data_a _audit_creation_method 'SHELXL-2016/6' _shelx_SHELXL_version_number '2016/6' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C66 H30 Cu6 N0 O36 S3' _chemical_formula_sum 'C66 H30 Cu6 N0 O36 S3' _chemical_formula_weight 1876.32 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cu' 'Cu' 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system orthorhombic _space_group_IT_number 63 _space_group_name_H-M_alt 'C m c m' _space_group_name_Hall '-C 2c 2' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z+1/2' '-x, y, -z+1/2' 'x, -y, -z' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z+1/2' '-x+1/2, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x, y, -z-1/2' 'x, -y, z-1/2' '-x, y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, y+1/2, -z-1/2' 'x+1/2, -y+1/2, z-1/2' '-x+1/2, y+1/2, z' _cell_length_a 26.2639(5) _cell_length_b 33.4313(6) _cell_length_c 18.7507(3) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 16463.8(5) _cell_formula_units_Z 4 _cell_measurement_temperature 103(2) _cell_measurement_reflns_used 32604 _cell_measurement_theta_min 2.1190 _cell_measurement_theta_max 29.2870 _exptl_crystal_description block _exptl_crystal_colour green _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 0.757 _exptl_crystal_F_000 3744 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.200 _exptl_crystal_size_mid 0.150 _exptl_crystal_size_min 0.120 _exptl_absorpt_coefficient_mu 0.841 _shelx_estimated_absorpt_T_min 0.850 _shelx_estimated_absorpt_T_max 0.906 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.91187 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.41q (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 103(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'fine-focus sealed X-ray tube' _diffrn_measurement_device_type 'dtrek-CrysAlisPro-abstract goniometer imported rigaku-d*trek images' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean 5.811 _diffrn_reflns_number 89598 _diffrn_reflns_av_unetI/netI 0.0220 _diffrn_reflns_av_R_equivalents 0.0462 _diffrn_reflns_limit_h_min -31 _diffrn_reflns_limit_h_max 31 _diffrn_reflns_limit_k_min -30 _diffrn_reflns_limit_k_max 39 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_limit_l_max 22 _diffrn_reflns_theta_min 1.972 _diffrn_reflns_theta_max 24.998 _diffrn_reflns_theta_full 24.998 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measured_fraction_theta_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_point_group_measured_fraction_full 0.998 _reflns_number_total 7665 _reflns_number_gt 6268 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. Structure factors included contributions from the .fab file. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'CrysAlisPro 1.171.38.41q (Rigaku OD, 2015)' _computing_cell_refinement 'CrysAlisPro 1.171.38.41q (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.41q (Rigaku OD, 2015)' _computing_structure_solution ? _computing_structure_refinement 'SHELXL-2016/6 (Sheldrick, 2016)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1164P)^2^+15.5686P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 7665 _refine_ls_number_parameters 280 _refine_ls_number_restraints 29 _refine_ls_R_factor_all 0.0565 _refine_ls_R_factor_gt 0.0484 _refine_ls_wR_factor_ref 0.1676 _refine_ls_wR_factor_gt 0.1573 _refine_ls_goodness_of_fit_ref 1.016 _refine_ls_restrained_S_all 1.059 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu1 Cu 0.28715(2) 0.26989(2) 0.53240(2) 0.03857(14) Uani 1 1 d . . . . . Cu2 Cu 0.500000 0.07373(2) 0.750000 0.0450(2) Uani 1 4 d S T P . . Cu3 Cu 0.500000 0.15372(2) 0.750000 0.0500(2) Uani 1 4 d S T P . . S1 S 0.34858(6) 0.000000 0.500000 0.0859(5) Uani 1 2 d S T P . . S2 S 0.000000 0.23652(8) 0.71864(12) 0.0570(6) Uani 0.5 2 d S T P . . O1 O 0.44731(9) 0.14704(6) 0.67723(13) 0.0646(6) Uani 1 1 d . . . . . O2 O 0.44758(9) 0.07993(6) 0.67797(14) 0.0646(6) Uani 1 1 d . . . . . O3 O 0.31359(9) 0.21643(7) 0.54950(13) 0.0591(6) Uani 1 1 d . . . . . O4 O 0.25174(9) 0.18267(6) 0.49481(13) 0.0568(5) Uani 1 1 d . . . . . O5 O 0.21650(15) 0.04194(14) 0.5216(5) 0.244(4) Uani 1 1 d . U . . . O6 O 0.18302(8) 0.23088(7) 0.56283(11) 0.0544(5) Uani 1 1 d . . . . . O7 O 0.24541(9) 0.26449(7) 0.61829(11) 0.0550(5) Uani 1 1 d . . . . . O8 O 0.0561(2) 0.1498(2) 0.8286(4) 0.111(2) Uani 0.5 1 d . U P . . O9 O 0.500000 0.21753(15) 0.750000 0.122(3) Uani 1 4 d S TU P . . O10 O 0.500000 0.01020(12) 0.750000 0.0626(12) Uani 1 4 d S T P . . O11 O 0.34797(11) 0.30310(9) 0.57767(17) 0.0907(9) Uani 1 1 d . . . . . C1 C 0.30462(15) 0.03552(11) 0.5210(2) 0.0686(10) Uani 1 1 d . . . . . C2 C 0.25892(17) 0.01995(15) 0.5112(5) 0.140(3) Uani 1 1 d . . . . . C3 C 0.1710(3) 0.0140(3) 0.5324(5) 0.258(6) Uani 1 1 d D U . . . H3A H 0.174724 -0.001179 0.576205 0.309 Uiso 1 1 calc R U . . . H3B H 0.139524 0.029115 0.534661 0.309 Uiso 1 1 calc R U . . . C4 C 0.32193(14) 0.07475(10) 0.5462(2) 0.0617(9) Uani 1 1 d . . . . . C5 C 0.29775(14) 0.11021(10) 0.52754(19) 0.0583(9) Uani 1 1 d . . . . . H5 H 0.268445 0.109551 0.499733 0.070 Uiso 1 1 calc R U . . . C6 C 0.31736(13) 0.14675(9) 0.55041(18) 0.0546(8) Uani 1 1 d . . . . . C7 C 0.36130(13) 0.14814(9) 0.59153(18) 0.0551(8) Uani 1 1 d . . . . . H7 H 0.374585 0.172657 0.605783 0.066 Uiso 1 1 calc R U . . . C8 C 0.38534(13) 0.11291(9) 0.61132(19) 0.0586(8) Uani 1 1 d . . . . . C9 C 0.36606(13) 0.07656(9) 0.5882(2) 0.0623(9) Uani 1 1 d . . . . . H9 H 0.382637 0.053011 0.600750 0.075 Uiso 1 1 calc R U . . . C10 C 0.29203(12) 0.18469(10) 0.52946(16) 0.0490(7) Uani 1 1 d . . . . . C11 C 0.43037(13) 0.11333(9) 0.65840(18) 0.0558(8) Uani 1 1 d . . . . . C12 C 0.04770(18) 0.20795(16) 0.750000 0.0625(12) Uani 1 2 d S TU P . . C13 C 0.0280(3) 0.1771(3) 0.7952(4) 0.080(2) Uani 0.5 1 d . U P . . C14 C 0.02812(18) 0.1247(4) 0.8741(8) 0.171(6) Uani 0.5 1 d D U P . . H14A H 0.038891 0.130702 0.922426 0.205 Uiso 0.5 1 calc R U P . . H14B H 0.038891 0.097503 0.864214 0.205 Uiso 0.5 1 calc R U P . . C15 C 0.10105(17) 0.21957(15) 0.750000 0.0546(11) Uani 1 2 d S T P . . C16 C 0.12682(13) 0.22685(10) 0.68615(16) 0.0572(8) Uani 1 1 d . . . . . H16 H 0.110391 0.222229 0.642990 0.069 Uiso 1 1 calc R U . . . C17 C 0.17667(12) 0.24090(9) 0.68612(15) 0.0495(7) Uani 1 1 d . . . . . C18 C 0.20087(17) 0.24852(13) 0.750000 0.0471(10) Uani 1 2 d S T P . . H18 H 0.233736 0.258870 0.750002 0.057 Uiso 1 2 calc R U P . . C19 C 0.20394(12) 0.24620(9) 0.61685(15) 0.0480(7) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu1 0.0471(2) 0.0387(2) 0.0300(2) 0.00192(12) -0.00597(13) -0.00218(13) Cu2 0.0558(4) 0.0221(3) 0.0571(4) 0.000 0.000 0.000 Cu3 0.0603(5) 0.0221(3) 0.0676(5) 0.000 0.000 0.000 S1 0.0641(8) 0.0573(8) 0.1363(14) -0.0285(9) 0.000 0.000 S2 0.0458(12) 0.0824(16) 0.0429(10) 0.0123(11) 0.000 0.000 O1 0.0755(15) 0.0363(12) 0.0821(16) 0.0089(11) -0.0137(13) 0.0054(10) O2 0.0752(15) 0.0380(12) 0.0806(16) 0.0015(11) -0.0153(13) 0.0115(10) O3 0.0706(15) 0.0443(12) 0.0625(13) 0.0022(11) -0.0177(12) 0.0080(11) O4 0.0641(14) 0.0395(11) 0.0667(14) 0.0033(10) -0.0105(12) 0.0020(9) O5 0.070(2) 0.096(3) 0.565(12) -0.130(5) -0.012(4) 0.008(2) O6 0.0572(13) 0.0716(14) 0.0345(11) -0.0010(9) 0.0000(10) -0.0081(10) O7 0.0618(14) 0.0685(14) 0.0346(10) -0.0028(9) -0.0005(10) -0.0137(11) O8 0.071(4) 0.117(5) 0.144(6) 0.062(4) -0.006(4) 0.007(3) O9 0.158(7) 0.023(2) 0.185(7) 0.000 0.000 0.000 O10 0.090(3) 0.028(2) 0.069(3) 0.000 0.000 0.000 O11 0.0751(18) 0.095(2) 0.102(2) -0.0211(17) -0.0297(16) -0.0234(15) C1 0.062(2) 0.0457(19) 0.098(3) -0.0023(18) -0.003(2) 0.0030(16) C2 0.055(3) 0.069(3) 0.296(9) -0.048(4) -0.002(4) 0.008(2) C3 0.109(5) 0.217(10) 0.448(16) -0.139(9) 0.038(8) -0.030(6) C4 0.059(2) 0.0434(18) 0.083(2) -0.0016(16) -0.0012(18) 0.0040(15) C5 0.0557(19) 0.0469(19) 0.072(2) 0.0000(15) -0.0031(16) 0.0074(14) C6 0.062(2) 0.0423(17) 0.0595(18) 0.0060(14) -0.0029(16) 0.0025(14) C7 0.065(2) 0.0383(16) 0.0616(19) 0.0029(14) -0.0022(16) 0.0023(14) C8 0.063(2) 0.0460(18) 0.067(2) 0.0052(14) -0.0035(17) 0.0088(14) C9 0.067(2) 0.0395(17) 0.080(2) 0.0072(16) -0.0054(18) 0.0081(14) C10 0.0541(18) 0.0459(18) 0.0471(17) 0.0047(13) -0.0011(14) 0.0054(14) C11 0.064(2) 0.0402(18) 0.063(2) 0.0061(14) -0.0028(16) 0.0079(14) C12 0.046(3) 0.082(4) 0.059(3) 0.000 0.000 0.002(2) C13 0.063(4) 0.110(7) 0.065(5) 0.027(4) -0.015(4) 0.009(4) C14 0.191(12) 0.137(9) 0.184(11) 0.103(9) 0.017(9) -0.001(8) C15 0.048(2) 0.071(3) 0.044(2) 0.000 0.000 0.002(2) C16 0.0573(19) 0.080(2) 0.0339(16) -0.0017(14) -0.0048(14) 0.0033(16) C17 0.0534(18) 0.0588(18) 0.0364(15) 0.0042(13) 0.0014(13) 0.0037(14) C18 0.052(2) 0.053(2) 0.037(2) 0.000 0.000 0.0042(19) C19 0.0555(18) 0.0550(18) 0.0335(15) 0.0044(13) -0.0027(13) 0.0043(14) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu1 O3 1.944(2) . ? Cu1 O4 1.954(2) 13_556 ? Cu1 O6 1.950(2) 13_556 ? Cu1 O7 1.957(2) . ? Cu1 O11 2.123(2) . ? Cu1 Cu1 2.6558(6) 13_556 ? Cu2 O2 1.940(2) . ? Cu2 O2 1.940(2) 3_656 ? Cu2 O2 1.940(2) 12_655 ? Cu2 O2 1.940(2) 10_557 ? Cu2 O10 2.124(4) . ? Cu2 Cu3 2.6744(9) . ? Cu3 O1 1.956(2) 3_656 ? Cu3 O1 1.956(2) 12_655 ? Cu3 O1 1.956(2) 10_557 ? Cu3 O1 1.956(2) . ? Cu3 O9 2.133(5) . ? S1 C1 1.702(4) 4_556 ? S1 C1 1.702(4) . ? S2 S2 1.176(5) 10_557 ? S2 C12 1.682(5) 3_556 ? S2 C12 1.682(5) . ? S2 C13 2.134(9) 3_556 ? S2 C13 2.134(9) 10_557 ? O1 C11 1.262(4) . ? O2 C11 1.259(4) . ? O3 C10 1.260(4) . ? O4 C10 1.244(4) . ? O5 C2 1.349(6) . ? O5 C3 1.531(10) . ? O6 C19 1.261(4) . ? O7 C19 1.249(4) . ? O8 C13 1.329(9) . ? O8 C14 1.405(11) . ? C1 C2 1.321(6) . ? C1 C4 1.467(5) . ? C2 C2 1.399(9) 4_556 ? C3 C3 1.533(9) 4_556 ? C3 H3A 0.9700 . ? C3 H3B 0.9700 . ? C4 C5 1.390(5) . ? C4 C9 1.402(5) . ? C5 C6 1.393(5) . ? C5 H5 0.9300 . ? C6 C7 1.389(5) . ? C6 C10 1.485(4) . ? C7 C8 1.387(4) . ? C7 H7 0.9300 . ? C8 C9 1.386(5) . ? C8 C11 1.476(5) . ? C9 H9 0.9300 . ? C12 C13 1.432(9) . ? C12 C13 1.432(9) 10_557 ? C12 C15 1.454(7) . ? C13 C13 1.470(15) 12 ? C13 C13 1.697(15) 10_557 ? C14 C14 1.477(10) 12 ? C14 H14A 0.9700 . ? C14 H14B 0.9700 . ? C15 C16 1.397(4) 10_557 ? C15 C16 1.397(4) . ? C16 C17 1.391(5) . ? C16 H16 0.9300 . ? C17 C18 1.380(4) . ? C17 C19 1.494(4) . ? C18 H18 0.9300 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O3 Cu1 O4 167.39(9) . 13_556 ? O3 Cu1 O6 89.74(10) . 13_556 ? O4 Cu1 O6 88.94(10) 13_556 13_556 ? O3 Cu1 O7 88.83(10) . . ? O4 Cu1 O7 89.83(10) 13_556 . ? O6 Cu1 O7 167.85(9) 13_556 . ? O3 Cu1 O11 98.41(11) . . ? O4 Cu1 O11 94.19(11) 13_556 . ? O6 Cu1 O11 94.06(11) 13_556 . ? O7 Cu1 O11 98.09(11) . . ? O3 Cu1 Cu1 82.97(7) . 13_556 ? O4 Cu1 Cu1 84.43(7) 13_556 13_556 ? O6 Cu1 Cu1 82.51(6) 13_556 13_556 ? O7 Cu1 Cu1 85.34(6) . 13_556 ? O11 Cu1 Cu1 176.31(9) . 13_556 ? O2 Cu2 O2 167.72(13) . 3_656 ? O2 Cu2 O2 90.43(16) . 12_655 ? O2 Cu2 O2 88.26(16) 3_656 12_655 ? O2 Cu2 O2 88.26(16) . 10_557 ? O2 Cu2 O2 90.43(16) 3_656 10_557 ? O2 Cu2 O2 167.73(13) 12_655 10_557 ? O2 Cu2 O10 96.14(6) . . ? O2 Cu2 O10 96.14(6) 3_656 . ? O2 Cu2 O10 96.14(6) 12_655 . ? O2 Cu2 O10 96.14(6) 10_557 . ? O2 Cu2 Cu3 83.86(6) . . ? O2 Cu2 Cu3 83.86(6) 3_656 . ? O2 Cu2 Cu3 83.86(6) 12_655 . ? O2 Cu2 Cu3 83.86(6) 10_557 . ? O10 Cu2 Cu3 180.0 . . ? O1 Cu3 O1 88.46(15) 3_656 12_655 ? O1 Cu3 O1 90.04(15) 3_656 10_557 ? O1 Cu3 O1 166.89(12) 12_655 10_557 ? O1 Cu3 O1 166.89(12) 3_656 . ? O1 Cu3 O1 90.05(15) 12_655 . ? O1 Cu3 O1 88.46(15) 10_557 . ? O1 Cu3 O9 96.55(6) 3_656 . ? O1 Cu3 O9 96.55(6) 12_655 . ? O1 Cu3 O9 96.55(6) 10_557 . ? O1 Cu3 O9 96.56(6) . . ? O1 Cu3 Cu2 83.45(6) 3_656 . ? O1 Cu3 Cu2 83.45(6) 12_655 . ? O1 Cu3 Cu2 83.45(6) 10_557 . ? O1 Cu3 Cu2 83.44(6) . . ? O9 Cu3 Cu2 180.0 . . ? C1 S1 C1 94.6(3) 4_556 . ? S2 S2 C12 69.53(10) 10_557 3_556 ? S2 S2 C12 69.53(10) 10_557 . ? C12 S2 C12 96.3(3) 3_556 . ? S2 S2 C13 97.0(2) 10_557 3_556 ? C12 S2 C13 42.0(3) 3_556 3_556 ? C12 S2 C13 76.7(3) . 3_556 ? S2 S2 C13 97.0(2) 10_557 10_557 ? C12 S2 C13 76.7(3) 3_556 10_557 ? C12 S2 C13 42.0(3) . 10_557 ? C13 S2 C13 40.3(4) 3_556 10_557 ? C11 O1 Cu3 123.1(2) . . ? C11 O2 Cu2 123.5(2) . . ? C10 O3 Cu1 124.4(2) . . ? C10 O4 Cu1 122.5(2) . 13_556 ? C2 O5 C3 109.4(6) . . ? C19 O6 Cu1 124.5(2) . 13_556 ? C19 O7 Cu1 121.05(19) . . ? C13 O8 C14 113.9(6) . . ? C2 C1 C4 132.8(4) . . ? C2 C1 S1 108.0(3) . . ? C4 C1 S1 119.2(3) . . ? C1 C2 C2 114.7(3) . 4_556 ? C1 C2 O5 121.1(4) . . ? C2 C2 O5 124.3(3) 4_556 . ? C3 C3 O5 105.5(8) 4_556 . ? C3 C3 H3A 110.6 4_556 . ? O5 C3 H3A 110.6 . . ? C3 C3 H3B 110.6 4_556 . ? O5 C3 H3B 110.6 . . ? H3A C3 H3B 108.8 . . ? C5 C4 C9 118.8(3) . . ? C5 C4 C1 122.7(3) . . ? C9 C4 C1 118.4(3) . . ? C4 C5 C6 120.1(3) . . ? C4 C5 H5 120.0 . . ? C6 C5 H5 120.0 . . ? C5 C6 C7 120.5(3) . . ? C5 C6 C10 120.1(3) . . ? C7 C6 C10 119.4(3) . . ? C8 C7 C6 119.9(3) . . ? C8 C7 H7 120.1 . . ? C6 C7 H7 120.1 . . ? C7 C8 C9 119.6(3) . . ? C7 C8 C11 121.1(3) . . ? C9 C8 C11 119.2(3) . . ? C8 C9 C4 121.0(3) . . ? C8 C9 H9 119.5 . . ? C4 C9 H9 119.5 . . ? O4 C10 O3 125.7(3) . . ? O4 C10 C6 118.2(3) . . ? O3 C10 C6 116.0(3) . . ? O1 C11 O2 125.7(3) . . ? O1 C11 C8 117.3(3) . . ? O2 C11 C8 117.0(3) . . ? C13 C12 C13 72.6(8) . 10_557 ? C13 C12 C15 122.7(4) . . ? C13 C12 C15 122.7(4) 10_557 . ? C13 C12 S2 110.3(4) . . ? C13 C12 S2 86.1(4) 10_557 . ? C15 C12 S2 124.5(4) . . ? C13 C12 S2 86.1(4) . 10_557 ? C13 C12 S2 110.3(4) 10_557 10_557 ? C15 C12 S2 124.5(4) . 10_557 ? S2 C12 S2 40.9(2) . 10_557 ? O8 C13 C12 124.9(7) . . ? O8 C13 C13 123.7(4) . 12 ? C12 C13 C13 111.2(3) . 12 ? O8 C13 C13 118.0(5) . 10_557 ? C12 C13 C13 53.7(4) . 10_557 ? C13 C13 C13 90.002(2) 12 10_557 ? O8 C13 S2 152.5(7) . 10_557 ? C12 C13 S2 51.8(3) . 10_557 ? C13 C13 S2 69.9(2) 12 10_557 ? C13 C13 S2 83.0(2) 10_557 10_557 ? O8 C14 C14 121.5(4) . 12 ? O8 C14 H14A 107.0 . . ? C14 C14 H14A 107.0 12 . ? O8 C14 H14B 107.0 . . ? C14 C14 H14B 107.0 12 . ? H14A C14 H14B 106.7 . . ? C16 C15 C16 118.0(4) 10_557 . ? C16 C15 C12 120.9(2) 10_557 . ? C16 C15 C12 120.9(2) . . ? C15 C16 C17 121.0(3) . . ? C15 C16 H16 119.5 . . ? C17 C16 H16 119.5 . . ? C18 C17 C16 119.7(3) . . ? C18 C17 C19 120.8(3) . . ? C16 C17 C19 119.5(3) . . ? C17 C18 C17 120.5(4) 10_557 . ? C17 C18 H18 119.8 10_557 . ? C17 C18 H18 119.8 . . ? O7 C19 O6 126.6(3) . . ? O7 C19 C17 117.2(3) . . ? O6 C19 C17 116.2(3) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C1 S1 C1 C2 -0.5(4) 4_556 . . . ? C1 S1 C1 C4 178.3(4) 4_556 . . . ? C4 C1 C2 C2 -177.3(7) . . . 4_556 ? S1 C1 C2 C2 1.3(12) . . . 4_556 ? C4 C1 C2 O5 3.6(14) . . . . ? S1 C1 C2 O5 -177.8(8) . . . . ? C3 O5 C2 C1 -160.2(8) . . . . ? C3 O5 C2 C2 20.7(17) . . . 4_556 ? C2 O5 C3 C3 -53.9(14) . . . 4_556 ? C2 C1 C4 C5 -39.0(9) . . . . ? S1 C1 C4 C5 142.6(3) . . . . ? C2 C1 C4 C9 144.0(7) . . . . ? S1 C1 C4 C9 -34.4(5) . . . . ? C9 C4 C5 C6 0.0(6) . . . . ? C1 C4 C5 C6 -177.0(4) . . . . ? C4 C5 C6 C7 0.4(5) . . . . ? C4 C5 C6 C10 179.0(3) . . . . ? C5 C6 C7 C8 -1.3(5) . . . . ? C10 C6 C7 C8 -179.9(3) . . . . ? C6 C7 C8 C9 1.8(5) . . . . ? C6 C7 C8 C11 -176.5(3) . . . . ? C7 C8 C9 C4 -1.3(6) . . . . ? C11 C8 C9 C4 177.0(3) . . . . ? C5 C4 C9 C8 0.4(6) . . . . ? C1 C4 C9 C8 177.5(4) . . . . ? Cu1 O4 C10 O3 -2.1(5) 13_556 . . . ? Cu1 O4 C10 C6 177.1(2) 13_556 . . . ? Cu1 O3 C10 O4 1.7(5) . . . . ? Cu1 O3 C10 C6 -177.6(2) . . . . ? C5 C6 C10 O4 4.0(5) . . . . ? C7 C6 C10 O4 -177.5(3) . . . . ? C5 C6 C10 O3 -176.7(3) . . . . ? C7 C6 C10 O3 1.9(5) . . . . ? Cu3 O1 C11 O2 -7.0(5) . . . . ? Cu3 O1 C11 C8 170.8(2) . . . . ? Cu2 O2 C11 O1 6.8(5) . . . . ? Cu2 O2 C11 C8 -171.0(2) . . . . ? C7 C8 C11 O1 -3.0(5) . . . . ? C9 C8 C11 O1 178.8(3) . . . . ? C7 C8 C11 O2 174.9(3) . . . . ? C9 C8 C11 O2 -3.3(5) . . . . ? S2 S2 C12 C13 57.6(4) 10_557 . . . ? C12 S2 C12 C13 -7.8(5) 3_556 . . . ? C13 S2 C12 C13 -45.2(6) 3_556 . . . ? C13 S2 C12 C13 -69.9(7) 10_557 . . . ? S2 S2 C12 C13 127.5(4) 10_557 . . 10_557 ? C12 S2 C12 C13 62.1(4) 3_556 . . 10_557 ? C13 S2 C12 C13 24.7(3) 3_556 . . 10_557 ? S2 S2 C12 C15 -104.9(3) 10_557 . . . ? C12 S2 C12 C15 -170.22(13) 3_556 . . . ? C13 S2 C12 C15 152.3(3) 3_556 . . . ? C13 S2 C12 C15 127.7(4) 10_557 . . . ? C12 S2 C12 S2 -65.4(2) 3_556 . . 10_557 ? C13 S2 C12 S2 -102.8(2) 3_556 . . 10_557 ? C13 S2 C12 S2 -127.5(4) 10_557 . . 10_557 ? C14 O8 C13 C12 175.4(11) . . . . ? C14 O8 C13 C13 -10.3(12) . . . 12 ? C14 O8 C13 C13 -121.1(10) . . . 10_557 ? C14 O8 C13 S2 102.4(15) . . . 10_557 ? C13 C12 C13 O8 101.5(8) 10_557 . . . ? C15 C12 C13 O8 -16.7(11) . . . . ? S2 C12 C13 O8 -179.5(8) . . . . ? S2 C12 C13 O8 -145.9(9) 10_557 . . . ? C13 C12 C13 C13 -73.4(4) 10_557 . . 12 ? C15 C12 C13 C13 168.4(3) . . . 12 ? S2 C12 C13 C13 5.6(4) . . . 12 ? S2 C12 C13 C13 39.2(2) 10_557 . . 12 ? C15 C12 C13 C13 -118.2(6) . . . 10_557 ? S2 C12 C13 C13 79.0(3) . . . 10_557 ? S2 C12 C13 C13 112.7(3) 10_557 . . 10_557 ? C13 C12 C13 S2 -112.7(3) 10_557 . . 10_557 ? C15 C12 C13 S2 129.1(4) . . . 10_557 ? S2 C12 C13 S2 -33.7(2) . . . 10_557 ? C13 O8 C14 C14 10.1(12) . . . 12 ? C13 C12 C15 C16 -47.8(8) . . . 10_557 ? C13 C12 C15 C16 -137.3(6) 10_557 . . 10_557 ? S2 C12 C15 C16 112.5(4) . . . 10_557 ? S2 C12 C15 C16 62.3(5) 10_557 . . 10_557 ? C13 C12 C15 C16 137.3(6) . . . . ? C13 C12 C15 C16 47.8(8) 10_557 . . . ? S2 C12 C15 C16 -62.3(5) . . . . ? S2 C12 C15 C16 -112.5(4) 10_557 . . . ? C16 C15 C16 C17 0.0(7) 10_557 . . . ? C12 C15 C16 C17 175.1(4) . . . . ? C15 C16 C17 C18 -1.2(5) . . . . ? C15 C16 C17 C19 176.7(3) . . . . ? C16 C17 C18 C17 2.4(6) . . . 10_557 ? C19 C17 C18 C17 -175.4(2) . . . 10_557 ? Cu1 O7 C19 O6 -3.0(4) . . . . ? Cu1 O7 C19 C17 175.4(2) . . . . ? Cu1 O6 C19 O7 3.0(5) 13_556 . . . ? Cu1 O6 C19 C17 -175.42(19) 13_556 . . . ? C18 C17 C19 O7 -12.8(5) . . . . ? C16 C17 C19 O7 169.3(3) . . . . ? C18 C17 C19 O6 165.7(3) . . . . ? C16 C17 C19 O6 -12.1(4) . . . . ? _refine_diff_density_max 1.337 _refine_diff_density_min -0.561 _refine_diff_density_rms 0.077 # SQUEEZE RESULTS (Version = 41016) # Note: Data are Listed for all Voids in the P1 Unit Cell # i.e. Centre of Gravity, Solvent Accessible Volume, # Recovered number of Electrons in the Void and # Details about the Squeezed Material loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 -0.015 -0.002 -0.001 11022 2171 ' ' _platon_squeeze_void_probe_radius 1.20 _platon_squeeze_details ? _shelx_res_file ; TITL a in Cmcm a.res created by SHELXL-2016/6 at 15:08:17 on 26-Nov-2016 CELL 0.71073 26.2639 33.4313 18.7507 90 90 90 ZERR 4 0.0005 0.0006 0.0003 0 0 0 LATT 7 SYMM -X,-Y,0.5+Z SYMM -X,+Y,0.5-Z SYMM +X,-Y,-Z SFAC C Cu H N O S UNIT 264 24 120 0 144 12 EQIV $1 -X,+Y,+Z EQIV $2 +X,-Y,1-Z DFIX 1.50 0.01 C14 C14_$1 DFIX 1.50 0.01 C3 C3_$2 DELU 0.02 0.02 C4 C12 O8 C13 O9 ISOR 0.02 0.04 C3 O5 O9 C14 L.S. 50 PLAN 80 SIZE 0.2 0.15 0.12 MORE -1 BOND $H CONF fmap 2 acta OMIT -3 50 omit 1 7 1 omit 3 1 0 omit 1 7 2 omit 0 2 2 omit 2 6 2 omit 9 13 1 omit 8 2 1 omit 4 12 1 omit 1 3 2 REM REM REM ABIN ACTA WGHT 0.116400 15.568601 FVAR 0.09477 CU1 2 0.287152 0.269886 0.532403 11.00000 0.04709 0.03866 = 0.02996 0.00192 -0.00597 -0.00218 CU2 2 0.500000 0.073728 0.750000 10.25000 0.05579 0.02209 = 0.05707 0.00000 0.00000 0.00000 CU3 2 0.500000 0.153724 0.750000 10.25000 0.06031 0.02206 = 0.06762 0.00000 0.00000 0.00000 S1 6 0.348579 0.000000 0.500000 10.50000 0.06413 0.05732 = 0.13632 -0.02854 0.00000 0.00000 S2 6 0.000000 0.236523 0.718643 10.25000 0.04577 0.08243 = 0.04290 0.01234 0.00000 0.00000 O1 5 0.447313 0.147043 0.677230 11.00000 0.07554 0.03634 = 0.08205 0.00887 -0.01372 0.00539 O2 5 0.447579 0.079934 0.677968 11.00000 0.07520 0.03799 = 0.08056 0.00155 -0.01528 0.01154 O3 5 0.313589 0.216429 0.549503 11.00000 0.07064 0.04432 = 0.06247 0.00224 -0.01774 0.00800 O4 5 0.251735 0.182666 0.494805 11.00000 0.06413 0.03946 = 0.06671 0.00328 -0.01053 0.00199 O5 5 0.216499 0.041940 0.521573 11.00000 0.07011 0.09642 = 0.56512 -0.12980 -0.01166 0.00845 O6 5 0.183020 0.230876 0.562828 11.00000 0.05716 0.07159 = 0.03450 -0.00100 0.00003 -0.00811 O7 5 0.245413 0.264486 0.618295 11.00000 0.06184 0.06853 = 0.03460 -0.00282 -0.00048 -0.01370 O8 5 0.056075 0.149825 0.828558 10.50000 0.07079 0.11726 = 0.14358 0.06176 -0.00611 0.00688 O9 5 0.500000 0.217533 0.750000 10.25000 0.15789 0.02278 = 0.18460 0.00000 0.00000 0.00000 O10 5 0.500000 0.010205 0.750000 10.25000 0.09033 0.02829 = 0.06907 0.00000 0.00000 0.00000 O11 5 0.347970 0.303102 0.577673 11.00000 0.07510 0.09462 = 0.10247 -0.02109 -0.02967 -0.02337 C1 1 0.304619 0.035521 0.520967 11.00000 0.06191 0.04573 = 0.09828 -0.00226 -0.00306 0.00302 C2 1 0.258924 0.019955 0.511190 11.00000 0.05530 0.06898 = 0.29590 -0.04843 -0.00224 0.00778 C3 1 0.170994 0.013981 0.532407 11.00000 0.10870 0.21685 = 0.44764 -0.13880 0.03781 -0.02990 AFIX 23 H3A 3 0.174724 -0.001179 0.576205 11.00000 -1.20000 H3B 3 0.139524 0.029115 0.534661 11.00000 -1.20000 AFIX 0 C4 1 0.321933 0.074748 0.546217 11.00000 0.05878 0.04342 = 0.08285 -0.00156 -0.00124 0.00405 C5 1 0.297755 0.110211 0.527538 11.00000 0.05573 0.04689 = 0.07225 0.00002 -0.00308 0.00739 AFIX 43 H5 3 0.268445 0.109551 0.499733 11.00000 -1.20000 AFIX 0 C6 1 0.317362 0.146747 0.550406 11.00000 0.06208 0.04232 = 0.05951 0.00601 -0.00287 0.00251 C7 1 0.361301 0.148140 0.591532 11.00000 0.06536 0.03831 = 0.06157 0.00292 -0.00222 0.00227 AFIX 43 H7 3 0.374585 0.172657 0.605783 11.00000 -1.20000 AFIX 0 C8 1 0.385339 0.112908 0.611317 11.00000 0.06282 0.04600 = 0.06694 0.00521 -0.00352 0.00882 C9 1 0.366057 0.076564 0.588212 11.00000 0.06708 0.03954 = 0.08015 0.00720 -0.00539 0.00810 AFIX 43 H9 3 0.382637 0.053011 0.600750 11.00000 -1.20000 AFIX 0 C10 1 0.292029 0.184693 0.529460 11.00000 0.05407 0.04590 = 0.04715 0.00471 -0.00108 0.00538 C11 1 0.430373 0.113326 0.658398 11.00000 0.06360 0.04023 = 0.06344 0.00613 -0.00278 0.00792 C12 1 0.047699 0.207949 0.750000 10.50000 0.04595 0.08228 = 0.05934 0.00000 0.00000 0.00195 C13 1 0.027979 0.177100 0.795247 10.50000 0.06332 0.11050 = 0.06497 0.02686 -0.01496 0.00931 C14 1 0.028121 0.124695 0.874116 10.50000 0.19121 0.13690 = 0.18423 0.10305 0.01748 -0.00128 AFIX 23 H14A 3 0.038891 0.130702 0.922426 10.50000 -1.20000 H14B 3 0.038891 0.097503 0.864214 10.50000 -1.20000 AFIX 0 C15 1 0.101047 0.219569 0.750000 10.50000 0.04803 0.07140 = 0.04444 0.00000 0.00000 0.00218 C16 1 0.126816 0.226848 0.686151 11.00000 0.05733 0.08048 = 0.03391 -0.00172 -0.00483 0.00332 AFIX 43 H16 3 0.110391 0.222229 0.642990 11.00000 -1.20000 AFIX 0 C17 1 0.176671 0.240900 0.686116 11.00000 0.05339 0.05877 = 0.03640 0.00420 0.00140 0.00372 C18 1 0.200868 0.248520 0.750000 10.50000 0.05192 0.05289 = 0.03652 0.00000 0.00000 0.00422 AFIX 43 H18 3 0.233736 0.258870 0.750002 10.50000 -1.20000 AFIX 0 C19 1 0.203939 0.246197 0.616848 11.00000 0.05554 0.05504 = 0.03346 0.00443 -0.00269 0.00428 HKLF 4 REM a in Cmcm REM R1 = 0.0484 for 6268 Fo > 4sig(Fo) and 0.0565 for all 7665 data REM 280 parameters refined using 29 restraints END WGHT 0.1031 16.6741 REM Highest difference peak 1.337, deepest hole -0.561, 1-sigma level 0.077 Q1 1 0.4554 0.2338 0.7500 10.50000 0.05 1.34 Q2 1 0.3548 0.2992 0.6439 11.00000 0.05 0.65 Q3 1 0.3497 0.3354 0.5880 11.00000 0.05 0.52 Q4 1 0.1783 -0.0314 0.5606 11.00000 0.05 0.51 Q5 1 0.0823 0.1090 0.8510 11.00000 0.05 0.50 Q6 1 0.2240 0.0314 0.5805 11.00000 0.05 0.49 Q7 1 0.2277 0.0494 0.4615 11.00000 0.05 0.45 Q8 1 0.0176 0.1107 0.8350 11.00000 0.05 0.43 Q9 1 0.3339 0.0107 0.4698 11.00000 0.05 0.41 Q10 1 0.1060 0.2295 0.7500 10.50000 0.05 0.38 Q11 1 0.0765 0.1547 0.7500 10.50000 0.05 0.34 Q12 1 0.0767 0.0890 0.8975 11.00000 0.05 0.33 Q13 1 0.1857 -0.0014 0.6092 11.00000 0.05 0.33 Q14 1 0.0000 0.2623 0.7500 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329.60 12.20 0 -10 -12 37.73 2.37 0 -10 12 31.73 1.73 0 10 12 32.78 2.15 0 -10 -12 34.33 2.29 0 10 12 36.39 2.24 0 -10 -12 30.27 2.34 0 10 -12 34.10 1.83 0 10 12 37.65 2.11 0 -10 12 33.62 2.24 0 -10 12 32.56 2.28 0 -10 -13 179.28 7.40 0 -10 13 178.74 7.46 0 10 13 188.86 7.37 0 -10 13 181.22 7.12 0 10 13 183.80 7.45 0 -10 13 185.03 7.45 0 -10 -13 185.86 7.39 0 10 13 184.55 7.38 0 10 -13 190.53 7.15 0 -10 14 155.65 6.26 0 10 -14 160.99 6.30 0 10 14 172.34 6.56 0 10 14 160.88 6.62 0 -10 14 162.72 6.66 0 10 14 158.33 6.57 0 -10 14 154.33 6.67 0 -10 15 0.90 1.27 0 10 15 -0.05 1.85 0 10 15 0.50 2.00 0 10 -15 2.48 1.45 0 -10 15 0.05 2.09 0 10 15 1.80 1.72 0 -10 15 2.82 2.04 0 10 16 1.31 1.89 0 -10 16 0.27 2.15 0 10 16 4.23 2.02 0 -10 16 -2.65 2.08 0 10 16 1.16 2.06 0 -10 16 1.19 1.37 0 -10 17 9.44 2.35 0 10 17 12.64 2.45 0 -10 17 10.98 1.58 0 -10 17 7.07 2.28 0 10 17 10.06 2.34 0 10 17 9.10 2.41 0 -10 18 9.45 1.54 0 -10 18 9.01 2.43 0 10 18 7.73 2.48 0 10 18 7.12 2.48 0 10 18 8.68 2.40 0 10 19 102.52 4.87 0 10 19 90.96 4.89 0 10 19 98.47 4.82 0 -10 19 96.37 4.93 0 -10 19 90.85 4.97 0 -10 20 4.67 2.94 0 -10 20 4.90 2.85 0 10 20 5.93 2.52 0 10 20 4.68 2.69 0 10 20 4.58 2.63 0 -10 21 59.51 4.20 0 10 21 63.79 4.20 0 10 21 65.97 3.96 0 -10 21 56.96 4.28 0 10 21 60.08 4.06 0 10 22 -4.63 2.82 0 10 22 -5.08 3.28 0 10 22 -6.92 3.26 0 -10 22 4.45 3.13 0 -10 22 3.01 3.22 0 -10 23 85.18 5.11 0 -10 23 83.13 5.18 0 10 23 88.14 4.87 0 10 23 73.05 4.97 0 -10 24 2.11 3.50 0 10 24 5.05 3.13 0 10 24 2.27 3.57 0 -10 24 0.52 3.73 0 10 24 2.98 3.38 0 10 25 7.34 3.52 0 10 25 15.41 3.53 0 -12 0 371.77 14.04 0 12 0 374.41 14.03 0 12 -1 749.22 28.19 0 -12 1 774.71 28.20 0 -12 1 764.92 28.19 0 12 1 743.07 28.33 0 12 -1 777.70 28.20 0 12 -1 787.79 28.32 0 -12 1 694.29 28.29 0 -12 -1 714.33 28.33 0 -12 2 500.42 18.41 0 -12 2 475.67 18.47 0 -12 2 494.57 18.40 0 12 -2 513.83 18.40 0 12 -2 452.42 18.46 0 -12 -2 487.54 18.53 0 12 2 445.92 18.52 0 12 -2 527.97 18.41 0 12 3 556.39 20.86 0 12 3 535.76 20.69 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5.73 0 14 8 143.63 5.80 0 -14 -8 152.59 5.84 0 14 8 145.39 5.98 0 14 -8 155.89 5.92 0 -14 8 168.38 5.95 0 -14 8 158.97 5.93 0 14 8 152.13 5.83 0 14 -8 138.30 5.88 0 -14 -8 144.82 5.81 0 -14 9 944.64 35.42 0 14 9 912.06 35.48 0 14 9 932.33 35.35 0 -14 9 913.04 35.25 0 -14 -9 943.24 35.34 0 14 -9 969.75 35.26 0 14 -9 930.77 35.40 0 -14 -9 979.34 35.33 0 -14 -9 951.73 35.47 0 14 9 950.95 35.35 0 -14 9 1003.21 35.42 0 14 -9 931.41 35.41 0 -14 -10 293.15 10.97 0 14 10 281.31 10.98 0 14 -10 293.12 10.85 0 -14 10 274.20 11.07 0 14 -10 306.11 11.09 0 -14 -10 276.30 10.97 0 -14 10 298.20 11.08 0 14 10 282.15 11.13 0 -14 10 285.04 10.84 0 14 -10 276.12 11.08 0 14 10 290.94 10.98 0 -14 11 871.51 32.54 0 -14 -11 922.56 32.68 0 14 11 873.34 32.70 0 14 11 906.43 32.82 0 14 -11 867.32 32.75 0 14 11 900.43 32.70 0 -14 11 828.59 32.74 0 -14 -11 888.04 32.68 0 14 -11 818.33 32.72 0 14 -11 877.86 32.55 0 -14 11 830.36 32.76 0 -14 -12 81.87 3.85 0 -14 12 87.66 4.01 0 -14 12 82.09 3.52 0 14 -12 89.44 3.57 0 14 12 86.94 3.82 0 14 12 89.61 3.86 0 -14 -12 83.68 3.81 0 -14 12 92.98 4.00 0 14 12 87.04 4.01 0 14 -13 31.13 1.71 0 -14 -13 26.07 2.31 0 -14 -13 29.68 2.26 0 -14 13 28.50 2.36 0 14 13 31.75 2.25 0 14 13 31.18 2.25 0 14 13 27.18 2.40 0 -14 13 27.09 1.63 0 -14 13 29.76 2.41 0 14 -14 76.08 3.15 0 14 14 72.54 3.53 0 14 14 69.75 3.71 0 -14 14 76.78 3.07 0 -14 14 66.60 3.61 0 -14 14 63.19 3.61 0 14 14 64.15 3.50 0 14 15 28.93 2.29 0 -14 15 25.08 1.64 0 14 15 25.50 2.74 0 -14 15 22.18 2.52 0 -14 15 22.18 2.50 0 14 15 26.22 2.41 0 -14 16 3.45 2.28 0 -14 16 1.91 2.38 0 14 16 6.48 2.04 0 -14 16 4.86 1.30 0 14 16 1.46 2.40 0 14 16 5.16 2.17 0 14 17 42.65 3.00 0 -14 17 34.52 3.12 0 14 17 44.44 2.96 0 14 17 43.32 3.21 0 -14 17 41.34 3.09 0 -14 18 12.82 2.74 0 14 18 13.48 2.46 0 14 18 9.36 2.44 0 14 18 9.75 2.69 0 -14 18 10.42 2.69 0 -14 19 17.74 2.91 0 14 19 18.65 2.84 0 14 19 26.19 3.18 0 14 19 20.68 2.69 0 -14 19 20.37 3.06 0 14 20 11.12 2.75 0 14 20 9.53 2.66 0 14 20 16.38 3.23 0 -14 20 4.11 2.88 0 -14 20 8.41 3.09 0 -14 21 51.95 4.09 0 14 21 56.77 3.92 0 14 21 59.18 4.15 0 -14 21 49.51 4.18 0 14 21 52.51 4.01 0 14 22 4.04 3.17 0 -14 22 4.26 3.15 0 -14 22 1.77 3.25 0 14 22 1.22 3.16 0 14 22 2.26 3.40 0 -14 23 60.72 4.66 0 14 23 60.16 4.57 0 14 23 71.27 4.75 0 14 23 68.56 4.45 0 -14 23 55.14 4.70 0 14 24 0.15 3.64 0 -14 24 -2.54 3.75 0 14 25 25.80 4.08 0 14 25 18.83 3.90 0 14 25 11.22 4.02 0 16 0 474.44 18.15 0 -16 0 491.92 18.16 0 16 -1 190.94 7.25 0 -16 1 189.97 7.28 0 16 -1 183.03 7.02 0 16 -1 193.73 7.03 0 -16 -1 196.21 7.31 0 16 -1 188.71 7.03 0 16 1 191.17 7.30 0 16 -1 184.54 7.03 0 16 2 1.69 1.09 0 16 -2 1.04 0.98 0 16 -2 1.34 0.61 0 -16 2 -0.04 1.19 0 16 -2 1.53 0.59 0 -16 -2 1.11 1.42 0 -16 3 80.61 3.24 0 -16 3 81.92 3.25 0 16 3 80.68 3.54 0 16 -3 87.40 3.36 0 16 -3 82.42 3.25 0 -16 -3 87.49 3.62 0 16 -3 80.62 3.26 0 16 -4 192.24 6.34 0 16 -4 179.01 6.30 0 16 -4 173.83 6.31 0 16 -4 194.01 6.34 0 16 4 146.64 6.16 0 -16 -4 175.03 6.52 0 -16 4 175.25 6.30 0 -16 -4 183.68 6.18 0 16 4 136.71 6.16 0 -16 -4 159.79 6.17 0 -16 4 172.77 6.31 0 16 4 181.86 6.52 0 -16 -5 713.90 25.21 0 -16 5 733.08 25.32 0 16 -5 706.76 25.30 0 16 5 668.11 25.21 0 -16 -5 645.00 25.42 0 16 5 654.68 25.43 0 16 5 675.05 25.21 0 16 -5 691.33 25.29 0 -16 -5 672.24 25.20 0 16 -5 632.07 25.28 0 -16 5 688.33 25.30 0 16 -5 619.71 25.28 0 -16 6 18.29 1.35 0 16 -6 13.51 1.22 0 16 6 15.73 1.06 0 -16 -6 14.16 1.79 0 16 -6 17.73 1.27 0 16 -6 16.52 1.14 0 -16 6 15.42 1.26 0 -16 -6 17.59 1.10 0 -16 -6 17.77 1.15 0 16 -6 16.93 1.24 0 16 6 13.40 1.03 0 16 -7 139.37 5.44 0 -16 7 137.01 5.45 0 -16 -7 145.37 5.32 0 -16 -7 142.93 5.32 0 16 -7 144.10 5.43 0 -16 7 132.60 5.43 0 16 7 137.37 5.34 0 16 -7 129.48 5.32 0 16 -7 134.63 5.32 0 16 7 131.39 5.32 0 -16 8 216.15 7.79 0 16 8 184.68 7.66 0 -16 8 201.12 7.76 0 16 8 186.07 7.66 0 -16 -8 204.64 7.66 0 16 -8 208.50 7.80 0 16 -8 203.10 7.61 0 -16 -8 214.27 7.65 0 16 -8 200.60 7.77 0 16 -8 188.98 7.60 0 -16 -9 533.78 19.60 0 16 9 506.53 19.80 0 16 9 530.94 19.64 0 -16 -9 537.69 19.61 0 -16 9 525.71 19.72 0 -16 9 514.23 19.70 0 16 -9 520.77 19.71 0 16 9 526.19 19.62 0 16 -9 519.68 19.55 0 16 -9 494.58 19.69 0 16 -9 519.66 19.55 0 -16 10 231.93 9.11 0 16 10 229.98 8.99 0 16 10 232.11 8.98 0 16 -10 229.31 9.10 0 16 -10 244.80 9.10 0 16 10 229.53 9.19 0 16 -10 231.23 8.86 0 -16 -10 230.90 8.97 0 -16 -10 244.08 8.97 0 -16 10 223.62 9.08 0 16 -11 51.11 2.84 0 16 11 54.69 2.64 0 -16 11 49.04 2.79 0 -16 11 47.35 2.81 0 16 -11 48.85 2.89 0 16 11 50.11 2.65 0 -16 -11 51.97 2.59 0 16 11 50.43 2.93 0 -16 11 61.31 2.32 0 -16 -11 45.97 2.67 0 16 -11 50.37 2.34 0 -16 12 21.93 1.32 0 -16 -12 18.73 1.91 0 -16 12 21.37 2.17 0 16 12 18.99 1.78 0 16 12 18.19 2.09 0 16 12 19.19 1.84 0 16 -12 19.09 1.36 0 -16 -12 20.70 1.98 0 -16 12 18.46 2.03 0 16 13 167.85 7.16 0 -16 -13 178.66 7.17 0 -16 13 172.92 7.26 0 16 -13 172.17 6.87 0 -16 -13 179.51 7.12 0 16 13 181.36 7.17 0 16 13 173.79 7.32 0 -16 13 180.04 7.23 0 -16 13 185.77 6.85 0 -16 14 64.34 3.49 0 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9.07 2.55 0 -18 19 11.23 3.02 0 18 19 16.13 2.66 0 18 19 15.89 3.18 0 -18 19 13.78 3.11 0 18 19 10.62 2.82 0 18 20 5.88 2.84 0 18 20 6.96 2.74 0 -18 20 7.25 3.17 0 18 21 15.80 3.20 0 -18 21 13.78 3.50 0 18 21 15.27 3.24 0 -18 21 15.69 3.44 0 18 22 -2.83 3.18 0 18 22 3.39 3.37 0 18 22 -0.74 3.00 0 -18 22 5.45 3.36 0 -18 22 -0.08 3.42 0 -18 23 15.25 3.66 0 18 23 19.73 3.36 0 18 23 15.17 3.47 0 -18 23 17.96 3.83 0 18 23 28.62 3.72 0 18 24 -1.32 3.56 0 20 0 418.59 15.16 0 -20 0 379.99 15.13 0 20 -1 42.75 2.20 0 20 1 47.95 2.32 0 -20 -1 45.62 2.49 0 -20 1 48.07 2.41 0 20 2 483.86 16.87 0 20 -2 432.48 16.56 0 20 -2 437.03 16.57 0 20 -2 450.02 16.57 0 20 -2 462.38 16.78 0 -20 -2 438.66 16.84 0 20 -2 440.85 16.56 0 -20 2 467.63 16.78 0 20 -3 65.17 2.81 0 20 -3 67.44 2.62 0 20 -3 58.89 2.58 0 20 -3 68.91 2.59 0 -20 -3 65.27 3.13 0 -20 3 59.04 2.93 0 20 3 69.05 3.06 0 20 -3 62.55 2.62 0 -20 4 194.30 7.04 0 -20 -4 189.60 7.35 0 20 4 169.48 7.27 0 20 -4 188.60 7.13 0 20 -4 196.49 7.04 0 -20 4 182.98 7.03 0 20 -4 169.65 7.01 0 20 -4 181.11 7.12 0 -20 -5 138.22 5.44 0 -20 -5 131.59 4.91 0 -20 -5 121.24 4.90 0 20 -5 142.36 5.16 0 -20 -5 118.97 4.90 0 -20 5 145.85 5.11 0 -20 -5 129.26 4.91 0 -20 5 131.85 5.11 0 20 -5 154.42 5.16 0 20 -5 138.36 5.11 0 20 -5 145.82 5.10 0 20 5 134.45 5.38 0 20 6 18.62 1.01 0 20 6 18.75 1.05 0 20 -6 19.68 1.32 0 -20 -6 18.38 1.05 0 -20 -6 19.91 1.05 0 20 -6 18.19 1.36 0 20 6 21.05 1.86 0 20 -6 21.42 1.41 0 20 -6 21.34 1.41 0 20 7 0.72 0.81 0 -20 7 0.45 1.25 0 20 7 0.35 0.85 0 -20 -7 0.50 0.87 0 20 -7 -0.85 1.13 0 20 -7 1.79 1.16 0 20 -7 -0.28 1.00 0 -20 7 1.39 1.22 0 20 7 1.42 1.63 0 20 -7 1.19 1.11 0 -20 -7 -0.04 0.85 0 -20 -8 18.54 1.29 0 20 8 15.64 1.26 0 20 -8 17.53 1.56 0 20 -8 15.98 1.58 0 20 -8 18.94 1.40 0 -20 8 19.80 1.69 0 -20 8 19.76 1.62 0 20 8 16.72 1.25 0 20 -8 16.00 1.32 0 -20 -8 18.92 1.31 0 20 9 439.78 16.62 0 20 -9 479.32 16.74 0 20 -9 413.98 16.71 0 -20 9 455.64 16.76 0 -20 9 469.64 16.76 0 20 -9 383.36 16.58 0 -20 -9 459.35 16.60 0 -20 -9 440.11 16.60 0 20 -9 448.51 16.60 0 20 9 453.48 16.61 0 -20 -10 74.83 3.13 0 20 -10 62.15 3.01 0 20 -10 66.56 3.05 0 -20 10 75.36 3.42 0 20 -10 67.46 3.41 0 20 -10 76.08 3.38 0 -20 10 72.96 3.38 0 -20 -10 73.06 3.17 0 20 10 75.36 3.15 0 20 10 72.59 3.17 0 20 11 6.92 1.50 0 20 -11 6.93 1.31 0 20 -11 7.79 1.24 0 20 11 3.56 2.10 0 20 11 9.31 1.48 0 -20 -11 9.63 1.60 0 -20 11 9.99 1.90 0 -20 -11 8.74 1.50 0 -20 11 5.95 1.86 0 -20 12 164.37 6.79 0 20 -12 160.95 6.41 0 -20 12 166.48 6.76 0 20 12 172.54 6.58 0 20 12 159.01 6.87 0 20 -12 161.85 6.38 0 -20 -12 163.98 6.57 0 20 12 163.99 6.58 0 -20 -12 164.76 6.53 0 20 13 24.08 1.96 0 20 -13 18.33 1.56 0 -20 -13 22.42 2.05 0 -20 13 24.35 2.42 0 -20 -13 21.49 1.96 0 20 13 21.21 2.56 0 20 13 20.04 2.00 0 -20 13 21.48 2.37 0 -20 14 67.08 3.64 0 20 14 72.20 3.41 0 20 14 67.00 3.41 0 -20 14 75.38 3.61 0 20 14 77.89 3.83 0 20 -14 57.85 2.95 0 20 15 1.50 2.06 0 20 15 2.65 1.96 0 20 15 4.62 2.48 0 -20 15 -1.02 2.29 0 -20 15 1.56 2.27 0 20 16 57.41 3.21 0 20 16 50.37 3.18 0 -20 16 54.88 3.49 0 20 16 58.19 3.69 0 -20 16 53.59 3.56 0 20 17 0.24 2.23 0 -20 17 5.95 2.83 0 20 17 3.60 2.77 0 -20 17 4.26 2.73 0 20 17 1.60 2.27 0 20 18 38.55 3.55 0 -20 18 37.54 3.44 0 -20 18 35.85 3.47 0 20 18 37.31 2.98 0 20 18 29.15 3.08 0 20 19 13.11 3.25 0 20 19 16.54 2.74 0 -20 19 18.10 3.33 0 20 19 8.27 2.71 0 -20 20 9.21 3.35 0 20 20 10.32 2.71 0 -20 20 10.23 3.42 0 20 20 13.91 2.76 0 -20 21 2.53 3.40 0 20 21 3.78 3.44 0 -20 21 -1.45 3.52 0 -20 22 -4.57 3.62 0 20 22 6.98 3.44 0 -20 22 -2.04 3.39 0 20 23 19.80 3.87 0 22 0 228.73 8.43 0 -22 0 199.93 8.43 0 22 1 13.58 1.69 0 -22 1 12.05 1.69 0 -22 -1 11.72 1.75 0 22 -1 11.81 1.58 0 -22 -2 1043.22 36.24 0 -22 2 998.47 36.17 0 22 2 1047.77 36.27 0 22 -2 1110.72 36.21 0 22 -2 904.96 35.93 0 22 -2 918.89 35.93 0 22 -2 997.93 35.93 0 22 -2 987.91 35.93 0 22 -3 78.39 3.19 0 -22 -3 85.84 3.76 0 22 -3 79.67 3.19 0 22 -3 78.44 3.20 0 -22 3 88.81 3.61 0 22 -3 85.69 3.52 0 22 -3 82.65 3.19 0 22 3 84.17 3.71 0 22 4 273.09 10.63 0 -22 -4 276.72 10.63 0 22 -4 284.04 10.48 0 22 -4 263.62 10.33 0 22 -4 258.65 10.31 0 22 -4 278.08 10.33 0 22 -4 280.35 10.33 0 22 -4 290.29 10.46 0 22 -5 95.67 3.82 0 -22 5 96.99 3.82 0 22 -5 94.25 3.80 0 22 -5 92.27 3.89 0 22 5 93.70 4.17 0 22 -5 84.54 3.91 0 -22 5 98.58 3.81 0 22 -6 382.02 14.25 0 22 -6 397.28 14.24 0 22 6 397.26 14.51 0 -22 -6 370.10 14.06 0 -22 -6 367.25 14.07 0 -22 -6 359.95 14.06 0 -22 6 418.65 14.25 0 22 -6 390.88 14.26 0 -22 6 375.81 14.23 0 22 -6 393.73 14.22 0 -22 7 25.93 1.67 0 -22 7 26.10 1.71 0 22 -7 25.54 1.67 0 22 -7 25.35 1.51 0 -22 -7 26.71 1.28 0 22 7 21.44 2.15 0 -22 -7 25.98 1.29 0 22 -7 21.50 1.65 0 22 -7 21.32 1.62 0 -22 -8 59.11 2.62 0 22 8 59.88 2.64 0 -22 -8 65.35 2.64 0 22 -8 65.67 2.83 0 22 8 56.45 3.20 0 22 -8 67.85 2.84 0 22 8 60.30 2.62 0 -22 8 61.74 2.94 0 -22 8 60.90 2.92 0 22 -8 64.81 2.76 0 22 -8 64.79 2.86 0 22 -9 101.03 3.96 0 22 9 86.26 3.87 0 -22 9 101.29 4.16 0 22 9 83.74 3.89 0 -22 -9 99.56 3.88 0 22 -9 99.06 3.97 0 -22 9 100.30 4.19 0 22 -9 98.53 4.11 0 -22 -9 96.37 3.87 0 22 -9 105.78 4.09 0 22 10 15.38 1.42 0 -22 -10 14.91 1.45 0 22 -10 14.75 1.37 0 -22 10 16.98 1.83 0 22 -10 11.34 1.80 0 22 -10 16.83 1.47 0 -22 10 15.85 1.90 0 -22 -10 13.20 1.50 0 22 10 15.62 1.43 0 22 -10 15.11 1.80 0 -22 11 27.22 2.29 0 -22 11 27.47 2.24 0 22 11 26.26 1.86 0 22 11 29.94 1.87 0 22 -11 25.17 1.71 0 22 -11 24.93 1.72 0 -22 12 165.01 6.48 0 22 12 153.45 6.26 0 -22 12 158.79 6.50 0 22 12 159.61 6.25 0 22 12 164.03 6.67 0 22 -12 143.41 6.08 0 -22 13 9.01 2.19 0 22 -13 7.09 1.36 0 22 13 6.91 1.74 0 22 13 5.80 1.80 0 22 13 7.16 2.32 0 -22 13 6.18 2.20 0 22 14 5.10 2.48 0 -22 14 5.72 2.28 0 -22 14 6.68 2.26 0 22 14 7.95 1.94 0 22 14 9.20 1.94 0 -22 15 -0.27 2.49 0 -22 15 -3.70 2.44 0 22 15 -1.68 1.93 0 22 15 2.51 1.97 0 22 15 2.38 2.69 0 22 16 78.19 3.91 0 -22 16 83.16 4.39 0 22 16 81.69 4.58 0 22 16 78.12 3.95 0 -22 16 79.79 4.44 0 22 17 2.31 2.28 0 22 17 4.79 2.20 0 -22 17 -2.86 2.80 0 -22 17 2.39 2.94 0 22 17 8.52 2.86 0 22 18 14.22 2.56 0 22 18 13.34 2.63 0 -22 18 12.33 2.86 0 -22 18 14.92 3.10 0 22 18 13.96 3.20 0 22 19 6.23 2.60 0 22 19 6.63 2.70 0 -22 19 7.39 3.13 0 -22 19 0.13 3.05 0 22 19 2.68 3.21 0 22 20 29.56 3.09 0 22 20 22.87 3.21 0 -22 20 22.78 3.64 0 22 20 24.08 3.83 0 -22 20 25.86 3.78 0 -22 21 4.28 3.46 0 22 21 2.57 3.62 0 -22 21 0.90 3.35 0 -22 22 -0.73 3.33 0 -22 22 1.65 3.26 0 24 0 706.26 24.84 0 -24 0 611.51 24.79 0 -24 1 235.03 9.39 0 -24 -1 234.56 9.43 0 24 1 255.64 9.41 0 24 -1 235.78 9.37 0 24 -2 307.40 9.70 0 -24 2 352.23 9.78 0 24 -2 239.74 9.27 0 24 2 309.17 9.81 0 -24 -2 300.70 9.81 0 -24 3 63.38 3.01 0 24 -3 60.02 2.44 0 24 -3 69.00 2.95 0 24 -3 56.45 2.44 0 24 3 64.74 3.13 0 24 -3 59.85 2.43 0 24 -3 64.43 2.43 0 24 -4 195.25 7.02 0 24 -4 176.76 7.02 0 24 -4 203.31 7.21 0 24 -4 187.46 7.23 0 24 -4 175.65 7.03 0 24 -4 178.81 7.03 0 24 4 185.12 7.40 0 24 -5 11.19 1.22 0 24 -5 13.03 1.47 0 24 -5 11.27 1.43 0 24 5 10.86 1.85 0 24 -5 13.01 1.15 0 24 -5 13.73 1.21 0 24 -5 10.55 1.17 0 24 -6 35.86 1.85 0 24 6 33.85 2.47 0 24 -6 29.42 1.79 0 -24 6 34.11 1.82 0 24 -6 33.96 2.00 0 -24 6 36.28 1.85 0 24 -6 30.71 1.91 0 -24 -7 16.61 0.97 0 -24 7 18.67 1.58 0 24 -7 20.68 1.46 0 24 -7 15.70 1.44 0 -24 -7 17.93 0.97 0 -24 -7 19.11 0.99 0 -24 7 18.09 1.53 0 24 7 16.19 2.12 0 24 -7 13.15 1.59 0 24 -7 19.58 1.50 0 -24 -7 18.82 0.99 0 -24 -8 40.57 1.84 0 -24 8 38.81 2.27 0 24 8 41.47 2.75 0 -24 -8 34.26 1.82 0 -24 -8 40.67 1.82 0 24 -8 46.83 2.16 0 24 -8 43.96 2.19 0 24 -8 42.07 2.20 0 -24 -8 41.00 1.83 0 24 -8 35.05 2.03 0 -24 8 41.25 2.24 0 -24 9 16.08 1.77 0 -24 9 14.84 1.79 0 24 -9 16.78 1.51 0 24 9 14.88 2.24 0 24 -9 15.48 1.72 0 24 -9 16.67 1.44 0 24 -9 16.31 1.66 0 -24 10 47.84 2.60 0 24 10 43.14 2.16 0 24 -10 41.23 2.52 0 24 10 40.48 2.19 0 24 -10 43.15 2.56 0 -24 10 45.85 2.63 0 24 -10 42.62 2.23 0 -24 11 27.75 2.32 0 24 11 23.18 1.83 0 24 -11 24.39 1.73 0 24 11 27.00 1.82 0 -24 11 28.91 2.28 0 -24 12 104.25 4.25 0 24 12 92.84 3.93 0 24 12 88.12 3.95 0 -24 12 91.25 4.27 0 24 -12 83.45 3.79 0 24 13 53.14 2.85 0 24 13 57.07 3.55 0 -24 13 52.84 3.10 0 24 13 52.77 2.83 0 -24 13 46.13 3.13 0 -24 14 90.23 4.75 0 24 14 100.20 4.47 0 24 14 109.30 5.13 0 24 14 98.84 4.42 0 -24 14 109.16 4.78 0 -24 15 8.51 2.63 0 24 15 2.51 2.88 0 -24 15 6.75 2.47 0 24 15 7.15 2.01 0 -24 16 79.48 4.43 0 24 16 81.51 4.03 0 24 16 78.84 3.95 0 24 16 73.14 4.62 0 -24 16 86.21 4.38 0 -24 17 5.29 2.87 0 -24 17 3.45 2.80 0 24 17 7.51 3.05 0 -24 18 32.32 3.51 0 24 18 35.15 3.71 0 -24 18 32.88 3.51 0 -24 19 -2.15 3.20 0 -24 19 -4.39 3.26 0 24 19 -4.45 3.48 0 24 20 17.28 3.63 0 -24 20 15.14 3.40 0 -24 20 11.77 3.51 0 -24 21 4.00 3.61 0 24 21 9.24 3.66 0 -24 21 -0.90 3.45 0 -24 22 -2.53 3.38 0 -24 22 -5.91 3.52 0 26 0 2133.24 84.38 0 -26 0 2405.01 84.39 0 26 -1 67.80 3.26 0 26 1 66.21 3.35 0 -26 1 62.65 3.36 0 26 -2 130.95 5.75 0 -26 2 145.82 5.83 0 26 2 149.79 5.91 0 26 -3 25.35 1.18 0 26 3 30.99 2.25 0 26 -3 27.80 1.19 0 26 -3 24.87 2.01 0 26 -4 296.48 11.34 0 26 -4 306.74 11.54 0 26 -4 334.19 11.63 0 26 -4 309.52 11.34 0 26 4 312.86 11.79 0 26 -4 288.01 11.35 0 26 -4 295.54 11.35 0 26 -5 35.70 1.92 0 26 -5 41.31 1.88 0 26 -5 46.59 2.27 0 26 5 36.36 2.59 0 26 -5 38.76 1.91 0 26 -5 38.99 2.22 0 26 -5 34.74 1.94 0 26 -6 6.10 1.32 0 26 -6 5.51 1.28 0 26 6 8.24 2.04 0 26 -6 4.75 1.33 0 26 -6 7.25 1.53 0 26 -6 7.76 1.46 0 26 -6 7.39 1.24 0 26 -7 2.13 1.33 0 26 -7 2.04 1.33 0 26 -7 1.20 1.27 0 26 -7 -0.94 1.48 0 26 7 2.79 1.93 0 26 -8 1.55 1.37 0 -26 -8 3.60 0.71 0 -26 8 4.47 1.54 0 26 -8 2.33 1.31 0 -26 8 5.13 1.45 0 26 -8 2.49 1.31 0 -26 -8 3.70 0.72 0 26 8 2.05 2.07 0 26 -8 3.55 1.48 0 -26 9 4.28 1.71 0 -26 -9 5.83 0.96 0 -26 -9 5.01 1.00 0 26 -9 4.45 1.51 0 -26 9 4.07 1.68 0 26 -9 7.41 1.29 0 26 -9 3.71 1.44 0 26 9 4.84 2.10 0 -26 10 70.69 3.30 0 26 10 61.44 3.67 0 -26 10 67.00 3.26 0 -26 -10 66.37 2.89 0 -26 -10 60.41 2.88 0 26 -10 67.56 2.99 0 -26 11 2.91 1.87 0 26 -11 5.19 1.37 0 -26 11 0.90 1.93 0 26 12 4.38 1.50 0 26 12 0.81 1.53 0 -26 12 1.45 2.01 0 -26 12 0.87 2.01 0 -26 13 3.99 2.22 0 -26 14 148.51 6.52 0 -26 14 158.51 6.52 0 26 14 145.62 6.85 0 -26 15 0.68 2.41 0 26 15 5.86 2.90 0 -26 15 2.18 2.49 0 -26 16 27.86 3.20 0 -26 16 29.38 3.11 0 26 16 29.93 3.39 0 -26 17 4.06 2.82 0 26 17 -2.68 3.25 0 -26 17 -2.76 2.93 0 26 18 52.69 4.08 0 -26 18 38.94 3.75 0 -26 19 0.47 3.31 0 26 19 -3.42 3.56 0 -26 19 1.93 3.22 0 26 20 12.71 3.81 0 -26 20 9.20 3.59 0 -26 20 2.28 3.43 0 -26 21 6.93 3.63 0 -26 21 2.32 3.47 0 28 0 18.01 2.06 0 28 -1 185.89 7.69 0 28 1 195.87 7.73 0 28 -2 75.86 3.55 0 28 2 75.88 3.66 0 -28 2 65.16 3.56 0 28 -3 7.10 0.45 0 28 -3 8.41 1.61 0 28 3 8.04 2.05 0 28 -3 7.22 0.45 0 28 -3 9.36 1.73 0 28 -4 0.57 0.68 0 28 -4 1.80 0.77 0 28 -4 -0.04 0.70 0 28 -4 0.88 0.79 0 28 -4 1.54 1.47 0 28 4 1.31 1.94 0 28 -4 0.92 1.63 0 28 -5 4.18 1.08 0 28 -5 4.09 1.11 0 28 -5 1.76 1.55 0 28 5 0.61 2.07 0 28 -5 2.30 1.61 0 28 -6 3.32 1.31 0 28 -6 3.57 1.54 0 28 -6 3.70 1.29 0 28 6 1.75 2.06 0 28 -6 3.81 1.65 0 28 -7 29.02 1.96 0 28 7 30.21 2.52 0 28 -7 28.59 1.92 0 28 -7 28.50 1.96 0 28 -8 11.78 1.48 0 28 -8 13.10 1.68 0 28 -8 10.84 1.71 0 28 8 12.55 2.28 0 28 -9 1.77 1.33 0 28 9 1.08 2.32 0 28 -10 7.06 1.38 0 28 10 8.36 2.44 0 -28 10 8.59 1.92 0 -28 10 8.90 1.86 0 -28 11 62.29 3.42 0 -28 11 68.25 3.42 0 28 11 65.59 3.91 0 -28 12 101.45 4.57 0 -28 12 95.34 4.56 0 -28 13 20.10 2.46 0 -28 13 16.73 2.48 0 -28 15 15.33 2.81 0 28 15 18.18 3.28 0 -28 15 16.08 2.71 0 -28 16 49.75 3.53 0 -28 16 42.14 3.56 0 28 16 46.79 3.96 0 -28 17 6.61 3.01 0 -28 17 5.81 3.07 0 28 17 5.44 3.30 0 -28 18 18.22 3.31 0 28 18 13.28 3.77 0 -28 18 23.75 3.47 0 28 19 -0.43 3.55 0 -28 19 4.83 3.24 0 -28 20 23.20 3.62 0 -28 21 5.75 3.70 0 -28 21 3.13 3.60 0 30 0 3.97 1.96 0 30 -1 106.98 4.62 0 30 1 97.31 4.67 0 30 -2 148.15 6.32 0 30 2 158.67 6.50 0 30 3 34.10 2.70 0 30 -3 40.75 2.61 0 30 4 25.49 2.45 0 30 -4 27.26 2.32 0 30 -5 68.24 3.06 0 30 -5 85.25 3.55 0 30 5 84.83 4.01 0 30 -5 82.00 3.61 0 30 -6 6.62 1.38 0 30 6 11.35 2.31 0 30 -6 4.41 1.73 0 30 -6 10.39 1.38 0 30 7 45.59 3.12 0 30 -7 46.83 2.37 0 30 -7 45.10 2.39 0 30 -8 3.33 1.60 0 30 -8 1.52 1.61 0 30 -8 3.19 1.56 0 30 8 -0.06 2.33 0 30 9 30.95 2.95 0 30 -9 29.99 2.20 0 30 -9 26.30 2.24 0 30 -9 27.26 1.93 0 30 -10 -1.46 1.87 0 30 -10 3.19 1.93 0 30 10 3.08 2.59 0 30 11 5.33 2.81 0 -30 12 47.80 3.03 0 -30 12 49.96 3.03 0 30 12 49.32 3.67 0 -30 13 16.16 2.44 0 -30 13 12.93 2.45 0 -30 14 2.18 2.46 0 -30 14 5.51 2.60 0 30 15 5.76 3.16 0 30 16 24.63 3.80 0 30 17 -1.17 3.46 0 30 18 7.53 3.74 0 32 0 100.30 4.70 0 32 -1 34.44 2.74 0 32 1 35.43 2.77 0 32 2 18.02 2.51 0 32 -2 20.41 2.32 0 32 -3 61.26 3.40 0 32 3 63.26 3.58 0 32 4 3.03 2.23 0 32 -4 0.38 1.86 0 32 5 11.82 2.51 0 32 -5 9.73 2.04 0 32 -6 9.91 1.98 0 32 6 2.23 2.49 0 32 7 97.52 4.87 0 32 8 29.58 3.10 0 32 -8 26.69 2.23 0 32 9 19.38 2.79 0 32 10 3.33 2.78 0 32 11 37.31 3.31 0 32 12 11.99 3.04 0 32 13 13.81 3.10 0 32 16 16.54 3.83 0 32 17 16.80 3.77 0 34 0 30.10 2.72 0 34 -1 17.16 2.52 0 34 1 17.29 2.56 0 34 -2 46.92 2.92 0 34 2 39.29 3.07 0 34 -3 3.17 2.18 0 34 3 0.35 2.42 0 34 4 3.41 2.60 0 34 -4 3.37 2.15 0 34 -5 186.41 7.43 0 34 5 172.42 7.71 0 34 6 48.67 3.55 0 34 -6 53.70 3.11 0 34 -7 11.74 1.99 0 34 7 10.61 2.66 0 34 8 7.97 2.83 0 34 9 94.36 4.98 0 34 10 10.91 2.84 0 34 11 4.57 2.93 0 34 12 2.63 3.04 0 34 13 9.66 3.30 0 34 14 0.08 3.28 0 36 -1 24.42 2.69 0 36 1 26.05 2.94 0 36 -2 7.73 2.42 0 36 2 4.56 2.53 0 36 -3 5.40 2.30 0 36 3 0.74 2.62 0 36 4 47.10 3.54 0 36 -4 49.71 3.24 0 36 -5 124.86 5.57 0 36 5 129.40 6.06 0 36 -6 24.73 2.53 0 36 6 21.21 3.01 0 36 7 24.69 3.18 0 36 8 7.30 2.92 0 36 9 88.24 5.04 0 36 10 15.36 3.39 0 36 11 16.39 3.51 0 36 12 -6.60 3.42 0 36 13 17.74 3.59 0 36 14 6.50 3.64 0 38 0 16.00 2.78 0 38 1 1.82 2.72 0 38 -1 2.14 2.59 0 38 2 -3.90 2.72 0 38 -2 -2.39 2.58 0 38 3 70.84 4.24 0 38 4 19.50 3.22 0 38 -4 17.26 2.63 0 38 5 2.92 2.84 0 38 6 0.57 3.04 0 38 7 92.83 5.08 0 38 8 14.83 3.38 0 38 9 12.72 3.53 0 38 10 3.94 3.21 0 38 11 51.22 4.27 0 38 12 3.80 3.37 0 38 13 0.52 3.63 0 40 0 46.03 3.52 0 40 -1 1.98 2.68 0 40 1 4.50 2.84 0 40 2 4.77 2.94 0 40 -2 4.36 2.76 0 40 -3 29.70 3.05 0 40 3 30.71 3.27 0 40 4 15.97 3.16 0 40 5 20.85 3.40 0 40 6 13.90 3.42 0 40 8 -2.30 3.44 0 40 10 8.58 3.49 0 40 11 14.82 3.85 0 42 0 5.75 3.10 0 42 -1 20.44 3.03 0 42 2 -0.90 3.03 0 42 3 2.39 3.13 0 42 4 5.66 3.30 0 42 5 30.88 3.65 0 42 7 0.97 3.55 0 42 8 4.82 3.38 0 42 9 5.72 3.61 0 44 1 2.99 3.33 0 44 3 2.58 3.42 0 44 4 7.87 3.59 0 44 5 2.73 3.67 0 44 6 5.99 3.66 0 44 7 3.54 3.48 0 46 2 11.56 3.69 0 46 3 2.92 3.35 0 46 4 0.08 3.66 0 46 5 7.41 3.84 -1 1 -2 168.28 6.75 -1 -1 -2 191.08 6.77 1 -1 -2 175.18 6.76 -1 -1 -2 191.72 6.76 1 1 2 177.41 6.76 1 -1 2 188.85 6.75 1 -1 -2 178.99 6.77 1 -1 -2 162.96 6.75 -1 1 2 194.54 6.76 -1 1 3 114.73 4.20 1 -1 -3 111.67 4.23 1 1 3 104.51 4.22 1 -1 3 109.27 4.20 -1 -1 -3 100.39 4.23 -1 -1 -3 94.88 4.22 1 -1 -3 115.15 4.21 -1 1 -3 111.20 4.21 -1 -1 -3 107.44 4.24 1 1 -3 117.82 4.17 -1 -1 3 113.14 4.16 1 -1 -3 114.11 4.24 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110.33 4.21 -10 14 0 96.95 4.33 10 -14 0 108.78 4.21 10 14 0 103.36 4.14 10 14 0 106.90 4.15 10 14 -1 26.92 1.51 -10 14 1 26.47 1.64 -10 -14 -1 24.22 1.53 -10 -14 1 28.23 1.58 -10 14 -1 26.96 1.55 10 -14 -1 26.50 1.65 -10 14 -1 24.45 1.56 -10 -14 1 27.27 1.60 -10 14 -1 28.08 1.90 10 14 1 29.02 1.65 -10 -14 -1 24.10 1.56 -10 -14 1 25.10 1.62 -10 -14 -1 24.80 1.74 10 14 -1 25.00 1.60 10 14 1 24.68 1.58 10 -14 -1 26.79 1.59 -10 14 -1 23.84 1.94 10 14 1 24.93 1.64 10 -14 1 27.48 1.78 10 -14 1 28.37 1.83 -10 14 1 26.29 1.67 10 14 -1 26.12 1.59 10 14 -2 75.04 3.20 -10 -14 -2 73.15 3.15 -10 -14 -2 71.39 3.29 10 14 -2 73.03 3.07 -10 14 2 78.86 3.17 -10 -14 2 71.29 3.13 -10 -14 2 76.11 3.16 10 -14 -2 74.02 3.29 -10 14 2 78.44 3.19 -10 14 -2 78.84 3.23 -10 -14 2 75.98 3.11 10 14 -2 76.18 3.22 -10 -14 -2 74.18 3.15 10 -14 2 74.65 3.31 -10 14 -2 75.90 3.37 -10 14 -2 74.71 3.40 10 -14 2 70.47 3.28 10 14 2 78.68 3.27 10 -14 -2 73.64 3.25 -10 14 -2 77.35 3.21 -10 -14 -3 381.50 13.76 -10 14 3 362.10 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5 10.13 1.48 10 14 -5 12.68 1.42 -10 -14 5 10.46 0.66 -10 -14 5 12.39 1.32 10 -14 -5 9.10 1.49 10 14 5 8.98 1.42 -10 14 5 12.04 1.25 10 -14 -5 10.74 1.72 -10 14 -5 14.32 1.73 -10 14 -5 8.15 1.33 -10 14 5 9.48 1.28 -10 -14 -5 8.89 1.32 -10 -14 5 9.02 1.36 -10 -14 -5 11.64 1.84 -10 14 -5 13.90 1.56 10 14 -5 9.32 0.62 -10 14 -5 10.65 1.59 10 14 5 11.27 1.38 -10 14 -5 9.90 1.28 -10 -14 -5 10.56 1.30 10 14 5 12.28 1.55 -10 14 6 193.89 7.75 10 -14 -6 187.70 7.60 10 14 -6 203.76 7.63 10 14 -6 201.23 7.65 -10 14 -6 200.10 7.68 -10 -14 -6 201.89 7.75 -10 -14 6 201.18 7.61 -10 -14 -6 194.10 7.57 -10 14 6 190.37 7.60 10 -14 6 188.23 7.66 -10 -14 6 200.32 7.63 -10 14 6 192.77 7.59 -10 14 -6 193.09 7.65 -10 -14 -6 194.67 7.60 -10 14 -6 193.77 7.66 -10 -14 -6 188.29 7.60 10 -14 -6 191.28 7.74 -10 14 -6 198.73 7.71 -10 14 -6 204.11 7.66 10 14 6 186.78 7.68 -10 -14 -6 196.77 7.56 10 -14 -6 186.22 7.61 -10 -14 7 745.86 26.39 10 -14 -7 721.64 26.32 -10 14 7 715.09 26.46 10 14 -7 701.05 26.34 -10 -14 -7 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3.56 -10 22 20 10.99 3.66 -10 -22 20 8.71 3.69 -10 22 -21 3.21 3.84 -10 -22 21 -1.44 3.61 -10 -22 21 -0.25 3.68 -10 22 -21 -3.54 3.72 -10 22 22 -2.87 3.46 -10 -24 0 99.34 3.83 -10 24 0 92.34 3.93 -10 -24 0 100.06 4.16 -10 24 0 96.91 3.96 10 24 0 91.15 3.88 -10 -24 0 95.45 3.85 10 -24 0 100.35 3.98 10 -24 0 88.44 3.97 10 24 0 101.97 4.17 10 24 0 92.95 3.87 -10 24 0 99.65 4.46 -10 24 1 51.68 2.99 -10 24 -1 50.34 2.47 -10 -24 1 53.43 2.64 -10 24 1 48.24 2.38 -10 -24 -1 56.11 2.85 -10 -24 -1 54.91 2.26 10 24 -1 44.59 2.35 -10 24 -1 48.30 2.48 -10 24 1 47.91 2.40 -10 -24 -1 53.02 2.27 10 -24 -1 48.45 2.47 10 24 1 56.50 2.77 10 24 -1 56.13 2.61 -10 -24 1 54.17 2.31 10 -24 -1 54.09 2.47 10 24 1 48.25 2.30 -10 -24 1 49.76 2.33 10 24 -1 51.16 2.33 10 24 1 49.15 2.31 -10 24 -1 56.39 3.07 -10 24 -2 84.72 3.49 -10 24 2 77.79 3.86 10 -24 -2 80.73 3.44 -10 -24 2 87.32 3.56 10 24 2 78.23 3.33 -10 24 2 81.86 3.40 -10 -24 -2 82.36 3.84 -10 -24 -2 77.38 3.27 -10 24 2 78.08 3.41 10 24 -2 82.74 3.41 -10 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24 4 89.19 3.96 -10 24 -4 108.03 4.47 10 -24 -4 94.08 3.96 -10 -24 4 95.47 3.94 -10 24 -4 90.99 4.06 -10 -24 4 106.63 4.03 10 24 -5 23.84 1.84 -10 -24 -5 27.77 1.55 -10 24 5 26.74 1.74 10 -24 -5 26.38 1.83 -10 -24 5 22.77 1.54 -10 24 5 27.65 1.79 -10 24 -5 26.69 1.96 10 24 -5 25.70 1.90 -10 -24 5 28.66 1.90 -10 -24 -5 26.42 1.58 -10 -24 5 25.83 1.93 -10 -24 -5 26.66 1.57 -10 24 -5 27.85 2.07 -10 -24 -5 26.68 1.59 -10 24 -5 28.13 2.09 10 24 5 26.42 2.33 -10 24 -5 26.86 2.39 10 24 -5 27.25 1.56 10 -24 -5 26.75 1.80 -10 24 -5 26.89 1.90 -10 -24 -6 9.57 1.24 10 24 -6 7.94 0.96 10 24 -6 9.48 1.58 -10 24 6 9.47 1.44 10 24 -6 10.63 1.65 -10 -24 6 6.93 1.63 -10 -24 -6 10.10 1.26 -10 24 6 12.44 1.52 -10 -24 6 9.38 1.67 -10 24 -6 8.13 1.71 -10 24 -6 8.65 1.77 10 24 6 9.47 2.13 -10 24 -6 9.12 1.72 10 -24 -6 9.54 1.56 -10 24 -6 6.35 2.01 -10 24 -6 11.52 1.69 10 -24 -6 9.78 1.46 10 24 -7 88.55 3.99 10 24 -7 85.72 3.96 -10 24 7 92.99 3.83 -10 -24 -7 85.19 3.75 -10 24 -7 88.66 4.04 -10 -24 7 89.19 3.98 -10 24 7 92.22 3.88 -10 24 -7 93.75 4.03 -10 -24 7 94.20 4.04 -10 24 -7 86.74 4.02 10 24 7 93.94 4.35 -10 24 -7 97.65 4.29 -10 24 -7 87.18 3.99 -10 -24 -7 86.90 3.74 10 24 -8 2.37 1.71 -10 -24 -8 1.49 1.37 10 24 -8 0.95 1.77 -10 -24 8 4.77 1.84 -10 24 8 -1.72 2.29 -10 24 8 3.02 1.61 -10 -24 8 1.93 1.90 -10 24 -8 1.78 1.89 10 24 8 1.84 2.09 -10 24 -8 -0.14 2.06 -10 24 -8 3.11 1.82 -10 -24 -8 0.59 1.32 -10 24 8 0.51 1.56 -10 24 9 18.86 2.70 -10 24 9 19.82 1.86 -10 -24 -9 18.02 1.76 -10 24 -9 16.55 2.15 -10 -24 9 19.95 2.03 -10 24 9 18.79 1.89 -10 -24 9 18.18 2.13 -10 24 -9 19.50 2.27 10 24 9 21.44 2.45 -10 24 -9 19.48 2.11 -10 -24 -9 17.99 1.74 -10 -24 -10 24.84 2.05 -10 24 -10 20.15 2.32 -10 24 10 25.65 2.09 -10 -24 10 25.32 2.25 -10 24 10 24.67 2.14 -10 -24 10 27.91 2.39 10 24 10 31.39 2.81 -10 24 -10 26.43 2.33 -10 24 10 25.80 2.93 -10 24 -10 22.47 2.29 -10 -24 -10 24.79 2.00 -10 24 -11 2.60 2.23 -10 24 11 2.46 1.84 -10 -24 -11 8.06 1.83 -10 -24 11 6.41 2.04 -10 24 11 5.56 1.93 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232.89 9.17 -10 26 -4 239.77 9.22 -10 26 -4 236.04 9.23 10 26 4 254.32 9.49 -10 26 4 241.90 9.11 -10 26 -4 260.96 9.57 -10 26 -4 250.70 9.23 -10 -26 5 29.27 2.02 -10 -26 -5 32.93 1.62 -10 26 5 30.89 2.67 -10 26 5 30.40 1.85 -10 -26 5 32.46 2.07 -10 -26 -5 29.31 1.65 -10 26 5 31.91 1.90 -10 26 -5 34.19 2.19 -10 26 -5 31.83 2.22 10 26 5 34.21 2.51 -10 26 -5 30.91 2.11 10 26 -5 33.03 1.83 -10 26 -5 36.23 2.59 -10 26 -5 27.98 2.04 -10 -26 -6 14.25 1.24 -10 26 -6 16.03 1.90 -10 -26 -6 13.39 1.27 -10 26 6 15.32 1.50 -10 -26 6 17.03 1.71 -10 26 6 14.46 1.51 -10 26 -6 14.31 1.83 -10 -26 6 14.48 1.79 -10 26 -6 15.38 1.89 10 26 6 18.09 2.33 10 26 -6 16.30 1.20 -10 26 -6 14.67 2.21 -10 26 -6 15.61 1.82 -10 -26 -7 1.43 1.24 -10 -26 -7 1.03 1.20 -10 26 7 3.59 1.45 -10 26 -7 1.31 1.81 -10 -26 7 0.61 1.59 -10 -26 7 1.71 1.69 10 26 7 -3.60 2.14 -10 26 -7 0.84 2.17 -10 26 -7 1.90 1.70 -10 26 7 2.00 1.48 -10 26 8 29.21 2.02 -10 26 -8 28.75 2.32 -10 -26 8 34.39 2.20 -10 26 8 29.38 2.08 -10 -26 8 29.71 2.34 10 26 8 26.68 2.80 -10 26 -8 26.93 2.25 -10 26 -8 27.41 2.62 -10 -26 9 16.70 2.23 -10 26 -9 17.35 2.13 -10 26 9 27.10 2.93 -10 26 9 19.00 1.85 -10 -26 9 20.60 2.15 -10 26 9 14.68 1.88 10 26 9 19.96 2.55 -10 26 -9 16.85 2.41 -10 26 -9 20.80 2.20 -10 26 10 59.75 3.84 -10 26 -10 55.30 3.40 -10 -26 10 58.57 3.29 -10 26 10 63.86 3.07 -10 26 10 56.15 3.08 -10 -26 10 67.40 3.43 10 26 10 64.13 3.75 -10 26 -10 58.78 3.51 -10 26 -10 66.07 3.39 -10 26 -11 2.26 2.29 -10 26 11 5.71 2.77 -10 26 11 4.77 1.78 -10 -26 11 1.14 2.14 -10 26 11 3.61 1.87 -10 -26 11 1.77 2.20 -10 26 -11 5.27 2.09 -10 26 -11 3.12 2.22 10 26 11 4.99 2.57 -10 26 12 8.92 2.81 -10 26 -12 8.98 2.48 -10 26 12 12.48 1.98 -10 -26 12 11.26 2.38 -10 -26 12 12.60 2.44 -10 26 -12 7.04 2.25 -10 26 -12 13.20 2.44 10 26 12 10.56 2.76 -10 26 -13 2.68 2.47 -10 26 13 0.56 2.81 -10 -26 13 0.60 2.34 -10 -26 13 2.18 2.49 -10 26 -13 3.97 2.10 -10 26 -13 -0.33 2.41 10 26 13 0.14 2.63 10 26 14 51.92 3.73 -10 -26 14 53.32 3.41 -10 26 -14 38.94 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1515.39 55.56 12 12 -5 1258.12 55.32 -12 -12 5 1640.07 55.34 12 12 -5 1450.20 55.52 -12 -12 -5 1544.70 55.58 -12 12 5 1538.90 55.57 12 -12 5 1544.53 55.56 12 12 5 1407.17 55.50 -12 12 -5 1586.02 55.60 -12 12 -5 1484.71 55.56 -12 -12 -5 1433.04 55.50 -12 12 5 1564.06 55.64 -12 12 6 10.59 1.62 12 -12 -6 14.44 1.61 12 12 -6 10.88 1.58 12 12 6 11.00 1.70 12 -12 -6 11.18 1.63 -12 12 -6 11.68 1.63 12 12 -6 11.83 1.63 -12 -12 6 8.52 0.61 -12 -12 6 11.24 1.60 -12 -12 -6 12.62 1.58 -12 12 6 13.94 1.57 -12 -12 6 10.66 1.65 12 -12 6 14.37 1.61 -12 -12 -6 10.66 1.94 -12 12 -6 12.19 1.78 -12 12 -6 13.92 1.75 12 12 6 11.53 1.73 -12 12 6 10.06 1.52 -12 12 -6 10.38 1.85 -12 12 -6 12.68 1.57 -12 -12 -6 13.90 1.55 12 12 6 11.85 1.77 -12 -12 -7 281.25 10.18 -12 12 7 273.23 10.24 12 -12 7 280.88 10.23 12 12 7 254.00 10.24 12 -12 -7 258.44 10.14 12 12 -7 241.87 10.14 -12 12 -7 262.54 10.24 12 -12 -7 259.90 10.15 12 12 -7 237.50 10.15 -12 12 7 267.11 10.18 -12 -12 7 281.61 10.22 -12 12 7 260.54 10.18 -12 12 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2.01 -12 -12 10 13.33 1.90 -12 12 10 12.45 1.89 -12 -12 10 11.12 1.95 -12 12 -10 13.37 2.04 -12 -12 -10 8.47 1.93 12 -12 10 11.09 1.74 -12 -12 11 103.02 4.46 -12 12 11 106.23 4.46 -12 12 -11 94.50 4.51 -12 12 11 98.43 4.30 12 -12 11 101.15 4.34 -12 -12 -11 90.17 4.37 -12 12 11 91.08 4.33 -12 -12 11 91.18 4.41 -12 12 -11 95.15 4.48 -12 -12 -11 97.34 4.34 -12 12 12 9.54 1.99 -12 -12 -12 10.22 2.04 -12 -12 12 9.69 2.06 -12 12 12 6.24 1.91 -12 12 12 11.41 2.02 -12 -12 12 10.69 2.14 12 -12 12 9.74 1.95 -12 12 -12 8.04 2.25 -12 -12 -12 7.46 1.98 -12 12 -12 6.84 2.27 12 12 13 73.32 3.89 12 -12 13 78.80 3.71 -12 -12 -13 65.12 3.76 -12 12 13 78.24 3.77 -12 -12 13 75.55 3.76 -12 12 13 74.70 3.66 -12 12 -13 65.06 3.86 -12 12 13 70.74 3.68 -12 -12 13 68.32 3.79 -12 12 -13 68.78 3.85 -12 -12 -13 71.28 3.74 12 12 14 1.22 2.45 -12 12 -14 -2.77 2.41 -12 -12 -14 0.05 2.34 -12 12 14 0.24 2.16 -12 12 14 -1.89 2.16 -12 -12 14 0.11 2.20 -12 12 14 0.26 2.20 -12 -12 14 0.29 2.24 12 -12 14 0.89 2.10 -12 12 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58.86 2.63 12 -14 0 51.76 2.70 12 14 0 54.82 2.64 -12 14 -1 70.21 3.11 -12 14 1 71.09 3.12 -12 -14 -1 72.78 3.14 12 14 1 70.14 3.16 -12 -14 1 71.64 3.12 12 14 -1 76.17 3.09 12 -14 1 71.77 3.30 12 14 1 72.97 3.20 12 -14 -1 72.10 3.23 -12 14 -1 67.71 3.12 -12 -14 1 77.19 3.11 -12 14 1 73.77 3.15 -12 -14 -1 72.09 3.16 -12 -14 1 68.53 3.13 12 14 -1 78.46 3.22 -12 -14 -1 71.81 3.22 -12 14 -1 64.64 3.34 12 -14 1 75.57 3.29 12 14 1 68.52 3.16 12 -14 -1 69.03 3.20 12 14 -1 76.86 3.20 12 14 2 11.81 1.52 12 14 -2 11.59 1.51 -12 -14 -2 15.13 1.34 12 -14 2 13.80 1.65 -12 14 2 12.59 1.34 -12 -14 2 15.19 1.29 12 14 2 13.86 1.42 -12 14 -2 11.34 1.35 12 14 -2 11.64 1.54 12 -14 -2 11.60 1.53 -12 14 2 10.69 1.36 -12 -14 2 11.63 1.31 -12 14 2 11.92 1.73 -12 -14 2 11.40 1.24 -12 -14 -2 13.45 1.55 -12 14 -2 14.07 1.71 -12 14 -2 13.18 1.68 12 14 -2 14.60 1.15 -12 -14 -2 14.63 1.34 12 -14 2 14.28 1.64 12 14 2 15.57 1.49 -12 14 2 11.20 1.63 12 -14 -2 12.81 1.47 -12 14 -2 13.69 1.34 -12 -14 3 7.94 1.07 -12 -14 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36.43 12 -14 -5 982.49 36.34 12 14 -5 998.65 36.34 12 14 -5 923.98 36.14 12 14 -5 985.88 36.34 -12 14 5 988.66 36.36 12 14 5 956.16 36.32 -12 -14 -5 904.31 36.32 -12 -14 5 949.56 36.14 12 -14 -5 940.10 36.34 -12 14 -5 944.31 36.39 -12 -14 5 1010.43 36.39 -12 14 5 951.78 36.35 -12 -14 5 1077.36 36.40 -12 -14 -5 1018.35 36.42 12 -14 5 1033.97 36.44 12 -14 5 990.08 36.37 12 14 5 993.03 36.32 -12 14 -5 975.39 36.38 -12 14 -5 978.38 36.43 12 -14 5 948.85 36.37 -12 -14 -5 966.64 36.32 -12 14 5 1011.65 36.49 12 14 6 184.65 5.61 -12 14 -6 169.57 5.54 -12 14 6 180.29 5.65 12 -14 -6 180.22 5.48 12 14 -6 181.23 5.48 -12 -14 6 178.63 5.44 -12 -14 -6 174.45 5.43 -12 14 6 186.63 5.46 12 14 -6 171.45 5.49 -12 14 6 174.81 5.45 -12 -14 6 169.20 5.46 -12 -14 -6 169.91 5.62 -12 14 -6 190.37 5.53 -12 14 -6 181.55 5.53 -12 14 -6 180.26 5.60 -12 14 -6 186.91 5.54 12 -14 -6 168.38 5.48 -12 -14 -6 176.79 5.40 12 -14 6 200.44 5.62 -12 14 7 174.33 7.08 12 -14 -7 178.49 6.98 12 14 -7 176.85 7.01 12 -14 7 188.48 7.05 -12 14 7 172.08 6.97 -12 14 -7 170.59 7.06 -12 -14 7 184.12 6.98 12 -14 -7 173.48 6.99 12 14 -7 165.66 7.01 -12 14 7 158.44 6.96 -12 -14 7 167.99 6.97 -12 14 -7 172.92 7.02 -12 -14 -7 185.09 6.95 -12 14 -7 171.02 7.02 -12 -14 -7 178.21 6.96 -12 -14 -7 167.00 6.95 -12 14 -7 178.66 7.04 -12 -14 -7 185.74 6.95 12 14 7 184.19 7.11 12 -14 8 150.17 5.79 12 -14 -8 143.30 5.69 -12 14 8 142.70 5.84 12 14 -8 145.67 5.76 12 -14 -8 138.46 5.71 -12 14 -8 135.56 5.81 -12 -14 -8 132.37 5.67 -12 -14 8 126.63 5.69 -12 14 8 137.01 5.71 -12 -14 8 141.61 5.76 -12 -14 -8 144.53 5.71 -12 -14 -8 136.73 5.72 12 14 -8 131.92 5.77 -12 14 -8 142.84 5.79 -12 -14 -8 133.17 5.63 -12 14 8 138.60 5.67 12 14 8 143.48 5.83 12 14 9 433.17 16.41 12 -14 -9 422.39 16.28 -12 14 9 431.79 16.39 -12 14 -9 407.15 16.37 -12 -14 -9 413.43 16.29 -12 14 9 429.75 16.30 12 -14 -9 413.97 16.29 -12 14 9 414.01 16.31 -12 -14 9 408.79 16.33 -12 -14 -9 452.02 16.28 -12 -14 -9 443.58 16.30 -12 14 -9 433.83 16.37 -12 -14 -9 444.04 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4.07 2.90 -12 14 18 4.04 2.87 -12 -14 18 1.09 3.06 12 -14 18 2.67 2.53 -12 -14 -18 -0.95 3.07 12 14 19 39.96 3.80 -12 -14 -19 26.05 3.74 -12 -14 19 31.65 3.59 -12 14 19 37.07 3.44 -12 14 19 32.00 3.30 -12 -14 19 35.74 3.76 12 -14 19 29.02 3.15 -12 14 -19 22.16 3.54 -12 -14 -19 37.09 3.65 -12 14 -19 28.28 3.58 -12 -14 -20 8.91 3.61 -12 14 -20 5.39 3.41 -12 14 20 4.47 3.09 -12 -14 20 3.59 3.37 -12 14 20 0.81 3.11 -12 14 20 3.14 3.14 -12 -14 20 1.19 3.37 12 -14 20 8.93 2.81 -12 14 -20 6.19 3.35 -12 -14 -20 10.86 3.60 12 14 20 1.44 3.49 -12 14 -21 8.70 3.63 -12 -14 -21 11.74 3.85 12 14 21 15.42 3.59 -12 -14 21 15.34 3.49 -12 14 21 10.46 3.29 -12 14 21 11.23 3.42 -12 -14 21 13.29 3.70 -12 14 -21 15.18 3.57 -12 -14 -21 17.47 3.85 12 14 22 1.87 3.54 -12 -14 -22 8.66 3.99 -12 14 22 4.18 3.21 -12 -14 22 10.87 3.75 -12 14 22 6.47 3.32 -12 -14 22 9.98 3.86 -12 -14 -22 5.63 3.78 -12 -14 -23 20.18 4.33 -12 14 23 15.80 3.65 -12 -14 -23 19.92 4.24 -12 16 0 162.73 7.01 -12 16 0 175.41 6.86 12 16 0 180.19 6.85 -12 -16 0 180.29 6.81 12 16 0 156.36 6.83 -12 -16 0 203.73 6.90 -12 16 0 170.05 6.87 -12 -16 0 178.15 6.83 12 -16 0 165.65 6.91 12 -16 0 178.05 6.90 12 16 0 170.83 6.83 12 16 -1 1.99 1.14 -12 16 -1 0.11 1.22 12 -16 -1 0.20 1.57 -12 16 1 1.61 1.20 -12 -16 -1 2.38 1.20 12 16 1 0.20 1.18 -12 -16 1 0.83 1.17 -12 16 -1 1.44 1.68 12 16 1 1.81 1.39 -12 16 -1 0.62 1.31 -12 16 1 0.22 1.21 -12 -16 -1 1.15 1.25 12 16 -1 -0.44 1.39 -12 -16 1 2.53 1.31 -12 -16 -1 1.41 1.54 12 -16 1 3.87 1.61 -12 16 -1 2.81 1.63 12 -16 1 2.52 1.55 12 -16 -1 -0.92 1.48 12 16 1 3.16 1.34 -12 -16 1 2.26 1.22 12 16 -1 1.95 1.36 -12 -16 2 123.72 4.86 -12 -16 -2 123.82 4.89 -12 16 2 122.12 4.93 12 16 -2 109.96 4.85 -12 -16 2 123.31 4.94 12 -16 2 119.47 5.06 -12 -16 2 122.11 4.94 -12 16 -2 124.82 5.02 12 16 -2 135.18 4.97 12 16 2 117.75 4.95 -12 -16 -2 123.72 4.90 -12 16 2 119.29 4.94 -12 -16 -2 114.46 5.04 -12 16 -2 115.40 5.13 -12 16 -2 129.10 5.18 12 -16 2 117.55 5.05 12 16 2 121.32 4.93 12 -16 -2 125.12 5.01 -12 16 -2 129.53 5.01 12 -16 -2 118.62 5.04 12 16 -2 130.03 4.95 12 16 2 125.65 4.99 12 16 -3 70.59 3.35 -12 -16 -3 76.06 3.32 -12 16 3 75.53 3.35 -12 -16 3 83.04 3.37 12 16 3 77.48 3.39 12 -16 -3 69.64 3.47 12 16 -3 78.04 3.39 -12 16 -3 78.92 3.63 -12 -16 -3 82.50 3.36 -12 16 3 74.22 3.35 -12 -16 3 73.63 3.19 -12 -16 -3 78.80 3.54 -12 -16 3 82.35 3.39 -12 16 -3 77.60 3.46 12 -16 3 83.67 3.55 -12 16 -3 78.14 3.59 12 -16 3 86.75 3.53 12 16 3 85.02 3.39 12 16 -3 73.50 3.17 -12 16 3 75.30 3.60 12 -16 -3 70.61 3.40 -12 16 -3 80.31 3.44 12 16 3 79.36 3.46 12 -16 -4 12.62 1.69 -12 16 4 16.88 1.91 -12 -16 -4 12.97 1.40 12 16 4 14.05 1.53 12 16 -4 12.39 1.48 -12 16 4 11.41 1.38 12 -16 4 9.98 1.82 -12 -16 -4 11.19 1.41 12 16 4 10.94 1.63 12 -16 -4 11.92 1.75 12 16 -4 11.65 1.52 -12 -16 4 14.31 1.44 12 16 -4 15.55 1.03 -12 16 4 11.64 1.42 -12 16 -4 14.27 1.69 -12 -16 -4 13.85 1.85 -12 -16 4 13.11 1.47 12 -16 4 14.52 1.74 12 -16 4 14.62 1.79 12 16 4 11.25 1.59 -12 16 -4 14.01 1.62 -12 -16 4 13.90 1.07 12 -16 -5 16.50 1.74 -12 16 5 18.89 1.98 12 16 -5 16.79 1.77 -12 -16 5 18.53 1.04 -12 16 5 17.29 1.55 -12 16 -5 15.02 1.81 -12 -16 -5 16.47 1.62 12 -16 -5 16.22 1.77 12 16 -5 17.82 1.83 12 16 5 16.00 1.72 12 -16 5 19.64 1.84 -12 -16 -5 20.53 1.99 -12 -16 5 18.73 1.63 -12 16 5 16.78 1.55 -12 16 -5 19.55 1.88 12 16 -5 18.69 1.01 -12 16 -5 18.24 1.83 12 16 5 17.33 1.67 -12 -16 5 19.68 1.65 -12 16 -5 16.75 1.75 12 16 5 19.40 1.79 -12 -16 -5 16.47 1.57 12 -16 6 103.05 4.36 -12 -16 -6 107.49 4.22 12 -16 -6 117.89 4.34 -12 16 6 111.93 4.49 -12 -16 6 84.23 3.77 12 16 -6 104.27 4.25 -12 16 6 112.86 4.23 -12 16 -6 98.07 4.38 12 16 -6 108.80 4.31 -12 16 6 105.27 4.22 -12 -16 6 115.72 4.36 -12 16 -6 103.46 4.31 -12 16 -6 109.18 4.34 -12 -16 -6 118.64 4.29 -12 -16 -6 112.16 4.30 12 -16 -6 109.64 4.33 -12 -16 6 107.55 4.31 -12 16 -6 99.90 4.33 -12 -16 -6 102.04 4.17 12 16 6 110.63 4.38 12 -16 -7 430.15 16.04 -12 16 7 415.97 16.22 12 16 -7 440.14 16.08 -12 16 -7 400.52 16.16 -12 -16 -7 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14 -0.83 2.25 -12 16 14 1.57 2.14 -12 -16 14 0.40 2.38 -12 16 -14 0.70 2.51 -12 -16 -14 0.43 2.25 12 16 15 34.06 3.05 -12 16 -15 29.14 3.17 -12 -16 -15 37.19 2.99 -12 16 15 33.80 3.12 -12 16 15 37.07 2.98 -12 -16 15 35.75 3.17 -12 16 15 33.56 3.02 -12 -16 15 36.50 3.27 12 -16 15 35.53 2.56 -12 -16 -15 34.10 2.86 -12 16 -15 28.73 3.08 -12 -16 -16 6.43 2.58 -12 16 -16 7.22 2.87 12 16 16 11.72 2.95 12 -16 16 10.68 2.19 -12 16 16 8.17 2.73 -12 16 16 8.00 2.55 -12 -16 16 10.07 2.70 -12 16 16 5.47 2.60 -12 -16 16 6.09 2.83 -12 16 -16 7.62 2.79 12 -16 17 16.09 2.58 12 16 17 17.33 3.09 -12 -16 -17 9.98 3.18 -12 16 -17 11.54 3.05 -12 16 17 15.23 2.88 -12 16 17 15.63 2.69 -12 -16 17 13.25 2.88 -12 16 17 16.21 2.86 -12 -16 17 15.10 3.09 -12 16 -17 17.98 3.16 -12 -16 -17 14.83 3.11 12 -16 18 5.80 2.49 -12 -16 -18 -2.61 3.19 12 16 18 3.34 3.08 -12 16 -18 2.26 3.10 -12 16 18 1.06 2.77 -12 16 18 1.32 2.93 -12 -16 18 6.26 3.15 -12 16 18 -0.07 2.89 -12 -16 18 1.45 3.13 -12 16 -18 2.71 2.97 -12 -16 -18 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185.52 7.72 12 18 7 194.38 7.80 -12 -18 -7 196.84 7.57 -12 -18 7 191.36 7.66 12 18 8 -0.75 1.97 12 -18 -8 -0.84 1.73 -12 18 8 1.58 1.64 -12 18 8 1.27 2.00 -12 -18 -8 1.69 1.60 12 -18 -8 -1.63 1.77 12 -18 8 2.98 1.70 -12 18 8 0.07 1.72 -12 -18 8 5.29 1.79 -12 -18 8 4.91 1.73 -12 -18 -8 1.96 1.71 -12 -18 -8 -0.03 1.78 -12 18 -8 -0.16 1.82 -12 18 -8 0.13 1.86 -12 -18 -8 2.22 1.58 12 -18 -9 66.40 3.24 -12 -18 -9 61.19 3.20 -12 18 9 68.22 3.55 -12 18 -9 68.69 3.34 -12 18 -9 62.42 3.38 -12 18 9 63.92 3.12 12 -18 -9 60.15 3.25 -12 -18 9 67.18 3.35 -12 18 9 58.80 3.15 -12 -18 9 62.13 3.40 -12 -18 -9 65.75 3.22 -12 -18 -9 61.56 3.26 12 -18 9 65.72 3.26 -12 -18 -9 66.08 3.20 12 18 9 65.52 3.50 12 18 10 5.47 2.08 -12 18 -10 8.85 2.18 -12 -18 -10 9.94 1.94 -12 -18 10 9.89 2.04 -12 18 10 7.40 1.88 12 -18 10 8.57 1.90 -12 18 10 8.17 1.93 -12 18 10 6.82 2.16 -12 -18 10 10.97 2.12 -12 -18 -10 8.14 1.90 -12 -18 -10 9.67 1.95 -12 18 -10 6.18 2.07 -12 -18 -10 8.84 1.88 12 -18 11 16.22 2.04 12 18 11 15.01 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36.07 2.07 -12 20 -4 34.91 2.27 12 20 -4 34.53 2.15 12 -20 -4 36.85 2.21 -12 -20 -4 30.28 1.95 -12 20 4 33.76 2.08 -12 -20 4 37.59 2.16 -12 20 -4 34.04 2.11 -12 20 -4 32.46 2.15 12 20 4 37.85 2.09 -12 20 -4 41.37 2.48 12 20 4 36.48 2.39 12 -20 -4 38.78 2.16 -12 20 -4 35.03 2.17 -12 -20 -5 33.09 1.85 -12 -20 5 25.43 1.46 -12 20 5 28.82 2.38 12 20 -5 29.67 2.07 -12 20 5 30.28 1.93 -12 20 5 27.28 1.96 12 20 -5 26.24 1.44 -12 -20 5 28.48 2.03 -12 20 -5 31.43 2.20 -12 20 -5 31.24 1.92 -12 20 -5 26.01 1.94 -12 -20 -5 30.09 1.89 -12 -20 -5 30.95 1.94 -12 20 -5 30.81 2.29 -12 -20 -5 28.63 1.88 12 20 5 29.83 2.19 12 20 -5 29.77 2.11 -12 20 -5 27.74 2.10 12 -20 -5 29.44 2.02 -12 -20 5 35.08 2.03 12 -20 -5 30.18 2.08 -12 20 6 14.04 1.59 12 -20 -6 18.25 1.80 12 -20 -6 14.00 1.83 12 20 -6 18.58 1.84 -12 20 6 15.69 2.20 -12 -20 -6 16.37 1.58 12 20 -6 17.87 1.89 -12 20 6 16.28 1.63 -12 20 -6 13.61 1.70 -12 -20 -6 15.19 1.60 -12 20 -6 14.35 1.76 -12 -20 -6 15.41 1.62 -12 20 -6 16.61 2.08 -12 -20 6 11.70 0.79 -12 20 -6 15.99 1.86 -12 20 -6 17.72 1.91 -12 -20 -6 18.53 1.60 12 20 6 16.36 1.94 12 -20 -7 83.35 3.68 12 20 -7 86.73 3.70 -12 20 7 83.58 4.03 -12 20 -7 80.63 3.85 12 -20 -7 80.04 3.68 -12 -20 -7 73.55 3.56 -12 -20 7 87.65 3.75 12 20 -7 76.03 3.72 -12 20 7 81.23 3.62 -12 20 7 80.07 3.67 -12 -20 7 84.43 3.79 -12 -20 -7 83.61 3.58 -12 -20 -7 76.13 3.59 -12 20 -7 76.81 3.79 12 20 7 79.58 3.93 -12 -20 -7 79.22 3.54 12 -20 -8 29.87 2.19 -12 -20 -8 24.48 2.04 -12 20 8 25.71 2.02 -12 20 8 25.89 2.60 -12 20 -8 25.84 2.40 12 -20 -8 27.36 2.11 -12 -20 8 30.70 2.22 -12 20 8 22.54 2.08 -12 -20 8 26.75 2.24 -12 -20 -8 27.66 2.03 -12 -20 -8 24.90 2.07 -12 20 -8 29.66 2.36 12 -20 8 33.79 2.31 12 20 8 28.19 2.48 -12 -20 -8 25.40 1.98 12 20 9 12.57 2.15 12 -20 -9 6.93 1.78 -12 20 -9 8.96 2.23 -12 20 9 7.93 2.25 -12 -20 -9 8.94 1.81 12 -20 9 8.56 1.93 -12 -20 9 11.56 2.02 -12 20 9 10.14 1.88 -12 -20 9 8.76 2.07 -12 -20 -9 10.05 1.81 -12 -20 -9 9.88 1.85 12 -20 -9 6.23 1.85 -12 20 9 8.40 1.76 -12 20 -9 6.43 2.13 -12 -20 -9 7.07 1.68 12 20 10 5.60 2.18 -12 20 10 7.68 2.24 -12 -20 -10 7.06 1.91 -12 20 10 7.84 1.88 -12 -20 10 1.05 2.08 -12 20 -10 4.60 2.21 -12 20 10 5.62 1.91 -12 -20 10 3.72 2.18 -12 -20 -10 3.14 1.74 -12 -20 -10 6.52 1.81 12 -20 10 8.52 2.02 -12 20 -10 5.44 2.16 -12 -20 -10 4.94 1.76 -12 20 11 44.95 3.10 -12 20 -11 37.91 3.13 -12 -20 -11 39.35 2.75 -12 20 11 45.48 2.73 -12 -20 11 51.95 2.93 -12 20 11 38.87 2.75 -12 -20 11 45.05 2.98 -12 20 -11 45.19 3.09 -12 -20 -11 39.05 2.70 12 20 11 50.52 3.17 12 -20 11 47.90 2.80 -12 -20 -12 33.50 2.63 -12 20 12 34.61 3.00 -12 20 -12 31.37 3.03 -12 20 12 44.07 2.67 -12 -20 12 36.96 2.94 -12 20 12 30.52 2.65 -12 -20 12 44.27 3.03 12 -20 12 38.66 2.83 -12 20 -12 32.15 2.99 -12 -20 -12 36.83 2.59 12 20 12 44.69 2.91 12 20 13 2.73 2.41 -12 20 13 -0.18 2.64 -12 20 -13 -2.77 2.67 -12 20 13 -0.46 2.02 -12 -20 13 0.89 2.28 -12 -20 -13 3.30 2.26 -12 20 13 1.30 2.08 -12 -20 13 3.12 2.38 12 -20 13 0.56 2.07 -12 20 -13 5.16 2.59 -12 -20 -13 2.93 2.18 -12 20 -14 35.98 3.24 -12 20 14 31.08 3.13 -12 20 14 32.06 2.66 12 -20 14 25.62 2.69 -12 -20 14 33.70 2.95 -12 -20 -14 29.50 2.83 -12 20 14 22.72 2.69 -12 20 -14 31.44 3.13 -12 -20 -14 33.80 2.76 12 -20 15 5.29 2.31 -12 -20 -15 9.06 2.67 -12 20 15 7.72 2.95 -12 20 -15 4.81 2.86 -12 20 15 7.07 2.34 -12 -20 15 8.23 2.81 -12 20 15 4.51 2.45 -12 -20 15 5.41 2.85 -12 20 -15 7.47 2.87 -12 -20 -15 8.19 2.52 -12 20 -16 44.41 3.76 -12 -20 -16 47.95 3.62 12 -20 16 52.45 3.33 -12 20 16 54.92 3.43 -12 20 16 44.59 3.52 -12 -20 16 47.03 3.76 -12 20 -16 50.32 3.73 -12 -20 -16 52.75 3.47 12 -20 17 8.39 2.55 12 20 17 -1.75 3.16 -12 20 -17 2.76 3.07 -12 20 17 5.44 3.16 -12 -20 -17 10.07 3.06 -12 20 17 5.28 2.74 -12 -20 17 2.69 2.91 -12 20 17 3.76 2.80 -12 -20 17 4.97 3.03 -12 20 -17 1.13 3.02 -12 -20 -17 7.19 2.91 12 -20 18 22.46 2.88 12 20 18 28.10 3.61 -12 20 -18 22.27 3.63 -12 20 18 33.84 3.19 -12 20 -18 30.13 3.68 -12 20 18 31.55 3.45 -12 -20 18 28.27 3.59 -12 20 18 26.05 3.23 -12 -20 18 30.34 3.83 12 20 19 0.17 3.44 -12 -20 -19 -0.26 3.10 -12 20 -19 3.36 3.53 -12 20 19 8.87 3.01 -12 20 19 10.45 3.50 -12 20 19 9.21 3.14 -12 20 -19 4.56 3.48 12 20 20 11.01 3.77 -12 20 -20 6.93 3.73 -12 20 20 10.32 3.20 -12 20 -20 11.82 3.88 -12 -20 20 9.00 3.47 -12 20 20 5.54 3.53 -12 20 20 9.51 3.24 -12 -20 20 13.69 3.62 -12 20 -21 7.73 3.86 -12 20 21 11.65 3.38 -12 20 21 8.85 3.59 -12 20 21 6.20 3.42 -12 20 -21 6.83 3.86 -12 20 22 -3.60 3.38 -12 20 22 -5.29 3.60 -12 22 0 292.50 10.89 12 -22 0 273.99 10.89 -12 -22 0 299.80 10.98 12 22 0 287.77 10.86 -12 22 0 283.80 10.90 -12 -22 0 281.16 10.83 -12 -22 0 283.40 10.82 12 -22 0 284.38 10.90 12 22 0 265.97 10.82 12 22 0 293.19 10.95 -12 22 0 293.02 11.21 -12 22 1 3.19 1.93 12 22 -1 1.50 1.37 -12 -22 1 3.00 1.53 -12 22 -1 1.17 1.42 -12 22 -1 2.64 1.46 -12 22 1 2.90 1.39 12 -22 1 1.70 1.59 12 22 -1 1.31 1.43 -12 -22 -1 1.89 1.88 -12 22 1 2.32 1.46 -12 -22 1 1.20 1.25 -12 -22 -1 2.03 1.27 12 -22 -1 2.28 1.56 12 22 1 1.70 1.42 -12 -22 -1 1.82 1.22 12 -22 1 2.25 1.56 12 -22 -1 1.99 1.50 12 22 1 1.76 1.37 12 22 -1 3.19 1.40 -12 22 -1 3.12 1.86 -12 -22 1 1.02 1.28 12 22 1 3.43 1.55 -12 22 2 17.79 2.15 -12 22 -2 18.89 1.73 -12 22 -2 17.36 1.77 -12 -22 -2 16.45 1.44 -12 22 2 19.11 1.62 -12 -22 2 21.12 1.64 -12 -22 -2 19.79 2.12 12 -22 2 16.94 1.82 12 22 2 16.76 1.59 -12 -22 2 17.58 1.50 12 22 -2 15.22 1.68 -12 22 2 18.05 1.62 -12 -22 -2 14.12 1.45 -12 -22 2 16.49 1.55 12 -22 -2 19.43 1.78 12 -22 2 15.96 1.79 12 22 2 17.50 1.56 12 -22 -2 21.10 1.75 -12 22 -2 23.39 2.22 12 22 -2 19.16 1.51 12 22 2 16.30 1.91 12 22 -2 16.04 1.63 -12 22 -3 0.06 1.54 12 22 -3 1.71 1.42 -12 -22 -3 2.36 1.23 12 22 -3 0.66 1.22 -12 -22 3 1.88 1.24 -12 22 3 0.40 1.31 12 22 3 3.14 1.37 12 -22 -3 5.28 1.56 12 22 -3 0.85 1.43 -12 22 3 0.44 1.38 -12 -22 3 1.62 1.40 -12 -22 -3 1.55 1.26 -12 -22 3 -0.46 1.42 -12 22 -3 2.25 1.60 -12 22 -3 3.32 1.54 12 22 3 0.85 1.35 -12 22 -3 0.29 1.79 12 -22 -3 2.50 1.47 -12 22 -3 2.32 1.58 12 22 3 1.85 1.78 12 22 -4 205.09 8.06 -12 -22 4 222.25 7.94 12 -22 -4 202.42 8.09 -12 22 4 193.40 8.05 -12 -22 -4 216.89 8.00 12 22 -4 202.25 7.95 12 22 4 193.16 8.01 -12 22 4 202.76 8.05 -12 22 -4 206.55 8.16 -12 -22 -4 200.04 7.99 12 22 -4 198.87 8.06 -12 -22 4 212.93 8.10 -12 22 -4 208.50 8.12 -12 22 -4 203.64 8.12 12 22 4 205.76 8.02 -12 22 -4 214.24 8.39 12 22 4 221.35 8.28 -12 -22 4 214.31 8.07 12 -22 -4 206.55 8.06 -12 22 -4 207.75 8.14 -12 -22 -5 37.26 2.07 12 22 -5 37.63 2.21 -12 -22 -5 29.62 2.04 12 22 -5 36.29 1.73 -12 22 5 36.33 2.12 -12 22 -5 35.38 2.34 12 -22 -5 33.34 2.26 12 22 -5 33.22 2.25 -12 22 5 31.12 2.14 -12 -22 5 32.04 2.19 -12 -22 5 37.85 2.18 -12 22 -5 44.36 2.27 -12 -22 -5 38.24 2.06 -12 22 -5 35.97 2.27 -12 -22 -5 33.72 2.06 -12 22 -5 35.99 2.64 12 22 5 40.19 2.51 -12 22 -5 35.81 2.29 12 -22 -5 35.35 2.20 -12 -22 5 37.71 1.74 -12 -22 6 3.44 1.57 -12 -22 -6 3.58 1.48 12 22 -6 3.75 1.63 -12 22 6 3.02 2.15 -12 22 6 3.38 1.56 -12 22 -6 0.30 1.73 12 22 -6 5.78 1.74 -12 22 6 3.64 1.61 -12 -22 6 1.75 1.65 -12 22 -6 3.28 2.02 -12 22 -6 2.97 1.65 -12 -22 -6 1.82 1.50 -12 -22 -6 2.79 1.41 -12 22 -6 3.24 1.65 -12 -22 -6 1.83 1.45 -12 22 -6 2.57 1.67 12 22 6 3.40 1.92 12 -22 -6 3.50 1.63 12 -22 -6 5.88 1.65 12 22 -7 59.37 2.90 -12 -22 -7 50.34 2.73 -12 22 7 55.32 3.33 -12 22 7 52.59 2.73 12 -22 -7 53.75 2.82 12 22 -7 52.84 2.90 -12 -22 7 60.39 2.93 -12 22 7 50.29 2.76 -12 -22 7 47.36 2.91 -12 22 -7 54.02 3.06 -12 -22 -7 52.19 2.70 -12 -22 -7 54.73 2.76 -12 22 -7 53.70 3.17 12 22 7 55.79 3.20 -12 22 -7 53.52 2.97 -12 -22 -7 56.50 2.71 12 -22 -7 58.85 2.82 12 -22 -8 1.95 1.77 -12 22 8 4.27 2.42 -12 -22 -8 5.12 1.66 -12 22 8 2.99 1.58 12 -22 -8 2.07 1.81 -12 -22 8 4.84 1.82 -12 22 8 0.98 1.66 -12 -22 8 4.34 1.95 -12 22 -8 -1.92 2.03 -12 22 -8 1.44 1.94 -12 22 -8 3.63 1.89 12 22 8 1.71 2.10 -12 -22 -8 1.73 1.51 -12 22 9 6.64 1.69 -12 22 -9 4.64 2.25 -12 22 9 4.87 2.50 -12 -22 -9 6.21 1.77 -12 -22 9 7.68 1.96 -12 22 9 2.97 1.72 -12 -22 9 2.76 2.02 -12 22 -9 5.91 2.18 -12 22 -9 6.20 2.19 -12 -22 -9 3.75 1.69 12 22 9 5.79 2.18 12 -22 10 92.52 4.27 -12 22 10 94.85 4.53 -12 -22 -10 82.37 3.99 -12 22 10 88.48 4.04 -12 22 -10 85.01 4.19 -12 22 10 85.99 4.07 -12 -22 10 84.90 4.13 -12 22 -10 90.50 4.16 12 22 10 93.10 4.43 -12 -22 -10 86.83 3.97 12 22 11 2.28 2.36 12 -22 11 4.98 2.09 -12 22 -11 3.39 2.21 -12 22 11 0.25 2.54 -12 22 11 3.59 1.93 -12 -22 11 1.64 2.21 -12 22 11 4.10 1.97 -12 -22 11 1.88 2.29 -12 22 -11 4.45 2.14 -12 -22 -11 1.28 1.94 -12 -22 -11 4.91 2.08 12 22 12 11.72 2.70 -12 22 12 14.89 2.20 -12 -22 -12 14.15 2.24 -12 22 -12 8.63 2.71 -12 22 12 16.79 2.78 12 -22 12 15.70 2.22 -12 22 12 14.31 2.26 -12 -22 12 17.91 2.28 -12 22 -12 17.76 2.69 -12 -22 -12 12.86 2.15 12 22 13 0.92 2.53 -12 22 -13 4.42 2.72 -12 -22 -13 0.21 2.29 -12 22 13 6.04 2.76 -12 22 13 2.32 2.17 -12 -22 13 3.93 2.30 -12 22 13 3.56 2.22 -12 -22 13 2.50 2.50 -12 22 -13 1.07 2.63 -12 -22 -13 2.60 2.23 12 -22 13 -2.14 2.04 -12 22 14 115.17 5.57 12 -22 14 113.58 5.11 -12 22 -14 109.84 5.49 -12 -22 -14 92.13 5.10 -12 22 14 116.36 5.10 -12 -22 14 113.82 5.27 -12 22 14 110.07 5.16 -12 -22 14 104.54 5.33 -12 22 -14 108.34 5.42 -12 -22 -14 107.08 5.09 12 22 14 119.76 5.43 -12 22 -15 -5.22 3.04 -12 -22 -15 4.70 2.67 12 -22 15 2.68 2.38 -12 22 15 0.75 2.96 -12 22 15 4.22 2.37 -12 22 15 3.49 2.50 -12 -22 15 6.92 2.71 -12 22 -15 5.83 2.96 -12 -22 -15 1.70 2.54 -12 -22 16 36.21 3.48 -12 22 -16 33.28 3.60 -12 -22 -16 36.37 3.28 -12 22 16 41.96 3.80 -12 22 16 39.20 3.09 -12 22 16 33.22 3.25 -12 -22 16 35.07 3.58 -12 22 -16 34.29 3.53 -12 -22 -16 35.71 3.19 12 -22 16 45.07 3.17 12 -22 17 1.19 2.58 -12 22 -17 -6.57 3.38 -12 22 17 -0.29 3.43 -12 22 17 0.51 2.59 -12 -22 17 5.12 3.15 -12 22 17 0.95 2.73 -12 -22 17 -2.00 3.22 -12 22 -17 0.43 3.18 12 22 18 64.67 4.42 -12 22 -18 42.66 4.44 -12 -22 18 57.44 4.07 -12 22 18 68.50 4.57 -12 22 18 55.94 3.72 -12 22 18 47.84 3.76 -12 -22 18 55.35 4.24 -12 22 -18 55.37 4.41 12 22 19 4.24 3.45 -12 22 -19 4.77 3.51 -12 22 19 -0.84 3.49 -12 22 19 2.51 2.99 -12 -22 19 3.25 3.42 -12 22 19 0.46 3.08 -12 -22 19 1.69 3.57 -12 22 -20 7.76 3.73 -12 22 -20 1.69 3.83 -12 22 20 6.38 3.52 -12 -22 20 1.17 3.59 -12 -22 20 5.91 3.79 -12 22 -21 1.95 4.07 -12 22 21 6.37 3.52 -12 -22 21 5.34 3.58 -12 22 -21 4.15 4.00 -12 24 0 57.97 2.74 12 -24 0 55.69 2.83 -12 -24 0 64.29 2.97 -12 -24 0 59.43 2.58 12 24 0 52.51 2.67 -12 24 0 55.94 2.76 -12 -24 0 57.22 2.61 12 -24 0 54.71 2.80 12 24 0 56.74 2.66 12 24 0 54.76 2.88 -12 24 0 58.26 3.25 -12 24 -1 25.12 1.90 -12 24 1 28.54 1.80 -12 -24 1 23.86 1.98 -12 -24 -1 25.55 1.64 -12 -24 -1 28.42 2.24 12 -24 1 27.05 2.03 12 -24 -1 26.06 1.97 12 24 1 28.80 2.12 12 24 1 26.30 1.81 -12 -24 1 26.28 1.70 12 24 -1 25.89 1.86 -12 -24 -1 27.06 1.66 -12 -24 1 27.07 1.76 -12 24 -1 23.52 1.94 12 -24 1 29.94 1.99 12 -24 -1 26.22 1.93 12 24 1 27.47 1.77 12 24 -1 28.33 1.94 12 24 -1 26.60 1.83 -12 24 -1 26.36 2.40 -12 24 1 24.94 1.81 -12 24 1 26.93 2.47 -12 24 2 124.83 5.30 -12 24 -2 124.93 4.88 -12 -24 2 118.53 4.80 -12 24 2 123.99 4.78 -12 -24 -2 109.53 4.65 12 24 2 111.60 4.72 12 -24 -2 114.35 4.81 12 24 -2 117.72 4.79 -12 24 2 109.28 4.77 -12 -24 -2 106.25 4.65 -12 -24 2 119.15 4.76 -12 -24 2 125.84 4.75 12 24 2 116.51 4.72 12 -24 -2 114.07 4.77 12 24 2 116.23 5.01 -12 24 -2 115.77 4.88 -12 24 -2 121.62 5.22 12 24 -2 123.83 4.80 12 24 -2 114.46 4.75 -12 24 3 92.62 4.44 -12 -24 3 92.54 3.91 -12 24 -3 87.33 4.06 -12 -24 -3 103.02 3.84 12 24 -3 92.13 3.98 -12 24 3 92.26 3.96 12 24 3 84.81 3.89 12 -24 -3 91.11 4.02 -12 -24 -3 87.31 3.85 -12 24 3 90.84 3.98 -12 -24 3 99.11 3.95 -12 -24 3 88.51 3.97 -12 24 -3 93.83 4.04 -12 24 -3 95.17 4.06 12 24 3 90.75 3.88 12 24 3 93.88 4.23 12 -24 -3 95.64 4.01 -12 24 -3 91.39 4.42 12 24 -3 99.93 3.94 12 24 -3 92.43 3.97 -12 24 -3 93.94 4.06 12 24 -4 45.90 2.51 12 24 -4 47.60 2.27 -12 -24 -4 45.73 2.22 -12 24 4 47.70 2.41 -12 24 -4 44.56 2.62 -12 -24 4 43.04 2.41 12 24 -4 46.14 2.54 -12 -24 -4 44.51 2.26 -12 24 4 45.14 2.42 12 -24 -4 47.54 2.49 -12 -24 4 46.10 2.49 -12 24 -4 44.24 2.94 -12 24 -4 46.29 2.58 -12 24 -4 43.37 2.58 12 24 4 51.85 2.87 12 -24 -4 47.97 2.46 -12 24 -4 48.04 2.60 12 24 -5 56.07 2.67 -12 -24 5 48.58 2.66 -12 -24 -5 49.36 2.44 -12 -24 -5 49.70 2.41 12 24 -5 50.77 2.29 -12 24 5 49.34 2.54 -12 24 -5 50.74 2.83 12 24 -5 48.77 2.70 -12 -24 5 53.80 2.65 -12 24 5 43.79 2.55 -12 24 -5 55.92 2.74 -12 24 -5 50.92 2.76 12 24 5 49.55 2.99 -12 24 -5 47.23 3.03 -12 24 -5 49.19 2.74 -12 -24 -6 44.79 2.28 12 24 -6 41.65 2.51 -12 24 -6 37.60 2.67 12 24 -6 38.38 2.55 -12 -24 6 45.71 2.48 -12 24 6 43.97 2.35 -12 -24 -6 38.05 2.27 -12 24 6 42.27 2.38 -12 -24 6 39.83 2.50 -12 24 -6 44.34 2.54 -12 24 -6 47.70 2.63 -12 24 -6 51.75 2.97 12 24 6 47.85 2.88 -12 24 -6 42.20 2.64 -12 -24 -7 1.90 1.41 12 24 -7 -1.28 1.76 -12 24 7 0.41 2.18 -12 24 7 2.24 1.53 -12 -24 -7 -0.05 1.49 12 24 -7 0.13 1.76 -12 -24 7 -0.04 1.88 -12 24 7 1.92 1.62 -12 -24 7 -1.93 1.97 -12 24 -7 2.27 2.16 -12 24 -7 0.28 1.95 -12 24 -7 -0.99 1.88 12 24 7 0.41 2.13 -12 24 8 14.84 1.81 -12 24 8 10.07 2.62 -12 -24 -8 11.28 1.79 -12 -24 8 19.62 2.09 -12 24 -8 13.68 2.23 -12 24 8 12.25 1.85 -12 -24 8 15.33 2.07 -12 24 -8 18.06 2.39 -12 24 -8 16.89 2.17 12 24 8 15.28 2.31 -12 -24 -8 17.42 1.81 -12 24 -9 31.25 2.67 -12 24 9 31.12 2.91 -12 24 9 30.35 2.23 -12 -24 9 36.78 2.44 -12 -24 -9 32.31 2.22 -12 24 9 30.03 2.33 -12 -24 9 31.52 2.53 -12 24 -9 32.01 2.76 12 24 9 34.41 2.77 -12 24 -9 29.69 2.60 -12 -24 -9 29.37 2.16 -12 24 10 12.04 2.55 -12 -24 -10 9.45 1.88 -12 24 -10 8.87 2.36 -12 24 10 10.55 1.86 -12 -24 10 7.64 2.11 -12 24 10 12.42 2.02 -12 -24 10 12.23 2.23 -12 24 -10 10.90 2.32 -12 24 -10 12.63 2.29 -12 -24 -10 9.25 1.83 12 24 10 10.06 2.42 -12 -24 -11 10.91 1.99 -12 24 11 13.43 2.05 -12 -24 11 14.93 2.22 -12 24 11 9.02 2.09 -12 -24 11 13.87 2.34 -12 24 -11 12.84 2.38 -12 24 -11 13.80 2.50 -12 24 11 14.92 2.73 -12 24 -11 11.74 2.55 -12 -24 -11 10.23 1.96 12 24 11 18.08 2.71 -12 -24 -12 40.16 2.85 -12 24 12 48.33 3.61 -12 24 12 52.71 2.99 -12 24 12 44.69 2.96 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5.28 3.51 -12 24 -20 9.51 3.94 -12 24 20 5.32 3.82 -12 24 -20 9.57 3.90 -12 -24 21 -1.14 3.65 -12 -24 21 3.44 3.82 -12 26 0 44.64 2.34 -12 -26 0 47.53 2.67 -12 -26 0 45.41 2.17 -12 26 0 43.44 2.36 -12 -26 0 40.12 2.18 12 26 0 42.70 2.56 -12 26 0 49.23 3.06 -12 26 -1 -0.11 2.12 -12 -26 -1 1.97 1.15 -12 26 1 2.90 2.30 -12 26 -1 4.18 1.49 -12 -26 1 3.51 1.76 -12 26 1 3.62 1.39 -12 -26 1 3.47 1.28 -12 26 -1 4.62 1.54 -12 26 1 3.33 1.45 -12 -26 -1 2.81 1.20 -12 -26 1 2.51 1.32 12 26 1 2.83 1.90 12 26 -1 1.47 1.65 -12 26 2 327.44 12.63 -12 26 -2 333.13 12.27 -12 26 2 307.33 12.21 -12 26 2 331.14 12.21 -12 -26 -2 321.42 12.12 -12 -26 2 350.57 12.18 -12 26 -2 315.95 12.27 -12 -26 -2 286.56 12.11 -12 -26 2 302.32 12.16 -12 26 -2 343.49 12.26 -12 26 -2 314.34 12.25 12 26 2 351.88 12.45 12 26 -2 314.66 12.25 -12 26 -2 314.06 12.59 -12 -26 3 4.45 1.44 -12 26 -3 8.45 1.70 12 26 -3 4.52 1.50 -12 26 3 4.50 2.23 -12 -26 -3 4.66 1.22 -12 26 3 6.71 1.42 -12 26 -3 5.33 1.73 -12 -26 -3 5.32 1.27 -12 26 3 4.68 1.46 -12 -26 3 7.27 1.49 12 26 3 4.37 2.07 -12 26 -3 1.24 2.20 -12 26 -4 9.42 1.75 -12 -26 4 4.01 1.55 -12 26 4 5.39 1.44 12 26 -4 7.92 1.40 -12 26 4 5.81 2.27 -12 -26 -4 6.25 1.24 -12 -26 4 6.18 1.51 -12 26 -4 6.43 1.77 -12 26 4 6.44 1.51 12 26 4 3.96 2.08 -12 -26 -4 5.67 1.25 -12 26 -4 6.11 2.13 -12 -26 -5 1.88 1.21 12 26 -5 1.99 1.20 -12 26 -5 1.78 1.74 -12 -26 -5 1.00 1.25 -12 -26 5 2.34 1.61 -12 26 5 0.27 1.50 -12 -26 5 2.88 1.67 12 26 5 -0.78 2.18 -12 26 -5 3.35 2.27 -12 26 -5 0.64 1.66 -12 26 5 -0.16 1.42 -12 -26 -6 142.93 5.60 -12 26 -6 133.52 5.89 -12 26 6 145.19 5.73 -12 -26 -6 127.98 5.60 -12 -26 6 150.33 5.80 -12 26 6 131.06 5.73 -12 -26 6 142.21 5.83 12 26 6 163.07 6.17 -12 26 -6 147.45 6.23 -12 26 -6 147.32 5.87 -12 -26 -7 16.79 1.64 -12 26 7 21.34 1.81 -12 -26 -7 16.52 1.63 -12 -26 7 17.97 1.96 -12 -26 7 20.13 2.06 -12 26 -7 18.66 2.39 12 26 7 20.16 2.52 -12 26 -7 14.25 2.04 -12 26 -7 15.13 2.09 -12 26 8 48.49 3.47 -12 26 -8 42.11 2.96 -12 -26 8 54.25 2.90 -12 26 8 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44.41 3.13 -12 28 -2 44.41 2.41 -12 28 2 45.04 2.32 -12 28 2 42.42 2.32 -12 -28 2 43.14 2.21 -12 28 -2 43.80 2.47 -12 -28 2 41.25 2.23 12 28 2 46.11 2.83 12 28 -2 42.72 2.54 -12 28 -2 42.20 3.13 -12 28 -3 10.10 2.47 12 28 -3 9.05 1.59 -12 28 -3 13.26 1.75 -12 28 3 13.14 2.37 -12 28 -3 9.90 1.74 -12 -28 3 7.56 1.42 -12 28 3 11.42 1.55 -12 -28 3 9.31 1.50 -12 28 3 12.51 1.54 12 28 3 11.78 2.11 -12 28 4 103.73 4.24 -12 28 4 99.97 4.98 -12 -28 4 105.48 4.28 -12 28 4 94.27 4.23 -12 28 -4 93.88 4.38 -12 -28 4 98.07 4.29 12 28 4 109.15 4.74 -12 28 -4 102.15 4.84 12 28 -4 104.13 4.25 -12 28 -4 103.52 4.38 -12 28 5 56.89 3.68 -12 28 5 59.10 2.88 -12 -28 5 60.76 2.95 -12 28 -5 58.31 3.15 -12 28 5 56.08 2.89 -12 -28 5 58.14 2.96 12 28 5 65.62 3.59 -12 28 -5 69.22 3.55 -12 28 -5 64.37 3.15 -12 28 -6 9.29 2.02 -12 28 6 8.10 1.56 -12 -28 6 8.94 1.73 -12 -28 6 10.91 1.79 -12 28 6 8.69 1.63 12 28 6 10.98 2.49 -12 28 -6 8.34 2.44 -12 28 -6 7.95 1.85 -12 28 -7 14.80 2.22 -12 28 7 16.29 1.73 -12 -28 7 14.83 2.00 -12 28 7 14.95 1.76 -12 -28 7 15.35 2.05 12 28 7 20.03 2.59 -12 28 -7 20.56 2.71 -12 28 -7 17.49 2.14 -12 -28 8 -1.28 2.01 -12 -28 8 -1.29 1.94 -12 28 -8 -1.82 2.12 -12 28 -8 2.09 2.43 12 28 8 -3.11 2.47 -12 28 -8 1.30 2.04 -12 28 9 65.18 4.02 -12 28 -9 48.57 3.38 -12 -28 9 62.07 3.26 -12 -28 9 59.20 3.33 12 28 9 70.74 3.86 -12 28 -9 52.79 3.35 -12 28 -9 64.51 3.71 -12 28 10 25.21 3.11 -12 28 -10 24.41 2.62 -12 -28 10 22.86 2.43 -12 -28 10 22.64 2.54 -12 28 -10 23.69 2.80 -12 28 -10 19.99 2.51 12 28 10 25.38 3.05 -12 28 -11 1.97 2.47 -12 28 11 -0.44 2.89 -12 -28 11 0.50 2.32 -12 28 -11 4.73 2.54 -12 28 -11 5.76 2.43 12 28 11 7.24 2.81 -12 28 12 5.18 3.19 -12 28 -12 3.48 2.66 -12 -28 12 7.38 2.43 -12 -28 12 4.25 2.49 -12 28 -12 7.51 2.64 -12 28 -12 6.74 2.57 12 28 12 6.69 2.88 -12 28 13 -1.99 3.15 -12 28 -13 3.12 2.74 -12 -28 13 2.76 2.58 -12 -28 13 -0.11 2.73 -12 28 -13 -3.81 2.55 -12 28 -13 -0.45 2.63 12 28 13 -1.78 3.00 12 28 14 24.96 3.51 -12 28 -14 20.79 3.08 -12 28 14 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154.05 6.07 -15 -15 7 123.63 5.45 -15 -15 7 163.10 6.03 -15 15 -7 151.44 6.13 -15 -15 -7 156.78 6.07 15 -15 7 176.57 6.12 -15 15 7 157.26 6.09 -15 -15 7 160.97 6.11 -15 -15 -7 166.71 6.05 -15 -15 -7 171.29 6.06 -15 15 -7 168.69 6.15 -15 -15 -7 163.55 6.02 -15 15 8 2.94 2.01 -15 -15 -8 3.06 1.95 15 15 8 5.36 2.04 -15 15 -8 2.61 2.02 -15 15 8 2.96 1.83 -15 -15 8 3.85 1.83 -15 15 8 8.19 1.86 -15 -15 8 6.20 1.94 -15 15 -8 7.09 1.95 -15 -15 -8 7.82 1.88 15 -15 8 7.55 1.92 -15 15 -9 7.61 2.01 -15 15 9 9.77 2.07 -15 15 9 7.18 1.88 15 15 9 9.85 2.16 -15 -15 -9 7.78 2.03 -15 15 9 3.56 1.91 -15 -15 9 5.99 2.08 15 -15 9 7.32 2.02 -15 -15 9 6.51 1.92 -15 15 -9 8.47 1.96 -15 -15 -9 5.44 1.99 -15 15 10 -2.92 2.21 -15 15 10 -3.94 1.88 -15 15 -10 -1.71 2.24 -15 -15 10 -0.33 1.96 15 15 10 -0.83 2.02 -15 15 10 -1.20 1.94 -15 -15 10 -2.42 2.11 15 -15 10 0.19 1.94 -15 -15 -10 0.60 2.04 -15 15 -10 -0.85 2.16 -15 -15 -10 0.49 2.00 -15 15 11 19.98 2.68 15 15 11 24.68 2.57 -15 15 -11 18.25 2.65 -15 -15 -11 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17 0.21 3.47 -15 -25 17 1.46 3.62 -15 25 -17 4.68 3.48 -15 25 -18 5.42 3.95 -15 25 18 0.50 3.81 -15 25 -18 7.46 3.79 -15 25 -19 3.04 3.96 -15 25 19 5.95 3.87 -15 -25 19 2.75 3.59 -15 -25 19 5.13 3.90 -15 25 -19 4.80 3.90 15 27 0 94.75 4.24 -15 27 0 95.99 4.13 -15 -27 0 90.36 3.94 -15 27 0 94.42 4.17 -15 -27 0 86.26 3.94 -15 27 0 93.47 4.57 -15 27 -1 9.02 2.48 -15 27 1 5.02 2.42 -15 27 -1 10.21 1.92 15 27 1 10.21 2.02 -15 27 1 9.83 1.76 15 27 -1 11.00 1.80 -15 -27 -1 7.73 1.54 -15 -27 1 7.50 1.60 -15 27 1 8.29 1.82 -15 -27 -1 9.12 1.55 -15 -27 1 7.77 1.66 -15 27 -1 10.62 1.96 -15 27 2 13.66 2.51 -15 27 -2 10.36 1.96 15 27 2 14.02 2.15 -15 27 2 14.16 1.81 15 27 -2 15.42 1.80 -15 -27 2 18.14 1.72 -15 27 -2 10.70 2.04 -15 27 2 13.34 1.89 -15 -27 2 11.70 1.78 -15 27 -2 17.08 2.65 -15 27 -3 1.77 1.89 -15 27 3 -0.71 2.36 15 27 3 -1.84 2.06 -15 27 3 0.90 1.72 -15 -27 3 0.73 1.63 15 27 -3 0.06 1.54 -15 27 -3 -2.80 1.94 -15 27 3 0.17 1.76 -15 -27 3 -0.66 1.70 -15 27 -3 -0.74 2.37 -15 27 -4 16.44 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6.01 0.00 3 7 22 -2.12 0.00 0 8 22 7.08 0.00 0 0 0 0.00 0.00 # SQUEEZE RESULTS (Version = 41016) # Note: Data are Listed for all Voids in the P1 Unit Cell # i.e. Centre of Gravity, Solvent Accessible Volume, # Recovered number of Electrons in the Void and # Details about the Squeezed Material loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 -0.015 -0.002 -0.001 11022 2171 ' ' # Missing Reflections Below sin(th)/lambda = 0.25 loop_ _platon_missing_refln_index_h _platon_missing_refln_index_k _platon_missing_refln_index_l _platon_missing_refln_theta 2 0 0 1.551 1 1 0 0.986 0 2 0 1.218 1 1 1 1.467 0 2 1 1.632 _platon_squeeze_void_probe_radius 1.20 _platon_squeeze_details ) TITL a C m c m R = 0.11 CELL 26.2639 33.4313 18.7507 90.00 90.00 90.00 SPGR Cmcm # Solvent Accessible Volume = 11021 # Electrons Found in S.A.V. = 2151 # Note: Atoms in Void as Cxxx and Qxxx all others C101 0.132 0.242 0.247 ! 2.94 eA-3 C102 0.094 0.203 0.254 ! 2.69 eA-3 C103 1.000 0.472 0.050 ! 2.49 eA-3 C104 0.220 0.391 0.253 ! 2.18 eA-3 C105 0.500 0.021 0.470 ! 2.06 eA-3 Q106 0.101 0.273 0.247 ! 2.03 eA-3 C107 0.673 0.376 0.381 ! 1.92 eA-3 Q108 0.446 0.234 0.756 ! 1.90 eA-3 C109 0.022 0.233 0.500 ! 1.71 eA-3 C110 0.555 0.285 0.016 ! 1.61 eA-3 C111 0.760 0.144 0.711 ! 1.55 eA-3 C112 0.500 0.085 0.499 ! 1.34 eA-3 C113 0.783 0.112 0.819 ! 1.34 eA-3 C114 0.523 0.238 0.500 ! 1.33 eA-3 Q115 0.892 0.190 0.296 ! 1.21 eA-3 C116 0.359 0.158 0.141 ! 1.20 eA-3 Q117 0.453 0.283 0.755 ! 1.19 eA-3 Q118 0.047 0.217 0.245 ! 1.19 eA-3 C119 0.646 0.375 0.048 ! 1.19 eA-3 Q120 0.554 0.271 0.791 ! 1.18 eA-3 C121 1.000 0.246 0.068 ! 1.17 eA-3 Q122 0.858 0.212 0.152 ! 1.14 eA-3 Q123 0.720 0.470 0.074 ! 1.12 eA-3 C124 0.203 0.141 0.341 ! 1.11 eA-3 Q125 0.546 0.035 0.153 ! 1.06 eA-3 C126 0.055 0.272-0.003 ! 1.05 eA-3 C127 0.272 0.423 0.200 ! 1.05 eA-3 C128 0.828 0.125 0.148 ! 0.98 eA-3 C129 0.210 0.445 0.252 ! 0.98 eA-3 C130 0.500 0.296 0.715 ! 0.96 eA-3 C131 0.648 0.085 0.344 ! 0.94 eA-3 C132 0.710 0.141 0.261 ! 0.94 eA-3 C133 0.336 0.073 0.349 ! 0.94 eA-3 C134 0.657 0.149 0.244 ! 0.93 eA-3 C135 0.860 0.500 0.742 ! 0.91 eA-3 C136 0.634 0.035 0.208 ! 0.87 eA-3 C137 0.109 0.393 0.624 ! 0.85 eA-3 C138 0.677 0.026 0.300 ! 0.83 eA-3 Q139 0.609 0.396 0.051 ! 0.82 eA-3 C140 1.000 0.467 0.626 ! 0.78 eA-3 C141 0.243 0.039 0.761 ! 0.75 eA-3 C142 0.500 0.133 0.248 ! 0.74 eA-3 C143 0.737 0.141 0.329 ! 0.73 eA-3 C144 0.278 0.453 0.206 ! 0.72 eA-3 C145 0.398 0.057 0.156 ! 0.71 eA-3 C146 0.072 0.088 0.004 ! 0.68 eA-3 C147 0.046 0.250 0.117 ! 0.67 eA-3 Q148 0.165 0.490 0.532 ! 0.67 eA-3 C149 0.790 0.420 0.847 ! 0.66 eA-3 Q150 0.899 0.087 0.870 ! 0.64 eA-3 C151 0.462 0.088 0.443 ! 0.64 eA-3 C152 0.952 0.067 0.486 ! 0.64 eA-3 Q153 0.775 0.048 0.454 ! 0.61 eA-3 Q154 0.162 0.145 0.407 ! 0.60 eA-3 Q155 0.838 0.848 0.905 ! 0.60 eA-3 Q156 0.338 0.348 0.905 ! 0.60 eA-3 C157 0.771 0.148 0.257 ! 0.58 eA-3 C158 0.455 0.477 0.434 ! 0.58 eA-3 Q159 0.825 0.030 0.045 ! 0.58 eA-3 C160 0.475 0.459 0.017 ! 0.56 eA-3 Q161 0.635 0.268 0.308 ! 0.55 eA-3 C162 0.540 0.452 0.499 ! 0.55 eA-3 C163 0.586 0.168 0.175 ! 0.55 eA-3 Q164 0.604 0.266 0.255 ! 0.54 eA-3 C165 0.548 0.442 0.022 ! 0.53 eA-3 Q166 1.000 0.266 0.744 ! 0.53 eA-3 Q167 1.000 0.277 0.232 ! 0.53 eA-3 Q168 0.320 0.492 0.097 ! 0.53 eA-3 C169 0.397 0.493 0.736 ! 0.52 eA-3 Q170 0.484 0.388 0.339 ! 0.51 eA-3 Q171 0.343 0.265 0.187 ! 0.51 eA-3 ) ; _shelx_fab_checksum 48260