data_tcd398 _audit_creation_date 2016-01-21 _audit_creation_method ; Olex2 1.2 (compiled 2015.09.30 svn.r3233 for OlexSys, GUI svn.r5103) ; _publ_contact_author_address ? _publ_contact_author_email ? _publ_contact_author_name '' _publ_contact_author_phone ? _publ_section_references ; Bruker (2008-2014). XP, Bruker AXS Inc., Madison, WI, USA. Bruker (2013). SAINT v8.34A, Bruker AXS Inc., Madison, WI, USA. Bruker (2014/5). SADABS, Bruker AXS Inc., Madison, Wisconsin, USA. Bruker (2015). APEX3 v2015.9-0, Bruker AXS Inc., Madison, WI, USA. Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2008). Acta Cryst. A64, 112-122. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C21 H17 Cl O S' _chemical_formula_sum 'C21 H17 Cl O S' _chemical_formula_weight 352.86 _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'monoclinic' _space_group_IT_number 14 _space_group_name_H-M_alt 'P 1 21/c 1' _space_group_name_Hall '-P 2ybc' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 20.6221(9) _cell_length_b 5.5829(2) _cell_length_c 16.5354(7) _cell_angle_alpha 90 _cell_angle_beta 112.4310(10) _cell_angle_gamma 90 _cell_volume 1759.70(12) _cell_formula_units_Z 4 _cell_measurement_reflns_used 9971 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 68.31 _cell_measurement_theta_min 4.64 _shelx_estimated_absorpt_T_max 0.750 _shelx_estimated_absorpt_T_min 0.567 _exptl_absorpt_coefficient_mu 3.049 _exptl_absorpt_correction_T_max 0.7531 _exptl_absorpt_correction_T_min 0.6382 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2014/5 (Bruker,2014/5) was used for absorption correction. wR2(int) was 0.0782 before and 0.0582 after correction. The Ratio of minimum to maximum transmission is 0.8474. The \l/2 correction factor is Not present. ; _exptl_absorpt_special_details ? _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.332 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description 'block' _exptl_crystal_F_000 736 _exptl_crystal_size_max 0.21 _exptl_crystal_size_mid 0.18 _exptl_crystal_size_min 0.1 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0360 _diffrn_reflns_av_unetI/netI 0.0211 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 24 _diffrn_reflns_limit_h_min -24 _diffrn_reflns_limit_k_max 6 _diffrn_reflns_limit_k_min -6 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 26907 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 67.679 _diffrn_reflns_theta_max 68.328 _diffrn_reflns_theta_min 2.318 _diffrn_ambient_temperature 100.0 _diffrn_detector 'Bruker APEX2 area detector' _diffrn_detector_area_resol_mean 7.9 _diffrn_detector_type 'CCD area detector' _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device 'Bruker DUO kappa diffractometer' _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator 'mirror optics' _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_source 'microfocus sealed X-ray tube' _diffrn_source_type 'Incoatec I\ms' _diffrn_standards_number 0 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 3096 _reflns_number_total 3222 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'SAINT v8.34A (Bruker, 2013)' _computing_data_collection 'APEX 3 (Bruker, 2015) ' _computing_data_reduction 'SAINT v8.34A (Bruker, 2013)' _computing_molecular_graphics 'XP (Bruker, 2008-2014)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _refine_diff_density_max 0.318 _refine_diff_density_min -0.348 _refine_diff_density_rms 0.048 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.045 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 217 _refine_ls_number_reflns 3222 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0355 _refine_ls_R_factor_gt 0.0347 _refine_ls_restrained_S_all 1.045 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0539P)^2^+0.7838P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0942 _refine_ls_wR_factor_ref 0.0951 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups 2.a Ternary CH refined with riding coordinates: C8(H8), C9(H9) 2.b Aromatic/amide H refined with riding coordinates: C1(H1), C2(H2), C3(H3), C4(H4), C5(H5), C11(H11), C12(H12), C13(H13), C14(H14), C15(H15), C17(H17), C18(H18), C19(H19), C20(H20), C21(H21) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary ? _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cl1 Cl 0.68581(2) 0.58032(10) 0.32088(2) 0.04749(16) Uani 1 1 d . . . . . S1 S 0.82907(2) 0.39511(8) 0.46754(2) 0.03301(13) Uani 1 1 d . . . . . O1 O 0.65724(6) 0.89860(19) 0.47617(8) 0.0365(3) Uani 1 1 d . . . . . C1 C 0.51632(8) 0.7689(3) 0.42564(10) 0.0300(3) Uani 1 1 d . . . . . H1 H 0.5314 0.9141 0.4573 0.036 Uiso 1 1 calc R . . . . C2 C 0.44638(8) 0.7051(3) 0.39553(12) 0.0369(4) Uani 1 1 d . . . . . H2 H 0.4136 0.8049 0.4071 0.044 Uiso 1 1 calc R . . . . C3 C 0.42405(8) 0.4948(3) 0.34831(12) 0.0373(4) Uani 1 1 d . . . . . H3 H 0.3759 0.4510 0.3272 0.045 Uiso 1 1 calc R . . . . C4 C 0.47189(8) 0.3488(3) 0.33196(11) 0.0350(4) Uani 1 1 d . . . . . H4 H 0.4564 0.2057 0.2991 0.042 Uiso 1 1 calc R . . . . C5 C 0.54230(8) 0.4100(3) 0.36317(10) 0.0288(3) Uani 1 1 d . . . . . H5 H 0.5750 0.3076 0.3526 0.035 Uiso 1 1 calc R . . . . C6 C 0.56515(7) 0.6221(2) 0.41005(9) 0.0237(3) Uani 1 1 d . . . . . C7 C 0.63942(7) 0.7029(3) 0.44324(9) 0.0245(3) Uani 1 1 d . . . . . C8 C 0.69447(7) 0.5346(3) 0.43237(9) 0.0262(3) Uani 1 1 d . . . . . H8 H 0.6826 0.3648 0.4404 0.031 Uiso 1 1 calc R . . . . C9 C 0.76883(7) 0.5910(3) 0.49622(10) 0.0250(3) Uani 1 1 d . . . . . H9 H 0.7798 0.7621 0.4889 0.030 Uiso 1 1 calc R . . . . C10 C 0.77557(7) 0.5513(2) 0.58945(9) 0.0224(3) Uani 1 1 d . . . . . C11 C 0.75213(8) 0.3409(3) 0.61442(10) 0.0294(3) Uani 1 1 d . . . . . H11 H 0.7318 0.2184 0.5725 0.035 Uiso 1 1 calc R . . . . C12 C 0.75821(8) 0.3093(3) 0.70007(11) 0.0351(4) Uani 1 1 d . . . . . H12 H 0.7418 0.1655 0.7164 0.042 Uiso 1 1 calc R . . . . C13 C 0.78806(8) 0.4854(3) 0.76210(10) 0.0338(4) Uani 1 1 d . . . . . H13 H 0.7917 0.4634 0.8207 0.041 Uiso 1 1 calc R . . . . C14 C 0.81248(8) 0.6934(3) 0.73827(10) 0.0317(3) Uani 1 1 d . . . . . H14 H 0.8335 0.8142 0.7807 0.038 Uiso 1 1 calc R . . . . C15 C 0.80640(7) 0.7261(3) 0.65226(10) 0.0266(3) Uani 1 1 d . . . . . H15 H 0.8235 0.8693 0.6363 0.032 Uiso 1 1 calc R . . . . C16 C 0.91088(7) 0.4925(3) 0.54659(9) 0.0253(3) Uani 1 1 d . . . . . C17 C 0.94577(8) 0.3531(3) 0.61912(10) 0.0303(3) Uani 1 1 d . . . . . H17 H 0.9249 0.2098 0.6287 0.036 Uiso 1 1 calc R . . . . C18 C 1.01151(8) 0.4229(3) 0.67811(11) 0.0344(4) Uani 1 1 d . . . . . H18 H 1.0359 0.3258 0.7276 0.041 Uiso 1 1 calc R . . . . C19 C 1.04146(8) 0.6327(3) 0.66505(11) 0.0318(3) Uani 1 1 d . . . . . H19 H 1.0864 0.6802 0.7055 0.038 Uiso 1 1 calc R . . . . C20 C 1.00600(8) 0.7735(3) 0.59301(12) 0.0358(4) Uani 1 1 d . . . . . H20 H 1.0264 0.9189 0.5843 0.043 Uiso 1 1 calc R . . . . C21 C 0.94078(8) 0.7036(3) 0.53329(11) 0.0348(4) Uani 1 1 d . . . . . H21 H 0.9167 0.8000 0.4835 0.042 Uiso 1 1 calc R . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cl1 0.0262(2) 0.0922(4) 0.0234(2) 0.00132(19) 0.00877(16) 0.01055(19) S1 0.0187(2) 0.0474(3) 0.0310(2) -0.01397(16) 0.00729(15) 0.00315(14) O1 0.0238(5) 0.0286(6) 0.0512(7) -0.0098(5) 0.0075(5) -0.0005(4) C1 0.0249(7) 0.0302(7) 0.0340(8) -0.0066(6) 0.0104(6) 0.0003(6) C2 0.0234(7) 0.0407(9) 0.0470(9) -0.0079(7) 0.0142(7) 0.0032(6) C3 0.0206(7) 0.0412(9) 0.0457(9) -0.0038(7) 0.0077(7) -0.0032(6) C4 0.0273(8) 0.0322(8) 0.0383(8) -0.0072(7) 0.0044(6) -0.0029(6) C5 0.0234(7) 0.0303(8) 0.0294(7) -0.0046(6) 0.0063(6) 0.0024(6) C6 0.0221(7) 0.0258(7) 0.0222(7) 0.0001(5) 0.0074(5) 0.0016(5) C7 0.0213(7) 0.0261(7) 0.0242(7) -0.0005(5) 0.0065(5) 0.0011(5) C8 0.0216(7) 0.0341(8) 0.0225(7) -0.0032(6) 0.0079(6) 0.0018(6) C9 0.0192(7) 0.0291(7) 0.0269(7) -0.0030(6) 0.0091(6) 0.0018(5) C10 0.0151(6) 0.0244(7) 0.0268(7) -0.0014(5) 0.0071(5) 0.0030(5) C11 0.0259(7) 0.0247(7) 0.0356(8) -0.0017(6) 0.0095(6) -0.0001(6) C12 0.0332(8) 0.0304(8) 0.0450(9) 0.0107(7) 0.0185(7) 0.0051(6) C13 0.0314(8) 0.0430(9) 0.0282(7) 0.0086(7) 0.0128(6) 0.0125(7) C14 0.0281(7) 0.0373(8) 0.0267(7) -0.0060(6) 0.0072(6) 0.0015(6) C15 0.0229(7) 0.0259(7) 0.0303(7) -0.0033(6) 0.0094(6) -0.0017(5) C16 0.0189(6) 0.0329(7) 0.0265(7) -0.0049(6) 0.0112(5) 0.0024(6) C17 0.0252(7) 0.0293(7) 0.0372(8) 0.0022(6) 0.0130(6) -0.0011(6) C18 0.0251(8) 0.0414(9) 0.0328(8) 0.0071(7) 0.0068(6) 0.0010(6) C19 0.0222(7) 0.0391(8) 0.0343(8) -0.0070(7) 0.0108(6) -0.0037(6) C20 0.0288(8) 0.0325(8) 0.0486(9) 0.0039(7) 0.0176(7) -0.0039(6) C21 0.0286(8) 0.0402(9) 0.0363(8) 0.0112(7) 0.0132(6) 0.0050(7) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cl1 C8 1.8012(14) . ? S1 C9 1.8477(14) . ? S1 C16 1.7798(15) . ? O1 C7 1.2133(18) . ? C1 H1 0.9500 . ? C1 C2 1.381(2) . ? C1 C6 1.396(2) . ? C2 H2 0.9500 . ? C2 C3 1.388(2) . ? C3 H3 0.9500 . ? C3 C4 1.384(2) . ? C4 H4 0.9500 . ? C4 C5 1.386(2) . ? C5 H5 0.9500 . ? C5 C6 1.395(2) . ? C6 C7 1.4863(19) . ? C7 C8 1.5364(19) . ? C8 H8 1.0000 . ? C8 C9 1.5263(19) . ? C9 H9 1.0000 . ? C9 C10 1.510(2) . ? C10 C11 1.391(2) . ? C10 C15 1.390(2) . ? C11 H11 0.9500 . ? C11 C12 1.385(2) . ? C12 H12 0.9500 . ? C12 C13 1.384(2) . ? C13 H13 0.9500 . ? C13 C14 1.381(2) . ? C14 H14 0.9500 . ? C14 C15 1.391(2) . ? C15 H15 0.9500 . ? C16 C17 1.379(2) . ? C16 C21 1.386(2) . ? C17 H17 0.9500 . ? C17 C18 1.390(2) . ? C18 H18 0.9500 . ? C18 C19 1.379(2) . ? C19 H19 0.9500 . ? C19 C20 1.381(2) . ? C20 H20 0.9500 . ? C20 C21 1.387(2) . ? C21 H21 0.9500 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C16 S1 C9 99.93(7) . . ? C2 C1 H1 119.7 . . ? C2 C1 C6 120.62(14) . . ? C6 C1 H1 119.7 . . ? C1 C2 H2 120.1 . . ? C1 C2 C3 119.87(15) . . ? C3 C2 H2 120.1 . . ? C2 C3 H3 120.0 . . ? C4 C3 C2 120.00(14) . . ? C4 C3 H3 120.0 . . ? C3 C4 H4 119.8 . . ? C3 C4 C5 120.39(15) . . ? C5 C4 H4 119.8 . . ? C4 C5 H5 120.0 . . ? C4 C5 C6 120.01(14) . . ? C6 C5 H5 120.0 . . ? C1 C6 C7 117.89(13) . . ? C5 C6 C1 119.09(13) . . ? C5 C6 C7 123.01(13) . . ? O1 C7 C6 122.15(13) . . ? O1 C7 C8 119.50(13) . . ? C6 C7 C8 118.33(12) . . ? Cl1 C8 H8 109.6 . . ? C7 C8 Cl1 104.12(10) . . ? C7 C8 H8 109.6 . . ? C9 C8 Cl1 111.09(10) . . ? C9 C8 C7 112.65(12) . . ? C9 C8 H8 109.6 . . ? S1 C9 H9 109.1 . . ? C8 C9 S1 107.26(10) . . ? C8 C9 H9 109.1 . . ? C10 C9 S1 111.47(10) . . ? C10 C9 C8 110.65(11) . . ? C10 C9 H9 109.1 . . ? C11 C10 C9 121.32(13) . . ? C15 C10 C9 119.82(13) . . ? C15 C10 C11 118.86(13) . . ? C10 C11 H11 119.8 . . ? C12 C11 C10 120.34(14) . . ? C12 C11 H11 119.8 . . ? C11 C12 H12 119.7 . . ? C13 C12 C11 120.58(15) . . ? C13 C12 H12 119.7 . . ? C12 C13 H13 120.2 . . ? C14 C13 C12 119.53(14) . . ? C14 C13 H13 120.2 . . ? C13 C14 H14 119.9 . . ? C13 C14 C15 120.11(14) . . ? C15 C14 H14 119.9 . . ? C10 C15 C14 120.57(14) . . ? C10 C15 H15 119.7 . . ? C14 C15 H15 119.7 . . ? C17 C16 S1 120.01(12) . . ? C17 C16 C21 120.10(14) . . ? C21 C16 S1 119.84(12) . . ? C16 C17 H17 120.1 . . ? C16 C17 C18 119.84(14) . . ? C18 C17 H17 120.1 . . ? C17 C18 H18 119.9 . . ? C19 C18 C17 120.22(15) . . ? C19 C18 H18 119.9 . . ? C18 C19 H19 120.1 . . ? C18 C19 C20 119.81(15) . . ? C20 C19 H19 120.1 . . ? C19 C20 H20 119.8 . . ? C19 C20 C21 120.31(15) . . ? C21 C20 H20 119.8 . . ? C16 C21 C20 119.71(15) . . ? C16 C21 H21 120.1 . . ? C20 C21 H21 120.1 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Cl1 C8 C9 S1 -58.02(12) . . . . ? Cl1 C8 C9 C10 -179.80(10) . . . . ? S1 C9 C10 C11 -70.16(15) . . . . ? S1 C9 C10 C15 109.16(13) . . . . ? S1 C16 C17 C18 176.31(12) . . . . ? S1 C16 C21 C20 -177.10(12) . . . . ? O1 C7 C8 Cl1 -97.24(14) . . . . ? O1 C7 C8 C9 23.23(19) . . . . ? C1 C2 C3 C4 0.4(3) . . . . ? C1 C6 C7 O1 -6.4(2) . . . . ? C1 C6 C7 C8 175.63(13) . . . . ? C2 C1 C6 C5 0.3(2) . . . . ? C2 C1 C6 C7 179.21(15) . . . . ? C2 C3 C4 C5 0.6(3) . . . . ? C3 C4 C5 C6 -1.2(3) . . . . ? C4 C5 C6 C1 0.7(2) . . . . ? C4 C5 C6 C7 -178.14(14) . . . . ? C5 C6 C7 O1 172.48(15) . . . . ? C5 C6 C7 C8 -5.5(2) . . . . ? C6 C1 C2 C3 -0.9(3) . . . . ? C6 C7 C8 Cl1 80.80(14) . . . . ? C6 C7 C8 C9 -158.73(13) . . . . ? C7 C8 C9 S1 -174.40(10) . . . . ? C7 C8 C9 C10 63.82(16) . . . . ? C8 C9 C10 C11 49.12(17) . . . . ? C8 C9 C10 C15 -131.57(13) . . . . ? C9 S1 C16 C17 103.78(12) . . . . ? C9 S1 C16 C21 -78.87(13) . . . . ? C9 C10 C11 C12 -179.36(13) . . . . ? C9 C10 C15 C14 179.44(13) . . . . ? C10 C11 C12 C13 -0.4(2) . . . . ? C11 C10 C15 C14 -1.2(2) . . . . ? C11 C12 C13 C14 -0.6(2) . . . . ? C12 C13 C14 C15 0.6(2) . . . . ? C13 C14 C15 C10 0.3(2) . . . . ? C15 C10 C11 C12 1.3(2) . . . . ? C16 S1 C9 C8 178.86(10) . . . . ? C16 S1 C9 C10 -59.87(11) . . . . ? C16 C17 C18 C19 1.0(2) . . . . ? C17 C16 C21 C20 0.3(2) . . . . ? C17 C18 C19 C20 -0.1(2) . . . . ? C18 C19 C20 C21 -0.7(2) . . . . ? C19 C20 C21 C16 0.6(2) . . . . ? C21 C16 C17 C18 -1.0(2) . . . . ? _shelx_res_file ; tcd398.res created by SHELXL-2014/7 TITL TCD398_a.res in P2(1)/c CELL 1.54178 20.6221 5.5829 16.5354 90 112.431 90 ZERR 4 0.0009 0.0002 0.0007 0 0.001 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H Cl O S UNIT 84 68 4 4 4 L.S. 10 PLAN -4 0 0 SIZE 0.21 0.18 0.1 TEMP -173.15 BOND $H CONF MORE -1 fmap 2 acta HTAB 2.0 REM REM REM WGHT 0.053900 0.783800 FVAR 0.51433 CL1 3 0.685814 0.580317 0.320879 11.00000 0.02625 0.09218 = 0.02342 0.00132 0.00877 0.01055 S1 5 0.829067 0.395112 0.467535 11.00000 0.01870 0.04742 = 0.03096 -0.01397 0.00729 0.00315 O1 4 0.657242 0.898599 0.476170 11.00000 0.02378 0.02858 = 0.05117 -0.00975 0.00751 -0.00054 C1 1 0.516322 0.768916 0.425636 11.00000 0.02490 0.03022 = 0.03405 -0.00657 0.01040 0.00028 AFIX 43 H1 2 0.531357 0.914075 0.457251 11.00000 -1.20000 AFIX 0 C2 1 0.446384 0.705063 0.395527 11.00000 0.02345 0.04074 = 0.04701 -0.00788 0.01416 0.00318 AFIX 43 H2 2 0.413628 0.804906 0.407115 11.00000 -1.20000 AFIX 0 C3 1 0.424048 0.494767 0.348311 11.00000 0.02057 0.04120 = 0.04567 -0.00384 0.00766 -0.00316 AFIX 43 H3 2 0.375910 0.451029 0.327219 11.00000 -1.20000 AFIX 0 C4 1 0.471890 0.348798 0.331956 11.00000 0.02728 0.03217 = 0.03834 -0.00721 0.00438 -0.00286 AFIX 43 H4 2 0.456371 0.205728 0.299128 11.00000 -1.20000 AFIX 0 C5 1 0.542301 0.410041 0.363170 11.00000 0.02345 0.03028 = 0.02940 -0.00462 0.00627 0.00238 AFIX 43 H5 2 0.575025 0.307585 0.352647 11.00000 -1.20000 AFIX 0 C6 1 0.565149 0.622127 0.410049 11.00000 0.02213 0.02584 = 0.02221 0.00014 0.00744 0.00161 C7 1 0.639416 0.702946 0.443238 11.00000 0.02129 0.02615 = 0.02421 -0.00050 0.00647 0.00109 C8 1 0.694475 0.534600 0.432367 11.00000 0.02159 0.03412 = 0.02248 -0.00315 0.00794 0.00175 AFIX 13 H8 2 0.682631 0.364836 0.440355 11.00000 -1.20000 AFIX 0 C9 1 0.768827 0.590993 0.496220 11.00000 0.01918 0.02908 = 0.02694 -0.00296 0.00913 0.00177 AFIX 13 H9 2 0.779848 0.762089 0.488860 11.00000 -1.20000 AFIX 0 C10 1 0.775568 0.551259 0.589446 11.00000 0.01506 0.02437 = 0.02684 -0.00137 0.00708 0.00299 C11 1 0.752131 0.340935 0.614423 11.00000 0.02588 0.02467 = 0.03560 -0.00171 0.00949 -0.00007 AFIX 43 H11 2 0.731849 0.218365 0.572498 11.00000 -1.20000 AFIX 0 C12 1 0.758212 0.309332 0.700070 11.00000 0.03316 0.03039 = 0.04502 0.01071 0.01848 0.00508 AFIX 43 H12 2 0.741754 0.165535 0.716397 11.00000 -1.20000 AFIX 0 C13 1 0.788057 0.485405 0.762104 11.00000 0.03143 0.04305 = 0.02821 0.00857 0.01284 0.01253 AFIX 43 H13 2 0.791725 0.463404 0.820662 11.00000 -1.20000 AFIX 0 C14 1 0.812477 0.693374 0.738271 11.00000 0.02806 0.03731 = 0.02672 -0.00597 0.00721 0.00154 AFIX 43 H14 2 0.833457 0.814212 0.780679 11.00000 -1.20000 AFIX 0 C15 1 0.806396 0.726140 0.652265 11.00000 0.02294 0.02591 = 0.03028 -0.00328 0.00941 -0.00169 AFIX 43 H15 2 0.823460 0.869265 0.636329 11.00000 -1.20000 AFIX 0 C16 1 0.910879 0.492487 0.546587 11.00000 0.01885 0.03289 = 0.02654 -0.00489 0.01117 0.00237 C17 1 0.945773 0.353128 0.619117 11.00000 0.02523 0.02933 = 0.03716 0.00225 0.01298 -0.00107 AFIX 43 H17 2 0.924926 0.209793 0.628721 11.00000 -1.20000 AFIX 0 C18 1 1.011508 0.422933 0.678115 11.00000 0.02512 0.04141 = 0.03278 0.00705 0.00683 0.00101 AFIX 43 H18 2 1.035883 0.325803 0.727605 11.00000 -1.20000 AFIX 0 C19 1 1.041463 0.632703 0.665049 11.00000 0.02220 0.03908 = 0.03425 -0.00700 0.01079 -0.00372 AFIX 43 H19 2 1.086365 0.680223 0.705496 11.00000 -1.20000 AFIX 0 C20 1 1.006005 0.773483 0.593009 11.00000 0.02876 0.03255 = 0.04859 0.00387 0.01756 -0.00395 AFIX 43 H20 2 1.026387 0.918897 0.584317 11.00000 -1.20000 AFIX 0 C21 1 0.940778 0.703578 0.533286 11.00000 0.02865 0.04017 = 0.03630 0.01122 0.01323 0.00495 AFIX 43 H21 2 0.916693 0.799964 0.483473 11.00000 -1.20000 AFIX 0 HKLF 4 REM TCD398_a.res in P2(1)/c REM R1 = 0.0347 for 3096 Fo > 4sig(Fo) and 0.0355 for all 3222 data REM 217 parameters refined using 0 restraints END WGHT 0.0539 0.7838 REM No hydrogen bonds found for HTAB generation REM Highest difference peak 0.318, deepest hole -0.348, 1-sigma level 0.048 Q1 1 0.6885 0.7389 0.3388 11.00000 0.05 0.32 Q2 1 0.7733 0.5550 0.5411 11.00000 0.05 0.26 Q3 1 0.6693 0.6056 0.4406 11.00000 0.05 0.23 Q4 1 0.7331 0.5722 0.4587 11.00000 0.05 0.21 ; _shelx_res_checksum 29904 _shelx_hkl_file ; 0 0 1 0.00 0.10 0 0 -1 0.10 0.10 0 0 2 1165.98 50.89 0 0 -2 1198.28 50.99 0 0 3 0.00 0.30 0 0 -3 0.30 0.30 0 0 -4 300.97 12.90 0 0 -4 273.77 12.60 0 0 -4 273.87 12.40 0 0 5 0.10 0.30 0 0 -5 0.10 0.30 0 0 -5 -0.10 0.40 0 0 -5 0.40 0.50 0 0 -6 449.66 20.80 0 0 6 444.36 20.00 0 0 -6 473.65 20.20 0 0 -6 454.35 20.00 0 0 -6 477.75 20.50 0 0 -7 0.50 0.40 0 0 -7 0.90 0.50 0 0 7 0.50 0.30 0 0 -7 0.40 0.60 0 0 7 0.50 0.30 0 0 -7 -0.10 0.40 0 0 -8 389.06 16.90 0 0 8 372.16 16.50 0 0 -8 394.76 17.30 0 0 -8 348.07 16.30 0 0 -9 -0.40 0.50 0 0 -9 -0.30 0.40 0 0 -10 62.89 4.00 0 0 10 65.69 4.40 0 0 -10 65.49 4.40 0 0 11 -0.20 0.50 0 0 -11 4.70 1.30 0 0 -11 0.30 0.50 0 0 -12 104.69 6.00 0 0 12 105.99 6.00 0 0 -12 100.39 6.30 0 0 -13 -0.20 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47.90 3.00 0 4 -10 42.60 2.60 0 -4 10 45.00 2.70 0 -4 -10 48.30 2.80 0 -4 10 47.70 2.80 0 -4 -10 45.00 2.50 0 -4 10 47.30 2.40 0 4 -11 146.19 7.10 0 4 11 149.69 7.20 0 4 -11 140.19 7.10 0 4 -11 149.29 7.40 0 4 -11 146.49 6.90 0 -4 11 148.19 6.80 0 -4 11 145.99 6.50 0 -4 -11 131.19 6.90 0 -4 -11 136.89 6.70 0 -4 11 152.38 6.90 0 4 -12 4.10 0.80 0 4 -12 5.30 1.00 0 4 -12 3.70 0.80 0 4 12 3.60 0.80 0 4 -12 3.50 0.90 0 -4 12 4.00 0.50 0 -4 -12 2.60 0.80 0 -4 12 3.30 0.60 0 -4 -12 2.80 0.70 0 -4 -12 2.50 0.50 0 -4 12 4.00 0.60 0 4 -13 38.30 2.70 0 4 13 53.09 2.90 0 4 -13 45.10 2.90 0 4 -13 52.09 2.70 0 4 -13 50.09 2.60 0 -4 13 49.40 2.70 0 -4 13 45.00 2.50 0 -4 13 51.69 2.60 0 -4 -13 44.90 2.60 0 -4 13 51.49 2.70 0 -4 -13 42.60 2.60 0 4 14 77.79 3.80 0 4 -14 71.49 3.70 0 4 14 70.39 3.50 0 4 -14 76.69 3.70 0 -4 14 82.59 3.70 0 -4 14 76.19 3.70 0 -4 14 77.39 3.60 0 -4 -14 67.29 3.60 0 -4 -14 75.79 3.70 0 5 0 -0.10 0.60 0 5 0 -0.20 0.40 0 5 0 -0.10 0.60 0 5 0 0.40 0.70 0 -5 0 0.20 0.50 0 -5 0 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1.00 -1 3 -15 10.90 1.10 -1 3 -15 11.20 1.00 1 3 15 11.50 0.90 1 3 15 9.00 1.00 -1 -3 -15 11.30 1.00 1 -3 15 10.10 0.90 1 -3 15 10.90 1.00 1 -3 15 10.50 0.90 -1 -3 -15 11.50 1.00 -1 3 -16 83.69 4.00 -1 3 -16 80.29 3.90 -1 -3 -16 82.39 4.00 1 -3 16 86.19 3.90 -1 4 15 20.40 1.30 -1 4 15 19.40 1.30 1 4 -15 20.20 1.20 -1 -4 15 21.00 1.20 -1 -4 15 17.10 1.10 1 4 -14 37.00 2.10 -1 4 14 40.20 2.30 1 4 -14 36.10 2.20 -1 4 14 31.40 1.90 1 -4 -14 37.70 2.10 -1 -4 14 36.40 2.10 -1 -4 14 43.10 2.10 1 -4 -14 36.10 2.10 -1 -4 14 38.90 2.00 1 4 -13 4.90 0.90 1 4 -13 4.20 0.80 1 4 -13 8.40 1.00 -1 4 13 5.40 0.90 1 4 -13 5.60 0.80 -1 -4 13 7.20 0.80 1 -4 -13 3.40 0.60 -1 -4 13 5.90 0.80 1 -4 -13 4.60 0.70 -1 -4 13 5.10 0.80 1 4 -12 39.40 2.80 1 4 -12 37.80 2.40 1 4 -12 37.80 2.50 1 4 -12 39.00 2.30 1 4 -12 40.20 2.50 -1 4 12 42.00 2.60 1 -4 -12 42.20 2.50 -1 -4 12 40.80 2.50 -1 -4 12 37.70 2.00 1 -4 -12 39.30 2.20 -1 -4 12 40.50 2.40 -1 -4 12 40.50 2.30 1 4 -11 230.68 10.50 1 4 -11 221.38 10.80 1 4 -11 204.08 10.40 1 4 -11 220.08 10.20 -1 4 11 232.58 10.60 1 4 -11 225.48 10.40 1 -4 -11 222.28 10.10 -1 -4 11 228.08 10.30 -1 -4 11 222.58 9.90 1 -4 -11 230.78 10.40 -1 -4 11 226.48 10.20 1 4 -10 3.10 1.00 1 4 -10 3.50 0.90 1 4 -10 1.90 0.80 -1 4 10 3.10 0.80 1 4 -10 1.70 1.00 1 4 -10 3.00 0.70 1 4 -10 2.40 0.70 -1 -4 10 2.70 0.70 -1 -4 10 2.60 0.70 -1 -4 10 2.10 0.50 1 -4 -10 2.60 0.80 1 -4 -10 2.40 0.50 -1 4 9 0.40 0.60 -1 4 9 0.90 0.70 1 4 -9 0.70 0.50 1 4 -9 0.00 0.60 1 4 -9 0.60 0.60 -1 4 9 0.80 0.60 1 4 -9 0.50 0.90 -1 -4 9 0.40 0.40 1 -4 -9 1.60 0.60 1 -4 -9 0.10 0.90 1 -4 -9 0.90 0.40 -1 -4 9 0.70 0.60 -1 -4 9 -0.10 0.60 -1 4 8 192.18 10.20 1 4 -8 220.18 10.00 -1 4 8 212.58 10.30 -1 4 8 215.58 10.20 1 4 -8 215.18 10.20 1 4 -8 221.28 10.60 1 4 -8 199.28 9.90 -1 -4 8 224.98 9.60 1 -4 -8 219.48 9.80 1 -4 -8 234.58 10.20 1 -4 -8 238.48 11.10 -1 -4 8 204.78 9.90 -1 -4 8 221.08 9.90 1 4 -7 10.40 1.20 1 4 -7 10.30 1.30 -1 4 7 11.50 1.40 1 4 -7 14.10 1.90 -1 4 7 11.10 1.30 1 4 -7 11.80 1.30 1 -4 -7 9.20 1.20 -1 -4 7 10.70 1.20 1 -4 -7 12.90 2.10 -1 -4 7 10.60 0.90 1 -4 -7 11.80 1.10 -1 -4 7 10.40 1.20 1 4 -6 132.09 7.50 1 -4 -6 144.59 7.80 1 -4 -6 146.79 7.80 1 4 -5 3.10 1.10 1 -4 -5 3.20 1.30 1 -4 -5 1.50 1.00 1 4 -4 1.90 0.80 -1 4 4 3.30 0.90 1 4 -4 5.20 1.10 1 -4 -4 3.40 1.00 1 4 -3 164.68 7.90 -1 4 3 157.28 7.90 1 -4 -3 158.38 8.40 1 4 -2 80.99 4.50 -1 4 2 81.99 4.50 1 -4 -2 76.99 4.80 -1 4 1 -0.10 0.30 1 4 -1 -0.20 0.30 -1 -4 1 -0.40 0.60 1 -4 -1 -0.40 0.30 1 4 0 0.10 0.50 -1 4 0 -0.20 0.30 1 -4 0 0.20 0.60 -1 -4 0 0.10 0.60 1 -4 0 0.60 0.40 -1 4 -1 25.10 1.90 1 4 1 22.80 1.80 1 -4 1 19.50 2.40 1 -4 1 19.10 1.60 -1 -4 -1 20.70 2.20 1 4 2 91.29 4.80 -1 4 -2 81.99 4.70 1 -4 2 83.19 4.40 -1 -4 -2 84.59 5.10 -1 -4 -2 86.49 5.10 -1 4 -3 152.98 7.70 1 4 3 160.18 7.80 -1 -4 -3 157.98 8.30 1 -4 3 149.29 7.50 -1 -4 -3 163.38 8.40 1 4 4 14.60 1.70 -1 -4 -4 19.90 2.50 -1 -4 -4 16.20 2.10 1 -4 4 15.40 1.60 1 4 5 0.00 0.60 -1 4 -5 0.00 0.50 1 -4 5 0.30 0.50 -1 -4 -5 0.00 0.60 -1 -4 -5 1.00 0.60 -1 4 -6 44.70 3.20 1 4 6 36.00 2.70 1 4 6 38.60 2.60 -1 4 -6 40.90 3.00 -1 4 -6 39.20 3.20 -1 4 -6 51.09 2.90 1 -4 6 39.60 2.40 1 -4 6 41.10 2.70 -1 -4 -6 42.00 2.60 -1 -4 -6 47.30 3.40 -1 -4 -6 47.70 3.50 -1 -4 -6 43.90 2.40 -1 4 -7 0.60 0.70 1 4 7 0.20 0.60 -1 4 -7 0.50 0.80 -1 4 -7 1.90 1.00 -1 4 -7 0.90 1.00 -1 4 -7 0.20 0.50 -1 4 -7 0.70 0.70 1 4 7 0.60 0.50 -1 -4 -7 -0.40 0.70 1 -4 7 0.30 0.50 1 -4 7 0.10 0.40 -1 -4 -7 0.50 0.40 -1 -4 -7 0.30 0.70 -1 4 -8 185.88 8.90 -1 4 -8 181.88 8.50 1 4 8 184.58 8.70 -1 4 -8 187.48 9.10 -1 4 -8 151.18 8.20 -1 4 -8 181.48 8.70 -1 4 -8 176.88 8.70 1 4 8 176.98 8.60 1 -4 8 184.48 8.10 1 -4 8 172.78 8.40 -1 -4 -8 186.28 9.00 1 -4 8 176.68 8.30 -1 -4 -8 179.68 8.20 -1 -4 -8 188.58 8.60 -1 4 -9 107.49 5.20 -1 4 -9 98.59 5.40 -1 4 -9 105.39 5.70 -1 4 -9 96.99 5.30 1 4 9 102.09 5.30 -1 4 -9 98.59 5.20 1 -4 9 101.29 5.00 -1 -4 -9 92.79 5.20 -1 -4 -9 93.59 4.80 1 -4 9 101.89 4.70 1 -4 9 97.99 5.00 -1 -4 -9 106.09 5.20 -1 4 -10 27.20 2.50 1 4 10 29.60 2.20 -1 4 -10 29.70 2.20 -1 4 -10 28.00 2.30 -1 4 -10 27.90 2.00 -1 -4 -10 25.30 1.70 1 -4 10 28.10 1.60 1 -4 10 28.30 1.90 1 -4 10 29.20 2.00 -1 -4 -10 27.60 2.10 -1 4 -11 240.08 11.40 1 4 11 247.68 11.20 -1 4 -11 237.18 11.10 -1 4 -11 238.98 11.00 -1 4 -11 243.58 11.20 1 -4 11 241.48 10.50 1 -4 11 233.98 10.80 1 -4 11 235.38 10.90 -1 -4 -11 221.68 11.00 -1 -4 -11 252.67 11.10 -1 4 -12 69.39 4.00 1 4 12 73.99 3.90 -1 4 -12 74.09 3.80 -1 4 -12 67.99 3.80 -1 4 -12 73.09 3.90 -1 -4 -12 76.39 3.80 1 -4 12 71.99 3.60 1 -4 12 74.29 3.70 -1 -4 -12 67.49 3.70 1 -4 12 72.79 3.40 -1 4 -13 0.20 0.40 -1 4 -13 0.10 0.50 1 4 13 0.60 0.40 1 4 13 0.00 0.40 -1 4 -13 0.20 0.40 -1 4 -13 0.10 0.60 1 -4 13 0.40 0.30 1 -4 13 0.10 0.30 1 -4 13 0.30 0.40 -1 -4 -13 0.20 0.40 1 -4 13 0.60 0.30 -1 -4 -13 0.50 0.60 -1 4 -14 22.50 1.40 1 4 14 21.10 1.40 -1 4 -14 22.00 1.50 -1 -4 -14 20.30 1.40 1 -4 14 21.40 1.30 1 -4 14 23.20 1.40 -1 -4 -14 21.10 1.30 -1 5 12 0.20 0.30 1 5 -12 0.00 0.30 -1 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0.50 1 -5 -6 1.40 0.70 1 -5 -6 0.80 0.40 -1 -5 6 1.20 0.80 -1 -5 6 0.50 0.50 1 5 -5 6.80 1.20 1 5 -5 8.20 1.50 1 5 -5 8.70 1.10 -1 5 5 7.00 1.00 -1 5 5 10.30 1.40 1 5 -5 7.90 1.10 -1 -5 5 9.20 1.00 1 -5 -5 7.20 1.80 1 -5 -5 10.30 1.10 -1 -5 5 8.70 1.20 1 -5 -5 11.30 1.40 1 5 -4 3.20 0.90 -1 5 4 2.80 0.90 1 5 -4 3.00 0.80 -1 5 4 3.20 0.70 1 5 -4 3.60 0.80 1 5 -4 2.50 1.10 1 -5 -4 3.50 0.80 -1 -5 4 5.40 1.10 1 -5 -4 3.30 0.70 -1 -5 4 3.20 0.60 1 -5 -4 3.40 0.90 -1 -5 4 3.10 0.90 1 -5 -4 2.20 1.30 1 5 -3 1.80 0.80 -1 5 3 0.80 0.50 -1 5 3 0.40 0.70 1 5 -3 0.50 0.60 1 5 -3 0.80 0.70 1 5 -3 1.10 0.90 1 -5 -3 0.90 0.80 1 -5 -3 0.30 0.60 1 -5 -3 0.80 0.40 -1 -5 3 0.50 0.60 -1 -5 3 0.50 0.40 -1 -5 3 1.90 1.10 -1 5 2 54.19 3.10 1 5 -2 55.09 3.20 1 5 -2 52.89 3.50 -1 5 2 59.99 3.60 1 5 -2 60.39 3.30 -1 5 2 58.39 3.20 1 -5 -2 57.79 3.30 -1 -5 2 58.59 3.50 1 -5 -2 56.89 3.00 1 -5 -2 55.99 3.40 -1 -5 2 57.79 3.10 -1 -5 2 53.39 3.20 -1 5 1 271.67 12.40 1 5 -1 270.27 12.10 -1 5 1 261.67 12.00 -1 5 1 256.27 11.90 1 5 -1 248.68 12.20 1 5 -1 269.57 12.00 -1 -5 1 268.67 11.90 1 -5 -1 256.77 12.10 -1 -5 1 269.07 12.30 1 -5 -1 267.87 11.90 1 5 0 149.09 7.00 -1 5 0 147.39 7.00 1 5 0 148.99 7.30 -1 5 0 144.29 6.90 -1 5 0 138.19 7.30 1 5 0 153.58 7.00 -1 5 0 133.69 7.20 1 -5 0 152.68 7.30 1 -5 0 148.19 6.90 -1 -5 0 138.69 7.90 -1 -5 0 147.89 6.90 -1 -5 0 150.68 7.30 -1 5 -1 60.59 3.80 1 5 1 65.79 3.80 1 5 1 65.19 3.50 -1 5 -1 64.29 3.60 1 5 1 63.89 3.50 -1 5 -1 57.09 3.30 -1 -5 -1 64.29 3.40 1 -5 1 66.39 3.70 -1 -5 -1 70.49 4.60 1 -5 1 66.49 3.40 -1 -5 -1 65.99 3.60 -1 -5 -1 64.19 3.70 -1 5 -2 5.90 1.30 -1 5 -2 4.90 1.00 -1 5 -2 4.30 0.80 1 5 2 4.70 0.90 1 5 2 4.90 1.10 1 5 2 4.70 0.80 -1 -5 -2 4.50 1.00 -1 -5 -2 5.70 0.90 1 -5 2 7.60 1.20 -1 -5 -2 4.50 1.00 1 -5 2 5.50 0.80 -1 -5 -2 4.00 1.30 1 5 3 5.50 1.10 1 5 3 6.90 1.00 -1 5 -3 8.50 1.40 -1 5 -3 6.00 1.00 -1 5 -3 6.90 0.90 -1 5 -3 5.20 1.20 1 5 3 6.00 1.00 -1 -5 -3 5.70 1.50 -1 -5 -3 8.30 1.20 1 -5 3 5.80 1.00 -1 -5 -3 7.60 0.90 1 -5 3 5.70 0.80 -1 -5 -3 6.40 1.10 -1 5 -4 48.70 2.80 -1 5 -4 54.29 3.40 1 5 4 51.19 2.90 1 5 4 56.99 3.40 -1 5 -4 51.89 3.10 -1 5 -4 51.69 3.60 1 -5 4 52.89 2.90 1 -5 4 52.79 3.10 -1 -5 -4 56.49 3.20 -1 -5 -4 55.39 2.90 -1 -5 -4 50.99 3.10 -1 -5 -4 52.59 3.90 -1 5 -5 1.30 0.70 -1 5 -5 1.60 1.10 -1 5 -5 0.80 0.70 1 5 5 1.70 0.70 -1 -5 -5 1.30 0.50 -1 -5 -5 1.50 0.60 1 -5 5 0.90 0.50 -1 -5 -5 1.80 0.70 1 -5 5 1.60 0.80 -1 5 -6 12.60 1.70 1 5 6 8.80 1.30 -1 5 -6 6.90 1.00 -1 5 -6 12.00 1.70 1 -5 6 8.20 1.10 1 -5 6 9.70 1.00 -1 -5 -6 10.00 1.10 -1 -5 -6 9.00 1.20 -1 -5 -6 7.70 1.00 1 5 7 9.00 1.20 -1 5 -7 11.40 1.40 -1 5 -7 7.30 1.10 -1 5 -7 9.90 1.50 1 5 7 9.30 1.30 -1 -5 -7 10.10 1.00 1 -5 7 10.20 1.30 1 -5 7 10.70 1.10 -1 -5 -7 10.80 1.20 -1 5 -8 1.70 0.60 -1 5 -8 1.70 0.90 1 5 8 0.70 0.50 -1 5 -8 1.50 0.80 1 5 8 2.00 0.60 -1 -5 -8 1.50 0.50 1 -5 8 1.70 0.50 1 -5 8 1.30 0.70 -1 -5 -8 0.70 0.70 -1 5 -9 31.90 2.00 -1 5 -9 32.70 2.40 1 5 9 31.80 2.10 1 5 9 31.70 2.10 -1 5 -9 30.20 2.10 -1 -5 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3 492.05 19.80 2 -2 3 476.85 19.60 -2 -2 -3 486.85 20.00 -2 -2 -3 431.96 20.00 -2 -2 -3 443.66 20.00 -2 2 -4 3.10 0.70 2 2 4 4.80 1.00 -2 2 -4 4.20 0.70 2 2 4 3.50 0.70 -2 -2 -4 3.20 0.80 2 -2 4 3.90 0.50 -2 -2 -4 2.20 0.70 -2 2 -5 365.06 16.30 2 2 5 361.16 16.10 -2 2 -5 355.96 16.20 2 2 5 356.16 16.50 -2 -2 -5 369.76 16.60 -2 -2 -5 346.87 16.20 -2 -2 -5 358.26 16.20 2 -2 5 376.76 15.80 2 2 6 252.97 12.00 -2 2 -6 269.77 12.30 -2 2 -6 271.47 12.30 2 2 6 256.77 12.40 -2 -2 -6 269.77 12.60 -2 -2 -6 244.08 12.00 2 -2 6 279.37 11.70 -2 -2 -6 262.57 12.10 2 2 7 43.70 3.20 -2 2 -7 41.40 2.80 2 2 7 43.40 2.70 2 -2 7 43.40 2.50 -2 -2 -7 40.90 2.60 -2 -2 -7 44.10 3.30 -2 2 -8 0.30 0.60 2 2 8 0.00 0.50 2 2 8 -0.30 0.90 -2 -2 -8 0.40 0.50 -2 -2 -8 0.10 0.50 2 -2 8 -0.10 0.40 -2 2 -9 342.67 16.30 2 2 9 350.26 16.40 2 -2 9 340.07 15.60 -2 -2 -9 347.37 16.80 2 2 10 167.38 8.50 -2 2 -10 159.78 8.40 -2 -2 -10 150.98 8.80 2 -2 10 148.19 7.60 2 2 11 9.40 1.10 -2 2 -11 11.20 1.30 2 2 11 9.50 1.30 2 2 11 8.90 1.70 -2 2 -11 9.40 1.30 -2 2 -11 8.80 1.40 -2 2 -11 8.20 1.00 2 2 11 11.30 1.20 -2 2 -11 11.50 1.40 -2 2 -11 10.10 1.30 2 -2 11 10.90 1.30 -2 -2 -11 9.90 1.30 -2 -2 -11 9.30 1.10 2 -2 11 9.70 0.80 2 2 12 1.10 0.50 2 2 12 0.10 0.90 -2 2 -12 0.30 0.50 2 2 12 0.60 0.80 -2 2 -12 0.90 0.70 -2 2 -12 0.80 0.50 -2 2 -12 1.00 0.60 -2 2 -12 0.50 0.60 -2 2 -12 0.30 0.90 2 2 12 0.50 0.50 2 -2 12 1.10 0.30 -2 -2 -12 1.20 0.60 2 -2 12 0.40 0.50 -2 -2 -12 1.60 0.70 -2 -2 -12 0.80 0.50 -2 2 -13 105.99 5.50 -2 2 -13 107.39 5.40 2 2 13 103.79 5.60 -2 2 -13 115.19 5.60 -2 2 -13 109.39 6.00 -2 2 -13 118.89 5.80 2 2 13 114.69 5.60 -2 2 -13 115.09 6.00 -2 -2 -13 111.99 5.60 2 -2 13 114.29 5.20 2 -2 13 113.79 5.60 -2 -2 -13 120.79 5.70 2 2 14 6.00 0.90 -2 2 -14 5.70 0.90 2 2 14 4.60 0.80 -2 2 -14 8.40 1.20 -2 2 -14 5.90 1.00 -2 2 -14 5.80 1.10 2 -2 14 5.10 0.50 -2 -2 -14 5.80 0.90 2 -2 14 4.40 0.90 -2 -2 -14 3.80 0.80 2 2 15 124.99 5.90 -2 2 -15 119.29 6.20 -2 2 -15 132.59 6.00 2 2 15 117.99 6.00 -2 2 -15 129.59 6.20 -2 -2 -15 127.79 6.00 -2 -2 -15 118.09 5.90 2 -2 15 116.19 5.50 2 -2 15 135.59 6.10 2 -2 15 125.89 5.90 2 2 16 0.40 0.30 -2 2 -16 0.00 0.40 2 2 16 0.50 0.40 -2 2 -16 0.20 0.30 -2 2 -16 0.40 0.40 -2 -2 -16 0.00 0.30 2 -2 16 0.00 0.40 2 -2 16 0.20 0.30 -2 -2 -16 0.20 0.40 -2 3 17 0.10 0.40 -2 3 17 0.10 0.20 2 3 -17 0.00 0.30 2 3 -17 -0.10 0.30 2 -3 -17 0.20 0.50 -2 -3 17 0.10 0.20 -2 -3 17 0.10 0.20 2 3 -16 27.80 1.70 2 3 -16 32.30 2.00 2 3 -16 35.90 2.00 -2 3 16 32.20 2.00 -2 3 16 36.60 1.90 2 -3 -16 31.60 1.90 -2 -3 16 35.20 1.90 -2 -3 16 36.00 2.00 -2 -3 16 34.60 2.00 2 3 -15 0.40 0.50 2 3 -15 0.30 0.40 2 3 -15 0.40 0.50 -2 3 15 0.90 0.60 -2 3 15 0.60 0.40 -2 3 15 0.20 0.50 2 3 -15 0.40 0.40 -2 -3 15 0.70 0.40 2 -3 -15 0.60 0.50 -2 -3 15 0.50 0.50 -2 -3 15 0.80 0.60 -2 3 14 178.48 8.20 2 3 -14 181.48 8.30 -2 3 14 180.08 8.50 2 3 -14 179.08 8.50 2 3 -14 180.58 8.20 2 3 -14 182.88 8.40 -2 -3 14 181.08 8.20 -2 -3 14 169.08 8.20 2 -3 -14 159.18 8.30 -2 3 13 27.30 2.10 2 3 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17.30 2 3 -5 1.90 0.80 2 3 -5 3.20 0.60 2 -3 -5 3.50 0.90 2 3 -4 580.74 25.00 2 3 -4 577.64 24.70 -2 3 4 557.94 24.60 2 -3 -4 499.15 24.40 2 -3 -4 589.94 25.20 -2 -3 4 567.34 24.70 2 3 -3 1.40 0.60 2 3 -3 0.30 0.30 -2 3 3 -0.10 0.30 2 -3 -3 1.50 0.70 -2 -3 3 0.20 0.40 2 -3 -3 0.10 0.40 -2 3 2 15.40 1.40 2 3 -2 16.10 1.50 2 3 -2 16.30 1.30 -2 -3 2 16.10 1.40 2 -3 -2 16.20 1.20 2 -3 -2 13.50 1.60 2 3 -1 -0.20 0.30 -2 3 1 -0.30 0.40 2 3 -1 0.30 0.50 2 3 -1 -0.20 0.40 -2 -3 1 0.60 0.50 2 -3 -1 0.60 0.60 2 -3 -1 0.40 0.30 2 3 0 1230.18 56.79 2 3 0 1361.96 57.09 -2 3 0 1396.86 57.09 2 3 0 1261.47 57.09 2 -3 0 1395.56 56.89 -2 -3 0 1397.46 57.39 2 -3 0 1372.06 57.29 -2 -3 0 1208.18 57.29 2 3 1 11.70 1.20 2 3 1 11.90 1.10 -2 3 -1 11.70 1.20 2 -3 1 14.10 1.50 -2 -3 -1 12.90 1.50 -2 -3 -1 14.60 1.70 2 -3 1 13.30 1.00 -2 3 -2 200.88 9.90 -2 3 -2 218.68 9.80 2 3 2 218.78 9.80 2 3 2 204.38 9.70 -2 -3 -2 196.48 10.00 -2 -3 -2 220.38 10.20 2 -3 2 223.88 9.60 -2 3 -3 1.30 0.50 2 3 3 0.60 0.60 2 3 3 1.30 0.50 -2 3 -3 0.50 0.40 -2 -3 -3 0.70 0.50 2 -3 3 1.40 0.40 -2 -3 -3 0.80 0.70 2 3 4 41.80 2.60 -2 3 -4 41.80 2.70 2 3 4 43.80 2.80 2 -3 4 41.60 2.30 -2 -3 -4 39.90 2.80 -2 -3 -4 35.60 2.70 2 3 5 186.18 8.90 2 3 5 167.88 8.60 -2 3 -5 192.68 9.00 -2 -3 -5 173.48 9.00 -2 -3 -5 183.28 8.90 2 -3 5 184.38 8.40 2 3 6 25.90 2.20 2 3 6 25.10 2.00 -2 3 -6 26.50 2.20 2 -3 6 29.10 1.80 -2 -3 -6 25.20 2.20 -2 -3 -6 22.70 2.10 2 3 7 17.60 1.80 2 3 7 18.30 2.00 -2 -3 -7 16.10 2.00 -2 -3 -7 20.00 1.90 2 -3 7 18.60 1.50 2 3 8 1.20 0.80 -2 -3 -8 0.70 0.60 2 -3 8 1.10 0.60 -2 3 -9 28.70 2.40 -2 3 -9 30.40 2.60 2 3 9 31.70 2.30 -2 3 -9 28.60 2.10 2 3 9 28.30 2.00 2 3 9 31.70 2.60 -2 3 -9 29.20 2.20 -2 3 -9 32.10 2.20 -2 -3 -9 32.70 2.20 2 -3 9 30.30 1.80 2 -3 9 35.10 2.40 -2 3 -10 79.19 4.60 -2 3 -10 80.79 4.30 -2 3 -10 74.49 4.10 2 3 10 78.09 4.30 -2 3 -10 69.39 4.30 2 3 10 74.99 4.50 -2 3 -10 71.79 4.10 2 3 10 72.29 4.00 -2 3 -10 79.39 4.40 -2 -3 -10 82.79 4.20 2 -3 10 73.69 3.70 -2 -3 -10 78.29 4.20 2 3 11 3.60 1.10 -2 3 -11 4.20 1.00 2 3 11 4.70 0.90 -2 3 -11 5.80 1.20 -2 3 -11 5.20 1.10 -2 3 -11 5.30 0.90 -2 3 -11 4.10 0.90 2 3 11 5.00 1.00 -2 -3 -11 4.70 1.00 2 -3 11 4.00 0.60 -2 -3 -11 5.60 0.90 -2 3 -12 34.70 2.50 2 3 12 38.40 2.50 2 3 12 39.30 2.30 -2 3 -12 32.50 2.30 -2 3 -12 34.50 2.60 -2 3 -12 38.40 2.50 -2 3 -12 36.00 2.60 2 -3 12 38.90 2.00 -2 -3 -12 36.80 2.40 -2 -3 -12 37.20 2.40 2 -3 12 33.80 2.30 2 3 13 8.40 1.10 -2 3 -13 6.30 1.10 -2 3 -13 6.60 1.00 -2 3 -13 6.70 1.20 2 3 13 6.50 0.90 -2 3 -13 8.40 1.10 2 -3 13 7.50 1.00 2 -3 13 8.30 0.70 2 -3 13 8.40 0.90 -2 -3 -13 7.10 1.00 -2 -3 -13 7.30 1.00 -2 3 -14 160.18 7.70 2 3 14 167.48 7.70 2 3 14 165.28 7.80 -2 3 -14 173.88 8.00 -2 -3 -14 164.78 7.80 2 -3 14 176.08 7.80 2 -3 14 159.48 7.70 2 -3 14 165.18 7.40 -2 -3 -14 176.78 7.80 -2 3 -15 0.40 0.50 2 3 15 0.30 0.30 -2 3 -15 0.80 0.50 -2 3 -15 0.40 0.40 2 -3 15 0.70 0.30 2 -3 15 0.50 0.30 -2 -3 -15 1.00 0.40 -2 -3 -15 0.60 0.30 2 -3 15 0.60 0.50 -2 4 15 13.30 1.00 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4 -3 3.70 0.90 2 4 -3 3.20 0.90 -2 4 3 3.20 0.80 2 -4 -3 3.30 0.90 -2 4 2 245.38 11.40 2 4 -2 257.67 11.40 2 -4 -2 219.98 11.10 2 -4 -2 248.78 11.80 -2 -4 2 237.88 11.60 -2 4 1 3.90 0.90 2 4 -1 4.70 0.90 -2 -4 1 5.20 1.20 2 -4 -1 5.50 0.90 -2 -4 1 6.60 1.50 2 -4 -1 4.70 1.10 2 4 0 15.60 1.70 -2 4 0 15.80 1.70 -2 -4 0 17.10 2.10 2 -4 0 13.80 1.80 -2 -4 0 18.10 2.10 2 -4 0 14.30 1.50 -2 4 -1 27.10 2.10 2 4 1 21.40 2.10 2 -4 1 21.20 1.70 -2 -4 -1 24.60 2.30 -2 -4 -1 23.90 2.30 2 4 2 208.98 9.90 -2 4 -2 202.78 9.80 2 -4 2 198.68 9.50 -2 -4 -2 214.58 10.30 -2 -4 -2 198.68 10.20 2 4 3 67.79 4.10 -2 -4 -3 70.89 4.50 -2 -4 -3 67.59 4.40 2 -4 3 68.29 3.80 2 4 4 197.98 10.20 2 -4 4 205.28 9.90 -2 -4 -4 238.58 10.90 -2 -4 -4 212.88 10.80 2 4 5 0.10 0.40 -2 -4 -5 1.20 1.00 2 -4 5 0.70 0.60 -2 -4 -5 -0.80 0.70 2 4 6 104.29 5.50 -2 4 -6 105.89 5.30 -2 4 -6 102.89 5.50 -2 4 -6 104.49 6.00 2 4 6 108.39 5.60 -2 4 -6 112.89 5.80 2 -4 6 108.59 5.50 -2 -4 -6 105.79 5.10 -2 -4 -6 105.89 5.40 2 -4 6 99.69 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1.70 0.40 10 -3 -17 3.20 0.50 -10 -3 17 3.00 0.50 -10 3 16 2.50 0.60 -10 3 16 3.00 0.50 -10 3 16 1.40 0.50 -10 3 16 2.70 0.50 10 3 -16 2.50 0.70 10 -3 -16 1.90 0.50 10 -3 -16 2.20 0.40 -10 -3 16 2.50 0.60 -10 -3 16 2.20 0.50 10 3 -15 5.90 0.90 -10 3 15 5.40 0.80 -10 3 15 3.70 0.70 -10 3 15 4.50 0.80 -10 3 15 5.70 0.90 -10 3 15 5.40 1.00 10 -3 -15 6.00 0.90 -10 -3 15 6.60 1.00 -10 -3 15 5.40 0.80 -10 -3 15 5.00 0.70 -10 -3 15 5.30 0.80 10 -3 -15 5.60 0.70 -10 3 14 54.89 3.20 -10 3 14 55.39 3.10 -10 3 14 55.99 3.20 -10 3 14 51.59 3.00 10 3 -14 54.69 3.30 -10 3 14 52.29 2.90 -10 -3 14 57.09 3.10 -10 -3 14 51.09 2.90 -10 -3 14 51.59 3.20 10 -3 -14 56.49 2.90 10 -3 -14 54.29 3.00 -10 -3 14 53.99 3.00 -10 3 13 166.88 8.10 10 3 -13 171.88 8.20 -10 3 13 168.88 8.20 -10 3 13 165.68 7.80 -10 3 13 169.48 7.90 -10 3 13 163.08 7.80 -10 3 13 172.38 8.30 10 -3 -13 172.08 7.70 -10 -3 13 164.48 8.00 -10 -3 13 172.78 7.90 10 -3 -13 178.88 7.90 -10 -3 13 153.48 7.70 -10 -3 13 152.88 8.10 -10 3 12 3.60 0.90 -10 3 12 3.50 0.70 -10 3 12 3.30 0.80 10 3 -12 3.40 0.90 -10 3 12 2.20 0.70 -10 3 12 3.30 0.90 -10 3 12 4.90 0.80 -10 3 12 4.10 1.00 -10 -3 12 3.30 0.80 10 -3 -12 3.50 0.70 -10 -3 12 3.30 0.60 10 -3 -12 2.70 0.80 -10 -3 12 3.20 1.00 -10 -3 12 3.30 0.70 -10 3 11 135.29 6.40 10 3 -11 119.49 6.40 10 3 -11 121.59 6.10 -10 3 11 127.89 6.60 -10 3 11 131.89 6.50 -10 3 11 132.19 6.50 -10 3 11 130.79 6.30 -10 3 11 120.09 6.00 -10 -3 11 117.69 6.40 10 -3 -11 126.29 6.00 -10 -3 11 128.49 6.30 -10 -3 11 133.79 6.30 -10 3 10 102.69 5.20 10 3 -10 101.09 5.10 -10 3 10 105.39 5.30 -10 3 10 94.39 5.00 -10 3 10 104.19 5.30 10 3 -10 93.59 5.00 -10 3 10 105.19 5.30 -10 3 10 103.09 5.40 10 3 -10 94.29 5.30 10 3 -10 104.39 5.30 -10 -3 10 102.59 5.10 10 -3 -10 97.39 4.80 -10 -3 10 93.29 5.30 -10 -3 10 98.69 5.10 10 3 -9 0.60 0.60 -10 3 9 0.70 0.60 -10 3 9 1.90 0.70 10 3 -9 0.20 0.80 -10 3 9 -0.10 0.80 -10 -3 9 -0.60 0.50 10 -3 -9 0.20 0.80 10 3 -8 139.39 7.80 10 3 -8 155.58 8.00 10 3 -8 160.78 7.80 10 -3 -8 144.89 8.10 10 3 -7 24.10 2.30 10 3 -7 25.60 2.60 10 3 -7 19.40 2.20 10 -3 -7 18.80 2.40 10 3 -6 31.40 2.60 10 3 -6 31.20 2.50 10 3 -6 23.30 2.20 10 -3 -6 32.20 2.70 -10 -3 6 24.10 2.30 -10 -3 6 29.00 2.30 10 3 -5 3.70 1.10 10 3 -5 3.20 1.10 -10 -3 5 3.50 1.00 -10 -3 5 4.10 1.10 10 -3 -5 3.90 1.20 10 3 -4 268.57 12.80 10 3 -4 276.47 12.90 10 -3 -4 272.77 13.00 -10 -3 4 255.87 12.80 -10 -3 4 257.87 12.70 10 3 -3 0.00 0.80 10 3 -3 -0.10 0.40 10 3 -3 -0.10 0.50 -10 -3 3 0.40 0.50 10 -3 -3 0.30 0.50 -10 -3 3 -0.10 0.40 10 3 -2 1.70 0.90 10 3 -2 3.20 0.80 10 3 -2 2.90 1.10 -10 -3 2 1.60 0.70 10 -3 -2 2.60 0.50 -10 -3 2 3.30 0.90 10 3 -1 115.19 5.90 10 3 -1 116.39 6.30 10 3 -1 117.79 6.50 -10 -3 1 108.39 6.40 -10 -3 1 110.79 6.20 10 -3 -1 111.39 5.20 10 3 0 1374.56 58.99 10 3 0 1380.06 59.69 10 3 0 1377.16 59.49 -10 -3 0 1368.26 59.39 10 -3 0 1349.07 58.19 -10 -3 0 1322.57 59.69 10 3 1 558.14 24.70 10 3 1 560.94 25.40 10 -3 1 557.04 23.80 -10 -3 -1 545.35 25.30 -10 -3 -1 534.35 25.00 10 3 2 744.63 33.20 10 3 2 754.62 32.60 -10 -3 -2 706.53 33.10 10 -3 2 741.83 31.60 -10 -3 -2 721.03 32.80 10 3 3 14.80 1.60 -10 3 -3 25.10 2.90 -10 3 -3 15.40 2.10 10 3 3 17.00 2.00 10 3 3 15.40 2.10 10 3 3 19.00 2.60 -10 3 -3 14.60 1.70 -10 -3 -3 13.20 2.00 -10 -3 -3 16.50 1.60 10 -3 3 17.40 1.20 -10 -3 -3 17.80 2.10 -10 -3 -3 19.70 1.50 -10 3 -4 36.80 2.50 -10 3 -4 37.30 2.60 10 3 4 38.20 2.00 -10 3 -4 36.60 2.50 10 3 4 39.40 3.40 -10 3 -4 32.20 2.20 -10 3 -4 41.80 2.90 10 3 4 38.80 2.60 -10 3 -4 39.60 2.90 -10 -3 -4 39.60 2.60 -10 -3 -4 40.20 2.50 -10 -3 -4 39.80 2.50 10 -3 4 38.70 2.20 -10 3 -5 191.48 9.10 10 3 5 192.08 8.90 -10 3 -5 172.28 8.60 -10 3 -5 194.58 9.30 -10 3 -5 176.48 8.70 10 3 5 173.58 8.10 -10 3 -5 166.58 8.40 10 3 5 181.18 9.90 -10 3 -5 181.78 8.60 -10 -3 -5 182.58 8.50 -10 -3 -5 194.18 8.80 -10 -3 -5 168.98 8.50 -10 -3 -5 179.88 8.60 -10 3 -6 33.40 2.20 10 3 6 34.10 3.40 -10 3 -6 37.30 2.60 10 3 6 36.10 2.50 -10 3 -6 35.70 2.40 -10 3 -6 38.00 2.50 -10 3 -6 35.80 2.60 -10 3 -6 35.70 2.80 10 3 6 33.30 1.90 -10 -3 -6 35.50 2.30 -10 -3 -6 34.20 2.30 -10 -3 -6 32.90 2.20 -10 -3 -6 32.20 2.30 -10 -3 -6 35.20 2.50 10 3 7 79.59 4.10 -10 3 -7 80.09 4.60 -10 3 -7 86.29 4.90 -10 3 -7 83.29 4.40 10 3 7 80.69 4.40 -10 3 -7 82.49 4.50 -10 3 -7 75.49 4.10 -10 3 -7 80.29 4.30 -10 -3 -7 82.99 4.50 -10 -3 -7 75.19 4.20 -10 -3 -7 78.99 4.20 -10 -3 -7 77.49 4.10 -10 -3 -7 74.89 4.20 -10 3 -8 5.40 1.10 -10 3 -8 5.70 0.90 -10 3 -8 3.30 1.10 -10 3 -8 4.10 0.90 10 3 8 6.10 1.00 -10 3 -8 4.20 0.90 -10 3 -8 4.90 1.00 10 3 8 5.70 0.80 -10 -3 -8 3.70 0.70 -10 -3 -8 6.00 0.80 -10 -3 -8 4.30 0.90 -10 -3 -8 4.50 0.80 10 3 9 2.60 0.70 10 3 9 4.00 0.70 -10 3 -9 1.90 0.90 -10 3 -9 2.90 0.90 -10 3 -9 2.50 0.70 -10 3 -9 3.30 0.70 -10 3 -9 1.90 0.70 -10 -3 -9 2.80 0.60 -10 -3 -9 1.90 0.60 -10 -3 -9 3.80 0.80 -10 -3 -9 3.80 0.70 -10 3 -10 33.90 2.10 10 3 10 29.70 1.90 -10 3 -10 35.50 2.30 -10 3 -10 34.10 2.30 -10 3 -10 33.40 2.10 10 3 10 33.10 2.10 -10 -3 -10 33.00 2.00 -10 -3 -10 32.40 1.80 -10 -3 -10 29.20 1.90 10 -3 10 30.90 1.70 -10 3 -11 39.00 2.10 10 3 11 39.80 2.00 -10 3 -11 35.80 2.20 10 3 11 34.20 2.00 -10 3 -11 37.10 2.30 -10 3 -11 28.80 1.90 10 -3 11 38.30 1.80 -10 -3 -11 32.00 1.80 -10 -3 -11 36.20 2.00 -10 -3 -11 36.80 2.00 -10 4 15 1.10 0.40 10 4 -15 1.60 0.50 -10 4 15 1.40 0.40 -10 -4 15 1.30 0.50 10 -4 -15 1.80 0.40 10 -4 -15 1.40 0.30 -10 4 14 0.10 0.50 -10 4 14 0.40 0.40 10 4 -14 0.30 0.40 -10 4 14 0.70 0.50 -10 4 14 0.20 0.30 -10 -4 14 0.50 0.40 10 -4 -14 -0.10 0.30 10 -4 -14 0.60 0.30 -10 -4 14 0.10 0.30 -10 4 13 3.00 0.80 -10 4 13 3.80 0.70 -10 4 13 2.10 0.70 -10 4 13 1.60 0.60 -10 4 13 2.80 0.60 10 4 -13 3.40 0.90 -10 4 13 3.00 0.60 10 -4 -13 3.20 0.60 10 -4 -13 2.80 0.50 -10 -4 13 2.40 0.60 -10 -4 13 3.40 0.60 -10 4 12 2.70 0.60 -10 4 12 2.70 0.70 10 4 -12 1.80 0.70 -10 4 12 1.40 0.70 -10 4 12 0.80 0.50 -10 4 12 1.70 0.70 10 -4 -12 1.70 0.60 10 -4 -12 2.40 0.60 -10 -4 12 2.20 0.60 -10 -4 12 1.90 0.60 10 4 -11 0.70 0.40 10 4 -11 1.60 0.80 -10 4 11 1.30 0.70 -10 4 11 0.60 0.70 -10 4 11 1.70 0.60 -10 4 11 0.60 0.60 -10 4 11 1.70 0.60 -10 -4 11 0.40 0.50 10 -4 -11 2.00 0.50 -10 -4 11 1.20 0.50 -10 -4 11 0.90 0.60 -10 -4 11 1.20 0.70 10 4 -10 105.49 5.30 10 4 -10 110.29 5.60 -10 4 10 113.19 5.80 -10 4 10 106.69 5.50 -10 4 10 107.69 5.30 -10 4 10 110.39 5.60 -10 4 10 110.89 5.60 -10 -4 10 107.39 5.50 -10 -4 10 98.59 5.60 -10 -4 10 102.59 5.20 -10 -4 10 112.29 5.40 10 -4 -10 105.39 5.10 -10 4 9 34.70 2.60 -10 4 9 32.40 2.40 10 4 -9 34.20 2.40 -10 4 9 33.10 2.10 10 4 -9 32.30 2.20 -10 4 9 35.00 2.40 -10 4 9 31.00 2.20 -10 -4 9 34.40 2.20 -10 -4 9 28.70 2.40 10 -4 -9 30.50 2.00 -10 -4 9 30.40 2.00 -10 -4 9 31.90 2.30 10 4 -8 112.09 6.00 -10 4 8 119.39 6.10 -10 4 8 123.39 6.20 -10 4 8 121.79 5.80 -10 4 8 114.29 5.90 10 4 -8 122.59 5.90 -10 -4 8 117.69 6.00 -10 -4 8 112.79 6.00 -10 -4 8 106.29 5.60 -10 -4 8 121.99 5.80 10 4 -7 24.70 2.00 10 4 -7 24.50 2.10 -10 4 7 26.90 2.00 -10 4 7 22.60 2.00 -10 4 7 26.60 2.10 -10 4 7 27.10 2.10 -10 4 7 25.40 1.90 -10 -4 7 23.90 1.90 -10 -4 7 23.80 2.00 -10 -4 7 25.60 1.90 -10 4 6 28.00 2.20 10 4 -6 28.70 2.10 -10 4 6 29.00 2.20 -10 4 6 29.70 2.20 -10 4 6 27.80 2.10 10 4 -6 26.40 2.20 10 4 -6 28.90 2.20 -10 4 6 29.30 2.00 -10 -4 6 27.30 2.10 -10 -4 6 30.50 2.00 -10 -4 6 29.10 2.10 -10 4 5 52.39 3.30 10 4 -5 51.19 3.20 10 4 -5 51.09 3.00 -10 4 5 48.20 2.90 -10 4 5 49.20 3.10 -10 4 5 51.39 3.10 10 4 -5 44.60 3.00 -10 4 5 50.19 3.10 -10 -4 5 48.60 3.00 -10 -4 5 49.10 2.90 -10 -4 5 47.80 3.00 10 4 -4 18.10 1.70 10 4 -4 18.40 1.70 -10 4 4 16.20 1.70 -10 4 4 19.70 1.70 -10 4 4 19.00 1.70 -10 4 4 18.70 1.80 -10 4 4 16.10 1.50 10 4 -4 21.00 2.00 -10 -4 4 20.20 1.70 -10 -4 4 16.50 1.70 -10 -4 4 16.80 1.50 -10 4 3 94.79 4.90 10 4 -3 100.29 5.00 -10 4 3 95.59 5.00 -10 4 3 101.89 5.30 -10 4 3 97.79 5.20 10 4 -3 110.79 5.60 10 4 -3 100.19 5.30 -10 -4 3 96.89 5.10 -10 -4 3 90.49 4.80 10 -4 -3 104.39 5.10 -10 -4 3 95.49 5.00 -10 -4 3 79.09 4.80 -10 4 2 2.40 0.90 -10 4 2 3.00 0.70 -10 4 2 4.50 0.90 10 4 -2 3.10 0.80 10 4 -2 4.70 1.10 -10 4 2 2.90 0.90 10 4 -2 3.10 1.00 -10 -4 2 3.30 0.90 -10 -4 2 3.20 0.90 -10 -4 2 3.00 0.70 10 4 -1 0.30 0.80 10 4 -1 0.00 0.60 -10 4 1 0.20 0.50 -10 4 1 -0.10 0.50 10 4 -1 0.10 0.70 -10 4 1 -0.20 0.60 -10 4 1 0.10 0.50 -10 -4 1 0.00 0.60 -10 -4 1 0.70 0.60 -10 -4 1 1.10 0.70 -10 4 0 355.36 15.70 10 4 0 362.16 16.20 10 4 0 349.17 15.60 -10 4 0 342.77 15.60 -10 4 0 336.57 15.40 -10 4 0 341.87 15.20 -10 -4 0 328.57 15.30 -10 -4 0 339.17 15.40 -10 -4 0 306.67 15.30 10 4 1 822.42 36.30 -10 4 -1 822.82 35.50 -10 4 -1 795.22 35.60 10 4 1 720.83 35.50 10 4 1 835.12 35.70 -10 4 -1 828.62 35.30 -10 4 -1 847.62 35.80 -10 -4 -1 831.12 35.40 -10 -4 -1 803.92 35.50 -10 -4 -1 820.22 35.50 -10 4 -2 111.29 5.60 10 4 2 106.29 5.60 10 4 2 96.69 6.10 -10 4 -2 114.89 5.90 -10 4 -2 104.09 5.30 10 4 2 108.49 5.70 -10 4 -2 107.99 5.70 -10 -4 -2 104.69 5.50 -10 -4 -2 111.69 5.50 -10 -4 -2 110.59 5.50 -10 4 -3 0.00 0.60 -10 4 -3 0.50 0.70 10 4 3 0.00 0.40 -10 4 -3 0.40 0.70 10 4 3 0.40 0.60 10 4 3 0.50 0.80 -10 4 -3 0.30 0.40 -10 4 -3 0.30 0.90 -10 -4 -3 0.30 0.40 -10 -4 -3 0.60 0.70 -10 -4 -3 0.00 0.60 -10 4 -4 71.89 3.80 -10 4 -4 77.69 4.20 10 4 4 75.59 4.20 -10 4 -4 70.89 4.50 -10 4 -4 74.79 4.40 10 4 4 69.19 4.00 -10 -4 -4 70.89 3.90 -10 -4 -4 71.69 3.90 -10 -4 -4 72.19 4.00 -10 4 -5 36.40 2.40 -10 4 -5 34.30 2.30 -10 4 -5 34.30 2.50 10 4 5 36.50 2.50 -10 4 -5 33.20 2.70 -10 -4 -5 32.70 2.20 -10 -4 -5 36.60 2.20 -10 -4 -5 35.90 2.40 10 4 6 62.79 3.50 -10 4 -6 62.29 3.70 -10 4 -6 63.39 3.60 -10 4 -6 58.49 3.80 -10 4 -6 60.89 3.30 -10 -4 -6 59.99 3.40 -10 -4 -6 59.89 3.30 -10 4 -7 1.60 0.70 10 4 7 1.90 0.70 -10 4 -7 2.00 0.60 -10 4 -7 2.60 0.90 -10 4 -7 1.80 0.70 -10 4 -7 3.40 0.80 -10 -4 -7 2.80 0.50 -10 -4 -7 2.00 0.60 -10 -4 -7 1.70 0.70 10 4 8 -0.40 0.50 -10 4 -8 0.20 0.60 -10 4 -8 0.20 0.60 -10 4 -8 0.10 0.40 -10 4 -8 0.30 0.50 -10 4 -8 0.50 0.40 -10 -4 -8 0.20 0.30 -10 -4 -8 0.30 0.30 -10 -4 -8 0.10 0.40 10 -4 8 0.20 0.20 -10 4 -9 26.10 1.80 -10 4 -9 24.30 1.70 10 4 9 20.60 1.50 -10 4 -9 25.70 1.60 -10 -4 -9 26.20 1.50 -10 -4 -9 19.50 1.40 -10 -4 -9 24.60 1.50 10 -4 9 24.50 1.30 -10 5 12 0.60 0.40 10 5 -12 1.10 0.40 -10 5 12 0.00 0.40 10 -5 -12 0.90 0.30 10 -5 -12 0.50 0.30 -10 -5 12 0.40 0.30 -10 -5 12 0.40 0.20 -10 -5 12 0.70 0.30 10 5 -11 1.90 0.50 -10 5 11 1.30 0.50 -10 5 11 1.30 0.50 10 -5 -11 0.40 0.30 -10 -5 11 0.90 0.40 -10 -5 11 0.70 0.40 10 -5 -11 1.20 0.40 -10 -5 11 0.90 0.40 10 5 -10 1.20 0.50 -10 5 10 0.70 0.50 -10 5 10 0.70 0.40 10 5 -10 0.80 0.40 -10 5 10 0.50 0.60 -10 -5 10 0.70 0.40 -10 -5 10 0.20 0.50 10 -5 -10 0.80 0.40 -10 -5 10 0.20 0.30 -10 5 9 74.19 4.00 -10 5 9 69.89 3.80 10 5 -9 75.69 3.80 -10 5 9 78.59 4.20 -10 5 9 73.69 3.80 10 5 -9 78.19 4.10 -10 -5 9 71.29 3.70 -10 -5 9 79.99 3.90 10 -5 -9 73.89 3.60 -10 -5 9 81.09 4.00 -10 5 8 2.20 0.70 -10 5 8 1.40 0.70 -10 5 8 1.00 0.60 10 5 -8 1.50 0.60 10 5 -8 1.80 0.60 -10 5 8 2.40 0.60 -10 -5 8 2.70 0.60 -10 -5 8 1.30 0.50 -10 -5 8 1.60 0.70 10 5 -7 92.29 4.60 10 5 -7 88.39 4.70 -10 5 7 90.49 4.90 -10 5 7 94.79 4.80 -10 5 7 95.29 4.60 -10 5 7 91.59 4.70 -10 -5 7 94.29 4.70 -10 -5 7 85.49 4.70 -10 -5 7 90.99 4.50 -10 -5 7 82.59 4.40 -10 5 6 12.00 1.30 -10 5 6 12.80 1.40 -10 5 6 13.20 1.30 -10 5 6 13.30 1.60 -10 5 6 13.70 1.30 10 5 -6 13.20 1.30 10 5 -6 12.70 1.40 -10 -5 6 13.10 1.10 -10 -5 6 11.70 1.40 -10 -5 6 13.60 1.30 -10 5 5 56.99 3.50 10 5 -5 60.29 3.30 -10 5 5 56.69 3.40 10 5 -5 58.79 3.40 -10 5 5 58.99 3.30 -10 5 5 60.99 3.50 -10 5 5 60.79 3.40 10 5 -5 56.69 3.40 -10 -5 5 64.19 3.50 -10 -5 5 58.49 3.40 10 5 -4 35.90 2.50 -10 5 4 33.80 2.40 -10 5 4 34.30 2.40 -10 5 4 35.40 2.50 -10 5 4 35.40 2.30 10 5 -4 37.30 2.40 10 5 -4 36.20 2.40 -10 5 4 37.50 2.50 -10 -5 4 34.80 2.30 -10 -5 4 39.50 2.40 -10 -5 4 34.20 2.40 10 5 -3 27.00 2.10 -10 5 3 32.40 2.30 10 5 -3 27.30 2.20 10 5 -3 31.10 2.10 -10 5 3 30.80 2.00 -10 5 3 28.80 2.00 -10 5 3 28.30 2.20 -10 -5 3 28.10 2.10 -10 -5 3 26.80 2.00 -10 -5 3 30.20 2.10 10 5 -2 64.79 3.50 10 5 -2 58.39 3.50 10 5 -2 68.09 3.90 -10 5 2 63.69 3.60 -10 5 2 67.49 3.90 -10 5 2 67.79 3.90 -10 5 2 68.29 3.50 -10 -5 2 65.39 3.70 -10 -5 2 68.89 3.70 -10 -5 2 62.89 3.60 -10 5 1 25.20 1.80 -10 5 1 27.00 2.10 -10 5 1 24.00 2.00 10 5 -1 21.90 1.90 -10 5 1 27.60 2.00 10 5 -1 23.20 1.70 10 5 -1 27.50 2.10 -10 -5 1 27.60 2.00 -10 -5 1 24.60 1.80 -10 -5 1 24.40 1.90 10 5 0 14.10 1.40 -10 5 0 14.40 1.50 -10 5 0 15.80 1.50 -10 5 0 14.40 1.50 -10 -5 0 14.80 1.50 -10 -5 0 14.20 1.30 -10 -5 0 15.30 1.40 -10 5 -1 0.50 0.70 -10 5 -1 0.30 0.50 -10 5 -1 -0.70 0.60 10 5 1 0.70 0.50 -10 -5 -1 0.40 0.40 -10 -5 -1 0.00 0.40 -10 -5 -1 0.30 0.40 10 5 2 1.20 0.50 -10 5 -2 1.00 0.70 -10 5 -2 1.00 0.50 -10 5 -2 0.80 0.60 -10 -5 -2 0.80 0.60 -10 -5 -2 0.50 0.50 -10 -5 -2 1.60 0.60 -10 5 -3 13.90 1.50 -10 5 -3 13.90 1.30 10 5 3 12.30 1.20 -10 5 -3 16.40 1.60 -10 -5 -3 14.90 1.30 -10 -5 -3 12.30 1.20 -10 -5 -3 12.50 1.10 10 5 4 -0.10 0.30 10 5 4 0.00 0.30 -10 5 -4 -0.10 0.40 -10 5 -4 0.30 0.40 -10 5 -4 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2.10 0.80 -11 -3 -5 2.80 0.80 -11 -3 -5 2.30 0.70 -11 -3 -5 1.50 0.50 -11 -3 -5 2.60 0.90 -11 3 -6 18.00 1.50 11 3 6 15.00 1.10 -11 3 -6 16.70 1.70 11 3 6 18.00 1.70 -11 3 -6 17.30 1.90 -11 3 -6 15.10 1.60 -11 3 -6 18.70 2.10 -11 -3 -6 13.60 1.40 -11 -3 -6 16.70 1.40 -11 -3 -6 16.40 1.40 -11 -3 -6 15.80 1.70 11 3 7 10.90 1.40 -11 3 -7 10.20 1.50 -11 3 -7 10.00 1.20 11 3 7 9.10 1.10 -11 3 -7 6.90 1.10 -11 3 -7 9.80 1.20 -11 3 -7 9.50 1.40 -11 -3 -7 8.50 1.10 -11 -3 -7 7.80 1.10 -11 -3 -7 9.60 1.00 -11 -3 -7 9.90 1.00 -11 -3 -7 8.90 1.00 11 3 8 260.87 11.40 -11 3 -8 267.57 11.70 -11 3 -8 265.57 12.00 11 3 8 263.57 11.80 -11 3 -8 261.27 12.00 -11 3 -8 251.17 11.70 -11 3 -8 263.37 11.60 -11 -3 -8 245.78 11.50 -11 -3 -8 249.08 11.60 -11 -3 -8 230.38 11.50 -11 -3 -8 237.28 11.30 11 3 9 3.50 0.60 -11 3 -9 3.30 0.80 11 3 9 4.10 0.80 -11 3 -9 3.30 0.70 -11 3 -9 5.70 0.80 -11 3 -9 5.50 0.90 -11 -3 -9 3.90 0.80 -11 -3 -9 3.60 0.60 -11 -3 -9 3.40 0.60 -11 -3 -9 3.70 0.60 -11 3 -10 27.20 1.80 -11 3 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122.89 5.80 -11 -4 6 110.89 5.90 -11 -4 6 117.29 6.00 11 4 -5 33.00 2.50 -11 4 5 33.40 2.50 -11 4 5 33.70 2.40 -11 4 5 32.50 2.10 -11 4 5 30.80 2.20 -11 4 5 34.40 2.60 11 4 -5 34.60 2.30 11 4 -5 31.60 2.50 -11 -4 5 33.30 2.40 -11 -4 5 30.30 2.10 -11 -4 5 30.70 2.20 -11 4 4 30.50 2.10 11 4 -4 31.70 2.60 11 4 -4 29.30 2.30 11 4 -4 29.40 2.20 -11 4 4 29.40 2.20 -11 4 4 30.40 2.30 -11 4 4 32.50 2.20 -11 4 4 30.30 2.40 -11 -4 4 29.10 1.90 -11 -4 4 28.30 2.20 -11 -4 4 29.00 2.20 -11 4 3 249.97 11.90 11 4 -3 260.97 12.10 -11 4 3 253.67 11.60 -11 4 3 251.27 11.80 11 4 -3 255.07 11.70 11 4 -3 273.27 12.50 -11 4 3 259.27 12.00 -11 -4 3 236.08 11.50 -11 -4 3 257.97 11.80 -11 -4 3 255.27 11.80 11 4 -2 3.50 0.90 -11 4 2 4.80 1.00 11 4 -2 2.30 1.10 -11 4 2 3.70 0.80 -11 4 2 2.80 0.80 -11 4 2 3.40 0.90 11 4 -2 3.00 0.80 -11 -4 2 3.70 0.90 -11 -4 2 3.00 0.70 -11 -4 2 4.50 0.80 -11 -4 2 3.50 0.80 -11 4 1 62.29 3.60 -11 4 1 61.99 3.80 11 4 -1 59.89 4.10 -11 4 1 60.99 3.70 11 4 -1 60.49 3.70 -11 -4 1 61.99 3.50 -11 -4 1 52.69 3.40 -11 -4 1 61.19 3.40 -11 4 0 0.70 0.70 11 4 0 0.10 0.90 -11 4 0 1.30 0.80 -11 4 0 0.80 0.70 11 4 0 0.40 0.70 -11 -4 0 0.20 0.50 -11 -4 0 0.90 0.50 -11 -4 0 1.10 0.60 -11 4 -1 1.90 0.80 11 4 1 1.90 0.80 -11 4 -1 2.30 0.70 -11 4 -1 2.30 0.60 11 4 1 1.90 0.80 -11 4 -1 1.30 0.80 11 4 1 3.10 1.00 -11 -4 -1 1.20 0.70 -11 -4 -1 1.80 0.60 -11 -4 -1 2.40 0.70 11 4 2 79.49 4.40 -11 4 -2 80.79 4.30 -11 4 -2 76.49 4.10 -11 4 -2 83.19 4.60 11 4 2 81.49 4.40 -11 4 -2 76.29 4.30 -11 -4 -2 80.89 4.40 -11 -4 -2 77.79 4.20 -11 -4 -2 72.19 4.40 -11 -4 -2 79.79 4.20 -11 4 -3 4.50 1.10 -11 4 -3 5.10 1.00 11 4 3 3.80 1.00 -11 4 -3 3.30 1.10 -11 4 -3 3.00 0.80 11 4 3 4.10 0.90 -11 4 -3 2.30 0.80 -11 -4 -3 4.00 0.80 -11 -4 -3 3.00 0.70 -11 -4 -3 3.70 0.80 -11 4 -4 176.48 8.50 -11 4 -4 170.68 8.00 -11 4 -4 168.68 8.70 11 4 4 177.48 8.40 11 4 4 163.58 8.20 -11 4 -4 179.18 8.30 -11 -4 -4 174.18 8.10 -11 -4 -4 167.18 8.10 -11 -4 -4 167.58 8.20 11 4 5 0.50 0.50 -11 4 -5 0.70 0.70 -11 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72.99 4.30 13 2 8 76.19 3.50 -13 -2 -8 75.39 3.90 -13 -2 -8 76.19 4.00 -13 -2 -8 77.89 4.10 -13 2 -9 19.50 1.50 -13 2 -9 18.30 1.40 -13 2 -9 18.90 1.60 13 2 9 19.50 1.30 -13 2 -9 19.00 1.80 13 2 9 19.80 1.10 -13 -2 -9 18.30 1.40 -13 -2 -9 18.40 1.40 -13 -2 -9 17.10 1.30 -13 -2 -9 18.40 1.40 -13 2 -10 0.40 0.40 -13 2 -10 0.50 0.40 13 2 10 0.20 0.30 -13 2 -10 0.10 0.30 -13 2 -10 0.40 0.40 13 2 10 0.20 0.40 -13 -2 -10 0.10 0.30 -13 -2 -10 0.30 0.30 -13 -2 -10 0.20 0.30 13 -2 10 0.10 0.20 -13 -2 -10 0.00 0.30 -13 3 17 6.30 0.60 -13 3 17 7.80 0.70 13 3 -17 7.30 0.70 13 -3 -17 6.30 0.60 13 -3 -17 8.50 0.70 -13 -3 17 8.00 0.80 -13 -3 17 8.10 0.80 -13 3 16 205.48 9.40 13 3 -16 204.28 9.60 -13 3 16 208.98 9.60 -13 3 16 218.18 9.70 13 -3 -16 226.78 9.40 -13 -3 16 220.58 9.60 -13 -3 16 215.98 9.70 13 -3 -16 219.98 9.50 -13 -3 16 188.38 9.40 -13 3 15 14.20 1.30 -13 3 15 14.70 1.30 13 3 -15 13.00 1.20 -13 3 15 14.60 1.10 -13 3 15 16.30 1.30 -13 -3 15 13.70 1.40 13 -3 -15 14.00 1.00 -13 -3 15 14.30 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25.70 2.00 -13 3 3 24.70 3.00 -13 -3 3 22.70 1.80 -13 -3 3 23.30 1.90 13 -3 -3 25.00 1.40 -13 -3 3 24.80 1.70 -13 -3 3 23.40 1.80 -13 3 2 183.78 9.90 13 3 -2 184.88 8.10 13 3 -2 190.08 8.90 -13 3 2 182.28 8.80 -13 3 2 183.28 8.80 -13 3 2 179.48 8.60 -13 -3 2 180.68 8.40 -13 -3 2 183.18 8.70 -13 -3 2 182.28 8.50 -13 -3 2 164.98 8.40 13 -3 -2 182.18 8.00 -13 3 1 102.99 5.40 -13 3 1 94.79 5.30 13 3 -1 103.79 5.40 -13 3 1 101.09 5.20 13 3 -1 100.39 4.70 -13 -3 1 103.59 5.10 -13 -3 1 98.99 5.00 -13 -3 1 105.19 5.30 -13 3 0 4.10 0.90 13 3 0 3.50 0.50 13 3 0 3.80 0.90 -13 3 0 2.80 0.80 -13 3 0 4.70 0.90 -13 -3 0 3.70 0.90 -13 -3 0 4.50 1.20 -13 -3 0 2.80 0.70 -13 -3 0 4.10 0.90 -13 -3 0 4.20 0.80 -13 3 -1 15.50 1.70 13 3 1 16.50 1.60 -13 3 -1 13.80 1.60 13 3 1 14.80 1.10 -13 -3 -1 15.30 1.40 -13 -3 -1 13.80 1.60 -13 -3 -1 14.60 1.30 -13 -3 -1 15.50 1.60 -13 -3 -1 17.20 1.50 -13 3 -2 126.19 6.90 -13 3 -2 129.09 6.40 -13 3 -2 131.59 6.60 13 3 2 132.59 5.90 13 3 2 126.39 6.40 -13 -3 -2 128.59 6.70 -13 -3 -2 125.19 6.20 -13 -3 -2 130.69 6.50 -13 -3 -2 125.39 6.20 -13 -3 -2 132.99 6.40 13 3 3 28.50 2.20 13 3 3 27.30 1.60 -13 3 -3 27.00 2.40 -13 3 -3 26.50 2.10 -13 3 -3 26.10 2.10 -13 -3 -3 26.00 2.30 -13 -3 -3 28.00 2.00 -13 -3 -3 26.90 1.80 -13 -3 -3 28.40 2.10 -13 -3 -3 27.60 1.80 13 3 4 91.69 4.90 13 3 4 92.29 4.30 -13 3 -4 87.59 4.70 -13 3 -4 91.29 5.20 -13 3 -4 90.19 4.70 -13 3 -4 95.89 5.00 -13 -3 -4 95.79 4.90 -13 -3 -4 87.69 4.50 -13 -3 -4 93.19 4.80 -13 -3 -4 82.79 4.90 -13 3 -5 3.40 1.00 13 3 5 3.40 0.80 -13 3 -5 2.80 0.70 13 3 5 3.20 0.50 -13 3 -5 3.40 0.80 -13 3 -5 4.40 1.10 -13 -3 -5 3.90 0.80 -13 -3 -5 1.60 0.70 -13 -3 -5 3.30 0.80 -13 -3 -5 4.10 0.60 13 3 6 128.29 6.10 13 3 6 128.09 5.80 13 3 6 105.19 5.40 -13 3 -6 136.19 6.40 -13 3 -6 128.59 6.00 -13 3 -6 111.39 5.90 -13 3 -6 113.89 6.30 -13 -3 -6 123.09 6.00 -13 -3 -6 114.79 5.60 -13 -3 -6 121.69 5.80 -13 -3 -6 121.59 5.90 -13 3 -7 3.50 0.80 13 3 7 3.90 0.60 -13 3 -7 2.70 0.60 13 3 7 2.90 0.70 -13 3 -7 4.20 0.70 -13 3 -7 1.60 0.80 -13 -3 -7 2.80 0.60 -13 -3 -7 3.00 0.70 -13 -3 -7 2.60 0.60 13 3 8 8.10 0.80 -13 3 -8 9.30 0.90 13 3 8 8.10 0.90 -13 3 -8 7.30 1.00 -13 3 -8 7.90 1.00 -13 -3 -8 6.00 0.80 -13 -3 -8 6.70 0.70 -13 -3 -8 8.20 0.90 -13 3 -9 20.00 1.30 13 3 9 16.60 1.20 13 3 9 18.40 1.30 -13 3 -9 21.70 1.50 -13 3 -9 19.80 1.40 -13 -3 -9 22.30 1.30 13 -3 9 16.40 1.00 13 4 -15 103.49 5.00 13 -4 -15 106.39 4.80 13 -4 -15 115.39 4.90 -13 -4 15 101.79 5.00 -13 4 14 1.40 0.40 13 4 -14 1.10 0.50 -13 4 14 0.70 0.40 -13 4 14 0.90 0.30 -13 4 14 0.70 0.40 -13 -4 14 1.40 0.50 -13 -4 14 0.80 0.30 -13 -4 14 1.10 0.40 13 -4 -14 0.80 0.40 13 -4 -14 0.90 0.30 -13 4 13 5.70 0.70 -13 4 13 6.20 0.80 -13 4 13 3.40 0.70 -13 4 13 6.00 0.80 -13 4 13 6.10 0.90 13 4 -13 4.60 0.70 13 -4 -13 5.80 0.70 -13 -4 13 4.50 0.70 13 -4 -13 3.60 0.50 -13 -4 13 3.90 0.70 13 4 -12 6.30 1.00 13 4 -12 6.00 0.80 -13 4 12 6.30 1.00 -13 4 12 7.80 0.90 -13 4 12 6.00 0.90 -13 4 12 6.30 1.00 -13 -4 12 8.30 0.90 13 -4 -12 5.00 0.70 13 -4 -12 7.20 0.60 -13 -4 12 5.20 1.00 -13 4 11 24.20 1.70 13 4 -11 24.30 1.70 -13 4 11 24.10 1.80 -13 4 11 23.40 1.80 -13 4 11 21.80 1.80 13 4 -11 21.90 1.80 -13 4 11 23.70 1.80 -13 -4 11 25.70 1.90 -13 -4 11 25.80 1.70 13 4 -10 52.79 3.00 -13 4 10 48.30 3.10 -13 4 10 49.99 3.10 -13 4 10 49.00 2.80 -13 4 10 52.09 3.20 -13 4 10 50.49 3.10 -13 -4 10 47.90 3.10 -13 -4 10 53.19 3.00 -13 4 9 0.60 0.80 -13 4 9 1.10 0.60 -13 4 9 1.80 0.70 -13 4 9 0.80 0.60 13 4 -9 0.80 0.70 -13 4 9 0.90 0.50 -13 4 9 1.10 0.50 -13 -4 9 0.40 0.80 -13 -4 9 1.70 0.60 -13 -4 9 0.60 0.60 -13 4 8 147.79 7.10 13 4 -8 138.39 6.80 -13 4 8 134.69 6.80 -13 4 8 142.99 7.10 -13 4 8 141.99 7.10 -13 4 8 146.79 7.00 -13 -4 8 142.29 6.80 -13 -4 8 128.59 6.80 -13 -4 8 143.39 7.00 -13 4 7 89.69 4.90 13 4 -7 88.69 4.70 -13 4 7 95.29 5.00 -13 4 7 87.29 4.70 -13 4 7 93.29 4.90 -13 4 7 94.79 4.90 13 4 -7 83.69 4.90 -13 -4 7 93.59 4.70 -13 -4 7 96.29 4.90 -13 -4 7 88.59 4.70 -13 4 6 426.06 19.60 -13 4 6 429.36 19.30 -13 4 6 448.76 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34.40 3.20 14 2 -8 37.70 3.10 14 2 -8 39.20 2.90 14 -2 -8 39.00 3.20 -14 2 7 14.20 2.20 14 2 -7 15.30 2.00 14 2 -7 17.00 2.10 -14 -2 7 12.60 1.90 14 -2 -7 16.20 2.10 14 2 -6 9.70 1.60 14 2 -6 9.00 1.70 14 2 -6 8.80 1.50 -14 -2 6 9.70 1.60 14 -2 -6 9.60 1.70 -14 2 5 63.59 4.60 14 2 -5 62.89 4.20 14 2 -5 63.69 4.40 14 2 -5 71.39 4.20 -14 -2 5 62.29 4.30 14 -2 -5 63.49 4.30 14 2 -4 3.60 1.00 14 2 -4 5.90 1.30 14 2 -4 4.70 1.20 -14 2 4 5.00 1.50 -14 -2 4 3.70 1.00 14 -2 -4 5.30 1.20 -14 -2 4 5.40 1.40 -14 2 3 163.78 9.30 14 2 -3 175.38 9.20 14 2 -3 170.58 8.90 14 2 -3 171.98 8.90 -14 -2 3 169.08 8.90 -14 -2 3 180.38 9.30 14 2 -2 62.59 4.10 -14 2 2 59.09 4.40 14 2 -2 60.89 4.10 -14 -2 2 59.29 4.10 -14 -2 2 62.29 4.40 14 2 -1 8.80 1.60 14 2 -1 9.10 1.60 -14 -2 1 7.00 1.60 -14 -2 1 7.40 1.50 14 2 0 1.10 0.70 14 2 0 1.20 0.80 -14 -2 0 0.70 0.70 -14 -2 0 1.70 0.60 -14 -2 0 0.50 0.60 14 2 1 43.00 2.20 -14 2 -1 42.60 3.20 -14 2 -1 39.50 2.70 -14 -2 -1 46.00 2.60 -14 -2 -1 40.40 2.70 -14 -2 -1 50.79 4.40 -14 -2 -1 41.90 2.50 -14 -2 -1 40.50 2.50 -14 -2 -1 48.20 3.10 -14 2 -2 102.49 5.30 14 2 2 96.69 4.70 -14 2 -2 104.39 5.80 14 2 2 92.19 5.60 -14 -2 -2 99.89 5.00 -14 -2 -2 99.19 5.50 -14 -2 -2 98.09 5.10 -14 -2 -2 97.19 5.10 -14 -2 -2 105.79 5.30 -14 -2 -2 99.39 5.30 -14 -2 -2 106.99 5.10 -14 2 -3 1.60 0.70 -14 2 -3 2.70 1.10 -14 2 -3 1.20 0.50 14 2 3 1.70 0.40 -14 -2 -3 1.80 0.80 -14 -2 -3 2.50 0.70 -14 -2 -3 2.00 0.80 -14 -2 -3 1.60 0.60 -14 -2 -3 1.70 0.90 -14 -2 -3 1.50 0.70 -14 2 -4 8.70 1.10 -14 2 -4 8.60 1.10 -14 2 -4 7.30 1.40 14 2 4 7.70 0.80 -14 2 -4 7.60 1.20 -14 -2 -4 8.30 1.10 -14 -2 -4 5.40 1.10 -14 -2 -4 8.30 1.10 -14 -2 -4 6.50 1.00 -14 -2 -4 8.60 1.20 14 2 5 59.29 3.50 -14 2 -5 60.29 3.80 -14 2 -5 56.29 3.40 14 2 5 60.69 2.90 -14 2 -5 53.29 3.50 -14 2 -5 50.59 3.50 -14 2 -5 62.79 3.50 -14 -2 -5 56.59 3.60 -14 -2 -5 56.99 3.30 -14 -2 -5 59.59 3.40 -14 -2 -5 62.29 3.40 -14 -2 -5 59.69 3.20 -14 2 -6 2.70 0.70 -14 2 -6 4.80 1.10 14 2 6 3.30 0.80 14 2 6 2.90 0.50 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0.80 -14 -3 11 1.60 0.60 -14 -3 11 1.20 0.80 -14 3 10 2.90 0.90 -14 3 10 2.20 0.60 14 3 -10 1.40 1.00 -14 3 10 2.80 1.00 14 3 -10 2.70 0.90 -14 3 10 1.70 0.70 -14 3 10 1.80 0.90 -14 3 10 2.30 0.80 -14 3 10 4.30 1.00 14 3 -10 3.20 0.70 -14 -3 10 1.60 0.90 -14 -3 10 2.70 0.80 -14 -3 10 1.90 0.80 -14 3 9 34.30 2.50 14 3 -9 38.00 2.50 14 3 -9 37.90 2.40 14 3 -9 38.80 3.10 -14 3 9 37.10 2.50 -14 3 9 35.70 2.40 -14 3 9 40.80 2.60 -14 3 9 39.70 2.50 -14 3 9 37.50 2.50 -14 3 9 35.90 2.70 -14 -3 9 36.40 2.50 -14 -3 9 35.70 2.40 -14 -3 9 37.30 2.40 -14 3 8 146.39 7.20 -14 3 8 143.69 7.10 -14 3 8 128.39 6.90 -14 3 8 134.09 6.90 14 3 -8 142.89 6.70 14 3 -8 144.19 6.90 14 3 -8 136.19 7.00 -14 3 8 144.29 6.80 -14 3 8 132.89 6.70 14 3 -8 143.59 7.70 -14 3 8 141.39 6.90 -14 -3 8 134.09 6.80 -14 -3 8 141.79 6.90 -14 -3 8 133.89 6.70 -14 3 7 2.80 0.90 -14 3 7 2.80 0.70 -14 3 7 2.70 0.80 14 3 -7 1.00 0.80 14 3 -7 2.30 0.70 -14 3 7 2.30 0.70 -14 3 7 1.50 0.70 14 3 -7 1.70 1.10 -14 3 7 2.20 0.80 -14 -3 7 1.90 0.60 -14 -3 7 2.20 0.80 -14 -3 7 3.00 0.80 -14 3 6 6.80 1.10 -14 3 6 7.00 1.00 14 3 -6 6.50 1.10 -14 3 6 7.40 1.10 -14 3 6 6.20 1.20 14 3 -6 8.60 1.70 14 3 -6 5.20 1.00 -14 3 6 7.40 1.10 -14 -3 6 7.60 1.10 -14 -3 6 6.90 1.00 -14 -3 6 5.40 1.00 -14 -3 6 7.40 1.00 -14 3 5 8.90 1.10 -14 3 5 11.00 1.50 -14 3 5 8.80 1.00 14 3 -5 11.50 1.60 14 3 -5 8.50 0.80 -14 3 5 8.90 1.30 -14 3 5 8.50 1.10 14 3 -5 10.80 1.80 14 3 -5 8.10 1.10 -14 -3 5 9.00 1.10 -14 -3 5 8.60 1.10 -14 -3 5 8.90 1.10 -14 -3 5 9.80 1.20 -14 3 4 330.17 15.40 -14 3 4 346.27 15.60 14 3 -4 334.27 15.40 -14 3 4 358.36 15.90 -14 3 4 336.87 15.70 14 3 -4 346.37 15.10 14 3 -4 372.56 16.00 -14 -3 4 316.27 15.40 -14 -3 4 353.06 15.60 -14 -3 4 347.27 15.40 -14 -3 4 345.17 15.60 -14 -3 4 359.46 15.50 14 3 -3 110.79 5.20 -14 3 3 111.29 5.60 -14 3 3 108.29 5.80 14 3 -3 120.09 6.00 -14 3 3 111.59 5.80 -14 -3 3 111.29 5.50 -14 -3 3 106.79 5.50 -14 -3 3 109.79 5.60 -14 -3 3 110.39 5.50 -14 3 2 97.19 5.30 14 3 -2 99.99 4.70 -14 3 2 102.69 5.20 14 3 -2 108.99 5.50 -14 3 2 101.69 5.40 -14 -3 2 102.09 5.20 -14 -3 2 92.39 5.00 -14 -3 2 100.39 5.10 -14 -3 2 102.89 5.10 -14 3 1 8.60 1.30 14 3 -1 9.60 1.30 14 3 -1 7.70 0.80 -14 3 1 8.50 1.10 -14 3 1 6.40 1.10 -14 -3 1 9.30 1.20 -14 -3 1 10.60 1.60 -14 -3 1 7.30 1.00 -14 -3 1 7.90 1.00 14 3 0 150.58 7.20 -14 3 0 127.89 7.00 14 3 0 147.89 6.60 -14 3 0 145.79 7.20 -14 3 0 142.99 7.00 -14 -3 0 143.79 7.10 -14 -3 0 139.79 6.80 -14 -3 0 149.88 7.40 -14 -3 0 148.79 6.90 -14 3 -1 77.69 4.20 -14 3 -1 73.89 4.30 14 3 1 79.99 3.70 14 3 1 79.79 4.30 -14 -3 -1 76.09 4.00 -14 -3 -1 75.39 4.30 -14 -3 -1 77.49 4.20 -14 -3 -1 79.59 4.00 -14 -3 -1 78.59 4.50 14 3 2 15.70 1.50 14 3 2 15.10 1.10 -14 3 -2 13.60 1.60 -14 3 -2 14.30 1.40 -14 3 -2 16.20 1.70 -14 -3 -2 14.70 1.20 -14 -3 -2 13.80 1.60 -14 -3 -2 14.00 1.50 -14 -3 -2 12.20 1.70 -14 -3 -2 14.50 1.30 14 3 3 0.40 0.30 14 3 3 0.50 0.70 -14 3 -3 0.60 0.90 -14 3 -3 0.60 0.70 -14 3 -3 1.20 0.70 -14 -3 -3 0.60 0.60 -14 -3 -3 -0.80 0.40 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1.30 -22 2 13 23.60 1.40 -22 2 13 21.10 1.30 -22 2 13 20.30 1.40 -22 2 13 23.70 1.50 -22 -2 13 17.30 1.30 -22 2 12 0.20 0.30 22 2 -12 0.10 0.20 -22 2 12 0.30 0.30 -22 2 12 0.50 0.40 -22 2 12 -0.20 0.30 -22 2 12 0.00 0.40 22 2 -12 -0.10 0.30 -22 -2 12 0.30 0.20 -22 -2 12 0.10 0.30 -22 -2 12 0.20 0.30 22 2 -11 21.20 1.60 -22 2 11 25.90 1.50 -22 2 11 24.80 1.50 -22 2 11 25.50 1.60 -22 2 11 28.90 1.80 22 2 -11 27.10 1.60 -22 -2 11 24.50 1.50 -22 -2 11 24.20 1.60 -22 -2 11 22.40 1.60 -22 2 10 3.10 0.50 -22 2 10 3.80 0.60 -22 2 10 3.20 0.80 22 2 -10 4.50 0.60 -22 2 10 2.30 0.60 22 2 -10 3.50 0.40 22 2 -10 4.00 0.70 -22 -2 10 2.80 0.60 -22 -2 10 3.60 0.60 -22 -2 10 1.70 0.50 22 2 -9 2.40 0.70 -22 2 9 2.20 0.60 22 2 -9 1.40 0.40 -22 2 9 1.90 0.50 22 2 -9 2.20 0.30 -22 -2 9 1.60 0.50 -22 -2 9 1.60 0.50 -22 -2 9 2.80 0.50 22 2 -8 10.50 0.90 22 2 -8 13.30 1.20 22 2 -8 12.60 0.80 -22 2 8 11.40 1.30 -22 2 8 11.60 1.20 -22 -2 8 11.00 1.10 -22 -2 8 11.00 1.20 -22 -2 8 11.40 1.00 -22 -2 8 11.70 1.00 -22 2 7 22.00 1.60 22 2 -7 23.00 1.30 -22 2 7 22.00 1.50 22 2 -7 22.80 1.70 -22 2 7 22.30 1.60 -22 -2 7 20.40 1.40 -22 -2 7 21.50 1.50 -22 -2 7 18.90 1.60 -22 -2 7 22.60 1.60 -22 2 6 27.60 1.90 22 2 -6 29.70 1.50 -22 2 6 28.40 1.80 -22 2 6 26.10 1.60 22 2 -6 28.40 1.90 -22 -2 6 27.20 1.90 -22 -2 6 28.40 1.80 -22 -2 6 28.40 1.80 -22 -2 6 27.90 1.80 -22 2 5 41.60 2.30 22 2 -5 43.30 2.10 22 2 -5 38.40 2.40 -22 -2 5 42.70 2.40 -22 -2 5 42.40 2.30 -22 -2 5 38.60 2.60 -22 -2 5 41.00 2.40 22 2 -4 12.90 1.20 22 2 -4 19.00 1.00 -22 2 4 17.20 1.20 -22 -2 4 18.20 1.40 -22 -2 4 18.20 1.30 -22 -2 4 16.10 1.60 -22 -2 4 18.70 1.30 22 2 -3 139.79 6.00 22 2 -3 125.19 6.30 -22 2 3 131.09 6.20 -22 -2 3 136.29 6.60 -22 -2 3 130.69 6.30 -22 -2 3 142.49 6.40 -22 -2 3 141.69 6.30 22 2 -2 0.30 0.20 -22 -2 2 0.30 0.30 -22 -2 2 0.00 0.40 -22 -2 2 0.30 0.30 -22 -2 2 0.30 0.30 22 2 -1 39.70 2.10 22 2 -1 35.60 1.80 -22 -2 1 40.30 2.30 -22 -2 1 38.20 2.00 -22 -2 1 31.60 2.00 22 3 -9 19.70 1.40 -22 3 9 25.70 1.60 -22 -3 9 29.90 1.70 22 3 -8 1.40 0.40 -22 3 8 0.80 0.40 -22 -3 8 0.90 0.40 -22 -3 8 1.30 0.40 -22 -3 8 0.90 0.30 22 3 -7 0.60 0.30 -22 3 7 1.00 0.40 -22 -3 7 0.40 0.30 -22 -3 7 0.70 0.30 -22 -3 7 0.80 0.30 22 3 -6 1.40 0.50 -22 3 6 1.90 0.50 -22 -3 6 1.70 0.40 -22 -3 6 2.10 0.40 -22 -3 6 1.40 0.40 22 3 -5 0.10 0.30 -22 -3 5 0.60 0.60 -22 -3 5 0.30 0.30 -22 -3 5 0.10 0.30 23 0 -14 144.89 6.70 -23 0 14 164.68 7.10 23 0 -13 0.00 0.30 -23 0 13 0.10 0.40 23 0 -13 0.00 0.10 -23 0 13 0.10 0.30 -23 0 13 0.10 0.20 -23 0 13 0.30 0.30 -23 0 12 16.50 1.20 -23 0 12 16.20 1.30 -23 0 12 18.70 1.50 -23 0 12 17.10 1.30 -23 0 12 19.00 1.20 23 0 -12 17.00 1.00 -23 0 11 -0.60 0.30 -23 0 11 -0.30 0.30 -23 0 11 0.10 0.50 -23 0 11 0.30 0.50 23 0 -11 0.10 0.20 -23 0 11 0.10 0.30 -23 0 10 521.25 21.70 -23 0 10 484.25 21.70 -23 0 10 484.75 21.40 23 0 -10 489.45 21.10 -23 0 10 475.95 21.40 23 0 -9 0.00 0.20 -23 0 9 0.20 0.40 -23 0 9 -0.10 0.30 -23 0 9 -0.60 0.30 -23 0 9 -0.10 0.50 -23 0 8 37.10 2.10 -23 0 8 38.90 2.20 -23 0 8 37.10 2.40 23 0 -8 35.50 1.80 -23 0 7 -0.50 0.50 -23 0 7 -0.10 0.30 -23 0 7 1.10 0.50 -23 0 6 8.00 1.00 -23 0 6 9.50 0.90 -23 0 6 8.40 0.90 -23 0 6 8.90 0.90 -23 0 6 9.60 0.90 -23 0 5 0.00 0.40 -23 0 5 -0.10 0.50 -23 0 5 0.10 0.40 -23 0 5 -0.10 0.30 -23 0 4 73.79 3.70 -23 0 4 74.69 3.80 -23 0 4 72.89 3.70 -23 0 3 -0.10 0.30 -23 0 3 0.10 0.30 -23 0 3 0.00 0.30 -23 0 2 318.77 14.10 -23 0 2 293.47 13.90 -23 0 2 344.57 14.20 -23 0 1 0.00 0.30 -23 0 1 -0.30 0.50 -23 0 1 0.30 0.40 -23 0 1 0.30 0.50 23 1 -13 0.40 0.30 -23 1 13 0.20 0.40 -23 1 13 0.00 0.30 -23 1 13 0.60 0.40 -23 1 13 0.20 0.30 -23 -1 13 0.30 0.30 23 -1 -13 0.30 0.10 23 1 -12 40.60 2.30 -23 1 12 44.80 2.30 -23 1 12 46.10 2.30 -23 1 12 46.90 2.50 -23 1 12 46.70 2.30 23 1 -12 39.80 2.10 -23 -1 12 43.50 2.50 -23 -1 12 42.00 2.30 -23 -1 12 42.40 2.30 23 -1 -12 46.90 2.10 -23 1 11 23.40 1.70 23 1 -11 26.20 1.30 -23 1 11 29.60 1.60 23 1 -11 25.90 1.50 -23 1 11 23.10 1.50 -23 1 11 25.90 1.70 -23 -1 11 25.70 1.70 -23 -1 11 25.50 1.50 -23 -1 11 23.40 1.50 -23 -1 11 26.20 1.80 -23 1 10 1.30 0.50 23 1 -10 0.80 0.20 -23 1 10 0.40 0.50 -23 1 10 1.30 0.40 -23 1 10 0.40 0.40 23 1 -10 1.10 0.40 -23 -1 10 0.60 0.40 -23 -1 10 0.70 0.40 -23 -1 10 0.70 0.40 -23 -1 10 1.00 0.50 -23 1 9 154.98 6.90 -23 1 9 142.49 7.10 -23 1 9 155.58 6.90 23 1 -9 159.68 6.60 23 1 -9 145.09 6.80 -23 1 9 132.49 6.80 -23 -1 9 152.68 7.10 -23 -1 9 152.68 6.90 -23 -1 9 138.59 6.80 23 1 -8 14.60 0.90 -23 1 8 13.30 1.10 -23 1 8 14.30 1.20 -23 1 8 12.40 1.20 -23 -1 8 13.00 1.20 -23 -1 8 14.20 1.30 -23 -1 8 13.80 1.20 -23 1 7 14.60 1.10 23 1 -7 14.00 0.90 -23 1 7 13.20 1.20 -23 -1 7 12.00 1.20 -23 -1 7 12.30 1.10 -23 -1 7 11.80 1.10 -23 -1 7 14.50 1.10 -23 -1 7 13.20 1.10 -23 1 6 64.79 3.20 -23 1 6 62.89 3.20 23 1 -6 62.99 3.00 -23 -1 6 59.19 3.20 -23 -1 6 61.69 3.30 -23 -1 6 62.59 3.40 -23 -1 6 60.79 3.20 -23 -1 6 62.69 3.20 23 1 -5 77.09 3.70 -23 1 5 80.99 4.00 -23 1 5 82.69 3.90 -23 -1 5 76.19 3.80 -23 -1 5 77.69 3.90 -23 -1 5 82.09 4.10 -23 -1 5 81.79 4.00 -23 1 4 24.60 1.60 23 1 -4 25.10 1.40 -23 1 4 26.00 1.60 -23 -1 4 25.10 1.60 -23 -1 4 26.20 1.70 -23 -1 4 26.00 1.60 -23 -1 4 26.50 1.60 -23 1 3 1.00 0.50 23 1 -3 1.60 0.30 -23 1 3 1.80 0.40 -23 -1 3 1.30 0.40 -23 -1 3 1.50 0.50 -23 -1 3 1.00 0.50 -23 -1 3 1.30 0.50 -23 -1 3 1.90 0.50 -23 -1 3 1.00 0.40 -23 1 2 0.00 0.30 -23 1 2 0.00 0.30 -23 1 2 0.00 0.20 23 1 -2 0.10 0.10 -23 -1 2 0.30 0.40 -23 -1 2 0.10 0.30 -23 -1 2 0.20 0.50 -23 -1 2 0.10 0.30 -23 -1 2 0.50 0.30 23 1 -1 208.48 8.90 -23 1 1 221.98 9.10 -23 1 1 211.38 9.10 -23 -1 1 210.18 9.10 -23 -1 1 175.28 9.10 23 2 -11 118.49 5.30 -23 2 11 119.39 5.50 -23 2 11 125.29 5.40 23 2 -11 111.99 5.40 -23 -2 11 114.89 5.50 -23 -2 11 119.19 5.40 -23 -2 11 103.39 5.30 23 2 -10 38.30 2.30 -23 2 10 45.10 2.20 -23 2 10 42.10 2.20 23 2 -10 41.70 2.10 23 2 -10 36.90 1.90 -23 2 10 42.20 2.40 -23 -2 10 39.70 2.20 -23 -2 10 42.10 2.30 -23 -2 10 42.50 2.20 23 2 -9 5.30 0.40 -23 2 9 5.10 0.80 -23 2 9 5.00 0.70 23 2 -9 6.30 0.70 23 2 -9 5.90 0.70 -23 -2 9 4.30 0.60 -23 -2 9 6.10 0.60 -23 -2 9 5.00 0.70 23 2 -8 1.70 0.30 -23 2 8 2.50 0.50 23 2 -8 1.20 0.50 -23 2 8 2.70 0.50 -23 -2 8 1.70 0.40 -23 -2 8 1.30 0.40 -23 -2 8 1.90 0.50 23 2 -7 94.59 5.30 -23 2 7 98.39 5.20 -23 2 7 124.89 5.20 23 2 -7 121.19 5.00 -23 -2 7 108.69 5.10 -23 -2 7 116.29 5.30 -23 2 6 16.90 1.20 23 2 -6 16.20 0.90 23 2 -6 14.00 1.20 -23 -2 6 17.00 1.20 -23 -2 6 16.80 1.20 23 2 -5 189.18 8.90 -23 2 5 201.38 9.10 -23 -2 5 211.78 9.20 -23 -2 5 214.78 9.20 -23 -2 5 206.98 9.10 23 2 -4 34.70 1.90 23 2 -4 27.00 1.50 -23 2 4 29.90 1.70 -23 -2 4 33.40 1.80 -23 -2 4 30.40 1.90 -23 -2 4 34.50 1.80 23 2 -3 6.90 0.50 -23 -2 3 7.20 0.70 -23 -2 3 5.60 0.60 -23 -2 3 5.60 0.80 24 0 -12 59.39 2.80 -24 0 12 62.39 3.00 24 0 -12 63.09 3.00 -24 0 11 0.10 0.30 -24 0 11 0.20 0.40 -24 0 11 0.30 0.30 24 0 -11 0.00 0.20 -24 0 11 0.10 0.40 24 0 -11 -0.20 0.40 24 0 -10 2.60 0.30 -24 0 10 2.00 0.50 -24 0 10 3.30 0.50 -24 0 10 3.20 0.50 24 0 -10 2.50 0.50 -24 0 10 2.30 0.60 -24 0 9 0.00 0.30 -24 0 9 0.10 0.30 24 0 -9 0.20 0.20 24 0 -9 0.00 0.30 24 0 -8 60.89 3.00 -24 0 8 70.69 3.50 -24 0 8 64.99 3.30 -24 0 7 0.40 0.50 24 0 -7 0.00 0.10 -24 0 7 0.20 0.30 -24 0 6 20.70 1.40 -24 0 6 22.00 1.40 -24 0 5 0.00 0.30 -24 0 5 0.00 0.20 -24 0 5 0.10 0.30 -24 0 4 36.70 2.10 -24 0 4 42.40 2.10 -24 0 3 0.00 0.20 -24 0 3 -0.10 0.40 -24 0 3 -0.20 0.30 24 1 -11 136.09 5.70 -24 1 11 129.19 5.60 24 1 -11 108.19 5.40 24 -1 -11 121.49 5.40 -24 -1 11 122.69 5.80 24 1 -10 -0.20 0.20 24 1 -10 0.00 0.10 -24 1 10 0.40 0.40 -24 1 10 -0.20 0.30 -24 -1 10 0.10 0.20 -24 -1 10 0.10 0.30 24 -1 -10 0.10 0.20 24 1 -9 10.00 0.70 -24 1 9 7.80 0.80 -24 1 9 10.30 0.90 -24 -1 9 8.90 0.90 24 -1 -9 8.70 0.60 -24 -1 9 9.20 0.80 -24 -1 9 7.30 0.70 -24 1 8 8.30 0.80 24 1 -8 9.10 0.60 -24 -1 8 8.20 0.80 -24 -1 8 8.50 0.80 24 1 -7 24.70 1.30 -24 1 7 23.70 1.50 -24 -1 7 22.80 1.40 -24 -1 7 23.60 1.50 -24 -1 7 24.80 1.50 24 1 -6 24.80 1.30 24 1 -6 20.80 1.40 -24 1 6 23.70 1.50 -24 -1 6 23.80 1.50 -24 -1 6 21.90 1.40 -24 -1 6 21.40 1.40 -24 -1 6 24.20 1.50 -24 1 5 2.30 0.40 24 1 -5 2.10 0.30 -24 1 5 2.30 0.50 -24 -1 5 1.60 0.40 -24 -1 5 1.60 0.40 -24 -1 5 2.00 0.50 -24 -1 5 1.50 0.40 24 1 -4 2.10 0.30 -24 1 4 1.70 0.50 -24 1 4 2.00 0.50 -24 -1 4 0.80 0.30 -24 -1 4 1.40 0.70 -24 -1 4 1.30 0.40 -24 -1 4 3.70 0.70 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 4903 _shelx_SHELXL_version_number '2014/7' _olex2_exptl_crystal_mounting_method 'Mitegen loop' _olex2_submission_original_sample_id DC1_RCSI _olex2_submission_special_instructions 'No special instructions were received'