data_shelx _audit_creation_method 'SHELXL-2014/7' _shelx_SHELXL_version_number '2014/7' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C26 H20 N3 P' _chemical_formula_sum 'C26 H20 N3 P' _chemical_formula_weight 405.42 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'P' 'P' 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/c' _space_group_name_Hall '-P 2ybc' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 13.2112(14) _cell_length_b 11.1621(9) _cell_length_c 14.5906(14) _cell_angle_alpha 90 _cell_angle_beta 108.833(11) _cell_angle_gamma 90 _cell_volume 2036.4(4) _cell_formula_units_Z 4 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 12861 _cell_measurement_theta_min 2.4200 _cell_measurement_theta_max 31.3840 _exptl_crystal_description prism _exptl_crystal_colour colourless _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.322 _exptl_crystal_F_000 848 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.23 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.16 _exptl_absorpt_coefficient_mu 0.153 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type numerical _exptl_absorpt_correction_T_min 0.70721 _exptl_absorpt_correction_T_max 1 _exptl_absorpt_process_details ? _exptl_absorpt_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'fine-focus sealed X-ray tube' _diffrn_measurement_device_type 'Rigaku Saturn724' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 20160 _diffrn_reflns_av_unetI/netI 0.0297 _diffrn_reflns_av_R_equivalents 0.0720 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_theta_min 1.629 _diffrn_reflns_theta_max 24.997 _diffrn_reflns_theta_full 24.997 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measured_fraction_theta_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_point_group_measured_fraction_full 0.997 _reflns_number_total 3580 _reflns_number_gt 3300 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'CrysAlisPro 1.171.38.41 (Rigaku OD, 2015)' _computing_cell_refinement 'CrysAlisPro 1.171.38.41 (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.41 (Rigaku OD, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0520P)^2^+1.5352P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 3580 _refine_ls_number_parameters 271 _refine_ls_number_restraints 284 _refine_ls_R_factor_all 0.0454 _refine_ls_R_factor_gt 0.0411 _refine_ls_wR_factor_ref 0.1059 _refine_ls_wR_factor_gt 0.1021 _refine_ls_goodness_of_fit_ref 1.037 _refine_ls_restrained_S_all 0.996 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group P1 P 0.33088(3) 0.38319(4) 0.51844(3) 0.01671(14) Uani 1 1 d . U . . . N1 N 0.19768(12) 0.57463(13) 0.55470(11) 0.0223(3) Uani 1 1 d . U . . . N3 N 0.25609(12) 0.58732(13) 0.71028(10) 0.0220(3) Uani 1 1 d . U . . . N2 N 0.19092(12) 0.63627(13) 0.63242(10) 0.0226(3) Uani 1 1 d . U . . . C8 C 0.30556(12) 0.49389(14) 0.68315(11) 0.0127(3) Uani 1 1 d . U . . . C22 C 0.27062(13) 0.15802(15) 0.44696(12) 0.0194(4) Uani 1 1 d . U . . . H22 H 0.3366 0.1604 0.4341 0.023 Uiso 1 1 calc R U . . . C20 C 0.22387(14) 0.42703(16) 0.31880(13) 0.0225(4) Uani 1 1 d . U . . . H20 H 0.1768 0.3632 0.3201 0.027 Uiso 1 1 calc R U . . . C1 C 0.13254(13) 0.61240(15) 0.45894(12) 0.0170(3) Uani 1 1 d . U . . . C16 C 0.37296(14) 0.55157(16) 0.39864(13) 0.0216(4) Uani 1 1 d . U . . . H16 H 0.4294 0.5734 0.4554 0.026 Uiso 1 1 calc R U . . . C9 C 0.38395(13) 0.42266(16) 0.75471(12) 0.0187(4) Uani 1 1 d . U . . . C7 C 0.27079(13) 0.48357(15) 0.58405(11) 0.0163(3) Uani 1 1 d . U . . . C2 C 0.04551(14) 0.54477(16) 0.40590(12) 0.0215(4) Uani 1 1 d . U . . . H2 H 0.0291 0.4716 0.4312 0.026 Uiso 1 1 calc R U . . . C26 C 0.14307(13) 0.25081(16) 0.50929(12) 0.0197(4) Uani 1 1 d . U . . . H26 H 0.1209 0.3165 0.5396 0.024 Uiso 1 1 calc R U . . . C15 C 0.30365(13) 0.45927(15) 0.40247(12) 0.0179(4) Uani 1 1 d . U . . . C21 C 0.23906(13) 0.25666(15) 0.48961(11) 0.0172(3) Uani 1 1 d . U . . . C23 C 0.20735(14) 0.05700(16) 0.42315(12) 0.0215(4) Uani 1 1 d . U . . . H23 H 0.2297 -0.0096 0.3939 0.026 Uiso 1 1 calc R U . . . C24 C 0.11150(15) 0.05290(16) 0.44186(12) 0.0236(4) Uani 1 1 d . U . . . H24 H 0.0675 -0.0163 0.4252 0.028 Uiso 1 1 calc R U . . . C3 C -0.01708(14) 0.58442(17) 0.31611(13) 0.0226(4) Uani 1 1 d . U . . . H3 H -0.0779 0.5393 0.2801 0.027 Uiso 1 1 calc R U . . . C14 C 0.38569(14) 0.29903(16) 0.74567(12) 0.0213(4) Uani 1 1 d . U . . . H14 H 0.3343 0.2604 0.6929 0.026 Uiso 1 1 calc R U . . . C25 C 0.07974(14) 0.14951(17) 0.48476(13) 0.0240(4) Uani 1 1 d . U . . . H25 H 0.0137 0.1465 0.4976 0.029 Uiso 1 1 calc R U . . . C17 C 0.36041(15) 0.61179(16) 0.31283(15) 0.0276(4) Uani 1 1 d . U . . . H17 H 0.4077 0.6752 0.3109 0.033 Uiso 1 1 calc R U . . . C6 C 0.15701(14) 0.71794(16) 0.42123(13) 0.0234(4) Uani 1 1 d . U . . . H6 H 0.2161 0.7649 0.4581 0.028 Uiso 1 1 calc R U . . . C18 C 0.27970(16) 0.57989(18) 0.23061(14) 0.0296(4) Uani 1 1 d . U . . . H18 H 0.2704 0.6219 0.1718 0.036 Uiso 1 1 calc R U . . . C10 C 0.45692(14) 0.47898(17) 0.83292(13) 0.0241(4) Uani 1 1 d . U . . . H10 H 0.4549 0.5635 0.8401 0.029 Uiso 1 1 calc R U . . . C4 C 0.00781(14) 0.68903(16) 0.27800(13) 0.0235(4) Uani 1 1 d . U . . . H4 H -0.0355 0.7156 0.2159 0.028 Uiso 1 1 calc R U . . . C13 C 0.46195(14) 0.23221(17) 0.81325(13) 0.0250(4) Uani 1 1 d . U . . . H13 H 0.4636 0.1476 0.8067 0.030 Uiso 1 1 calc R U . . . C11 C 0.53255(15) 0.41136(19) 0.90029(13) 0.0288(4) Uani 1 1 d . U . . . H11 H 0.5829 0.4496 0.9540 0.035 Uiso 1 1 calc R U . . . C12 C 0.53587(14) 0.28831(19) 0.89038(13) 0.0285(4) Uani 1 1 d . U . . . H12 H 0.5889 0.2425 0.9366 0.034 Uiso 1 1 calc R U . . . C5 C 0.09570(15) 0.75500(16) 0.33024(13) 0.0268(4) Uani 1 1 d . U . . . H5 H 0.1140 0.8261 0.3034 0.032 Uiso 1 1 calc R U . . . C19 C 0.21196(15) 0.48681(18) 0.23314(13) 0.0276(4) Uani 1 1 d . U . . . H19 H 0.1570 0.4638 0.1757 0.033 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 P1 0.0164(2) 0.0182(2) 0.0165(2) -0.00235(16) 0.00665(17) -0.00182(16) N1 0.0242(8) 0.0215(8) 0.0221(8) -0.0020(6) 0.0089(6) -0.0017(6) N3 0.0266(8) 0.0217(8) 0.0182(7) -0.0025(6) 0.0079(6) -0.0005(6) N2 0.0272(8) 0.0216(8) 0.0200(8) -0.0036(6) 0.0091(6) 0.0010(6) C8 0.0141(7) 0.0134(7) 0.0113(7) -0.0011(6) 0.0052(6) -0.0030(6) C22 0.0193(8) 0.0216(9) 0.0179(8) 0.0005(7) 0.0067(7) 0.0005(7) C20 0.0225(9) 0.0246(9) 0.0229(9) -0.0014(7) 0.0110(7) -0.0023(7) C1 0.0167(8) 0.0187(8) 0.0161(8) -0.0012(6) 0.0061(7) 0.0034(6) C16 0.0208(8) 0.0201(9) 0.0264(9) -0.0012(7) 0.0110(7) -0.0003(7) C9 0.0182(8) 0.0247(9) 0.0150(8) 0.0025(7) 0.0077(7) -0.0008(7) C7 0.0165(8) 0.0170(8) 0.0155(8) -0.0005(6) 0.0053(6) -0.0028(6) C2 0.0231(9) 0.0228(9) 0.0201(9) -0.0003(7) 0.0090(7) -0.0034(7) C26 0.0212(8) 0.0226(9) 0.0168(8) 0.0013(7) 0.0083(7) 0.0001(7) C15 0.0188(8) 0.0192(8) 0.0191(8) -0.0013(7) 0.0107(7) 0.0024(7) C21 0.0189(8) 0.0185(8) 0.0134(8) 0.0013(6) 0.0043(6) -0.0010(7) C23 0.0267(9) 0.0188(9) 0.0176(8) -0.0002(7) 0.0050(7) 0.0006(7) C24 0.0266(9) 0.0220(9) 0.0204(9) 0.0024(7) 0.0051(7) -0.0071(7) C3 0.0193(8) 0.0274(9) 0.0199(9) -0.0029(7) 0.0048(7) -0.0015(7) C14 0.0241(9) 0.0247(9) 0.0175(8) 0.0017(7) 0.0101(7) -0.0012(7) C25 0.0225(9) 0.0288(10) 0.0231(9) 0.0048(8) 0.0108(7) -0.0035(8) C17 0.0282(10) 0.0218(9) 0.0380(11) 0.0058(8) 0.0182(9) 0.0004(8) C6 0.0236(9) 0.0208(9) 0.0228(9) -0.0011(7) 0.0034(7) -0.0035(7) C18 0.0341(10) 0.0312(10) 0.0280(10) 0.0104(8) 0.0162(9) 0.0095(9) C10 0.0239(9) 0.0264(9) 0.0218(9) 0.0010(7) 0.0073(7) -0.0057(7) C4 0.0256(9) 0.0246(9) 0.0186(8) 0.0010(7) 0.0048(7) 0.0067(7) C13 0.0275(9) 0.0266(9) 0.0259(9) 0.0074(8) 0.0156(8) 0.0039(8) C11 0.0217(9) 0.0414(11) 0.0208(9) 0.0041(8) 0.0033(7) -0.0070(8) C12 0.0204(9) 0.0398(11) 0.0267(10) 0.0137(8) 0.0095(8) 0.0049(8) C5 0.0343(10) 0.0192(9) 0.0250(9) 0.0049(7) 0.0070(8) -0.0004(8) C19 0.0267(9) 0.0353(11) 0.0209(9) 0.0006(8) 0.0080(8) 0.0023(8) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag P1 C7 1.8146(17) . ? P1 C21 1.8204(17) . ? P1 C15 1.8224(17) . ? N1 N2 1.354(2) . ? N1 C7 1.372(2) . ? N1 C1 1.447(2) . ? N3 N2 1.303(2) . ? N3 C8 1.356(2) . ? C8 C7 1.373(2) . ? C8 C9 1.448(2) . ? C22 C23 1.380(2) . ? C22 C21 1.393(2) . ? C22 H22 0.9500 . ? C20 C15 1.378(2) . ? C20 C19 1.380(3) . ? C20 H20 0.9500 . ? C1 C6 1.382(2) . ? C1 C2 1.384(2) . ? C16 C17 1.383(3) . ? C16 C15 1.391(2) . ? C16 H16 0.9500 . ? C9 C10 1.384(2) . ? C9 C14 1.387(3) . ? C2 C3 1.377(2) . ? C2 H2 0.9500 . ? C26 C25 1.383(3) . ? C26 C21 1.389(2) . ? C26 H26 0.9500 . ? C23 C24 1.380(3) . ? C23 H23 0.9500 . ? C24 C25 1.379(3) . ? C24 H24 0.9500 . ? C3 C4 1.378(3) . ? C3 H3 0.9500 . ? C14 C13 1.379(2) . ? C14 H14 0.9500 . ? C25 H25 0.9500 . ? C17 C18 1.370(3) . ? C17 H17 0.9500 . ? C6 C5 1.377(3) . ? C6 H6 0.9500 . ? C18 C19 1.379(3) . ? C18 H18 0.9500 . ? C10 C11 1.378(3) . ? C10 H10 0.9500 . ? C4 C5 1.378(3) . ? C4 H4 0.9500 . ? C13 C12 1.379(3) . ? C13 H13 0.9500 . ? C11 C12 1.383(3) . ? C11 H11 0.9500 . ? C12 H12 0.9500 . ? C5 H5 0.9500 . ? C19 H19 0.9500 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C7 P1 C21 103.21(7) . . ? C7 P1 C15 102.31(7) . . ? C21 P1 C15 103.29(8) . . ? N2 N1 C7 110.20(14) . . ? N2 N1 C1 118.77(14) . . ? C7 N1 C1 131.03(14) . . ? N2 N3 C8 108.24(13) . . ? N3 N2 N1 108.27(14) . . ? N3 C8 C7 110.05(14) . . ? N3 C8 C9 120.78(14) . . ? C7 C8 C9 129.15(15) . . ? C23 C22 C21 120.93(16) . . ? C23 C22 H22 119.5 . . ? C21 C22 H22 119.5 . . ? C15 C20 C19 120.45(17) . . ? C15 C20 H20 119.8 . . ? C19 C20 H20 119.8 . . ? C6 C1 C2 120.08(16) . . ? C6 C1 N1 119.34(15) . . ? C2 C1 N1 120.57(15) . . ? C17 C16 C15 120.53(17) . . ? C17 C16 H16 119.7 . . ? C15 C16 H16 119.7 . . ? C10 C9 C14 120.11(16) . . ? C10 C9 C8 119.38(16) . . ? C14 C9 C8 120.51(15) . . ? N1 C7 C8 103.24(14) . . ? N1 C7 P1 132.58(12) . . ? C8 C7 P1 123.54(13) . . ? C3 C2 C1 119.46(17) . . ? C3 C2 H2 120.3 . . ? C1 C2 H2 120.3 . . ? C25 C26 C21 120.09(16) . . ? C25 C26 H26 120.0 . . ? C21 C26 H26 120.0 . . ? C20 C15 C16 118.86(16) . . ? C20 C15 P1 124.47(13) . . ? C16 C15 P1 116.56(13) . . ? C26 C21 C22 118.68(15) . . ? C26 C21 P1 124.99(13) . . ? C22 C21 P1 116.30(12) . . ? C24 C23 C22 119.83(16) . . ? C24 C23 H23 120.1 . . ? C22 C23 H23 120.1 . . ? C25 C24 C23 119.82(16) . . ? C25 C24 H24 120.1 . . ? C23 C24 H24 120.1 . . ? C2 C3 C4 120.53(17) . . ? C2 C3 H3 119.7 . . ? C4 C3 H3 119.7 . . ? C13 C14 C9 120.05(17) . . ? C13 C14 H14 120.0 . . ? C9 C14 H14 120.0 . . ? C24 C25 C26 120.63(16) . . ? C24 C25 H25 119.7 . . ? C26 C25 H25 119.7 . . ? C18 C17 C16 119.89(17) . . ? C18 C17 H17 120.1 . . ? C16 C17 H17 120.1 . . ? C5 C6 C1 119.97(16) . . ? C5 C6 H6 120.0 . . ? C1 C6 H6 120.0 . . ? C17 C18 C19 120.04(17) . . ? C17 C18 H18 120.0 . . ? C19 C18 H18 120.0 . . ? C11 C10 C9 119.39(18) . . ? C11 C10 H10 120.3 . . ? C9 C10 H10 120.3 . . ? C3 C4 C5 119.85(17) . . ? C3 C4 H4 120.1 . . ? C5 C4 H4 120.1 . . ? C14 C13 C12 119.94(18) . . ? C14 C13 H13 120.0 . . ? C12 C13 H13 120.0 . . ? C10 C11 C12 120.62(18) . . ? C10 C11 H11 119.7 . . ? C12 C11 H11 119.7 . . ? C13 C12 C11 119.87(17) . . ? C13 C12 H12 120.1 . . ? C11 C12 H12 120.1 . . ? C6 C5 C4 120.07(17) . . ? C6 C5 H5 120.0 . . ? C4 C5 H5 120.0 . . ? C18 C19 C20 120.20(18) . . ? C18 C19 H19 119.9 . . ? C20 C19 H19 119.9 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C8 N3 N2 N1 0.18(18) . . . . ? C7 N1 N2 N3 -0.63(19) . . . . ? C1 N1 N2 N3 -179.80(14) . . . . ? N2 N3 C8 C7 0.34(19) . . . . ? N2 N3 C8 C9 179.35(14) . . . . ? N2 N1 C1 C6 71.0(2) . . . . ? C7 N1 C1 C6 -107.9(2) . . . . ? N2 N1 C1 C2 -108.00(18) . . . . ? C7 N1 C1 C2 73.0(2) . . . . ? N3 C8 C9 C10 -40.6(2) . . . . ? C7 C8 C9 C10 138.15(18) . . . . ? N3 C8 C9 C14 138.86(17) . . . . ? C7 C8 C9 C14 -42.3(2) . . . . ? N2 N1 C7 C8 0.80(17) . . . . ? C1 N1 C7 C8 179.83(16) . . . . ? N2 N1 C7 P1 -169.98(13) . . . . ? C1 N1 C7 P1 9.0(3) . . . . ? N3 C8 C7 N1 -0.69(18) . . . . ? C9 C8 C7 N1 -179.59(16) . . . . ? N3 C8 C7 P1 171.17(12) . . . . ? C9 C8 C7 P1 -7.7(2) . . . . ? C21 P1 C7 N1 -89.88(17) . . . . ? C15 P1 C7 N1 17.16(18) . . . . ? C21 P1 C7 C8 100.90(14) . . . . ? C15 P1 C7 C8 -152.06(14) . . . . ? C6 C1 C2 C3 -0.9(3) . . . . ? N1 C1 C2 C3 178.11(15) . . . . ? C19 C20 C15 C16 -1.1(3) . . . . ? C19 C20 C15 P1 -177.26(14) . . . . ? C17 C16 C15 C20 1.5(3) . . . . ? C17 C16 C15 P1 177.96(13) . . . . ? C7 P1 C15 C20 -102.04(15) . . . . ? C21 P1 C15 C20 4.93(16) . . . . ? C7 P1 C15 C16 81.73(14) . . . . ? C21 P1 C15 C16 -171.30(13) . . . . ? C25 C26 C21 C22 -1.4(2) . . . . ? C25 C26 C21 P1 -179.51(13) . . . . ? C23 C22 C21 C26 1.0(2) . . . . ? C23 C22 C21 P1 179.34(13) . . . . ? C7 P1 C21 C26 4.56(16) . . . . ? C15 P1 C21 C26 -101.74(15) . . . . ? C7 P1 C21 C22 -173.64(12) . . . . ? C15 P1 C21 C22 80.06(14) . . . . ? C21 C22 C23 C24 -0.2(3) . . . . ? C22 C23 C24 C25 -0.4(3) . . . . ? C1 C2 C3 C4 1.5(3) . . . . ? C10 C9 C14 C13 -1.7(2) . . . . ? C8 C9 C14 C13 178.79(15) . . . . ? C23 C24 C25 C26 0.0(3) . . . . ? C21 C26 C25 C24 0.8(3) . . . . ? C15 C16 C17 C18 -0.5(3) . . . . ? C2 C1 C6 C5 -0.9(3) . . . . ? N1 C1 C6 C5 -179.97(16) . . . . ? C16 C17 C18 C19 -0.9(3) . . . . ? C14 C9 C10 C11 1.4(3) . . . . ? C8 C9 C10 C11 -179.06(16) . . . . ? C2 C3 C4 C5 -0.3(3) . . . . ? C9 C14 C13 C12 0.6(3) . . . . ? C9 C10 C11 C12 -0.1(3) . . . . ? C14 C13 C12 C11 0.7(3) . . . . ? C10 C11 C12 C13 -1.0(3) . . . . ? C1 C6 C5 C4 2.2(3) . . . . ? C3 C4 C5 C6 -1.5(3) . . . . ? C17 C18 C19 C20 1.3(3) . . . . ? C15 C20 C19 C18 -0.3(3) . . . . ? _refine_diff_density_max 0.333 _refine_diff_density_min -0.382 _refine_diff_density_rms 0.077 _shelx_res_file ; shelx.res created by SHELXL-2014/7 TITL msb-rk-23-1_mo_a.res in P2(1)/c REM Old TITL MSB-RK-23-1_Mo in P21/c #14 REM SHELXT solution in P2(1)/c REM R1 0.148, Rweak 0.018, Alpha 0.021, Orientation as input REM Formula found by SHELXT: C26 N3 Cl CELL 0.71073 13.211161 11.162059 14.590576 90 108.8334 90 ZERR 4 0.001358 0.000934 0.00141 0 0.0112 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H N P UNIT 104 80 12 4 DELU DELU SIMU SIMU L.S. 10 PLAN 20 TEMP -173 BOND $H LIST 6 MORE -1 CONF fmap 2 acta 52 OMIT -3 50 OMIT 1 4 6 OMIT -6 0 2 OMIT 4 1 1 OMIT 3 2 4 OMIT -5 4 3 OMIT 0 0 8 OMIT 4 0 4 OMIT 0 4 0 OMIT 2 2 4 OMIT 3 3 1 REM REM REM WGHT 0.052000 1.535200 FVAR 0.54017 P1 4 0.330880 0.383188 0.518442 11.00000 0.01645 0.01818 = 0.01647 -0.00235 0.00665 -0.00182 N1 3 0.197681 0.574633 0.554704 11.00000 0.02422 0.02153 = 0.02213 -0.00204 0.00893 -0.00174 N3 3 0.256090 0.587317 0.710281 11.00000 0.02657 0.02168 = 0.01822 -0.00251 0.00794 -0.00054 N2 3 0.190923 0.636266 0.632419 11.00000 0.02722 0.02160 = 0.01996 -0.00360 0.00909 0.00102 C8 1 0.305564 0.493888 0.683154 11.00000 0.01408 0.01335 = 0.01134 -0.00109 0.00516 -0.00301 C22 1 0.270616 0.158025 0.446959 11.00000 0.01930 0.02156 = 0.01794 0.00046 0.00667 0.00050 AFIX 43 H22 2 0.336637 0.160360 0.434086 11.00000 -1.20000 AFIX 0 C20 1 0.223874 0.427034 0.318800 11.00000 0.02249 0.02464 = 0.02286 -0.00137 0.01096 -0.00227 AFIX 43 H20 2 0.176764 0.363234 0.320103 11.00000 -1.20000 AFIX 0 C1 1 0.132538 0.612400 0.458937 11.00000 0.01668 0.01872 = 0.01611 -0.00123 0.00605 0.00340 C16 1 0.372958 0.551567 0.398643 11.00000 0.02079 0.02011 = 0.02640 -0.00121 0.01095 -0.00034 AFIX 43 H16 2 0.429354 0.573402 0.455433 11.00000 -1.20000 AFIX 0 C9 1 0.383954 0.422660 0.754710 11.00000 0.01817 0.02472 = 0.01504 0.00246 0.00773 -0.00079 C7 1 0.270789 0.483573 0.584053 11.00000 0.01649 0.01696 = 0.01547 -0.00052 0.00527 -0.00278 C2 1 0.045510 0.544772 0.405900 11.00000 0.02311 0.02280 = 0.02006 -0.00028 0.00904 -0.00335 AFIX 43 H2 2 0.029094 0.471602 0.431236 11.00000 -1.20000 AFIX 0 C26 1 0.143074 0.250806 0.509285 11.00000 0.02118 0.02263 = 0.01679 0.00127 0.00833 0.00013 AFIX 43 H26 2 0.120902 0.316462 0.539621 11.00000 -1.20000 AFIX 0 C15 1 0.303652 0.459273 0.402468 11.00000 0.01881 0.01916 = 0.01906 -0.00133 0.01070 0.00239 C21 1 0.239057 0.256659 0.489613 11.00000 0.01887 0.01852 = 0.01345 0.00127 0.00431 -0.00102 C23 1 0.207345 0.056997 0.423148 11.00000 0.02666 0.01877 = 0.01757 -0.00023 0.00498 0.00060 AFIX 43 H23 2 0.229726 -0.009576 0.393946 11.00000 -1.20000 AFIX 0 C24 1 0.111496 0.052904 0.441855 11.00000 0.02656 0.02202 = 0.02038 0.00237 0.00505 -0.00708 AFIX 43 H24 2 0.067496 -0.016304 0.425212 11.00000 -1.20000 AFIX 0 C3 1 -0.017083 0.584419 0.316106 11.00000 0.01929 0.02739 = 0.01995 -0.00294 0.00483 -0.00148 AFIX 43 H3 2 -0.077903 0.539285 0.280149 11.00000 -1.20000 AFIX 0 C14 1 0.385693 0.299032 0.745674 11.00000 0.02414 0.02469 = 0.01746 0.00174 0.01013 -0.00121 AFIX 43 H14 2 0.334318 0.260361 0.692898 11.00000 -1.20000 AFIX 0 C25 1 0.079738 0.149509 0.484764 11.00000 0.02251 0.02882 = 0.02314 0.00485 0.01077 -0.00355 AFIX 43 H25 2 0.013723 0.146484 0.497615 11.00000 -1.20000 AFIX 0 C17 1 0.360413 0.611787 0.312827 11.00000 0.02823 0.02184 = 0.03803 0.00584 0.01820 0.00041 AFIX 43 H17 2 0.407684 0.675159 0.310897 11.00000 -1.20000 AFIX 0 C6 1 0.157012 0.717941 0.421229 11.00000 0.02359 0.02076 = 0.02280 -0.00109 0.00337 -0.00345 AFIX 43 H6 2 0.216118 0.764900 0.458077 11.00000 -1.20000 AFIX 0 C18 1 0.279696 0.579887 0.230610 11.00000 0.03409 0.03120 = 0.02802 0.01044 0.01624 0.00949 AFIX 43 H18 2 0.270369 0.621895 0.171823 11.00000 -1.20000 AFIX 0 C10 1 0.456923 0.478981 0.832916 11.00000 0.02395 0.02641 = 0.02183 0.00098 0.00732 -0.00568 AFIX 43 H10 2 0.454899 0.563454 0.840086 11.00000 -1.20000 AFIX 0 C4 1 0.007806 0.689034 0.278003 11.00000 0.02557 0.02460 = 0.01855 0.00103 0.00476 0.00671 AFIX 43 H4 2 -0.035513 0.715635 0.215873 11.00000 -1.20000 AFIX 0 C13 1 0.461951 0.232211 0.813254 11.00000 0.02752 0.02655 = 0.02591 0.00744 0.01563 0.00391 AFIX 43 H13 2 0.463570 0.147620 0.806688 11.00000 -1.20000 AFIX 0 C11 1 0.532548 0.411357 0.900294 11.00000 0.02168 0.04143 = 0.02078 0.00414 0.00335 -0.00697 AFIX 43 H11 2 0.582856 0.449619 0.954035 11.00000 -1.20000 AFIX 0 C12 1 0.535865 0.288310 0.890382 11.00000 0.02042 0.03977 = 0.02669 0.01374 0.00946 0.00494 AFIX 43 H12 2 0.588950 0.242526 0.936607 11.00000 -1.20000 AFIX 0 C5 1 0.095697 0.754996 0.330240 11.00000 0.03426 0.01921 = 0.02502 0.00487 0.00699 -0.00037 AFIX 43 H5 2 0.113985 0.826108 0.303427 11.00000 -1.20000 AFIX 0 C19 1 0.211962 0.486810 0.233136 11.00000 0.02671 0.03533 = 0.02089 0.00064 0.00804 0.00230 AFIX 43 H19 2 0.156951 0.463782 0.175746 11.00000 -1.20000 AFIX 0 HKLF 4 REM msb-rk-23-1_mo_a.res in P2(1)/c REM R1 = 0.0411 for 3300 Fo > 4sig(Fo) and 0.0454 for all 3580 data REM 271 parameters refined using 284 restraints END WGHT 0.0520 1.5352 REM Highest difference peak 0.333, deepest hole -0.382, 1-sigma level 0.077 Q1 1 0.2757 0.5107 0.2369 11.00000 0.05 0.33 Q2 1 0.3244 0.5819 0.2679 11.00000 0.05 0.30 Q3 1 0.3088 0.6058 0.2749 11.00000 0.05 0.30 Q4 1 0.2788 0.5026 0.6946 11.00000 0.05 0.29 Q5 1 0.3385 0.4632 0.7130 11.00000 0.05 0.27 Q6 1 0.3757 0.5630 0.3427 11.00000 0.05 0.27 Q7 1 0.2981 0.4812 0.6525 11.00000 0.05 0.27 Q8 1 0.2774 0.3208 0.5042 11.00000 0.05 0.26 Q9 1 0.3572 0.5977 0.3532 11.00000 0.05 0.25 Q10 1 0.3691 0.7005 0.4070 11.00000 0.05 0.22 Q11 1 -0.0174 0.4627 0.4709 11.00000 0.05 0.22 Q12 1 0.1011 0.2046 0.4790 11.00000 0.05 0.22 Q13 1 0.3739 0.6392 0.3164 11.00000 0.05 0.21 Q14 1 0.4410 0.6807 0.3451 11.00000 0.05 0.21 Q15 1 0.3454 0.7400 0.2861 11.00000 0.05 0.21 Q16 1 -0.0291 0.6597 0.3141 11.00000 0.05 0.21 Q17 1 0.6691 0.2854 1.0138 11.00000 0.05 0.20 Q18 1 0.3862 0.7254 0.3274 11.00000 0.05 0.20 Q19 1 0.2313 0.5712 0.2356 11.00000 0.05 0.20 Q20 1 0.0736 0.5939 0.4411 11.00000 0.05 0.20 ; _shelx_res_checksum 40226 _shelx_hkl_file ; 0 0 2 0.04 0.14 0 0 -2 273.81 3.77 0 0 -2 269.48 3.79 0 0 2 -0.01 0.10 0 0 -2 264.79 4.87 0 0 2 -0.06 0.11 0 0 -3 0.57 0.31 0 0 -3 0.01 0.24 0 0 -3 0.40 0.27 0 0 3 0.40 0.26 0 0 3 0.77 0.42 0 0 3 0.36 0.25 0 0 4 1507.28 12.40 0 0 -4 1581.53 12.60 0 0 4 1660.45 13.09 0 0 -4 1495.95 16.16 0 0 4 1701.35 17.04 0 0 -4 1555.48 13.42 0 0 -5 -0.24 0.50 0 0 5 -0.06 0.40 0 0 5 0.52 0.42 0 0 5 0.31 0.36 0 0 -5 0.42 0.48 0 0 -5 -0.06 0.28 0 0 6 44.57 2.64 0 0 -6 45.39 2.60 0 0 6 52.08 3.63 0 0 -6 46.00 2.83 0 0 -6 48.50 3.49 0 0 6 54.85 3.10 0 0 -7 0.30 0.39 0 0 7 -0.36 0.46 0 0 7 0.06 0.40 0 0 -7 0.57 0.69 0 0 7 1.50 0.97 0 0 -8 208.82 6.44 0 0 8 196.97 6.36 0 0 8 244.21 7.24 0 0 8 232.27 9.02 0 0 9 -0.06 0.48 0 0 9 -0.43 0.94 0 0 9 0.32 0.46 0 0 -9 0.17 0.46 0 0 10 402.82 13.08 0 0 10 402.15 10.45 0 0 10 371.50 9.96 0 0 -10 385.76 12.39 0 0 11 1.81 0.76 0 0 -11 -0.23 0.96 0 0 11 1.68 0.78 0 0 -12 398.73 13.64 0 0 12 394.78 11.28 0 0 -13 0.01 0.83 0 0 13 0.69 0.79 0 0 13 1.69 1.19 0 0 -14 161.91 9.44 0 0 14 154.26 7.70 0 0 14 167.74 8.58 0 0 15 -0.48 0.79 0 0 -15 -0.01 1.02 0 0 -15 0.24 0.88 0 0 -16 14.69 3.01 0 0 -16 16.06 3.39 0 0 16 18.02 2.87 0 0 17 0.24 1.06 0 0 -17 1.74 1.93 0 0 -17 -0.65 1.42 0 0 -18 2.99 1.89 0 0 18 1.32 1.93 0 0 -18 0.53 1.45 0 0 -19 0.88 1.66 0 0 -19 -0.10 1.65 0 0 -20 1.91 2.02 0 0 -20 5.55 2.93 0 -1 1 2779.81 11.98 0 -1 1 3476.33 15.65 0 1 -1 3001.78 10.27 0 1 -1 3170.20 13.04 0 1 -1 2396.18 11.15 0 -1 2 260.86 4.75 0 -1 2 0.03 0.09 0 1 -2 258.82 3.90 0 -1 2 183.98 3.14 0 1 -2 0.29 0.18 0 -1 -2 267.73 3.13 0 -1 -2 256.30 4.08 0 -1 -2 331.80 5.21 0 1 2 40.36 1.18 0 1 -2 296.48 5.88 0 1 -2 258.79 4.60 0 1 -2 -0.05 0.17 0 1 2 243.25 3.94 0 -1 -3 468.71 6.92 0 1 -3 443.46 5.64 0 -1 3 461.03 6.80 0 -1 3 448.44 5.77 0 1 -3 431.44 7.07 0 1 -3 490.79 7.30 0 1 3 455.00 6.66 0 -1 -3 485.76 5.45 0 1 3 384.56 4.94 0 -1 -3 520.00 7.13 0 1 -3 436.26 8.96 0 1 4 55.66 2.16 0 1 -4 50.67 2.18 0 1 4 61.38 2.90 0 1 -4 55.74 3.54 0 1 -4 54.16 2.76 0 1 -4 52.21 2.80 0 1 4 55.24 2.80 0 -1 4 56.61 2.33 0 -1 -4 64.21 2.90 0 -1 -4 55.43 2.23 0 -1 -4 52.55 2.79 0 -1 4 49.60 2.50 0 1 5 276.21 5.58 0 -1 -5 300.89 7.39 0 1 5 296.18 7.36 0 -1 5 302.76 6.10 0 1 5 355.39 7.38 0 1 -5 294.61 5.83 0 -1 -5 320.02 6.77 0 1 -5 336.91 9.23 0 -1 5 325.52 8.78 0 1 -5 299.82 7.17 0 -1 -5 319.01 6.05 0 -1 5 285.40 6.69 0 -1 -6 212.32 6.91 0 -1 -6 208.65 5.62 0 -1 6 207.10 5.54 0 1 6 202.76 6.91 0 -1 6 193.99 5.97 0 1 -6 211.80 7.90 0 1 -6 199.61 5.28 0 1 6 236.44 6.46 0 1 -6 209.32 6.79 0 -1 -6 220.24 6.17 0 1 6 189.41 5.16 0 1 -7 16.32 1.97 0 1 -7 15.75 1.62 0 1 7 14.96 2.07 0 -1 -7 15.44 1.85 0 -1 7 14.71 1.64 0 -1 -7 12.02 1.52 0 1 7 15.61 1.81 0 1 -7 11.21 2.02 0 1 7 11.96 1.48 0 -1 7 10.45 1.50 0 -1 -7 14.02 2.12 0 1 8 83.01 5.21 0 -1 -8 82.52 4.34 0 1 8 93.53 4.75 0 -1 -8 85.78 4.28 0 1 -8 66.67 4.78 0 1 8 83.97 3.97 0 1 -8 76.77 3.81 0 -1 8 89.73 4.30 0 -1 8 80.41 4.29 0 -1 9 25.82 2.56 0 1 9 20.34 2.30 0 1 9 27.44 3.21 0 1 -9 30.27 3.47 0 1 -9 23.15 2.36 0 -1 9 24.04 2.34 0 1 10 2.77 0.99 0 -1 10 3.88 1.13 0 1 10 4.79 1.46 0 -1 10 1.99 1.00 0 1 -10 0.45 0.86 0 1 10 3.74 1.64 0 1 11 301.70 8.94 0 -1 11 300.75 9.68 0 1 -11 329.61 12.25 0 1 11 383.80 13.38 0 -1 11 359.11 10.33 0 1 -11 306.94 11.47 0 -1 -11 310.71 11.27 0 1 12 37.23 3.33 0 -1 -12 38.68 4.30 0 1 -12 45.62 4.63 0 -1 12 53.52 4.18 0 1 -12 34.60 4.17 0 -1 12 42.60 3.90 0 1 12 50.75 5.09 0 -1 13 232.72 9.40 0 1 -13 220.48 10.59 0 -1 -13 225.07 10.49 0 1 13 222.92 8.49 0 1 -13 230.06 11.01 0 -1 14 203.93 9.13 0 1 -14 195.10 10.39 0 1 14 190.91 8.18 0 -1 14 191.46 8.93 0 -1 -14 192.80 10.05 0 1 -14 197.32 10.73 0 1 15 5.64 1.87 0 -1 15 5.97 1.93 0 -1 -15 3.73 1.79 0 1 -15 2.82 1.48 0 1 -15 2.87 1.71 0 -1 15 6.29 1.84 0 -1 -16 20.53 3.70 0 -1 16 20.97 3.41 0 1 -16 21.80 3.91 0 1 -16 20.97 4.03 0 1 16 14.58 3.27 0 -1 17 71.94 6.05 0 -1 -17 64.01 6.68 0 1 -17 76.29 7.53 0 1 17 67.16 5.80 0 1 -17 67.67 6.87 0 1 -18 6.35 2.45 0 -1 18 6.59 2.24 0 1 -18 10.99 3.10 0 -1 -18 6.79 2.47 0 -1 -18 5.84 2.56 0 -1 19 17.09 3.58 0 1 -19 22.95 4.45 0 -1 -19 20.78 4.33 0 -1 -19 21.36 4.49 0 1 -19 22.34 4.53 0 -2 0 1914.48 12.38 0 2 0 2118.98 12.10 0 -2 -1 2309.33 11.43 0 2 -1 2453.68 15.43 0 -2 1 2040.78 12.02 0 -2 -1 2390.94 10.61 0 2 1 2210.79 10.02 0 2 -1 2178.85 13.07 0 -2 1 2541.01 15.93 0 2 1 2218.06 12.38 0 2 2 256.79 4.40 0 2 -2 255.60 4.30 0 2 2 262.03 4.80 0 2 2 250.75 3.56 0 -2 2 306.86 6.66 0 -2 -2 249.92 4.69 0 2 -2 286.67 5.69 0 -2 2 255.85 5.25 0 2 -2 298.36 6.17 0 -2 2 252.95 4.89 0 -2 2 286.05 5.49 0 -2 -2 270.16 3.86 0 2 -3 714.31 9.53 0 2 -3 743.90 11.15 0 -2 -3 704.39 7.43 0 -2 3 731.91 8.42 0 -2 -3 719.31 8.65 0 2 3 697.05 8.14 0 2 -3 753.79 10.10 0 -2 -3 740.17 5.84 0 -2 -3 692.89 8.31 0 -2 3 696.53 9.41 0 -2 -4 816.67 9.57 0 -2 -4 759.96 10.12 0 2 4 795.74 10.10 0 -2 -4 766.01 7.30 0 -2 -4 937.27 12.02 0 2 -4 704.18 9.35 0 2 -4 810.35 11.70 0 2 -4 754.55 10.96 0 -2 4 759.69 9.01 0 2 -4 843.32 13.31 0 2 -4 939.60 15.09 0 2 4 685.49 6.93 0 -2 -4 753.79 9.69 0 -2 4 811.66 11.14 0 2 -5 2653.30 19.25 0 -2 -5 3437.78 18.17 0 2 -5 2860.57 23.85 0 2 -5 3201.48 25.19 0 2 5 2950.18 16.16 0 -2 5 3100.41 19.91 0 -2 -5 3468.80 24.45 0 -2 5 3136.30 23.38 0 -2 -5 3076.42 22.60 0 2 -5 3080.78 27.67 0 2 -5 3432.92 31.36 0 2 5 2995.07 22.07 0 2 -6 1131.37 18.02 0 2 -6 1047.99 12.90 0 2 -6 1195.39 16.60 0 2 6 950.92 12.16 0 -2 -6 1171.10 15.54 0 -2 6 1105.63 14.96 0 -2 -6 1295.52 16.42 0 -2 -6 1309.36 12.85 0 -2 6 1135.48 12.96 0 2 -6 1098.53 15.78 0 2 6 1185.11 15.59 0 2 -7 49.93 4.08 0 -2 -7 48.67 3.48 0 2 7 53.74 2.74 0 -2 7 57.16 3.74 0 -2 7 53.44 3.03 0 -2 -7 57.60 3.70 0 2 -7 48.16 3.57 0 2 -7 52.69 3.09 0 2 7 53.12 3.64 0 -2 -7 57.24 2.96 0 2 8 447.40 11.56 0 2 8 426.45 8.19 0 -2 8 439.32 10.62 0 2 -8 425.67 11.20 0 -2 8 462.96 9.74 0 -2 -8 502.79 9.77 0 2 -8 412.42 12.13 0 2 -8 378.04 8.76 0 -2 9 147.87 6.43 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5.06 -2 6 -15 7.14 2.61 2 -6 15 1.86 1.55 2 6 15 3.20 2.44 2 -6 16 4.47 1.98 -2 6 -16 2.50 2.15 2 7 -17 69.88 8.30 -2 -7 17 69.92 7.29 -2 -7 16 12.18 3.10 2 7 -16 12.13 3.75 -2 -7 15 1.21 1.46 2 7 -15 -0.04 1.51 -2 -7 15 2.81 1.84 -2 -7 14 15.20 2.74 2 7 -14 9.05 3.24 -2 -7 14 15.51 2.91 2 7 -13 9.67 2.88 -2 -7 13 5.19 1.99 -2 -7 13 5.30 1.66 -2 -7 12 71.04 5.57 2 7 -12 70.97 7.03 -2 -7 12 52.00 5.13 2 7 -11 127.12 8.96 -2 -7 11 131.39 7.89 -2 -7 11 142.44 7.59 2 7 -10 94.06 7.51 2 -7 -10 99.92 5.92 -2 -7 10 100.85 6.71 -2 -7 10 97.85 6.09 -2 7 10 75.77 4.40 2 7 -9 20.34 3.55 2 -7 -9 21.21 2.71 -2 7 9 16.47 1.94 -2 -7 9 23.85 3.31 -2 -7 9 25.65 3.13 2 -7 -8 19.00 2.48 -2 -7 8 15.82 2.66 -2 -7 8 11.59 2.11 2 7 -8 15.15 2.89 2 -7 -8 11.20 1.52 -2 7 8 12.07 1.43 2 -7 -7 372.61 10.36 -2 -7 7 377.70 11.67 2 7 -7 386.57 13.70 -2 -7 7 381.69 11.50 -2 7 7 356.68 7.48 -2 -7 6 29.24 3.17 2 -7 -6 22.89 2.60 -2 -7 6 33.46 3.43 2 7 -6 36.11 3.98 -2 7 6 21.93 1.74 2 7 -5 104.54 6.67 -2 -7 5 94.51 5.41 2 -7 -5 111.70 5.51 -2 7 5 97.77 3.65 -2 -7 5 104.98 6.07 -2 7 4 40.53 2.55 2 7 -4 36.01 3.84 2 -7 -4 40.10 3.27 -2 -7 4 28.64 3.30 -2 -7 3 71.59 4.30 -2 7 3 79.14 2.61 2 7 -3 92.69 5.69 2 -7 -3 87.08 4.73 -2 -7 3 84.81 5.66 -2 -7 2 136.19 6.25 -2 -7 2 147.21 6.01 2 -7 -2 148.06 6.24 -2 7 2 137.41 4.32 -2 -7 2 145.92 7.46 2 7 -2 138.43 6.66 -2 7 1 12.69 1.56 -2 -7 1 13.55 2.09 -2 -7 1 13.09 1.74 2 7 -1 15.34 2.12 2 -7 -1 13.07 1.92 2 7 -1 18.13 2.34 -2 7 0 177.29 6.19 2 7 0 166.76 6.63 -2 -7 0 131.98 4.86 2 7 0 163.35 6.20 -2 -7 0 155.03 6.97 2 -7 0 145.46 6.32 2 -7 1 0.67 0.57 -2 -7 -1 0.53 0.69 2 -7 1 1.12 0.73 -2 7 -1 0.06 0.55 -2 -7 -1 0.01 0.42 2 7 1 0.20 0.47 -2 -7 -1 0.26 0.52 2 7 1 0.75 0.70 2 -7 2 344.43 8.97 -2 -7 -2 352.44 11.23 -2 7 -2 395.31 10.95 2 -7 2 357.78 10.17 2 7 2 395.77 8.57 -2 -7 -2 324.38 6.28 -2 -7 -2 342.76 9.48 2 7 2 352.22 9.02 2 -7 3 250.60 7.33 -2 -7 -3 220.01 5.22 -2 -7 -3 280.02 10.44 -2 7 -3 297.47 9.94 -2 -7 -3 251.93 7.96 2 -7 3 277.97 9.29 2 7 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6.10 1.43 2 -8 6 9.86 2.24 2 8 6 6.54 1.34 -2 -8 -6 4.04 1.51 -2 8 -6 6.74 1.79 2 8 6 10.33 1.96 2 -8 7 9.27 2.39 2 8 7 14.35 2.43 -2 8 -7 11.57 2.66 2 -8 7 10.79 1.91 2 -8 8 5.39 1.45 -2 8 -8 5.77 2.20 2 -8 8 4.24 1.71 2 8 8 3.16 1.37 2 8 9 35.35 3.91 2 -8 9 39.52 3.60 -2 8 -9 46.21 5.38 2 -8 10 -0.36 0.98 2 -8 10 1.05 1.43 -2 8 -10 0.08 1.20 2 8 10 2.23 1.20 2 -8 11 4.64 1.59 -2 8 -11 5.73 2.02 2 8 11 3.40 1.96 2 -8 11 4.45 1.69 2 8 12 53.52 5.21 -2 8 -12 68.96 7.45 2 -8 12 69.32 6.45 -2 8 -13 17.49 4.20 2 -8 13 26.75 4.11 -2 8 -14 23.58 4.76 2 -8 14 24.17 4.23 2 -8 15 13.55 3.46 -2 8 -15 11.21 3.38 -2 -9 15 52.22 6.38 2 9 -15 50.30 7.03 2 9 -14 19.39 4.53 -2 -9 14 16.14 3.14 -2 -9 14 19.16 3.87 -2 -9 13 85.53 7.37 -2 -9 13 73.05 6.35 2 9 -13 90.99 8.75 -2 -9 12 -0.67 1.19 -2 -9 12 -1.49 1.46 2 9 -12 0.71 2.18 -2 -9 11 88.27 7.03 -2 -9 11 72.68 5.90 2 9 -11 89.59 8.23 -2 -9 10 37.19 4.51 -2 -9 10 37.14 4.11 2 9 -10 43.59 5.58 2 9 -9 83.74 7.47 -2 -9 9 81.12 6.11 -2 -9 9 61.76 5.74 2 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2 434.15 8.21 4 -7 -2 421.93 12.27 4 7 -2 466.44 12.99 -4 -7 2 485.81 13.94 4 7 -1 2.98 0.90 -4 -7 1 3.19 1.06 -4 -7 1 4.00 1.34 -4 7 1 2.35 0.74 -4 -7 1 3.16 0.94 -4 7 1 1.22 1.06 4 7 -1 2.40 0.96 4 -7 -1 1.79 0.88 4 -7 0 52.66 4.30 -4 -7 0 56.96 4.49 -4 -7 0 57.64 4.95 -4 -7 0 52.62 2.89 -4 7 0 52.18 3.57 4 7 0 53.94 3.09 -4 7 0 37.77 3.53 4 7 0 52.32 4.13 -4 -7 -1 27.46 1.89 -4 -7 -1 24.94 3.02 -4 7 -1 20.91 2.42 4 7 1 24.62 1.91 4 -7 1 19.17 2.67 4 7 1 23.59 2.73 4 7 2 1.41 0.80 -4 7 -2 -0.17 0.75 -4 -7 -2 0.25 0.65 4 7 2 -0.14 0.38 4 7 2 1.73 1.26 4 -7 2 0.07 0.56 4 -7 2 1.93 0.85 4 -7 3 4.16 1.24 4 -7 3 7.56 1.29 4 7 3 8.38 1.97 -4 7 -3 7.36 1.75 -4 -7 -3 8.25 1.88 4 7 3 10.54 1.81 4 7 4 34.10 3.24 4 7 4 23.94 1.32 -4 -7 -4 30.23 3.59 4 -7 4 37.00 3.40 4 7 4 26.00 3.31 -4 7 -4 34.12 3.87 4 -7 4 32.65 3.50 4 -7 4 30.98 2.34 4 7 5 1323.64 20.42 -4 -7 -5 1406.44 24.79 4 7 5 1263.53 22.53 4 -7 5 1453.79 19.98 -4 7 -5 1381.22 25.21 4 -7 5 1280.97 22.53 -4 -7 -6 134.40 7.92 4 7 6 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17.87 3.43 -4 -8 13 12.76 2.88 4 8 -13 17.44 3.92 4 -8 -12 257.49 11.78 -4 -8 12 279.31 12.86 -4 -8 12 279.80 11.94 4 8 -12 261.85 14.48 -4 -8 11 38.13 4.62 -4 -8 11 42.91 4.51 4 8 -11 41.21 5.70 4 -8 -11 36.16 4.38 -4 -8 10 12.99 2.64 4 -8 -10 13.64 2.75 -4 -8 10 9.43 2.30 4 8 -10 15.19 3.44 4 -8 -9 5.77 1.88 -4 -8 9 8.41 2.00 -4 -8 9 6.30 1.78 4 8 -9 7.51 2.40 -4 -8 8 138.30 7.78 4 -8 -8 122.29 7.31 -4 -8 8 120.83 7.29 4 8 -8 137.29 9.05 4 -8 -7 95.01 6.32 4 8 -7 100.48 7.46 -4 -8 7 98.13 6.49 -4 -8 7 106.18 6.54 4 -8 -6 13.70 2.52 -4 -8 6 12.63 2.31 -4 -8 6 10.47 2.01 4 8 -6 14.71 2.89 4 -8 -5 230.02 9.66 4 8 -5 236.95 10.73 -4 -8 5 241.15 9.09 -4 -8 5 218.23 9.56 -4 -8 4 30.28 3.11 -4 -8 4 27.07 3.50 4 -8 -4 28.73 3.45 4 8 -4 24.68 3.42 -4 -8 3 304.53 9.33 -4 8 3 318.65 5.87 4 -8 -3 289.96 10.41 4 8 -3 301.25 11.67 -4 -8 3 309.72 11.74 -4 8 2 3.08 0.74 4 -8 -2 2.95 1.18 -4 -8 2 2.19 0.82 -4 8 2 1.07 0.78 4 8 -2 2.72 1.10 -4 -8 2 3.79 1.23 -4 -8 1 147.07 7.43 4 -8 -1 139.94 7.22 -4 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304.26 10.38 7 5 1 285.10 11.14 7 5 1 243.63 9.77 7 5 2 225.83 10.11 7 5 2 232.69 6.62 -7 -5 -2 263.27 9.46 7 -5 2 250.21 10.03 7 -5 2 211.48 9.41 7 5 2 223.60 9.24 7 5 3 52.11 4.54 7 -5 3 39.57 1.64 7 -5 3 51.49 4.87 -7 -5 -3 54.21 4.29 7 5 3 50.42 4.85 -7 -5 -3 58.03 4.50 7 -5 3 49.05 4.59 7 5 3 51.93 2.46 7 5 4 35.75 3.89 -7 5 -4 33.28 3.59 7 -5 4 29.90 2.04 -7 -5 -4 38.14 3.67 7 5 4 34.13 4.09 7 5 4 4.43 0.64 -7 -5 -4 43.07 3.91 7 -5 4 42.75 4.72 7 -5 4 34.19 3.84 7 5 4 27.11 1.28 7 -5 4 1.40 0.45 7 5 5 210.79 9.58 -7 5 -5 208.31 9.43 -7 -5 -5 234.09 9.33 -7 -5 -5 255.53 9.85 7 5 5 204.74 10.02 7 -5 5 194.45 3.74 7 -5 5 242.70 11.56 7 -5 5 197.35 9.14 -7 5 -6 105.80 7.08 -7 -5 -6 109.79 6.49 -7 -5 -6 112.77 6.60 7 5 6 105.69 7.42 7 -5 6 107.80 8.05 7 -5 6 88.00 6.17 7 -5 7 -0.52 0.98 -7 -5 -7 0.61 0.81 -7 5 -7 -0.69 0.94 -7 -5 -7 -0.56 1.05 7 5 7 -0.01 0.77 7 -5 7 0.96 1.23 7 -5 8 1.18 0.91 -7 -5 -8 -0.39 0.88 -7 5 -8 0.77 0.81 -7 -5 -8 -0.16 0.92 7 5 8 1.37 0.86 7 -5 8 3.23 2.19 7 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3.33 7 6 13 15.62 3.91 -7 6 -13 16.40 4.25 7 -6 13 10.76 2.89 7 6 14 11.89 3.55 7 -6 14 12.64 3.25 -7 -7 19 0.75 1.79 -7 -7 18 2.44 2.71 -7 -7 17 62.96 7.21 7 7 -17 61.16 7.90 -7 -7 17 71.48 7.51 -7 -7 16 27.49 4.57 7 7 -16 28.62 5.48 -7 -7 16 19.53 3.82 7 7 -15 29.74 5.39 -7 -7 15 23.44 4.10 -7 -7 14 0.85 0.99 7 7 -14 0.69 1.40 -7 -7 14 2.02 1.37 -7 -7 13 39.59 4.86 7 7 -13 41.69 5.89 -7 -7 13 38.75 4.85 -7 -7 12 0.23 0.80 -7 -7 12 1.05 1.26 7 7 -12 3.21 1.89 -7 -7 11 10.02 2.48 7 7 -11 14.30 3.15 -7 -7 11 14.51 2.76 -7 -7 10 1.14 1.15 -7 -7 10 2.88 1.63 7 7 -10 5.69 2.26 7 -7 -9 58.55 6.30 -7 -7 9 68.24 5.75 7 7 -9 57.38 6.13 -7 -7 9 62.69 5.45 7 -7 -8 8.70 2.42 -7 -7 8 11.77 2.52 7 7 -8 11.95 2.99 -7 -7 8 14.29 2.55 -7 -7 7 46.33 4.38 7 -7 -7 38.39 4.90 -7 -7 7 38.95 4.16 7 7 -7 42.38 4.96 7 -7 -6 109.62 8.08 -7 -7 6 124.08 7.32 7 7 -6 134.86 8.62 7 -7 -5 27.48 3.94 -7 -7 5 30.59 3.19 -7 -7 5 26.56 3.50 -7 7 5 13.24 1.10 -7 7 5 12.05 1.12 7 7 -5 23.64 3.72 7 -7 -4 19.41 3.25 -7 -7 4 16.36 2.65 -7 -7 4 18.62 2.44 7 7 -4 20.05 3.34 -7 7 4 16.38 1.70 -7 7 4 18.48 1.37 -7 7 3 3.03 0.95 -7 -7 3 1.09 0.60 -7 7 3 3.89 0.86 -7 -7 3 4.29 1.69 7 -7 -3 6.11 1.85 7 7 -3 5.37 1.73 7 -7 -2 18.27 3.18 -7 -7 2 18.03 2.78 -7 7 2 14.39 1.99 7 7 -2 11.51 2.40 -7 7 2 14.73 2.01 7 7 -1 192.25 6.70 -7 -7 1 220.55 9.85 7 -7 -1 200.46 10.02 7 7 -1 215.84 9.95 7 7 0 245.07 11.78 -7 -7 0 241.88 10.42 7 -7 0 224.35 10.38 7 7 0 229.49 10.21 7 7 1 200.73 5.79 7 7 1 222.57 11.05 -7 -7 -1 237.53 10.37 7 -7 1 191.08 9.57 7 7 1 202.14 9.48 7 -7 2 52.56 3.26 7 7 2 44.08 2.37 -7 -7 -2 61.37 5.16 7 7 2 63.20 5.81 -7 -7 -2 70.33 5.91 7 -7 2 50.91 5.06 7 7 2 53.77 4.88 7 7 3 1.84 1.13 7 -7 3 0.04 0.39 -7 -7 -3 4.59 1.60 7 7 3 3.49 1.96 -7 -7 -3 6.04 1.79 7 -7 3 3.01 1.46 7 7 4 333.07 12.35 -7 -7 -4 337.44 12.44 7 -7 4 332.39 9.33 7 7 4 345.86 13.58 7 -7 4 317.69 12.37 7 -7 5 11.14 2.40 -7 -7 -5 6.70 1.75 -7 -7 -5 12.65 2.86 7 7 5 9.23 2.30 7 -7 5 5.81 1.24 7 7 5 6.21 1.86 7 7 6 5.26 1.90 7 -7 6 3.99 1.78 -7 -7 -6 4.71 1.74 -7 -7 -6 5.82 2.09 7 7 6 2.42 1.37 7 -7 7 6.06 1.89 -7 -7 -7 6.20 1.94 -7 -7 -7 5.58 1.90 7 7 7 4.11 1.94 -7 -7 -8 6.35 2.02 -7 -7 -8 6.96 2.06 7 -7 8 3.97 1.59 7 7 8 4.22 1.70 -7 -7 -9 1.60 1.25 -7 -7 -9 4.62 1.78 7 7 9 2.30 1.59 -7 7 -9 1.64 1.62 7 -7 9 2.51 1.72 -7 -7 -10 1.01 1.49 7 7 10 2.44 2.17 7 -7 10 1.00 1.46 -7 7 -10 2.43 1.61 -7 -7 -11 9.28 2.56 7 7 11 5.21 2.41 7 -7 11 3.22 1.57 -7 7 -11 4.87 2.25 7 7 12 1.03 1.66 -7 7 -12 0.02 1.93 7 -7 12 2.47 2.02 7 7 13 30.94 5.57 7 -7 13 21.33 3.94 7 7 14 2.90 1.87 -7 -8 18 13.21 3.62 -7 -8 17 6.66 2.33 -7 -8 16 138.55 9.92 7 8 -16 129.82 12.34 -7 -8 16 167.19 11.74 -7 -8 15 5.58 2.39 7 8 -15 8.78 3.33 -7 -8 14 62.56 6.32 7 8 -14 60.16 7.38 -7 -8 14 54.13 5.98 7 -8 -13 56.93 6.87 -7 -8 13 71.76 6.69 7 8 -13 73.94 7.92 -7 -8 13 69.81 6.68 7 -8 -12 166.97 11.12 -7 -8 12 169.75 9.99 7 8 -12 173.17 11.88 7 -8 -11 5.98 2.49 -7 -8 11 10.99 2.55 -7 -8 11 11.95 2.73 7 8 -11 7.82 2.71 7 -8 -10 184.19 11.41 -7 -8 10 180.58 9.79 7 8 -10 155.31 10.69 -7 -8 10 177.88 9.48 7 -8 -9 82.32 7.43 -7 -8 9 83.99 6.56 7 8 -9 87.89 7.89 -7 -8 9 83.15 6.31 7 -8 -8 1.50 1.65 -7 -8 8 1.95 1.20 -7 -8 8 1.16 1.24 7 8 -8 1.11 1.27 7 -8 -7 11.10 2.82 -7 -8 7 12.07 2.51 7 8 -7 14.94 3.51 -7 -8 7 13.21 2.43 7 -8 -6 0.33 1.08 -7 -8 6 0.82 1.34 7 8 -6 0.43 1.07 -7 -8 6 0.99 0.91 -7 -8 5 11.52 2.33 7 -8 -5 11.53 2.51 -7 -8 5 15.49 2.79 7 8 -5 11.86 2.72 7 -8 -4 56.03 5.67 -7 -8 4 59.64 4.43 -7 -8 4 56.28 5.24 7 8 -4 57.57 5.79 -7 -8 3 144.79 8.27 7 -8 -3 149.95 9.10 -7 8 3 153.29 5.67 7 8 -3 146.43 8.74 -7 -8 3 160.73 6.96 7 -8 -2 63.15 5.83 -7 8 2 85.81 4.83 7 8 -2 71.60 5.95 -7 -8 2 81.75 6.30 -7 -8 1 34.47 4.19 7 -8 -1 28.31 3.91 -7 8 1 39.18 3.60 7 8 -1 31.52 3.90 7 8 0 0.65 1.45 -7 -8 0 0.68 0.81 7 -8 0 2.51 1.38 7 8 0 1.31 1.29 7 8 1 47.88 5.41 -7 -8 -1 46.72 4.92 7 -8 1 51.45 5.11 7 8 1 37.07 4.28 7 8 2 3.00 1.60 7 -8 2 4.27 1.08 7 8 2 3.65 1.81 -7 -8 -2 6.51 2.02 -7 -8 -2 4.81 1.81 7 -8 2 5.08 1.90 7 8 3 0.71 0.90 7 -8 3 1.74 0.85 -7 -8 -3 -0.59 1.40 7 8 3 0.15 1.24 -7 -8 -3 1.26 0.93 7 -8 3 1.41 1.13 7 8 4 32.05 3.99 -7 -8 -4 36.19 4.33 7 -8 4 31.75 3.26 -7 -8 -4 45.51 5.15 7 8 4 35.42 4.58 7 -8 4 30.47 3.91 7 8 5 20.22 3.34 -7 -8 -5 19.75 3.20 -7 -8 -5 20.68 3.73 7 8 5 14.76 3.08 -7 8 -5 23.99 3.86 7 -8 5 18.03 3.22 7 8 6 82.90 6.52 7 8 6 95.99 7.68 -7 -8 -6 86.73 6.89 -7 -8 -6 94.19 7.50 -7 8 -6 113.48 8.58 7 -8 6 87.46 6.90 -7 -8 -7 11.30 2.99 -7 -8 -7 7.29 2.21 7 8 7 6.98 2.38 -7 8 -7 5.22 2.36 7 -8 7 7.63 2.13 7 -8 8 148.37 9.49 -7 -8 -8 134.12 9.31 7 8 8 145.59 9.79 -7 8 -8 172.11 11.35 -7 -8 -9 8.31 2.62 -7 -8 -9 10.44 2.80 7 -8 9 10.39 2.81 7 8 9 9.38 2.66 -7 8 -9 9.62 3.14 7 -8 10 119.03 8.80 -7 -8 -10 145.74 9.69 7 8 10 132.06 9.90 -7 8 -10 140.37 11.09 -7 -8 -11 33.62 4.82 7 -8 11 21.72 4.25 7 8 11 20.26 4.01 -7 8 -11 29.00 5.11 7 8 12 8.02 2.83 -7 8 -12 14.67 3.91 7 -8 12 10.94 2.99 7 8 13 1.18 1.96 -7 -9 17 29.71 4.97 -7 -9 16 59.30 6.67 -7 -9 16 57.33 6.77 -7 -9 15 1.68 1.73 -7 -9 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9 0 91.74 7.82 -7 -9 0 99.07 7.47 -7 9 0 100.00 6.16 7 -9 0 90.59 6.99 7 9 0 93.88 7.07 7 9 1 6.55 2.27 7 -9 1 5.50 1.35 7 9 1 7.04 2.34 -7 -9 -1 7.62 2.30 -7 9 -1 4.88 1.71 7 -9 1 5.00 1.70 7 -9 2 80.05 4.83 -7 -9 -2 79.26 6.55 7 9 2 83.29 7.08 -7 -9 -2 90.53 7.41 -7 9 -2 81.19 6.24 7 -9 2 76.39 6.43 7 9 2 81.55 6.37 -7 -9 -3 50.57 5.75 -7 -9 -3 44.62 4.94 7 9 3 50.81 5.68 -7 9 -3 45.50 4.99 7 -9 3 42.83 4.82 7 9 3 38.32 4.35 7 -9 4 7.70 2.27 7 9 4 4.92 1.95 -7 -9 -4 12.84 2.81 7 -9 4 6.25 1.84 7 9 4 5.18 1.99 -7 -9 -4 9.59 2.51 -7 9 -4 6.78 2.05 7 9 5 110.50 7.45 -7 -9 -5 112.45 8.68 -7 -9 -5 119.81 8.34 7 9 5 99.86 7.95 -7 9 -5 132.48 8.88 7 -9 5 101.28 7.69 7 9 6 25.26 3.74 -7 -9 -6 39.13 4.87 -7 -9 -6 39.46 5.23 7 9 6 31.38 4.53 -7 9 -6 33.75 4.67 7 -9 6 31.76 4.37 -7 -9 -7 300.77 13.82 -7 -9 -7 256.76 13.52 7 9 7 240.72 12.59 -7 9 -7 296.84 14.54 7 -9 7 272.69 13.02 -7 -9 -8 1.10 2.01 7 9 8 1.18 1.51 -7 -9 -8 0.48 1.85 7 -9 8 0.21 1.06 -7 9 -8 -1.05 1.79 -7 -9 -9 180.07 11.11 -7 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45.32 5.36 7 11 -7 60.72 7.13 -7 -11 7 52.75 5.23 -7 -11 6 223.70 11.97 7 -11 -6 191.60 10.68 7 11 -6 204.66 12.33 -7 -11 6 210.74 10.05 -7 -11 5 1.37 1.79 7 -11 -5 3.12 1.64 -7 -11 5 0.73 0.90 7 11 -5 -0.93 1.22 -7 -11 4 77.68 7.17 7 -11 -4 70.18 6.49 7 11 -4 69.92 6.92 -7 -11 3 1.27 1.46 -7 -11 3 -0.17 0.83 7 -11 -3 -0.37 1.14 -7 -11 2 229.48 12.47 7 -11 -2 222.79 11.59 7 11 -2 237.77 12.02 7 11 -1 5.56 2.38 -7 -11 1 4.04 2.23 7 -11 -1 2.08 1.46 7 11 -1 7.34 2.28 7 -11 0 98.81 6.91 -7 -11 0 91.09 8.08 7 -11 0 82.58 7.09 7 11 0 99.13 7.83 7 11 1 1.26 1.01 7 -11 1 -0.41 1.16 7 11 1 0.12 1.23 7 -11 1 0.49 0.99 -7 -11 -1 3.45 2.34 7 11 2 114.48 9.05 -7 -11 -2 120.31 9.53 -7 11 -2 96.09 7.01 7 -11 2 92.96 7.47 7 11 2 100.56 7.51 -7 -11 -3 37.75 5.22 7 11 3 44.80 5.65 -7 -11 -3 35.04 5.35 -7 11 -3 32.15 4.49 7 -11 3 36.32 4.78 7 11 3 34.73 4.36 7 11 4 156.61 9.22 7 11 4 159.74 10.64 -7 11 -4 180.50 10.42 -7 -11 -4 180.86 12.28 7 -11 4 149.56 9.57 -7 -11 -4 170.14 10.88 7 11 5 27.16 4.06 -7 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13.39 1.86 8 5 -4 6.72 1.84 8 -5 -3 269.47 12.23 -8 5 3 306.48 8.51 -8 -5 3 267.43 9.65 8 -5 -3 275.49 7.82 8 5 -3 292.43 11.38 8 5 -2 74.42 6.20 8 -5 -2 56.67 5.52 -8 5 2 61.62 4.10 -8 -5 2 59.31 4.55 8 -5 -2 53.59 3.89 8 5 -2 56.23 4.97 8 5 -1 34.02 3.29 8 -5 -1 37.44 4.43 8 5 -1 26.84 3.75 -8 -5 1 34.14 3.45 8 -5 -1 32.65 3.24 8 5 -1 37.51 4.17 8 5 0 -0.72 0.78 8 5 0 0.40 0.83 8 5 0 0.51 0.49 8 5 0 1.86 1.07 -8 -5 0 0.79 0.97 8 -5 0 1.67 1.00 8 -5 0 1.20 1.39 8 5 1 31.18 2.41 8 5 1 27.95 3.76 8 5 1 16.48 2.60 -8 -5 -1 34.57 3.46 8 -5 1 33.21 3.69 8 -5 1 9.74 1.77 8 -5 1 36.56 4.26 8 5 1 33.25 3.78 8 5 2 94.86 6.39 8 5 2 104.83 4.93 8 5 2 100.98 7.08 -8 -5 -2 111.90 6.17 8 5 2 81.63 3.69 8 -5 2 112.20 6.99 8 -5 2 94.06 6.61 8 5 3 67.36 5.60 8 5 3 73.82 6.14 -8 -5 -3 80.89 5.26 8 5 3 74.06 3.52 8 5 3 25.94 1.97 8 -5 3 79.09 6.35 8 -5 3 65.60 5.57 8 -5 3 7.09 1.34 8 5 4 122.61 7.56 -8 5 -4 119.85 7.02 8 -5 4 96.44 3.09 -8 -5 -4 154.03 7.39 8 5 4 125.45 8.12 8 -5 4 167.13 9.61 8 -5 4 113.50 7.28 8 5 4 113.62 3.51 8 5 5 142.68 8.33 -8 5 -5 153.19 8.36 -8 -5 -5 179.47 7.95 8 5 5 143.46 8.86 8 -5 5 175.90 10.05 8 -5 5 138.98 8.33 -8 5 -6 35.00 4.29 -8 -5 -6 41.48 4.10 -8 -5 -6 41.37 3.85 8 5 6 30.35 4.21 8 -5 6 41.82 5.21 8 -5 6 35.86 4.03 -8 -5 -7 23.10 3.22 -8 5 -7 14.39 2.96 -8 -5 -7 18.29 2.62 8 5 7 20.21 3.49 8 -5 7 26.26 4.56 8 -5 7 17.09 2.92 -8 5 -8 77.16 6.79 -8 -5 -8 82.79 5.95 8 5 8 89.30 7.55 8 -5 8 78.61 7.86 8 -5 8 77.70 6.08 8 -5 9 15.76 3.32 -8 -5 -9 22.62 3.34 -8 5 -9 16.45 3.47 8 5 9 15.94 3.55 8 -5 9 18.82 4.10 -8 5 -10 1.28 1.29 8 -5 10 2.34 1.73 8 5 10 0.45 1.13 8 -5 10 5.09 2.43 8 -5 11 83.57 6.93 -8 5 -11 89.54 8.30 8 5 11 81.30 7.97 8 -5 12 19.78 3.85 -8 5 -12 19.28 4.22 8 5 12 23.51 4.50 8 -5 13 33.51 4.53 8 5 13 39.73 6.21 8 -5 14 2.10 2.00 -8 -6 19 21.07 5.45 8 6 -18 13.79 4.12 -8 -6 18 16.27 3.64 -8 -6 18 14.23 3.50 -8 -6 17 6.79 2.61 8 6 -17 8.94 3.44 -8 -6 16 1.41 1.46 8 6 -16 2.60 2.36 -8 -6 16 3.02 1.81 -8 -6 15 55.37 6.15 -8 -6 15 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29.08 3.18 8 6 -1 29.94 3.72 8 6 0 167.65 6.68 8 6 0 183.02 10.14 -8 -6 0 163.18 7.95 8 -6 0 158.47 8.96 8 6 0 176.12 6.16 8 6 0 169.33 8.89 8 6 1 131.04 4.84 8 6 1 137.83 8.54 -8 -6 -1 152.37 7.76 8 -6 1 83.49 6.41 8 -6 1 157.17 8.03 8 6 1 89.96 3.89 8 6 1 126.63 7.59 8 6 2 105.33 4.55 -8 -6 -2 139.92 7.55 8 6 2 135.04 8.53 8 -6 2 128.02 7.83 8 -6 2 121.65 7.80 8 6 2 98.21 6.71 8 6 3 158.50 8.65 8 -6 3 137.21 3.46 8 6 3 160.42 9.23 -8 -6 -3 187.56 8.83 8 -6 3 180.82 9.61 8 -6 3 176.71 9.39 8 6 4 198.63 9.74 8 6 4 180.05 9.96 8 -6 4 147.88 5.16 -8 -6 -4 216.51 9.45 8 -6 4 197.04 10.54 8 -6 4 169.93 9.22 8 6 5 201.96 10.01 -8 -6 -5 233.42 10.01 -8 -6 -5 227.34 9.80 8 6 5 199.08 10.68 8 -6 5 248.04 12.42 8 -6 5 204.11 10.01 8 -6 6 -0.13 0.91 -8 -6 -6 -0.22 0.92 -8 -6 -6 1.30 1.16 8 6 6 -0.32 1.26 8 -6 6 1.68 1.38 8 -6 7 0.97 1.45 -8 -6 -7 -0.92 1.28 -8 -6 -7 1.82 1.25 8 6 7 -0.98 1.56 8 -6 8 2.66 1.45 -8 -6 -8 0.93 1.26 -8 6 -8 1.53 1.47 8 6 8 1.48 1.75 -8 -6 -9 8.61 2.28 -8 6 -9 8.23 2.54 8 -6 9 5.76 1.84 8 6 9 9.80 2.89 8 -6 10 34.38 4.52 -8 6 -10 26.85 4.54 -8 -6 -10 28.00 4.00 8 6 10 32.73 5.11 -8 6 -11 -1.57 1.57 8 6 11 0.77 1.78 8 -6 11 0.41 1.04 -8 6 -12 10.19 3.39 8 6 12 18.85 4.30 -8 6 -12 19.02 4.63 8 -6 12 19.53 3.77 8 -6 13 38.47 5.30 8 6 13 45.89 6.73 -8 -7 18 25.71 4.61 -8 -7 17 10.14 2.95 8 7 -17 13.08 4.40 -8 -7 17 8.21 3.19 -8 -7 16 51.58 6.21 -8 -7 16 54.25 6.35 8 7 -16 50.56 7.07 -8 -7 15 0.54 1.44 8 7 -15 -1.55 2.19 -8 -7 15 2.17 1.71 -8 -7 14 182.75 11.24 -8 -7 14 169.99 10.44 8 7 -14 158.88 11.90 -8 -7 13 69.64 7.02 -8 -7 13 69.40 6.46 8 7 -13 66.18 7.78 -8 -7 12 96.67 7.88 -8 -7 12 76.73 6.61 8 7 -12 78.24 8.15 -8 -7 11 238.78 11.84 -8 -7 11 225.74 11.12 8 7 -11 224.71 13.03 -8 -7 10 50.65 5.14 8 7 -10 41.68 5.58 8 -7 -9 151.20 10.43 -8 -7 9 173.91 9.30 -8 -7 9 164.24 9.03 8 7 -9 166.89 10.58 8 -7 -8 98.03 8.30 -8 -7 8 116.60 7.28 8 7 -8 95.01 7.82 -8 -7 7 79.39 6.13 -8 -7 7 93.34 6.27 8 7 -7 81.14 7.10 -8 -7 6 5.18 1.71 8 -7 -6 1.55 1.38 -8 -7 6 4.80 1.85 8 7 -6 2.83 1.59 8 -7 -5 20.42 3.55 -8 -7 5 26.79 3.20 -8 -7 5 27.58 3.53 8 7 -5 19.76 3.39 8 -7 -4 64.56 6.25 -8 -7 4 59.85 5.26 8 7 -4 69.35 6.17 8 -7 -3 153.37 9.46 -8 -7 3 181.72 9.04 8 7 -3 170.05 9.27 8 -7 -2 99.66 7.61 -8 -7 2 107.11 6.95 8 7 -2 98.56 7.10 8 7 -1 17.94 3.42 -8 -7 1 22.58 3.26 8 -7 -1 24.57 3.76 8 7 -1 22.57 3.48 8 7 0 2.74 1.13 8 7 0 9.34 2.40 -8 -7 0 7.05 1.81 8 -7 0 3.79 1.59 8 7 1 2.46 1.42 8 7 1 1.13 0.56 8 7 1 3.85 1.79 -8 -7 -1 -0.14 1.11 8 -7 1 0.46 0.94 8 7 2 151.29 9.37 8 -7 2 141.04 8.64 -8 -7 -2 170.66 8.85 8 7 2 144.92 8.30 8 7 3 6.11 1.89 8 7 3 1.44 1.12 -8 -7 -3 5.51 1.65 8 -7 3 3.62 1.55 8 7 4 83.54 6.61 8 -7 4 84.28 4.55 8 7 4 97.19 7.59 8 -7 4 76.38 6.45 8 7 5 112.09 7.61 -8 -7 -5 142.91 8.40 8 7 5 124.09 8.67 8 -7 5 126.48 8.11 8 -7 6 3.72 1.51 -8 -7 -6 8.07 2.30 -8 -7 -6 5.35 1.61 8 7 6 4.53 1.79 8 -7 7 4.19 1.53 -8 -7 -7 6.20 2.01 -8 -7 -7 1.83 1.73 8 7 7 1.49 1.94 8 -7 8 0.29 0.94 -8 -7 -8 0.77 1.03 -8 -7 -8 2.66 2.10 8 7 8 1.89 1.85 -8 -7 -9 1.10 1.28 8 -7 9 -0.69 1.41 8 7 9 1.43 2.00 8 -7 10 42.69 5.19 -8 -7 -10 53.92 5.92 8 7 10 33.95 5.35 -8 7 -10 47.54 6.58 8 -7 11 35.89 5.12 8 7 11 49.91 6.34 -8 7 -11 46.53 6.82 8 7 12 5.41 2.49 8 -7 12 2.92 2.03 -8 -8 17 -0.03 1.92 -8 -8 16 25.29 4.58 8 8 -16 22.24 4.78 -8 -8 16 16.00 3.76 -8 -8 15 85.18 8.43 -8 -8 15 80.19 7.54 8 8 -15 81.93 9.05 -8 -8 14 4.43 1.85 -8 -8 14 1.62 1.21 8 8 -14 2.64 2.18 8 -8 -13 31.73 5.29 -8 -8 13 43.79 5.59 -8 -8 13 32.90 4.82 8 8 -13 49.48 6.85 -8 -8 12 7.36 2.47 8 -8 -12 5.61 2.64 -8 -8 12 4.89 2.36 8 8 -12 5.66 2.46 -8 -8 11 9.40 2.67 8 -8 -11 3.04 2.15 -8 -8 11 8.55 2.33 8 8 -11 6.70 3.03 -8 -8 10 65.28 6.25 8 -8 -10 52.78 6.33 -8 -8 10 65.33 6.01 8 8 -10 52.54 6.32 8 -8 -9 46.25 5.87 -8 -8 9 57.54 5.77 -8 -8 9 43.83 4.84 8 8 -9 46.17 5.78 8 -8 -8 107.95 8.71 -8 -8 8 124.12 7.79 -8 -8 8 120.12 7.82 8 8 -8 111.23 8.80 8 -8 -7 56.14 6.14 -8 -8 7 43.83 4.72 -8 -8 7 56.07 5.04 8 8 -7 51.87 5.93 8 -8 -6 62.88 6.37 -8 -8 6 78.27 6.28 -8 -8 6 81.76 5.94 8 8 -6 79.14 6.96 -8 -8 5 -0.67 1.19 8 -8 -5 0.29 0.85 -8 -8 5 1.88 1.50 8 8 -5 0.29 1.10 8 -8 -4 98.70 7.80 -8 -8 4 82.49 6.39 -8 8 4 79.89 4.07 -8 -8 4 111.16 6.34 8 8 -4 97.97 7.53 8 -8 -3 54.29 5.81 -8 -8 3 41.59 4.61 8 8 -3 45.15 4.99 -8 -8 2 200.97 9.96 8 -8 -2 186.55 10.41 8 8 -2 171.26 9.54 -8 -8 1 201.03 10.03 8 -8 -1 182.01 10.06 8 8 -1 179.91 9.83 8 8 0 137.95 9.47 -8 -8 0 124.81 8.04 8 -8 0 114.53 7.96 8 8 0 107.06 7.84 8 8 1 135.62 9.19 -8 -8 -1 134.57 8.36 8 -8 1 122.76 8.30 8 8 1 124.25 7.95 8 -8 2 47.10 3.34 8 8 2 48.54 5.53 -8 -8 -2 55.77 5.54 8 -8 2 40.96 4.86 8 8 2 37.15 4.42 8 8 3 25.71 3.76 8 8 3 25.74 3.96 -8 -8 -3 18.31 3.22 8 -8 3 29.61 4.11 8 -8 4 0.14 1.14 8 8 4 0.61 1.00 -8 -8 -4 2.98 1.74 8 8 4 0.87 1.34 -8 -8 -4 2.08 1.65 8 -8 5 0.79 1.01 8 8 5 1.73 1.58 -8 -8 -5 1.25 1.18 8 8 5 2.18 1.76 -8 -8 -5 0.87 1.32 8 8 6 8.34 2.43 8 -8 6 10.52 2.55 -8 -8 -6 14.32 3.06 -8 -8 -6 9.97 2.71 8 8 6 9.34 2.66 8 -8 7 3.89 2.03 -8 -8 -7 8.54 2.43 -8 -8 -7 7.60 2.60 8 8 7 5.78 2.27 -8 8 -7 7.78 2.85 -8 -8 -8 1.70 1.38 8 -8 8 5.52 2.05 -8 -8 -8 4.70 2.07 8 8 8 1.29 1.22 -8 8 -8 2.78 1.98 -8 -8 -9 9.38 2.84 8 -8 9 4.90 2.36 8 8 9 3.64 1.90 -8 8 -9 4.23 2.44 8 -8 10 62.80 6.74 -8 -8 -10 79.58 7.34 8 8 10 57.87 6.81 -8 8 -10 73.49 8.29 8 -8 11 105.10 9.09 8 8 11 104.66 9.28 8 8 12 2.57 2.39 -8 -9 16 12.14 3.30 -8 -9 15 31.02 5.09 8 9 -15 35.72 6.52 -8 -9 15 17.97 3.76 -8 -9 14 17.60 4.15 -8 -9 14 18.82 3.84 8 9 -14 12.39 3.74 8 -9 -13 8.31 3.25 -8 -9 13 15.02 3.32 -8 -9 13 14.28 3.36 8 -9 -12 7.13 2.81 -8 -9 12 6.57 2.28 8 9 -12 4.52 2.55 -8 -9 12 5.78 2.12 -8 -9 11 78.86 7.24 8 -9 -11 72.83 7.65 -8 -9 11 74.93 6.84 8 9 -11 71.30 8.21 8 -9 -10 0.15 1.30 -8 -9 10 3.55 1.88 8 9 -10 0.10 1.89 -8 -9 10 -1.78 1.67 -8 -9 9 307.68 13.40 8 -9 -9 277.41 13.91 -8 -9 9 274.98 12.54 8 9 -9 272.74 15.48 -8 -9 8 4.82 1.62 8 -9 -8 5.47 2.53 -8 -9 8 4.64 1.94 8 9 -8 5.99 2.55 8 -9 -7 277.90 13.68 -8 -9 7 303.90 13.04 8 9 -7 299.95 14.52 8 -9 -6 33.27 4.83 -8 -9 6 27.34 4.00 -8 -9 6 31.46 3.70 8 9 -6 28.37 4.56 8 -9 -5 66.11 6.61 -8 -9 5 75.97 6.54 8 9 -5 72.05 6.85 -8 -9 5 77.63 5.64 -8 -9 4 1.03 1.18 -8 -9 4 1.59 1.06 8 -9 -4 0.11 0.93 8 9 -4 0.57 1.52 -8 -9 3 2.29 1.17 8 -9 -3 5.31 1.98 8 9 -3 4.81 1.61 -8 -9 2 25.73 3.95 8 -9 -2 27.25 4.13 -8 9 2 27.11 2.97 8 9 -2 24.89 3.88 8 9 -1 26.69 4.52 -8 -9 1 23.74 3.73 8 -9 -1 29.52 4.23 -8 9 1 28.57 3.33 8 9 -1 24.13 3.86 -8 -9 0 23.75 3.85 8 9 0 16.57 3.47 -8 9 0 14.75 2.71 8 -9 0 18.80 3.43 8 9 0 15.40 3.22 8 -9 1 30.18 3.13 8 9 1 38.82 5.13 -8 -9 -1 33.91 4.65 -8 9 -1 36.28 4.28 8 -9 1 35.53 4.64 8 9 1 38.05 4.62 8 9 2 0.88 1.07 8 9 2 -1.35 1.56 -8 -9 -2 0.87 1.13 -8 9 -2 2.66 1.36 8 -9 2 -0.26 1.00 8 9 3 -0.26 1.01 8 9 3 2.09 1.39 -8 -9 -3 2.65 1.82 -8 9 -3 2.00 1.68 8 -9 3 -0.27 1.08 8 9 4 28.06 4.02 -8 -9 -4 28.99 4.36 -8 -9 -4 30.09 4.47 8 9 4 16.84 3.49 -8 9 -4 36.71 4.85 8 -9 4 30.94 4.25 8 9 5 6.07 2.13 8 -9 5 12.71 2.86 -8 -9 -5 7.12 2.42 8 9 5 6.51 2.49 -8 -9 -5 7.30 2.57 -8 9 -5 6.00 1.95 8 9 6 40.16 4.88 -8 -9 -6 31.20 4.54 -8 -9 -6 42.60 5.43 8 9 6 44.19 5.60 -8 9 -6 35.82 5.11 8 -9 6 34.75 4.64 8 -9 7 2.81 1.38 -8 -9 -7 1.12 1.44 -8 -9 -7 1.31 1.60 8 9 7 2.00 1.61 -8 9 -7 5.29 2.43 -8 -9 -8 26.35 4.35 8 -9 8 15.77 3.51 -8 -9 -8 12.28 3.06 8 9 8 19.08 4.10 -8 9 -8 21.54 4.62 -8 -9 -9 11.67 3.23 8 -9 9 10.56 3.14 8 9 9 13.77 3.81 -8 9 -9 15.68 4.01 -8 -9 -10 -1.25 1.78 8 9 10 0.71 2.15 8 -9 10 1.35 2.19 -8 9 -10 -0.30 1.97 8 9 11 10.04 3.38 -8 -10 15 3.55 1.90 -8 -10 14 59.95 7.42 -8 -10 14 49.05 6.15 -8 -10 13 44.84 5.92 -8 -10 13 37.98 5.40 8 10 -13 29.71 5.75 -8 -10 12 57.75 6.44 8 -10 -12 32.01 5.04 -8 -10 12 44.53 5.59 8 10 -12 50.81 7.36 8 -10 -11 2.98 2.26 -8 -10 11 0.58 1.23 8 10 -11 1.08 2.44 -8 -10 11 1.36 1.33 -8 -10 10 52.02 5.77 8 -10 -10 36.58 5.39 -8 -10 10 39.93 5.20 8 10 -10 46.48 6.48 -8 -10 9 10.25 2.77 8 -10 -9 8.19 2.79 -8 -10 9 12.09 2.97 8 10 -9 14.34 4.07 -8 -10 8 41.10 4.96 8 -10 -8 35.81 5.20 -8 -10 8 35.43 4.70 8 10 -8 34.78 5.51 -8 -10 7 -0.52 1.26 -8 -10 7 0.01 1.13 8 -10 -7 -1.49 1.53 8 10 -7 -0.72 1.55 8 -10 -6 117.17 9.11 -8 -10 6 123.45 8.72 -8 -10 6 138.83 8.11 8 10 -6 125.18 9.40 -8 -10 5 3.98 1.81 8 -10 -5 1.40 1.84 -8 -10 5 4.89 1.53 8 10 -5 5.10 2.44 -8 -10 4 44.22 4.22 -8 -10 4 35.50 4.82 8 -10 -4 41.07 5.09 8 10 -4 38.62 5.19 -8 -10 3 105.30 8.10 8 -10 -3 85.46 7.24 8 10 -3 93.09 7.65 8 -10 -2 107.38 8.18 8 10 -2 95.99 8.45 8 10 -1 38.28 5.48 -8 -10 1 50.04 5.62 8 -10 -1 41.97 5.13 8 10 -1 54.16 5.74 8 10 0 1.44 1.45 8 10 0 0.33 1.55 -8 -10 0 1.20 1.66 -8 10 0 0.10 1.25 8 -10 0 1.91 1.42 8 10 1 88.11 8.09 -8 -10 -1 81.94 7.38 -8 10 -1 65.85 5.65 8 -10 1 67.42 6.47 8 10 1 82.79 7.02 8 10 2 31.56 4.80 -8 -10 -2 24.51 4.29 -8 10 -2 19.84 3.44 8 -10 2 22.89 3.98 8 10 2 27.23 4.09 8 10 3 49.83 5.51 8 10 3 44.74 5.85 -8 -10 -3 56.16 6.32 -8 10 -3 49.33 5.43 8 -10 3 56.40 6.02 8 10 4 2.80 1.44 8 -10 4 3.94 1.77 8 10 4 8.34 3.31 -8 -10 -4 5.36 2.37 -8 10 -4 1.30 1.25 8 10 5 73.70 6.60 -8 -10 -5 89.68 7.76 -8 -10 -5 84.48 7.75 8 10 5 78.31 7.66 -8 10 -5 78.36 7.57 8 -10 5 65.54 6.46 8 10 6 13.21 3.09 8 -10 6 12.31 2.93 -8 -10 -6 14.57 3.33 -8 -10 -6 15.47 3.64 8 10 6 15.71 3.48 -8 10 -6 13.47 3.55 -8 -10 -7 33.44 5.00 -8 -10 -7 35.12 5.10 8 10 7 36.74 5.47 -8 10 -7 30.95 5.02 8 -10 7 28.73 4.44 -8 -10 -8 15.69 3.71 8 -10 8 12.74 3.41 -8 -10 -8 5.45 3.05 8 10 8 12.40 3.58 -8 10 -8 8.75 2.87 -8 -10 -9 39.22 5.63 8 10 9 28.09 4.90 -8 10 -9 30.82 5.89 8 10 10 2.89 2.14 -8 -10 -10 6.75 2.71 -8 -11 13 34.17 5.39 -8 -11 13 24.07 4.55 8 11 -13 30.77 6.00 -8 -11 12 35.52 5.58 -8 -11 12 34.05 5.15 8 11 -12 31.04 5.75 -8 -11 11 22.33 4.14 -8 -11 11 16.87 3.66 8 11 -11 20.60 4.91 -8 -11 10 33.21 4.86 8 -11 -10 26.91 4.72 -8 -11 10 36.58 5.08 8 11 -10 43.63 6.88 -8 -11 9 -0.18 1.62 8 -11 -9 -0.24 1.67 8 11 -9 2.63 2.16 -8 -11 9 1.78 1.68 -8 -11 8 1.60 1.61 -8 -11 8 1.99 1.86 8 -11 -8 1.78 1.54 8 11 -8 -0.85 1.82 -8 -11 7 27.42 4.04 -8 -11 7 14.72 3.22 8 -11 -7 16.45 3.62 8 11 -7 16.18 3.65 -8 -11 6 37.40 5.08 8 -11 -6 45.34 5.58 -8 -11 6 43.18 4.59 8 11 -6 26.32 4.58 -8 -11 5 14.00 3.30 8 -11 -5 13.41 3.08 -8 -11 5 11.38 2.34 8 11 -5 11.51 3.38 -8 -11 4 16.53 3.53 8 -11 -4 16.34 3.51 8 11 -4 20.42 3.87 -8 -11 3 7.73 2.48 8 -11 -3 3.74 1.85 8 11 -3 6.32 2.31 -8 -11 2 76.27 7.37 8 -11 -2 69.69 6.60 8 11 -2 73.26 7.01 -8 -11 1 82.56 7.78 8 11 -1 93.09 9.02 8 -11 -1 74.68 7.05 8 11 -1 70.72 6.85 8 -11 0 46.04 4.60 8 11 0 50.84 6.55 -8 -11 0 44.36 5.75 8 -11 0 39.47 5.23 8 11 0 41.04 5.33 8 11 1 5.30 2.10 8 11 1 5.03 2.14 -8 -11 -1 8.00 2.64 8 -11 1 8.54 2.53 8 11 2 35.11 5.33 -8 -11 -2 38.62 5.32 8 -11 2 30.95 4.61 8 11 2 30.47 4.45 8 11 3 130.46 8.83 8 11 3 138.05 10.51 -8 -11 -3 117.46 9.67 -8 11 -3 114.63 8.18 8 -11 3 123.55 9.13 8 11 4 84.12 7.23 8 11 4 87.46 8.09 -8 -11 -4 95.94 8.66 -8 11 -4 97.82 8.08 8 -11 4 89.27 7.77 8 11 5 9.63 2.73 8 -11 5 9.72 2.68 -8 -11 -5 8.31 2.87 8 11 5 7.09 2.56 -8 -11 -5 12.17 3.49 -8 11 -5 9.30 2.99 -8 -11 -6 42.48 5.90 -8 -11 -6 31.67 5.55 8 11 6 36.55 5.39 -8 11 -6 38.08 5.65 8 -11 6 30.84 5.16 -8 -11 -7 10.68 3.42 8 -11 7 5.82 2.30 -8 -11 -7 9.84 2.98 8 11 7 3.53 2.04 -8 11 -7 3.95 2.49 -8 -11 -8 25.92 4.73 8 11 8 15.91 3.69 -8 11 -8 19.03 4.27 -8 -11 -9 35.46 5.53 8 11 9 19.67 4.37 -8 11 -9 31.77 5.62 -8 -12 12 164.96 11.40 -8 -12 11 27.21 4.67 -8 -12 11 28.37 4.88 8 12 -11 23.57 5.78 -8 -12 10 110.52 8.90 -8 -12 10 95.80 8.81 8 12 -10 94.98 9.77 -8 -12 9 6.34 2.60 8 -12 -9 1.18 1.87 8 12 -9 3.82 2.73 -8 -12 8 96.69 8.18 -8 -12 8 83.60 7.94 8 -12 -8 79.74 7.56 8 12 -8 74.02 8.33 -8 -12 7 7.27 2.36 -8 -12 7 6.46 2.62 8 -12 -7 2.95 1.77 8 12 -7 3.01 2.03 -8 -12 6 34.46 5.24 8 -12 -6 28.21 4.61 8 12 -6 27.61 5.03 -8 -12 5 10.22 2.92 8 -12 -5 7.76 2.50 8 12 -5 9.70 2.97 -8 -12 4 0.42 1.66 8 -12 -4 5.34 2.61 8 12 -4 0.64 1.91 -8 -12 3 55.09 6.64 8 -12 -3 51.56 6.07 8 12 -3 42.26 5.83 8 12 -2 116.19 10.65 -8 -12 2 111.47 9.41 8 -12 -2 105.29 8.37 8 12 -2 109.41 8.97 8 -12 -1 1.47 1.56 8 12 -1 3.76 2.85 -8 -12 1 -2.73 2.37 8 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66.04 6.60 9 6 9 71.93 7.58 9 -6 9 75.23 6.73 9 -6 10 26.84 4.27 -9 6 -10 23.85 4.44 9 6 10 30.95 5.12 9 -6 11 61.16 6.44 -9 6 -11 71.73 7.48 9 6 11 67.88 7.71 9 6 12 1.15 2.76 9 -6 12 -0.64 1.59 -9 -7 17 106.58 9.38 9 7 -17 115.66 11.33 -9 -7 17 131.20 10.64 9 7 -16 17.61 4.65 -9 -7 16 14.72 3.43 -9 -7 16 9.89 3.00 -9 -7 15 7.68 2.42 9 7 -15 8.86 2.98 -9 -7 15 11.48 3.04 -9 -7 14 65.81 6.89 -9 -7 14 79.05 7.45 9 7 -14 77.72 8.47 -9 -7 13 6.88 2.40 9 7 -13 5.10 2.37 -9 -7 13 4.69 1.81 -9 -7 12 -0.52 0.98 9 7 -12 -0.07 1.58 -9 -7 12 -0.94 1.28 -9 -7 11 22.41 3.65 -9 -7 11 23.16 3.78 9 7 -11 22.54 4.12 9 -7 -10 42.65 5.87 -9 -7 10 40.48 4.82 9 7 -10 30.95 4.83 -9 -7 10 37.69 4.56 -9 -7 9 45.55 4.96 9 -7 -9 33.20 5.27 -9 -7 9 42.10 4.73 9 7 -9 34.92 4.91 -9 -7 8 0.84 1.43 9 -7 -8 -1.31 1.81 -9 -7 8 0.33 0.94 9 7 -8 0.72 1.62 9 -7 -7 24.81 4.38 -9 -7 7 31.72 3.96 -9 -7 7 23.50 3.37 9 -7 -6 13.92 3.20 -9 -7 6 13.79 2.57 9 7 -6 13.01 2.93 9 -7 -5 0.28 1.13 -9 -7 5 1.30 0.76 9 7 -5 2.67 1.76 9 -7 -4 61.99 6.35 -9 -7 4 68.38 5.66 9 7 -4 73.95 6.47 9 -7 -3 529.76 18.41 -9 -7 3 565.20 16.14 9 7 -3 579.77 17.94 9 -7 -2 64.45 6.34 -9 -7 2 71.81 5.73 9 7 -2 62.31 5.89 9 7 -1 77.24 7.09 -9 -7 1 77.47 6.04 9 -7 -1 70.61 6.72 9 7 -1 75.47 6.63 9 7 0 50.49 3.75 9 7 0 45.86 5.52 -9 -7 0 61.05 5.38 9 -7 0 43.28 5.15 9 7 0 52.77 5.31 9 7 1 65.47 6.43 -9 -7 -1 76.51 5.95 9 -7 1 59.13 5.87 9 7 1 72.05 6.16 9 7 2 124.28 8.95 -9 -7 -2 101.73 6.86 9 -7 2 106.10 7.76 9 7 2 98.44 7.29 9 7 3 3.18 1.76 9 7 3 0.05 1.32 -9 -7 -3 5.54 1.88 9 -7 3 1.17 1.22 9 7 4 24.46 3.87 9 7 4 34.51 4.82 -9 -7 -4 38.37 4.50 9 -7 4 18.50 3.63 9 7 5 113.39 8.07 9 7 5 120.39 8.87 9 -7 5 107.06 7.68 -9 -7 -5 122.43 7.80 9 -7 6 14.64 2.92 9 7 6 15.87 3.53 -9 -7 -6 15.46 2.81 9 7 7 32.24 4.89 9 -7 7 27.41 4.03 9 7 8 60.13 6.86 9 -7 8 57.74 5.89 9 -7 9 18.69 3.68 9 7 9 15.54 3.65 9 -7 10 27.67 4.46 9 7 10 19.97 4.34 9 7 11 15.25 3.83 9 -7 11 9.48 2.68 -9 7 -11 10.93 3.78 -9 -8 16 17.01 3.69 -9 -8 16 8.45 2.96 9 8 -16 18.54 5.14 -9 -8 15 104.06 8.91 -9 -8 15 96.76 8.52 9 8 -15 110.82 10.61 -9 -8 14 17.48 3.81 -9 -8 14 22.83 4.15 9 8 -14 16.26 4.30 -9 -8 13 31.02 4.60 -9 -8 13 33.85 4.78 9 8 -13 29.53 5.84 9 -8 -13 21.55 4.69 9 -8 -12 0.21 2.14 -9 -8 12 0.15 1.10 -9 -8 12 3.01 1.72 9 8 -12 4.39 2.15 9 -8 -11 6.32 2.40 -9 -8 11 11.34 2.66 -9 -8 11 13.23 2.95 9 8 -11 5.81 2.42 9 -8 -10 3.48 1.56 -9 -8 10 9.86 2.75 -9 -8 10 6.21 2.12 9 8 -10 11.93 3.04 -9 -8 9 3.84 1.54 -9 -8 9 4.66 1.97 9 8 -9 5.56 2.37 -9 -8 8 181.16 9.59 -9 -8 8 167.43 9.51 9 8 -8 158.72 10.69 -9 -8 7 6.48 2.00 9 -8 -7 7.52 2.61 -9 -8 7 12.00 2.62 9 8 -7 9.97 2.71 9 -8 -6 13.06 3.06 -9 -8 6 8.34 2.30 9 8 -6 9.80 2.51 9 -8 -5 94.12 8.04 -9 -8 5 92.98 6.93 9 8 -5 98.15 7.97 9 -8 -4 356.00 15.49 -9 -8 4 337.50 13.23 9 8 -4 348.46 14.64 9 -8 -3 176.28 10.75 -9 -8 3 164.90 9.21 9 8 -3 170.99 10.02 9 8 -2 6.07 2.26 -9 -8 2 7.82 2.03 9 -8 -2 4.68 1.78 9 8 -2 5.29 2.40 -9 -8 1 32.12 4.12 9 -8 -1 22.41 3.70 9 8 -1 32.44 4.29 9 8 0 163.25 10.61 -9 -8 0 137.29 8.35 9 -8 0 140.82 9.25 9 8 0 149.69 9.36 9 8 1 0.30 0.97 9 8 1 -1.10 1.03 -9 -8 -1 1.26 1.13 9 -8 1 -1.00 1.10 9 8 2 110.06 8.77 -9 -8 -2 108.84 7.72 9 -8 2 113.98 8.37 9 8 2 99.61 7.47 9 8 3 10.69 2.41 -9 -8 -3 17.43 3.36 9 8 3 11.06 2.96 9 -8 3 7.21 2.29 9 8 4 46.84 5.24 9 8 4 37.61 5.10 -9 -8 -4 50.95 5.35 9 -8 4 35.59 4.58 9 -8 5 14.37 2.94 9 8 5 13.29 3.18 -9 -8 -5 15.09 3.10 9 8 5 13.06 2.98 -9 -8 -6 65.94 6.27 9 8 6 50.93 6.18 9 -8 6 58.56 6.05 9 -8 7 4.48 1.82 9 8 7 0.35 1.27 9 8 8 148.79 10.78 9 -8 8 115.69 8.85 9 -8 9 4.37 2.19 9 8 9 1.20 1.77 -9 8 -9 1.06 2.32 9 -8 10 0.11 1.32 9 8 10 2.47 1.82 -9 8 -10 -1.53 2.55 9 8 11 114.37 10.33 -9 -9 15 35.81 5.42 -9 -9 15 36.50 5.57 9 9 -15 38.56 6.59 9 -9 -14 61.23 7.80 -9 -9 14 92.68 8.48 -9 -9 14 93.34 8.31 9 9 -14 76.33 9.71 9 -9 -13 22.59 4.73 -9 -9 13 24.90 4.25 -9 -9 13 19.44 3.85 9 9 -13 26.53 5.14 9 -9 -12 11.43 3.35 -9 -9 12 7.92 2.21 -9 -9 12 11.37 3.14 9 9 -12 15.74 4.31 9 -9 -11 1.16 1.83 -9 -9 11 3.01 2.44 -9 -9 11 2.95 2.18 9 9 -11 1.82 2.34 9 -9 -10 10.34 2.98 -9 -9 10 15.09 3.13 -9 -9 10 14.74 3.20 9 9 -10 19.55 4.35 9 -9 -9 18.45 3.83 -9 -9 9 16.68 3.25 -9 -9 9 27.26 4.18 9 9 -9 17.02 3.87 9 -9 -8 15.76 3.52 -9 -9 8 14.80 3.01 9 9 -8 9.47 2.90 -9 -9 8 21.30 3.40 9 -9 -7 0.11 1.28 -9 -9 7 0.74 1.06 -9 -9 7 2.33 1.37 9 9 -7 3.56 2.32 9 -9 -6 26.56 4.54 -9 -9 6 31.93 4.37 -9 -9 6 32.77 4.03 9 9 -6 28.39 4.46 9 -9 -5 66.16 6.84 -9 -9 5 69.35 6.34 9 9 -5 50.53 5.80 -9 -9 4 19.22 3.46 9 -9 -4 16.45 3.47 9 9 -4 25.10 4.06 -9 -9 3 139.99 8.92 9 9 -3 123.47 8.96 9 9 -2 3.11 1.33 -9 -9 2 2.11 1.26 -9 9 2 0.07 0.93 9 -9 -2 1.54 1.24 9 9 -2 0.26 1.08 9 9 -1 29.42 4.94 -9 -9 1 24.58 3.93 -9 9 1 16.36 2.68 9 -9 -1 15.33 3.27 9 9 -1 15.96 3.18 9 9 0 26.37 4.53 -9 -9 0 27.35 4.06 9 -9 0 14.65 3.28 9 9 0 20.77 3.76 9 9 1 171.82 11.06 -9 -9 -1 199.83 10.98 9 -9 1 181.08 10.80 9 9 1 175.73 10.14 9 9 2 -0.80 1.26 9 9 2 -1.20 1.84 -9 -9 -2 0.66 1.48 9 -9 2 0.53 0.97 9 9 3 111.81 8.32 9 9 3 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158.49 9.32 10 -8 2 147.47 9.98 10 8 3 15.26 3.44 10 8 3 17.01 3.57 -10 -8 -3 17.93 3.23 10 -8 3 14.81 3.36 10 8 4 50.42 5.82 10 8 4 46.04 6.03 -10 -8 -4 56.94 5.61 10 -8 4 51.51 5.72 10 -8 5 9.12 2.58 10 8 5 11.37 2.86 10 8 5 10.16 3.01 -10 -8 -5 8.39 2.24 10 8 6 62.50 7.07 10 -8 6 68.80 6.67 10 -8 7 14.59 3.53 10 8 7 16.14 3.99 10 -8 8 10.47 2.76 10 8 8 5.82 2.26 10 -8 9 1.23 1.48 10 8 9 3.73 2.46 -10 8 -9 0.53 2.24 -10 -9 15 0.52 1.60 -10 -9 15 -0.33 1.57 -10 -9 14 9.68 3.12 10 -9 -14 6.85 3.31 -10 -9 14 16.30 3.93 10 9 -14 15.77 4.39 10 -9 -13 64.36 8.10 -10 -9 13 79.17 7.75 10 9 -13 73.78 8.69 -10 -9 13 83.75 8.11 -10 -9 12 22.46 4.16 10 -9 -12 14.17 4.10 -10 -9 12 27.05 4.54 10 9 -12 21.60 4.84 -10 -9 11 90.16 7.91 10 -9 -11 63.84 7.82 -10 -9 11 86.04 7.72 10 9 -11 75.22 8.51 -10 -9 10 10.48 2.73 10 -9 -10 3.12 2.49 -10 -9 10 7.86 2.37 10 9 -10 14.09 3.79 10 -9 -9 3.33 2.22 -10 -9 9 3.47 1.94 10 9 -9 3.05 2.49 -10 -9 9 4.79 1.80 10 -9 -8 15.48 3.74 -10 -9 8 16.78 3.51 10 9 -8 17.87 3.96 10 -9 -7 92.44 8.50 -10 -9 7 81.92 7.14 10 9 -7 93.86 8.57 10 -9 -6 6.82 2.77 -10 -9 6 10.69 2.76 10 9 -6 1.74 1.51 10 -9 -5 47.40 6.14 -10 -9 5 43.30 5.21 10 9 -5 37.21 5.29 10 -9 -4 75.65 7.56 -10 -9 4 84.29 7.13 10 9 -4 79.49 7.55 10 9 -3 9.70 3.20 -10 -9 3 10.51 2.78 10 -9 -3 5.30 2.33 10 9 -3 4.04 1.99 10 9 -2 12.64 3.36 -10 -9 2 17.05 3.38 10 -9 -2 5.32 2.16 10 9 -2 15.79 3.69 10 9 -1 0.81 1.54 10 9 -1 2.63 2.13 -10 -9 1 5.66 2.00 10 -9 -1 -0.47 1.35 10 9 0 4.86 1.99 10 9 0 1.31 1.57 -10 -9 0 5.43 2.45 10 -9 0 4.52 2.43 10 9 1 41.14 5.64 -10 -9 -1 46.18 5.41 10 -9 1 43.98 5.62 10 9 1 41.25 5.27 10 9 2 4.41 2.31 10 9 2 8.83 3.02 -10 -9 -2 4.61 2.12 10 -9 2 4.25 2.28 10 9 3 10.99 2.87 10 9 3 16.52 3.52 -10 -9 -3 19.85 3.75 10 -9 3 13.51 3.25 10 9 4 19.88 3.96 10 9 4 26.34 4.65 -10 -9 -4 19.98 3.70 10 -9 4 21.07 3.82 10 9 5 41.98 5.46 10 9 5 35.41 5.35 -10 -9 -5 43.81 5.34 10 -9 5 31.55 4.93 10 -9 6 6.08 2.18 10 9 6 5.95 2.54 -10 9 -6 4.71 2.17 10 9 7 41.62 6.30 -10 9 -7 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190.84 12.92 -10 -10 1 171.15 10.78 10 -10 -1 153.07 10.70 10 10 -1 158.92 11.07 10 10 0 3.04 1.68 10 10 0 10.42 3.13 -10 -10 0 11.88 3.06 10 -10 0 3.75 1.87 10 10 1 21.08 4.44 -10 -10 -1 28.89 4.55 10 -10 1 23.12 4.15 10 10 1 27.64 4.41 10 10 2 0.77 1.68 10 10 2 1.85 1.96 -10 -10 -2 0.07 1.23 -10 10 -2 3.16 2.19 10 -10 2 3.67 1.92 10 10 3 20.94 4.01 10 10 3 30.89 5.23 -10 -10 -3 32.07 4.84 -10 10 -3 34.19 5.04 10 -10 3 30.43 4.71 10 10 4 65.76 6.98 10 10 4 53.02 6.68 -10 -10 -4 68.07 7.00 -10 10 -4 70.79 7.28 10 -10 4 64.16 6.88 10 10 5 7.73 2.76 10 -10 5 2.18 1.52 10 10 5 2.00 2.20 -10 -10 -5 6.38 2.61 -10 10 -5 1.80 1.55 10 -10 6 0.72 1.71 10 10 6 -0.21 1.65 -10 10 -6 -0.71 2.05 10 10 7 53.59 6.93 -10 10 -7 51.73 6.91 -10 10 -8 6.30 3.60 -10 -11 13 0.83 1.79 -10 -11 12 28.16 4.90 -10 -11 11 60.27 6.89 10 -11 -11 45.21 6.82 -10 -11 11 51.91 6.47 10 11 -11 43.97 6.82 10 -11 -10 1.25 1.89 -10 -11 10 2.03 1.58 -10 -11 10 4.73 2.45 10 11 -10 4.57 2.68 -10 -11 9 15.90 3.39 10 -11 -9 11.63 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6.29 11 -4 3 122.11 8.40 11 4 4 5.87 2.12 -11 4 -4 3.49 1.83 11 4 4 3.40 1.83 11 -4 4 2.62 1.93 11 -4 4 2.33 1.35 -11 4 -5 2.55 1.56 11 4 5 7.55 2.79 11 -4 5 3.68 1.92 11 -4 5 7.18 2.33 -11 4 -6 11.52 2.93 11 4 6 7.98 2.79 11 -4 6 7.43 2.84 11 -4 6 9.71 2.44 11 -4 7 -0.67 1.16 -11 4 -7 1.11 1.68 11 4 7 2.37 2.18 11 -4 7 -0.35 1.86 -11 4 -8 29.74 4.85 11 4 8 28.91 4.94 11 -4 8 24.63 4.98 11 -4 8 28.66 4.07 11 -4 9 0.42 1.22 -11 4 -9 1.26 2.04 11 4 9 4.23 3.07 11 -4 9 -0.78 2.40 11 -4 10 61.65 6.35 -11 4 -10 68.82 7.70 11 4 10 51.66 7.04 11 -4 10 70.72 8.85 11 -4 11 0.16 1.46 11 -5 -18 52.88 8.27 11 5 -18 40.02 6.70 11 -5 -17 7.53 3.64 11 5 -17 1.83 1.74 -11 -5 17 3.57 2.12 11 -5 -16 4.69 2.98 11 5 -16 2.45 1.89 -11 -5 16 8.75 3.18 11 -5 -15 9.57 3.44 11 5 -15 6.01 3.12 -11 -5 15 7.37 2.61 -11 -5 14 3.58 2.24 11 5 -14 3.68 2.58 -11 -5 13 146.72 9.79 11 5 -13 151.32 11.17 -11 -5 12 4.94 2.38 11 5 -12 3.67 1.99 -11 5 11 20.61 3.80 -11 -5 11 19.25 3.47 11 5 -11 17.93 3.86 -11 -5 10 15.83 3.07 11 5 -10 14.42 3.17 11 -5 -9 110.70 5.53 -11 -5 9 114.57 7.77 11 5 -9 131.32 9.44 11 -5 -8 104.26 5.48 -11 -5 8 96.72 7.07 11 -5 -7 18.35 4.17 -11 -5 7 20.68 3.29 11 5 -7 18.17 3.48 11 5 -6 5.43 1.90 11 -5 -6 7.11 2.59 11 -5 -6 9.04 1.44 -11 -5 6 8.14 2.16 11 5 -6 9.47 2.74 11 5 -5 88.22 7.36 11 -5 -5 63.32 7.16 11 5 -5 77.99 7.43 11 -5 -5 71.88 4.44 -11 -5 5 70.15 5.69 11 5 -5 75.33 6.87 11 5 -4 12.00 2.65 11 5 -4 12.20 3.36 11 -5 -4 10.53 3.14 11 -5 -4 11.93 2.16 -11 -5 4 8.98 2.20 11 5 -4 9.73 2.64 11 5 -3 164.89 9.08 11 -5 -3 153.07 10.47 11 5 -3 162.66 10.27 11 -5 -3 155.24 7.35 -11 -5 3 152.55 8.11 11 5 -3 157.49 9.88 11 5 -2 21.41 3.12 11 -5 -2 23.17 4.33 11 5 -2 16.23 3.24 11 -5 -2 19.04 2.77 -11 -5 2 18.22 2.90 11 5 -2 16.52 3.19 11 5 -1 29.77 3.47 11 5 -1 33.98 4.66 11 -5 -1 31.17 4.83 11 -5 -1 37.27 4.06 -11 -5 1 33.32 3.81 11 5 -1 33.15 4.38 11 5 0 198.06 11.38 11 -5 0 182.32 10.96 11 -5 0 196.54 9.67 -11 -5 0 194.10 8.72 11 5 0 167.32 9.78 11 5 1 24.54 3.89 11 5 1 18.64 2.89 11 5 1 25.13 4.13 11 -5 1 19.40 3.64 11 -5 1 26.20 3.84 -11 -5 -1 23.34 3.14 11 5 2 32.67 4.54 11 5 2 23.51 2.93 11 5 2 25.78 4.14 11 -5 2 28.90 4.15 -11 -5 -2 29.00 3.45 11 -5 2 30.52 4.38 11 5 3 58.16 6.09 11 5 3 57.11 6.23 11 -5 3 61.86 6.27 -11 -5 -3 56.70 4.59 11 -5 3 42.40 5.10 11 5 4 61.79 6.29 11 5 4 59.83 6.63 11 -5 4 71.42 6.95 11 -5 4 71.91 6.72 -11 5 -5 -0.17 1.01 11 5 5 0.89 1.20 11 -5 5 -0.27 1.15 11 -5 6 1.59 1.28 -11 5 -6 0.69 1.11 11 5 6 1.71 1.83 11 -5 6 1.31 1.99 -11 5 -7 32.77 4.72 11 5 7 28.18 4.93 11 -5 7 38.32 5.78 11 -5 7 32.00 4.54 11 -5 8 12.40 2.99 -11 5 -8 8.86 2.66 11 5 8 14.29 3.59 11 -5 8 11.31 3.71 11 -5 9 9.07 2.95 -11 5 -9 8.48 2.77 11 5 9 12.49 3.63 11 -5 9 12.37 3.97 -11 5 -10 3.56 2.58 11 -5 10 1.41 1.89 11 5 10 1.79 1.69 11 -5 10 1.92 2.22 11 -5 11 36.98 5.20 11 6 -17 8.80 3.35 -11 -6 17 6.09 2.69 11 6 -16 0.50 2.10 -11 -6 16 -0.89 1.42 -11 -6 15 62.92 7.10 11 6 -15 76.70 8.62 -11 -6 14 69.14 7.05 11 6 -14 77.28 8.48 -11 -6 13 57.28 6.25 11 6 -13 55.47 6.89 -11 -6 12 26.26 4.19 11 6 -12 34.95 5.65 -11 -6 11 9.51 2.51 11 6 -11 8.11 2.65 -11 -6 10 16.32 3.13 11 6 -10 21.71 4.12 11 -6 -9 16.71 4.21 -11 -6 9 16.20 3.13 11 6 -9 20.81 4.14 11 -6 -8 39.35 5.94 -11 -6 8 51.26 5.30 11 6 -8 37.29 5.18 11 -6 -7 102.91 9.39 -11 -6 7 103.24 7.34 11 6 -7 96.81 8.11 11 -6 -6 92.02 8.69 -11 -6 6 96.05 6.97 11 6 -6 92.19 7.79 11 -6 -5 0.70 1.62 -11 -6 5 2.41 1.40 11 6 -5 3.02 1.63 11 6 -4 4.76 2.24 11 6 -4 6.67 2.70 11 -6 -4 2.47 1.42 11 -6 -4 6.93 1.61 -11 -6 4 5.90 1.88 11 6 -4 3.20 1.98 11 6 -3 3.65 1.46 11 6 -3 6.06 2.38 11 -6 -3 2.20 1.32 11 -6 -3 3.30 1.34 -11 -6 3 3.21 1.54 11 6 -3 5.55 1.97 11 6 -2 274.73 11.07 11 6 -2 287.41 14.03 11 -6 -2 293.67 10.99 -11 -6 2 280.02 11.18 11 6 -2 283.41 13.22 11 6 -1 3.98 1.98 11 6 -1 3.71 1.59 11 6 -1 1.85 1.82 11 -6 -1 5.04 1.75 -11 -6 1 4.07 1.45 11 -6 -1 2.07 1.38 11 6 0 18.89 3.76 11 -6 0 26.20 4.31 -11 -6 0 24.86 3.38 11 -6 0 27.74 3.87 11 6 0 17.75 3.62 11 6 1 132.37 9.04 11 6 1 121.49 9.05 -11 -6 -1 129.48 7.58 11 -6 1 122.54 8.22 11 -6 1 110.09 8.36 11 6 2 107.99 8.25 11 6 2 112.62 8.76 -11 -6 -2 128.27 7.44 11 -6 2 124.94 8.68 11 -6 2 115.84 8.65 11 6 3 60.95 6.45 11 6 3 72.49 7.22 -11 -6 -3 67.34 5.35 11 -6 3 72.03 6.87 11 -6 3 67.11 6.59 11 6 4 66.68 6.77 11 6 4 62.12 6.72 -11 -6 -4 63.83 5.18 11 -6 4 68.42 7.13 11 -6 4 59.45 6.23 11 6 5 31.49 5.09 11 -6 5 34.54 5.23 11 -6 5 29.21 4.58 11 -6 6 0.40 1.30 11 6 6 0.65 1.23 11 6 7 30.94 5.22 11 -6 7 34.97 5.73 11 -6 7 26.92 4.15 11 -6 8 5.42 2.30 11 6 8 5.00 3.18 11 -6 8 6.57 2.70 11 6 9 77.62 8.62 11 -6 9 92.95 7.88 11 -6 10 2.60 1.50 -11 -7 16 25.66 4.91 11 7 -16 25.73 6.60 -11 -7 15 4.84 2.30 11 7 -15 6.55 3.17 -11 -7 14 25.43 4.35 11 7 -14 38.00 6.13 -11 -7 13 2.37 1.89 11 7 -13 -1.34 2.60 -11 -7 12 10.24 3.17 11 7 -12 6.63 2.24 11 -7 -11 61.56 7.85 -11 -7 11 81.67 7.39 11 7 -11 71.79 7.84 11 -7 -10 98.49 10.11 -11 -7 10 126.31 8.94 11 7 -10 120.17 9.83 11 -7 -9 3.23 2.21 -11 -7 9 7.14 2.24 11 7 -9 7.93 2.75 11 -7 -8 62.47 7.68 -11 -7 8 66.65 6.16 11 7 -8 57.62 6.55 11 -7 -7 9.54 2.92 -11 -7 7 12.88 2.79 11 7 -7 8.96 3.02 11 -7 -6 1.78 1.72 -11 -7 6 1.16 1.61 11 7 -6 0.43 1.33 11 -7 -5 549.54 20.65 -11 -7 5 576.42 17.35 11 7 -5 567.47 19.50 11 7 -4 4.32 2.13 11 -7 -4 4.45 1.92 -11 -7 4 3.52 1.60 11 7 -4 3.86 1.66 11 7 -3 53.19 5.48 11 7 -3 69.11 7.47 11 -7 -3 60.25 6.81 -11 -7 3 60.97 5.62 11 7 -3 58.24 6.41 11 7 -2 111.32 7.21 11 7 -2 123.23 9.70 11 -7 -2 111.41 9.14 -11 -7 2 102.95 7.17 11 -7 -2 118.24 6.86 11 7 -2 100.18 8.32 11 7 -1 18.75 3.82 11 -7 -1 18.70 3.80 -11 -7 1 21.57 3.46 11 -7 -1 22.51 3.26 11 7 -1 21.79 3.77 11 7 0 177.85 11.48 -11 -7 0 178.59 9.37 11 -7 0 163.45 10.58 11 -7 0 195.38 10.04 11 7 1 -0.25 1.38 11 7 1 1.41 1.69 -11 -7 -1 1.15 1.53 11 -7 1 0.68 1.38 11 -7 1 1.24 1.00 11 7 2 171.58 10.63 11 7 2 172.41 11.22 -11 -7 -2 187.05 9.54 11 -7 2 190.39 10.92 11 -7 2 173.84 10.90 11 7 3 4.07 1.74 11 7 3 10.82 3.00 -11 -7 -3 6.65 1.99 11 -7 3 7.69 2.32 11 -7 3 7.43 2.59 11 7 4 147.30 10.13 11 7 4 172.06 11.54 -11 -7 -4 182.73 9.48 11 -7 4 193.36 11.76 11 -7 4 170.62 10.71 11 -7 5 16.28 3.39 11 7 5 22.71 4.24 11 -7 6 17.47 3.47 11 7 6 21.71 4.19 11 -7 7 2.94 1.59 11 7 7 1.60 1.31 11 -7 8 8.52 2.36 11 7 8 6.64 2.86 11 -7 9 65.64 7.48 11 -8 -15 6.69 3.53 11 8 -15 12.23 4.10 11 -8 -14 26.26 5.75 -11 -8 14 20.08 4.17 11 8 -14 24.67 5.17 11 -8 -13 -1.22 2.30 -11 -8 13 2.57 2.22 11 8 -13 -2.41 2.12 11 -8 -12 16.60 4.57 -11 -8 12 10.87 3.36 11 8 -12 5.65 2.84 11 -8 -11 0.35 2.44 -11 -8 11 0.24 1.15 11 8 -11 0.80 1.91 11 -8 -10 40.05 6.46 -11 -8 10 34.55 4.91 11 8 -10 25.90 4.68 11 -8 -9 5.66 2.59 -11 -8 9 8.12 2.51 11 8 -9 8.96 3.05 11 -8 -8 342.38 17.30 -11 -8 8 331.69 14.36 11 8 -8 319.97 16.03 11 -8 -7 1.93 1.96 -11 -8 7 0.23 1.07 11 8 -7 2.09 1.73 11 -8 -6 16.92 4.04 -11 -8 6 11.54 2.68 11 8 -6 15.27 3.35 11 -8 -5 9.53 2.96 -11 -8 5 10.00 2.39 11 8 -5 7.97 2.77 11 -8 -4 376.99 17.23 -11 -8 4 342.58 13.78 11 8 -4 336.85 15.62 11 8 -3 34.48 4.54 11 8 -3 44.39 6.24 11 -8 -3 28.54 4.86 -11 -8 3 28.56 4.05 11 8 -3 36.75 5.24 11 8 -2 32.81 5.19 11 -8 -2 31.44 4.96 -11 -8 2 35.09 4.52 11 8 -2 37.37 5.20 11 8 -1 1.36 1.88 11 8 -1 0.21 1.54 -11 -8 1 -0.46 1.51 11 -8 -1 1.80 1.91 11 8 0 69.31 7.42 -11 -8 0 59.88 5.88 11 -8 0 61.74 6.67 11 8 0 54.02 6.01 11 8 1 -0.84 1.35 11 8 1 -1.38 1.34 -11 -8 -1 0.77 1.60 11 -8 1 1.74 1.74 11 8 2 110.52 8.84 11 8 2 130.29 10.00 -11 -8 -2 125.47 8.41 11 -8 2 118.10 9.18 11 8 3 165.04 10.89 11 8 3 177.60 11.84 -11 -8 -3 163.46 9.53 11 -8 3 158.59 10.67 11 8 4 104.07 8.57 11 8 4 89.87 8.66 -11 -8 -4 109.41 7.91 11 -8 4 97.74 8.25 11 8 5 54.50 6.40 11 8 5 67.28 7.49 11 -8 5 48.16 5.81 11 -8 6 4.77 1.97 11 8 6 11.27 3.38 11 8 7 123.49 10.50 11 -8 7 124.58 9.44 11 8 8 -0.16 1.80 11 -9 -15 1.87 2.63 11 -9 -14 1.15 2.09 -11 -9 14 0.40 1.78 11 9 -14 -0.75 1.84 -11 -9 14 2.40 1.95 11 -9 -13 4.57 3.22 -11 -9 13 4.98 2.81 -11 -9 13 3.73 2.40 11 9 -13 1.40 2.01 11 -9 -12 3.23 2.76 -11 -9 12 0.23 1.25 11 9 -12 -0.48 2.13 11 -9 -11 0.46 1.78 -11 -9 11 -0.05 1.64 11 9 -11 0.79 1.66 11 -9 -10 1.80 2.08 -11 -9 10 3.95 2.19 11 9 -10 1.32 1.75 11 -9 -9 112.01 10.10 -11 -9 9 99.67 8.32 11 9 -9 104.39 9.74 11 -9 -8 -1.11 1.91 -11 -9 8 2.91 1.89 11 9 -8 -0.05 1.48 11 -9 -7 166.65 12.06 -11 -9 7 159.40 10.17 11 9 -7 159.76 11.39 11 -9 -6 9.94 3.42 -11 -9 6 13.27 3.12 11 9 -6 10.21 3.13 11 -9 -5 120.47 9.99 -11 -9 5 126.40 8.82 11 9 -5 118.89 9.43 11 -9 -4 144.14 10.93 -11 -9 4 166.38 10.13 11 9 -4 178.09 11.88 11 9 -3 92.63 9.49 11 -9 -3 101.32 9.01 -11 -9 3 82.92 7.24 11 9 -3 82.44 7.93 11 9 -2 1.36 1.33 11 9 -2 2.47 1.58 -11 -9 2 1.28 1.78 11 -9 -2 3.84 1.78 11 9 -1 39.63 5.87 -11 -9 1 36.48 4.83 11 -9 -1 35.79 5.23 11 9 -1 32.37 5.00 11 9 0 40.05 6.03 -11 -9 0 40.21 5.15 11 -9 0 47.48 5.96 11 9 0 39.84 5.41 11 9 1 17.77 3.71 11 9 1 22.14 4.53 -11 -9 -1 23.77 3.93 11 -9 1 22.30 4.45 11 9 2 -0.64 1.76 11 9 2 3.73 2.49 -11 -9 -2 3.80 1.68 11 -9 2 2.64 1.68 11 9 3 9.13 2.79 11 9 3 15.67 4.62 -11 -9 -3 14.44 3.31 11 -9 3 13.25 3.27 11 -9 4 4.87 2.11 11 9 4 2.19 1.64 -11 -9 -4 4.05 1.72 11 -9 5 5.11 2.24 11 9 5 6.98 2.54 11 9 5 7.66 2.91 11 9 6 54.58 7.09 11 -9 6 53.50 6.31 -11 9 -7 4.22 2.71 11 -10 -13 4.47 2.83 -11 -10 13 5.02 2.67 11 -10 -12 15.84 4.40 -11 -10 12 20.56 4.30 -11 -10 12 19.50 4.45 11 10 -12 17.66 4.46 11 -10 -11 17.21 4.37 -11 -10 11 20.34 4.60 11 10 -11 15.33 4.66 11 -10 -10 3.27 2.07 -11 -10 10 6.42 2.68 11 10 -10 7.05 3.47 11 -10 -9 1.97 2.31 -11 -10 9 1.84 2.12 11 10 -9 2.24 2.93 -11 -10 8 28.95 4.71 11 -10 -8 23.04 4.55 11 10 -8 39.53 6.30 11 -10 -7 4.54 3.00 -11 -10 7 1.05 1.58 11 10 -7 -0.04 1.37 11 -10 -6 61.07 7.32 -11 -10 6 41.04 5.33 11 10 -6 54.37 7.27 11 -10 -5 45.75 6.31 -11 -10 5 28.40 4.69 11 10 -5 38.95 5.78 11 10 -4 1.41 2.54 -11 -10 4 0.36 1.21 11 -10 -4 0.11 1.20 11 10 -4 -0.18 1.52 11 10 -3 13.37 3.89 -11 -10 3 16.31 3.41 11 -10 -3 14.42 3.58 11 10 -3 14.58 3.79 11 10 -2 13.65 3.56 11 10 -2 23.24 5.47 -11 -10 2 26.63 4.43 11 -10 -2 23.03 4.35 11 10 -1 1.13 1.59 11 10 -1 -0.22 1.44 -11 -10 1 2.10 1.55 11 -10 -1 -2.38 1.94 11 10 0 -0.31 1.61 11 10 0 -1.63 1.85 -11 -10 0 0.13 1.18 11 -10 0 2.03 1.61 11 10 1 50.82 6.98 -11 -10 -1 56.00 6.26 11 -10 1 45.29 6.21 11 10 1 41.72 5.58 11 10 2 73.55 7.55 11 10 2 84.49 8.95 -11 -10 -2 93.67 8.22 11 -10 2 95.44 8.77 11 -10 3 4.97 2.50 11 10 3 4.91 1.91 11 10 3 7.55 3.09 -11 -10 -3 7.82 3.06 -11 10 -3 7.97 2.92 11 -10 4 11.82 3.46 11 10 4 8.03 2.87 11 10 4 12.71 3.95 -11 -10 -4 7.94 3.01 -11 10 -4 3.36 2.03 11 10 5 93.67 8.61 11 10 5 94.67 9.38 -11 10 -5 111.67 9.69 -11 10 -6 15.51 4.16 11 -11 -12 51.65 7.75 -11 -11 12 93.75 9.11 11 -11 -11 8.77 3.38 -11 -11 10 1.58 1.70 11 11 -10 -2.43 2.96 11 -11 -9 12.37 3.82 -11 -11 9 13.97 3.67 11 11 -9 15.14 3.96 11 -11 -8 48.28 6.93 -11 -11 8 60.66 7.01 11 11 -8 57.78 7.68 -11 -11 7 -2.41 1.70 11 -11 -7 0.99 1.97 11 11 -7 -2.43 2.47 -11 -11 6 2.88 2.40 11 -11 -6 8.54 3.11 11 11 -6 10.75 3.42 -11 -11 5 5.81 2.24 11 -11 -5 3.14 1.79 11 11 -4 18.43 4.62 -11 -11 4 22.38 4.26 11 -11 -4 16.57 3.75 11 11 -4 15.14 3.78 11 11 -3 22.76 5.14 -11 -11 3 12.41 3.31 11 -11 -3 12.34 3.42 11 11 -3 10.70 3.39 11 11 -2 0.67 1.87 11 11 -2 3.60 2.44 -11 -11 2 -0.24 1.52 11 -11 -2 0.57 1.34 11 11 -1 6.20 2.32 11 11 -1 6.62 2.65 -11 -11 1 6.28 2.38 11 -11 -1 11.54 3.17 11 11 0 -1.00 1.69 11 11 0 -1.34 1.87 -11 -11 0 2.78 2.36 11 -11 0 1.59 1.32 11 11 1 4.68 2.16 11 11 1 4.41 2.69 -11 -11 -1 2.14 1.68 11 -11 1 6.22 2.81 11 -11 2 18.69 4.18 11 11 2 11.60 3.02 11 11 2 18.05 4.29 -11 -11 -2 22.47 4.52 11 11 3 15.32 3.97 11 11 3 17.01 4.36 -11 -11 -3 16.88 3.90 11 11 4 2.48 2.41 -11 -11 -4 2.48 2.05 11 11 5 1.56 2.16 11 -12 -10 1.80 2.26 11 -12 -9 6.70 3.01 11 -12 -8 1.10 1.54 11 12 -8 7.37 3.68 11 -12 -7 -1.51 1.63 11 12 -7 1.79 2.17 -11 -12 6 -0.75 1.48 11 -12 -6 2.28 2.29 11 12 -6 0.45 2.50 11 12 -5 0.98 2.73 -11 -12 5 -0.45 2.18 11 -12 -5 0.42 1.85 11 12 -5 0.41 1.92 11 12 -4 65.83 8.90 -11 -12 4 76.08 8.03 11 -12 -4 59.76 7.40 11 12 -4 55.08 7.40 11 12 -3 1.76 2.59 -11 -12 3 0.37 1.54 11 -12 -3 2.84 2.44 11 12 -3 2.97 2.77 11 12 -2 92.82 10.28 -11 -12 2 86.56 8.66 11 -12 -2 92.58 8.96 11 12 -2 81.28 8.56 11 12 -1 21.41 4.62 11 12 -1 10.18 3.90 -11 -12 1 7.82 3.08 11 -12 -1 13.48 3.37 11 12 0 22.59 4.51 11 12 0 22.80 5.10 -11 -12 0 16.84 4.23 11 12 1 10.52 3.16 -11 -12 -1 7.97 3.16 11 12 2 -0.28 1.80 -11 -12 -2 0.99 1.72 11 12 3 17.10 4.36 -11 -12 -3 13.88 3.92 11 -13 -8 0.64 2.22 11 -13 -7 11.33 3.52 11 -13 -6 10.62 3.64 11 -13 -5 -1.02 2.28 11 13 -3 83.49 9.96 11 13 -2 14.74 3.97 11 13 -1 20.52 4.63 -12 0 18 22.62 4.91 12 0 -18 25.60 5.97 -12 0 17 0.51 1.63 12 0 -17 2.33 2.28 12 0 -17 -1.85 1.46 -12 0 16 4.89 2.48 12 0 -16 1.72 2.11 12 0 -16 1.85 1.96 -12 0 15 2.80 2.01 12 0 -15 -0.83 1.66 12 0 -15 -0.22 1.50 12 0 -14 336.76 18.73 12 0 -14 334.33 14.61 -12 0 13 0.11 1.13 12 0 -13 -2.00 2.30 12 0 -13 -1.15 1.13 12 0 -12 39.96 6.15 -12 0 12 27.49 4.31 12 0 -12 30.08 4.31 12 0 -11 -2.22 2.14 12 0 -11 -0.50 1.26 -12 0 11 2.78 1.42 12 0 -10 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4.38 12 5 -4 36.34 5.01 12 5 -3 9.78 2.68 12 5 -3 6.98 2.18 12 5 -3 12.11 3.21 12 -5 -3 7.56 2.53 12 -5 -3 6.86 1.93 -12 -5 3 3.95 1.43 12 5 -2 26.59 3.88 12 5 -2 28.12 4.46 12 -5 -2 22.17 4.14 12 -5 -2 25.68 3.38 -12 -5 2 23.13 3.31 12 5 -2 18.73 3.60 12 5 -1 65.43 6.74 12 -5 -1 46.84 5.91 12 -5 -1 53.04 5.03 -12 -5 1 64.56 5.30 12 5 -1 51.97 5.75 12 5 0 38.56 5.03 12 5 0 24.44 3.81 12 5 0 30.23 4.60 12 -5 0 37.46 5.22 12 -5 0 38.08 4.58 -12 -5 0 36.50 4.02 12 5 1 1.97 1.83 12 5 1 3.91 2.10 12 -5 1 1.83 1.23 -12 -5 -1 1.97 1.20 12 -5 1 2.17 1.48 12 5 2 10.68 2.94 12 5 2 11.62 2.91 12 -5 2 18.22 3.76 12 -5 2 9.68 2.79 -12 -5 -2 11.68 2.21 12 5 3 61.49 6.52 12 5 3 56.16 6.40 12 -5 3 77.78 7.48 12 -5 3 58.84 6.14 12 5 4 61.40 6.61 12 5 4 63.39 7.01 12 -5 4 79.17 8.26 12 -5 4 54.48 6.07 12 5 5 73.71 7.71 12 -5 5 81.92 8.16 12 -5 6 6.48 2.40 -12 5 -6 1.23 1.18 12 5 6 4.59 2.23 12 -5 6 4.34 2.42 12 -5 7 -2.06 1.48 -12 5 -7 -0.32 1.44 12 5 7 0.66 1.38 12 -5 7 -0.24 1.98 12 -5 8 -0.41 1.62 -12 5 -8 1.69 1.56 12 5 8 1.93 2.22 12 -5 8 2.40 2.32 -12 5 -9 30.42 5.37 12 -5 9 35.26 6.46 12 -5 9 22.34 4.47 12 -5 10 39.06 5.45 12 6 -17 13.83 4.30 -12 -6 16 81.24 8.39 12 6 -16 77.62 9.92 -12 -6 15 129.52 10.24 12 6 -15 128.71 11.20 -12 -6 14 4.32 2.10 12 6 -14 2.30 2.30 -12 -6 13 227.94 12.71 12 6 -13 192.28 13.16 -12 -6 12 2.16 1.70 12 6 -12 8.37 2.83 -12 -6 11 44.86 5.45 12 6 -11 45.72 6.09 -12 -6 10 -0.59 1.21 12 6 -10 2.02 2.08 12 -6 -9 88.75 9.45 -12 -6 9 91.51 7.45 12 6 -9 97.97 8.82 12 -6 -8 9.68 3.35 -12 -6 8 6.11 2.20 12 6 -8 2.94 1.89 12 -6 -7 6.32 2.38 -12 -6 7 11.54 2.93 12 6 -7 8.52 2.64 12 6 -6 399.52 17.01 12 -6 -6 330.53 17.20 12 6 -6 415.73 18.38 -12 -6 6 336.26 13.51 12 6 -6 377.54 16.37 12 6 -5 12.16 3.11 12 6 -5 13.75 3.62 12 -6 -5 8.91 2.89 -12 -6 5 13.23 2.88 12 6 -5 10.49 2.66 12 6 -4 21.01 3.74 12 6 -4 17.80 3.81 12 -6 -4 16.51 3.68 -12 -6 4 20.41 3.41 12 6 -4 21.35 4.11 12 6 -3 52.71 5.33 12 6 -3 60.94 6.77 12 -6 -3 44.00 5.99 12 -6 -3 52.98 4.70 -12 -6 3 45.14 4.73 12 6 -3 42.46 5.73 12 6 -2 2.85 1.92 12 6 -2 0.20 1.13 12 6 -2 2.52 2.11 12 -6 -2 2.48 1.32 12 -6 -2 0.37 1.31 -12 -6 2 0.19 1.02 12 6 -1 4.64 2.18 12 6 -1 6.28 2.33 12 -6 -1 10.66 2.37 12 -6 -1 3.60 1.72 -12 -6 1 10.51 2.40 12 6 0 3.78 1.79 12 6 0 5.51 2.24 12 -6 0 2.15 1.54 -12 -6 0 2.64 1.45 12 -6 0 0.67 1.02 12 6 1 4.55 1.93 12 6 1 9.32 2.93 12 -6 1 5.63 2.13 -12 -6 -1 5.85 2.09 12 -6 1 2.99 1.96 12 6 2 11.79 3.22 12 -6 2 12.04 2.93 -12 -6 -2 11.39 2.37 12 -6 2 9.22 2.69 12 6 3 63.35 6.68 12 6 3 68.23 7.43 12 -6 3 84.55 7.59 12 -6 3 69.15 6.92 12 6 4 39.50 5.47 12 6 4 44.45 6.07 12 -6 4 51.26 6.33 12 -6 4 47.10 5.60 12 6 5 6.37 2.47 12 -6 5 10.03 2.99 12 -6 5 8.63 2.57 12 -6 6 1.54 1.65 12 6 6 3.45 2.48 12 -6 6 2.55 2.34 12 -6 7 -0.09 1.26 12 6 7 -0.08 1.86 12 -6 7 1.24 1.99 12 -6 8 1.38 1.51 12 -6 8 0.27 1.74 -12 -7 15 -0.82 1.86 12 7 -15 0.64 2.28 -12 -7 14 143.53 10.51 12 7 -14 154.89 12.42 -12 -7 13 31.90 5.04 12 7 -13 38.48 6.11 12 -7 -12 159.48 13.14 -12 -7 12 150.54 10.39 12 7 -12 152.29 11.71 12 -7 -11 5.79 3.30 -12 -7 11 6.59 2.66 12 7 -11 7.72 2.89 12 -7 -10 59.77 8.14 -12 -7 10 50.61 5.80 12 7 -10 55.53 7.44 12 -7 -9 48.90 6.99 -12 -7 9 35.55 4.94 12 7 -9 35.52 5.55 12 -7 -8 5.45 2.64 -12 -7 8 5.95 2.10 12 7 -8 7.44 3.03 12 -7 -7 39.23 6.13 -12 -7 7 38.94 4.87 12 7 -7 43.41 5.69 12 -7 -6 33.07 5.41 -12 -7 6 25.63 3.95 12 7 -6 28.28 5.02 12 7 -5 40.41 5.33 12 7 -5 52.48 6.86 12 -7 -5 48.93 6.45 -12 -7 5 40.58 4.85 12 7 -5 45.06 5.93 12 7 -4 45.84 5.41 12 7 -4 46.81 6.46 12 -7 -4 50.70 6.66 -12 -7 4 38.19 4.68 12 7 -4 46.79 5.95 12 7 -3 4.35 1.96 12 7 -3 1.17 1.28 12 7 -3 4.17 2.20 12 -7 -3 1.78 1.26 12 7 -2 54.80 6.71 12 -7 -2 50.21 6.29 -12 -7 2 55.13 5.45 12 7 -2 53.38 6.29 12 7 -1 4.02 1.87 12 7 -1 4.01 2.44 12 -7 -1 7.44 2.21 -12 -7 1 4.40 1.58 12 -7 -1 6.03 2.47 12 7 0 60.56 7.11 -12 -7 0 61.37 5.58 12 -7 0 44.27 5.72 12 -7 0 67.12 6.27 12 7 0 64.50 6.67 12 7 1 3.07 1.76 12 7 1 2.03 1.66 12 -7 1 2.51 1.09 -12 -7 -1 1.36 1.09 12 -7 1 2.48 1.89 12 7 2 12.57 3.15 12 7 2 13.08 3.44 12 -7 2 13.29 3.25 -12 -7 -2 10.53 2.66 12 -7 2 12.29 3.18 12 7 3 27.18 4.63 12 7 3 24.01 4.50 12 -7 3 25.12 4.46 12 -7 3 23.74 4.44 12 7 4 2.30 1.95 12 7 4 -2.50 2.20 12 -7 4 2.47 1.96 12 -7 4 1.96 1.35 12 -7 5 2.11 1.94 12 7 5 1.87 2.27 12 -7 5 1.41 1.65 12 7 6 18.47 3.97 12 -7 6 23.10 4.58 12 7 7 107.90 10.22 12 -7 7 92.21 8.20 12 -8 -16 3.24 4.07 12 -8 -15 0.12 2.21 12 -8 -14 9.18 4.07 -12 -8 14 2.79 2.00 12 8 -14 3.16 2.31 12 -8 -13 5.72 3.30 -12 -8 13 2.93 1.66 12 8 -13 6.50 2.40 12 -8 -12 -0.16 2.38 -12 -8 12 0.58 1.34 12 8 -12 1.51 2.11 12 -8 -11 1.14 2.07 -12 -8 11 1.86 1.57 12 8 -11 0.58 1.78 12 -8 -10 65.87 8.38 -12 -8 10 65.26 6.80 12 8 -10 51.71 7.54 12 -8 -9 3.40 2.80 -12 -8 9 0.86 1.69 12 8 -9 1.73 2.18 12 -8 -8 24.90 5.01 -12 -8 8 19.85 3.65 12 8 -8 26.83 5.05 12 -8 -7 62.63 7.65 -12 -8 7 78.55 7.10 12 8 -7 87.18 9.05 12 -8 -6 39.77 6.17 -12 -8 6 35.21 4.72 12 8 -6 33.86 5.35 12 8 -5 0.26 1.92 12 8 -5 0.33 1.85 12 -8 -5 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15.24 3.42 12 9 -10 30.51 5.48 12 -9 -9 169.09 12.91 -12 -9 9 183.32 11.61 12 9 -9 180.32 12.85 12 -9 -8 63.32 7.77 -12 -9 8 69.76 7.12 12 -9 -7 6.03 2.57 -12 -9 7 2.04 1.96 12 9 -7 0.99 1.77 12 -9 -6 94.80 9.60 -12 -9 6 101.96 8.30 12 9 -6 98.55 10.10 12 9 -5 6.20 3.01 12 -9 -5 2.51 1.89 -12 -9 5 0.41 1.13 12 9 -5 6.15 3.21 12 9 -4 59.12 7.84 12 -9 -4 56.77 7.08 -12 -9 4 56.90 6.21 12 9 -4 52.17 6.84 12 9 -3 49.03 6.94 12 -9 -3 36.52 5.60 -12 -9 3 42.45 5.29 12 9 -3 30.53 5.28 12 9 -2 11.27 3.60 12 9 -2 14.61 3.83 -12 -9 2 11.74 3.01 12 -9 -2 16.48 3.77 12 9 -1 51.03 6.98 -12 -9 1 68.69 6.72 12 -9 -1 63.08 7.06 12 9 -1 46.78 6.19 12 9 0 1.20 1.36 12 9 0 -1.27 2.09 -12 -9 0 -1.07 1.44 12 -9 0 2.84 2.35 12 9 1 126.31 10.05 12 9 1 122.82 10.53 -12 -9 -1 147.67 9.79 12 -9 1 128.06 10.33 12 9 2 26.70 4.78 12 9 2 32.05 5.38 -12 -9 -2 31.89 4.66 12 -9 2 16.14 3.74 12 9 3 42.78 5.95 12 9 3 42.17 6.34 12 -9 3 34.51 5.44 12 -9 4 2.10 1.92 12 9 4 0.77 1.62 12 9 4 3.23 2.66 12 9 5 0.72 1.85 12 9 5 -1.70 2.51 12 -10 -13 9.19 3.51 12 -10 -12 19.55 5.05 12 -10 -11 33.58 6.14 -12 -10 11 28.56 4.96 12 10 -11 32.99 5.99 12 -10 -10 3.66 2.37 -12 -10 10 9.04 3.10 12 10 -10 3.53 2.96 12 -10 -9 65.68 8.32 -12 -10 9 73.60 7.66 12 10 -9 77.81 8.86 12 -10 -8 -0.98 2.04 -12 -10 8 -1.69 1.81 12 10 -8 -0.54 1.55 -12 -10 7 23.87 4.36 12 -10 -7 15.65 3.94 12 10 -7 17.41 4.29 -12 -10 6 -2.50 2.19 12 -10 -6 0.25 2.02 12 10 -6 0.21 1.62 12 10 -5 162.53 13.25 12 -10 -5 119.09 10.46 -12 -10 5 152.04 10.42 12 10 -5 131.18 10.87 12 10 -4 4.19 3.09 -12 -10 4 0.85 1.62 12 -10 -4 1.95 1.64 12 10 -4 0.41 1.50 12 10 -3 7.32 3.02 12 10 -3 12.56 3.93 -12 -10 3 8.44 2.73 12 -10 -3 6.98 3.02 12 10 -2 13.41 3.46 12 10 -2 8.45 3.50 -12 -10 2 9.47 2.80 12 -10 -2 12.25 3.47 12 10 -1 1.22 1.61 12 10 -1 -1.87 2.02 -12 -10 1 1.66 1.58 12 -10 -1 -0.38 1.97 12 10 0 10.21 3.25 12 10 0 14.26 4.05 -12 -10 0 12.31 3.37 12 -10 0 15.25 3.73 12 10 1 15.74 3.86 -12 -10 -1 17.24 3.71 12 -10 1 14.12 3.79 12 10 2 23.90 4.69 12 10 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10.34 3.87 12 -12 -6 -1.67 2.24 12 -12 -5 51.08 7.05 12 12 -5 57.57 7.81 12 -12 -4 82.27 8.84 12 12 -4 92.74 9.75 12 12 -3 0.32 2.21 12 12 -2 17.36 4.67 -12 -12 2 14.15 3.73 12 12 -1 20.97 4.65 -12 -12 1 21.82 4.57 12 12 0 -1.48 2.63 -12 -12 0 0.40 1.65 -13 0 17 -0.93 1.68 13 0 -17 5.07 3.41 13 0 -16 89.95 10.39 -13 0 16 108.32 9.82 -13 0 15 1.20 1.76 13 0 -15 1.87 2.11 13 0 -15 2.03 1.78 13 0 -14 143.77 12.56 13 0 -14 109.47 8.51 -13 0 14 145.87 10.74 -13 0 13 1.06 1.50 13 0 -13 0.16 1.47 13 0 -13 1.36 1.50 13 0 -12 1145.18 33.70 -13 0 12 1166.06 27.47 13 0 -12 1126.44 26.62 13 0 -11 3.64 2.30 13 0 -11 -0.33 1.24 13 0 -11 -0.56 1.52 -13 0 11 -0.98 1.50 13 0 -10 190.14 13.04 13 0 -10 183.90 10.02 -13 0 10 200.71 10.80 13 0 -10 169.67 9.97 13 0 -9 2.40 2.07 13 0 -9 -0.76 0.91 -13 0 9 1.56 1.69 13 0 -9 -0.40 1.05 13 0 -8 160.97 11.64 13 0 -8 159.74 8.97 -13 0 8 174.20 9.57 13 0 -8 156.67 9.45 13 0 -7 0.35 1.01 13 0 -7 -2.19 1.66 13 0 -7 -0.69 1.27 -13 0 7 1.98 1.48 13 0 -6 85.03 8.18 13 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17.73 4.45 14 -5 5 15.88 3.69 14 -5 6 18.53 4.63 14 -5 6 24.38 4.38 14 6 -15 100.61 10.51 -14 -6 14 3.50 2.10 14 6 -14 2.21 2.23 14 6 -13 1.42 2.46 -14 -6 13 9.60 3.56 14 6 -13 5.86 2.84 14 6 -12 3.12 2.61 -14 -6 12 0.33 1.87 14 6 -12 3.55 2.52 14 6 -11 -1.32 2.96 14 -6 -11 2.41 2.69 -14 -6 11 2.49 1.41 14 6 -11 1.76 2.04 14 6 -10 0.77 1.69 14 -6 -10 6.36 3.39 -14 -6 10 5.99 2.34 14 6 -10 5.61 2.80 14 6 -9 5.80 2.59 14 -6 -9 7.25 3.53 -14 -6 9 6.11 2.21 14 6 -9 4.21 2.47 14 6 -8 32.83 5.85 14 -6 -8 41.66 6.98 14 6 -8 21.74 4.83 -14 -6 8 24.14 4.06 14 6 -8 25.47 4.90 14 6 -7 -0.54 1.54 14 6 -7 0.46 2.39 14 -6 -7 1.05 2.24 -14 -6 7 1.51 1.43 14 6 -7 2.85 2.21 14 6 -6 20.86 4.25 14 6 -6 17.77 4.73 14 -6 -6 14.73 3.98 -14 -6 6 19.92 3.69 14 6 -6 14.71 3.59 14 6 -5 18.39 3.81 14 6 -5 22.42 4.62 14 -6 -5 17.64 4.35 -14 -6 5 26.81 4.10 14 6 -5 23.61 4.79 14 6 -4 19.68 4.39 14 -6 -4 17.28 4.16 -14 -6 4 22.81 3.83 14 6 -4 20.91 4.56 14 6 -3 28.04 5.17 14 -6 -3 38.75 6.16 -14 -6 3 41.58 5.06 14 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17 6 -11 6.58 3.82 17 6 -10 4.33 3.11 17 6 -9 37.20 6.72 -17 -6 9 37.22 5.81 17 6 -8 8.00 3.94 -17 -6 8 7.08 3.11 17 6 -7 6.73 3.06 -17 -6 7 10.12 3.56 17 6 -6 3.01 2.57 -17 -6 6 0.43 1.58 -17 -6 5 0.94 1.65 -17 -7 8 33.51 5.47 -17 -7 7 46.20 6.27 -17 -7 6 2.03 2.31 -17 -7 5 15.58 3.68 18 0 -12 15.60 4.05 -18 0 12 11.92 3.82 18 0 -11 1.32 2.33 -18 0 11 -0.32 1.76 18 0 -10 142.82 10.97 -18 0 10 188.47 12.90 -18 0 9 3.31 2.15 18 0 -9 -1.22 2.03 -18 0 8 2.65 2.53 18 0 -8 1.35 1.84 18 0 -7 -1.76 1.99 18 0 -7 -1.56 3.17 18 0 -6 133.28 10.89 18 0 -6 141.66 13.63 18 0 -6 114.34 9.77 18 0 -5 4.26 2.98 18 0 -5 0.65 2.47 18 0 -5 2.12 2.33 18 0 -4 146.67 11.41 18 0 -4 136.27 12.52 18 0 -4 131.16 10.65 18 0 -3 0.34 2.03 18 0 -3 4.43 3.25 18 0 -2 10.10 3.31 18 0 -2 13.53 4.18 18 0 -1 -0.15 1.98 18 0 -1 -2.37 2.68 18 1 -13 19.98 4.93 -18 -1 12 0.59 1.78 18 1 -12 1.11 2.00 -18 1 12 3.42 2.98 18 -1 -11 22.66 4.63 -18 -1 11 39.22 5.96 -18 1 11 45.14 6.46 18 1 -11 31.95 5.68 -18 -1 10 3.10 2.04 18 1 -10 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2 10 13.37 3.51 18 2 -10 10.08 3.53 -18 2 9 78.13 7.83 18 -2 -9 49.88 6.20 18 2 -9 53.76 6.86 -18 -2 9 79.89 8.09 18 2 -9 69.06 8.15 18 2 -8 7.47 3.07 18 -2 -8 7.37 3.95 18 2 -8 5.84 2.87 -18 -2 8 14.56 3.47 18 2 -7 21.77 4.80 18 -2 -7 17.39 4.17 18 -2 -7 25.28 6.04 18 2 -7 24.06 4.89 18 2 -6 17.76 4.46 18 2 -6 3.48 2.99 18 2 -6 14.73 3.84 18 -2 -6 18.44 5.46 18 2 -5 151.36 12.15 18 2 -5 137.04 13.07 18 -2 -5 137.11 13.18 18 2 -5 148.69 11.65 18 2 -4 9.95 3.37 18 2 -4 5.11 3.59 18 2 -4 4.27 3.09 18 -2 -4 9.25 3.80 18 2 -3 35.89 5.97 18 2 -3 19.06 4.94 18 -2 -3 22.99 5.35 18 2 -2 3.21 1.77 18 -2 -2 5.36 2.96 18 -2 -2 3.89 2.64 18 -2 -1 3.76 2.89 18 -2 -1 -0.50 2.30 18 -2 0 0.47 2.20 18 -2 0 1.56 3.23 -18 3 11 0.84 1.81 18 3 -11 1.79 3.02 18 3 -11 6.33 3.10 -18 -3 11 3.35 3.12 18 3 -10 12.09 4.00 18 3 -10 11.96 4.38 18 3 -10 18.08 4.48 -18 -3 10 14.35 3.89 18 3 -9 7.63 3.45 18 3 -9 7.38 2.91 -18 -3 9 1.15 1.59 18 3 -8 7.12 2.87 18 3 -8 5.41 2.53 -18 -3 8 4.81 2.46 18 3 -7 6.25 3.17 18 3 -7 1.27 1.85 18 3 -6 0.07 1.96 18 3 -6 2.00 2.30 18 -3 -6 -0.83 2.65 18 3 -5 9.39 4.45 18 3 -5 15.37 4.15 18 -3 -5 11.29 4.05 18 3 -4 86.94 10.10 18 -3 -4 96.87 11.17 18 3 -4 90.90 9.54 18 3 -3 11.05 3.91 18 4 -11 4.18 4.94 18 4 -11 -0.39 2.00 18 4 -10 6.76 4.18 18 4 -10 7.73 3.52 -18 -4 10 5.19 2.77 18 4 -9 2.05 2.78 18 4 -9 0.15 2.05 18 4 -8 20.27 4.74 -18 -4 8 15.71 3.90 18 4 -7 3.17 2.72 -18 -4 7 3.84 2.15 18 4 -6 51.43 7.39 18 4 -5 30.18 5.90 -18 -5 9 6.64 2.99 -18 -5 8 8.61 3.35 -18 -5 7 33.37 5.50 19 0 -10 7.34 3.39 19 0 -9 1.22 2.20 19 0 -8 18.70 4.53 19 0 -7 -1.38 2.51 19 -1 -9 31.37 7.47 19 -1 -8 -0.49 2.09 19 -1 -7 0.22 1.99 19 -1 -6 2.76 2.59 19 1 -6 3.76 3.56 19 1 -6 -0.34 2.08 19 1 -5 29.94 6.45 19 1 -4 4.53 2.82 19 1 -4 1.25 2.53 19 -2 -7 49.82 6.78 19 2 -7 64.50 8.13 19 2 -6 12.44 4.85 19 2 -6 25.92 7.91 19 2 -5 122.93 12.61 19 3 -7 23.08 6.12 TITL MSB-RK-23-1_Mo in P2(1)/c REM P2(1)/c (#14 in standard setting) CELL 0.71073 13.211161 11.162059 14.590576 90.0000 108.8334 90.0000 ZERR 9.00 0.001358 0.000934 0.001410 0.0000 0.0112 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C H N O UNIT 99.00 90.00 9.00 9.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 77884