3 10 1631.42 185.398 11 -11 -3 10 1220.91 190.075 18 -11 -3 10 1373.68 191.341 30 -11 -3 9 2506.97 269.831 18 -11 -3 9 1790.6 226.316 30 -11 -3 8 697.689 151.428 18 -11 -3 8 701.607 144.416 30 -11 -3 7 270.034 108.852 18 -11 -3 7 206.801 77.0443 30 -11 -3 6 314.793 116.204 18 -11 -3 6 288.374 94.4874 30 -11 -3 5 717.569 139.913 30 -11 -3 4 1243.71 176.942 30 -11 -3 3 3971.66 319.114 30 11 -3 -3 4362.84 546.321 6 11 -3 -3 4446.65 595.169 2 -11 -3 3 4147.4 489.614 4 -11 -3 2 857.087 225.95 4 11 -3 -2 1354.25 306.087 6 -11 -3 2 1081.6 266.975 3 -11 -3 2 734.124 131.843 30 11 -3 -2 1368.1 318.385 2 11 -3 -2 1201.94 423.881 26 -11 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11 11 -3 13 70.4811 35.7458 19 11 -3 13 92.4887 38.3496 14 11 -3 14 795.646 89.6148 11 11 -3 14 864.117 103.795 19 11 -3 14 793.047 96.9309 14 11 -3 15 77.7039 27.2126 19 -11 -1 16 100.292 36.9261 22 -11 -1 15 47.808 29.6803 22 -11 -1 15 5.62251 45.9435 18 -11 -1 14 210.751 72.7477 18 -11 -1 13 261.185 83.6164 18 -11 -1 13 228.408 66.2872 11 -11 -1 12 2909.43 245.255 11 -11 -1 12 3523.85 327.379 18 -11 -1 11 1219.52 198.074 18 -11 -1 10 1790.02 249.951 18 -11 -1 9 956.035 189.954 18 -11 -1 8 2044.11 254.945 18 -11 -1 8 1535.6 363.36 25 11 -1 -7 5890.37 650 2 -11 -1 7 4291.44 654.798 28 11 -1 -7 3737.75 585.862 26 -11 -1 7 3753.5 531.223 25 -11 -1 6 3664.57 457.857 3 11 -1 -6 4029.66 528.57 2 -11 -1 6 3787.73 593.387 28 11 -1 -6 3920.37 603.986 26 -11 -1 6 3588.23 495.762 25 -11 -1 5 138.278 81.9258 3 11 -1 -5 295.37 162.484 2 -11 -1 5 391.293 181.799 28 11 -1 -5 143.613 110.482 26 -11 -1 5 18.2256 49.6456 25 -11 -1 4 4499.56 492.578 3 11 -1 -4 4606.9 573.95 2 -11 -1 4 4251.64 562.492 28 11 -1 -4 3629.71 574.168 26 11 -1 -3 24660.6 1217.96 6 -11 -1 3 23801.9 1176.23 3 11 -1 -3 26338.9 1352.38 2 -11 -1 3 22288.1 1279.9 28 11 -1 -3 22146.8 1422.24 26 11 -1 -2 19350.3 1008.06 7 11 -1 -2 20213.9 1079.81 6 11 -1 -2 19639 1133.91 2 -11 -1 2 18443.3 1016.96 3 -11 -1 2 21696.6 1213.63 28 11 -1 -2 17171.4 1218.96 26 -11 -1 1 -24.9881 41.9381 4 11 -1 -1 118.487 106.517 7 11 -1 -1 38.689 61.2223 6 -11 -1 1 6.71176 67.8021 3 -11 -1 1 257.346 130.389 28 11 -1 -1 155.986 140.684 26 11 -1 0 10218.1 783.08 7 11 -1 0 10573.6 801.075 6 -11 -1 0 10002.9 745.148 3 -11 -1 0 9786.63 768.884 28 11 -1 0 10212.5 810.41 26 -11 -1 0 9396.96 665.225 4 11 -1 1 22109 1221.8 7 11 -1 1 21975 1202.99 6 -11 -1 -1 21774.4 1122.16 3 -11 -1 -1 20784.5 1127.34 28 -11 -1 -1 19976.9 1151.62 27 11 -1 1 20931 1157.59 26 -11 -1 -1 19373.2 986.121 4 -11 -1 -2 2915.68 367.113 4 11 -1 2 4301.99 527.812 7 11 -1 2 3701.36 483.786 6 -11 -1 -2 3556.05 435.641 3 -11 -1 -2 2718.96 411.815 28 -11 -1 -2 2893.61 415.541 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5062.94 368.003 22 11 -1 8 5547.98 359.051 11 11 -1 8 5442.04 375.263 19 11 -1 8 5936.84 395.946 14 -11 -1 -8 4383.35 703.196 27 11 -1 9 2078 212.427 11 11 -1 9 2304.87 238.205 19 11 -1 9 2291.6 246.87 14 11 -1 9 2276.62 248.392 22 11 -1 10 650.949 134.412 22 11 -1 10 578.249 111.202 11 11 -1 10 1147.11 164.595 19 11 -1 10 1013.89 162.301 14 11 -1 11 1818.3 222.877 22 11 -1 11 2206.79 220.651 19 11 -1 11 2161.64 232.312 14 11 -1 12 2895.73 275.263 22 11 -1 12 3503.51 268.904 19 11 -1 12 3386.94 279.288 14 11 -1 13 489.607 106.875 22 11 -1 13 531.568 98.6378 19 11 -1 13 509.928 101.951 14 11 -1 14 1456.86 164.976 22 11 -1 14 1732.02 170.918 19 11 -1 14 1691.49 170.07 14 11 -1 15 769.952 106.238 22 11 -1 15 791.423 105.067 19 11 -1 15 862.617 110.573 14 11 -1 15 1021.02 107.977 9 11 -1 16 467.982 68.378 22 11 -1 16 465.206 70.0701 19 11 -1 16 571.315 80.5478 14 11 -1 16 583.473 69.7169 9 -11 1 16 45.7715 24.2182 22 -11 1 16 45.39 17.4362 13 -11 1 15 33.1739 20.4358 22 -11 1 15 -8.67655 20.2155 16 -11 1 15 -9.51955 20.8624 13 -11 1 14 146.599 62.4486 22 -11 1 14 117.053 41.7573 16 -11 1 14 187.183 55.9489 13 -11 1 13 194.293 60.9186 16 -11 1 13 253.267 69.2171 13 -11 1 12 2762.35 282.598 18 -11 1 12 3221.32 256.765 16 -11 1 12 3253.53 263.655 13 -11 1 11 475.076 132.251 18 -11 1 11 861.406 138.425 16 -11 1 11 841.58 144.007 13 -11 1 10 1690.73 234.328 18 -11 1 10 1719.24 197.58 16 -11 1 10 1733.78 207.568 13 -11 1 9 869.352 149.129 20 -11 1 9 760.373 154.638 18 -11 1 9 774.857 129.953 16 -11 1 9 720.451 134.552 13 -11 1 8 1608.67 168.001 21 -11 1 8 1904.14 211.902 20 11 1 -8 1800.61 187.837 10 -11 1 8 2158.95 215.948 16 11 1 -7 4965.74 650.345 2 -11 1 7 3162.61 523.137 28 -11 1 7 4032.64 615.107 25 11 1 -6 3864.5 563.196 2 -11 1 6 3432.76 525.623 28 11 1 -6 3199.06 507.187 26 -11 1 6 4063.57 580.366 25 11 1 -5 203.947 120.913 2 -11 1 5 277.453 155.737 28 11 1 -5 -42.6966 80.3459 26 -11 1 5 -13.0737 85.2039 25 11 1 -4 3977.32 521.738 2 -11 1 4 4133.97 559.945 28 11 1 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1 6 1654.64 360.139 7 -11 1 -6 1672.74 360.095 1 -11 1 -6 1720.16 361.905 3 -11 1 -6 1206.22 317.459 27 11 1 7 3283.58 281.634 22 -11 1 -7 3890.21 593.281 1 11 1 7 4418.47 582.341 7 -11 1 -7 3902.22 598.918 3 -11 1 -7 3187.2 550.496 27 11 1 8 5006.03 366.194 22 11 1 8 4304.53 331.336 19 11 1 8 4440.57 326.418 14 11 1 9 2840.1 277.275 22 11 1 9 2422.75 246.513 19 11 1 9 2233.4 231.993 14 11 1 10 685.448 134.352 22 11 1 10 793.534 140.479 19 11 1 10 719.188 131.205 14 11 1 11 2657.39 268.255 22 11 1 11 2518.69 224.529 15 11 1 11 2361.03 233.396 14 11 1 11 2937.97 215.848 9 11 1 12 2667.93 257.789 22 11 1 12 2633.2 232.026 19 11 1 12 3294.44 256.122 17 11 1 12 2800.48 244.378 14 11 1 12 3119.42 215.761 9 11 1 13 583.72 112.037 22 11 1 13 671.477 107.53 17 11 1 13 717.657 98.7284 9 11 1 13 560.194 100.7 14 11 1 14 1401.44 160.838 22 11 1 14 1263.8 137.065 14 11 1 15 1108.02 132.276 22 11 1 15 1309.79 119.166 9 11 1 16 460.811 76.3146 22 11 1 16 487.21 65.5575 9 11 1 17 29.6112 12.1995 22 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118.462 16 -11 3 4 1452 174.016 20 11 3 -4 1602.83 189.701 10 -11 3 4 1341.9 159.48 16 -11 3 3 4771.1 313.128 20 11 3 -3 4204.59 314.971 10 -11 3 3 3775.39 266.546 16 11 3 -3 4265.31 295.109 15 -11 3 2 751.246 233.713 24 11 3 -2 573.707 189.68 7 -11 3 2 820.957 131.446 20 11 3 -2 775.68 131.156 10 11 3 -2 649.174 111.253 15 -11 3 2 1046.05 297.192 28 -11 3 1 890.148 266.371 24 11 3 -1 908.277 269.76 8 11 3 -1 1008.25 250.592 7 -11 3 1 1223.52 161.333 20 11 3 -1 1115.2 159.12 10 11 3 -1 1037.7 135.788 15 -11 3 1 999.941 289.597 28 -11 3 0 422.727 182.151 24 11 3 0 718.011 223.467 8 11 3 0 731.057 217.466 7 -11 3 0 482.048 100.396 20 11 3 0 475.915 93.0316 15 -11 3 0 292.601 155.397 28 -11 3 -1 380.03 178.119 24 11 3 1 478.99 171.014 8 -11 3 -1 591.508 101.713 12 11 3 1 782.664 233.491 7 11 3 1 517.859 97.0172 15 -11 3 -2 -67.2597 79.8669 24 11 3 2 147.849 104.44 8 -11 3 -2 130.558 45.8425 12 11 3 2 19.8295 41.2994 7 -11 3 -2 94.7065 55.6855 20 11 3 2 118.992 48.3604 15 11 3 3 8229.76 800.121 8 -11 3 -3 6468.47 378.387 12 -11 3 -3 5663.44 379.312 20 11 3 3 7348.51 392.387 15 -11 3 -3 6316.32 753.326 27 -11 3 -3 6691.69 705.714 1 11 3 4 7850.67 452.054 17 11 3 4 7298.68 406.953 15 -11 3 -5 2786.76 249.387 12 11 3 5 2892.43 260.965 22 11 3 5 3351.74 286.526 17 11 3 5 3093.39 268.163 15 11 3 5 2724.25 224.309 9 -11 3 -6 1840.56 198.864 12 11 3 6 1751.8 206.768 22 11 3 6 2234.38 227.118 17 11 3 6 1704.85 201.928 15 11 3 6 1630.19 183.835 9 -11 3 -7 1475.46 175.153 12 11 3 7 1182.24 174.343 22 11 3 7 1496.09 179.147 17 11 3 7 1422.03 171.261 9 -11 3 -8 3508.4 266.967 12 11 3 8 3143.95 288.5 22 11 3 8 3620.91 268.772 17 11 3 8 3329.51 266.594 9 -11 3 -9 543.894 100.421 12 11 3 9 527.501 115.076 22 11 3 9 485.738 95.4004 17 11 3 9 510.622 99.0076 9 -11 3 -10 255.689 66.836 12 11 3 10 167.536 64.0952 22 11 3 10 202.586 54.4291 17 11 3 10 301.466 74.7482 9 11 3 11 833.521 133.728 22 11 3 11 997.41 125.946 17 11 3 11 1007.18 126.908 9 11 3 12 276.068 75.5334 22 11 3 12 280.732 62.6537 17 11 3 12 324.491 65.0752 9 11 3 13 46.8594 24.0404 22 11 3 13 115.082 37.9497 17 11 3 13 40.1476 24.559 9 11 3 14 674.086 88.9962 22 11 3 14 805.31 90.5605 17 11 3 14 842.567 89.8499 9 11 3 15 41.6575 19.7135 9 -11 5 10 227.562 46.5723 21 -11 5 9 244.791 51.454 21 11 5 -9 200.803 45.2081 10 -11 5 8 117.423 38.2109 21 -11 5 8 113.673 46.2038 20 11 5 -8 201.676 48.6908 10 -11 5 7 38.312 31.699 21 -11 5 7 11.3742 23.8427 20 11 5 -7 81.8524 42.2239 10 -11 5 6 164.822 57.923 21 -11 5 6 93.523 48.1475 20 11 5 -6 73.5818 37.445 10 11 5 -5 1934.93 182.713 23 -11 5 5 2356.84 207.041 20 11 5 -5 2271.23 206.507 10 11 5 -4 2068.23 194.444 23 -11 5 4 2541.18 217.538 20 11 5 -4 2163.64 211.217 10 11 5 -3 751.494 119.541 23 -11 5 3 824.435 123.443 20 11 5 -3 708.465 122.362 10 11 5 -2 442.865 91.8363 23 -11 5 2 583.614 107.165 20 11 5 -2 534.32 108.614 10 11 5 -1 738.82 121.565 23 -11 5 1 787.161 124.993 20 11 5 -1 736.147 122.89 10 11 5 0 208.155 70.4865 23 -11 5 0 339.476 75.822 12 -11 5 0 336.37 86.0053 20 11 5 0 367.623 85.9374 10 -11 5 -1 678.543 105.859 12 11 5 1 555.437 111.847 23 -11 5 -1 828.904 133.737 20 11 5 1 713.647 117.556 10 11 5 2 83.2888 37.5628 23 -11 5 -2 106.745 48.6985 12 -11 5 -2 143.03 67.0776 20 11 5 2 73.8153 46.0047 10 11 5 3 504.395 108.087 23 -11 5 -3 385.798 82.6321 12 -11 5 -3 416.867 98.4731 20 11 5 4 425.337 96.3331 23 -11 5 -4 322.453 75.8492 12 -11 5 -4 339.986 86.7821 20 11 5 4 265.152 69.1058 17 11 5 5 281.993 74.0676 23 -11 5 -5 321.826 76.9305 12 -11 5 -5 366.665 83.5486 20 11 5 5 341.475 81.0574 17 -11 5 -6 1538.31 161.766 12 11 5 6 1801.52 179.742 23 11 5 6 1677.6 161.585 9 11 5 6 1588.41 169.637 17 11 5 7 96.8381 40.0991 23 -11 5 -7 114.087 47.9378 12 11 5 7 59.0524 42.9217 17 11 5 7 98.5811 26.3092 9 -11 5 -8 59.5541 30.719 12 11 5 8 47.793 22.2849 17 11 5 8 22.6186 19.3284 9 -11 5 -9 416.011 70.1906 12 11 5 9 629.447 87.3892 17 11 5 9 456.267 77.2749 9 -11 5 -10 1760.89 130.115 12 11 5 10 1924.43 141.743 17 11 5 10 1826.07 142.576 9 11 5 11 275.831 47.0648 17 11 5 11 182.994 39.7547 9 -12 -6 5 41.549 30.1529 30 -12 -6 4 31.5996 28.8339 30 -12 -4 13 191.065 40.3449 11 -12 -4 12 681.752 86.8449 11 -12 -4 12 360.884 67.0401 30 -12 -4 11 117.888 42.5697 11 -12 -4 11 102.838 43.9975 30 -12 -4 10 303.883 68.0096 11 -12 -4 10 225.775 69.2976 30 -12 -4 9 26.5215 33.6906 11 -12 -4 9 81.329 37.2448 30 -12 -4 8 511.827 110.653 30 -12 -4 8 592.474 104.767 11 -12 -4 7 392.022 89.3644 11 -12 -4 7 185.285 68.8605 30 -12 -4 6 113.993 47.4126 11 -12 -4 6 98.7168 57.6037 30 -12 -4 5 573.821 116.75 11 -12 -4 5 557.344 125.942 30 -12 -4 4 553.737 126.593 30 -12 -4 3 1216.02 186.218 30 -12 -4 2 217.834 90.2571 30 -12 -4 1 1914.99 244.302 30 -12 -4 0 2324.09 271.788 30 -12 -4 -1 968.113 178.343 30 12 -4 2 7080.94 386.239 11 12 -4 3 4523.74 307.473 11 12 -4 4 1463.89 175.18 11 12 -4 5 786.171 129.703 11 12 -4 6 143.107 58.1388 11 12 -4 7 121.311 57.2054 11 12 -4 8 197.782 61.6034 11 12 -4 8 131.39 49.5872 19 12 -4 9 1413.77 161.172 11 12 -4 9 1356.01 163.74 19 12 -4 10 1200.63 136.612 11 12 -4 10 984.495 130.984 19 12 -4 11 394.465 72.4438 11 12 -4 11 312.928 69.0577 19 12 -4 12 2652.21 169.586 11 12 -4 12 2242.82 163.282 19 12 -4 13 279.611 45.1206 11 -12 -2 15 175.297 47.4082 22 -12 -2 15 164.664 36.4158 11 -12 -2 14 2.57902 20.4541 22 -12 -2 14 3.82308 32.8692 18 -12 -2 14 26.8452 17.4848 11 -12 -2 13 636.885 101.136 11 -12 -2 13 551.372 116.138 18 -12 -2 12 173.49 73.1858 18 -12 -2 12 158.77 60.4554 11 -12 -2 11 1385.16 172.167 11 -12 -2 11 1452 205.107 18 -12 -2 10 5782.92 416.61 18 -12 -2 9 3161.47 311.82 18 -12 -2 9 1873.44 228.411 30 -12 -2 8 2390.34 274.489 18 -12 -2 8 2237.94 247.931 30 -12 -2 7 2466.23 288.003 18 -12 -2 7 2618.63 267.806 30 -12 -2 6 2649.7 297.436 18 -12 -2 6 2623.39 263.359 30 12 -2 -5 1876.26 407.877 2 -12 -2 5 1407.62 189.609 30 -12 -2 5 1350.55 209.06 18 -12 -2 5 941.4 313.022 28 12 -2 -4 1032.93 264.178 6 -12 -2 4 1011.89 260.159 3 -12 -2 4 901.153 149.322 30 12 -2 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1467.1 189.018 19 12 -2 5 1580.55 333.531 6 12 -2 5 1321.9 166.54 14 12 -2 5 1500.96 389.444 29 12 -2 6 814.774 136.774 11 12 -2 6 942.688 155.993 19 12 -2 6 624.714 118.321 14 12 -2 7 7313.8 424.784 11 12 -2 7 6715.32 442.59 19 12 -2 7 6530.44 412.783 14 12 -2 8 728.566 128.428 11 12 -2 8 795.269 150.396 19 12 -2 8 682.608 135.496 14 12 -2 9 1140.19 160.078 11 12 -2 9 1289.65 183.483 19 12 -2 9 1171.64 175.761 14 12 -2 10 258.842 72.1784 11 12 -2 10 374.461 98.0091 19 12 -2 10 242.22 81.8174 14 12 -2 11 54.4911 34.5901 11 12 -2 11 115.432 63.3742 19 12 -2 11 17.9543 28.5173 14 12 -2 12 2938.88 216.696 11 12 -2 12 2867.32 236.207 19 12 -2 12 2862.53 241.299 14 12 -2 13 218.634 55.6698 11 12 -2 13 230.685 62.0959 19 12 -2 13 278.603 71.5916 14 12 -2 14 3.33008 17.9303 19 12 -2 14 19.7381 18.2342 14 12 -2 15 1059.92 109.138 19 12 -2 15 1173.3 112.054 14 -12 0 16 184.815 45.841 22 -12 0 15 728.21 112.833 22 -12 0 15 387.713 84.7285 18 -12 0 14 576.783 108.014 22 -12 0 14 363.911 91.2283 18 -12 0 13 46.8316 35.6853 18 -12 0 12 73.6136 62.6298 18 -12 0 12 121.615 51.1492 13 -12 0 11 5.04772 62.7654 18 -12 0 11 -18.1639 47.3485 16 -12 0 11 0.60033 33.6114 13 -12 0 10 88.8713 39.1664 16 -12 0 10 59.727 34.5229 13 -12 0 9 48.0968 45.4807 18 -12 0 9 130.851 58.8965 16 -12 0 8 68.0157 66.0225 18 -12 0 8 28.1715 26.6683 16 12 0 -8 81.7293 48.6225 10 -12 0 7 1431.03 217.079 18 12 0 -7 1044.1 149.729 10 -12 0 7 1055.8 140.354 16 12 0 -7 1167.26 304.814 2 -12 0 7 1532.35 401.098 28 -12 0 7 1181.91 315.371 25 12 0 -6 968.867 291.379 2 -12 0 6 1208.39 325.915 28 12 0 -6 1226.06 321.168 26 -12 0 6 942.477 266.737 25 12 0 -5 231.814 118.437 2 -12 0 5 233.286 138.82 28 12 0 -5 282.789 173.065 26 -12 0 5 603.193 206.088 25 -12 0 4 2070.4 338.396 3 12 0 -4 1933.13 364.8 2 -12 0 4 1944.53 399.884 28 12 0 -4 1983.97 428.085 26 -12 0 3 6033 570.168 3 -12 0 3 5929.18 681.393 28 12 0 -3 4781.49 645.891 26 -12 0 2 834.135 206.79 3 -12 0 2 1224.14 294.429 28 12 0 -2 1261.89 324.939 26 12 0 -1 42.4619 33.0619 7 -12 0 1 -47.4547 59.4957 3 -12 0 1 30.5234 57.0186 28 12 0 -1 64.1825 100.69 26 12 0 0 871 228.811 7 -12 0 0 709.116 198.623 3 -12 0 0 918.15 248.424 28 12 0 0 1071.63 278.816 26 12 0 1 4576.35 552.188 7 -12 0 -1 4284.48 485.507 3 -12 0 -1 4254.05 538.617 28 -12 0 -1 4012.1 539.339 27 12 0 1 4184.81 532.775 26 12 0 2 1898.46 386.685 7 -12 0 -2 1606.42 299.806 3 -12 0 -2 1680.53 325.777 1 -12 0 -2 1251.56 288.618 28 -12 0 -2 949.975 263.266 27 12 0 2 1229.91 276.72 26 -12 0 -3 69.15 70.46 1 12 0 3 128.757 100.434 7 -12 0 -3 61.8084 99.8166 3 -12 0 -3 196.005 170.879 28 -12 0 -3 32.8413 59.6051 27 12 0 3 -13.1487 55.6544 26 12 0 4 23448.4 1388.38 7 -12 0 -4 21040 1227.06 3 -12 0 -4 20334.1 1215.89 1 -12 0 -5 16073.8 1118.74 3 -12 0 -5 13929.9 1098.91 27 -12 0 -5 16174.8 1120.63 1 12 0 6 1280.74 312.912 7 -12 0 -6 1375.35 329.667 1 -12 0 -6 1113.77 300.293 3 -12 0 -6 663.79 241.209 27 12 0 7 14.9863 31.7276 22 12 0 7 24.9013 54.3441 7 -12 0 -7 140.029 129.157 1 12 0 7 64.2977 46.2942 19 12 0 7 25.0688 20.1169 14 12 0 8 194.547 66.3505 22 12 0 8 134.033 63.7967 19 12 0 8 144.363 65.5421 14 12 0 9 1352.31 193.421 22 12 0 9 1717.14 205.427 19 12 0 9 1737.27 211.439 14 12 0 10 3194.58 303.36 22 12 0 10 3660.57 298.065 19 12 0 10 3545.91 302.424 14 12 0 11 257.546 84.2721 22 12 0 11 223.065 72.0436 19 12 0 11 297.33 81.8937 14 12 0 12 25.7736 35.9176 22 12 0 12 38.2551 35.5479 19 12 0 12 105.578 50.3649 14 12 0 13 19.2739 22.1944 22 12 0 13 96.8193 42.4744 19 12 0 13 114.14 46.7565 14 12 0 14 -9.43009 22.3714 22 12 0 14 -9.78832 22.7864 19 12 0 14 7.45329 21.3207 14 12 0 14 -13.89 21.4078 9 12 0 15 31.3839 26.3502 22 12 0 15 4.46659 15.3055 14 12 0 15 24.7566 18.5841 9 12 0 16 113.613 33.4262 22 12 0 16 169.374 35.7463 9 -12 2 15 199.411 42.8401 16 -12 2 15 185.818 43.3294 13 -12 2 14 12.5037 22.663 16 -12 2 14 41.023 28.7441 13 -12 2 13 667.898 108.645 16 -12 2 13 726.48 110.67 13 -12 2 12 183.851 63.4335 16 -12 2 12 172.139 60.5829 13 -12 2 11 1394.59 178.612 16 -12 2 11 1649.57 190.701 13 -12 2 10 5436.08 366.818 16 -12 2 10 5544.58 368.218 13 -12 2 9 3095.26 226.59 21 -12 2 9 2916.64 275.305 20 -12 2 9 2142.16 280.849 18 12 2 -9 3146.69 249.21 10 -12 2 9 3111.89 273.562 16 -12 2 9 3263.73 282.24 13 -12 2 8 2067.33 191.908 21 -12 2 8 1639.79 208.652 20 12 2 -8 2008.33 200.03 10 -12 2 7 2852.47 225.147 21 -12 2 7 2577.96 249.793 20 12 2 -7 2638.32 232.912 10 -12 2 7 3334.08 273.889 16 -12 2 6 2765.81 251.051 20 12 2 -6 2641.8 234.486 10 -12 2 6 3362.41 266.346 16 -12 2 5 1609.86 188.977 20 12 2 -5 1859.26 198.777 10 12 2 -5 1675.63 384.191 2 -12 2 5 1869.66 189.953 16 12 2 -5 1518.72 176.812 15 -12 2 5 1538.25 374.068 28 -12 2 5 1598.08 362.534 25 -12 2 4 1074.78 149.122 20 12 2 -4 1038.27 150.423 10 -12 2 4 1092.12 138.891 16 -12 2 4 1372.56 344.256 28 -12 2 4 774.789 237.458 25 -12 2 3 8119.19 835.751 28 -12 2 3 6574.47 684.491 25 -12 2 3 7425.59 782.641 24 -12 2 2 4232.76 598.03 28 -12 2 2 3430.55 477.299 25 -12 2 2 4201.17 575.513 24 12 2 -1 6757.85 637.068 7 -12 2 1 7947.66 806.924 28 -12 2 1 6651.28 720.42 24 12 2 0 12968.8 918.689 7 -12 2 0 12592.5 1017.35 28 -12 2 0 12579.7 1000.45 24 12 2 1 6184.25 655.577 7 -12 2 -1 5609.44 627.559 1 -12 2 -1 5889.38 699.302 28 -12 2 -1 5776.12 678.114 24 12 2 2 3314.89 483.892 8 12 2 2 3822 542.932 7 -12 2 -2 2899.68 499.336 27 -12 2 -2 3541.97 498.265 1 12 2 3 812.94 236.44 8 12 2 3 1085.39 298.137 7 -12 2 -3 766.011 229.643 1 -12 2 -3 625.897 226.78 27 -12 2 -4 866.5 135.166 12 12 2 4 1078.05 152.82 22 12 2 4 1557.56 368.149 7 -12 2 -4 1130.76 283.832 1 12 2 4 922.143 136.572 19 12 2 4 1035.36 142.014 15 -12 2 -4 1015.5 304.397 27 -12 2 -5 1115.77 158.297 12 12 2 5 1463.95 179.151 22 12 2 5 1361.48 174.223 19 -12 2 -5 1540.19 348.616 3 12 2 5 1431.26 177.216 15 -12 2 -6 511.805 105.434 12 12 2 6 544.486 116.295 22 12 2 6 564.531 121.388 19 12 2 6 516.052 107.483 15 12 2 6 452.91 96.3094 9 -12 2 -7 6587.43 379.519 12 12 2 7 7842.48 451.796 22 12 2 7 6653.3 425.286 19 12 2 7 6622.85 413.704 15 12 2 7 6617.57 381.941 9 -12 2 -8 682.207 116.548 12 12 2 8 929.361 157.364 22 12 2 8 868.525 151.008 19 12 2 8 749.345 134.045 15 12 2 8 821.547 130.558 9 12 2 9 1033.54 168.387 22 12 2 9 724.716 139.46 19 12 2 9 759.759 131.236 15 12 2 9 1060.12 141.273 9 12 2 10 139.632 60.4477 22 12 2 10 220.698 66.9226 17 12 2 10 146.164 50.511 9 12 2 11 53.1102 39.7095 22 12 2 11 155.366 52.1886 17 12 2 11 55.15 32.1276 9 12 2 12 2832.23 249.191 22 12 2 12 3332.65 234.417 17 12 2 12 2789.47 197.047 9 12 2 13 281.102 71.2103 22 12 2 13 219.131 55.7554 17 12 2 13 281.487 59.3583 9 12 2 14 -43.7032 30.011 22 12 2 14 0.6737 20.9916 17 12 2 14 9.33004 13.4162 9 12 2 15 917.208 104.578 22 12 2 15 1105.19 97.1822 9 -12 4 13 251.833 42.1471 16 -12 4 12 593.198 76.1535 16 -12 4 12 520.947 68.7983 13 -12 4 11 111.052 39.7053 16 -12 4 11 34.2601 22.9649 13 -12 4 10 325.205 61.8087 21 12 4 -10 232.483 54.9892 10 -12 4 10 269.548 60.9361 16 -12 4 10 207.076 54.3454 13 -12 4 9 57.6536 40.4198 21 -12 4 9 26.7285 33.3118 20 12 4 -9 -37.547 27.4002 10 -12 4 9 50.7165 35.0381 16 -12 4 9 6.67086 18.7807 13 -12 4 8 640.901 97.4017 21 -12 4 8 643.928 117.196 20 12 4 -8 541.667 94.0022 10 -12 4 8 607.58 102.364 16 -12 4 8 541.167 94.1638 13 -12 4 7 219.366 61.9307 21 -12 4 7 256.662 78.4036 20 12 4 -7 260.945 68.248 10 -12 4 7 205.981 65.2668 16 -12 4 7 239.847 66.5688 13 -12 4 6 125.737 48.2333 20 -12 4 6 64.5472 40.8167 16 -12 4 6 97.6029 46.0829 13 -12 4 5 544.015 107.01 20 12 4 -5 431.078 97.3034 10 -12 4 5 422.128 96.9536 16 12 4 -4 416.095 91.3267 23 -12 4 4 583.71 110.842 20 12 4 -4 500.714 105.946 10 12 4 -3 938.199 139.536 23 -12 4 3 1491.87 176.78 20 12 4 -3 1238.66 172.393 10 12 4 -2 191.489 64.7985 23 -12 4 2 191.93 69.2597 20 12 4 -2 131.749 53.5574 10 -12 4 1 1720.47 177.007 12 12 4 -1 1613.01 186.246 23 -12 4 1 2236.52 225.89 20 12 4 -1 1681.76 203.154 10 -12 4 0 2072.21 197.238 12 12 4 0 2039.17 214.358 23 -12 4 0 2289.56 238.351 20 12 4 0 2101.47 220.652 10 12 4 0 2405.79 220.17 15 -12 4 -1 1011.24 139.492 12 12 4 1 988.211 153.594 23 -12 4 -1 1303.67 179.538 20 12 4 1 1072.74 150.701 10 12 4 1 1184.3 157.946 15 -12 4 -2 8032.5 410.556 12 12 4 2 7362.04 434.755 23 -12 4 -2 7513.58 452.215 20 12 4 2 8167.18 428.532 15 -12 4 -3 4529.05 308.472 12 12 4 3 3930.75 318.325 23 -12 4 -3 3780.81 313.56 20 12 4 3 3752.52 292.617 17 12 4 3 4287.16 314.343 15 -12 4 -4 1087.25 149.133 12 12 4 4 1378.32 186.238 23 -12 4 -4 1291.89 178.865 20 12 4 4 1299.12 175.316 17 12 4 4 1287.84 172.549 15 -12 4 -5 940.048 138.068 12 12 4 5 1108.53 162.711 23 12 4 5 898.032 144.453 17 12 4 5 595.71 120.069 15 12 4 6 84.3208 48.8738 23 -12 4 -6 100.762 49.4542 12 12 4 6 123.055 51.7622 17 12 4 6 101.94 49.3403 9 12 4 7 76.5037 34.9635 23 -12 4 -7 77.7742 42.2 12 12 4 7 90.5554 43.4917 17 12 4 7 72.1834 40.3371 9 12 4 8 142.078 47.3369 23 -12 4 -8 113.085 46.9681 12 12 4 8 94.4453 45.7474 17 12 4 8 155.845 46.0824 9 -12 4 -9 1292.51 140.101 12 12 4 9 1503.12 152.277 17 12 4 9 1196.04 142.222 9 -12 4 -10 1188.3 124.735 12 12 4 10 1228.29 128.868 17 12 4 10 1319.34 139.457 9 -12 4 -11 203.331 47.4813 12 12 4 11 247.714 56.3367 17 12 4 11 259.805 58.1505 9 12 4 12 2461.52 156.644 17 12 4 12 2602.38 161.285 9 12 4 13 335.454 48.7194 17 12 4 13 367.867 50.3073 9 12 6 -6 107.968 32.454 12 -12 6 5 19.5385 19.5743 20 12 6 -4 94.3551 32.3645 23 -12 6 4 109.828 41.0846 20 12 6 -3 160.235 44.6469 23 -12 6 3 200.356 58.5338 20 12 6 -2 21.5354 19.9008 23 -12 6 2 54.4147 34.8835 20 12 6 -1 78.7916 38.1249 23 -12 6 1 139.881 53.7755 20 12 6 0 176.509 53.5595 23 -12 6 0 258.305 67.9097 20 12 6 1 343.118 73.3975 23 -12 6 -1 341.244 58.7728 12 -12 6 -1 509.843 93.9004 20 12 6 2 136.866 48.2376 23 -12 6 -2 100.578 31.564 12 -12 6 -2 141.465 48.4661 20 12 6 3 101.091 40.3101 23 -12 6 -3 52.9107 27.2671 12 -12 6 -3 120.588 45.2164 20 12 6 4 317.059 67.137 23 -12 6 -4 242.256 55.2708 12 -12 6 -4 405.551 74.2591 20 -12 6 -5 672.6 87.1669 12 12 6 5 540.121 77.9745 23 -12 6 -6 195.608 44.6959 12 -13 -5 9 -8.73531 14.8912 30 -13 -5 8 220.65 47.1644 11 -13 -5 8 188.358 49.2257 30 -13 -5 7 264.006 69.4875 30 -13 -5 6 306.611 75.6329 30 -13 -5 5 344.498 88.0444 30 -13 -5 4 454.403 108.215 30 -13 -5 3 460.403 106.465 30 -13 -5 2 291.906 89.128 30 -13 -5 1 88.9931 45.951 30 -13 -5 0 40.746 40.0725 30 13 -5 4 697.848 102.769 11 13 -5 5 764.292 109.681 11 13 -5 6 814.653 112.421 11 13 -5 7 145.099 45.3834 11 13 -5 8 294.465 59.0866 11 13 -5 9 517.414 72.9719 11 -13 -3 14 390.974 56.1967 11 -13 -3 13 66.518 29.1292 11 -13 -3 12 75.5559 35.1819 11 -13 -3 11 415.861 93.073 18 -13 -3 11 550.133 96.0182 11 -13 -3 11 353.819 85.5443 30 -13 -3 10 134.778 46.4165 18 -13 -3 10 187.071 61.1543 11 -13 -3 10 129.905 58.6586 30 -13 -3 9 401.883 107.533 18 -13 -3 9 223.039 69.5545 11 -13 -3 9 174.89 62.1982 30 -13 -3 8 1343.11 197.755 18 -13 -3 8 1453.19 198.751 30 -13 -3 7 5.18468 41.9299 18 -13 -3 7 72.6805 54.2628 30 -13 -3 6 70.2424 51.6031 30 -13 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355.923 65.9944 19 13 -3 14 1108.14 99.4301 19 -13 -1 15 77.6575 35.7049 22 -13 -1 14 84.3659 42.4755 22 -13 -1 14 93.5569 48.4649 18 -13 -1 13 265.051 76.9176 18 -13 -1 13 254.794 63.879 11 -13 -1 12 51.7108 38.3193 18 -13 -1 12 -7.91124 25.208 11 -13 -1 11 1042.54 173.536 18 -13 -1 10 157.879 86.2977 18 -13 -1 9 2647.85 302.54 18 -13 -1 8 3400.14 340.365 18 13 -1 -8 3255.59 276.702 10 -13 -1 7 2464.32 288.642 18 -13 -1 6 1049.51 188.373 18 -13 -1 6 995.91 156.976 30 -13 -1 5 65.0443 40.8478 30 -13 -1 5 21.4256 75.8879 18 -13 -1 5 339.417 146.695 3 13 -1 -5 217.069 154.564 2 -13 -1 5 -247.268 150.989 28 13 -1 -5 -261.218 172.526 26 -13 -1 5 120.084 98.7302 25 -13 -1 4 1113.11 264.237 3 -13 -1 4 1044.52 297.128 28 13 -1 -4 978.506 306.715 26 -13 -1 3 3945.74 512.583 3 -13 -1 3 3643.75 537.95 28 13 -1 -3 3452.11 575.43 26 -13 -1 2 1094.34 258.422 3 -13 -1 2 707.472 231.315 28 13 -1 -2 584.81 216.347 26 13 -1 -1 1373.75 302.53 7 -13 -1 1 1666.46 318.766 3 -13 -1 1 1665.56 358.774 28 13 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390.923 101.983 22 13 -1 9 509.892 101.156 11 13 -1 9 391.879 97.2656 19 13 -1 9 581.339 120.839 14 13 -1 10 7807.44 479.378 22 13 -1 10 6253.91 369.878 11 13 -1 10 10464.8 506.683 19 13 -1 10 8934.54 486.582 14 13 -1 11 1264.45 179.758 22 13 -1 11 1574 180.483 19 13 -1 11 1311.71 176.895 14 13 -1 12 723.212 128.169 22 13 -1 12 830.962 124.166 19 13 -1 12 826.073 131.629 14 13 -1 13 149.518 50.4032 22 13 -1 13 144.945 50.8126 19 13 -1 13 146.002 52.0391 14 13 -1 14 482.356 83.7463 22 13 -1 14 489.8 80.4202 19 13 -1 14 565.391 91.6554 14 13 -1 15 311.974 50.4844 15 13 -1 15 416.426 67.0799 19 13 -1 15 398.776 65.965 14 13 -1 15 518.027 67.6265 9 -13 1 15 87.3971 36.2276 22 -13 1 15 67.0069 23.9067 13 -13 1 14 50.5327 37.1218 22 -13 1 14 44.2859 28.3188 16 -13 1 14 42.0927 24.1857 13 -13 1 13 279.159 73.4346 18 -13 1 13 300.082 66.9099 16 -13 1 13 382.918 77.9167 13 -13 1 12 26.8774 33.8126 18 -13 1 12 -8.02166 35.1547 16 -13 1 12 42.5196 42.6795 13 -13 1 11 856.547 156.697 18 -13 1 11 826.119 132.03 16 -13 1 11 892.053 138.384 13 -13 1 10 62.7039 51.1754 18 -13 1 10 -8.69194 33.8408 16 -13 1 10 48.6294 44.3969 13 -13 1 9 2660.02 308.638 18 13 1 -9 2489.55 226.859 10 -13 1 9 2332.45 234.414 16 -13 1 9 2810.93 257.127 13 -13 1 8 3577.37 301.416 20 13 1 -8 3597.84 276.746 10 -13 1 8 3909.1 298.397 16 -13 1 7 2444.86 243.232 20 13 1 -7 2703.47 239.488 10 -13 1 7 2666.55 242.163 16 -13 1 6 803.596 139.708 20 13 1 -6 1031.24 149.117 10 -13 1 6 1112.87 152.48 16 -13 1 5 13.57 29.7784 20 13 1 -5 60.5298 46.9457 10 -13 1 5 149.489 62.4764 16 -13 1 5 217.025 144.582 28 13 1 -5 56.6192 88.8496 26 -13 1 5 26.6243 66.3554 25 13 1 -4 1190.45 162.828 10 -13 1 4 1112.05 145.957 16 -13 1 4 1502.49 385.968 28 13 1 -4 683.317 265.411 26 -13 1 4 1365.56 324.059 25 -13 1 3 3428.99 550.394 28 13 1 -3 2635.76 520.587 26 -13 1 2 784.024 253.032 28 13 1 -2 260.206 161.54 26 13 1 -1 1457.95 297.382 7 -13 1 1 1470.54 350.772 28 13 1 -1 924.886 295.244 26 13 1 0 4873.45 559.577 7 -13 1 0 4640.11 599.571 28 13 1 1 1665.65 342.556 7 -13 1 -1 1445.02 296.711 3 -13 1 -1 1024.75 280.506 28 13 1 2 14195.4 1085.06 7 -13 1 -2 11684.7 876.915 3 -13 1 -2 12665.2 971.564 1 -13 1 -2 11742.8 999.582 28 -13 1 -2 10929.3 984.927 27 -13 1 -3 614.763 208.129 1 13 1 3 605.803 226.439 7 -13 1 -3 839.722 232.35 3 -13 1 -3 649.423 230.62 27 13 1 4 991.165 145.321 22 -13 1 -4 940.321 262.548 1 13 1 4 1174.49 322.777 7 13 1 4 904.888 135.597 19 13 1 4 935.665 135.099 15 -13 1 -4 1192.85 290.01 3 -13 1 -4 542.737 215.036 27 -13 1 -5 1551.81 182.496 12 13 1 5 1968.12 210.928 22 13 1 5 2036.53 210.671 19 -13 1 -5 2161.2 419.571 3 -13 1 -5 1842.97 419.37 27 13 1 5 1923.18 205.246 15 -13 1 -6 1203.49 158.966 12 13 1 6 1392.5 183.165 22 13 1 6 1341.47 177.549 19 13 1 6 1340.26 175.262 15 -13 1 -7 1297.24 161.487 12 13 1 7 1682.9 206.567 22 13 1 7 1386.72 184.298 19 13 1 7 1414.12 181.179 15 13 1 8 1485.36 197.915 22 13 1 8 1322.92 182.847 19 13 1 8 1383.77 179.128 15 13 1 9 407.371 106.621 22 13 1 9 528.355 117.791 19 13 1 9 626.637 117.075 15 13 1 9 538.795 115.043 14 13 1 10 8430.11 502.538 22 13 1 10 9781.28 486.84 19 13 1 10 10100.3 470.53 15 13 1 10 9164.41 482.053 14 13 1 10 10633.3 437.925 9 13 1 11 1164.54 172.657 22 13 1 11 1045.71 144.147 19 13 1 11 1172.13 145.473 15 13 1 11 1179.19 130.408 9 13 1 12 942.437 146.866 22 13 1 12 866.572 119.234 19 13 1 12 1061.79 136.256 17 13 1 12 792.071 109.689 15 13 1 12 953.942 109.897 9 13 1 13 188.029 63.6953 22 13 1 13 215.602 60.0697 17 13 1 13 202.715 49.8296 9 13 1 14 502.582 89.9226 22 13 1 14 437.027 66.3804 9 13 1 15 516.986 79.46 22 13 1 15 565.28 69.5665 9 -13 3 14 535.48 67.0832 16 -13 3 14 503.93 65.3049 13 -13 3 13 78.6964 34.3996 16 -13 3 13 65.1601 29.603 13 -13 3 12 111.463 44.8532 16 -13 3 12 108.525 40.573 13 -13 3 11 608.315 101.534 16 -13 3 11 682.723 106 13 -13 3 10 163.237 60.6824 20 13 3 -10 162.059 52.8184 10 -13 3 10 138.623 52.8611 16 -13 3 10 200.815 65.3878 13 -13 3 9 233.744 59.0863 21 -13 3 9 250.024 80.8913 20 13 3 -9 251.647 65.8417 10 -13 3 9 216.33 73.7293 16 -13 3 9 280.112 76.623 13 -13 3 8 1548.98 156.348 21 -13 3 8 1082.88 161.356 20 13 3 -8 1465.09 163.096 10 -13 3 8 1327.5 165.828 16 -13 3 8 1437.86 169.447 13 -13 3 7 -15.7082 41.1104 20 13 3 -7 -19.6624 17.6884 10 -13 3 7 -37.1833 35.4776 13 -13 3 6 46.4082 24.2959 20 13 3 -6 7.74643 30.9666 10 -13 3 6 28.9016 23.5863 16 -13 3 6 20.828 26.8981 13 -13 3 5 922.811 146.011 20 13 3 -5 870.973 134.453 10 -13 3 5 1040.43 144.422 16 -13 3 4 1061.11 156.807 20 13 3 -4 1080.67 158.821 10 -13 3 4 974.475 135.743 16 -13 3 3 811.529 142.883 20 -13 3 3 805.626 122.57 16 13 3 -3 674.546 129.259 10 13 3 -3 892.35 136.945 15 -13 3 2 4583.94 299.73 12 -13 3 2 5835.97 380.615 20 13 3 -2 4794.67 355.499 10 -13 3 2 4662.94 299.992 16 13 3 -2 4901.59 319.754 15 -13 3 1 7371.9 385.126 12 -13 3 1 8761.5 482.762 20 13 3 -1 7730.73 455.936 10 -13 3 1 7236.33 374.069 16 13 3 -1 7595.77 397.807 15 -13 3 0 739.086 117.64 12 -13 3 0 886.911 152.565 20 13 3 0 900.88 144.406 10 -13 3 0 813.976 117.712 16 13 3 0 731.252 117.309 15 -13 3 -1 4654.97 312.615 12 -13 3 -1 4661.63 364.416 20 13 3 1 5363.55 348.701 10 13 3 1 4727.78 308.779 15 -13 3 -2 198.069 72.8678 12 -13 3 -2 215.6 80.7086 20 13 3 2 228.973 73.0014 10 13 3 2 252.747 73.2803 15 -13 3 -3 6588.26 388.964 12 -13 3 -3 6669.26 430.962 20 13 3 3 5908.03 408.129 17 13 3 3 7408 406.741 15 -13 3 -4 4894.73 338.385 12 13 3 4 5653.38 397.681 17 13 3 4 5686.77 363.309 15 13 3 5 256.062 78.4885 22 -13 3 -5 321.966 84.3262 12 13 3 5 304.818 92.9578 17 13 3 5 169.567 64.7728 15 -13 3 -6 539.41 107.497 12 13 3 6 765.171 140.695 22 13 3 6 576.356 111.876 17 13 3 6 500.971 110.787 15 13 3 6 559.377 105.094 9 -13 3 -7 1218.95 158.502 12 13 3 7 1293.11 181.392 22 13 3 7 1235.56 161.461 17 13 3 7 1107 159.542 15 13 3 7 870.824 130.055 9 -13 3 -8 128.196 47.5438 12 13 3 8 106.248 56.649 22 13 3 8 57.9088 32.4958 17 13 3 8 114.923 48.6631 15 13 3 8 148.058 54.4666 9 -13 3 -9 2299.01 202.424 12 13 3 9 2290.42 236.078 22 13 3 9 2162.57 195.386 17 13 3 9 2549.81 214.682 9 -13 3 -10 -5.1383 17.2595 12 13 3 10 53.2198 25.1626 22 13 3 10 53.1623 31.9671 17 13 3 11 2702.91 194.078 17 13 3 11 2872.69 197.446 9 13 3 12 1304.3 142.578 22 13 3 12 1446.57 132.82 17 13 3 12 1449.54 128.207 9 13 3 13 353.193 63.9712 22 13 3 13 366.591 60.5244 17 13 3 13 394.443 59.0142 9 13 3 14 1205.65 90.8955 9 13 5 -9 35.4664 19.3505 10 -13 5 8 167.32 45.364 20 13 5 -8 341.276 57.02 10 -13 5 7 259.092 62.2643 20 13 5 -7 458.321 73.3739 10 -13 5 6 247.205 65.3607 20 13 5 -6 379.744 74.1128 10 -13 5 5 351.84 78.9225 20 13 5 -5 437.92 83.7656 10 13 5 -4 267.257 63.1345 23 -13 5 4 404.122 86.6739 20 13 5 -4 424.601 90.076 10 13 5 -3 368.177 77.3638 23 -13 5 3 431.661 90.8643 20 13 5 -3 353.098 84.3798 10 13 5 -2 434.205 81.9718 23 -13 5 2 503.841 98.2185 20 13 5 -2 399.445 85.8473 10 13 5 -1 149.013 55.1596 23 -13 5 1 231.555 72.3293 20 13 5 -1 225.098 66.2511 10 13 5 0 49.4861 42.0841 23 -13 5 0 48.9931 18.6303 12 13 5 0 25.5392 19.2464 10 -13 5 -1 510.027 89.8306 12 13 5 1 376.239 91.0356 23 -13 5 -1 463.438 106.016 20 13 5 1 474.251 89.8227 10 13 5 2 193.434 65.6168 23 -13 5 -2 176.556 54.9813 12 -13 5 -2 178.681 67.5671 20 13 5 2 188.501 53.2316 10 13 5 3 283.4 77.01 23 -13 5 -3 326.468 75.3301 12 -13 5 -3 246.209 64.773 20 -13 5 -4 617.499 103.081 12 13 5 4 689.096 117.539 23 -13 5 -4 730.874 113.188 20 -13 5 -5 758.777 111.038 12 13 5 5 786.552 122.517 23 13 5 5 504.867 83.572 17 -13 5 -6 930.963 116.276 12 13 5 6 956.264 120.055 23 13 5 6 728.306 103.055 17 13 5 7 292.334 58.9754 23 -13 5 -7 303.752 63.0052 12 13 5 7 252.591 56.3391 17 -13 5 -8 280.546 54.9478 12 13 5 8 307.604 58.7674 17 -13 5 -9 391.107 58.541 12 13 5 9 402.353 59.6144 17 -14 -4 11 953.352 93.2288 11 -14 -4 11 619.315 83.3201 30 -14 -4 10 284.822 58.5057 11 -14 -4 10 156.351 51.0193 30 -14 -4 9 865.396 106.782 11 -14 -4 9 697.898 116.485 30 -14 -4 8 566.459 93.3102 11 -14 -4 8 508.569 106.685 30 -14 -4 7 94.1851 40.0545 11 -14 -4 7 28.7011 27.4129 30 -14 -4 6 20.6567 22.553 11 -14 -4 6 0.07196 40.0318 30 -14 -4 5 250.093 75.6515 11 -14 -4 5 204.694 76.8214 30 -14 -4 4 1066.38 167.384 30 -14 -4 3 2546.18 256.495 30 -14 -4 2 644.573 136.036 30 -14 -4 1 790.982 153.358 30 -14 -4 0 642.275 140.042 30 14 -4 1 547.605 97.3622 11 -14 -4 -1 556.599 131.054 30 14 -4 2 427.044 89.4654 11 -14 -4 -2 162.935 78.243 30 14 -4 3 237.002 69.7341 11 14 -4 4 123.198 54.4374 11 14 -4 5 322.03 81.5279 11 14 -4 6 2336.68 214.511 11 14 -4 7 212.657 66.1924 11 14 -4 8 786.335 115.491 11 14 -4 9 175.289 56.5687 11 14 -4 9 122.756 43.2947 19 14 -4 10 716.503 92.0166 11 14 -4 10 479.508 76.0001 19 14 -4 11 360.327 57.7137 11 -14 -2 14 211.752 51.3092 22 -14 -2 14 152.196 36.2913 11 -14 -2 13 11.332 42.7466 18 -14 -2 13 -8.12995 18.9272 11 -14 -2 12 753.842 109.836 11 -14 -2 12 653.724 116.175 18 -14 -2 11 403.363 100.577 18 -14 -2 11 581.131 105.667 11 -14 -2 10 759.668 147.905 18 -14 -2 9 396.322 101.669 18 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93.672 19 14 -2 11 445.286 90.3843 14 14 -2 12 510.955 79.688 11 14 -2 12 615.903 101.194 19 14 -2 12 486.931 90.9271 14 14 -2 13 1889.6 160.451 19 14 -2 14 65.3379 29.3972 19 -14 0 15 4.81116 15.4166 22 -14 0 14 -5.85074 20.2421 22 -14 0 14 -20.0077 32.435 18 -14 0 13 332.298 84.7296 18 -14 0 12 58.5955 33.1683 18 -14 0 12 52.0474 42.3131 13 -14 0 11 153.841 71.8116 18 -14 0 11 56.5021 36.5291 16 -14 0 11 128.571 47.7007 13 -14 0 10 219.161 70.6267 18 -14 0 10 109.384 53.0528 16 -14 0 10 175.372 55.0642 13 -14 0 9 4277.94 381.372 18 14 0 -9 3913.83 290.105 10 -14 0 9 3485.44 275.043 16 -14 0 8 12.3647 60.0693 18 -14 0 8 59.288 47.5382 16 14 0 -8 13.0301 37.6006 10 -14 0 7 300.104 123.768 18 -14 0 7 271.382 75.4368 16 14 0 -7 212.432 71.3979 10 -14 0 6 262.327 70.6917 16 14 0 -6 270.746 77.405 10 14 0 -5 820.21 140.758 10 -14 0 5 1029.65 138.587 16 -14 0 5 829.957 132.139 12 -14 0 4 104.048 54.0011 12 -14 0 4 19.8694 38.8082 16 14 0 -4 47.768 55.4053 10 -14 0 3 5165.15 399.847 20 14 0 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2692.6 242.458 16 -15 1 9 2853.36 253.839 13 -15 1 8 4373.54 384.452 18 15 1 -8 3538.53 266.456 10 -15 1 8 3620.44 286.87 16 15 1 -7 668.554 119.709 10 -15 1 7 849.763 136.995 16 -15 1 6 1599.45 201.952 20 15 1 -6 1820.73 200.088 10 -15 1 6 1790.6 197.067 16 -15 1 5 3066.23 287.443 20 15 1 -5 3611.51 291.187 10 -15 1 5 4077.9 292.687 16 -15 1 5 3222.69 268.834 12 -15 1 4 760.22 150.468 20 15 1 -4 1047.59 159.809 10 -15 1 4 1079 147.991 16 -15 1 4 946.581 140.907 12 -15 1 3 553.605 130.395 20 -15 1 3 716.49 116.468 16 15 1 -3 622.969 126.583 10 15 1 -3 535.137 104.365 15 -15 1 3 654.996 116.669 12 -15 1 2 3995.47 356.903 20 15 1 -2 4543.69 308.641 15 -15 1 2 5095.44 323.992 12 15 1 -1 4292.71 347.683 10 15 1 -1 3694.64 272.396 15 -15 1 1 4074.18 287.612 12 -15 1 0 589.049 128.218 20 15 1 0 966.267 144.014 19 15 1 0 1162.83 175.134 10 15 1 0 763.362 120.498 15 -15 1 0 992.371 144.741 12 -15 1 -1 4275.93 309.743 12 15 1 1 4077.63 295.269 19 15 1 1 3942.8 282.617 15 -15 1 -2 4220.05 314.297 12 15 1 2 3666.52 281.637 19 15 1 2 4436.85 320.164 10 15 1 2 3892.04 281.992 15 -15 1 -3 1891.57 214.762 12 15 1 3 2076.52 211.944 19 15 1 3 1972.92 204.398 15 15 1 4 -17.914 47.7929 22 15 1 4 30.7066 38.6308 19 15 1 4 19.9546 26.8949 15 -15 1 -5 2947.34 266.068 12 15 1 5 2917.13 271.04 22 15 1 5 2801.19 257.458 19 15 1 5 2594.05 244.667 15 -15 1 -6 1170.15 161.597 12 15 1 6 1355.17 186.084 22 15 1 6 1129.03 166.446 19 15 1 6 884.535 142.265 15 -15 1 -7 125.034 50.9662 12 15 1 7 73.4666 50.0224 22 15 1 7 135.369 62.1859 19 15 1 7 71.6487 45.58 15 15 1 7 124.7 48.2848 9 15 1 8 570.648 111.698 15 15 1 8 615.18 129.38 22 15 1 8 485.689 107.091 19 15 1 8 577.155 98.1522 9 15 1 9 284.141 85.1727 22 15 1 9 283.954 79.985 19 15 1 9 326.328 80.6205 15 15 1 9 265.053 64.882 9 15 1 10 1298.58 180.703 22 15 1 10 1278.95 156.54 19 15 1 10 1404.88 155.519 15 15 1 10 1502.69 144.165 9 15 1 11 757.022 130.398 22 15 1 11 691.824 105.114 19 15 1 11 684.978 98.9825 15 15 1 11 701.909 91.9559 9 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77.4254 44.5765 12 20 0 3 44.6319 28.9284 15 20 0 4 5.46397 24.044 15 -20 0 -4 17.0144 24.4652 12 20 0 5 27.7343 27.3695 19 20 0 5 0.97972 19.6867 15 20 0 6 5.05634 24.0951 19 20 0 6 36.3538 33.7279 15 20 0 7 102.484 42.7378 19 20 0 7 79.6231 39.2667 15 20 0 8 424.03 75.5693 19 20 0 8 374.656 75.0882 15 20 0 9 273.976 55.6502 19 20 0 9 131.586 45.3259 15 -20 2 8 250.558 60.166 18 -20 2 8 182.335 43.4432 16 -20 2 8 205.381 42.7311 13 -20 2 7 80.4514 38.8924 18 20 2 -7 88.9431 31.8321 10 -20 2 7 34.6452 23.6377 16 -20 2 7 59.3931 25.2519 13 -20 2 6 -11.7649 35.7279 18 20 2 -6 89.3965 32.1206 10 -20 2 6 76.1121 31.788 16 -20 2 6 103.594 36.3479 13 -20 2 5 133.915 66.2772 18 20 2 -5 105.234 42.9263 10 -20 2 5 110.025 39.9967 16 -20 2 5 177.385 47.3119 13 20 2 -4 337.515 71.199 10 -20 2 4 239.266 56.7484 16 -20 2 3 154.093 46.6415 12 20 2 -3 264.606 64.4681 10 -20 2 3 257.797 60.3641 16 -20 2 2 37.3556 19.6855 12 20 2 -2 87.7305 39.8397 10 -20 2 2 88.337 41.9711 16 -20 2 1 202.094 56.6164 12 20 2 -1 160.803 51.7842 10 -20 2 1 129.57 41.8749 16 20 2 -1 98.6811 38.6279 15 -20 2 0 316.169 76.0486 12 20 2 0 291.661 64.9921 10 -20 2 0 355.972 70.2172 16 20 2 0 187.185 60.1761 15 -20 2 -1 150.098 54.9579 12 20 2 1 28.3482 20.8696 10 -20 2 -1 125.393 47.8573 16 20 2 1 69.1493 44.613 15 -20 2 -2 1283.56 133.47 16 20 2 2 931.213 126.963 15 -20 2 -2 944.358 133.195 12 -20 2 -3 286.577 70.7326 12 -20 2 -3 332.109 70.3774 16 20 2 3 306.008 77.0697 15 -20 2 -4 317.113 75.0114 12 20 2 4 173.39 51.2915 17 -20 2 -4 189.871 51.8719 16 20 2 4 244.538 65.9185 15 -20 2 -5 71.5045 39.6615 12 20 2 5 35.3534 27.2066 17 -20 2 -5 9.84973 19.9439 16 20 2 5 -0.90872 16.3142 15 -20 2 -6 356.325 66.8772 12 20 2 6 263.86 51.4568 17 -20 2 -6 238.473 46.7152 16 20 2 6 192.21 61.8896 15 -20 2 -7 -6.7842 11.0956 12 20 2 7 35.6414 22.8508 17 20 2 7 1.56154 21.5275 15 20 2 8 298.44 47.1064 17 20 2 8 295.662 52.6719 15 21 -3 -2 88.1854 33.3055 10 -21 -3 2 22.5768 21.795 30 -21 -3 1 267.823 62.0933 30 -21 -3 0 61.3664 32.7577 30 -21 -3 -1 -1.48032 18.6889 30 21 -1 -7 -14.3164 15.3934 10 -21 -1 6 87.2243 37.7981 18 21 -1 -6 82.5216 32.6344 10 -21 -1 5 249.762 69.5227 18 -21 -1 5 169.331 46.2402 30 -21 -1 4 196.858 72.6502 18 21 -1 -4 169.205 49.0387 10 -21 -1 4 99.0419 40.6994 30 -21 -1 3 175.734 43.1709 16 -21 -1 3 169.821 57.4639 30 21 -1 -2 -13.7618 19.8286 10 -21 -1 2 14.5803 14.714 16 21 -1 -1 146.697 55.644 10 -21 -1 1 237.605 52.3898 16 -21 -1 1 147.952 58.0173 30 21 -1 0 217.174 60.2059 10 -21 -1 0 207.159 47.1716 16 -21 -1 0 137.117 61.6292 30 -21 -1 -1 526.299 81.6233 16 21 -1 1 376.05 70.4726 10 -21 -1 -1 537.047 100.855 30 -21 -1 -2 637.686 87.3599 16 -21 -1 -2 390.441 90.0614 30 -21 -1 -3 229.611 69.5497 30 21 -1 4 317.351 66.7023 15 -21 -1 -4 371.131 83.3025 30 21 -1 5 66.2248 33.8399 15 -21 -1 -5 75.3216 39.8151 30 21 -1 6 104.078 34.6742 15 -21 -1 -6 112.604 39.7153 30 21 -1 7 -1.88102 14.7133 15 -21 1 7 7.79846 21.3825 18 21 1 -7 -7.76785 12.9756 10 -21 1 7 -26.2343 16.4519 16 -21 1 7 -17.6139 20.3933 13 -21 1 6 87.8514 39.3165 18 21 1 -6 48.9654 29.6218 10 -21 1 6 93.2084 37.4714 16 -21 1 6 45.9881 29.6641 13 -21 1 5 311.795 82.5652 18 21 1 -5 338.171 64.1648 10 -21 1 5 343.819 64.019 16 -21 1 4 180.095 65.3871 18 21 1 -4 52.3115 27.827 10 -21 1 4 203.941 52.8266 16 -21 1 3 281.32 87.5818 18 21 1 -3 338.171 71.3343 10 -21 1 3 272.539 55.6853 16 -21 1 2 -1.24689 49.8059 18 21 1 -2 15.7205 25.8831 10 -21 1 2 51.0282 32.9357 16 21 1 -1 143.962 49.0855 10 -21 1 1 232.725 53.5422 16 -21 1 1 153.174 49.2223 30 -21 1 1 227.346 61.2354 12 -21 1 0 228.46 63.1785 12 21 1 0 159.066 45.4238 10 -21 1 0 194.385 54.1368 16 21 1 0 136.697 44.6983 15 -21 1 -1 475.248 95.2041 12 -21 1 -1 608.697 87.3118 16 21 1 1 324.73 60.6508 10 21 1 1 350.235 77.7449 15 -21 1 -2 449.968 89.604 12 -21 1 -2 634.89 88.6022 16 21 1 2 374.145 81.0907 15 -21 1 -3 413.12 83.6096 12 -21 1 -3 456.88 75.0085 16 21 1 3 314.595 79.3157 15 -21 1 -4 375.333 75.3182 12 -21 1 -4 457.011 74.4146 16 21 1 4 340.899 79.6097 15 -21 1 -5 93.6203 41.5153 12 -21 1 -5 85.552 35.1295 16 21 1 5 128.277 42.3397 15 21 1 6 132.45 36.2482 17 -21 1 -6 171.568 41.7301 16 21 1 6 128.452 40.1054 15 21 1 7 -33.5544 24.2627 17 -21 1 -7 -28.0381 18.4238 16 21 1 7 8.50691 11.5389 15 -21 3 2 69.2 45.1121 18 -21 3 0 146.708 37.9924 12 -21 3 -1 21.6016 16.6936 12 -21 3 -2 53.4586 28.2845 12 22 -2 -2 5.98264 17.6043 10 -22 -2 2 29.292 27.1014 30 -22 -2 1 32.1342 25.1597 30 -22 -2 0 115.815 45.1556 30 -22 -2 -1 63.1988 27.5904 30 -22 -2 -2 379.282 69.0718 30 22 0 -5 228.184 49.167 10 -22 0 5 156.075 36.3077 13 -22 0 4 29.4366 28.6592 18 22 0 -4 79.4693 35.4414 10 -22 0 4 54.8836 26.4609 16 -22 0 3 80.372 47.5995 18 22 0 -3 91.8723 39.2332 10 -22 0 3 111.565 32.2309 16 -22 0 2 -16.2267 44.7296 18 22 0 -2 -5.08551 20.8548 10 -22 0 2 -4.84557 17.1666 16 -22 0 2 7.1213 17.332 30 22 0 -1 1.46621 20.2052 10 -22 0 1 12.7548 15.3241 16 -22 0 1 29.8097 19.0813 30 22 0 0 126.469 39.0903 10 -22 0 0 180.033 45.6969 16 -22 0 0 126.783 43.8602 30 -22 0 -1 468.742 71.0869 16 -22 0 -1 320.192 74.4051 30 -22 0 -2 8.42723 17.7823 16 -22 0 -2 -23.6903 23.8614 30 -22 0 -3 43.0247 31.9176 16 22 0 3 18.7717 18.9343 15 -22 0 -3 30.7532 27.7799 30 -22 0 -4 234.109 48.2314 16 22 0 4 178.485 51.1982 15 -22 0 -4 209.047 58.6978 30 -22 0 -5 893.12 89.8208 16 -22 0 -5 438.321 78.3559 30 -22 2 2 65.6174 33.3795 18 -22 2 2 15.8192 16.9843 16 -22 2 1 0.45171 25.7141 18 -22 2 1 91.668 31.749 16 -22 2 0 206.949 78.0692 18 -22 2 0 218.761 47.2994 16 -22 2 -1 130.083 37.1147 16 -22 2 -2 695.384 87.9325 12 _iucr_refine_instructions_details ; fxm-lww-4-cl.res created by SHELXL-2014/7 TITL fxm-lww-4-cl_a.res in C2 REM Old TITL fxm-lww-4-cl in C2 #5 REM SHELXT solution in C2 REM R1 0.159, Rweak 0.069, Alpha 0.004, Orientation as input REM Flack x = 0.096 ( 0.019 ) from Parsons' quotients REM Formula found by SHELXT: C36 N3 O6 Cl2 CELL 1.54184 18.64345 6.199883 15.81215 90 90.1374 90 ZERR 4 0.000691 0.000208 0.000566 0 0.0034 0 LATT -7 SYMM -X,+Y,-Z SFAC C H Cl O UNIT 76 104 4 14 L.S. 10 PLAN 20 BOND $H LIST 6 MORE -1 CONF fmap 2 acta SHEL 999 0.837 REM REM REM WGHT 0.108000 0.091000 FVAR 3.83368 CL01 3 0.436867 -0.036710 0.886622 11.00000 0.12078 0.11891 = 0.07683 0.03441 -0.01601 0.02665 O002 4 0.264627 0.521601 0.468574 11.00000 0.06053 0.06203 = 0.06275 -0.00500 -0.01410 -0.00079 AFIX 147 H002 2 0.251773 0.422050 0.437944 11.00000 -1.50000 AFIX 0 O003 4 0.274608 0.655093 0.630017 11.00000 0.09129 0.06866 = 0.05428 0.00299 0.00695 0.02693 O004 4 0.453222 0.744248 0.367732 11.00000 0.07672 0.07216 = 0.05075 -0.00078 0.00298 -0.02173 C005 1 0.324596 0.456988 0.516256 11.00000 0.05882 0.04516 = 0.04187 -0.00315 -0.00445 0.00262 AFIX 13 H005 2 0.333251 0.302570 0.507843 11.00000 -1.20000 AFIX 0 O006 4 0.500000 1.038284 0.500000 10.50000 0.11263 0.05742 = 0.06719 0.00000 -0.02438 0.00000 AFIX 3 H00W 2 0.488460 0.949744 0.461240 10.50000 -1.50000 H00X 2 0.507940 0.969884 0.545660 10.50000 -1.50000 AFIX 0 C007 1 0.310942 0.501761 0.609935 11.00000 0.05822 0.04938 = 0.04748 0.00091 0.00428 -0.00129 C008 1 0.345074 0.365477 0.676077 11.00000 0.05113 0.05400 = 0.04661 0.00377 0.00333 -0.00404 C009 1 0.363039 0.482363 0.221000 11.00000 0.05556 0.04819 = 0.04386 0.00150 0.00062 0.00081 AFIX 13 H009 2 0.320187 0.414824 0.245111 11.00000 -1.20000 AFIX 0 C00A 1 0.404637 0.576548 0.396369 11.00000 0.05538 0.05696 = 0.04556 -0.00294 -0.00076 -0.00729 C00B 1 0.419515 0.360613 0.357034 11.00000 0.07126 0.05423 = 0.04796 0.00401 -0.00370 0.01282 AFIX 23 H00A 2 0.380697 0.262808 0.370989 11.00000 -1.20000 H00B 2 0.463273 0.302372 0.381241 11.00000 -1.20000 AFIX 0 C00C 1 0.390705 0.584623 0.489903 11.00000 0.06016 0.06170 = 0.04300 -0.00313 -0.00526 -0.00883 AFIX 23 H00C 2 0.384629 0.733842 0.506878 11.00000 -1.20000 H00D 2 0.432216 0.527984 0.519593 11.00000 -1.20000 AFIX 0 C00D 1 0.343483 0.436706 0.759750 11.00000 0.06900 0.06240 = 0.04797 -0.00273 0.00583 0.00332 AFIX 43 H00E 2 0.322392 0.568784 0.772297 11.00000 -1.20000 AFIX 0 C00E 1 0.427383 0.370303 0.261025 11.00000 0.06211 0.05578 = 0.04770 -0.00323 -0.00188 0.01221 AFIX 23 H00F 2 0.470837 0.448071 0.246714 11.00000 -1.20000 H00G 2 0.431440 0.225143 0.238657 11.00000 -1.20000 AFIX 0 C00F 1 0.357459 0.454370 0.123406 11.00000 0.06936 0.05722 = 0.04346 -0.00005 -0.00500 -0.00013 C00G 1 0.377755 0.168329 0.658531 11.00000 0.06949 0.05884 = 0.05389 -0.00066 0.00071 0.00366 AFIX 43 H00H 2 0.380304 0.119201 0.603048 11.00000 -1.20000 AFIX 0 C00H 1 0.377918 0.749367 0.343238 11.00000 0.07291 0.04689 = 0.05259 -0.00192 0.00800 -0.00046 AFIX 13 H00I 2 0.348639 0.857931 0.372093 11.00000 -1.20000 AFIX 0 C00I 1 0.406268 0.046116 0.723044 11.00000 0.06951 0.06082 = 0.07287 0.00327 -0.00243 0.00909 AFIX 43 H00J 2 0.427978 -0.085724 0.711626 11.00000 -1.20000 AFIX 0 C00J 1 0.362249 0.720353 0.249733 11.00000 0.08561 0.05039 = 0.04927 0.00467 -0.00271 0.01260 AFIX 23 H00K 2 0.397637 0.799841 0.217415 11.00000 -1.20000 H00L 2 0.315555 0.781671 0.237182 11.00000 -1.20000 AFIX 0 C00K 1 0.372425 0.315624 0.823755 11.00000 0.08120 0.08702 = 0.04632 -0.00259 0.00139 0.00337 AFIX 43 H00M 2 0.371735 0.365034 0.879281 11.00000 -1.20000 AFIX 0 C00L 1 0.402189 0.121618 0.804372 11.00000 0.06381 0.07619 = 0.05905 0.02043 -0.00340 0.00049 C00M 1 0.423735 0.534311 0.079022 11.00000 0.09894 0.10466 = 0.04833 -0.00093 0.00463 -0.02062 AFIX 137 H00N 2 0.430953 0.684025 0.091991 11.00000 -1.50000 H00O 2 0.417942 0.517181 0.019053 11.00000 -1.50000 H00P 2 0.464547 0.452674 0.097736 11.00000 -1.50000 AFIX 0 C00N 1 0.347147 0.214999 0.102317 11.00000 0.11335 0.07621 = 0.05518 -0.00994 -0.00621 -0.01271 AFIX 137 H00Q 2 0.390738 0.138063 0.114038 11.00000 -1.50000 H00R 2 0.335182 0.199967 0.043526 11.00000 -1.50000 H00S 2 0.309063 0.157075 0.136179 11.00000 -1.50000 AFIX 0 C00O 1 0.291664 0.575676 0.089815 11.00000 0.11151 0.10701 = 0.06831 -0.01150 -0.03446 0.02731 AFIX 137 H00T 2 0.249244 0.521098 0.116648 11.00000 -1.50000 H00U 2 0.287972 0.555241 0.029780 11.00000 -1.50000 H00V 2 0.296567 0.726669 0.101976 11.00000 -1.50000 AFIX 0 HKLF 4 REM fxm-lww-4-cl_a.res in C2 REM R1 = 0.0572 for 2891 Fo > 4sig(Fo) and 0.0600 for all 3123 data REM 217 parameters refined using 1 restraints END WGHT 0.1081 0.0910 REM Highest difference peak 0.304, deepest hole -0.254, 1-sigma level 0.052 Q1 1 0.4287 0.0780 0.8643 11.00000 0.05 0.30 Q2 1 0.4440 -0.0684 0.9348 11.00000 0.05 0.23 Q3 1 0.3980 -0.0788 0.8974 11.00000 0.05 0.20 Q4 1 0.3180 0.4223 0.5630 11.00000 0.05 0.20 Q5 1 0.3632 0.4644 0.1745 11.00000 0.05 0.19 Q6 1 0.3288 0.3906 0.6366 11.00000 0.05 0.18 Q7 1 0.3385 0.4094 0.7188 11.00000 0.05 0.17 Q8 1 0.2632 0.5506 0.6536 11.00000 0.05 0.17 Q9 1 0.3231 0.3597 0.3825 11.00000 0.05 0.16 Q10 1 0.4509 0.3777 0.0799 11.00000 0.05 0.16 Q11 1 0.3918 0.0485 0.6667 11.00000 0.05 0.16 Q12 1 0.4159 0.0728 0.7554 11.00000 0.05 0.15 Q13 1 0.4043 0.1353 0.6817 11.00000 0.05 0.15 Q14 1 0.3629 0.5845 0.3623 11.00000 0.05 0.15 Q15 1 0.2607 0.6439 0.6935 11.00000 0.05 0.15 Q16 1 0.4078 0.6522 0.5317 11.00000 0.05 0.15 Q17 1 0.3387 0.5928 0.2432 11.00000 0.05 0.15 Q18 1 0.4674 0.5721 0.2432 11.00000 0.05 0.14 Q19 1 0.2545 0.7286 0.5952 11.00000 0.05 0.14 Q20 1 0.3674 0.4230 0.4943 11.00000 0.05 0.14 REM The information below was added by Olex2. REM REM R1 = 0.0572 for 2891 Fo > 4sig(Fo) and 0.0600 for all 9965 data REM n/a parameters refined using n/a restraints REM Highest difference peak 0.30, deepest hole -0.25 REM Mean Shift 0, Max Shift 0.000. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0600 REM R1_gt = 0.0572 REM wR_ref = 0.1587 REM GOOF = 1.074 REM Shift_max = 0.000 REM Shift_mean = 0 REM Reflections_all = 9965 REM Reflections_gt = 2891 REM Parameters = n/a REM Hole = -0.25 REM Peak = 0.30 REM Flack = -0.016(16) ; _olex2_date_sample_data_collection 2017-03-14 _olex2_submission_special_instructions 'No special instructions were received'