data_3m _audit_creation_date 2015-09-13 _audit_creation_method ; Olex2 1.2 (compiled 2014.07.22 svn.r2960 for OlexSys, GUI svn.r4862) ; _shelxl_version_number 2014-1 _publ_contact_author_address ? _publ_contact_author_email ? _publ_contact_author_name '' _publ_contact_author_phone ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2008). Acta Cryst. A64, 112-122. ; _chemical_name_common ? _chemical_name_systematic ; ? ; _chemical_formula_moiety 'C19 H17 F3 O3' _chemical_formula_sum 'C19 H17 F3 O3' _chemical_formula_weight 350.32 _chemical_absolute_configuration rm _chemical_melting_point ? _chemical_oxdiff_formula 'C1 H1 O1 F1' loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'F' 'F' 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'monoclinic' _space_group_IT_number 4 _space_group_name_H-M_alt 'P 1 21 1' _space_group_name_Hall 'P 2yb' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' _cell_length_a 12.5614(2) _cell_length_b 5.24978(10) _cell_length_c 13.4122(3) _cell_angle_alpha 90 _cell_angle_beta 91.3092(16) _cell_angle_gamma 90 _cell_volume 884.23(3) _cell_formula_units_Z 2 _cell_measurement_reflns_used 6648 _cell_measurement_temperature 290.70(10) _cell_measurement_theta_max 71.1290 _cell_measurement_theta_min 4.7530 _shelx_estimated_absorpt_T_max ? _shelx_estimated_absorpt_T_min ? _exptl_absorpt_coefficient_mu 0.933 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.38905 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro, Agilent Technologies, Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET) (compiled Aug 13 2014,18:06:01) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'clear light colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier light _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.316 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description block _exptl_crystal_F_000 364 _exptl_crystal_size_max 0.13 _exptl_crystal_size_mid 0.12 _exptl_crystal_size_min 0.11 _exptl_special_details ; ? ; _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0302 _diffrn_reflns_av_unetI/netI 0.0210 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.987 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_k_max 6 _diffrn_reflns_limit_k_min -5 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_limit_l_min -16 _diffrn_reflns_number 9062 _diffrn_reflns_point_group_measured_fraction_full 0.916 _diffrn_reflns_point_group_measured_fraction_max 0.894 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 71.284 _diffrn_reflns_theta_min 4.769 _diffrn_ambient_environment air _diffrn_ambient_temperature 290.70(10) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 8.0243 _diffrn_detector_type EosS2 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.987 _diffrn_measurement_details ; #__ type_ start__ end____ width___ exp.time_ 1 omega 20.00 104.00 1.0000 1.0000 omega____ theta____ kappa____ phi______ frames - 36.7203 57.0000 -120.0000 84 #__ type_ start__ end____ width___ exp.time_ 2 omega 18.00 106.00 1.0000 1.0000 omega____ theta____ kappa____ phi______ frames - 36.7203 38.0000 -180.0000 88 #__ type_ start__ end____ width___ exp.time_ 3 omega 57.00 109.00 1.0000 1.0000 omega____ theta____ kappa____ phi______ frames - 36.7203 178.0000 60.0000 52 #__ type_ start__ end____ width___ exp.time_ 4 omega 57.00 109.00 1.0000 1.0000 omega____ theta____ kappa____ phi______ frames - 36.7203 178.0000 30.0000 52 #__ type_ start__ end____ width___ exp.time_ 5 omega 20.00 104.00 1.0000 1.0000 omega____ theta____ kappa____ phi______ frames - 36.7203 57.0000 60.0000 84 #__ type_ start__ end____ width___ exp.time_ 6 omega 1.00 76.00 1.0000 1.0000 omega____ theta____ kappa____ phi______ frames - 36.7203 -99.0000 -180.0000 75 #__ type_ start__ end____ width___ exp.time_ 7 omega 39.00 110.00 1.0000 5.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 -95.0000 -90.0000 71 #__ type_ start__ end____ width___ exp.time_ 8 omega 38.00 91.00 1.0000 5.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 -30.0000 150.0000 53 #__ type_ start__ end____ width___ exp.time_ 9 omega 41.00 126.00 1.0000 5.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 -61.0000 -150.0000 85 #__ type_ start__ end____ width___ exp.time_ 10 omega 38.00 91.00 1.0000 5.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 -30.0000 -180.0000 53 #__ type_ start__ end____ width___ exp.time_ 11 omega 40.00 98.00 1.0000 5.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 -45.0000 30.0000 58 #__ type_ start__ end____ width___ exp.time_ 12 omega 40.00 98.00 1.0000 5.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 -45.0000 120.0000 58 #__ type_ start__ end____ width___ exp.time_ 13 omega 87.00 178.00 1.0000 5.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 30.0000 0.0000 91 #__ type_ start__ end____ width___ exp.time_ 14 omega 39.00 110.00 1.0000 5.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 -95.0000 150.0000 71 #__ type_ start__ end____ width___ exp.time_ 15 omega 38.00 91.00 1.0000 5.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 -30.0000 60.0000 53 #__ type_ start__ end____ width___ exp.time_ 16 omega -35.00 66.00 1.0000 1.0000 omega____ theta____ kappa____ phi______ frames - 36.7203 -19.0000 -60.0000 101 #__ type_ start__ end____ width___ exp.time_ 17 omega -35.00 66.00 1.0000 1.0000 omega____ theta____ kappa____ phi______ frames - 36.7203 -19.0000 -180.0000 101 #__ type_ start__ end____ width___ exp.time_ 18 omega 20.00 104.00 1.0000 1.0000 omega____ theta____ kappa____ phi______ frames - 36.7203 57.0000 -30.0000 84 #__ type_ start__ end____ width___ exp.time_ 19 omega 10.00 104.00 1.0000 1.0000 omega____ theta____ kappa____ phi______ frames - 36.7203 77.0000 60.0000 94 #__ type_ start__ end____ width___ exp.time_ 20 omega -31.00 53.00 1.0000 1.0000 omega____ theta____ kappa____ phi______ frames - 36.7203 -57.0000 90.0000 84 #__ type_ start__ end____ width___ exp.time_ 21 omega 55.00 109.00 1.0000 1.0000 omega____ theta____ kappa____ phi______ frames - 36.7203 -178.0000 150.0000 54 #__ type_ start__ end____ width___ exp.time_ 22 omega 70.00 178.00 1.0000 5.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 15.0000 -150.0000 108 #__ type_ start__ end____ width___ exp.time_ 23 omega 91.00 176.00 1.0000 5.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 45.0000 120.0000 85 #__ type_ start__ end____ width___ exp.time_ 24 omega 39.00 110.00 1.0000 5.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 -95.0000 60.0000 71 #__ type_ start__ end____ width___ exp.time_ 25 omega 87.00 178.00 1.0000 5.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 30.0000 -90.0000 91 #__ type_ start__ end____ width___ exp.time_ 26 omega 87.00 178.00 1.0000 5.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 30.0000 90.0000 91 #__ type_ start__ end____ width___ exp.time_ 27 omega 40.00 98.00 1.0000 5.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 -45.0000 -60.0000 58 #__ type_ start__ end____ width___ exp.time_ 28 omega 10.00 104.00 1.0000 1.0000 omega____ theta____ kappa____ phi______ frames - 36.7203 77.0000 -90.0000 94 #__ type_ start__ end____ width___ exp.time_ 29 omega 20.00 104.00 1.0000 1.0000 omega____ theta____ kappa____ phi______ frames - 36.7203 57.0000 -180.0000 84 #__ type_ start__ end____ width___ exp.time_ 30 omega 1.00 60.00 1.0000 1.0000 omega____ theta____ kappa____ phi______ frames - 36.7203 -99.0000 -60.0000 59 #__ type_ start__ end____ width___ exp.time_ 31 omega 10.00 104.00 1.0000 1.0000 omega____ theta____ kappa____ phi______ frames - 36.7203 77.0000 -30.0000 94 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at zero, EosS2' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_UB_11 -0.0037661000 _diffrn_orient_matrix_UB_12 -0.0948220000 _diffrn_orient_matrix_UB_13 -0.1087843000 _diffrn_orient_matrix_UB_21 -0.1121708000 _diffrn_orient_matrix_UB_22 0.1146508000 _diffrn_orient_matrix_UB_23 -0.0143924000 _diffrn_orient_matrix_UB_31 0.0495577000 _diffrn_orient_matrix_UB_32 0.2527979000 _diffrn_orient_matrix_UB_33 -0.0341694000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_source 'sealed X-ray tube' _diffrn_source_type 'SuperNova (Cu) X-ray Source' _reflns_Friedel_coverage 0.622 _reflns_Friedel_fraction_full 0.812 _reflns_Friedel_fraction_max 0.775 _reflns_number_gt 2983 _reflns_number_total 3088 _reflns_odcompleteness_completeness 99.83 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 66.97 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement ; CrysAlisPro, Agilent Technologies, Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET) (compiled Aug 13 2014,18:06:01) ; _computing_data_collection ; CrysAlisPro, Agilent Technologies, Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET) (compiled Aug 13 2014,18:06:01) ; _computing_data_reduction ; CrysAlisPro, Agilent Technologies, Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET) (compiled Aug 13 2014,18:06:01) ; _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2008)' _computing_structure_solution 'ShelXS (Sheldrick, 2008)' _refine_diff_density_max 0.390 _refine_diff_density_min -0.173 _refine_diff_density_rms 0.041 _refine_ls_abs_structure_details ; Flack x determined using 1126 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.04(9) _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.047 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 227 _refine_ls_number_reflns 3088 _refine_ls_number_restraints 1 _refine_ls_R_factor_all 0.0481 _refine_ls_R_factor_gt 0.0472 _refine_ls_restrained_S_all 1.047 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0815P)^2^+0.1200P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1321 _refine_ls_wR_factor_ref 0.1334 _refine_special_details ; ? ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C11(H11) 2.b Secondary CH2 refined with riding coordinates: C10(H10A,H10B), C22(H22A,H22B) 2.c Aromatic/amide H refined with riding coordinates: C20(H20), C19(H19), C8(H8), C7(H7), C2(H2), C4(H4), C6(H6), C3(H3), C5(H5) 2.d Idealised Me refined as rotating group: C25(H25A,H25B,H25C) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O17 O 0.13573(14) 0.2287(4) 0.85864(13) 0.0509(4) Uani 1 1 d . . . . . C18 C 0.19333(19) 0.3830(5) 0.92262(17) 0.0463(5) Uani 1 1 d . . . . . F13 F 0.48054(15) 0.3451(7) 0.88084(19) 0.1016(9) Uani 1 1 d . . . . . O16 O 0.2570(2) 0.0115(5) 1.10458(18) 0.0721(6) Uani 1 1 d . . . . . C10 C 0.3428(2) 0.3869(6) 1.0488(2) 0.0558(6) Uani 1 1 d . . . . . H10A H 0.4198 0.3742 1.0550 0.067 Uiso 1 1 calc R . . . . H10B H 0.3232 0.5630 1.0602 0.067 Uiso 1 1 calc R . . . . F14 F 0.38281(18) 0.6737(5) 0.8684(2) 0.0961(8) Uani 1 1 d . . . . . C11 C 0.30670(19) 0.3078(6) 0.9430(2) 0.0516(6) Uani 1 1 d . . . . . H11 H 0.3114 0.1218 0.9385 0.062 Uiso 1 1 calc R . . . . F15 F 0.35143(19) 0.3510(7) 0.77418(15) 0.1045(9) Uani 1 1 d . . . . . C21 C 0.03527(19) 0.3334(6) 0.85146(18) 0.0496(6) Uani 1 1 d . . . . . C20 C 0.0302(2) 0.5411(6) 0.9080(2) 0.0527(6) Uani 1 1 d . . . . . H20 H -0.0292 0.6445 0.9160 0.063 Uiso 1 1 calc R . . . . C9 C 0.2924(2) 0.2193(6) 1.1269(2) 0.0571(7) Uani 1 1 d . . . . . C19 C 0.1330(2) 0.5758(6) 0.95427(19) 0.0510(6) Uani 1 1 d . . . . . H19 H 0.1537 0.7060 0.9976 0.061 Uiso 1 1 calc R . . . . C22 C -0.0425(2) 0.2020(7) 0.7836(2) 0.0623(7) Uani 1 1 d . . . . . H22A H -0.1143 0.2500 0.8011 0.075 Uiso 1 1 calc R . . . . H22B H -0.0357 0.0192 0.7920 0.075 Uiso 1 1 calc R . . . . C8 C 0.2868(3) 0.3003(7) 1.2315(2) 0.0661(8) Uani 1 1 d . . . . . H8 H 0.2500 0.1965 1.2751 0.079 Uiso 1 1 calc R . . . . C7 C 0.3301(2) 0.5092(7) 1.2676(2) 0.0634(7) Uani 1 1 d . . . . . H7 H 0.3659 0.6122 1.2230 0.076 Uiso 1 1 calc R . . . . C12 C 0.3791(3) 0.4202(8) 0.8662(3) 0.0711(9) Uani 1 1 d . . . . . C23 C -0.0240(3) 0.2711(7) 0.6760(2) 0.0679(8) Uani 1 1 d . . . . . O24 O -0.0616(4) 0.4633(8) 0.6416(2) 0.1205(13) Uani 1 1 d . . . . . C1 C 0.3278(3) 0.5973(8) 1.3724(2) 0.0700(9) Uani 1 1 d . . . . . C2 C 0.3883(3) 0.8023(9) 1.3979(3) 0.0827(11) Uani 1 1 d . . . . . H2 H 0.4293 0.8816 1.3502 0.099 Uiso 1 1 calc R . . . . C4 C 0.3288(5) 0.7789(11) 1.5667(3) 0.1086(17) Uani 1 1 d . . . . . H4 H 0.3296 0.8409 1.6316 0.130 Uiso 1 1 calc R . . . . C6 C 0.2671(4) 0.4827(10) 1.4448(3) 0.0946(13) Uani 1 1 d . . . . . H6 H 0.2249 0.3425 1.4285 0.113 Uiso 1 1 calc R . . . . C25 C 0.0438(5) 0.0934(15) 0.6202(4) 0.128(2) Uani 1 1 d . . . . . H25A H 0.1108 0.0726 0.6552 0.192 Uiso 1 1 calc GR . . . . H25B H 0.0558 0.1609 0.5549 0.192 Uiso 1 1 calc GR . . . . H25C H 0.0089 -0.0687 0.6144 0.192 Uiso 1 1 calc GR . . . . C3 C 0.3891(4) 0.8944(11) 1.4950(4) 0.1033(15) Uani 1 1 d . . . . . H3 H 0.4308 1.0351 1.5118 0.124 Uiso 1 1 calc R . . . . C5 C 0.2689(5) 0.5767(13) 1.5417(4) 0.1166(18) Uani 1 1 d . . . . . H5 H 0.2281 0.4981 1.5898 0.140 Uiso 1 1 calc R . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O17 0.0530(9) 0.0479(11) 0.0518(9) -0.0072(8) -0.0008(7) -0.0004(8) C18 0.0493(12) 0.0445(14) 0.0452(11) -0.0019(11) 0.0025(9) -0.0013(10) F13 0.0559(10) 0.131(2) 0.1190(17) 0.0122(17) 0.0267(10) 0.0241(13) O16 0.0837(14) 0.0596(14) 0.0726(13) 0.0005(11) -0.0026(11) -0.0145(12) C10 0.0475(12) 0.0545(17) 0.0652(15) -0.0047(14) -0.0067(11) -0.0016(12) F14 0.0808(14) 0.0847(18) 0.1243(19) 0.0259(15) 0.0317(12) -0.0060(12) C11 0.0477(12) 0.0491(16) 0.0581(14) -0.0035(12) 0.0034(10) 0.0057(11) F15 0.0990(15) 0.149(3) 0.0664(12) -0.0002(15) 0.0238(10) 0.0060(17) C21 0.0462(12) 0.0557(17) 0.0467(12) 0.0070(11) 0.0009(9) -0.0034(11) C20 0.0474(12) 0.0549(16) 0.0559(13) 0.0026(13) 0.0035(10) 0.0052(12) C9 0.0507(13) 0.0607(18) 0.0593(14) -0.0034(14) -0.0097(11) 0.0104(13) C19 0.0499(13) 0.0504(16) 0.0527(13) -0.0057(11) 0.0034(10) 0.0010(11) C22 0.0591(15) 0.069(2) 0.0587(15) 0.0050(14) -0.0040(12) -0.0160(14) C8 0.0681(16) 0.061(2) 0.0690(17) 0.0049(15) -0.0056(13) -0.0028(15) C7 0.0596(15) 0.0626(19) 0.0676(17) 0.0045(15) -0.0043(13) -0.0004(14) C12 0.0570(16) 0.084(3) 0.0733(19) -0.0012(18) 0.0140(14) 0.0095(16) C23 0.0796(19) 0.068(2) 0.0561(16) -0.0025(15) -0.0090(13) -0.0156(16) O24 0.174(4) 0.103(3) 0.084(2) 0.0265(18) -0.016(2) 0.015(2) C1 0.0775(19) 0.070(2) 0.0615(16) -0.0010(16) -0.0105(14) 0.0147(17) C2 0.091(2) 0.082(3) 0.074(2) -0.0040(19) -0.0133(17) -0.001(2) C4 0.158(5) 0.100(4) 0.067(2) -0.021(2) -0.012(3) 0.020(3) C6 0.114(3) 0.086(3) 0.084(2) -0.012(2) 0.001(2) -0.010(2) C25 0.152(5) 0.146(6) 0.087(3) -0.036(4) 0.031(3) -0.014(4) C3 0.128(4) 0.086(3) 0.094(3) -0.022(3) -0.027(3) 0.001(3) C5 0.166(5) 0.112(4) 0.072(2) -0.007(3) 0.016(3) -0.009(4) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O17 C18 1.374(3) . ? O17 C21 1.378(3) . ? C18 C11 1.497(3) . ? C18 C19 1.340(4) . ? F13 C12 1.343(4) . ? O16 C9 1.213(4) . ? C10 C11 1.537(4) . ? C10 C9 1.517(4) . ? F14 C12 1.332(5) . ? C11 C12 1.511(4) . ? F15 C12 1.325(4) . ? C21 C20 1.331(4) . ? C21 C22 1.489(4) . ? C20 C19 1.431(4) . ? C9 C8 1.469(4) . ? C22 C23 1.511(4) . ? C8 C7 1.312(5) . ? C7 C1 1.480(5) . ? C23 O24 1.202(5) . ? C23 C25 1.478(7) . ? C1 C2 1.357(6) . ? C1 C6 1.386(6) . ? C2 C3 1.388(6) . ? C4 C3 1.379(8) . ? C4 C5 1.339(8) . ? C6 C5 1.390(7) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C18 O17 C21 106.1(2) . . ? O17 C18 C11 116.4(2) . . ? C19 C18 O17 110.5(2) . . ? C19 C18 C11 133.2(2) . . ? C9 C10 C11 111.2(2) . . ? C18 C11 C10 110.9(2) . . ? C18 C11 C12 111.0(2) . . ? C12 C11 C10 110.8(3) . . ? O17 C21 C22 116.4(3) . . ? C20 C21 O17 110.1(2) . . ? C20 C21 C22 133.5(3) . . ? C21 C20 C19 107.3(2) . . ? O16 C9 C10 120.5(3) . . ? O16 C9 C8 118.1(3) . . ? C8 C9 C10 121.4(3) . . ? C18 C19 C20 106.1(2) . . ? C21 C22 C23 111.0(2) . . ? C7 C8 C9 124.5(3) . . ? C8 C7 C1 126.5(3) . . ? F13 C12 C11 111.7(3) . . ? F14 C12 F13 104.9(3) . . ? F14 C12 C11 113.3(3) . . ? F15 C12 F13 106.5(3) . . ? F15 C12 F14 107.7(4) . . ? F15 C12 C11 112.2(3) . . ? O24 C23 C22 120.0(4) . . ? O24 C23 C25 124.2(4) . . ? C25 C23 C22 115.8(4) . . ? C2 C1 C7 117.7(4) . . ? C2 C1 C6 118.8(4) . . ? C6 C1 C7 123.6(4) . . ? C1 C2 C3 120.4(4) . . ? C5 C4 C3 119.3(4) . . ? C1 C6 C5 120.2(5) . . ? C4 C3 C2 120.5(5) . . ? C4 C5 C6 120.8(5) . . ? _shelx_res_file ; TITL cyc0912 in P21 #4 CELL 1.54184 12.561443 5.249781 13.412165 90 91.3092 90 ZERR 2 0.000208 0.000104 0.000258 0 0.0016 0 LATT -1 SYMM -X,0.5+Y,-Z SFAC C H F O UNIT 38 34 6 6 L.S. 20 PLAN 20 REM reset to P21 #4 BOND fmap 2 acta REM D:/data/cyc0912/struct/olex2_cyc0912/cyc0912.hkl WGHT 0.081500 0.120000 FVAR 13.69058 O17 4 0.135729 0.228722 0.858644 11.00000 0.05297 0.04789 = 0.05179 -0.00716 -0.00076 -0.00044 C18 1 0.193333 0.382964 0.922624 11.00000 0.04933 0.04454 = 0.04522 -0.00191 0.00252 -0.00134 F13 3 0.480536 0.345094 0.880845 11.00000 0.05595 0.13102 = 0.11897 0.01216 0.02674 0.02409 O16 4 0.256972 0.011468 1.104578 11.00000 0.08373 0.05964 = 0.07263 0.00054 -0.00261 -0.01450 C10 1 0.342844 0.386925 1.048825 11.00000 0.04747 0.05446 = 0.06522 -0.00469 -0.00667 -0.00161 AFIX 23 H10A 2 0.419751 0.374162 1.054955 11.00000 -1.20000 H10B 2 0.323179 0.563037 1.060221 11.00000 -1.20000 AFIX 0 F14 3 0.382808 0.673696 0.868420 11.00000 0.08076 0.08471 = 0.12428 0.02586 0.03166 -0.00600 C11 1 0.306702 0.307800 0.943001 11.00000 0.04767 0.04911 = 0.05811 -0.00349 0.00339 0.00572 AFIX 13 H11 2 0.311368 0.121832 0.938490 11.00000 -1.20000 AFIX 0 F15 3 0.351433 0.351027 0.774179 11.00000 0.09896 0.14912 = 0.06642 -0.00022 0.02379 0.00604 C21 1 0.035273 0.333428 0.851461 11.00000 0.04621 0.05575 = 0.04675 0.00704 0.00091 -0.00335 C20 1 0.030168 0.541130 0.908027 11.00000 0.04743 0.05495 = 0.05594 0.00262 0.00347 0.00515 AFIX 43 H20 2 -0.029154 0.644497 0.916025 11.00000 -1.20000 AFIX 0 C9 1 0.292416 0.219323 1.126906 11.00000 0.05072 0.06067 = 0.05929 -0.00344 -0.00973 0.01042 C19 1 0.132976 0.575839 0.954274 11.00000 0.04989 0.05037 = 0.05271 -0.00568 0.00337 0.00102 AFIX 43 H19 2 0.153693 0.706018 0.997558 11.00000 -1.20000 AFIX 0 C22 1 -0.042518 0.202033 0.783604 11.00000 0.05909 0.06869 = 0.05874 0.00498 -0.00399 -0.01601 AFIX 23 H22A 2 -0.114295 0.250024 0.801068 11.00000 -1.20000 H22B 2 -0.035679 0.019186 0.791954 11.00000 -1.20000 AFIX 0 C8 1 0.286791 0.300349 1.231516 11.00000 0.06809 0.06096 = 0.06900 0.00489 -0.00556 -0.00284 AFIX 43 H8 2 0.250002 0.196481 1.275097 11.00000 -1.20000 AFIX 0 C7 1 0.330129 0.509249 1.267646 11.00000 0.05965 0.06257 = 0.06759 0.00449 -0.00431 -0.00037 AFIX 43 H7 2 0.365865 0.612219 1.222980 11.00000 -1.20000 AFIX 0 C12 1 0.379148 0.420228 0.866156 11.00000 0.05696 0.08357 = 0.07333 -0.00123 0.01401 0.00946 C23 1 -0.023980 0.271120 0.676027 11.00000 0.07955 0.06767 = 0.05612 -0.00247 -0.00904 -0.01565 O24 4 -0.061580 0.463330 0.641630 11.00000 0.17406 0.10286 = 0.08377 0.02648 -0.01580 0.01456 C1 1 0.327805 0.597302 1.372377 11.00000 0.07748 0.07038 = 0.06150 -0.00095 -0.01046 0.01471 C2 1 0.388254 0.802337 1.397943 11.00000 0.09130 0.08187 = 0.07429 -0.00405 -0.01328 -0.00059 AFIX 43 H2 2 0.429325 0.881636 1.350183 11.00000 -1.20000 AFIX 0 C4 1 0.328758 0.778944 1.566656 11.00000 0.15822 0.09976 = 0.06704 -0.02112 -0.01177 0.02043 AFIX 43 H4 2 0.329566 0.840850 1.631637 11.00000 -1.20000 AFIX 0 C6 1 0.267062 0.482741 1.444795 11.00000 0.11351 0.08615 = 0.08403 -0.01217 0.00109 -0.01039 AFIX 43 H6 2 0.224906 0.342516 1.428482 11.00000 -1.20000 AFIX 0 C25 1 0.043808 0.093384 0.620219 11.00000 0.15247 0.14562 = 0.08653 -0.03604 0.03131 -0.01429 AFIX 137 H25A 2 0.110800 0.072581 0.655154 11.00000 -1.50000 H25B 2 0.055796 0.160860 0.554904 11.00000 -1.50000 H25C 2 0.008852 -0.068716 0.614355 11.00000 -1.50000 AFIX 0 C3 1 0.389148 0.894436 1.494985 11.00000 0.12843 0.08595 = 0.09405 -0.02179 -0.02669 0.00069 AFIX 43 H3 2 0.430812 1.035145 1.511775 11.00000 -1.20000 AFIX 0 C5 1 0.268927 0.576683 1.541708 11.00000 0.16620 0.11249 = 0.07182 -0.00741 0.01614 -0.00934 AFIX 43 H5 2 0.228107 0.498070 1.589828 11.00000 -1.20000 AFIX 0 HKLF 4 REM cyc0912 in P21 #4 REM R1 = 0.0472 for 2983 Fo > 4sig(Fo) and 0.0481 for all 3088 data REM 227 parameters refined using 1 restraints END WGHT 0.0815 0.1200 REM Highest difference peak 0.390, deepest hole -0.173, 1-sigma level 0.041 Q1 1 0.2866 0.3708 1.3019 11.00000 0.05 0.39 Q2 1 0.3334 0.4187 1.2007 11.00000 0.05 0.30 Q3 1 0.2945 0.4622 1.3850 11.00000 0.05 0.14 Q4 1 0.3754 0.7719 1.0195 11.00000 0.05 0.13 Q5 1 0.3117 0.3751 1.1245 11.00000 0.05 0.12 Q6 1 0.4628 0.1955 0.8404 11.00000 0.05 0.12 Q7 1 0.3575 0.7695 1.2042 11.00000 0.05 0.12 Q8 1 0.2237 0.4032 1.4801 11.00000 0.05 0.12 Q9 1 0.2759 0.1141 1.3040 11.00000 0.05 0.11 Q10 1 0.3054 -0.1322 0.9418 11.00000 0.05 0.11 Q11 1 0.0903 -0.3519 0.5792 11.00000 0.05 0.10 Q12 1 0.2602 0.2519 1.4368 11.00000 0.05 0.10 Q13 1 -0.0874 0.0247 0.8169 11.00000 0.05 0.10 Q14 1 0.3187 0.6409 1.0988 11.00000 0.05 0.10 Q15 1 -0.1730 0.0337 0.8077 11.00000 0.05 0.10 Q16 1 0.3441 0.5912 0.8103 11.00000 0.05 0.10 Q17 1 0.4031 0.3728 0.6905 11.00000 0.05 0.10 Q18 1 0.3122 0.1951 0.7630 11.00000 0.05 0.10 Q19 1 0.4690 0.5008 1.2451 11.00000 0.05 0.10 Q20 1 0.0133 0.4069 0.6216 11.00000 0.05 0.10 ; _shelx_res_checksum 29942 _shelx_hkl_file ; 0 -4 0 7331.01 697.511 29 0 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164.681 22 0 -3 -13 287.567 53.4205 22 0 -3 -14 771.004 72.7945 22 0 -2 0 114678. 2000.95 5 0 -2 0 119265. 2487.33 19 0 -2 1 42690.2 1261.47 5 0 -2 -1 43122.4 1140.45 19 0 -2 -1 42228.5 1171.44 2 0 -2 1 43625.2 1532.87 19 0 -2 -2 67516.3 1362.94 16 0 -2 -2 65429.2 1595.27 29 0 -2 2 64710.1 2116.67 19 0 -2 2 65031.7 1867.50 5 0 -2 -2 60641.8 1474.17 2 0 -2 3 71223.3 1441.78 31 0 -2 -3 72176.2 1517.63 16 0 -2 3 65401.1 2147.69 5 0 -2 -3 68574.4 1561.74 2 0 -2 -3 69152.1 1631.57 29 0 -2 3 68165.3 2364.76 19 0 -2 4 12429.0 965.129 5 0 -2 4 12859.9 1060.19 19 0 -2 -4 14655.6 633.134 29 0 -2 -4 14192.0 617.247 16 0 -2 -5 17620.4 683.864 29 0 -2 5 16222.8 1273.44 19 0 -2 -5 17018.4 723.427 16 0 -2 -5 17209.6 701.031 2 0 -2 5 14540.4 1170.54 5 0 -2 -6 11299.8 551.753 29 0 -2 -6 10747.2 583.186 2 0 -2 6 10129.4 1081.75 19 0 -2 6 8655.71 979.574 5 0 -2 -6 11666.2 619.669 16 0 -2 -7 32804.5 1045.08 29 0 -2 7 28484.1 1972.68 19 0 -2 -7 32627.5 1146.92 2 0 -2 7 27889.0 1918.03 5 0 -2 -7 32996.7 1171.51 16 0 -2 -8 863.504 164.711 29 0 -2 -8 793.802 183.330 16 0 -2 -8 777.525 183.089 2 0 -2 8 694.081 301.541 5 0 -2 8 724.959 315.278 19 0 -2 -9 1692.84 295.654 16 0 -2 -9 1330.51 114.586 22 0 -2 -10 1386.83 123.505 22 0 -2 -11 41611.8 862.789 22 0 -2 -12 2147.98 158.429 22 0 -2 -13 2662.18 171.841 22 0 -2 -14 2172.59 144.134 22 0 -2 -15 822.406 76.8223 22 0 -1 0 5.09670 25.5416 19 0 -1 0 1.47070 23.3487 5 0 -1 1 470315. 6838.09 5 0 -1 -1 476888. 6365.91 19 0 -1 2 564105. 7532.03 17 0 -1 2 565928. 8506.02 5 0 -1 2 556965. 7659.00 31 0 -1 -2 556231. 7747.50 16 0 -1 2 581663. 7555.54 18 0 -1 3 288925. 5301.69 5 0 -1 3 301004. 4319.31 18 0 -1 3 296033. 4366.52 31 0 -1 -3 293822. 4367.21 16 0 -1 4 54139.0 1939.41 5 0 -1 4 52167.5 1292.41 31 0 -1 -4 54947.5 1250.59 16 0 -1 -4 57945.1 1134.14 29 0 -1 -4 58154.2 1182.10 2 0 -1 4 58953.4 1340.16 18 0 -1 -5 130085. 2225.47 2 0 -1 5 123659. 2486.34 18 0 -1 -5 120478. 2082.05 29 0 -1 5 114520. 2420.24 31 0 -1 5 108001. 3276.36 5 0 -1 5 125832. 3373.05 19 0 -1 -5 125806. 2299.54 16 0 -1 -6 86240.2 1831.61 16 0 -1 -6 76293.1 1697.94 2 0 -1 6 82601.0 2073.64 18 0 -1 6 81579.6 2049.51 31 0 -1 6 84651.9 2959.80 5 0 -1 6 86199.8 2877.51 19 0 -1 -6 79238.4 1587.77 29 0 -1 7 15308.0 1290.95 5 0 -1 7 14560.7 867.557 18 0 -1 7 15731.3 1261.14 19 0 -1 7 14683.6 862.596 31 0 -1 -7 15117.8 596.801 29 0 -1 -7 15171.7 686.826 2 0 -1 -7 15873.5 738.852 16 0 -1 -7 15427.4 533.273 1 0 -1 -8 29416.4 1063.86 2 0 -1 8 26792.7 1309.54 31 0 -1 8 27529.9 1899.25 5 0 -1 -8 28702.8 922.339 29 0 -1 8 27937.6 1823.80 19 0 -1 -8 28107.9 1099.57 16 0 -1 9 452.900 281.822 5 0 -1 -9 288.693 121.290 16 0 -1 9 354.218 164.095 31 0 -1 -9 273.542 98.1464 29 0 -1 -9 393.015 129.846 2 0 -1 9 251.889 204.269 19 0 -1 -10 2964.63 335.511 29 0 -1 10 2298.78 594.177 5 0 -1 -10 3052.60 182.500 23 0 -1 -10 3012.45 172.950 22 0 -1 10 3057.97 649.720 19 0 -1 -11 160.568 45.9517 22 0 -1 -11 70.4507 34.4010 23 0 -1 -12 13632.6 431.061 22 0 -1 -12 14424.8 459.046 23 0 -1 -13 780.201 98.3301 23 0 -1 -13 791.655 94.1566 22 0 -1 -14 189.539 47.1392 22 0 -1 -15 1689.93 118.274 22 0 0 -2 66609.1 973.020 1 0 0 -3 307548. 4138.18 1 0 0 3 307839. 4730.14 18 0 0 -4 659782. 9105.57 2 0 0 -4 670358. 8817.10 1 0 0 -4 672114. 8750.31 4 0 0 -4 660898. 8987.07 29 0 0 4 644020. 9587.19 31 0 0 4 673320. 9675.52 18 0 0 -5 61859.1 1383.45 16 0 0 5 61862.2 1745.40 18 0 0 -5 63597.1 1000.51 4 0 0 -5 61469.2 1063.15 1 0 0 -5 63633.6 1356.44 2 0 0 -5 65886.9 1413.65 21 0 0 -5 63509.2 1249.82 29 0 0 -6 99991.6 2016.45 16 0 0 6 99005.9 2683.43 19 0 0 6 96052.4 2940.61 5 0 0 -6 100754. 1981.35 21 0 0 6 84130.8 2302.65 31 0 0 -6 90363.0 1893.84 2 0 0 6 95922.0 2456.72 18 0 0 -6 92756.8 1776.87 29 0 0 7 16928.4 1255.56 5 0 0 -7 17463.7 771.297 16 0 0 -7 15194.2 617.941 29 0 0 7 17436.4 1123.08 19 0 0 7 15720.3 958.877 31 0 0 -7 17405.1 746.235 21 0 0 7 16952.5 1016.54 18 0 0 8 54574.9 2497.34 5 0 0 -8 54672.4 1592.59 16 0 0 8 51885.7 2025.64 18 0 0 8 50796.9 1969.31 31 0 0 8 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1478.41 16 3 -1 3 63018.2 2081.12 19 3 -1 3 64245.3 1672.26 17 -3 -1 -3 69814.1 1278.59 29 -3 -1 -4 8339.84 422.071 2 -3 -1 -4 7506.15 349.869 29 -3 -1 -4 7754.15 457.923 16 3 -1 4 7903.80 738.914 19 3 -1 4 8134.85 720.984 5 3 -1 4 7641.02 536.894 17 -3 -1 -4 8105.83 378.943 1 -3 -1 -5 10408.0 520.990 2 3 -1 5 10585.2 928.512 19 3 -1 5 10387.2 911.931 5 -3 -1 -5 10326.8 577.738 16 -3 -1 -5 10938.7 456.040 29 3 -1 5 9441.52 659.131 17 -3 -1 -5 10159.3 451.113 1 -3 -1 -6 56562.6 1490.07 2 3 -1 6 58750.9 2469.21 5 -3 -1 -6 61003.8 1368.26 29 3 -1 6 53944.7 2385.86 19 -3 -1 -6 59704.9 1663.15 16 3 -1 6 53525.1 1836.27 17 -3 -1 -6 58725.3 1333.39 1 -3 -1 -7 13821.5 626.427 29 -3 -1 -7 12943.0 766.727 16 -3 -1 -7 13483.3 589.800 1 3 -1 7 13315.3 1220.63 19 3 -1 7 14431.4 1284.62 5 3 -1 7 11351.2 857.740 17 -3 -1 -8 13054.0 611.837 1 3 -1 8 14453.3 1371.07 5 -3 -1 -8 13437.1 848.629 16 -3 -1 -8 13318.3 668.149 29 3 -1 8 14712.0 1356.24 19 3 -1 8 10936.8 903.309 17 -3 -1 -9 2269.33 367.782 16 3 -1 9 1905.08 529.708 5 3 -1 9 2402.07 561.891 19 -3 -1 -9 2112.37 280.576 29 -3 -1 -10 774.158 96.4794 22 -3 -1 -11 2295.33 171.304 22 -3 -1 -12 2015.06 159.996 22 -3 -1 -13 1982.63 153.783 22 -3 -1 -14 874.979 96.1613 22 -3 -1 -15 650.645 72.9775 22 3 0 -16 88.2664 28.0705 27 -3 0 15 60.9268 49.3733 13 3 0 -15 40.4560 23.8340 27 3 0 -14-4.13905 23.6841 27 -3 0 14 50.1791 66.2752 13 3 0 -14 8.11147 28.1096 23 3 0 -13 3608.60 241.754 27 3 0 -13 3241.98 215.199 23 -3 0 13 3513.46 295.371 13 -3 0 12 1412.44 188.581 13 3 0 -12 1307.46 133.996 23 -3 0 11 7897.98 448.044 13 3 0 -11 7564.49 344.226 9 3 0 -11 7349.39 321.453 23 3 0 -10 32108.3 739.564 23 3 0 -10 35428.0 1514.98 3 -3 0 10 32983.2 960.113 13 3 0 -10 34004.7 803.794 9 -3 0 9 3786.47 570.639 31 -3 0 9 4357.84 625.906 18 3 0 -9 3989.80 428.602 16 -3 0 8 224.254 139.240 18 3 0 -8 189.219 97.5825 16 3 0 -8 232.026 81.9976 2 -3 0 8 133.383 100.269 31 3 0 -7 2765.92 263.329 2 3 0 -7 2935.25 249.420 4 -3 0 7 2985.02 436.624 18 -3 0 7 2771.27 402.631 31 3 0 -7 2684.02 305.915 16 -3 0 6 53314.0 1724.55 31 3 0 -6 51257.2 1198.37 2 -3 0 6 50569.8 1303.18 28 3 0 -6 55075.6 1202.33 4 3 0 -6 54375.4 1476.07 30 3 0 -6 52096.5 1102.04 29 3 0 -6 54033.3 1466.96 16 -3 0 5 177114. 3599.44 18 3 0 -5 182057. 2875.05 2 -3 0 5 185510. 3589.77 31 -3 0 5 176130. 3098.36 28 3 0 -5 186006. 2752.91 29 3 0 -5 192118. 3296.48 30 3 0 -5 181745. 3258.00 16 -3 0 4 18288.8 655.157 28 3 0 -4 18042.5 435.825 29 3 0 -4 18114.4 512.251 2 -3 0 4 17859.7 789.791 31 -3 0 4 17344.6 397.349 20 3 0 -4 18589.6 708.346 16 -3 0 4 17581.8 794.226 18 3 0 -4 19341.7 733.694 30 -3 0 3 69765.9 1196.63 20 -3 0 3 63990.5 1549.03 31 3 0 -3 67319.7 1158.89 2 -3 0 3 63948.7 1564.06 18 3 0 -3 66525.7 1483.66 30 3 0 -3 72553.8 1053.71 29 -3 0 3 67099.3 1378.06 28 -3 0 2 955911. 13109.3 1 3 0 -2 995004. 12997.3 2 -3 0 2 999999. 13051.4 20 3 0 -2 971934. 13487.1 17 -3 0 2 981431. 13203.4 28 3 0 -2 974332. 13364.1 30 -3 0 2 984136. 13364.0 31 -3 0 1 507545. 7001.93 1 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12908.3 1070.32 17 3 0 9 31422.5 1959.03 5 -3 0 -9 27663.3 1370.63 16 3 0 9 28458.6 1729.13 17 3 0 10 7550.74 429.382 13 -3 0 -10 7211.04 330.905 27 3 0 11 362.615 88.9844 13 -3 0 -11 288.390 58.0738 22 -3 0 -11 347.826 74.9119 27 -3 0 -12 1397.62 141.397 27 3 0 12 1327.67 177.949 13 -3 0 -12 1100.33 118.188 22 -3 0 -13 77.1612 33.4753 27 -3 0 -13 47.7211 22.5464 22 3 0 13 100.711 49.9786 13 3 0 14 629.723 114.425 13 -3 0 -14 575.989 78.0241 22 -3 0 -15 441.197 59.9360 22 3 0 15 482.202 81.6425 13 3 1 -16 355.916 51.2306 27 3 1 -15 359.135 63.4229 27 -3 1 15 430.053 85.5182 13 -3 1 14 284.911 82.1852 13 3 1 -14 277.992 63.4060 27 3 1 -13 918.679 121.326 27 -3 1 13 892.929 150.772 13 -3 1 12 4185.62 329.436 13 3 1 -12 3740.58 230.779 23 3 1 -12 4176.22 267.968 27 3 1 -11 5092.27 270.897 23 3 1 -11 5668.17 286.411 9 3 1 -11 5834.93 316.763 27 -3 1 11 5607.64 379.093 13 3 1 -10 19029.8 554.965 9 3 1 -10 20179.7 570.093 7 3 1 -10 16670.3 510.734 23 -3 1 10 17263.7 672.363 13 3 1 -9 4700.83 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70.4753 27 3 2 14 339.588 75.0711 13 -3 2 -15 233.710 41.4967 24 3 2 15 266.763 53.9164 13 -3 2 -15 346.279 51.3818 27 -3 3 13 1048.35 121.498 13 3 3 -13 1109.20 103.803 27 -3 3 12 3809.74 264.471 13 3 3 -12 3441.21 210.373 27 -3 3 11 711.862 107.066 15 -3 3 11 528.285 107.191 13 3 3 -11 504.051 89.5000 27 -3 3 10 2857.78 209.727 15 3 3 -10 3058.51 220.778 7 -3 3 10 2534.69 246.295 13 -3 3 9 28332.6 747.645 15 3 3 -9 29271.8 782.357 7 -3 3 8 18415.1 570.942 15 3 3 -8 18731.3 601.933 7 -3 3 8 18206.1 662.887 25 -3 3 7 7518.52 390.858 25 3 3 -7 7350.97 355.086 7 -3 3 7 7779.64 340.654 15 -3 3 6 3056.86 628.645 6 3 3 -6 3618.54 236.753 7 -3 3 6 3885.51 262.011 11 -3 3 6 3438.85 450.734 20 -3 3 6 3386.79 253.956 25 -3 3 6 3072.80 205.147 15 -3 3 5 2505.15 384.371 20 -3 3 5 2347.03 522.682 6 -3 3 4 13877.2 1193.80 6 -3 3 4 12382.7 869.081 20 3 3 -3 15049.6 912.962 6 -3 3 3 14302.0 951.236 20 -3 3 3 15247.4 1152.39 6 -3 3 2 4041.35 535.060 6 -3 3 2 4658.57 538.905 20 3 3 -2 4428.46 480.211 6 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79.4544 27 3 3 12 395.123 87.0056 13 -3 3 -12 490.655 91.1899 24 3 3 12 553.101 78.4487 12 3 3 13 1698.04 149.205 13 -3 3 -13 1856.73 141.879 24 -3 3 -13 1932.87 144.465 27 -3 3 -14 2159.43 123.799 24 -3 4 12 641.342 62.4918 12 -3 4 11 1177.94 110.702 15 -3 4 11 999.426 96.1644 12 -3 4 10 976.139 107.572 15 3 4 -9 1482.02 150.961 24 3 4 -9 1911.84 160.967 7 -3 4 9 1616.35 151.155 15 -3 4 8 522.034 91.7986 15 3 4 -8 412.296 76.6422 24 3 4 -8 655.028 100.421 7 -3 4 7 276.084 72.4400 15 3 4 -7 159.968 56.4316 24 3 4 -7 255.286 64.7498 7 3 4 -6 9645.29 404.005 7 -3 4 6 10919.0 511.711 25 -3 4 6 10637.0 464.655 11 -3 4 6 9375.27 390.276 15 -3 4 5 8422.27 447.596 25 -3 4 5 7117.40 333.757 15 3 4 -5 8080.48 366.160 7 -3 4 5 7870.49 388.784 11 -3 4 4 575.154 90.5267 15 3 4 -4 696.576 103.012 7 -3 4 4 843.855 124.521 11 3 4 -4 691.725 112.201 24 -3 4 4 674.929 126.064 25 3 4 -3 5034.33 218.814 14 -3 4 3 5714.27 354.717 25 3 4 -3 4925.84 302.143 24 -3 4 3 5071.58 301.139 11 -3 4 3 4882.99 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3687.58 201.442 14 -3 5 1 3726.10 226.838 24 3 5 -1 3544.98 243.079 24 -3 5 1 3503.36 253.240 11 -3 5 1 3062.58 202.847 14 3 5 0 396.792 67.2692 14 -3 5 0 316.984 60.5886 14 3 5 0 508.304 96.1358 24 -3 5 0 327.327 65.2734 24 -3 5 0 424.310 87.2731 11 3 5 1 309.302 60.7356 14 -3 5 -1 236.436 49.6308 14 3 5 1 538.673 103.812 24 -3 5 -1 356.906 79.3870 11 -3 5 -1 362.229 77.8295 24 3 5 2 2708.52 188.860 14 3 5 2 3332.61 235.208 24 -3 5 -2 2707.42 213.996 24 -3 5 -2 2574.24 223.181 11 -3 5 -3 21087.5 666.270 24 -3 5 -3 19788.4 663.671 11 -3 5 -4 8535.52 407.541 24 3 5 4 9473.31 371.904 12 3 5 4 10275.9 366.171 14 -3 5 -4 8008.87 393.234 11 3 5 5 514.652 75.2867 14 -3 5 -5 409.853 87.1858 24 3 5 5 530.689 86.8471 12 -3 5 -5 459.784 92.2963 11 3 5 6 708.461 77.1233 14 3 5 6 765.285 103.408 12 3 5 7 364.618 49.9675 14 -3 5 -7 166.036 47.0361 24 3 5 7 331.823 66.9503 12 -3 5 -8-19.7281 27.2506 24 3 5 8 86.6766 30.0134 12 -3 5 -9 133.301 40.4867 24 3 5 9 137.383 37.2696 12 -3 6 5 265.153 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928.842 90.8967 15 -7 5 5 295.880 60.2571 15 7 5 -4 1288.34 82.3818 14 -7 5 4 1620.27 148.073 11 -7 5 4 1645.89 137.309 15 -7 5 3 299.704 62.0525 15 -7 5 3 375.490 84.8098 25 7 5 -3 228.903 38.4680 14 -7 5 3 331.389 79.5916 11 -7 5 2-0.83168 28.6565 15 7 5 -2 0.58570 16.9919 14 -7 5 2 1.46655 25.9228 11 7 5 -1 1354.31 107.722 14 -7 5 1 1355.21 143.193 11 -7 5 1 1224.73 125.631 15 7 5 0 4947.84 215.196 14 -7 5 0 4940.27 278.932 11 -7 5 -1 1581.12 136.519 15 7 5 1 2104.35 139.960 14 -7 5 -1 1890.00 171.889 11 7 5 2 934.857 92.5675 14 -7 5 -2 907.440 115.524 11 7 5 3 1088.51 96.4863 14 -7 5 -3 953.370 116.348 11 7 5 4 1754.38 112.196 14 -7 5 -4 1498.13 143.257 11 7 5 5 2007.56 105.651 14 -7 5 -5 1771.56 144.292 11 -7 5 -6 446.246 62.6633 11 8 -5 -5 1241.28 77.6190 23 8 -5 -4 168.638 32.0706 23 8 -5 -3 485.086 57.5432 23 8 -5 -2 410.358 55.6575 23 8 -5 -1 153.023 35.9795 23 8 -5 0 297.012 48.4074 23 8 -5 1 35.8324 18.5911 23 8 -5 2 483.892 58.3015 23 8 -4 -9 186.876 35.5563 23 8 -4 -9 198.213 36.5545 22 8 -4 -8 388.565 55.5813 23 8 -4 -7 1017.29 97.7631 23 8 -4 -6 208.207 48.4591 23 8 -4 -5 1358.70 123.494 23 8 -4 -4 1870.32 150.954 23 8 -4 -3 1246.03 125.496 23 8 -4 -2 510.989 81.7467 23 8 -4 -1 952.909 109.092 23 8 -4 1 29.3877 34.3269 26 8 -4 2 1528.77 139.838 26 8 -4 3 1840.56 153.051 26 8 -4 4 1461.31 132.957 26 8 -4 5 389.366 65.3084 26 8 -4 6 677.616 86.6128 26 8 -4 7 389.215 60.6063 26 8 -4 8 216.490 40.8110 26 8 -3 -11 1001.67 86.8054 23 8 -3 -11 932.549 72.9124 22 8 -3 -10 1444.95 114.012 23 8 -3 -10 1340.21 101.363 22 8 -3 -9 49.1649 31.8052 26 8 -3 -9 13.9882 31.6355 23 8 -3 -8 38.7340 26.9388 26 8 -3 -8 84.6957 46.7564 23 8 -3 -7 100.063 52.0084 26 8 -3 -7 217.626 55.6072 23 8 -3 -6 478.419 87.4654 26 8 -3 -6 432.802 75.4042 23 8 -3 -5 1163.43 137.936 26 8 -3 -5 960.291 116.724 23 8 -3 -4 1107.34 134.173 26 8 -3 -4 912.768 115.239 23 8 -3 -3 1305.22 147.594 26 8 -3 -3 1239.83 132.836 23 8 -3 -2 9568.60 411.205 26 8 -3 -1 14356.4 517.551 26 8 -3 0 4443.51 278.457 26 8 -3 1 1539.91 160.005 26 8 -3 2 2619.81 222.224 26 8 -3 3 11913.4 497.571 26 8 -3 4 11529.3 497.728 26 8 -3 5 2280.59 218.418 26 8 -3 6 1172.56 153.992 26 8 -3 7 241.526 72.8408 26 8 -3 8 415.350 89.5322 26 8 -3 9 369.246 78.9104 26 8 -3 10 742.216 100.995 26 8 -3 11 107.152 32.6918 26 8 -2 -13 281.469 41.4419 23 8 -2 -12 238.846 46.7218 23 8 -2 -11 1157.43 113.776 23 8 -2 -11 937.417 83.1639 22 8 -2 -10 2045.53 176.111 26 8 -2 -10 1987.65 154.067 23 8 -2 -10 1775.03 126.284 22 8 -2 -9 1490.22 154.767 26 8 -2 -9 1167.35 124.152 23 8 -2 -8-15.9934 41.3642 26 8 -2 -8 25.7534 32.4141 23 8 -2 -7 2840.67 223.540 26 8 -2 -7 2735.58 189.168 23 8 -2 -6 4707.47 291.384 26 8 -2 -6 4097.48 236.865 23 8 -2 -5 4000.08 263.183 26 8 -2 -5 3948.57 229.288 23 8 -2 -4 161.924 60.7732 26 8 -2 -4 171.410 48.9851 23 8 -2 -4 219.509 58.8944 10 8 -2 -3 74.2444 40.1393 26 8 -2 -3 80.5803 39.3915 23 -8 -2 3-9.38356 105.899 18 8 -2 -3 71.6208 37.0425 10 -8 -2 3 150.562 97.8325 28 8 -2 -2 9456.20 406.121 26 8 -2 -2 9112.24 782.968 2 -8 -2 2 10804.2 979.424 18 -8 -2 2 10221.3 694.801 28 8 -2 -1 2526.55 444.785 17 8 -2 -1 2157.38 390.685 2 -8 -2 1 2562.24 337.815 28 8 -2 0 1724.10 409.872 19 8 -2 0 1633.45 360.482 17 -8 -2 0 1698.45 267.898 28 8 -2 0 1409.60 327.440 2 8 -2 1 52637.5 2374.91 19 -8 -2 -1 56223.3 1723.18 1 8 -2 1 51138.6 2091.01 17 -8 -2 -1 55928.2 1690.02 28 8 -2 2 4610.23 293.672 26 8 -2 2 5862.68 800.375 19 8 -2 2 4447.89 587.706 17 -8 -2 -2 5990.36 528.583 1 -8 -2 -2 6455.49 520.106 28 8 -2 3 5122.84 317.489 26 8 -2 3 5200.02 644.127 17 8 -2 4 4745.22 318.524 26 8 -2 5 942.813 141.594 26 8 -2 6 2070.96 223.574 26 -8 -2 -9 1207.56 127.483 22 -8 -2 -10 3128.52 191.696 22 8 -2 11 210.970 73.5943 26 -8 -2 -11 177.623 39.8510 22 8 -2 12 425.052 81.2108 26 -8 -2 -12 312.292 47.6879 22 8 -1 -13 322.070 51.8730 23 8 -1 -12 215.082 49.8150 23 8 -1 -11 3436.72 199.871 23 8 -1 -11 3244.97 202.898 9 8 -1 -10 506.498 85.5245 9 8 -1 -10 542.881 99.1698 26 8 -1 -10 605.397 89.7033 23 8 -1 -9 6660.03 347.589 26 8 -1 -9 6126.76 283.228 23 8 -1 -9 6225.43 313.631 9 8 -1 -8 1922.02 183.842 26 8 -1 -8 2065.87 158.181 23 8 -1 -8 1981.38 173.054 9 8 -1 -7 1835.14 182.923 26 8 -1 -7 1856.86 150.860 23 8 -1 -7 1955.83 170.476 9 8 -1 -6 2287.00 195.178 26 8 -1 -6 2099.53 154.670 23 8 -1 -6 2240.73 179.125 9 8 -1 -5 4077.01 255.328 26 8 -1 -5 4028.50 258.387 10 -8 -1 5 3654.77 589.960 18 -8 -1 5 4538.14 636.424 31 8 -1 -5 4349.00 544.856 3 -8 -1 5 3676.72 452.535 28 -8 -1 4 21127.8 1372.40 18 -8 -1 4 20836.2 1304.61 31 8 -1 -4 17201.5 1106.58 30 8 -1 -4 19567.6 1112.15 3 -8 -1 4 19844.2 1031.84 28 -8 -1 3 4356.07 453.496 28 -8 -1 3 4806.13 613.835 18 -8 -1 3 4939.03 592.647 31 8 -1 -3 4047.56 522.787 30 -8 -1 2 18203.7 1188.46 18 8 -1 -2 19169.9 1227.76 17 -8 -1 2 19029.5 1148.10 31 -8 -1 2 19183.5 950.266 28 -8 -1 1 16867.6 878.451 1 8 -1 -1 15768.7 1102.35 17 -8 -1 1 17185.7 873.561 28 -8 -1 0 7602.70 584.817 1 8 -1 0 6332.77 697.379 17 -8 -1 0 7318.28 551.109 28 -8 -1 -1 16248.5 887.065 1 8 -1 1 15592.2 1153.79 19 8 -1 1 15601.4 1129.95 17 -8 -1 -1 16240.9 828.890 28 -8 -1 -2 5595.01 515.858 1 8 -1 2 5749.15 718.018 19 8 -1 2 5331.65 669.856 17 -8 -1 -2 5706.00 470.850 28 8 -1 3 9790.04 981.075 19 -8 -1 -3 10460.3 728.891 1 8 -1 3 8486.37 866.540 17 8 -1 3 9117.84 974.592 5 -8 -1 -3 9445.13 605.887 28 8 -1 4 838.965 325.749 5 8 -1 4 631.445 277.291 19 -8 -1 -4 722.765 183.530 1 8 -1 4 566.637 229.042 17 -8 -1 -4 831.293 177.098 28 8 -1 5 9418.19 426.063 13 8 -1 5 9351.48 1047.91 19 8 -1 5 9899.12 1007.67 17 8 -1 5 10461.3 1150.30 5 8 -1 6 13723.4 535.397 13 -8 -1 -6 14186.0 479.338 22 8 -1 7 16587.3 617.160 13 -8 -1 -7 17645.1 557.268 22 8 -1 8 2965.66 247.611 13 -8 -1 -8 3478.03 233.407 22 8 -1 9 1555.46 179.244 13 -8 -1 -9 1875.84 166.960 22 8 -1 10 10176.5 446.124 13 -8 -1 -10 11583.0 421.760 22 8 -1 11 1203.67 134.020 13 -8 -1 -11 1211.12 120.932 22 -8 -1 -12-5.77382 26.3269 22 8 -1 13 281.898 60.4524 26 -8 -1 -13 237.829 43.9084 22 8 0 -14 67.9418 26.5535 27 8 0 -13 135.231 41.1961 27 8 0 -13 105.587 30.8910 23 -8 0 13 147.962 55.1266 13 -8 0 12 2088.16 216.265 13 8 0 -12 1421.09 118.034 23 8 0 -12 1804.43 150.008 9 8 0 -11 1300.69 119.540 23 8 0 -11 1439.29 146.312 9 8 0 -10 9272.53 345.311 23 8 0 -10 10414.4 430.524 9 8 0 -9 328.139 83.4412 9 8 0 -9 298.334 78.3466 26 8 0 -9 419.243 78.9062 23 8 0 -8 1698.15 163.684 26 8 0 -8 1802.43 140.617 23 8 0 -8 1715.03 172.200 9 8 0 -7 7315.98 342.300 26 8 0 -7 7262.29 364.821 9 8 0 -6 3428.85 224.650 26 8 0 -6 3906.09 257.103 10 -8 0 6 3215.43 530.340 31 8 0 -6 2959.43 479.919 30 8 0 -6 3553.09 560.423 3 8 0 -6 3833.06 253.153 9 -8 0 6 3322.71 473.015 28 8 0 -5 2223.53 339.393 4 -8 0 5 2251.35 453.257 18 -8 0 5 2164.03 408.898 31 8 0 -5 2081.29 404.562 30 8 0 -5 1817.37 323.291 16 -8 0 5 2159.67 372.948 28 8 0 -5 2141.89 414.081 3 8 0 -4 46108.7 1634.73 4 -8 0 4 44383.2 1979.61 18 -8 0 4 47282.8 1929.65 31 8 0 -4 48845.3 1993.97 3 8 0 -4 46564.7 1921.34 30 -8 0 4 46614.6 1806.50 28 8 0 -3 104593. 2640.06 4 -8 0 3 113036. 3199.61 18 8 0 -3 108024. 3138.10 17 8 0 -3 116896. 3068.05 3 -8 0 3 116861. 3064.82 31 8 0 -3 102900. 2984.77 30 -8 0 3 105372. 2809.27 28 8 0 -2 82.8627 96.2064 4 -8 0 2 122.109 104.688 18 8 0 -2 135.736 90.3972 17 -8 0 2-51.3098 76.0331 31 8 0 -2 296.661 157.549 30 8 0 -2 182.730 114.814 3 -8 0 2 230.835 142.927 28 -8 0 1 32356.2 1359.66 1 8 0 -1 32650.7 1281.23 4 -8 0 1 30576.1 1447.00 18 8 0 -1 30913.1 1545.50 17 -8 0 1 31467.0 1338.99 31 8 0 -1 29001.4 1431.60 30 -8 0 1 32906.6 1332.38 28 -8 0 0 20979.1 1115.78 1 8 0 0 19974.9 966.767 4 -8 0 0 21014.4 1157.50 18 8 0 0 18989.3 1211.79 17 -8 0 0 20671.8 1007.08 28 -8 0 -1 226.909 111.738 1 8 0 1 160.159 90.2475 4 8 0 1 269.534 138.599 17 -8 0 -1 193.729 98.3202 28 -8 0 -2 5828.82 580.277 1 8 0 2 5016.46 641.580 17 -8 0 -2 4947.64 467.537 28 -8 0 -3 6935.61 647.954 1 8 0 3 8226.70 833.669 19 8 0 3 6140.79 735.509 17 -8 0 -3 6602.63 523.122 28 -8 0 -4 105.785 110.130 1 8 0 4 73.5426 84.3416 19 8 0 4-35.3441 59.0451 17 -8 0 -5 11709.6 878.774 1 8 0 5 12566.9 1180.37 17 8 0 5 11325.4 1127.75 5 8 0 6 4651.83 316.425 13 8 0 6 4316.85 289.260 8 8 0 6 3305.14 203.076 12 -8 0 -6 4712.41 273.478 22 8 0 6 4090.18 709.073 5 8 0 7 25962.9 843.729 13 8 0 7 23564.3 745.069 8 -8 0 -7 25760.5 720.301 22 8 0 8 26823.5 868.954 13 -8 0 -8 25759.0 726.167 22 8 0 9 8294.20 410.443 8 8 0 9 9251.41 493.209 13 -8 0 -9 9231.88 397.615 22 8 0 10 4917.10 294.527 8 8 0 10 5414.85 361.420 13 -8 0 -10 4930.30 280.332 22 8 0 11 5974.69 298.388 8 8 0 11 7124.25 390.123 13 -8 0 -11 6800.06 313.067 22 8 0 12 64.2862 37.3035 13 -8 0 -12 23.6069 21.3863 22 8 0 13 1144.82 114.892 13 -8 0 -13 1029.95 95.2371 22 -8 1 14 431.498 72.4931 13 8 1 -13 343.226 58.0710 27 -8 1 13 452.167 91.6151 13 8 1 -12 159.743 44.7464 9 8 1 -12 203.519 55.5091 27 -8 1 12 228.464 82.3927 13 8 1 -11 3532.33 234.278 9 8 1 -10 454.933 89.7605 9 8 1 -9 6437.42 353.160 9 8 1 -8 2104.52 199.596 9 8 1 -7 2003.25 185.348 7 8 1 -7 2030.44 193.909 9 8 1 -6 2017.07 183.415 7 8 1 -6 1997.65 187.149 9 8 1 -5 3983.49 556.358 4 -8 1 5 4230.90 650.279 18 8 1 -5 3925.43 637.916 3 8 1 -5 3653.66 551.876 30 -8 1 5 4516.45 622.409 28 8 1 -5 4006.72 258.541 9 8 1 -4 21723.8 1301.22 4 -8 1 4 20695.6 1379.59 18 8 1 -4 20140.1 1389.10 3 8 1 -4 20090.6 1294.72 30 -8 1 4 21234.7 1331.63 28 8 1 -3 4657.08 586.485 4 -8 1 3 4297.82 585.582 18 8 1 -3 5071.19 647.148 3 8 1 -3 5053.80 580.918 17 8 1 -3 4198.70 569.993 30 -8 1 3 5505.72 649.213 28 8 1 -2 19190.7 1228.54 30 8 1 -2 19563.6 1209.56 4 -8 1 2 18898.5 1085.07 20 8 1 -2 17076.7 1133.61 3 -8 1 2 18679.5 1185.56 18 8 1 -2 18730.1 1127.97 17 -8 1 2 19657.6 1229.45 28 8 1 -1 17309.8 1132.00 4 -8 1 1 16297.6 1041.16 20 8 1 -1 15328.5 1000.28 3 -8 1 1 16062.1 1049.57 18 8 1 -1 14991.7 1033.84 17 8 1 -1 17116.0 1144.59 30 -8 1 1 16661.5 1104.38 28 8 1 0 7296.42 710.996 4 -8 1 0 7830.81 733.004 20 -8 1 0 7958.22 703.288 18 8 1 0 6568.01 687.167 17 8 1 0 6833.73 716.008 30 -8 1 0 7204.20 691.407 28 8 1 1 17529.5 1074.48 4 -8 1 -1 17416.5 1124.77 20 8 1 1 14786.0 1057.55 17 8 1 1 16341.0 1122.95 30 -8 1 -1 14243.4 959.516 28 -8 1 -2 5369.82 633.377 1 8 1 2 5212.00 644.275 17 8 1 2 6433.63 708.102 30 -8 1 -2 5339.03 555.035 28 -8 1 -3 9327.12 864.085 1 8 1 3 9000.13 896.459 17 8 1 3 10347.8 925.244 30 -8 1 -4 831.781 249.917 1 8 1 4 785.902 279.218 17 -8 1 -5 10012.4 907.978 1 8 1 5 8912.90 433.757 13 8 1 5 9191.78 433.411 8 -8 1 -5 9243.01 416.128 22 8 1 5 8201.23 361.061 12 8 1 5 10183.0 1058.10 17 8 1 6 13886.5 573.546 13 8 1 6 13710.0 560.623 8 8 1 6 12730.0 469.375 12 -8 1 -6 13592.0 519.009 22 8 1 7 17360.2 680.217 13 8 1 7 18010.8 669.643 8 8 1 7 17121.9 557.921 12 -8 1 -7 17817.2 610.265 22 8 1 8 3812.68 312.295 13 8 1 8 3487.82 282.356 8 8 1 8 3202.44 224.394 12 -8 1 -8 3167.97 243.433 22 -8 1 -9 1746.28 162.769 25 8 1 9 1811.97 214.116 13 8 1 9 2071.92 218.254 8 8 1 9 1719.71 155.859 12 -8 1 -9 1812.97 176.737 22 8 1 10 12939.0 568.682 13 8 1 10 12215.7 515.900 8 8 1 10 10836.8 392.315 12 -8 1 -10 11596.1 449.556 22 8 1 11 1334.76 166.231 13 8 1 11 1236.70 146.708 8 -8 1 -11 1168.86 125.876 22 8 1 12-4.04667 26.0736 8 8 1 12 53.7361 40.5012 13 -8 1 -12 0.56751 20.4951 22 8 1 13 334.620 54.7390 8 8 1 13 282.108 57.3429 13 -8 1 -13 317.243 50.5972 22 -8 2 13 247.733 56.1086 13 8 2 -12 262.382 46.2279 9 -8 2 12 289.411 72.5161 13 8 2 -11 1041.74 107.271 7 -8 2 11 883.026 132.474 13 8 2 -11 958.820 102.420 9 8 2 -10 1755.95 158.393 7 8 2 -10 1675.01 155.742 9 -8 2 9 1375.25 163.177 25 8 2 -9 1371.68 160.109 7 8 2 -9 1193.41 141.102 9 -8 2 8 16.4419 30.1592 25 8 2 -8 4.47433 29.5777 7 8 2 -8 15.0452 24.4087 9 -8 2 7 2397.53 221.050 25 8 2 -7 2595.19 221.453 7 8 2 -7 2860.60 226.628 9 -8 2 6 4271.41 293.581 25 8 2 -6 4412.37 291.390 7 8 2 -6 4837.93 293.835 9 -8 2 5 3830.39 277.851 25 8 2 -5 4066.37 276.022 7 8 2 -5 4108.87 268.473 9 8 2 -4 196.093 58.8546 9 8 2 -4 189.336 41.2027 14 -8 2 4 191.711 72.3302 25 8 2 -4 149.252 56.2508 7 8 2 -3 115.176 43.6793 9 8 2 -3 72.0724 29.4711 14 8 2 -3 46.5577 122.857 3 8 2 -3 160.794 52.8878 7 -8 2 2 8335.94 416.801 25 8 2 -2 8726.16 956.713 4 8 2 -2 9048.60 402.478 7 -8 2 2 9497.82 879.048 20 -8 2 2 9995.15 994.491 28 -8 2 1 2760.22 488.962 20 8 2 -1 2950.89 555.901 4 8 2 -1 2704.64 491.921 30 -8 2 1 2422.07 472.468 28 8 2 0 2117.68 464.473 4 -8 2 0 1463.95 367.651 20 8 2 0 1561.57 388.788 30 -8 2 0 1609.08 370.223 28 8 2 1 56270.6 2355.10 4 -8 2 -1 56927.5 2443.84 20 8 2 1 58459.1 2453.33 30 -8 2 -1 52847.4 2139.40 28 -8 2 -2 5243.62 324.554 25 -8 2 -2 4237.47 280.402 22 -8 2 -2 5228.79 738.671 20 8 2 3 5948.96 247.780 14 -8 2 -3 5326.81 329.887 25 8 2 3 4812.19 287.875 13 8 2 3 5189.31 298.571 8 -8 2 -3 4854.02 307.762 22 8 2 3 5123.36 274.123 12 -8 2 -4 4577.36 303.408 25 8 2 4 4687.33 295.460 13 8 2 4 4969.52 304.801 8 -8 2 -4 4588.85 305.994 22 8 2 4 4639.01 274.779 12 -8 2 -5 969.271 139.659 25 8 2 5 1080.90 146.569 8 8 2 5 895.130 133.615 13 -8 2 -5 962.252 138.542 22 8 2 5 1009.40 129.633 12 8 2 6 1873.31 202.543 13 8 2 6 2175.38 220.189 8 -8 2 -6 1921.95 198.569 22 8 2 6 2076.46 187.829 12 8 2 7 8396.69 446.322 13 8 2 7 8452.38 443.538 8 -8 2 -7 8142.10 410.426 22 8 2 7 8706.60 398.948 12 8 2 8 15133.4 619.692 13 8 2 8 16141.6 627.536 8 -8 2 -8 14430.1 551.086 22 8 2 8 16120.7 546.462 12 8 2 9 1280.04 174.590 13 8 2 9 1146.36 156.821 8 -8 2 -9 1040.69 134.041 22 8 2 9 1088.62 128.355 12 8 2 10 3012.57 245.915 13 8 2 10 3258.68 250.656 8 -8 2 -10 2912.43 207.389 22 8 2 10 3109.86 202.411 12 8 2 11 118.149 57.9077 13 8 2 11 148.263 53.1908 8 8 2 11 150.425 37.1564 12 -8 2 -11 122.735 38.2713 22 8 2 12 420.004 73.3536 13 8 2 12 405.233 68.6373 8 -8 2 -12 310.941 49.3592 22 -8 3 11 843.891 100.996 13 8 3 -11 1047.35 95.5930 7 -8 3 10 1127.99 132.373 13 8 3 -10 1443.15 129.262 7 -8 3 9-23.0134 41.4157 15 -8 3 9 32.1339 41.3613 25 -8 3 9 37.3381 48.7147 13 8 3 -9 20.9749 27.7809 7 -8 3 8 41.3686 35.7581 15 -8 3 8 6.36857 34.5440 25 8 3 -8 52.3882 35.5856 7 -8 3 7 162.648 48.8587 15 -8 3 7 164.174 60.1315 25 8 3 -7 116.570 50.4016 7 -8 3 6 279.354 58.7553 15 -8 3 6 288.456 84.2254 25 8 3 -6 331.687 80.6693 7 -8 3 5 923.658 116.757 15 8 3 -5 824.844 85.2922 14 -8 3 5 975.028 144.845 25 8 3 -5 1020.99 134.902 7 8 3 -5 1061.14 125.812 9 8 3 -4 1043.82 97.6448 14 -8 3 4 870.443 136.278 25 8 3 -4 1032.87 141.680 7 -8 3 4 992.414 131.930 11 8 3 -4 979.870 122.258 9 8 3 -3 1250.46 112.307 14 -8 3 3 1390.57 178.694 25 8 3 -3 1357.00 160.840 7 -8 3 3 1359.90 155.301 11 8 3 -3 1277.87 140.893 9 8 3 -2 9749.28 336.581 14 -8 3 2 9647.31 474.997 25 8 3 -2 9096.17 428.588 7 -8 3 2 9967.26 433.392 11 8 3 -2 8950.40 390.969 9 8 3 -1 15881.7 451.601 14 -8 3 1 15401.7 615.272 25 8 3 -1 14277.4 549.090 7 -8 3 1 15348.0 553.024 11 8 3 0 4318.95 267.202 9 8 3 0 5185.65 246.645 14 -8 3 0 4762.06 331.373 25 8 3 0 4325.00 290.368 7 -8 3 0 4808.02 301.220 11 8 3 1 1998.94 156.970 14 -8 3 -1 2032.68 218.506 25 8 3 1 1742.79 182.295 7 -8 3 -1 1842.76 187.596 11 8 3 2 2573.42 185.671 12 8 3 2 2802.04 235.347 7 -8 3 -2 2880.01 243.039 11 8 3 2 3108.43 195.227 14 8 3 3 13370.5 416.399 14 8 3 3 11937.6 438.811 12 8 3 3 12833.2 527.082 7 -8 3 -3 13072.0 540.186 11 8 3 4 13617.7 409.449 14 8 3 4 11195.6 441.409 12 8 3 5 2413.30 212.846 8 8 3 5 2379.00 197.173 12 8 3 6 1238.94 156.297 8 8 3 6 1322.53 148.621 12 8 3 7 228.781 68.1403 8 -8 3 -7 184.382 58.5166 22 8 3 7 234.003 67.8880 12 8 3 8 502.907 97.7520 8 8 3 8 445.328 81.1441 12 8 3 9 472.364 90.7006 8 8 3 9 436.067 73.2812 12 8 3 10 1029.31 119.004 8 8 3 10 1225.80 107.738 12 8 3 11 185.374 44.9169 8 8 3 11 130.273 30.0552 12 -8 4 9 121.722 31.6504 15 8 4 -9 188.773 43.7558 7 -8 4 8 321.309 54.1724 15 8 4 -8 314.479 59.4912 7 -8 4 7 998.079 131.845 25 8 4 -7 905.653 106.881 7 -8 4 7 1005.98 105.384 15 -8 4 6 192.330 51.1024 15 -8 4 6 175.891 61.9120 25 8 4 -6 259.523 64.1835 7 -8 4 5 1460.57 172.530 25 8 4 -5 1289.71 141.354 7 -8 4 5 1247.47 143.443 11 -8 4 5 1078.45 118.862 15 8 4 -4 1750.41 118.660 14 -8 4 4 2184.42 215.961 25 8 4 -4 2190.63 188.640 7 -8 4 4 2115.06 189.433 11 -8 4 4 1865.00 162.581 15 -8 4 3 953.443 112.832 15 8 4 -3 1035.37 97.6838 14 -8 4 3 1154.58 164.395 25 8 4 -3 1125.60 140.683 7 -8 4 3 1111.88 138.841 11 8 4 -2 494.823 72.9271 14 -8 4 2 714.206 126.297 25 8 4 -2 561.715 100.866 7 -8 4 2 492.271 90.7753 11 8 4 -1 1126.89 110.622 14 -8 4 1 1191.73 162.644 25 8 4 -1 1310.37 151.561 7 -8 4 1 1287.67 150.370 11 8 4 0 685.205 93.0223 14 -8 4 0 597.905 117.134 25 -8 4 0 554.673 102.121 11 8 4 1 60.7210 37.0982 14 -8 4 -1 71.6816 49.9971 11 8 4 2 1971.17 147.840 14 -8 4 -2 1883.31 193.913 11 8 4 3 2360.24 158.303 14 -8 4 -3 2375.80 218.957 11 8 4 4 1935.03 134.050 14 8 4 4 1699.65 146.439 12 -8 4 -4 1994.65 197.104 11 8 4 5 536.491 66.5418 14 8 4 5 553.326 84.4204 12 -8 4 -5 614.311 104.536 11 8 4 6 1051.25 113.398 12 -8 4 -6 1180.96 138.277 11 8 4 7 581.370 80.4408 12 -8 4 -7 572.281 91.4088 11 8 4 8 426.649 64.4296 12 -8 4 -8 397.868 68.6330 11 8 4 9 104.889 29.1628 12 -8 4 -9 164.372 40.5683 11 -8 5 6 542.613 54.1197 14 -8 5 6 705.071 68.6535 15 -8 5 5 1203.08 98.4682 15 -8 5 4 236.698 54.8181 15 -8 5 3 489.889 73.1440 15 8 5 -3 369.687 46.0937 14 -8 5 3 528.083 82.1160 25 -8 5 3 445.336 72.0781 11 -8 5 2 446.197 67.9026 15 8 5 -2 408.218 52.4088 14 -8 5 2 575.782 85.1957 11 -8 5 1 86.5736 31.7781 15 8 5 -1 195.564 39.5789 14 -8 5 1 161.946 48.5717 11 -8 5 0 362.672 59.4286 15 8 5 0 408.938 58.3315 14 -8 5 0 451.689 77.5798 11 8 5 1 142.117 40.0870 14 -8 5 -1 18.1826 21.2335 15 -8 5 -1 111.083 46.1696 11 8 5 2 679.062 72.6962 14 -8 5 -2 587.790 84.0284 11 -8 5 -3 258.186 43.9336 15 -8 5 -3 375.970 65.2129 11 -8 5 -4 416.911 65.4785 11 8 5 4 481.529 50.7136 14 -8 5 -5 656.948 74.5592 11 9 -5 -3 468.457 47.7651 23 9 -5 -2 268.554 41.9203 23 9 -5 -1 394.620 50.7941 23 9 -5 0 308.397 44.7241 23 9 -5 1 296.445 43.0042 23 9 -5 2 31.6546 13.4636 23 9 -5 3 14.6724 16.8964 23 9 -4 -8 694.628 65.4136 23 9 -4 -7 1957.14 121.505 23 9 -4 -6 385.178 60.0827 23 9 -4 -5 2394.11 153.275 23 9 -4 -4 325.778 63.0609 23 9 -4 -3 804.049 94.5063 26 9 -4 -3 872.075 101.466 23 9 -4 -2 1677.31 137.981 26 9 -4 -2 1725.52 142.059 23 9 -4 -1 98.5852 32.7039 26 9 -4 -1 41.3697 36.2983 23 9 -4 0 741.287 95.8223 26 9 -4 1 573.409 83.9684 26 9 -4 2 388.921 67.3930 26 9 -4 3 255.477 56.7983 26 9 -4 4 593.754 80.4130 26 9 -4 5 244.696 46.9784 26 9 -4 6 385.559 57.2653 26 9 -4 7 266.201 43.7238 26 9 -3 -11 713.038 63.6476 23 9 -3 -10 490.486 63.8418 23 9 -3 -10 427.385 51.1606 22 9 -3 -9 105.237 39.3920 23 9 -3 -9 190.899 49.2614 26 9 -3 -8 746.408 95.6853 26 9 -3 -8 695.536 87.5995 23 9 -3 -7 615.540 89.9483 26 9 -3 -7 631.784 89.8078 23 9 -3 -6 3632.79 235.045 26 9 -3 -6 3579.82 212.532 23 9 -3 -5 3560.42 240.070 26 9 -3 -5 3525.27 216.833 23 9 -3 -4 724.449 113.089 26 9 -3 -4 661.810 98.0409 23 9 -3 -3 20514.2 625.094 26 9 -3 -3 18225.1 555.052 23 9 -3 -2 14292.1 513.067 26 9 -3 -2 13134.2 461.732 23 9 -3 -1 2968.66 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2337.18 3 -9 0 4 65120.6 2418.85 31 9 0 -4 60450.4 2390.05 30 9 0 -4 59797.3 1240.02 9 9 0 -3 11870.4 864.801 4 -9 0 3 12184.2 1036.30 18 9 0 -3 12377.1 1039.37 17 -9 0 3 14232.3 1049.79 31 9 0 -3 12464.0 1017.66 30 -9 0 3 12529.5 945.386 28 9 0 -2 27990.7 1348.05 4 -9 0 2 27991.3 1546.62 18 9 0 -2 28446.7 1578.21 17 -9 0 2 31847.1 1516.43 31 9 0 -2 26296.3 1491.86 30 -9 0 2 29584.9 1434.12 28 -9 0 1 36990.9 1591.59 1 9 0 -1 37259.0 1525.21 4 -9 0 1 35959.0 1721.73 18 9 0 -1 34389.4 1759.06 17 9 0 -1 36896.8 1777.56 30 -9 0 1 35787.8 1551.62 28 -9 0 0 22158.2 1245.31 1 9 0 0 21718.5 1120.12 4 -9 0 0 19578.2 1223.65 18 9 0 0 18213.0 1282.01 17 9 0 0 20953.3 1324.80 30 -9 0 0 19579.2 1093.10 28 -9 0 -1 14311.1 1011.85 1 9 0 1 14182.3 875.870 4 9 0 1 12597.3 1083.98 17 -9 0 -1 13228.2 868.567 28 -9 0 -2 22572.5 1301.09 1 9 0 2 21270.7 1444.48 17 -9 0 -2 21869.6 1105.86 28 9 0 3 35135.2 903.016 8 -9 0 -3 37174.9 1700.91 1 9 0 3 38744.8 2036.54 17 -9 0 -3 38255.1 1459.08 28 9 0 4 475.344 92.7029 8 9 0 4 363.939 84.3871 13 -9 0 -4 343.254 69.1617 22 9 0 5 8856.60 425.956 8 9 0 5 8913.36 449.804 13 -9 0 -5 9097.39 405.061 22 9 0 6 8756.28 431.740 8 9 0 6 9381.07 476.356 13 -9 0 -6 9338.88 416.438 22 9 0 7 6543.57 374.159 8 9 0 7 7220.13 421.063 13 -9 0 -7 7220.30 362.710 22 9 0 8 163.362 63.4352 8 9 0 8 82.1047 46.4281 13 -9 0 -8 129.239 63.2064 22 9 0 9 2179.29 200.275 8 9 0 9 2040.78 218.342 13 -9 0 -9 2151.87 184.490 22 9 0 10 91.6185 47.2050 8 9 0 10 131.249 62.7868 13 -9 0 -10 83.6169 46.3118 22 9 0 11 2002.50 155.103 8 -9 0 -11 1768.94 139.212 25 9 0 11 2017.63 187.617 13 -9 0 -11 1862.39 151.404 22 9 0 12 72.9198 33.8640 13 -9 0 -12 79.3990 34.0925 22 -9 0 -13 1347.49 94.8404 22 9 1 -13 44.9048 20.1123 27 -9 1 13 94.9227 46.0427 13 9 1 -12 741.414 86.0662 27 -9 1 12 777.062 122.344 13 9 1 -12 791.286 89.0516 9 9 1 -11 1551.19 143.046 9 9 1 -10 517.326 94.1461 9 9 1 -9 1797.08 182.018 9 9 1 -8 3551.67 257.597 9 9 1 -7 6597.14 343.501 7 9 1 -7 7184.09 376.076 9 9 1 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6563.16 779.588 17 9 1 2 8043.84 881.584 30 -9 1 -2 7034.56 693.619 28 -9 1 -3 4978.39 310.377 25 9 1 3 4206.10 282.670 13 9 1 3 4713.51 293.971 8 9 1 3 4189.48 247.169 12 -9 1 -3 4269.45 279.135 22 9 1 3 3925.98 623.420 17 9 1 3 5307.20 730.313 30 -9 1 -4 9102.27 429.998 25 9 1 4 8023.98 410.850 13 9 1 4 8656.37 419.416 8 9 1 4 7709.92 354.512 12 -9 1 -4 8031.96 395.988 22 -9 1 -5 2775.73 232.845 25 9 1 5 2443.74 226.551 13 9 1 5 2436.50 227.334 8 9 1 5 2317.62 194.674 12 -9 1 -5 2449.04 217.975 22 -9 1 -6 7404.55 380.262 25 9 1 6 7375.68 415.296 13 9 1 6 6916.21 396.242 8 9 1 6 6689.62 338.297 12 -9 1 -6 7115.98 375.338 22 -9 1 -7 11332.4 466.549 25 9 1 7 10934.5 526.761 13 9 1 7 10579.9 500.795 8 9 1 7 10313.5 425.047 12 -9 1 -7 10855.6 467.556 22 -9 1 -8 9165.85 397.826 25 9 1 8 8603.97 462.347 13 9 1 8 9034.20 454.926 8 9 1 8 8179.86 365.208 12 -9 1 -8 8638.17 404.598 22 -9 1 -9 3571.42 226.175 25 9 1 9 3917.85 303.777 13 9 1 9 4170.29 294.362 8 9 1 9 3414.03 215.548 12 -9 1 -9 3625.80 247.295 22 9 1 10 3014.17 250.222 13 9 1 10 3223.14 241.511 8 -9 1 -10 2880.07 206.100 22 9 1 11 370.424 80.0655 13 9 1 11 311.480 71.5810 8 -9 1 -11 324.061 64.5349 22 9 1 12 158.364 41.1403 8 9 1 12 148.802 44.8498 13 -9 1 -12 139.553 37.6671 22 -9 2 12 290.610 64.5362 13 9 2 -12 179.959 33.5748 9 -9 2 11 543.178 100.646 13 9 2 -11 617.245 77.6579 9 9 2 -10 3678.87 211.306 7 9 2 -10 3828.84 219.776 9 -9 2 9 1180.28 143.490 25 9 2 -9 1084.55 131.209 7 9 2 -9 1226.34 133.967 9 -9 2 8 2084.80 199.492 25 9 2 -8 1917.74 180.655 7 9 2 -8 2167.59 188.544 9 -9 2 7 3113.59 250.436 25 9 2 -7 3467.22 257.000 7 9 2 -7 3256.14 241.646 9 -9 2 6 12379.9 521.874 25 9 2 -6 12908.4 518.842 7 9 2 -6 13498.3 514.260 9 -9 2 5 9096.65 444.217 25 9 2 -5 9410.90 435.975 7 9 2 -5 9427.07 427.551 9 -9 2 4 16735.9 618.228 25 9 2 -4 16373.4 594.455 7 9 2 -4 17674.2 593.075 9 -9 2 3 6815.37 379.678 25 9 2 -3 6515.73 357.546 7 9 2 -3 6480.43 341.114 9 9 2 -2 2604.67 165.401 14 -9 2 2 2031.60 207.660 25 9 2 -2 2208.11 200.166 7 9 2 -2 2138.53 189.806 9 9 2 -1 4567.54 224.264 14 -9 2 1 3985.63 293.887 25 9 2 -1 3830.45 268.102 7 9 2 -1 3743.46 254.984 9 9 2 0 2127.50 191.087 9 9 2 0 2600.20 170.301 14 -9 2 0 2398.97 228.825 25 -9 2 -1 3787.89 290.959 25 9 2 1 3615.84 217.658 12 9 2 1 3438.33 234.174 10 -9 2 -2 20754.7 718.568 25 9 2 2 20673.3 632.186 8 -9 2 -2 19057.7 657.464 22 9 2 2 19889.8 582.559 12 9 2 2 18926.3 613.235 10 -9 2 -3 7841.85 421.601 25 9 2 3 7824.06 382.647 8 -9 2 -3 7475.35 397.320 22 9 2 3 7240.26 342.943 12 -9 2 -4 12389.8 530.241 25 9 2 4 12529.0 513.903 13 9 2 4 13440.6 530.551 8 -9 2 -4 12904.7 531.406 22 9 2 4 13005.8 482.015 12 -9 2 -5 10210.5 465.960 25 9 2 5 9993.61 464.941 13 9 2 5 10570.4 478.821 8 -9 2 -5 9462.14 455.101 22 9 2 5 10197.2 428.100 12 -9 2 -6 4999.06 306.418 25 9 2 6 4939.48 331.183 13 9 2 6 5431.04 344.002 8 -9 2 -6 4872.49 315.429 22 9 2 6 5454.65 308.820 12 9 2 7 3193.27 264.410 13 9 2 7 3088.04 258.587 8 -9 2 -7 3084.33 244.357 22 9 2 7 3455.18 239.722 12 9 2 8 2298.83 221.520 13 9 2 8 2450.44 227.579 8 -9 2 -8 2188.67 195.880 22 9 2 8 2387.96 194.447 12 9 2 9 4695.27 304.495 13 9 2 9 4948.71 303.051 8 -9 2 -9 4371.65 260.086 22 9 2 9 4483.48 251.252 12 9 2 10 1077.92 134.164 13 9 2 10 1032.47 129.117 8 9 2 10 925.949 98.4356 12 -9 2 -10 936.017 107.252 22 9 2 11 578.461 84.4125 13 9 2 11 663.653 89.1430 8 -9 2 -11 516.864 67.1337 22 9 2 12 72.8637 27.2775 8 -9 3 10 365.895 69.7265 13 9 3 -10 420.795 62.4532 7 -9 3 9 85.2252 47.9516 25 -9 3 9 73.3392 42.9336 13 9 3 -9 80.9092 25.5283 7 -9 3 8 652.459 113.474 25 9 3 -8 657.422 97.1601 7 -9 3 7 549.510 84.1255 15 9 3 -7 522.937 83.0333 9 -9 3 7 575.621 110.665 25 9 3 -7 495.893 91.0030 7 -9 3 6 3231.74 258.131 25 9 3 -6 3407.11 243.786 7 9 3 -6 3237.96 216.270 9 -9 3 6 3435.54 214.552 15 -9 3 5 3073.59 210.487 15 -9 3 5 3467.61 268.678 25 9 3 -5 3590.25 257.353 7 9 3 -5 3569.17 233.128 9 9 3 -4 681.587 105.252 9 -9 3 4 651.500 121.864 25 9 3 -4 772.094 122.200 7 9 3 -3 19521.2 498.872 14 -9 3 3 20090.3 705.852 25 9 3 -3 19464.9 659.966 7 9 3 -3 18871.7 598.007 9 9 3 -2 14912.0 431.259 14 -9 3 2 14980.4 607.545 25 9 3 -2 14654.3 556.041 7 -9 3 2 14545.4 520.318 11 9 3 -2 13563.6 500.671 9 9 3 -1 2800.34 177.740 14 -9 3 1 2868.93 257.198 25 9 3 -1 2574.18 226.967 7 -9 3 1 2649.86 213.437 11 9 3 -1 2432.92 200.466 9 9 3 0 357.577 73.6695 9 9 3 0 588.242 80.8572 14 -9 3 0 730.257 139.129 25 9 3 0 416.028 93.6675 7 -9 3 0 512.963 99.3173 11 9 3 1 256.648 62.1760 9 9 3 1 365.534 66.0172 14 -9 3 -1 320.402 90.2029 25 9 3 1 285.786 75.1807 7 -9 3 -1 275.825 72.4989 11 9 3 2 1546.04 131.584 14 -9 3 -2 1223.43 172.167 25 9 3 2 1189.08 124.160 12 9 3 2 1591.79 182.454 7 -9 3 -2 1373.22 161.519 11 9 3 3 3332.19 192.718 14 9 3 3 2717.86 194.958 12 9 3 3 2850.51 246.465 7 -9 3 -3 2976.23 246.037 11 9 3 4 1588.83 127.007 14 -9 3 -4 1255.20 158.186 25 9 3 4 1374.33 143.942 12 9 3 4 1696.78 189.283 7 -9 3 -4 1533.25 174.517 11 9 3 5 685.585 109.004 8 9 3 5 698.233 103.161 12 9 3 6 29.6126 40.7915 8 9 3 6-31.0680 45.7526 12 9 3 7 1512.67 161.654 8 9 3 7 1322.85 136.131 12 9 3 8 4516.21 268.664 8 9 3 8 4259.33 235.812 12 9 3 9 2078.06 165.685 8 9 3 9 2032.21 144.986 12 9 3 10 713.123 87.1254 8 9 3 10 661.289 70.3123 12 -9 3 -10 786.422 86.4328 11 9 4 -8 674.146 76.8229 7 -9 4 8 632.789 64.0864 15 -9 4 7 1921.52 164.117 25 9 4 -7 1766.48 136.909 7 -9 4 7 1815.72 125.663 15 -9 4 6 353.872 63.8746 15 -9 4 6 362.350 87.7327 25 9 4 -6 330.197 71.3629 7 -9 4 5 2180.88 195.880 25 9 4 -5 2284.42 176.494 7 -9 4 5 1995.02 152.352 15 -9 4 4 212.973 53.3326 15 -9 4 4 342.718 84.9886 25 9 4 -4 265.275 71.1569 7 -9 4 4 282.645 68.3144 11 -9 4 3 656.101 91.8266 15 9 4 -3 786.772 81.2204 14 -9 4 3 1008.89 142.209 25 -9 4 3 867.904 113.416 11 9 4 -3 811.144 112.390 7 9 4 -2 1898.74 130.181 14 -9 4 2 2050.82 202.806 25 9 4 -2 1949.46 181.210 7 -9 4 2 1948.82 173.347 11 9 4 -1 117.259 41.7308 14 -9 4 1 80.8231 40.3744 25 9 4 -1 119.878 47.2907 7 -9 4 1 58.3212 29.5221 11 9 4 0 893.758 98.5527 14 -9 4 0 840.173 126.950 25 9 4 0 969.633 127.754 7 -9 4 0 668.507 104.973 11 9 4 1 738.745 89.4371 14 -9 4 -1 545.042 98.1756 25 -9 4 -1 715.974 107.704 11 9 4 2 612.036 78.2580 14 -9 4 -2 529.293 96.4694 11 9 4 3 351.327 59.9364 14 -9 4 -3 356.634 82.5027 11 9 4 4 833.398 82.0180 14 9 4 4 651.508 82.2057 12 -9 4 -4 814.385 115.359 11 9 4 5 342.222 47.7349 14 9 4 5 286.323 56.0782 12 -9 4 -5 410.387 77.4034 11 9 4 6 497.896 74.8353 9 9 4 6 595.657 80.0014 12 -9 4 -6 627.011 89.6583 11 9 4 7 358.566 55.9696 12 -9 4 -7 433.722 72.3646 11 9 4 8 132.854 31.3006 12 -9 4 -8 144.175 38.3411 11 -9 5 4 359.382 53.5024 15 -9 5 3 583.334 69.3913 15 -9 5 2 265.392 48.1907 15 -9 5 2 237.377 49.2190 11 -9 5 1 353.679 56.7736 15 -9 5 1 449.972 68.1084 11 -9 5 0 281.886 51.0603 15 9 5 0 261.709 39.7454 14 -9 5 0 393.849 66.5286 11 9 5 1 352.558 46.2002 14 -9 5 -1 410.632 61.8305 11 -9 5 -2 8.96245 14.4886 15 9 5 2 68.3786 23.0671 14 -9 5 -2 46.4286 22.0680 11 -9 5 -3 115.493 30.6573 11 10 -4 -7 514.836 53.6005 23 10 -4 -6 1048.94 85.7678 23 10 -4 -5 1394.76 100.924 26 10 -4 -5 1538.62 110.254 23 10 -4 -4 1057.52 95.7918 26 10 -4 -4 1212.15 105.831 23 10 -4 -3 527.575 71.6381 26 10 -4 -3 531.930 74.6121 23 10 -4 -2 2516.62 159.553 26 10 -4 -2 2698.32 167.531 23 10 -4 -1 1361.24 118.872 26 10 -4 -1 1444.34 123.497 23 10 -4 0 305.036 56.5309 26 10 -4 0 225.303 47.6756 23 10 -4 1 317.882 61.1432 26 10 -4 1 196.744 45.0445 23 10 -4 2 2156.18 151.752 26 10 -4 3 3667.49 194.102 26 10 -4 4 738.049 83.9229 26 10 -4 5 2128.57 132.734 26 10 -4 6 126.183 29.6634 26 10 -3 -10 1001.37 73.8942 23 10 -3 -9 1630.88 107.528 23 10 -3 -9 1494.51 91.1714 22 10 -3 -8 1560.51 127.898 26 10 -3 -8 1709.46 120.375 23 10 -3 -7 800.062 98.9590 26 10 -3 -7 718.808 83.9449 23 10 -3 -6 1116.69 122.591 26 10 -3 -6 1126.96 110.805 23 10 -3 -5 3039.34 210.970 26 10 -3 -5 3039.32 189.998 23 10 -3 -4 6687.70 326.111 26 10 -3 -4 6410.30 289.168 23 10 -3 -3 9991.15 413.097 26 10 -3 -3 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232.974 8 -10 0 -2 3114.63 241.964 25 10 0 2 2898.87 231.731 10 10 0 3 2970.65 240.330 8 -10 0 -3 3016.63 239.637 25 -10 0 -3 2773.87 218.475 22 10 0 3 2706.09 230.872 10 10 0 4 3422.67 262.560 8 -10 0 -4 3216.91 239.372 22 10 0 4 3077.31 252.055 10 10 0 5 963.392 143.098 8 -10 0 -5 1048.20 135.736 22 10 0 6 93.2009 49.8341 13 10 0 6 131.150 55.4910 8 -10 0 -6 147.975 57.4484 22 10 0 7-19.9331 53.3445 13 10 0 7 106.562 57.4655 8 -10 0 -7 55.0962 43.3322 22 10 0 8 624.328 110.170 8 10 0 8 555.142 115.337 13 -10 0 -8 659.535 106.647 22 10 0 9 30.6908 45.4202 13 10 0 9 63.2939 38.1175 8 -10 0 -9 67.1830 45.0116 22 10 0 10 1567.03 142.198 8 -10 0 -10 1488.15 130.910 25 -10 0 -10 1574.72 140.468 22 -10 0 -11 150.193 37.4651 25 -10 0 -11 217.254 48.0377 22 10 0 11 208.168 50.0749 10 -10 0 -12 16.6056 18.1851 22 10 1 -12 332.722 50.2850 9 10 1 -12 274.628 44.0451 27 -10 1 12 362.132 71.4441 13 10 1 -11 678.759 82.0385 27 10 1 -11 566.408 77.2583 9 -10 1 11 750.681 117.222 13 10 1 -10 6245.14 297.134 9 10 1 -9 9476.65 402.336 9 10 1 -8 438.241 88.2347 9 10 1 -7 8440.98 405.692 9 10 1 -6 5712.13 319.085 7 10 1 -6 6367.88 348.338 9 -10 1 5 7993.64 403.169 25 10 1 -5 7451.69 376.552 7 10 1 -5 8491.30 380.866 10 10 1 -5 8871.77 413.772 9 -10 1 4 9362.77 443.413 25 10 1 -4 8849.98 412.688 7 10 1 -4 9639.35 410.673 10 10 1 -4 9516.79 428.016 9 -10 1 3 10928.7 487.791 25 10 1 -3 12117.2 486.589 7 10 1 -3 11992.2 463.466 10 10 1 -3 12437.4 487.425 9 10 1 -2 601.998 101.906 9 10 1 -2 585.731 97.4180 8 -10 1 2 513.322 102.835 25 10 1 -2 476.439 87.8274 10 10 1 -1 5409.21 298.418 8 -10 1 1 4702.71 314.190 25 10 1 -1 5026.87 293.046 10 10 1 -1 4939.29 296.397 9 10 1 0 2995.27 227.009 9 10 1 0 3317.59 237.882 8 -10 1 0 3098.62 250.696 25 10 1 0 3035.43 228.914 10 10 1 1 6665.71 347.591 9 10 1 1 7259.74 362.663 8 -10 1 -1 7404.83 395.761 25 10 1 1 6685.57 350.361 10 10 1 2 5031.84 306.112 8 -10 1 -2 5223.41 330.056 25 -10 1 -2 4770.48 299.754 22 10 1 2 4553.37 295.215 10 -10 1 -3 12020.5 513.557 25 10 1 3 11966.8 501.219 8 -10 1 -3 10908.1 475.494 22 10 1 3 11076.3 481.319 10 -10 1 -4 13122.2 535.574 25 10 1 4 12167.2 520.657 8 -10 1 -4 11529.8 491.388 22 -10 1 -5 4877.49 312.613 25 10 1 5 4764.55 321.576 8 -10 1 -5 4519.67 299.480 22 -10 1 -6 1183.82 150.100 25 10 1 6 1128.56 158.371 13 10 1 6 1248.78 166.327 8 -10 1 -6 1129.69 143.521 22 -10 1 -7 2522.11 209.508 25 10 1 7 2190.86 225.791 13 10 1 7 2731.79 242.632 8 -10 1 -7 2486.92 211.744 22 -10 1 -8 107.513 51.9762 25 10 1 8 25.4034 44.8355 13 10 1 8 70.1697 44.3917 8 -10 1 -8 45.9194 29.9707 22 -10 1 -9 1469.48 136.631 25 10 1 9 1497.27 164.378 8 10 1 9 1509.83 171.989 13 -10 1 -9 1491.48 148.906 22 10 1 10 932.182 116.787 8 10 1 10 912.131 126.146 13 -10 1 -10 958.293 107.873 22 10 1 11 435.912 70.5607 8 -10 1 -11 367.075 58.9103 22 -10 1 -12 70.3125 25.0806 22 -10 2 11 1253.63 127.982 13 10 2 -11 1206.43 92.2466 9 -10 2 10 875.666 123.380 13 10 2 -10 900.674 88.2032 7 10 2 -10 1001.18 103.329 9 10 2 -9 1744.18 145.377 7 10 2 -9 1848.94 153.187 9 -10 2 8 2702.90 213.561 25 10 2 -8 3002.42 213.334 7 10 2 -8 2952.52 211.256 9 -10 2 7 1417.59 161.126 25 10 2 -7 1435.32 156.840 7 10 2 -7 1717.29 169.549 9 -10 2 6 3458.46 259.599 25 10 2 -6 3335.70 248.324 7 10 2 -6 3746.98 254.834 9 -10 2 5 819.710 129.747 25 10 2 -5 1005.57 137.091 7 10 2 -5 936.036 130.255 9 -10 2 4 2012.78 204.069 25 10 2 -4 1910.12 192.002 7 10 2 -4 2028.29 191.196 9 -10 2 3 8104.86 422.898 25 10 2 -3 7322.69 385.887 7 10 2 -3 7919.26 382.591 9 -10 2 2 11124.6 507.714 25 10 2 -2 9663.56 451.504 7 10 2 -2 10029.1 438.233 9 10 2 -1 165.293 56.8471 9 -10 2 1 134.412 62.7736 25 10 2 -1 107.223 47.9842 7 -10 2 0 3820.46 297.977 25 10 2 0 3883.45 265.294 9 10 2 1 1388.11 159.642 9 10 2 1 1704.42 163.976 8 -10 2 -1 1471.69 180.862 25 10 2 1 1408.10 149.672 10 -10 2 -2 2545.70 240.759 25 10 2 2 2764.75 216.168 8 10 2 2 2377.44 182.923 12 10 2 2 2218.40 195.005 10 -10 2 -3 1067.30 157.063 25 10 2 3 1184.04 145.789 8 10 2 3 1140.99 129.430 12 10 2 3 1072.46 141.350 10 -10 2 -4 6564.19 377.909 25 10 2 4 6806.70 369.017 8 -10 2 -4 6599.74 371.077 22 10 2 4 6579.11 330.326 12 -10 2 -5 2219.93 207.926 25 10 2 5 2380.14 218.500 8 -10 2 -5 2328.15 216.317 22 10 2 5 2246.09 191.447 12 -10 2 -6 2939.00 226.388 25 10 2 6 2828.12 235.650 8 -10 2 -6 2726.87 228.370 22 10 2 6 2800.64 213.324 12 -10 2 -7 2666.17 198.093 25 10 2 7 2991.49 243.792 8 10 2 7 2781.23 205.662 12 -10 2 -7 2769.75 221.832 22 10 2 8 2802.01 223.909 8 10 2 8 2580.22 187.131 12 -10 2 -8 2730.38 204.471 22 10 2 9 1762.51 164.067 8 -10 2 -9 1570.64 142.109 22 10 2 10 98.8743 36.6037 8 -10 2 -10 88.4043 34.1306 22 10 2 11 164.298 38.0519 8 10 2 11 154.567 39.8703 10 10 3 -9 1388.03 111.350 7 -10 3 8 1578.05 151.445 25 10 3 -8 1591.98 136.951 7 10 3 -8 1424.62 112.228 9 -10 3 7 640.710 101.406 25 10 3 -7 678.739 99.5730 7 10 3 -7 785.178 95.0183 9 -10 3 6 940.240 129.180 25 10 3 -6 922.379 122.356 7 10 3 -6 987.990 112.637 9 -10 3 6 1038.54 106.677 15 -10 3 5 2908.08 236.768 25 10 3 -5 2862.09 223.148 7 10 3 -5 3012.29 205.945 9 -10 3 5 2699.49 182.643 15 -10 3 4 5787.94 283.667 15 -10 3 4 6432.85 369.264 25 10 3 -4 6193.39 345.808 7 10 3 -4 6219.13 309.071 9 -10 3 3 10421.0 482.051 25 10 3 -3 10218.3 448.407 7 10 3 -3 9627.64 401.923 9 -10 3 2 7858.51 423.885 25 10 3 -2 8026.23 398.014 7 10 3 -2 7597.48 359.761 9 10 3 -1 56.9981 26.6590 9 10 3 -1 56.8051 43.0463 14 -10 3 1 56.9590 55.0754 25 10 3 -1 68.3938 34.2496 7 10 3 0 4913.35 237.961 14 -10 3 0 4985.00 337.155 25 10 3 0 4909.85 316.878 7 10 3 0 4317.51 273.789 9 10 3 1 13621.8 418.195 14 -10 3 -1 12768.8 551.188 25 10 3 1 13087.3 540.325 7 -10 3 -1 12769.8 479.178 11 10 3 1 11413.9 467.452 9 10 3 2 8952.46 410.491 9 10 3 2 11409.9 367.263 14 -10 3 -2 9431.71 464.431 25 10 3 2 10704.8 487.684 7 -10 3 -2 9637.67 417.792 11 10 3 3 6019.85 333.437 9 10 3 3 7524.95 281.627 14 -10 3 -3 6525.79 365.024 25 10 3 3 5959.19 287.845 12 10 3 3 7045.79 389.630 7 -10 3 -3 6631.84 342.703 11 -10 3 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84.0844 23 11 -3 -8 213.305 42.5462 26 11 -3 -8 246.557 39.8612 23 11 -3 -7 721.755 82.7923 26 11 -3 -7 779.622 77.1580 23 11 -3 -6 381.977 68.3937 26 11 -3 -6 442.499 64.0067 23 11 -3 -5 99.2419 41.0988 26 11 -3 -5 226.233 50.6462 23 11 -3 -4 374.142 73.9304 26 11 -3 -4 463.428 73.0181 23 11 -3 -3 1206.76 130.931 26 11 -3 -3 1142.18 113.475 23 11 -3 -2 2270.35 182.953 26 11 -3 -2 2256.18 160.205 23 11 -3 -1 221.122 61.1439 26 11 -3 -1 207.817 52.9172 23 11 -3 0 437.381 87.2534 26 11 -3 0 336.600 58.3366 23 11 -3 1 5196.06 291.527 26 11 -3 1 4716.99 245.040 23 11 -3 2 6570.75 328.203 26 11 -3 3 739.628 108.518 26 11 -3 4 2115.08 183.802 26 11 -3 5 53.6796 33.2879 26 11 -3 6 49.7782 30.7038 26 11 -3 7 247.208 55.3291 26 -11 -3 -7 216.625 50.7255 25 11 -3 8 159.449 36.8980 26 11 -2 -10 345.524 44.8055 23 11 -2 -9 47.5556 27.3310 26 11 -2 -9 186.339 40.6634 23 11 -2 -8 356.554 71.1827 26 11 -2 -8 367.650 56.8061 23 11 -2 -7 4521.02 255.728 26 11 -2 -7 4335.52 206.842 23 11 -2 -6 837.490 112.851 26 11 -2 -6 877.476 96.3428 23 11 -2 -5 145.260 51.9730 26 11 -2 -5 214.393 50.2543 23 11 -2 -4 1958.20 179.677 26 11 -2 -4 1896.47 148.217 23 11 -2 -3 2562.90 209.943 26 11 -2 -3 2571.67 176.324 23 11 -2 -3 3138.64 228.435 10 11 -2 -2 5186.86 301.594 26 11 -2 -2 4664.72 241.091 23 11 -2 -2 5410.77 296.843 10 11 -2 -1 2115.66 194.793 26 11 -2 -1 1787.22 147.630 23 11 -2 -1 2386.71 192.625 10 11 -2 0 2706.69 224.515 26 11 -2 0 2653.27 180.427 23 11 -2 0 2916.29 209.587 10 11 -2 1 5921.76 338.229 26 11 -2 1 6082.96 301.395 10 11 -2 2 4085.10 278.538 26 11 -2 3 4128.44 288.367 26 -11 -2 -3 4897.26 287.237 25 11 -2 4 1153.00 153.200 26 11 -2 5 306.523 83.7868 26 11 -2 6 900.116 136.541 26 11 -2 7 387.499 85.0524 26 11 -2 8 971.384 123.407 26 11 -2 9 186.342 52.6553 26 11 -2 10 77.9815 29.2526 26 -11 -2 -10 23.7968 18.3030 25 11 -1 -10 625.482 65.7644 9 11 -1 -9 2008.50 153.894 26 11 -1 -9 1842.74 130.663 9 11 -1 -8 28.9786 25.2592 9 11 -1 -8 24.4243 37.6530 26 11 -1 -7 774.325 111.411 26 11 -1 -7 938.153 106.981 9 11 -1 -6 370.172 78.4761 26 11 -1 -5 6116.02 319.036 26 11 -1 -4 12107.6 469.969 26 11 -1 -4 13704.1 521.779 10 11 -1 -3 7434.22 357.493 26 11 -1 -3 8049.27 391.439 10 11 -1 -2 689.917 109.903 26 11 -1 -2 708.193 112.298 10 11 -1 -1 10696.2 441.991 26 11 -1 -1 11624.4 476.162 10 11 -1 0 4768.54 288.595 26 11 -1 0 4975.43 302.761 10 11 -1 1 13849.2 523.359 26 -11 -1 -1 15613.1 556.184 25 11 -1 1 14588.8 544.542 10 11 -1 2 1830.90 179.352 26 11 -1 2 2193.53 202.971 8 -11 -1 -2 2402.20 211.283 25 11 -1 2 2082.74 196.588 10 11 -1 3 1601.27 176.309 26 11 -1 3 1887.16 188.612 8 -11 -1 -3 1926.36 191.836 25 11 -1 3 1818.07 183.252 10 11 -1 4 8302.58 409.623 26 11 -1 4 8288.32 398.054 8 11 -1 4 8480.36 403.628 10 11 -1 5 4069.42 283.099 26 11 -1 5 3894.20 261.042 8 11 -1 5 3883.35 265.702 10 11 -1 6 422.651 96.7217 26 11 -1 6 393.012 80.1582 8 11 -1 6 390.049 82.6937 10 11 -1 7 1151.86 144.819 26 11 -1 7 1015.41 117.262 8 11 -1 7 894.539 115.972 10 11 -1 8 2349.43 197.991 26 11 -1 8 1914.46 153.454 10 11 -1 9 2308.40 180.266 26 -11 -1 -9 2497.89 170.641 25 -11 -1 -9 2427.34 153.865 22 11 -1 10 766.037 89.6902 26 -11 -1 -10 655.621 77.0933 25 -11 -1 -10 719.442 74.0248 22 -11 0 11 552.898 89.7708 13 11 0 -11 457.674 60.2975 9 11 0 -10 1799.82 135.824 9 11 0 -9 466.645 76.6930 9 11 0 -8 782.221 98.4278 26 11 0 -8 725.462 104.037 9 11 0 -7 522.349 88.1738 9 11 0 -7 448.438 77.1503 26 11 0 -6 1452.14 140.908 26 11 0 -6 1324.83 149.642 9 11 0 -5 522.620 99.8698 9 11 0 -5 424.374 78.7962 26 11 0 -5 409.049 85.0087 10 11 0 -4 3021.29 210.646 26 11 0 -4 3065.59 239.281 10 11 0 -4 3178.81 233.946 9 11 0 -3 27749.4 792.067 10 11 0 -3 28831.9 777.889 9 -11 0 2 24199.4 745.956 25 11 0 -2 26028.0 754.235 10 11 0 -2 26119.7 732.245 9 -11 0 1 13566.0 531.162 25 11 0 -1 13105.2 514.301 10 11 0 -1 12981.4 488.968 9 11 0 0 9325.57 429.610 8 -11 0 0 9083.73 430.834 25 11 0 0 8322.31 408.470 10 11 0 0 8506.52 386.477 9 11 0 1 679.757 102.856 9 -11 0 -1 948.413 132.814 25 11 0 1 865.223 128.374 8 11 0 1 733.870 118.012 10 11 0 2 18288.2 639.091 8 -11 0 -2 18720.7 644.202 25 11 0 2 17459.9 621.975 10 11 0 2 17065.3 575.044 9 11 0 3 16383.4 568.388 9 11 0 3 18313.5 644.120 8 -11 0 -3 18496.8 639.131 25 11 0 3 17315.5 625.161 10 11 0 4 13696.0 554.483 8 -11 0 -4 14266.9 549.453 25 -11 0 -4 12558.3 491.402 22 11 0 4 13173.5 544.427 10 -11 0 -5 20.4923 30.8906 25 11 0 5 38.2569 48.2023 8 -11 0 -5 30.8404 36.6934 22 11 0 5-1.44472 38.5785 10 11 0 6 1099.57 150.949 8 -11 0 -6 1306.10 153.910 25 -11 0 -6 1138.59 136.905 22 11 0 6 1141.92 156.906 10 -11 0 -7 418.730 87.8924 25 11 0 7 290.113 77.5037 8 -11 0 -7 285.011 67.9410 22 11 0 7 301.733 79.7483 10 -11 0 -8 71.5826 46.9053 25 11 0 8 58.0020 45.2865 8 -11 0 -8 48.0355 34.1612 22 11 0 8 18.4958 23.3196 10 11 0 9 2388.89 181.194 8 -11 0 -9 2335.47 170.715 25 -11 0 -9 2362.66 167.804 22 11 0 9 2360.97 187.359 10 -11 0 -10 287.385 50.5123 25 11 0 10 402.599 62.6410 8 -11 0 -10 349.862 59.0138 22 11 0 10 380.299 67.2250 10 -11 0 -11 59.7247 23.9783 22 11 1 -11 48.0233 25.9746 9 -11 1 11-12.8700 34.5995 13 11 1 -10 712.589 85.7170 9 11 1 -9 2000.06 164.075 9 11 1 -8 15.0271 26.1775 9 11 1 -7 856.219 120.604 9 11 1 -6 420.711 88.2948 9 11 1 -6 344.152 74.7946 7 -11 1 5 5768.51 334.201 25 11 1 -5 5661.51 315.204 7 11 1 -5 6276.13 319.876 10 11 1 -5 6380.64 341.394 9 -11 1 4 11775.5 501.545 25 11 1 -4 11379.0 468.918 7 11 1 -4 12393.1 469.174 10 11 1 -4 12606.2 494.312 9 -11 1 3 6929.11 388.905 25 11 1 -3 6934.17 364.263 7 11 1 -3 8064.07 374.858 10 11 1 -3 8049.42 385.137 9 11 1 -2 799.361 120.581 9 -11 1 2 679.037 121.966 25 11 1 -2 826.978 126.429 7 11 1 -2 736.653 109.908 10 11 1 -1 11641.6 460.806 8 -11 1 1 10456.1 486.253 25 11 1 -1 10307.3 439.773 10 11 1 -1 10332.9 448.041 9 11 1 0 5166.84 304.813 8 -11 1 0 4894.91 322.631 25 11 1 0 4650.13 290.444 10 11 1 0 4930.00 298.931 9 11 1 1 14374.9 539.141 8 -11 1 -1 14311.3 574.701 25 11 1 1 13968.2 531.984 10 11 1 1 13739.5 526.659 9 11 1 2 1869.77 185.167 9 11 1 2 2079.52 200.268 8 -11 1 -2 2093.66 210.825 25 11 1 2 1914.50 191.577 10 11 1 3 1812.03 189.224 8 -11 1 -3 1623.47 179.591 25 -11 1 -3 1648.80 173.864 22 11 1 3 1619.37 180.116 10 11 1 4 9054.93 443.073 8 -11 1 -4 9297.34 443.768 25 -11 1 -4 8503.90 409.106 22 11 1 4 8237.02 419.283 10 11 1 5 4519.23 310.916 8 -11 1 -5 4157.30 284.221 25 -11 1 -5 4115.18 275.955 22 11 1 5 3903.65 286.454 10 -11 1 -6 489.910 91.9954 25 11 1 6 541.786 105.552 8 -11 1 -6 546.046 101.225 22 11 1 6 439.674 97.3515 10 -11 1 -7 1226.66 138.986 25 11 1 7 1178.92 149.417 8 -11 1 -7 1126.67 133.430 22 11 1 7 1059.55 145.222 10 -11 1 -8 2312.74 173.398 25 11 1 8 2469.94 206.373 8 -11 1 -8 2131.48 174.937 22 11 1 8 2328.40 204.165 10 11 1 9 2632.52 196.143 8 -11 1 -9 2324.63 153.797 25 -11 1 -9 2380.45 167.753 22 11 1 9 2496.25 193.944 10 11 1 10 834.891 96.9148 8 -11 1 -10 685.500 79.1986 22 11 1 10 752.162 95.2249 10 -11 1 -11 3.69048 11.6981 22 11 2 -10 355.743 52.1844 9 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3 4310.78 284.712 9 -11 2 -3 4138.49 296.027 25 11 2 3 4331.51 278.868 8 11 2 3 4051.36 268.449 10 -11 2 -4 1250.30 157.472 25 11 2 4 1232.91 148.830 8 11 2 4 1172.29 149.108 10 -11 2 -5 199.255 57.3526 25 11 2 5 308.537 76.1334 8 11 2 5 161.709 54.0482 10 -11 2 -6 974.346 123.548 25 11 2 6 977.740 131.513 8 11 2 6 928.176 127.569 10 -11 2 -7 356.690 68.9233 25 11 2 7 546.525 98.5915 8 -11 2 -7 381.148 74.8600 22 11 2 7 394.116 83.8638 10 11 2 8 910.342 114.719 8 11 2 8 822.222 110.929 10 11 2 9 157.497 44.6742 8 -11 2 -9 92.3101 24.8649 11 11 2 9 161.906 46.4907 10 11 2 10 120.426 32.3183 8 11 2 10 54.1616 25.3189 10 11 3 -8 217.567 39.0126 9 -11 3 8 276.739 58.3633 25 11 3 -8 241.407 46.0551 7 -11 3 7 679.713 93.6874 25 11 3 -7 664.617 85.9547 7 11 3 -7 671.715 75.2642 9 11 3 -6 317.912 58.7905 9 -11 3 6 331.404 74.8155 25 11 3 -6 350.142 67.2126 7 -11 3 5 95.3068 41.1540 15 11 3 -5 131.842 40.5678 9 -11 3 5 100.036 49.3135 25 11 3 -5 166.764 51.7521 7 -11 3 4 383.898 67.6198 15 11 3 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56.6282 25 11 4 -5 237.461 44.6510 7 -11 4 4 40.5044 27.0521 15 -11 4 4 64.3006 32.9274 25 11 4 -4 118.729 40.0368 7 -11 4 3 2167.16 168.561 25 11 4 -3 2443.58 163.795 7 -11 4 3 1984.51 128.755 15 -11 4 2 3130.70 170.642 15 -11 4 2 3247.77 211.405 25 -11 4 1 474.789 64.8172 15 -11 4 1 535.591 84.5026 25 11 4 -1 637.544 87.3456 7 -11 4 0 1096.69 117.734 25 11 4 0 1383.67 129.132 7 -11 4 -1 668.261 86.8467 25 -11 4 -1 864.347 84.1647 11 -11 4 -2 15.3512 15.6637 11 -11 4 -3 259.819 44.1931 11 12 -4 -1 175.767 33.4410 23 12 -4 0 130.463 30.0590 23 12 -3 -7 161.978 35.6753 26 12 -3 -6 562.010 68.8448 26 12 -3 -6 614.403 62.5699 23 12 -3 -5 2780.93 165.481 26 12 -3 -5 2792.04 141.326 23 12 -3 -4 169.074 48.9823 26 12 -3 -4 82.9572 25.9259 23 12 -3 -3 2628.85 175.090 26 12 -3 -3 2853.93 156.032 23 12 -3 -2 1401.86 130.297 26 12 -3 -2 1456.18 115.343 23 12 -3 -1 999.359 110.347 26 12 -3 -1 934.210 94.3306 23 12 -3 0 1484.25 137.176 26 12 -3 0 1417.45 116.694 23 12 -3 1 137.971 42.7657 26 12 -3 1 91.7276 33.2454 23 12 -3 2 754.996 100.031 26 12 -3 2 575.046 72.8368 23 12 -3 3 1475.04 136.676 26 12 -3 3 1349.38 107.169 23 12 -3 4 419.062 71.0198 26 12 -3 4 241.603 41.7847 23 12 -3 5 225.727 53.4965 26 12 -3 6 137.062 39.0544 26 12 -2 -8 969.339 93.3998 26 12 -2 -8 987.224 75.4990 23 12 -2 -7 643.445 84.1310 26 12 -2 -7 587.436 62.4973 23 12 -2 -6 532.658 82.0740 26 12 -2 -6 558.883 67.5154 23 12 -2 -5-0.87974 26.8252 26 12 -2 -5 22.0519 22.9773 23 12 -2 -4 2621.82 194.689 26 12 -2 -4 2824.85 160.944 23 12 -2 -3 3400.03 230.242 26 12 -2 -3 3653.97 189.072 23 12 -2 -2 3993.03 252.036 26 12 -2 -2 4387.81 258.296 10 12 -2 -1 736.646 112.697 26 12 -2 -1 735.053 105.558 10 12 -2 0 6444.14 328.494 26 12 -2 0 6711.08 316.094 10 12 -2 1 4106.88 261.003 26 12 -2 1 3918.97 231.103 10 12 -2 2 775.921 111.593 26 12 -2 2 668.413 89.3596 10 12 -2 3 346.490 76.5787 26 12 -2 4 67.0647 36.6275 26 -12 -2 -4 61.0145 36.6131 25 12 -2 5 341.491 71.6822 26 -12 -2 -5 263.263 66.2044 25 12 -2 6 205.992 53.0563 26 -12 -2 -6 360.597 70.4407 25 12 -2 7 361.938 66.4401 26 -12 -2 -7 512.934 77.5527 25 12 -2 8 505.029 71.9869 26 -12 -2 -8 386.512 58.6131 25 12 -1 -8 2940.44 178.418 26 12 -1 -7 3626.42 211.547 26 12 -1 -6 774.308 104.996 26 12 -1 -5 1748.64 161.695 26 12 -1 -4 2520.18 193.166 26 12 -1 -4 2719.55 221.233 10 12 -1 -3 1406.60 147.322 26 12 -1 -3 1446.94 163.600 10 12 -1 -2 1260.09 139.107 26 12 -1 -2 1295.29 152.945 10 12 -1 -1 3490.72 236.362 26 12 -1 -1 3596.12 252.138 10 12 -1 0 241.977 62.0100 26 12 -1 0 145.056 45.9199 10 12 -1 1 1078.03 131.640 26 -12 -1 -1 839.650 117.164 25 12 -1 1 997.868 132.844 10 12 -1 2 1788.33 171.241 26 -12 -1 -2 1745.45 176.250 25 12 -1 2 1619.30 170.709 10 12 -1 3 1232.11 143.035 26 -12 -1 -3 1396.43 156.022 25 12 -1 3 1347.74 155.377 10 12 -1 4 1878.61 176.896 26 12 -1 4 1958.31 185.978 8 -12 -1 -4 1958.43 181.927 25 12 -1 4 1896.52 179.896 10 12 -1 5 986.642 127.051 26 12 -1 5 956.811 122.733 8 -12 -1 -5 1019.87 132.587 25 12 -1 5 877.199 118.932 10 12 -1 6 301.242 66.8294 26 12 -1 6 226.656 60.9614 8 -12 -1 -6 297.289 75.1157 25 12 -1 6 291.417 65.8053 10 12 -1 7 182.795 50.1626 26 -12 -1 -7 116.762 45.1738 25 12 -1 7 114.423 44.6275 10 12 -1 8 634.001 85.4594 26 -12 -1 -8 632.066 83.8133 25 12 -1 9 660.455 75.3743 26 -12 -1 -9 644.741 76.7447 25 12 0 -10 3328.41 154.869 9 12 0 -9 980.652 95.0869 9 12 0 -8 248.702 57.8148 9 12 0 -7 38.8251 30.9909 9 12 0 -7 16.2644 26.0638 26 12 0 -6 3176.25 215.615 9 12 0 -5 15.1210 27.4953 9 12 0 -5 16.4729 37.0513 10 12 0 -4 8803.40 398.584 10 12 0 -4 9005.59 390.282 9 12 0 -3 16690.0 577.717 10 12 0 -3 17258.0 565.220 9 -12 0 2 4895.56 307.593 25 12 0 -2 4838.23 280.662 7 12 0 -2 5511.01 317.946 10 12 0 -2 5714.04 309.163 9 -12 0 1 1917.80 189.647 25 12 0 -1 2340.60 203.382 10 12 0 -1 2345.61 195.594 9 -12 0 0 11112.1 479.520 25 12 0 0 11166.7 475.187 10 12 0 0 12073.8 460.904 9 12 0 1 12144.8 499.301 8 -12 0 -1 11294.7 488.392 25 12 0 1 11269.8 481.548 10 12 0 1 11453.2 449.449 9 12 0 2 1610.23 176.046 8 -12 0 -2 1689.19 182.273 25 12 0 2 1621.34 176.615 10 12 0 2 1409.56 152.073 9 12 0 3 1671.37 180.252 8 -12 0 -3 1780.00 182.320 25 12 0 3 1922.77 193.115 10 12 0 3 1806.22 171.340 9 -12 0 -4 643.046 109.505 25 12 0 4 585.165 105.946 8 12 0 4 682.333 115.562 10 -12 0 -5 115.157 51.4022 25 12 0 5 205.015 64.3275 8 -12 0 -5 200.906 56.0098 22 12 0 5 169.009 56.1927 10 -12 0 -6-3.85137 31.8301 25 12 0 6-4.50959 25.3530 8 -12 0 -6 21.2195 23.4437 22 12 0 6 64.7296 45.2387 10 12 0 7 2836.05 210.496 8 -12 0 -7 2940.07 201.590 25 -12 0 -7 2472.85 175.279 22 12 0 7 2550.42 202.880 10 12 0 8 1733.16 149.834 8 -12 0 -8 1638.99 137.918 25 -12 0 -8 1487.53 123.440 22 12 0 8 1772.15 155.193 10 12 0 9 1851.02 133.351 8 -12 0 -9 1655.00 121.530 25 -12 0 -9 1782.56 122.373 22 12 0 9 1709.72 133.853 10 12 1 -10 113.941 29.7066 9 -12 1 10 120.953 41.3637 13 12 1 -9 248.042 47.8905 9 12 1 -8 2821.97 184.879 9 12 1 -7 3706.15 229.262 9 12 1 -6 838.293 118.167 9 12 1 -5 1635.22 153.399 7 12 1 -5 1854.86 172.606 9 -12 1 4 2177.93 200.289 25 12 1 -4 2527.94 201.970 7 12 1 -4 2381.56 189.899 10 12 1 -4 2557.95 208.553 9 -12 1 3 1448.96 165.723 25 12 1 -3 1173.32 140.013 7 12 1 -3 1400.28 148.246 10 12 1 -3 1383.47 150.721 9 -12 1 2 1123.47 150.556 25 12 1 -2 1244.61 146.687 7 12 1 -2 1270.34 147.728 10 12 1 -2 1323.72 151.056 9 -12 1 1 3241.45 260.372 25 12 1 -1 3533.27 257.620 7 12 1 -1 3203.43 234.509 10 12 1 -1 3479.23 249.486 9 12 1 0 193.600 56.1691 9 -12 1 0 172.625 63.4687 25 12 1 0 215.705 66.4449 8 12 1 0 231.950 61.0121 10 12 1 1 931.003 129.793 8 -12 1 -1 815.920 131.048 25 12 1 1 891.749 125.684 10 12 1 1 894.888 122.926 9 12 1 2 1776.69 181.225 8 -12 1 -2 1712.71 187.880 25 12 1 2 1701.66 175.372 10 12 1 2 1541.56 164.308 9 12 1 3 1320.31 157.953 8 -12 1 -3 1339.59 163.110 25 12 1 3 1428.48 163.655 10 12 1 3 1264.82 147.157 9 12 1 4 1909.28 182.607 9 12 1 4 2093.48 195.475 8 -12 1 -4 2040.89 193.060 25 12 1 4 1859.71 189.522 10 12 1 5 840.311 116.545 9 12 1 5 1120.86 141.168 8 -12 1 -5 1016.94 132.224 25 -12 1 -5 899.471 116.505 22 12 1 5 1015.56 133.431 10 12 1 6 165.558 51.1373 9 -12 1 -6 198.019 53.9998 25 12 1 6 358.997 83.5330 8 -12 1 -6 186.095 52.2046 22 12 1 6 278.564 75.1731 10 -12 1 -7 131.373 46.1999 25 12 1 7 146.956 62.5392 8 -12 1 -7 160.951 46.2556 22 12 1 7 104.134 52.3829 10 12 1 8 565.426 82.1555 9 -12 1 -8 597.359 77.5535 25 12 1 8 635.490 94.2573 8 -12 1 -8 477.593 71.0437 22 12 1 8 633.225 95.9781 10 12 1 9 617.033 70.5348 9 12 1 9 765.690 89.0980 8 -12 1 -9 595.511 65.8598 25 12 1 9 793.574 92.0476 10 12 2 -9 99.8233 26.8218 9 -12 2 9 105.829 39.4771 13 12 2 -8 888.086 80.6078 7 12 2 -8 954.225 94.1757 9 12 2 -7 597.968 81.6711 9 -12 2 7 613.915 84.6853 25 12 2 -7 544.703 76.2658 7 12 2 -6 551.155 86.1582 9 -12 2 6 533.077 86.8913 25 12 2 -6 500.904 77.8576 7 12 2 -5-3.87672 29.8093 9 -12 2 5-1.87137 31.1878 25 12 2 -5 6.52507 37.8422 7 -12 2 4 2645.93 214.907 25 12 2 -4 2620.09 202.514 7 12 2 -4 2708.50 202.938 9 -12 2 3 3599.47 257.247 25 12 2 -3 3436.69 242.954 7 12 2 -3 3562.06 236.186 9 -12 2 2 3946.05 285.334 25 12 2 -2 4049.97 268.509 7 12 2 -2 3843.52 250.514 9 12 2 -1 699.566 108.871 9 -12 2 1 762.411 134.266 25 12 2 -1 610.627 107.974 7 -12 2 0 6070.18 362.796 25 12 2 0 6473.45 354.579 7 12 2 0 6285.47 301.767 10 12 2 0 6509.54 336.448 9 12 2 1 4151.36 244.475 8 -12 2 -1 3656.03 275.864 25 12 2 1 3940.55 280.268 7 12 2 1 3694.84 234.024 10 12 2 1 3891.25 258.193 9 12 2 2 745.296 112.564 9 -12 2 -2 710.223 118.903 25 12 2 2 690.449 100.873 8 12 2 2 907.566 132.949 7 12 2 2 789.391 109.378 10 12 2 3 366.618 74.8803 9 -12 2 -3 347.556 79.1200 25 12 2 3 477.982 86.3627 8 12 2 3 375.652 80.8294 10 12 2 4 52.4234 29.9533 9 -12 2 -4 97.7787 44.6618 25 12 2 4-1.05983 26.3917 8 12 2 4 76.9524 39.3833 10 12 2 5 288.739 68.5716 9 -12 2 -5 264.505 62.1621 25 12 2 5 244.070 60.0755 8 12 2 5 257.118 64.5693 10 12 2 6 208.786 54.3257 9 -12 2 -6 238.458 52.1905 25 12 2 6 304.395 69.6187 8 12 2 6 232.779 58.9114 10 12 2 7 476.009 76.3091 9 -12 2 -7 512.636 67.5098 25 12 2 7 572.310 85.4217 8 12 2 7 510.391 80.6951 10 12 2 8 365.682 61.6032 9 12 2 8 466.170 68.0794 8 12 2 8 500.741 70.3778 10 12 3 -7 115.218 28.5925 7 -12 3 6 616.116 83.4982 25 12 3 -6 596.746 75.8972 7 12 3 -6 631.755 69.1954 9 -12 3 5 2570.25 181.656 25 12 3 -5 2553.73 168.970 7 12 3 -5 2703.20 158.968 9 12 3 -4 149.614 47.0365 9 -12 3 4 126.371 48.3611 25 12 3 -4 105.864 39.7603 7 -12 3 3 2176.47 138.033 15 -12 3 3 2676.79 201.249 25 12 3 -3 2576.40 189.187 7 12 3 -3 2536.75 170.221 9 -12 3 2 1417.95 153.838 25 12 3 -2 1500.00 148.897 7 12 3 -2 1505.38 134.716 9 -12 3 1 903.194 121.586 25 12 3 -1 1129.49 136.153 7 12 3 -1 952.648 110.083 9 -12 3 0 1380.48 150.684 25 12 3 0 1518.22 156.993 7 12 3 0 1348.01 134.200 9 12 3 1 188.880 54.7247 9 -12 3 -1 116.372 42.2306 25 12 3 1 136.596 50.4612 7 -12 3 -2 717.853 103.668 25 12 3 2 869.503 121.486 7 12 3 2 809.864 103.895 9 -12 3 -3 1550.89 140.090 25 12 3 3 1542.76 154.251 7 12 3 3 1642.32 146.022 9 12 3 4 378.610 70.2179 9 -12 3 -4 416.331 70.5990 25 12 3 4 388.787 72.3913 7 12 3 5 179.263 46.9724 9 12 3 6 96.6829 33.2262 9 -12 4 0 58.1181 19.8035 15 -12 4 -1 111.874 27.8420 15 13 -3 -4 566.292 67.2684 26 13 -3 -3 96.4204 33.9434 26 13 -3 -3 39.1233 17.2226 23 13 -3 -2 896.683 90.0502 26 13 -3 -2 1007.90 75.6227 23 13 -3 -1 1961.05 137.509 26 13 -3 -1 1985.78 108.438 23 13 -3 0 747.877 87.5043 26 13 -3 1 469.351 68.8056 26 13 -3 2 37.0029 19.4328 26 13 -3 3 936.627 91.4320 26 13 -3 4 1643.76 114.801 26 13 -2 -7 116.140 30.6377 26 13 -2 -6 875.747 90.1726 26 13 -2 -5 2682.84 168.007 26 13 -2 -4 352.610 64.1859 26 13 -2 -3 327.984 64.1742 26 13 -2 -2 545.680 81.9051 26 13 -2 -1 2433.65 178.571 26 13 -2 0 1451.48 139.598 26 13 -2 0 1487.40 132.932 10 13 -2 1 2216.23 175.063 26 13 -2 1 2027.22 151.153 10 13 -2 2 1832.41 157.422 26 13 -2 3 250.225 57.8933 26 13 -2 4 335.118 68.2700 26 13 -2 5 186.589 48.5621 26 -13 -2 -5 219.714 47.0040 25 13 -2 6 394.506 64.5087 26 13 -1 -7 443.832 62.1437 26 13 -1 -6 49.1340 28.6799 26 13 -1 -5 960.482 103.577 26 13 -1 -4 2414.35 173.511 26 13 -1 -3 1033.93 115.119 26 13 -1 -3 1152.42 132.350 10 13 -1 -2 823.535 105.860 26 13 -1 -2 1031.40 128.957 10 13 -1 -1 210.455 52.3252 26 13 -1 -1 262.411 72.4603 10 13 -1 0 1732.51 155.047 26 13 -1 0 1665.63 163.590 10 13 -1 1 1219.34 130.317 26 13 -1 1 1172.92 135.991 10 13 -1 2 1350.18 137.257 26 -13 -1 -2 1349.90 140.957 25 13 -1 2 1457.02 152.853 10 13 -1 3 157.522 48.0230 26 -13 -1 -3 191.264 55.4215 25 13 -1 3 73.3460 34.7914 10 13 -1 4 64.8070 38.0310 26 -13 -1 -4 81.6283 39.2071 25 13 -1 4 23.6491 23.6030 10 13 -1 5 718.598 92.0801 26 -13 -1 -5 739.598 97.5832 25 13 -1 5 660.772 90.7222 10 13 -1 6 1188.49 111.197 26 -13 -1 -6 1222.25 118.782 25 13 -1 6 1057.87 104.503 10 -13 -1 -7 726.084 85.3632 25 -13 -1 -8 1449.55 105.139 25 13 0 -8 3410.47 165.080 9 13 0 -7 4994.15 224.700 9 13 0 -6 3259.33 193.088 9 13 0 -5 24.3012 32.5218 9 13 0 -4 155.631 51.1364 9 13 0 -4 155.553 56.0063 10 13 0 -3 19.2241 29.3954 9 13 0 -3 126.781 49.1061 10 13 0 -2 99.3033 47.0240 9 13 0 -2 57.3896 34.9240 10 13 0 -1 57.4777 22.9892 9 -13 0 1 26.6840 23.6953 25 13 0 -1 15.1213 23.9175 7 -13 0 0 1849.52 180.631 25 13 0 0 2115.40 191.237 10 13 0 0 2180.36 176.457 9 -13 0 -1 1248.97 148.663 25 13 0 1 1530.88 162.637 10 13 0 1 1485.31 145.110 9 -13 0 -2 1092.03 136.287 25 13 0 2 1181.86 140.850 10 13 0 3 170.980 58.5830 8 -13 0 -3 77.2705 36.8309 25 13 0 3 102.348 51.0426 10 13 0 4 1790.20 175.769 8 -13 0 -4 1781.86 166.619 25 13 0 4 1747.62 171.121 10 -13 0 -5 17.5713 33.6929 25 13 0 5-37.1228 35.6205 8 13 0 5 0.69654 24.3854 10 -13 0 -6 17.8749 25.6477 25 13 0 6 66.6519 34.8780 8 13 0 6 71.0400 30.0994 10 -13 0 -7-27.7571 24.0106 25 13 0 7 6.96856 21.2305 8 13 0 7-9.27799 25.5871 10 -13 0 -8 38.4991 20.4883 25 13 0 8 61.2928 23.2657 10 13 1 -8 1591.71 113.420 9 13 1 -7 508.986 71.4399 9 13 1 -6 122.154 39.4128 9 13 1 -5 907.128 110.842 9 -13 1 4 2444.06 185.279 25 13 1 -4 2242.29 167.736 7 13 1 -4 2536.46 177.898 10 13 1 -4 2369.07 181.492 9 -13 1 3 933.354 123.076 25 13 1 -3 922.554 114.611 7 13 1 -3 886.618 109.171 10 13 1 -3 1059.72 123.300 9 -13 1 2 874.178 123.128 25 13 1 -2 902.098 118.478 7 13 1 -2 855.545 111.075 10 13 1 -2 846.334 111.570 9 13 1 -1 264.622 64.7298 9 -13 1 1 179.876 60.7098 25 13 1 -1 241.704 62.7527 7 13 1 -1 228.324 63.4765 10 -13 1 0 1456.27 163.190 25 13 1 0 1412.68 154.867 7 13 1 0 1512.80 152.438 10 13 1 0 1728.39 168.035 9 -13 1 -1 1246.50 148.898 25 13 1 1 1152.91 132.221 10 13 1 1 1232.44 137.069 9 13 1 2 1433.61 150.509 8 -13 1 -2 1372.10 154.797 25 13 1 2 1352.83 150.229 10 13 1 2 1489.20 150.793 9 13 1 3 104.414 41.0602 9 -13 1 -3 36.3235 32.2156 25 13 1 3 135.610 53.2280 8 13 1 3 120.562 45.6480 10 13 1 4 8.56906 26.6113 9 -13 1 -4 77.2554 43.3539 25 13 1 4 26.7643 28.3038 8 13 1 4 81.4494 39.3639 10 13 1 5 865.793 113.199 8 -13 1 -5 699.349 97.1875 25 13 1 5 737.701 104.728 10 13 1 5 722.919 97.2703 9 13 1 6 1226.19 128.032 8 -13 1 -6 1204.05 118.325 25 13 1 6 1272.27 130.110 10 13 1 6 1131.77 112.936 9 13 1 7 949.893 103.412 8 -13 1 -7 770.243 85.7766 25 13 1 7 797.416 96.0685 10 13 1 7 730.832 80.9980 9 13 1 8 1847.94 127.054 8 13 1 8 1719.07 124.445 10 13 2 -7 105.299 29.9793 9 -13 2 6 784.667 85.2332 25 13 2 -6 872.732 85.4861 7 13 2 -6 945.961 93.5811 9 -13 2 5 2528.15 172.797 25 13 2 -5 2478.94 163.091 7 13 2 -5 2690.59 171.942 9 13 2 -4 401.110 70.1542 9 -13 2 4 237.192 57.8264 25 13 2 -4 241.830 52.2201 7 13 2 -3 307.203 65.2924 9 -13 2 3 263.559 64.4910 25 13 2 -3 313.952 67.6603 7 13 2 -2 555.668 87.3335 9 -13 2 2 586.104 97.4611 25 13 2 -2 627.579 97.1889 7 -13 2 1 2285.47 195.889 25 13 2 -1 2325.37 191.572 7 13 2 -1 2223.33 172.879 9 -13 2 0 1432.09 152.746 25 13 2 0 1367.63 150.581 7 13 2 0 1485.74 145.533 9 -13 2 -1 2392.58 197.330 25 13 2 1 2285.85 194.929 7 13 2 1 2085.44 157.094 10 13 2 1 2278.25 180.020 9 13 2 2 1702.97 141.061 8 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772.310 87.1058 9 13 3 1 466.962 67.5788 9 -13 3 -1 516.357 78.6389 25 13 3 1 590.368 85.7189 7 13 3 2 35.7443 22.5867 9 -13 3 -2 57.3463 32.1139 25 13 3 2 71.4281 41.0865 7 -13 3 -3 840.242 84.1165 25 13 3 3 878.864 96.0816 7 13 3 3 1005.55 96.5926 9 13 3 4 1638.85 118.897 9 14 -2 -4 256.714 44.3678 26 14 -2 -3 88.3981 30.6144 26 14 -2 -2 264.291 50.9191 26 14 -2 -1 1124.10 102.335 26 14 -2 0 379.404 59.7389 26 14 -2 1 267.245 51.7027 26 14 -2 2 285.442 52.2807 26 14 -2 3 748.051 80.0000 26 14 -1 -5 345.148 52.0664 26 14 -1 -4 956.302 91.2912 26 14 -1 -3 2179.97 142.313 26 14 -1 -2 1715.90 130.495 26 14 -1 -2 2022.25 159.991 10 14 -1 -1 1624.69 128.129 26 14 -1 -1 2039.46 162.481 10 14 -1 0 1014.19 102.135 26 14 -1 0 1068.34 119.773 10 14 -1 1 527.548 70.2196 26 14 -1 1 494.909 81.4492 10 14 -1 2 585.650 75.4500 26 14 -1 2 612.773 86.0224 10 14 -1 3 117.930 32.9772 26 -14 -1 -3 115.002 39.3861 25 14 -1 3 154.782 43.5127 10 -14 -1 -4 492.887 71.9842 25 14 -1 4 429.166 66.1435 10 -14 -1 -5 571.854 70.0129 25 14 -1 5 551.584 66.4913 10 14 0 -6 41.8257 20.9483 9 14 0 -5 44.6209 19.9430 9 14 0 -4 1149.43 103.984 9 14 0 -3 421.239 65.9950 9 14 0 -3 409.624 73.9044 10 14 0 -2 34.0835 29.3604 9 14 0 -2 47.0124 33.1639 10 14 0 -1 22.3807 32.8077 10 -14 0 0 1218.87 127.054 25 14 0 0 1296.26 124.064 7 -14 0 -1-30.0149 24.8635 25 14 0 1-18.8185 30.9438 7 14 0 1 47.9564 34.5255 10 -14 0 -2-54.7563 45.2764 25 14 0 2 37.5411 24.6709 10 -14 0 -3 8.18299 20.0949 25 14 0 3 7.27392 25.9769 10 -14 0 -4 799.364 96.4497 25 14 0 4 700.529 93.8522 10 -14 0 -5 1562.94 125.972 25 14 0 5 1523.55 129.435 10 -14 0 -6 937.950 89.5477 25 14 0 6 1054.25 97.6786 10 14 1 -6 1386.53 103.250 9 14 1 -5 431.447 63.1677 9 14 1 -4 940.236 99.4831 9 -14 1 3 1959.12 148.112 25 14 1 -3 2147.40 147.696 7 14 1 -3 2246.95 151.327 10 14 1 -3 2366.12 161.812 9 -14 1 2 1617.67 141.809 25 14 1 -2 1694.10 139.216 7 14 1 -2 1753.81 141.157 10 14 1 -2 1843.97 147.951 9 -14 1 1 1730.33 151.644 25 14 1 -1 1617.11 142.854 7 14 1 -1 1757.53 143.307 10 14 1 -1 1782.67 145.741 9 -14 1 0 1027.57 119.868 25 14 1 0 957.920 112.896 7 14 1 0 929.223 108.259 10 14 1 0 1007.55 110.914 9 14 1 1 565.272 84.8361 9 -14 1 -1 398.888 75.1519 25 14 1 1 524.825 85.1477 7 14 1 1 487.695 78.1806 10 -14 1 -2 484.082 81.5708 25 14 1 2 514.623 85.3904 7 14 1 2 434.718 72.0084 10 14 1 2 620.231 86.0320 9 14 1 3 138.601 43.6041 9 -14 1 -3 66.9909 32.0483 25 14 1 3 47.8168 29.8782 7 14 1 3 89.4849 37.2513 10 14 1 4 479.987 69.1082 9 -14 1 -4 438.332 72.9404 25 14 1 4 470.797 77.9797 7 14 1 4 377.048 64.7184 10 -14 1 -5 481.247 68.3962 25 14 1 5 649.064 80.7295 10 -14 1 -6 181.459 37.5500 25 14 1 6 207.842 44.2824 7 14 1 6 224.937 45.4144 10 14 2 -5 1265.53 93.7501 9 14 2 -4 169.237 38.2000 9 14 2 -4 190.381 37.2098 7 14 2 -3 129.558 37.6686 9 -14 2 3 137.600 43.2725 25 14 2 -3 69.9954 28.3019 7 14 2 -2 171.862 41.8592 9 -14 2 2 161.362 46.7395 25 14 2 -2 213.601 45.0703 7 -14 2 1 857.906 101.361 25 14 2 -1 1047.50 108.268 7 14 2 -1 1066.29 103.728 9 14 2 0 425.080 67.4280 9 -14 2 0 370.325 67.7911 25 14 2 0 479.185 79.2962 7 14 2 1 312.419 55.8146 9 -14 2 -1 218.873 54.3579 25 14 2 1 281.103 60.9750 7 14 2 2 279.302 52.9122 9 -14 2 -2 414.580 69.2627 25 14 2 2 280.829 60.7066 7 14 2 2 309.836 51.4497 10 -14 2 -3 766.898 85.3694 25 14 2 3 744.562 96.5053 7 14 2 3 717.630 83.7489 9 -14 2 -4 553.381 67.2782 25 14 2 4 452.480 66.3911 7 14 2 4 552.007 68.9587 9 15 -1 1 537.796 69.1185 10 15 0 -1 66.6027 31.1762 10 15 0 0 151.597 42.4431 10 15 0 1 74.5781 28.7352 10 15 0 2 9.62599 16.0592 10 15 0 3 29.6578 18.3106 10 15 1 -1 364.975 54.2296 10 -15 1 0 750.114 78.6383 25 15 1 0 807.962 81.9746 7 15 1 0 904.041 84.5356 10 -15 1 -1 472.512 67.3024 25 15 1 1 404.144 59.6668 7 15 1 1 458.222 60.7421 10 -15 1 -2 493.941 65.3382 25 15 1 2 379.811 58.1399 7 15 1 2 422.148 57.8062 10 0 0 0 0.00 0.00 0 TITL cyc0912 in P2(1) REM P2(1) (#4 in standard setting) CELL 1.54184 12.561443 5.249781 13.412165 90.0000 91.3092 90.0000 ZERR 17.00 0.000208 0.000104 0.000258 0.0000 0.0016 0.0000 LATT -1 SYMM -x, y+1/2,-z SFAC C H O F UNIT 17.00 17.00 17.00 17.00 TREF HKLF 4 END ; _shelx_hkl_checksum 26383 _olex2_submission_special_instructions 'No special instructions were received'