data_shelx _audit_creation_method SHELXL-2014 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C50 H84 N4 O36 Zn4' _chemical_formula_weight 1578.69 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Zn' 'Zn' 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/c' _space_group_name_Hall '-P 2ybc' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 16.0116(7) _cell_length_b 29.3742(10) _cell_length_c 14.5726(6) _cell_angle_alpha 90 _cell_angle_beta 105.562(5) _cell_angle_gamma 90 _cell_volume 6602.6(5) _cell_formula_units_Z 4 _cell_measurement_temperature 293(2) _cell_measurement_reflns_used 6646 _cell_measurement_theta_min 1.9080 _cell_measurement_theta_max 27.2170 _exptl_crystal_description Block _exptl_crystal_colour yellow _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_density_diffrn 1.588 _exptl_crystal_F_000 3280 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.3670 _exptl_crystal_size_mid 0.3300 _exptl_crystal_size_min 0.2283 _exptl_absorpt_coefficient_mu 1.534 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type 'gaussian' _exptl_absorpt_correction_T_min 0.975 _exptl_absorpt_correction_T_max 0.983 _exptl_absorpt_process_details ; CrysAlisPro, Agilent Technologies, Version 1.171.37.33c (release 11-04-2014 CrysAlis171 .NET) (compiled Apr 11 2014,15:12:41) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_special_details ; Chemistry Department AMRC IIT Mandi Himachal Pradesh 175001 ; _diffrn_ambient_temperature 293(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'SuperNova (Mo) X-ray Source' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at zero, Eos' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean 7.9987 _diffrn_reflns_number 22971 _diffrn_reflns_av_unetI/netI 0.0775 _diffrn_reflns_av_R_equivalents 0.0320 _diffrn_reflns_limit_h_min -20 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_k_min -39 _diffrn_reflns_limit_k_max 25 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_theta_min 1.817 _diffrn_reflns_theta_max 28.303 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.848 _diffrn_measured_fraction_theta_full 0.970 _diffrn_reflns_Laue_measured_fraction_max 0.848 _diffrn_reflns_Laue_measured_fraction_full 0.970 _diffrn_reflns_point_group_measured_fraction_max 0.848 _diffrn_reflns_point_group_measured_fraction_full 0.970 _reflns_number_total 13939 _reflns_number_gt 8359 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection ; CrysAlisPro, Agilent Technologies, Version 1.171.37.33c (release 11-04-2014 CrysAlis171 .NET) (compiled Apr 11 2014,15:12:41) ; _computing_cell_refinement ; CrysAlisPro, Agilent Technologies, Version 1.171.37.33c (release 11-04-2014 CrysAlis171 .NET) (compiled Apr 11 2014,15:12:41) ; _computing_data_reduction ; CrysAlisPro, Agilent Technologies, Version 1.171.37.33c (release 11-04-2014 CrysAlis171 .NET) (compiled Apr 11 2014,15:12:41) ; _computing_structure_solution ? _computing_structure_refinement 'SHELXL-2014 (Sheldrick, 2014)' _computing_molecular_graphics 'Ortep for Windows (Farrugia, 2012)' _computing_publication_material 'WinGX publication routines (Farrugia, 2012)' _refine_special_details ; Chemistry Department AMRC IIT Mandi Himachal Pradesh 175001 ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0622P)^2^+17.0332P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 13939 _refine_ls_number_parameters 873 _refine_ls_number_restraints 6 _refine_ls_R_factor_all 0.1296 _refine_ls_R_factor_gt 0.0737 _refine_ls_wR_factor_ref 0.2082 _refine_ls_wR_factor_gt 0.1640 _refine_ls_goodness_of_fit_ref 1.066 _refine_ls_restrained_S_all 1.066 _refine_ls_shift/su_max 0.014 _refine_ls_shift/su_mean 0.001 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Zn2 Zn 0.80412(4) 0.35898(2) 0.47727(5) 0.03857(19) Uani 1 1 d . . . . . Zn3 Zn 0.70713(4) 0.63559(2) 1.03468(5) 0.03885(19) Uani 1 1 d . . . . . Zn1 Zn 0.75716(5) 0.30960(2) 0.65221(5) 0.0427(2) Uani 1 1 d . . . . . Zn4 Zn 0.75972(5) 0.68444(2) 0.86241(5) 0.0465(2) Uani 1 1 d . . . . . O1 O 0.7977(3) 0.37247(13) 0.6150(3) 0.0446(10) Uani 1 1 d . . . . . O14 O 0.7154(3) 0.62175(13) 0.8974(3) 0.0427(10) Uani 1 1 d . . . . . O17 O 0.6984(3) 0.63680(15) 1.1778(3) 0.0463(10) Uani 1 1 d D . . . . O18 O 0.8298(3) 0.65167(16) 1.0851(3) 0.0531(12) Uani 1 1 d . . . . . O7 O 0.6798(3) 0.34524(16) 0.4297(3) 0.0524(11) Uani 1 1 d . . . . . O9 O 0.8120(3) 0.35715(15) 0.3349(3) 0.0495(11) Uani 1 1 d D . . . . O13 O 0.8924(3) 0.52191(15) 0.9296(3) 0.0566(12) Uani 1 1 d . . . . . N2 N 0.8570(3) 0.42128(16) 0.4720(3) 0.0352(11) Uani 1 1 d . . . . . N3 N 0.6533(3) 0.57336(16) 1.0390(3) 0.0343(10) Uani 1 1 d . . . . . O22 O 0.8123(4) 0.73996(17) 0.8049(4) 0.0676(15) Uani 1 1 d D . . . . O5 O 0.8605(3) 0.27564(15) 0.6425(4) 0.0580(12) Uani 1 1 d . . . . . O4 O 0.7184(5) 0.25248(17) 0.7177(5) 0.090(2) Uani 1 1 d . . . . . O60 O 0.6077(3) 0.47471(16) 0.5775(4) 0.0628(13) Uani 1 1 d . . . . . O63 O 0.5689(4) 0.43603(17) 0.6917(4) 0.0789(17) Uani 1 1 d . . . . . O19 O 0.8676(3) 0.68418(18) 0.9656(3) 0.0659(15) Uani 1 1 d . . . . . O21 O 0.6235(3) 0.68545(17) 0.9969(4) 0.0591(13) Uani 1 1 d . . . . . N1 N 0.7464(3) 0.33646(16) 0.7751(4) 0.0387(11) Uani 1 1 d . . . . . O6 O 0.8833(3) 0.30676(15) 0.5128(3) 0.0526(11) Uani 1 1 d . . . . . O15 O 0.4741(3) 0.55836(15) 1.0375(4) 0.0549(12) Uani 1 1 d . . . . . H H 0.4361 0.5750 1.0059 0.082 Uiso 1 1 calc R U . . . O8 O 0.6526(3) 0.30512(18) 0.5485(4) 0.0645(14) Uani 1 1 d . . . . . N4 N 0.7495(3) 0.66175(16) 0.7298(3) 0.0368(11) Uani 1 1 d . . . . . O12 O 0.9290(4) 0.56166(15) 0.8156(4) 0.0705(15) Uani 1 1 d . . . . . O20 O 0.6593(4) 0.71925(16) 0.8779(4) 0.0711(15) Uani 1 1 d . . . . . O10 O 1.0338(3) 0.44065(15) 0.4656(4) 0.0569(12) Uani 1 1 d . . . . . H10 H 1.0727 0.4246 0.4976 0.085 Uiso 1 1 calc R U . . . O16 O 0.7042(3) 0.49404(18) 1.1673(4) 0.0749(16) Uani 1 1 d . . . . . H16 H 0.7397 0.5071 1.2103 0.112 Uiso 1 1 calc R U . . . O23 O 0.9085(4) 0.7092(2) 0.6133(4) 0.0740(16) Uani 1 1 d . . . . . HB H 0.9022 0.7001 0.5587 0.111 Uiso 1 1 calc R U . . . C33 C 0.6338(3) 0.54498(19) 0.9700(4) 0.0350(12) Uani 1 1 d . . . . . HC H 0.6052 0.5188 0.9808 0.042 Uiso 1 1 calc R U . . . O27 O 0.6461(5) 0.3861(2) 0.0568(5) 0.114(3) Uani 1 1 d . . . . . O11 O 0.7980(4) 0.5000(2) 0.3520(4) 0.0744(15) Uani 1 1 d . . . . . H11 H 0.7623 0.4920 0.3031 0.112 Uiso 1 1 calc R U . . . C31 C 0.6504(3) 0.54820(18) 0.8777(4) 0.0335(12) Uani 1 1 d . . . . . C8 C 0.8741(3) 0.45074(18) 0.5395(4) 0.0352(12) Uani 1 1 d . . . . . H8 H 0.9006 0.4774 0.5277 0.042 Uiso 1 1 calc R U . . . O3 O 0.5834(4) 0.2986(2) 0.8990(5) 0.093(2) Uani 1 1 d . . . . . H3 H 0.5418 0.2868 0.8612 0.139 Uiso 1 1 calc R U . . . C6 C 0.8333(4) 0.45074(19) 0.8148(4) 0.0404(14) Uani 1 1 d . . . . . H6 H 0.8251 0.4521 0.8756 0.048 Uiso 1 1 calc R U . . . O26 O 1.1561(4) 0.3823(2) 0.5525(5) 0.097(2) Uani 1 1 d . . . . . C7 C 0.7692(4) 0.3765(2) 0.8056(4) 0.0423(14) Uani 1 1 d . . . . . H7 H 0.7595 0.3841 0.8638 0.051 Uiso 1 1 calc R U . . . C4 C 0.8204(3) 0.40878(17) 0.6676(4) 0.0326(12) Uani 1 1 d . . . . . C14 C 0.9760(4) 0.4137(2) 0.3976(5) 0.0487(16) Uani 1 1 d . . . . . H14A H 0.9806 0.3822 0.4186 0.058 Uiso 1 1 calc R U . . . H14B H 0.9911 0.4151 0.3375 0.058 Uiso 1 1 calc R U . . . C30 C 0.6875(3) 0.58667(18) 0.8432(4) 0.0326(12) Uani 1 1 d . . . . . O28 O 0.6809(5) 0.3182(2) 0.1082(5) 0.101(2) Uani 1 1 d . . . . . O2 O 0.7971(4) 0.3276(2) 0.9916(4) 0.0850(18) Uani 1 1 d . . . . . H2 H 0.7569 0.3454 0.9874 0.127 Uiso 1 1 calc R U . . . C28 C 0.6666(4) 0.54680(19) 0.6913(4) 0.0421(14) Uani 1 1 d . . . . . HD H 0.6714 0.5462 0.6291 0.050 Uiso 1 1 calc R U . . . C5 C 0.8082(4) 0.41157(18) 0.7606(4) 0.0369(13) Uani 1 1 d . . . . . C29 C 0.6945(4) 0.58495(19) 0.7473(4) 0.0398(14) Uani 1 1 d . . . . . C43 C 0.7794(4) 0.6940(2) 0.6666(4) 0.0413(14) Uani 1 1 d . . . . . C34 C 0.7270(4) 0.6216(2) 0.6988(5) 0.0431(14) Uani 1 1 d . . . . . HE H 0.7320 0.6150 0.6381 0.052 Uiso 1 1 calc R U . . . C35 C 0.6244(3) 0.5652(2) 1.1257(4) 0.0360(13) Uani 1 1 d . . . . . C1 C 0.8698(4) 0.48757(19) 0.7814(4) 0.0385(13) Uani 1 1 d . . . . . C38 C 0.5319(4) 0.5842(2) 1.1082(5) 0.0453(15) Uani 1 1 d . . . . . H38A H 0.5143 0.5831 1.1668 0.054 Uiso 1 1 calc R U . . . H38B H 0.5307 0.6157 1.0880 0.054 Uiso 1 1 calc R U . . . C3 C 0.8569(3) 0.44734(18) 0.6322(4) 0.0332(12) Uani 1 1 d . . . . . C27 C 0.6319(4) 0.50955(19) 0.7261(4) 0.0399(14) Uani 1 1 d . . . . . C21 C 0.8995(4) 0.5278(2) 0.8420(5) 0.0463(15) Uani 1 1 d . . . . . C9 C 0.7072(4) 0.3059(2) 0.8338(4) 0.0436(15) Uani 1 1 d . . . . . O25 O 1.1686(5) 0.3118(2) 0.5911(5) 0.113(3) Uani 1 1 d . . . . . C32 C 0.6235(4) 0.51120(19) 0.8182(4) 0.0389(13) Uani 1 1 d . . . . . HG H 0.5989 0.4865 0.8410 0.047 Uiso 1 1 calc R U . . . C37 C 0.6848(4) 0.5915(2) 1.2063(4) 0.0471(15) Uani 1 1 d D . . . . HH H 0.6601 0.5926 1.2602 0.056 Uiso 1 1 calc R U . . . HI H 0.7400 0.5758 1.2263 0.056 Uiso 1 1 calc R U . . . C2 C 0.8808(3) 0.48528(19) 0.6905(4) 0.0384(13) Uani 1 1 d . . . . . H2A H 0.9051 0.5101 0.6675 0.046 Uiso 1 1 calc R U . . . C26 C 0.5997(4) 0.4692(2) 0.6653(5) 0.0500(16) Uani 1 1 d . . . . . C13 C 0.8829(4) 0.4304(2) 0.3836(4) 0.0393(13) Uani 1 1 d . . . . . C15 C 0.8230(4) 0.4025(2) 0.3050(5) 0.0523(16) Uani 1 1 d D . . . . H15A H 0.7668 0.4173 0.2853 0.063 Uiso 1 1 calc R U . . . H15B H 0.8467 0.4015 0.2503 0.063 Uiso 1 1 calc R U . . . C17 C 0.9007(4) 0.2791(2) 0.5792(5) 0.0467(15) Uani 1 1 d . . . . . C41 C 0.8836(4) 0.6699(2) 1.0481(5) 0.0467(15) Uani 1 1 d . . . . . O24 O 0.7061(4) 0.6619(3) 0.5091(4) 0.095(2) Uani 1 1 d . . . . . HJ H 0.6545 0.6576 0.4835 0.142 Uiso 1 1 calc R U . . . C22 C 0.9215(5) 0.5577(3) 0.9988(6) 0.067(2) Uani 1 1 d . . . . . H22A H 0.8922 0.5861 0.9760 0.081 Uiso 1 1 calc R U . . . H22B H 0.9835 0.5624 1.0107 0.081 Uiso 1 1 calc R U . . . C20 C 0.5365(4) 0.3209(3) 0.4114(6) 0.067(2) Uani 1 1 d . . . . . H20A H 0.5278 0.3401 0.3564 0.101 Uiso 1 1 calc R U . . . H20B H 0.4998 0.3308 0.4499 0.101 Uiso 1 1 calc R U . . . H20C H 0.5225 0.2900 0.3914 0.101 Uiso 1 1 calc R U . . . C25 C 0.5761(6) 0.4388(3) 0.5084(6) 0.077(2) Uani 1 1 d . . . . . HK H 0.5140 0.4353 0.4968 0.092 Uiso 1 1 calc R U . . . HL H 0.6039 0.4102 0.5314 0.092 Uiso 1 1 calc R U . . . C18 C 0.9742(5) 0.2473(3) 0.5850(7) 0.081(3) Uani 1 1 d . . . . . H18A H 1.0082 0.2448 0.6500 0.122 Uiso 1 1 calc R U . . . H18B H 1.0099 0.2587 0.5466 0.122 Uiso 1 1 calc R U . . . H18C H 0.9521 0.2178 0.5620 0.122 Uiso 1 1 calc R U . . . C39 C 0.6109(4) 0.7133(2) 0.9313(5) 0.0511(17) Uani 1 1 d . . . . . C50 C 1.1406(5) 0.3505(3) 0.6012(6) 0.063(2) Uani 1 1 d . . . . . C47 C 0.6420(5) 0.3542(3) 0.1123(6) 0.062(2) Uani 1 1 d . . . . . C16 C 0.8786(4) 0.4805(2) 0.3553(5) 0.0493(16) Uani 1 1 d . . . . . H16A H 0.9238 0.4970 0.4007 0.059 Uiso 1 1 calc R U . . . H16B H 0.8895 0.4833 0.2931 0.059 Uiso 1 1 calc R U . . . C42 C 0.9761(4) 0.6729(3) 1.1095(6) 0.071(2) Uani 1 1 d . . . . . HM H 0.9918 0.7043 1.1220 0.106 Uiso 1 1 calc R U . . . HN H 1.0142 0.6589 1.0770 0.106 Uiso 1 1 calc R U . . . HO H 0.9809 0.6574 1.1687 0.106 Uiso 1 1 calc R U . . . C36 C 0.6230(4) 0.5149(2) 1.1532(5) 0.0514(16) Uani 1 1 d . . . . . HP H 0.6046 0.5125 1.2112 0.062 Uiso 1 1 calc R U . . . HQ H 0.5809 0.4989 1.1033 0.062 Uiso 1 1 calc R U . . . C45 C 0.8684(4) 0.6777(2) 0.6638(5) 0.0558(18) Uani 1 1 d . . . . . HR H 0.9047 0.6742 0.7284 0.067 Uiso 1 1 calc R U . . . HS H 0.8633 0.6482 0.6330 0.067 Uiso 1 1 calc R U . . . C19 C 0.6303(4) 0.3235(2) 0.4689(5) 0.0463(16) Uani 1 1 d . . . . . C49 C 1.0910(5) 0.3593(3) 0.6703(6) 0.086(3) Uani 1 1 d . . . . . HT H 1.0333 0.3476 0.6464 0.129 Uiso 1 1 calc R U . . . HU H 1.0884 0.3915 0.6804 0.129 Uiso 1 1 calc R U . . . HV H 1.1188 0.3446 0.7295 0.129 Uiso 1 1 calc R U . . . C24 C 0.5978(7) 0.4527(3) 0.4197(6) 0.098(3) Uani 1 1 d . . . . . HW H 0.5720 0.4317 0.3696 0.147 Uiso 1 1 calc R U . . . HX H 0.6596 0.4526 0.4302 0.147 Uiso 1 1 calc R U . . . HY H 0.5759 0.4828 0.4020 0.147 Uiso 1 1 calc R U . . . C46 C 0.7783(6) 0.7412(2) 0.7095(6) 0.067(2) Uani 1 1 d D . . . . H46A H 0.8116 0.7620 0.6816 0.081 Uiso 1 1 calc R U . . . H46B H 0.7192 0.7523 0.6950 0.081 Uiso 1 1 calc R U . . . C23 C 0.8999(6) 0.5424(3) 1.0883(6) 0.082(3) Uani 1 1 d . . . . . H23A H 0.8381 0.5405 1.0769 0.123 Uiso 1 1 calc R U . . . H23B H 0.9226 0.5640 1.1384 0.123 Uiso 1 1 calc R U . . . H23C H 0.9252 0.5131 1.1068 0.123 Uiso 1 1 calc R U . . . C11 C 0.6265(4) 0.3284(3) 0.8489(7) 0.078(3) Uani 1 1 d . . . . . H11A H 0.6425 0.3563 0.8850 0.093 Uiso 1 1 calc R U . . . H11B H 0.5874 0.3363 0.7877 0.093 Uiso 1 1 calc R U . . . C40 C 0.5324(5) 0.7423(3) 0.9133(7) 0.084(3) Uani 1 1 d . . . . . H0AA H 0.4973 0.7329 0.9540 0.126 Uiso 1 1 calc R U . . . H1AA H 0.4996 0.7393 0.8479 0.126 Uiso 1 1 calc R U . . . H2AA H 0.5493 0.7735 0.9263 0.126 Uiso 1 1 calc R U . . . C44 C 0.7153(5) 0.6986(3) 0.5678(5) 0.066(2) Uani 1 1 d . . . . . H44A H 0.6588 0.7059 0.5765 0.079 Uiso 1 1 calc R U . . . H44B H 0.7332 0.7243 0.5358 0.079 Uiso 1 1 calc R U . . . C10 C 0.7710(5) 0.2933(3) 0.9282(6) 0.066(2) Uani 1 1 d . . . . . H10A H 0.7447 0.2698 0.9581 0.079 Uiso 1 1 calc R U . . . H10B H 0.8220 0.2801 0.9147 0.079 Uiso 1 1 calc R U . . . C48 C 0.5948(6) 0.3622(3) 0.1834(6) 0.085(3) Uani 1 1 d . . . . . H4AA H 0.5409 0.3458 0.1661 0.128 Uiso 1 1 calc R U . . . H5AA H 0.5834 0.3941 0.1866 0.128 Uiso 1 1 calc R U . . . H6AA H 0.6289 0.3518 0.2445 0.128 Uiso 1 1 calc R U . . . O29 O 0.7528(5) 0.4479(3) 1.0304(3) 0.139(3) Uani 1 1 d G . . . . H7AA H 0.7962 0.4306 1.0343 0.209 Uiso 1 1 d G U . . . H8AA H 0.7672 0.4694 1.0704 0.209 Uiso 1 1 d G U . . . O32 O 0.4451(5) 0.3634(3) 0.6249(5) 0.199(5) Uani 1 1 d G . . . . H9AA H 0.4989 0.3696 0.6396 0.298 Uiso 1 1 d G U . . . H0BA H 0.4158 0.3876 0.6093 0.298 Uiso 1 1 d G U . . . O31 O 0.7210(6) 0.5549(3) 0.4740(4) 0.172(4) Uani 1 1 d G . . . . H1BA H 0.7262 0.5310 0.4428 0.259 Uiso 1 1 d G U . . . H2BA H 0.7571 0.5748 0.4665 0.259 Uiso 1 1 d G U . . . O30 O 0.9101(6) 0.3970(4) 1.0855(8) 0.195(5) Uani 1 1 d . . . . . C12 C 0.6858(9) 0.2623(3) 0.7801(8) 0.151(6) Uani 1 1 d . . . . . H12A H 0.6991 0.2379 0.8266 0.181 Uiso 1 1 calc R U . . . H12B H 0.6235 0.2619 0.7527 0.181 Uiso 1 1 calc R U . . . O34 O 0.9164(3) 0.1997(2) 0.7790(6) 0.107(2) Uani 1 1 d G . . . . H3BA H 0.9656 0.2100 0.8095 0.160 Uiso 1 1 d G U . . . H4BA H 0.8940 0.2172 0.7326 0.160 Uiso 1 1 d G U . . . O33 O 0.4096(3) 0.3065(2) 0.7717(6) 0.117(3) Uani 1 1 d G . . . . H5BA H 0.3849 0.3024 0.7130 0.176 Uiso 1 1 d G U . . . H6BA H 0.4229 0.2807 0.7988 0.176 Uiso 1 1 d G U . . . H7BA H 0.653(3) 0.6527(14) 1.173(9) 0.176 Uiso 1 1 d D U . . . H9 H 0.851(5) 0.3402(12) 0.323(8) 0.176 Uiso 1 1 d D U . . . H4 H 0.715(3) 0.2314(19) 0.688(4) 0.026(15) Uiso 1 1 d . . . . . H22 H 0.793(6) 0.761(2) 0.835(2) 0.16(5) Uiso 1 1 d D . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Zn2 0.0478(4) 0.0332(4) 0.0404(4) -0.0056(3) 0.0217(3) -0.0114(3) Zn3 0.0458(4) 0.0380(4) 0.0368(4) -0.0059(3) 0.0182(3) -0.0134(3) Zn1 0.0626(5) 0.0294(4) 0.0448(4) -0.0053(3) 0.0295(4) -0.0101(3) Zn4 0.0685(5) 0.0394(4) 0.0381(4) -0.0085(3) 0.0258(4) -0.0218(3) O1 0.067(3) 0.032(2) 0.044(2) -0.008(2) 0.029(2) -0.0165(19) O14 0.064(3) 0.035(2) 0.036(2) -0.0097(19) 0.024(2) -0.0206(19) O17 0.051(2) 0.053(3) 0.040(2) -0.008(2) 0.022(2) -0.016(2) O18 0.046(2) 0.073(3) 0.045(3) -0.014(2) 0.019(2) -0.022(2) O7 0.049(2) 0.065(3) 0.048(3) -0.010(2) 0.021(2) -0.014(2) O9 0.061(3) 0.048(3) 0.048(3) -0.012(2) 0.029(2) -0.019(2) O13 0.078(3) 0.045(3) 0.051(3) -0.020(2) 0.024(3) -0.016(2) N2 0.041(2) 0.035(3) 0.032(3) 0.001(2) 0.014(2) -0.007(2) N3 0.040(2) 0.035(2) 0.028(2) 0.001(2) 0.011(2) -0.007(2) O22 0.117(4) 0.044(3) 0.053(3) -0.012(3) 0.041(3) -0.035(3) O5 0.075(3) 0.046(3) 0.065(3) 0.002(2) 0.041(3) 0.006(2) O4 0.185(7) 0.031(3) 0.089(5) -0.022(3) 0.098(5) -0.041(3) O60 0.094(4) 0.046(3) 0.053(3) -0.023(2) 0.030(3) -0.021(3) O63 0.131(5) 0.047(3) 0.065(4) -0.022(3) 0.037(3) -0.047(3) O19 0.072(3) 0.082(4) 0.043(3) 0.002(3) 0.012(2) -0.042(3) O21 0.065(3) 0.064(3) 0.056(3) 0.005(3) 0.030(3) 0.004(2) N1 0.049(3) 0.031(2) 0.041(3) 0.000(2) 0.021(2) -0.008(2) O6 0.064(3) 0.045(3) 0.055(3) 0.003(2) 0.027(2) 0.009(2) O15 0.042(2) 0.042(2) 0.074(3) 0.009(3) 0.003(2) -0.0066(19) O8 0.071(3) 0.073(3) 0.050(3) 0.007(3) 0.016(3) -0.031(3) N4 0.047(3) 0.033(3) 0.035(3) 0.000(2) 0.019(2) -0.005(2) O12 0.110(4) 0.038(3) 0.068(3) -0.018(3) 0.032(3) -0.035(3) O20 0.101(4) 0.050(3) 0.080(4) -0.003(3) 0.057(3) -0.008(3) O10 0.043(2) 0.045(3) 0.078(4) 0.005(3) 0.008(2) -0.005(2) O16 0.072(3) 0.070(4) 0.071(4) 0.009(3) -0.002(3) 0.023(3) O23 0.077(3) 0.084(4) 0.071(4) 0.002(3) 0.037(3) -0.032(3) C33 0.039(3) 0.031(3) 0.036(3) 0.001(3) 0.012(2) -0.008(2) O27 0.135(6) 0.107(5) 0.117(6) 0.067(5) 0.062(5) 0.062(4) O11 0.080(4) 0.069(4) 0.066(4) 0.001(3) 0.005(3) 0.020(3) C31 0.042(3) 0.029(3) 0.033(3) 0.000(2) 0.016(2) -0.008(2) C8 0.041(3) 0.027(3) 0.040(3) 0.001(3) 0.014(3) -0.004(2) O3 0.070(4) 0.109(5) 0.109(5) 0.017(4) 0.040(4) -0.030(3) C6 0.052(3) 0.034(3) 0.040(3) -0.007(3) 0.021(3) -0.008(3) O26 0.114(5) 0.081(4) 0.103(5) 0.038(4) 0.039(4) 0.017(4) C7 0.059(4) 0.037(3) 0.038(3) -0.006(3) 0.026(3) -0.014(3) C4 0.038(3) 0.023(3) 0.037(3) -0.006(2) 0.012(2) -0.006(2) C14 0.054(4) 0.039(3) 0.062(4) -0.006(3) 0.030(3) -0.009(3) C30 0.038(3) 0.027(3) 0.033(3) -0.004(2) 0.010(2) -0.006(2) O28 0.153(6) 0.074(4) 0.099(5) 0.030(4) 0.071(5) 0.049(4) O2 0.092(4) 0.087(5) 0.067(4) 0.013(4) 0.006(3) -0.018(3) C28 0.053(3) 0.036(3) 0.041(3) -0.009(3) 0.019(3) -0.006(3) C5 0.049(3) 0.026(3) 0.041(3) 0.004(3) 0.021(3) -0.002(2) C29 0.043(3) 0.035(3) 0.045(4) -0.002(3) 0.017(3) -0.005(2) C43 0.061(4) 0.034(3) 0.035(3) 0.003(3) 0.024(3) -0.010(3) C34 0.056(4) 0.039(3) 0.040(3) -0.009(3) 0.023(3) -0.013(3) C35 0.041(3) 0.040(3) 0.030(3) -0.002(3) 0.015(2) -0.006(2) C1 0.045(3) 0.028(3) 0.044(4) -0.008(3) 0.015(3) -0.007(2) C38 0.042(3) 0.044(4) 0.053(4) 0.003(3) 0.019(3) -0.006(3) C3 0.039(3) 0.027(3) 0.036(3) -0.002(2) 0.015(2) -0.003(2) C27 0.045(3) 0.032(3) 0.042(4) -0.008(3) 0.012(3) -0.006(2) C21 0.049(3) 0.034(3) 0.056(4) -0.015(3) 0.015(3) -0.009(3) C9 0.064(4) 0.034(3) 0.036(3) 0.000(3) 0.021(3) -0.014(3) O25 0.175(7) 0.080(4) 0.107(5) 0.047(4) 0.080(5) 0.049(5) C32 0.043(3) 0.031(3) 0.043(4) 0.000(3) 0.012(3) -0.010(2) C37 0.056(4) 0.051(4) 0.037(3) -0.008(3) 0.018(3) -0.006(3) C2 0.037(3) 0.032(3) 0.048(4) 0.002(3) 0.014(3) -0.005(2) C26 0.056(4) 0.040(4) 0.054(4) -0.016(3) 0.016(3) -0.011(3) C13 0.050(3) 0.037(3) 0.036(3) -0.004(3) 0.021(3) -0.007(3) C15 0.067(4) 0.047(4) 0.044(4) -0.005(3) 0.019(3) -0.009(3) C17 0.047(3) 0.045(4) 0.049(4) -0.007(3) 0.014(3) -0.005(3) C41 0.048(3) 0.049(4) 0.046(4) -0.007(3) 0.019(3) -0.015(3) O24 0.103(5) 0.115(5) 0.056(4) 0.000(4) 0.005(4) -0.029(4) C22 0.082(5) 0.054(4) 0.068(5) -0.026(4) 0.023(4) -0.010(4) C20 0.051(4) 0.080(6) 0.074(5) -0.016(5) 0.024(4) -0.020(4) C25 0.113(7) 0.060(5) 0.061(5) -0.034(4) 0.029(5) -0.025(5) C18 0.061(5) 0.085(6) 0.109(7) 0.018(6) 0.043(5) 0.021(4) C39 0.052(4) 0.045(4) 0.056(4) -0.011(4) 0.013(3) -0.013(3) C50 0.077(5) 0.044(4) 0.073(5) 0.015(4) 0.029(4) 0.005(4) C47 0.082(5) 0.046(4) 0.056(5) 0.007(4) 0.013(4) 0.006(4) C16 0.056(4) 0.045(4) 0.050(4) 0.008(3) 0.019(3) 0.002(3) C42 0.048(4) 0.093(6) 0.073(6) -0.008(5) 0.019(4) -0.024(4) C36 0.062(4) 0.048(4) 0.045(4) 0.016(3) 0.015(3) 0.002(3) C45 0.057(4) 0.056(4) 0.059(5) 0.007(4) 0.025(4) -0.009(3) C19 0.043(3) 0.046(4) 0.054(4) -0.013(3) 0.020(3) -0.011(3) C49 0.078(5) 0.117(8) 0.058(5) -0.004(5) 0.011(5) -0.006(5) C24 0.145(9) 0.087(7) 0.065(6) -0.033(6) 0.035(6) -0.005(6) C46 0.101(6) 0.042(4) 0.062(5) 0.005(4) 0.026(5) -0.014(4) C23 0.093(6) 0.083(6) 0.076(6) -0.025(5) 0.033(5) -0.011(5) C11 0.050(4) 0.082(6) 0.107(7) 0.032(5) 0.033(4) -0.008(4) C40 0.064(5) 0.082(6) 0.102(7) 0.016(6) 0.015(5) 0.010(4) C44 0.076(5) 0.074(5) 0.048(4) 0.025(4) 0.015(4) -0.003(4) C10 0.073(5) 0.065(5) 0.061(5) 0.020(4) 0.022(4) -0.003(4) C48 0.089(6) 0.098(7) 0.070(6) -0.012(5) 0.023(5) -0.002(5) O29 0.176(8) 0.123(7) 0.120(7) -0.009(6) 0.042(6) -0.015(6) O32 0.166(8) 0.260(13) 0.182(10) -0.084(9) 0.068(8) -0.109(8) O31 0.259(11) 0.146(8) 0.143(8) -0.034(7) 0.107(8) -0.070(8) O30 0.152(8) 0.209(11) 0.246(12) -0.086(10) 0.092(8) -0.077(7) C12 0.312(17) 0.067(6) 0.137(10) -0.059(6) 0.172(12) -0.111(9) O34 0.071(4) 0.106(5) 0.151(7) 0.071(5) 0.043(4) 0.009(3) O33 0.093(5) 0.098(5) 0.178(8) -0.028(5) 0.067(5) -0.011(4) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Zn2 O7 1.966(4) . ? Zn2 O6 1.969(4) . ? Zn2 N2 2.026(4) . ? Zn2 O1 2.076(4) . ? Zn2 O9 2.113(4) . ? Zn3 O18 1.961(4) . ? Zn3 O21 1.961(5) . ? Zn3 N3 2.029(4) . ? Zn3 O14 2.080(4) . ? Zn3 O17 2.128(4) . ? Zn1 O8 1.935(5) . ? Zn1 O5 1.969(4) . ? Zn1 N1 2.006(5) . ? Zn1 O1 2.077(4) . ? Zn1 O4 2.104(5) . ? Zn4 O19 1.962(5) . ? Zn4 O20 1.969(5) . ? Zn4 N4 2.009(5) . ? Zn4 O14 2.085(4) . ? Zn4 O22 2.109(5) . ? O1 C4 1.306(6) . ? O14 C30 1.302(6) . ? O17 C37 1.429(7) . ? O18 C41 1.252(7) . ? O7 C19 1.267(7) . ? O9 C15 1.428(7) . ? O13 C21 1.324(8) . ? O13 C22 1.445(8) . ? N2 C8 1.283(7) . ? N2 C13 1.480(7) . ? N3 C33 1.278(7) . ? N3 C35 1.477(7) . ? O22 C46 1.351(9) . ? O5 C17 1.262(7) . ? O4 C12 1.200(9) . ? O60 C26 1.330(8) . ? O60 C25 1.451(8) . ? O63 C26 1.202(8) . ? O19 C41 1.234(8) . ? O21 C39 1.233(8) . ? N1 C7 1.275(7) . ? N1 C9 1.490(7) . ? O6 C17 1.238(8) . ? O15 C38 1.408(7) . ? O8 C19 1.243(8) . ? N4 C34 1.278(7) . ? N4 C43 1.487(7) . ? O12 C21 1.208(7) . ? O20 C39 1.249(8) . ? O10 C14 1.404(7) . ? O16 C36 1.402(8) . ? O23 C45 1.434(7) . ? C33 C31 1.443(7) . ? O27 C47 1.252(9) . ? O11 C16 1.401(7) . ? C31 C32 1.385(7) . ? C31 C30 1.429(7) . ? C8 C3 1.452(7) . ? O3 C11 1.429(8) . ? C6 C1 1.380(8) . ? C6 C5 1.393(8) . ? O26 C50 1.236(9) . ? C7 C5 1.450(7) . ? C4 C5 1.422(8) . ? C4 C3 1.433(7) . ? C14 C13 1.531(8) . ? C30 C29 1.432(8) . ? O28 C47 1.236(9) . ? O2 C10 1.355(9) . ? C28 C27 1.383(8) . ? C28 C29 1.387(8) . ? C29 C34 1.459(8) . ? C43 C45 1.514(9) . ? C43 C46 1.523(9) . ? C43 C44 1.532(9) . ? C35 C37 1.517(8) . ? C35 C36 1.531(8) . ? C35 C38 1.539(8) . ? C1 C2 1.383(8) . ? C1 C21 1.475(8) . ? C3 C2 1.391(7) . ? C27 C32 1.385(8) . ? C27 C26 1.486(8) . ? C9 C12 1.492(10) . ? C9 C11 1.519(9) . ? C9 C10 1.523(9) . ? O25 C50 1.246(9) . ? C13 C15 1.521(8) . ? C13 C16 1.526(8) . ? C17 C18 1.487(9) . ? C41 C42 1.513(9) . ? O24 C44 1.359(10) . ? C22 C23 1.505(11) . ? C20 C19 1.512(9) . ? C25 C24 1.481(11) . ? C39 C40 1.483(10) . ? C50 C49 1.463(11) . ? C47 C48 1.456(11) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O7 Zn2 O6 116.89(19) . . ? O7 Zn2 N2 124.45(19) . . ? O6 Zn2 N2 117.88(19) . . ? O7 Zn2 O1 94.12(17) . . ? O6 Zn2 O1 95.14(18) . . ? N2 Zn2 O1 89.64(17) . . ? O7 Zn2 O9 88.29(17) . . ? O6 Zn2 O9 91.99(19) . . ? N2 Zn2 O9 81.39(17) . . ? O1 Zn2 O9 170.44(16) . . ? O18 Zn3 O21 117.7(2) . . ? O18 Zn3 N3 126.6(2) . . ? O21 Zn3 N3 114.68(19) . . ? O18 Zn3 O14 95.27(17) . . ? O21 Zn3 O14 95.19(18) . . ? N3 Zn3 O14 89.46(16) . . ? O18 Zn3 O17 87.22(17) . . ? O21 Zn3 O17 92.47(19) . . ? N3 Zn3 O17 81.07(17) . . ? O14 Zn3 O17 169.69(16) . . ? O8 Zn1 O5 118.5(2) . . ? O8 Zn1 N1 117.4(2) . . ? O5 Zn1 N1 122.6(2) . . ? O8 Zn1 O1 97.02(19) . . ? O5 Zn1 O1 96.01(18) . . ? N1 Zn1 O1 89.46(17) . . ? O8 Zn1 O4 90.1(2) . . ? O5 Zn1 O4 89.1(2) . . ? N1 Zn1 O4 78.6(2) . . ? O1 Zn1 O4 168.0(2) . . ? O19 Zn4 O20 119.5(2) . . ? O19 Zn4 N4 124.3(2) . . ? O20 Zn4 N4 115.1(2) . . ? O19 Zn4 O14 95.56(18) . . ? O20 Zn4 O14 95.07(18) . . ? N4 Zn4 O14 89.83(17) . . ? O19 Zn4 O22 86.8(2) . . ? O20 Zn4 O22 94.0(2) . . ? N4 Zn4 O22 79.21(19) . . ? O14 Zn4 O22 168.02(19) . . ? C4 O1 Zn2 130.1(3) . . ? C4 O1 Zn1 129.1(4) . . ? Zn2 O1 Zn1 100.52(16) . . ? C30 O14 Zn3 129.7(3) . . ? C30 O14 Zn4 129.4(3) . . ? Zn3 O14 Zn4 100.15(16) . . ? C37 O17 Zn3 108.9(3) . . ? C41 O18 Zn3 132.6(4) . . ? C19 O7 Zn2 129.9(4) . . ? C15 O9 Zn2 108.7(4) . . ? C21 O13 C22 118.8(5) . . ? C8 N2 C13 119.6(5) . . ? C8 N2 Zn2 125.8(4) . . ? C13 N2 Zn2 114.4(3) . . ? C33 N3 C35 120.0(5) . . ? C33 N3 Zn3 125.4(4) . . ? C35 N3 Zn3 114.0(3) . . ? C46 O22 Zn4 109.6(4) . . ? C17 O5 Zn1 128.0(5) . . ? C12 O4 Zn1 113.1(5) . . ? C26 O60 C25 118.4(5) . . ? C41 O19 Zn4 131.1(4) . . ? C39 O21 Zn3 132.1(5) . . ? C7 N1 C9 118.7(5) . . ? C7 N1 Zn1 126.1(4) . . ? C9 N1 Zn1 115.2(4) . . ? C17 O6 Zn2 135.4(4) . . ? C19 O8 Zn1 132.1(4) . . ? C34 N4 C43 118.4(5) . . ? C34 N4 Zn4 126.0(4) . . ? C43 N4 Zn4 115.3(4) . . ? C39 O20 Zn4 131.4(5) . . ? N3 C33 C31 128.5(5) . . ? C32 C31 C30 119.3(5) . . ? C32 C31 C33 115.4(5) . . ? C30 C31 C33 125.3(5) . . ? N2 C8 C3 127.7(5) . . ? C1 C6 C5 122.1(6) . . ? N1 C7 C5 128.0(5) . . ? O1 C4 C5 121.2(5) . . ? O1 C4 C3 120.7(5) . . ? C5 C4 C3 118.1(5) . . ? O10 C14 C13 110.3(5) . . ? O14 C30 C31 121.3(5) . . ? O14 C30 C29 121.1(5) . . ? C31 C30 C29 117.6(5) . . ? C27 C28 C29 121.4(6) . . ? C6 C5 C4 119.8(5) . . ? C6 C5 C7 115.1(5) . . ? C4 C5 C7 125.1(5) . . ? C28 C29 C30 120.3(5) . . ? C28 C29 C34 114.4(5) . . ? C30 C29 C34 125.3(5) . . ? N4 C43 C45 106.1(5) . . ? N4 C43 C46 106.5(5) . . ? C45 C43 C46 114.3(6) . . ? N4 C43 C44 113.1(5) . . ? C45 C43 C44 113.6(6) . . ? C46 C43 C44 103.2(6) . . ? N4 C34 C29 127.9(6) . . ? N3 C35 C37 107.4(4) . . ? N3 C35 C36 114.3(5) . . ? C37 C35 C36 109.8(5) . . ? N3 C35 C38 107.9(5) . . ? C37 C35 C38 109.1(5) . . ? C36 C35 C38 108.2(5) . . ? C6 C1 C2 118.4(5) . . ? C6 C1 C21 121.0(6) . . ? C2 C1 C21 120.6(5) . . ? O15 C38 C35 109.9(5) . . ? C2 C3 C4 119.0(5) . . ? C2 C3 C8 115.1(5) . . ? C4 C3 C8 125.9(5) . . ? C28 C27 C32 118.7(5) . . ? C28 C27 C26 121.4(6) . . ? C32 C27 C26 119.8(5) . . ? O12 C21 O13 123.9(6) . . ? O12 C21 C1 124.0(6) . . ? O13 C21 C1 112.1(5) . . ? N1 C9 C12 106.8(5) . . ? N1 C9 C11 109.1(5) . . ? C12 C9 C11 111.4(7) . . ? N1 C9 C10 112.4(5) . . ? C12 C9 C10 105.5(8) . . ? C11 C9 C10 111.5(6) . . ? C27 C32 C31 122.7(5) . . ? O17 C37 C35 111.4(5) . . ? C1 C2 C3 122.6(5) . . ? O63 C26 O60 124.0(6) . . ? O63 C26 C27 124.2(7) . . ? O60 C26 C27 111.7(5) . . ? N2 C13 C15 107.0(5) . . ? N2 C13 C16 114.0(5) . . ? C15 C13 C16 110.0(5) . . ? N2 C13 C14 108.5(5) . . ? C15 C13 C14 108.9(5) . . ? C16 C13 C14 108.4(5) . . ? O9 C15 C13 112.1(5) . . ? O6 C17 O5 124.8(6) . . ? O6 C17 C18 117.7(6) . . ? O5 C17 C18 117.4(7) . . ? O19 C41 O18 125.3(6) . . ? O19 C41 C42 118.1(6) . . ? O18 C41 C42 116.6(6) . . ? O13 C22 C23 106.3(6) . . ? O60 C25 C24 106.7(6) . . ? O21 C39 O20 125.2(7) . . ? O21 C39 C40 118.2(7) . . ? O20 C39 C40 116.6(7) . . ? O26 C50 O25 119.1(8) . . ? O26 C50 C49 119.4(8) . . ? O25 C50 C49 121.5(8) . . ? O28 C47 O27 119.6(8) . . ? O28 C47 C48 122.5(8) . . ? O27 C47 C48 117.8(8) . . ? O11 C16 C13 112.2(5) . . ? O16 C36 C35 112.4(5) . . ? O23 C45 C43 111.4(6) . . ? O8 C19 O7 125.6(6) . . ? O8 C19 C20 119.3(6) . . ? O7 C19 C20 115.1(6) . . ? O22 C46 C43 110.7(6) . . ? O3 C11 C9 110.7(6) . . ? O24 C44 C43 117.0(7) . . ? O2 C10 C9 116.3(6) . . ? O4 C12 C9 121.3(7) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C35 N3 C33 C31 175.3(5) . . . . ? Zn3 N3 C33 C31 5.0(8) . . . . ? N3 C33 C31 C32 178.3(6) . . . . ? N3 C33 C31 C30 -4.9(9) . . . . ? C13 N2 C8 C3 -177.5(5) . . . . ? Zn2 N2 C8 C3 -2.6(8) . . . . ? C9 N1 C7 C5 -180.0(6) . . . . ? Zn1 N1 C7 C5 -0.6(10) . . . . ? Zn2 O1 C4 C5 178.3(4) . . . . ? Zn1 O1 C4 C5 -9.0(8) . . . . ? Zn2 O1 C4 C3 -0.6(8) . . . . ? Zn1 O1 C4 C3 172.1(4) . . . . ? Zn3 O14 C30 C31 -5.4(8) . . . . ? Zn4 O14 C30 C31 -172.9(4) . . . . ? Zn3 O14 C30 C29 175.7(4) . . . . ? Zn4 O14 C30 C29 8.3(8) . . . . ? C32 C31 C30 O14 -178.5(5) . . . . ? C33 C31 C30 O14 4.8(9) . . . . ? C32 C31 C30 C29 0.4(8) . . . . ? C33 C31 C30 C29 -176.3(5) . . . . ? C1 C6 C5 C4 0.2(9) . . . . ? C1 C6 C5 C7 -178.7(6) . . . . ? O1 C4 C5 C6 179.9(5) . . . . ? C3 C4 C5 C6 -1.2(8) . . . . ? O1 C4 C5 C7 -1.4(9) . . . . ? C3 C4 C5 C7 177.5(5) . . . . ? N1 C7 C5 C6 -174.5(6) . . . . ? N1 C7 C5 C4 6.7(11) . . . . ? C27 C28 C29 C30 -0.3(9) . . . . ? C27 C28 C29 C34 -178.3(6) . . . . ? O14 C30 C29 C28 178.3(5) . . . . ? C31 C30 C29 C28 -0.6(8) . . . . ? O14 C30 C29 C34 -3.9(9) . . . . ? C31 C30 C29 C34 177.2(5) . . . . ? C34 N4 C43 C45 -72.5(7) . . . . ? Zn4 N4 C43 C45 101.8(5) . . . . ? C34 N4 C43 C46 165.3(6) . . . . ? Zn4 N4 C43 C46 -20.5(6) . . . . ? C34 N4 C43 C44 52.7(8) . . . . ? Zn4 N4 C43 C44 -133.1(5) . . . . ? C43 N4 C34 C29 -178.9(6) . . . . ? Zn4 N4 C34 C29 7.5(9) . . . . ? C28 C29 C34 N4 173.3(6) . . . . ? C30 C29 C34 N4 -4.6(10) . . . . ? C33 N3 C35 C37 157.2(5) . . . . ? Zn3 N3 C35 C37 -31.4(5) . . . . ? C33 N3 C35 C36 35.1(7) . . . . ? Zn3 N3 C35 C36 -153.5(4) . . . . ? C33 N3 C35 C38 -85.3(6) . . . . ? Zn3 N3 C35 C38 86.1(5) . . . . ? C5 C6 C1 C2 0.6(9) . . . . ? C5 C6 C1 C21 -177.1(5) . . . . ? N3 C35 C38 O15 67.2(6) . . . . ? C37 C35 C38 O15 -176.4(5) . . . . ? C36 C35 C38 O15 -57.0(6) . . . . ? O1 C4 C3 C2 -179.6(5) . . . . ? C5 C4 C3 C2 1.4(8) . . . . ? O1 C4 C3 C8 -1.1(9) . . . . ? C5 C4 C3 C8 180.0(5) . . . . ? N2 C8 C3 C2 -178.5(5) . . . . ? N2 C8 C3 C4 2.9(9) . . . . ? C29 C28 C27 C32 1.3(9) . . . . ? C29 C28 C27 C26 178.2(6) . . . . ? C22 O13 C21 O12 -0.3(10) . . . . ? C22 O13 C21 C1 178.0(6) . . . . ? C6 C1 C21 O12 -177.2(7) . . . . ? C2 C1 C21 O12 5.2(10) . . . . ? C6 C1 C21 O13 4.5(8) . . . . ? C2 C1 C21 O13 -173.1(5) . . . . ? C7 N1 C9 C12 178.9(8) . . . . ? Zn1 N1 C9 C12 -0.5(9) . . . . ? C7 N1 C9 C11 58.4(8) . . . . ? Zn1 N1 C9 C11 -121.0(5) . . . . ? C7 N1 C9 C10 -65.8(8) . . . . ? Zn1 N1 C9 C10 114.7(5) . . . . ? C28 C27 C32 C31 -1.6(9) . . . . ? C26 C27 C32 C31 -178.5(6) . . . . ? C30 C31 C32 C27 0.7(9) . . . . ? C33 C31 C32 C27 177.7(5) . . . . ? Zn3 O17 C37 C35 -38.4(5) . . . . ? N3 C35 C37 O17 46.0(6) . . . . ? C36 C35 C37 O17 170.9(5) . . . . ? C38 C35 C37 O17 -70.7(6) . . . . ? C6 C1 C2 C3 -0.3(9) . . . . ? C21 C1 C2 C3 177.4(5) . . . . ? C4 C3 C2 C1 -0.7(8) . . . . ? C8 C3 C2 C1 -179.4(5) . . . . ? C25 O60 C26 O63 1.0(11) . . . . ? C25 O60 C26 C27 -177.8(6) . . . . ? C28 C27 C26 O63 -179.9(7) . . . . ? C32 C27 C26 O63 -3.0(10) . . . . ? C28 C27 C26 O60 -1.1(9) . . . . ? C32 C27 C26 O60 175.8(6) . . . . ? C8 N2 C13 C15 -155.7(5) . . . . ? Zn2 N2 C13 C15 28.8(6) . . . . ? C8 N2 C13 C16 -33.9(7) . . . . ? Zn2 N2 C13 C16 150.6(4) . . . . ? C8 N2 C13 C14 87.0(6) . . . . ? Zn2 N2 C13 C14 -88.5(5) . . . . ? O10 C14 C13 N2 -67.7(6) . . . . ? O10 C14 C13 C15 176.2(5) . . . . ? O10 C14 C13 C16 56.6(7) . . . . ? Zn2 O9 C15 C13 39.0(6) . . . . ? N2 C13 C15 O9 -44.7(7) . . . . ? C16 C13 C15 O9 -169.0(5) . . . . ? C14 C13 C15 O9 72.3(6) . . . . ? Zn2 O6 C17 O5 7.4(11) . . . . ? Zn2 O6 C17 C18 -172.9(5) . . . . ? Zn1 O5 C17 O6 3.5(10) . . . . ? Zn1 O5 C17 C18 -176.3(5) . . . . ? Zn4 O19 C41 O18 -0.7(12) . . . . ? Zn4 O19 C41 C42 177.2(5) . . . . ? Zn3 O18 C41 O19 3.2(11) . . . . ? Zn3 O18 C41 C42 -174.7(5) . . . . ? C21 O13 C22 C23 176.5(6) . . . . ? C26 O60 C25 C24 -176.8(7) . . . . ? Zn3 O21 C39 O20 -9.7(11) . . . . ? Zn3 O21 C39 C40 170.4(5) . . . . ? Zn4 O20 C39 O21 9.5(11) . . . . ? Zn4 O20 C39 C40 -170.6(5) . . . . ? N2 C13 C16 O11 -51.9(7) . . . . ? C15 C13 C16 O11 68.2(7) . . . . ? C14 C13 C16 O11 -172.9(5) . . . . ? N3 C35 C36 O16 57.6(7) . . . . ? C37 C35 C36 O16 -63.2(7) . . . . ? C38 C35 C36 O16 177.8(5) . . . . ? N4 C43 C45 O23 -173.5(5) . . . . ? C46 C43 C45 O23 -56.4(8) . . . . ? C44 C43 C45 O23 61.7(8) . . . . ? Zn1 O8 C19 O7 12.6(11) . . . . ? Zn1 O8 C19 C20 -167.0(5) . . . . ? Zn2 O7 C19 O8 -1.4(10) . . . . ? Zn2 O7 C19 C20 178.2(4) . . . . ? Zn4 O22 C46 C43 -46.2(7) . . . . ? N4 C43 C46 O22 43.8(8) . . . . ? C45 C43 C46 O22 -73.1(8) . . . . ? C44 C43 C46 O22 163.1(6) . . . . ? N1 C9 C11 O3 175.7(6) . . . . ? C12 C9 C11 O3 58.0(9) . . . . ? C10 C9 C11 O3 -59.6(9) . . . . ? N4 C43 C44 O24 -69.2(8) . . . . ? C45 C43 C44 O24 51.8(8) . . . . ? C46 C43 C44 O24 176.2(7) . . . . ? N1 C9 C10 O2 66.9(8) . . . . ? C12 C9 C10 O2 -177.2(7) . . . . ? C11 C9 C10 O2 -56.1(8) . . . . ? Zn1 O4 C12 C9 -26.2(16) . . . . ? N1 C9 C12 O4 18.3(16) . . . . ? C11 C9 C12 O4 137.4(13) . . . . ? C10 C9 C12 O4 -101.5(13) . . . . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A O16 H16 O11 0.82 2.04 2.714(8) 139.8 1_556 O11 H11 O16 0.82 1.95 2.714(8) 155.0 1_554 C34 HE O24 0.93 2.28 2.943(9) 128.1 . O31 H1BA O11 0.85 2.17 2.906(10) 144.5 . O15 H O27 0.82 1.80 2.615(7) 176.3 3_666 O10 H10 O26 0.82 1.84 2.655(8) 170.6 . O23 HB O25 0.82 2.20 2.967(10) 155.6 3_766 C33 HC O15 0.93 2.58 3.480(7) 164.0 3_667 C8 H8 O10 0.93 2.62 3.524(7) 165.3 3_766 O3 H3 O33 0.82 2.24 2.910(9) 138.6 . C7 H7 O2 0.93 2.45 2.994(9) 117.6 . O2 H2 O27 0.82 2.56 3.308(9) 152.0 1_556 O24 HJ O32 0.82 2.02 2.773(13) 153.1 3_666 C16 H16A O10 0.97 2.63 3.491(8) 148.6 3_766 C36 HQ O15 0.97 2.62 3.530(9) 156.9 3_667 C49 HV O18 0.96 2.61 3.463(10) 148.7 3_767 C11 H11A O27 0.97 2.64 3.410(13) 136.9 1_556 C48 H6AA O7 0.96 2.61 3.516(10) 157.6 . O29 H7AA O30 0.85 2.03 2.852(14) 162.1 . O29 H8AA O16 0.85 2.07 2.694(9) 129.4 . O32 H9AA O63 0.85 2.28 2.898(7) 130.2 . O31 H2BA O26 0.85 1.95 2.800(9) 176.6 3_766 O34 H3BA O23 0.85 2.03 2.836(9) 158.4 2_746 O34 H4BA O5 0.85 2.14 2.963(7) 163.4 . O17 H7BA O33 0.848(10) 1.88(15) 2.64(6) 149(19) 3_667 O9 H9 O34 0.851(10) 1.80(3) 2.641(7) 169(12) 4_565 O15 H O27 0.82 1.80 2.615(7) 176.3 3_666 O10 H10 O26 0.82 1.84 2.655(8) 170.6 . O16 H16 O11 0.82 2.04 2.714(8) 139.8 1_556 O23 HB O25 0.82 2.20 2.967(10) 155.6 3_766 C33 HC O15 0.93 2.58 3.480(7) 164.0 3_667 O11 H11 O16 0.82 1.95 2.714(8) 155.0 1_554 C8 H8 O10 0.93 2.62 3.524(7) 165.3 3_766 O3 H3 O33 0.82 2.24 2.910(9) 138.6 . C7 H7 O2 0.93 2.45 2.994(9) 117.6 . O2 H2 O27 0.82 2.56 3.308(9) 152.0 1_556 C34 HE O24 0.93 2.28 2.943(9) 128.1 . O24 HJ O32 0.82 2.02 2.773(13) 153.1 3_666 C16 H16A O10 0.97 2.63 3.491(8) 148.6 3_766 C36 HQ O15 0.97 2.62 3.530(9) 156.9 3_667 C49 HV O18 0.96 2.61 3.463(10) 148.7 3_767 C11 H11A O27 0.97 2.64 3.410(13) 136.9 1_556 C48 H6AA O7 0.96 2.61 3.516(10) 157.6 . O29 H7AA O30 0.85 2.03 2.852(14) 162.1 . O29 H8AA O16 0.85 2.07 2.694(9) 129.4 . O32 H9AA O63 0.85 2.28 2.898(7) 130.2 . O31 H1BA O11 0.85 2.17 2.906(10) 144.5 . O31 H2BA O26 0.85 1.95 2.800(9) 176.6 3_766 O34 H3BA O23 0.85 2.03 2.836(9) 158.4 2_746 O34 H4BA O5 0.85 2.14 2.963(7) 163.4 . O17 H7BA O33 0.848(10) 1.88(15) 2.64(6) 149(19) 3_667 O9 H9 O34 0.851(10) 1.80(3) 2.641(7) 169(12) 4_565 _refine_diff_density_max 0.842 _refine_diff_density_min -0.802 _refine_diff_density_rms 0.111 _shelxl_version_number 2014-1 _shelx_res_file ; TITL CF solution in P21/c CELL 0.71073 16.0116 29.3742 14.5726 90.000 105.562 90.000 ZERR 4.00 0.0007 0.0010 0.0006 0.000 0.005 0.000 LATT 1 SYMM - X, 1/2 + Y, 1/2 - Z SFAC C H N O ZN UNIT 200 336 16 144 16 MERG 2 EQIV $1 +X,+Y,1+Z EQIV $2 +X,+Y,-1+Z EQIV $3 1-X,1-Y,1-Z EQIV $4 2-X,1-Y,1-Z EQIV $5 1-X,1-Y,2-Z EQIV $6 2-X,1-Y,2-Z EQIV $7 2-X,-0.5+Y,1.5-Z EQIV $8 +X,0.5-Y,-0.5+Z DFIX 0.85 0.01 O17 H7ba DFIX 0.85 0.01 O9 H9 DFIX 0.85 0.01 O22 H22 DANG 1.88837 0.02 C37 H7ba DANG 1.886222 0.02 C15 H9 DANG 1.886222 0.02 C46 H22 HTAB O16 O11_$1 HTAB O11 O16_$2 HTAB C34 O24 HTAB O31 O11 HTAB O15 O27_$3 HTAB O10 O26 HTAB O23 O25_$4 HTAB C33 O15_$5 HTAB C8 O10_$4 HTAB O3 O33 HTAB C7 O2 HTAB O2 O27_$1 HTAB O24 O32_$3 HTAB C16 O10_$4 HTAB C36 O15_$5 HTAB C49 O18_$6 HTAB C11 O27_$1 HTAB C48 O7 HTAB O29 O30 HTAB O29 O16 HTAB O32 O63 HTAB O31 O26_$4 HTAB O34 O23_$7 HTAB O34 O5 HTAB O17 O33_$5 HTAB O9 O34_$8 HTAB O15 O27_$3 HTAB O10 O26 HTAB O16 O11_$1 HTAB O23 O25_$4 HTAB C33 O15_$5 HTAB O11 O16_$2 HTAB C8 O10_$4 HTAB O3 O33 HTAB C7 O2 HTAB O2 O27_$1 HTAB C34 O24 HTAB O24 O32_$3 HTAB C16 O10_$4 HTAB C36 O15_$5 HTAB C49 O18_$6 HTAB C11 O27_$1 HTAB C48 O7 HTAB O29 O30 HTAB O29 O16 HTAB O32 O63 HTAB O31 O11 HTAB O31 O26_$4 HTAB O34 O23_$7 HTAB O34 O5 HTAB O17 O33_$5 HTAB O9 O34_$8 FMAP 2 PLAN 30 ACTA CONF L.S. 1 WGHT 0.062200 17.033201 FVAR 1.34182 ZN2 5 0.804117 0.358982 0.477275 11.00000 0.04780 0.03324 = 0.04040 -0.00557 0.02173 -0.01142 ZN3 5 0.707133 0.635587 1.034683 11.00000 0.04582 0.03804 = 0.03683 -0.00592 0.01822 -0.01341 ZN1 5 0.757163 0.309596 0.652211 11.00000 0.06265 0.02940 = 0.04478 -0.00529 0.02952 -0.01011 ZN4 5 0.759718 0.684440 0.862414 11.00000 0.06851 0.03944 = 0.03812 -0.00855 0.02583 -0.02179 O1 4 0.797669 0.372470 0.615038 11.00000 0.06653 0.03202 = 0.04361 -0.00807 0.02901 -0.01646 O14 4 0.715360 0.621754 0.897379 11.00000 0.06402 0.03460 = 0.03569 -0.00970 0.02426 -0.02063 O17 4 0.698391 0.636796 1.177786 11.00000 0.05132 0.05276 = 0.04036 -0.00777 0.02213 -0.01566 O18 4 0.829795 0.651674 1.085088 11.00000 0.04591 0.07290 = 0.04459 -0.01388 0.01934 -0.02181 O7 4 0.679822 0.345239 0.429705 11.00000 0.04884 0.06515 = 0.04817 -0.00988 0.02145 -0.01414 O9 4 0.812027 0.357153 0.334880 11.00000 0.06083 0.04768 = 0.04842 -0.01215 0.02916 -0.01858 O13 4 0.892365 0.521909 0.929634 11.00000 0.07755 0.04548 = 0.05065 -0.02039 0.02385 -0.01635 N2 3 0.856957 0.421281 0.472037 11.00000 0.04057 0.03532 = 0.03245 0.00052 0.01445 -0.00719 N3 3 0.653287 0.573361 1.038954 11.00000 0.04039 0.03532 = 0.02809 0.00056 0.01095 -0.00716 O22 4 0.812264 0.739960 0.804947 11.00000 0.11693 0.04417 = 0.05253 -0.01215 0.04126 -0.03487 O5 4 0.860471 0.275636 0.642516 11.00000 0.07542 0.04617 = 0.06530 0.00248 0.04132 0.00641 O4 4 0.718439 0.252478 0.717682 11.00000 0.18450 0.03135 = 0.08886 -0.02170 0.09775 -0.04126 O60 4 0.607657 0.474708 0.577480 11.00000 0.09433 0.04634 = 0.05340 -0.02348 0.02967 -0.02143 O63 4 0.568909 0.436030 0.691716 11.00000 0.13055 0.04675 = 0.06549 -0.02194 0.03677 -0.04658 O19 4 0.867623 0.684178 0.965571 11.00000 0.07152 0.08156 = 0.04279 0.00213 0.01224 -0.04207 O21 4 0.623484 0.685449 0.996900 11.00000 0.06536 0.06398 = 0.05557 0.00480 0.02956 0.00398 N1 3 0.746421 0.336464 0.775089 11.00000 0.04947 0.03119 = 0.04094 0.00013 0.02144 -0.00755 O6 4 0.883294 0.306764 0.512844 11.00000 0.06435 0.04465 = 0.05521 0.00289 0.02735 0.00889 O15 4 0.474126 0.558364 1.037518 11.00000 0.04155 0.04250 = 0.07368 0.00944 0.00349 -0.00657 AFIX 147 H 2 0.436074 0.575021 1.005885 11.00000 -1.50000 AFIX 0 O8 4 0.652589 0.305116 0.548549 11.00000 0.07089 0.07257 = 0.04998 0.00667 0.01630 -0.03069 N4 3 0.749470 0.661753 0.729761 11.00000 0.04691 0.03331 = 0.03475 0.00031 0.01886 -0.00454 O12 4 0.929012 0.561657 0.815553 11.00000 0.11043 0.03804 = 0.06769 -0.01793 0.03174 -0.03463 O20 4 0.659306 0.719249 0.877922 11.00000 0.10131 0.05048 = 0.08038 -0.00316 0.05691 -0.00848 O10 4 1.033776 0.440646 0.465563 11.00000 0.04334 0.04487 = 0.07771 0.00533 0.00807 -0.00468 AFIX 147 H10 2 1.072699 0.424603 0.497608 11.00000 -1.50000 AFIX 0 O16 4 0.704180 0.494037 1.167257 11.00000 0.07188 0.06958 = 0.07122 0.00928 -0.00169 0.02302 AFIX 83 H16 2 0.739716 0.507074 1.210305 11.00000 -1.50000 AFIX 0 O23 4 0.908473 0.709155 0.613342 11.00000 0.07738 0.08405 = 0.07078 0.00242 0.03742 -0.03178 AFIX 147 HB 2 0.902247 0.700054 0.558722 11.00000 -1.50000 AFIX 0 C33 1 0.633841 0.544975 0.970038 11.00000 0.03879 0.03120 = 0.03594 0.00108 0.01155 -0.00764 AFIX 43 HC 2 0.605241 0.518785 0.980827 11.00000 -1.20000 AFIX 0 O27 4 0.646072 0.386077 0.056768 11.00000 0.13523 0.10671 = 0.11717 0.06659 0.06236 0.06182 O11 4 0.798031 0.500030 0.352024 11.00000 0.08006 0.06869 = 0.06616 0.00109 0.00527 0.02013 AFIX 147 H11 2 0.762291 0.492048 0.303066 11.00000 -1.50000 AFIX 0 C31 1 0.650409 0.548203 0.877694 11.00000 0.04206 0.02897 = 0.03300 -0.00018 0.01619 -0.00835 C8 1 0.874067 0.450739 0.539527 11.00000 0.04062 0.02663 = 0.04024 0.00063 0.01395 -0.00397 AFIX 43 H8 2 0.900589 0.477442 0.527660 11.00000 -1.20000 AFIX 0 O3 4 0.583418 0.298624 0.898981 11.00000 0.06951 0.10892 = 0.10900 0.01733 0.03975 -0.02996 AFIX 147 H3 2 0.541801 0.286754 0.861150 11.00000 -1.50000 AFIX 0 C6 1 0.833277 0.450738 0.814838 11.00000 0.05153 0.03431 = 0.04004 -0.00732 0.02053 -0.00777 AFIX 43 H6 2 0.825131 0.452101 0.875611 11.00000 -1.20000 AFIX 0 O26 4 1.156067 0.382265 0.552509 11.00000 0.11371 0.08126 = 0.10266 0.03775 0.03879 0.01688 C7 1 0.769178 0.376483 0.805562 11.00000 0.05945 0.03690 = 0.03804 -0.00564 0.02606 -0.01353 AFIX 43 H7 2 0.759544 0.384119 0.863812 11.00000 -1.20000 AFIX 0 C4 1 0.820365 0.408776 0.667598 11.00000 0.03844 0.02306 = 0.03746 -0.00615 0.01226 -0.00606 C14 1 0.976033 0.413670 0.397594 11.00000 0.05367 0.03913 = 0.06171 -0.00568 0.03005 -0.00914 AFIX 23 H14A 2 0.980599 0.382211 0.418592 11.00000 -1.20000 H14B 2 0.991129 0.415135 0.337495 11.00000 -1.20000 AFIX 0 C30 1 0.687515 0.586671 0.843183 11.00000 0.03805 0.02716 = 0.03267 -0.00424 0.00969 -0.00611 O28 4 0.680907 0.318196 0.108222 11.00000 0.15308 0.07428 = 0.09872 0.03039 0.07136 0.04865 O2 4 0.797125 0.327554 0.991562 11.00000 0.09156 0.08723 = 0.06742 0.01314 0.00630 -0.01771 AFIX 147 H2 2 0.756941 0.345424 0.987447 11.00000 -1.50000 AFIX 0 C28 1 0.666605 0.546795 0.691344 11.00000 0.05335 0.03550 = 0.04077 -0.00888 0.01857 -0.00623 AFIX 43 HD 2 0.671350 0.546245 0.629132 11.00000 -1.20000 AFIX 0 C5 1 0.808246 0.411574 0.760569 11.00000 0.04904 0.02557 = 0.04125 0.00400 0.02115 -0.00235 C29 1 0.694485 0.584952 0.747281 11.00000 0.04339 0.03452 = 0.04458 -0.00216 0.01696 -0.00525 C43 1 0.779370 0.693998 0.666584 11.00000 0.06082 0.03447 = 0.03501 0.00335 0.02392 -0.00967 C34 1 0.726989 0.621634 0.698838 11.00000 0.05628 0.03875 = 0.04016 -0.00889 0.02293 -0.01285 AFIX 43 HE 2 0.731963 0.615041 0.638108 11.00000 -1.20000 AFIX 0 C35 1 0.624421 0.565168 1.125651 11.00000 0.04126 0.03955 = 0.03028 -0.00183 0.01505 -0.00624 C1 1 0.869764 0.487575 0.781365 11.00000 0.04510 0.02802 = 0.04397 -0.00797 0.01480 -0.00745 C38 1 0.531948 0.584192 1.108180 11.00000 0.04214 0.04399 = 0.05316 0.00251 0.01858 -0.00588 AFIX 23 H38A 2 0.514311 0.583095 1.166835 11.00000 -1.20000 H38B 2 0.530738 0.615709 1.087999 11.00000 -1.20000 AFIX 0 C3 1 0.856948 0.447344 0.632217 11.00000 0.03891 0.02718 = 0.03598 -0.00214 0.01451 -0.00291 C27 1 0.631901 0.509550 0.726113 11.00000 0.04542 0.03225 = 0.04227 -0.00848 0.01194 -0.00639 C21 1 0.899535 0.527780 0.841997 11.00000 0.04934 0.03434 = 0.05565 -0.01467 0.01478 -0.00925 C9 1 0.707184 0.305935 0.833811 11.00000 0.06442 0.03442 = 0.03612 0.00031 0.02069 -0.01364 O25 4 1.168603 0.311795 0.591091 11.00000 0.17542 0.07954 = 0.10720 0.04725 0.07989 0.04920 C32 1 0.623550 0.511197 0.818191 11.00000 0.04342 0.03064 = 0.04320 0.00018 0.01246 -0.00980 AFIX 43 HG 2 0.598908 0.486454 0.841010 11.00000 -1.20000 AFIX 0 C37 1 0.684752 0.591467 1.206285 11.00000 0.05624 0.05145 = 0.03667 -0.00809 0.01790 -0.00577 AFIX 23 HH 2 0.660080 0.592574 1.260198 11.00000 -1.20000 HI 2 0.740000 0.575803 1.226322 11.00000 -1.20000 AFIX 0 C2 1 0.880782 0.485277 0.690544 11.00000 0.03740 0.03153 = 0.04770 0.00157 0.01392 -0.00481 AFIX 43 H2A 2 0.905096 0.510082 0.667537 11.00000 -1.20000 AFIX 0 C26 1 0.599718 0.469234 0.665320 11.00000 0.05630 0.04001 = 0.05443 -0.01561 0.01635 -0.01081 C13 1 0.882862 0.430362 0.383595 11.00000 0.04962 0.03720 = 0.03648 -0.00370 0.02073 -0.00713 C15 1 0.822958 0.402528 0.304953 11.00000 0.06698 0.04747 = 0.04441 -0.00516 0.01858 -0.00854 AFIX 23 H15A 2 0.766818 0.417328 0.285303 11.00000 -1.20000 H15B 2 0.846660 0.401502 0.250319 11.00000 -1.20000 AFIX 0 C17 1 0.900705 0.279050 0.579247 11.00000 0.04715 0.04518 = 0.04852 -0.00735 0.01415 -0.00522 C41 1 0.883631 0.669857 1.048093 11.00000 0.04813 0.04947 = 0.04634 -0.00736 0.01933 -0.01508 O24 4 0.706105 0.661888 0.509093 11.00000 0.10334 0.11544 = 0.05637 0.00025 0.00534 -0.02868 AFIX 147 HJ 2 0.654491 0.657628 0.483489 11.00000 -1.50000 AFIX 0 C22 1 0.921543 0.557740 0.998799 11.00000 0.08181 0.05362 = 0.06762 -0.02629 0.02263 -0.00971 AFIX 23 H22A 2 0.892162 0.586082 0.976002 11.00000 -1.20000 H22B 2 0.983516 0.562357 1.010653 11.00000 -1.20000 AFIX 0 C20 1 0.536541 0.320881 0.411393 11.00000 0.05115 0.08003 = 0.07424 -0.01595 0.02358 -0.02010 AFIX 137 H20A 2 0.527762 0.340149 0.356412 11.00000 -1.50000 H20B 2 0.499832 0.330788 0.449879 11.00000 -1.50000 H20C 2 0.522506 0.290028 0.391399 11.00000 -1.50000 AFIX 0 C25 1 0.576146 0.438848 0.508357 11.00000 0.11290 0.06001 = 0.06113 -0.03381 0.02870 -0.02508 AFIX 23 HK 2 0.513961 0.435269 0.496828 11.00000 -1.20000 HL 2 0.603886 0.410150 0.531444 11.00000 -1.20000 AFIX 0 C18 1 0.974235 0.247258 0.584967 11.00000 0.06141 0.08502 = 0.10897 0.01814 0.04337 0.02109 AFIX 137 H18A 2 1.008184 0.244766 0.649959 11.00000 -1.50000 H18B 2 1.009875 0.258671 0.546611 11.00000 -1.50000 H18C 2 0.952101 0.217819 0.562023 11.00000 -1.50000 AFIX 0 C39 1 0.610869 0.713271 0.931272 11.00000 0.05234 0.04481 = 0.05557 -0.01055 0.01346 -0.01327 C50 1 1.140630 0.350527 0.601240 11.00000 0.07675 0.04365 = 0.07295 0.01535 0.02917 0.00497 C47 1 0.641974 0.354152 0.112302 11.00000 0.08192 0.04647 = 0.05550 0.00740 0.01294 0.00628 C16 1 0.878611 0.480480 0.355251 11.00000 0.05560 0.04458 = 0.05030 0.00790 0.01865 0.00194 AFIX 23 H16A 2 0.923761 0.497042 0.400691 11.00000 -1.20000 H16B 2 0.889493 0.483276 0.293143 11.00000 -1.20000 AFIX 0 C42 1 0.976075 0.672885 1.109539 11.00000 0.04835 0.09293 = 0.07303 -0.00768 0.01918 -0.02415 AFIX 137 HM 2 0.991793 0.704271 1.121952 11.00000 -1.50000 HN 2 1.014216 0.658948 1.076954 11.00000 -1.50000 HO 2 0.980869 0.657356 1.168695 11.00000 -1.50000 AFIX 0 C36 1 0.622999 0.514925 1.153191 11.00000 0.06222 0.04796 = 0.04472 0.01610 0.01545 0.00191 AFIX 23 HP 2 0.604613 0.512545 1.211246 11.00000 -1.20000 HQ 2 0.580934 0.498902 1.103306 11.00000 -1.20000 AFIX 0 C45 1 0.868412 0.677742 0.663805 11.00000 0.05710 0.05633 = 0.05944 0.00692 0.02495 -0.00920 AFIX 23 HR 2 0.904745 0.674242 0.728385 11.00000 -1.20000 HS 2 0.863307 0.648220 0.632969 11.00000 -1.20000 AFIX 0 C19 1 0.630284 0.323522 0.468857 11.00000 0.04325 0.04555 = 0.05400 -0.01265 0.01959 -0.01051 C49 1 1.091021 0.359328 0.670337 11.00000 0.07813 0.11715 = 0.05775 -0.00432 0.01051 -0.00645 AFIX 137 HT 2 1.033319 0.347576 0.646376 11.00000 -1.50000 HU 2 1.088441 0.391534 0.680442 11.00000 -1.50000 HV 2 1.118754 0.344650 0.729528 11.00000 -1.50000 AFIX 0 C24 1 0.597820 0.452695 0.419743 11.00000 0.14543 0.08654 = 0.06549 -0.03272 0.03483 -0.00494 AFIX 137 HW 2 0.572023 0.431721 0.369631 11.00000 -1.50000 HX 2 0.659624 0.452581 0.430198 11.00000 -1.50000 HY 2 0.575861 0.482756 0.401967 11.00000 -1.50000 AFIX 0 C46 1 0.778335 0.741184 0.709539 11.00000 0.10142 0.04156 = 0.06178 0.00467 0.02649 -0.01364 AFIX 23 H46A 2 0.811649 0.762016 0.681622 11.00000 -1.20000 H46B 2 0.719179 0.752298 0.694954 11.00000 -1.20000 AFIX 0 C23 1 0.899892 0.542434 1.088312 11.00000 0.09251 0.08335 = 0.07642 -0.02510 0.03347 -0.01116 AFIX 137 H23A 2 0.838093 0.540503 1.076868 11.00000 -1.50000 H23B 2 0.922587 0.563961 1.138360 11.00000 -1.50000 H23C 2 0.925190 0.513079 1.106788 11.00000 -1.50000 AFIX 0 C11 1 0.626450 0.328433 0.848915 11.00000 0.04969 0.08235 = 0.10744 0.03169 0.03261 -0.00815 AFIX 23 H11A 2 0.642487 0.356313 0.885017 11.00000 -1.20000 H11B 2 0.587354 0.336258 0.787698 11.00000 -1.20000 AFIX 0 C40 1 0.532350 0.742317 0.913301 11.00000 0.06383 0.08176 = 0.10226 0.01555 0.01460 0.01025 AFIX 137 H0AA 2 0.497326 0.732913 0.954028 11.00000 -1.50000 H1AA 2 0.499642 0.739320 0.847939 11.00000 -1.50000 H2AA 2 0.549267 0.773516 0.926305 11.00000 -1.50000 AFIX 0 C44 1 0.715316 0.698572 0.567847 11.00000 0.07566 0.07366 = 0.04819 0.02495 0.01523 -0.00251 AFIX 23 H44A 2 0.658837 0.705877 0.576499 11.00000 -1.20000 H44B 2 0.733242 0.724257 0.535845 11.00000 -1.20000 AFIX 0 C10 1 0.771005 0.293275 0.928165 11.00000 0.07312 0.06465 = 0.06116 0.01962 0.02159 -0.00316 AFIX 23 H10A 2 0.744678 0.269843 0.958130 11.00000 -1.20000 H10B 2 0.821985 0.280075 0.914714 11.00000 -1.20000 AFIX 0 C48 1 0.594776 0.362164 0.183428 11.00000 0.08913 0.09802 = 0.06981 -0.01165 0.02296 -0.00188 AFIX 137 H4AA 2 0.540893 0.345824 0.166101 11.00000 -1.50000 H5AA 2 0.583422 0.394135 0.186590 11.00000 -1.50000 H6AA 2 0.628902 0.351815 0.244476 11.00000 -1.50000 AFIX 6 O29 4 0.752837 0.447851 1.030401 11.00000 0.17564 0.12275 = 0.12024 -0.00949 0.04172 -0.01530 H7AA 2 0.796239 0.430555 1.034280 11.00000 -1.50000 H8AA 2 0.767242 0.469388 1.070429 11.00000 -1.50000 O32 4 0.445100 0.363361 0.624915 11.00000 0.16554 0.26040 = 0.18192 -0.08370 0.06752 -0.10919 H9AA 2 0.498889 0.369648 0.639551 11.00000 -1.50000 H0BA 2 0.415849 0.387649 0.609311 11.00000 -1.50000 O31 4 0.721033 0.554857 0.473977 11.00000 0.25919 0.14599 = 0.14266 -0.03427 0.10675 -0.07034 H1BA 2 0.726233 0.531027 0.442750 11.00000 -1.50000 H2BA 2 0.757104 0.574834 0.466523 11.00000 -1.50000 AFIX 0 O30 4 0.910111 0.396989 1.085533 11.00000 0.15160 0.20942 = 0.24576 -0.08594 0.09198 -0.07739 C12 1 0.685835 0.262339 0.780140 11.00000 0.31249 0.06735 = 0.13675 -0.05944 0.17155 -0.11064 AFIX 23 H12A 2 0.699128 0.237921 0.826603 11.00000 -1.20000 H12B 2 0.623546 0.261945 0.752659 11.00000 -1.20000 AFIX 6 O34 4 0.916393 0.199688 0.779018 11.00000 0.07125 0.10627 = 0.15104 0.07110 0.04325 0.00911 H3BA 2 0.965630 0.210007 0.809464 11.00000 -1.50000 H4BA 2 0.894008 0.217249 0.732576 11.00000 -1.50000 O33 4 0.409616 0.306488 0.771747 11.00000 0.09303 0.09783 = 0.17832 -0.02813 0.06720 -0.01088 H5BA 2 0.384865 0.302414 0.712979 11.00000 -1.50000 H6BA 2 0.422854 0.280730 0.798786 11.00000 -1.50000 AFIX 0 H7BA 2 0.653245 0.652693 1.173067 11.00000 -1.50000 H9 2 0.850678 0.340153 0.322573 11.00000 -1.50000 H4 2 0.714896 0.231420 0.687601 11.00000 0.02623 H22 2 0.793308 0.760856 0.834854 11.00000 0.15997 HKLF 4 REM CF solution in P21/c REM R1 = 0.0737 for 8359 Fo > 4sig(Fo) and 0.1296 for all 13939 data REM 873 parameters refined using 6 restraints END WGHT 0.0623 16.9978 REM Highest difference peak 0.842, deepest hole -0.802, 1-sigma level 0.111 Q1 1 0.3999 0.4092 0.5749 11.00000 0.05 0.83 Q2 1 0.7054 0.3273 0.6277 11.00000 0.05 0.82 Q3 1 0.6583 0.2656 0.7670 11.00000 0.05 0.81 Q4 1 0.6162 0.6366 0.9432 11.00000 0.05 0.77 Q5 1 0.7033 0.6865 0.8355 11.00000 0.05 0.76 Q6 1 0.7468 0.3599 0.3833 11.00000 0.05 0.70 Q7 1 0.7427 0.3694 0.4607 11.00000 0.05 0.69 Q8 1 1.1907 0.3310 0.6762 11.00000 0.05 0.69 Q9 1 0.7763 0.6359 1.1236 11.00000 0.05 0.68 Q10 1 0.7167 0.3450 0.5936 11.00000 0.05 0.65 Q11 1 0.6834 0.3453 0.5989 11.00000 0.05 0.65 Q12 1 0.8440 0.7336 0.7371 11.00000 0.05 0.64 Q13 1 0.7589 0.3918 0.4196 11.00000 0.05 0.64 Q14 1 0.8821 0.3590 0.5614 11.00000 0.05 0.63 Q15 1 0.8429 0.7006 0.9988 11.00000 0.05 0.62 Q16 1 0.6841 0.3265 0.1818 11.00000 0.05 0.61 Q17 1 0.7016 0.3091 0.5638 11.00000 0.05 0.61 Q18 1 0.8015 0.3465 0.7176 11.00000 0.05 0.60 Q19 1 0.8477 0.3945 0.5381 11.00000 0.05 0.60 Q20 1 0.7571 0.6739 1.0999 11.00000 0.05 0.60 Q21 1 0.8135 0.6820 0.9548 11.00000 0.05 0.60 Q22 1 0.8165 0.3085 0.7411 11.00000 0.05 0.60 Q23 1 0.9492 0.3589 1.1360 11.00000 0.05 0.60 Q24 1 0.8045 0.6471 0.9236 11.00000 0.05 0.59 Q25 1 0.7526 0.7488 0.7806 11.00000 0.05 0.59 Q26 1 0.8106 0.7198 0.9204 11.00000 0.05 0.58 Q27 1 0.6538 0.6531 1.0057 11.00000 0.05 0.57 Q28 1 0.7009 0.6848 0.7688 11.00000 0.05 0.55 Q29 1 1.0935 0.3582 0.5267 11.00000 0.05 0.54 Q30 1 0.7717 0.6581 0.5216 11.00000 0.05 0.53 ; _shelx_res_checksum 26073 _shelx_hkl_file ; -3 0 0 1367.52 151.505 1 -4 0 0 45487.1 1012.12 1 -5 0 0 3067.10 310.863 1 -6 0 0 15491.8 731.874 1 -7 0 0 3145.11 385.065 1 -8 0 0 12920.1 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66487.5 1602.82 3 -10 8 0 66777.8 1898.74 1 -11 8 0 14228.9 959.885 1 -11 -8 0 15383.5 1060.36 1 -12 -8 0 20818.6 1240.93 1 -12 8 0 20265.8 1164.91 1 -13 -8 0 4346.61 620.066 1 -13 8 0 3962.03 553.941 1 -14 8 0 5517.50 674.041 1 -14 -8 0 5972.66 724.740 1 -15 -8 0 1279.40 362.401 1 -15 8 0 1282.71 360.219 1 -16 -8 0 1089.69 356.667 1 -16 8 0 561.465 262.178 1 -17 -8 0 134.142 111.507 1 -17 8 0 428.328 223.152 1 -18 8 0 407.084 198.322 1 -18 -8 0 267.279 165.531 1 -19 8 0-60.9821 129.076 1 0 -9 0 60.0940 62.5198 2 1 -9 0 669.009 123.909 2 -1 -9 0 593.959 125.548 2 2 -9 0 97.7181 45.6954 2 -3 -9 0 7.75251 31.0700 1 3 -9 0-10.2077 28.1058 2 -4 -9 0 32244.9 982.395 1 4 -9 0 30875.1 851.683 2 -5 9 0 4550.79 342.755 1 -5 -9 0 4441.73 411.084 1 -6 -9 0 65845.5 1670.39 1 -6 9 0 64090.9 1423.75 1 6 -9 0 66240.2 1331.85 2 -6 9 0 65902.5 1477.77 3 -7 -9 0 995.560 239.290 1 7 -9 0 542.733 88.1286 2 -7 9 0 801.071 177.306 1 -7 9 0 706.831 159.637 3 -8 9 0 2187.10 277.354 3 -8 -9 0 2512.00 387.863 1 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10 0 46582.4 1190.69 1 -7 10 0 2266.89 294.365 1 -7 -10 0 2445.18 364.505 1 7 -10 0 2470.88 289.057 2 -8 -10 0 38757.0 1422.91 1 8 -10 0 40428.1 1202.20 2 -8 10 0 38634.8 1226.24 3 -8 10 0 38151.3 1268.03 1 -9 -10 0 6067.43 618.813 1 -9 10 0 5421.56 484.112 3 -9 10 0 5320.17 509.148 1 9 -10 0 5437.81 473.663 2 -10 10 0 8926.52 610.528 3 10 -10 0 8070.21 584.315 2 -10 -10 0 9633.84 793.736 1 -10 10 0 9211.18 702.973 1 -11 -10 0 5089.33 627.239 1 -11 10 0 4287.32 515.002 1 -12 10 0 6072.30 628.876 1 -12 -10 0 7179.07 741.313 1 -13 10 0 3656.27 563.573 1 -13 -10 0 4755.96 672.062 1 -14 10 0 787.281 265.526 1 -14 -10 0 1120.05 346.655 1 -15 10 0 1370.66 350.028 1 -15 -10 0 1422.96 380.083 1 -16 10 0 84.0861 101.953 1 -16 -10 0 217.320 148.791 1 -17 10 0 257.537 177.446 1 -17 -10 0 109.287 96.8906 1 -18 10 0 177.400 134.397 1 -18 -10 0-33.8676 133.086 1 0 -11 0 344.067 122.655 2 1 -11 0 449.310 117.751 2 -1 -11 0 424.713 117.429 2 2 -11 0 8854.65 478.610 2 -3 -11 0 105.894 25.0797 1 3 -11 0 196.440 67.3059 2 4 -11 0 2233.93 201.821 2 -4 -11 0 3277.23 324.055 1 -5 -11 0 1380.38 242.498 1 5 -11 0 1059.44 137.982 2 6 -11 0 3674.47 356.198 2 -6 11 0 2703.73 284.735 1 -6 -11 0 3094.48 362.784 1 -7 11 0 697.270 164.575 1 7 -11 0 1043.06 208.946 2 -7 -11 0 822.050 225.605 1 -8 -11 0 6881.51 626.105 1 -8 11 0 6887.42 532.644 1 8 -11 0 7288.79 503.110 2 -9 11 0 483.731 141.854 1 -9 -11 0 750.343 221.053 1 10 -11 0 6085.69 514.499 2 -10 -11 0 7318.96 693.550 1 -10 11 0 6414.61 586.594 1 -11 11 0 790.164 219.056 1 -11 -11 0 1248.28 335.483 1 -12 11 0 2511.94 405.800 1 -12 -11 0 3008.26 493.875 1 -13 11 0-25.2402 73.2528 1 -13 -11 0 233.408 174.059 1 -14 -11 0 994.684 332.104 1 -14 11 0 941.057 290.563 1 -15 11 0 97.8528 214.520 1 -15 -11 0 455.598 272.287 1 -16 -11 0 1204.79 377.084 1 -16 11 0 1041.01 308.387 1 -17 11 0 66.4119 85.5990 1 -17 -11 0-202.451 176.843 1 -18 -11 0 1159.50 378.478 1 0 -12 0 3360.15 346.545 2 1 -12 0 521.323 133.470 2 -1 -12 0 429.617 120.924 2 2 -12 0 1649.27 222.510 2 -2 -12 0 1515.54 228.715 2 -3 -12 0 889.167 159.040 1 3 -12 0 1007.12 175.676 2 4 -12 0 2018.43 230.099 2 -4 -12 0 2014.38 270.615 1 -5 -12 0 1893.74 289.096 1 5 -12 0 1521.55 182.247 2 -6 -12 0 10502.3 683.977 1 6 -12 0 10137.2 577.706 2 -7 -12 0 111.042 97.7587 1 7 -12 0 279.213 127.395 2 -7 12 0 47.0802 45.6625 1 -8 12 0 1003.80 197.487 1 -8 -12 0 1020.42 245.065 1 8 -12 0 799.550 160.822 2 9 -12 0 465.278 77.0582 2 -9 12 0 1294.46 247.501 1 -9 -12 0 1392.64 321.253 1 -10 -12 0 1417.92 331.661 1 -10 12 0 1271.02 255.076 1 -11 12 0 222.777 92.2671 1 -11 -12 0 340.050 163.862 1 -12 -12 0 553.699 241.178 1 -12 12 0 235.205 114.062 1 -13 12 0 275.684 137.695 1 -13 -12 0 304.441 177.053 1 -14 12 0 3158.76 486.069 1 -14 -12 0 3322.52 564.448 1 -15 -12 0 75.0595 115.700 1 -15 12 0 20.7124 68.7675 1 -16 -12 0 2700.86 541.839 1 -17 -12 0 165.288 120.503 1 -18 -12 0 519.767 254.033 1 0 -13 0 665.482 178.253 2 1 -13 0 13.7961 27.8494 2 -1 -13 0-26.1071 42.2482 2 -2 -13 0 36230.0 1216.50 2 2 -13 0 33602.7 1063.03 2 -3 -13 0-39.9669 62.9325 1 3 -13 0-4.25248 34.0453 2 -4 -13 0 138712. 2214.38 1 4 -13 0 144685. 2118.65 2 -5 -13 0 65.8562 75.5025 1 -6 -13 0 23709.0 1046.99 1 6 -13 0 25032.5 939.116 2 -7 -13 0 776.649 208.909 1 7 -13 0 883.224 199.611 2 -8 -13 0 26847.6 1221.97 1 8 -13 0 28309.2 1051.97 2 -9 13 0 331.009 120.877 1 -9 -13 0 227.678 166.991 1 -10 13 0 5730.87 554.264 1 -10 -13 0 6611.09 680.923 1 -11 13 0 3.66365 30.5239 1 -11 -13 0 273.925 156.482 1 -12 13 0 310.676 147.321 1 -12 -13 0 413.816 199.070 1 -13 -13 0 1561.10 397.691 1 -13 13 0 1270.01 304.935 1 -14 13 0 1768.06 359.010 1 -14 -13 0 1758.75 425.420 1 -15 -13 0 1037.12 352.234 1 -16 -13 0 523.371 257.135 1 -17 -13 0 481.942 240.569 1 -18 -13 0 265.930 173.188 1 0 -14 0 9499.14 614.096 2 -1 -14 0-9.16206 50.4530 2 1 -14 0 35.0469 44.1651 2 -2 -14 0 1510.29 255.234 2 2 -14 0 1790.21 253.363 2 3 -14 0 110.338 58.8567 2 -3 -14 0-6.54784 65.8760 1 -3 -14 0-10.0762 75.7194 2 4 -14 0 12049.9 630.898 2 -4 -14 0 12518.6 669.131 1 -5 -14 0 1248.79 245.101 1 5 -14 0 741.411 109.550 2 -6 -14 0 19929.4 965.265 1 6 -14 0 20665.8 881.588 2 -7 -14 0 1826.48 327.057 1 7 -14 0 1618.93 271.085 2 8 -14 0 53486.9 1458.89 2 -8 -14 0 53858.5 1777.47 1 9 -14 0 2658.75 345.959 2 -9 -14 0 2831.67 462.078 1 -10 -14 0 25232.0 1350.03 1 -10 14 0 25096.9 1155.30 1 -11 14 0 2978.81 427.865 1 -11 -14 0 3334.63 528.688 1 -12 14 0 7759.64 710.773 1 -12 -14 0 7888.06 816.126 1 -13 -14 0 1626.49 382.967 1 -14 -14 0 3369.29 585.706 1 -15 -14 0 616.758 269.472 1 -16 -14 0 208.530 148.995 1 -17 -14 0 343.023 255.593 1 -18 -14 0 509.716 236.009 1 0 -15 0 1153.40 259.367 2 1 -15 0 5188.61 468.685 2 -1 -15 0 4772.53 474.504 2 -2 -15 0 41541.5 1393.57 2 2 -15 0 41899.2 1269.03 2 3 -15 0 602.850 156.116 2 -3 -15 0 485.719 143.240 1 -3 -15 0 581.565 191.000 2 -4 -15 0 15449.2 764.490 1 4 -15 0 16424.1 768.449 2 -5 -15 0 253.737 124.689 1 6 -15 0 10976.9 656.694 2 -6 -15 0 12073.5 779.481 1 -7 -15 0 47.4579 62.6631 1 7 -15 0 172.318 105.296 2 -8 -15 0 559.445 187.680 1 8 -15 0 549.006 155.153 2 -9 -15 0 538.223 186.438 1 -10 -15 0 942.923 264.868 1 -11 -15 0 404.589 207.305 1 -12 -15 0 2047.60 415.927 1 -13 -15 0 262.480 199.116 1 -14 -15 0 3920.76 636.849 1 -15 -15 0 465.237 252.093 1 -16 -15 0 335.606 228.920 1 -17 -15 0 139.228 153.125 1 0 -16 0 164294. 2737.10 2 1 -16 0 1884.93 333.461 2 -1 -16 0 1781.61 339.297 2 -2 -16 0 52027.0 1609.00 2 2 -16 0 49704.8 1441.59 2 -3 -16 0 239.557 117.330 2 3 -16 0 333.293 137.536 2 -3 -16 0 191.822 74.1019 1 -4 -16 0 58088.3 1813.89 2 -4 -16 0 57625.8 1498.80 1 4 -16 0 57480.8 1477.26 2 -5 -16 0 335.510 126.990 1 5 -16 0-82.2382 151.733 2 6 -16 0 31729.0 1157.72 2 -6 -16 0 30223.2 1220.39 1 -7 -16 0 1013.78 260.710 1 7 -16 0 211.560 95.7386 2 -8 -16 0 11489.6 825.657 1 8 -16 0 11023.7 691.467 2 -9 -16 0 23.2395 29.8050 1 -10 -16 0 7483.30 723.319 1 -11 -16 0 823.972 285.304 1 -12 -16 0 1745.07 396.130 1 -13 -16 0 790.800 298.437 1 -14 -16 0 2928.14 559.731 1 -15 -16 0 922.467 321.246 1 -16 -16 0 360.866 233.826 1 -17 -16 0 834.438 317.909 1 0 -17 0 2137.42 366.744 2 1 -17 0 39.0378 52.9495 2 -1 -17 0 193.276 129.954 2 2 -17 0 6276.62 524.101 2 -2 -17 0 5913.75 568.476 2 -3 -17 0 222.998 145.122 1 3 -17 0 44.4236 70.5722 2 4 -17 0 5653.65 479.400 2 -4 -17 0 5682.10 478.229 1 -4 -17 0 5631.88 575.765 2 5 -17 0 35.3381 34.2856 2 -5 -17 0 55.0338 78.4734 1 -6 -17 0 9055.58 674.439 1 6 -17 0 7673.16 580.298 2 -7 -17 0 173.181 96.4570 1 7 -17 0-48.5291 47.8341 2 8 -17 0 8439.00 629.625 2 -8 -17 0 9297.42 749.097 1 -9 -17 0 136.049 69.4515 1 -10 -17 0 8123.15 774.220 1 -11 -17 0 562.698 226.635 1 -12 -17 0 1213.06 327.242 1 -13 -17 0 1043.25 330.400 1 -14 -17 0 3349.13 598.116 1 -15 -17 0 589.894 264.479 1 -16 -17 0 561.218 255.941 1 -17 -17 0 445.090 250.524 1 0 -18 0 94053.6 2206.61 2 1 -18 0 444.899 196.423 2 -1 -18 0 87.5034 91.4546 2 -2 -18 0 62355.9 1418.09 1 -2 -18 0 64285.7 1913.08 2 2 -18 0 61002.8 1717.41 2 3 -18 0 945.422 206.826 2 -3 -18 0 904.884 244.867 2 -3 -18 0 715.253 172.070 1 -4 -18 0 14668.2 777.881 1 4 -18 0 12626.3 747.670 2 -4 -18 0 14579.0 967.470 2 -5 -18 0 1303.38 260.319 1 5 -18 0 1019.09 223.627 2 -6 -18 0 2561.76 369.250 1 6 -18 0 1854.60 243.286 2 7 -18 0 137.096 54.2256 2 -7 -18 0 249.733 133.965 1 -8 -18 0 3315.98 454.118 1 -9 -18 0 1.81714 73.5773 1 -10 -18 0 9419.61 828.106 1 -11 -18 0 91.9063 63.6788 1 -12 -18 0 687.460 259.338 1 -13 -18 0 35.6697 9.03321 1 -14 -18 0 102.657 101.508 1 -15 -18 0 100.087 77.1915 1 -16 -18 0 322.176 208.468 1 -17 -18 0 945.906 340.045 1 0 -19 0 2387.96 392.226 2 -1 -19 0 10723.0 805.215 2 1 -19 0 10718.3 773.580 2 -2 -19 0 6557.56 639.036 2 2 -19 0 6448.39 558.838 2 -2 -19 0 6491.16 468.872 1 3 -19 0 2905.34 378.449 2 -3 -19 0 2900.78 447.591 2 -3 -19 0 2524.61 323.270 1 4 -19 0 4811.70 473.126 2 -4 -19 0 4489.53 434.626 1 -4 -19 0 4932.68 552.878 2 -5 -19 0 347.513 143.947 1 -5 -19 0 518.166 282.761 2 5 -19 0 463.614 162.507 2 -6 -19 0 31520.7 1305.45 1 6 -19 0 31977.4 1254.44 2 -6 -19 0 32863.6 1547.16 2 7 -19 0-317.408 198.002 2 -7 -19 0 358.107 227.027 1 -8 -19 0 189.181 119.883 1 -9 -19 0-12.9228 46.1666 1 -10 -19 0 1406.38 329.076 1 -11 -19 0 18.9184 60.2848 1 -12 -19 0 4990.25 668.345 1 -13 -19 0 599.722 243.719 1 -14 -19 0 586.525 249.496 1 -15 -19 0 312.564 176.942 1 -16 -19 0 238.423 185.787 1 -17 -19 0 125.312 129.769 1 0 -20 0 4976.21 547.091 2 -1 -20 0 1114.04 306.619 2 1 -20 0 973.433 368.218 2 2 -20 0 1214.10 247.437 2 -2 -20 0 1306.51 208.427 1 -2 -20 0 1257.47 279.682 2 -3 -20 0 1222.39 330.979 2 3 -20 0 889.135 204.904 2 -3 -20 0 846.205 205.257 1 -4 -20 0 1485.60 327.047 2 4 -20 0 1326.51 252.290 2 -4 -20 0 1383.06 248.683 1 5 -20 0 2205.48 343.494 2 -5 -20 0 1844.45 308.466 1 -5 -20 0 2288.27 431.691 2 6 -20 0 3231.23 345.053 2 -6 -20 0 4076.29 479.939 1 -6 -20 0 4373.22 587.310 2 7 -20 0 359.948 124.921 2 -7 -20 0 785.779 231.289 1 -8 -20 0 4913.52 572.180 1 -9 -20 0 93.8976 76.7760 1 -10 -20 0 573.900 208.752 1 -11 -20 0 559.961 217.968 1 -12 -20 0 2692.85 493.051 1 -13 -20 0 78.7107 37.8872 1 -14 -20 0 376.449 210.807 1 -15 -20 0 80.5141 80.5453 1 -16 -20 0 487.021 242.383 1 0 -21 0 2096.46 396.683 2 1 -21 0 10239.3 784.174 2 -1 -21 0 10752.6 857.047 2 -2 -21 0 4089.40 384.716 1 -2 -21 0 4270.22 537.633 2 2 -21 0 3967.35 479.825 2 -3 -21 0 7933.98 763.150 2 3 -21 0 6669.36 607.796 2 -3 -21 0 5987.00 512.218 1 4 -21 0 6547.87 588.137 2 -4 -21 0 7008.82 697.968 2 -4 -21 0 6728.37 543.870 1 5 -21 0 2282.50 354.898 2 -5 -21 0 2185.03 433.667 2 -5 -21 0 2001.30 326.275 1 6 -21 0 26706.8 1207.40 2 -6 -21 0 29789.8 1549.58 2 -6 -21 0 28233.1 1243.73 1 -7 -21 0 570.082 205.467 1 -7 -21 0 1015.06 323.155 2 -8 -21 0 274.820 171.090 2 -8 -21 0 354.839 134.575 1 -9 -21 0-15.3801 115.365 1 -10 -21 0 2663.12 457.075 1 -11 -21 0 31.9185 51.1199 1 -12 -21 0 986.459 302.806 1 -13 -21 0 24.0053 56.5281 1 -14 -21 0 226.889 152.399 1 -15 -21 0 138.401 157.428 1 -16 -21 0 2289.90 535.885 1 0 -22 0 58039.3 1931.47 2 -1 -22 0 358.384 158.091 2 1 -22 0 189.686 131.332 2 2 -22 0 46603.6 1651.11 2 -2 -22 0 47504.4 1821.09 2 -3 -22 0 835.080 256.094 2 3 -22 0 703.823 194.508 2 4 -22 0 6602.53 613.316 2 -4 -22 0 6688.01 557.796 1 -4 -22 0 7172.29 745.048 2 -5 -22 0 1246.35 268.609 1 -5 -22 0 1248.69 336.761 2 5 -22 0 1137.08 255.876 2 6 -22 0 3297.71 345.468 2 -6 -22 0 4841.45 632.692 2 -6 -22 0 4576.67 511.760 1 -7 -22 0 465.679 226.588 2 -7 -22 0 277.351 131.090 1 -8 -22 0 2632.66 404.857 1 -8 -22 0 2337.91 452.058 2 -9 -22 0-86.2459 111.119 1 -9 -22 0-250.620 224.651 2 -10 -22 0 977.083 262.796 1 -11 -22 0-66.9805 61.6983 1 -12 -22 0 1816.41 413.952 1 -13 -22 0 170.215 129.304 1 -14 -22 0 210.760 170.202 1 -15 -22 0 112.053 98.0373 1 -16 -22 0 604.702 292.528 1 -16 -22 0 374.581 191.012 2 0 -23 0 2324.67 434.890 2 1 -23 0 750.556 246.989 2 -1 -23 0 924.098 277.367 2 -2 -23 0 14110.7 1028.96 2 2 -23 0 14399.8 954.134 2 3 -23 0 84.9637 82.2570 2 -3 -23 0 206.060 169.580 2 -4 -23 0 11603.8 962.757 2 4 -23 0 11384.3 822.567 2 5 -23 0 1526.45 308.652 2 -5 -23 0 1613.84 381.778 2 -6 -23 0-20.0759 56.4021 2 -6 -23 0 73.4515 84.3634 1 -7 -23 0 2066.46 377.400 1 -7 -23 0 2170.31 462.842 2 -8 -23 0 1401.28 307.893 1 -8 -23 0 1432.18 375.683 2 -9 -23 0 829.012 248.182 1 -9 -23 0 698.127 245.520 2 -10 -23 0 616.256 231.686 1 -10 -23 0 519.231 205.980 2 -11 -23 0 107.731 107.721 1 -11 -23 0 34.3292 93.1774 2 -12 -23 0 4079.97 623.979 1 -12 -23 0 3891.52 661.536 2 -13 -23 0 301.100 199.986 1 -13 -23 0 54.1356 64.0336 2 -14 -23 0 3427.38 622.534 1 -14 -23 0 3273.65 635.485 2 -15 -23 0 160.335 62.4381 2 -15 -23 0 384.114 248.696 1 -16 -23 0 269.586 196.765 1 0 -24 0 27673.5 1406.00 2 -1 -24 0 1120.95 297.922 2 1 -24 0 1058.62 281.462 2 -2 -24 0 2965.23 482.852 2 2 -24 0 2801.21 435.175 2 3 -24 0 7543.72 702.290 2 -3 -24 0 7833.08 810.472 2 4 -24 0 166.138 103.405 2 -4 -24 0 250.131 161.066 2 -5 -24 0 2624.34 486.280 2 5 -24 0 2725.06 418.010 2 -6 -24 0 2624.31 473.325 2 6 -24 0 1298.60 134.705 2 -7 -24 0 1889.53 433.250 2 -8 -24 0 1283.16 292.236 1 -8 -24 0 1179.98 340.968 2 -9 -24 0 557.988 215.469 2 -9 -24 0 673.806 236.939 1 -10 -24 0 1117.46 299.056 1 -10 -24 0 851.201 280.708 2 -11 -24 0 310.565 179.130 1 -11 -24 0 30.1583 56.5758 2 -12 -24 0 1349.11 373.653 1 -12 -24 0 1319.64 391.186 2 -13 -24 0-208.173 206.098 2 -13 -24 0 125.002 87.5889 1 -14 -24 0 1608.00 442.825 1 -14 -24 0 1829.65 477.092 2 -15 -24 0 193.898 213.572 1 -15 -24 0 19.5975 116.423 2 -16 -24 0 1084.71 387.852 1 0 -25 0 1499.58 371.114 2 1 -25 0 2891.81 460.903 2 -1 -25 0 2857.62 475.809 2 2 -25 0 10307.3 848.907 2 -2 -25 0 11219.6 944.676 2 -3 -25 0 230.879 131.872 2 3 -25 0 252.990 167.993 2 -4 -25 0 6602.20 763.730 2 4 -25 0 6723.81 667.575 2 5 -25 0 120.821 66.0550 2 -5 -25 0-109.380 148.658 2 -6 -25 0 202.419 116.229 2 -7 -25 0 195.576 171.601 2 -8 -25 0-17.2119 119.915 2 -9 -25 0 508.912 249.590 2 -10 -25 0-17.5571 93.9192 2 -11 -25 0 417.158 235.351 2 -11 -25 0 597.579 255.560 1 -12 -25 0-55.5462 145.823 2 -12 -25 0 162.379 144.780 1 -13 -25 0 111.867 127.299 1 -13 -25 0 91.1904 48.4060 2 -14 -25 0 360.538 221.781 1 -14 -25 0 87.7051 91.9023 2 -15 -25 0 77.2301 146.892 1 0 -26 0 3253.58 522.302 2 1 -26 0 103.366 98.2294 2 -1 -26 0 62.0254 46.9062 2 2 -26 0 2296.60 408.620 2 -2 -26 0 2383.42 449.536 2 -3 -26 0 142.661 147.753 2 3 -26 0 211.080 127.532 2 4 -26 0 853.329 233.652 2 -4 -26 0 1035.82 312.458 2 5 -26 0 690.879 225.814 2 -5 -26 0 466.854 223.830 2 -6 -26 0 871.206 291.168 2 -7 -26 0 417.156 184.791 2 -8 -26 0 6273.36 829.247 2 -9 -26 0 471.581 227.016 2 -10 -26 0 11122.4 1142.17 2 -11 -26 0 726.840 323.615 2 -12 -26 0 6733.71 933.162 2 -13 -26 0 94.5473 19.6157 2 -14 -26 0 218.776 149.022 2 0 -27 0 873.696 282.292 2 1 -27 0 551.901 222.896 2 -1 -27 0 495.860 215.462 2 2 -27 0 1838.14 376.998 2 -2 -27 0 1787.64 400.799 2 3 -27 0 625.783 214.324 2 -3 -27 0 376.834 211.992 2 4 -27 0 5920.37 656.689 2 -4 -27 0 6174.79 774.808 2 5 -27 0 1353.11 311.175 2 -5 -27 0 1285.40 372.670 2 -6 -27 0 4058.71 651.171 2 -7 -27 0 2595.96 528.323 2 -8 -27 0 71.5106 86.5556 2 -9 -27 0 822.921 299.392 2 -10 -27 0 5175.63 800.863 2 -11 -27 0 49.6835 87.4979 2 -12 -27 0 2942.99 613.716 2 -13 -27 0-41.0576 80.9932 2 0 -28 0 1322.43 341.811 2 -1 -28 0 135.535 90.7729 2 1 -28 0 68.3369 45.1061 2 -2 -28 0 133.928 88.6137 2 2 -28 0 66.5519 80.4673 2 -3 -28 0 201.059 144.553 2 3 -28 0 131.494 36.8926 2 4 -28 0 217.567 128.632 2 -4 -28 0 329.837 189.684 2 -5 -28 0 2483.54 541.037 2 -6 -28 0 588.143 235.570 2 -7 -28 0 1395.15 431.647 2 -8 -28 0 1545.86 422.540 2 -9 -28 0 52.4587 121.856 2 -10 -28 0 1527.22 450.665 2 -11 -28 0 497.760 263.813 2 -12 -28 0 534.492 276.347 2 0 -29 0 809.606 263.212 2 1 -29 0 151.267 29.1326 2 -1 -29 0 163.278 47.2384 2 2 -29 0 1573.66 352.257 2 -2 -29 0 1485.55 354.523 2 -3 -29 0 42.4707 75.6007 2 3 -29 0 42.1043 43.8280 2 -4 -29 0 1449.45 377.293 2 4 -29 0 1332.29 305.423 2 -5 -29 0 12.5061 66.4428 2 -6 -29 0 1624.17 412.866 2 -7 -29 0 1513.78 442.541 2 -8 -29 0 3149.46 628.484 2 -9 -29 0 2387.81 569.529 2 -10 -29 0 1560.79 482.150 2 -11 -29 0 736.813 333.863 2 -12 -29 0 1393.71 453.292 2 0 -30 0 4548.81 645.503 2 1 -30 0 148.574 100.815 2 -1 -30 0 110.418 59.2625 2 -2 -30 0 413.522 161.187 2 2 -30 0 291.923 148.058 2 -3 -30 0 811.045 282.496 2 3 -30 0 489.394 186.222 2 4 -30 0-6.61215 66.5181 2 -4 -30 0 80.5375 89.1269 2 -5 -30 0 268.466 192.116 2 -6 -30 0 20.7105 59.8939 2 -7 -30 0 160.525 148.691 2 -8 -30 0 4186.62 725.963 2 -9 -30 0 671.407 306.449 2 -10 -30 0 3455.82 695.979 2 -11 -30 0 406.472 262.934 2 0 -31 0-14.1323 84.2422 2 1 -31 0-94.3174 122.069 2 -1 -31 0-102.866 141.486 2 2 -31 0 2257.39 450.215 2 -2 -31 0 2573.47 506.620 2 3 -31 0 45.8717 45.5619 2 -3 -31 0 2.17803 13.7604 2 -4 -31 0 1051.91 344.711 2 -5 -31 0 60.2003 118.076 2 -6 -31 0 1394.75 409.457 2 -7 -31 0 1.75361 95.6650 2 -8 -31 0 490.255 253.639 2 -9 -31 0 127.686 144.796 2 -10 -31 0 496.962 254.628 2 0 -32 0 446.309 185.824 2 1 -32 0-187.882 161.459 2 -1 -32 0-313.171 223.827 2 2 -32 0 543.654 224.334 2 -2 -32 0 589.854 245.221 2 3 -32 0 159.746 92.9599 2 -3 -32 0 154.742 107.412 2 -4 -32 0 5688.03 815.270 2 -5 -32 0 54.9991 132.603 2 -6 -32 0 7252.67 945.450 2 -7 -32 0 24.4879 102.038 2 -8 -32 0 2721.24 612.529 2 -9 -32 0-13.3837 29.4371 2 0 -33 0 176.057 133.495 2 -1 -33 0-104.380 182.519 2 1 -33 0-67.4627 105.388 2 -2 -33 0 68.9493 84.1568 2 2 -33 0 226.929 158.097 2 -3 -33 0-67.0118 112.792 2 -4 -33 0 967.520 371.488 2 -5 -33 0 1366.98 428.036 2 -6 -33 0 1559.16 460.474 2 -7 -33 0 602.313 304.033 2 -8 -33 0 70.9275 149.554 2 0 -34 0 2139.22 482.435 2 1 -34 0 119.167 77.4185 2 -1 -34 0-43.0766 86.7401 2 2 -34 0 4528.75 677.474 2 -2 -34 0 4463.14 734.338 2 -3 -34 0 918.933 359.251 2 -4 -34 0 642.439 293.963 2 -5 -34 0 1530.03 466.187 2 -6 -34 0 2526.09 594.630 2 -7 -34 0 595.639 312.863 2 0 -35 0 182.810 164.170 2 1 -35 0 998.819 329.215 2 -1 -35 0 738.700 285.688 2 2 -35 0 2416.50 505.903 2 -2 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167.538 1 -18 3 -1 56.6655 36.3535 1 -18 -3 -1 177.029 156.377 1 -19 3 -1 191.449 162.386 1 -19 -3 -1 247.754 136.304 1 -19 4 1 199.606 187.443 1 -19 -4 1 149.031 100.892 1 -18 -4 1 33.5317 68.4098 1 -18 4 1 46.3760 78.0358 1 -17 -4 1 167.993 148.048 1 -17 4 1 188.008 136.830 1 -16 -4 1 447.378 213.341 1 -16 4 1 436.992 229.926 1 -15 4 1 4798.60 660.019 1 -15 -4 1 4711.42 669.700 1 -14 -4 1 256.620 165.635 1 -14 4 1 284.065 147.992 1 -13 4 1 1484.76 323.784 1 -13 -4 1 1636.30 367.187 1 -12 4 1 1.32746 27.0873 1 -12 -4 1 20.5225 62.0046 1 -11 4 1 367.192 134.415 1 -11 4 1 492.869 140.327 3 -10 4 1 130.299 101.767 3 -10 4 1 89.7241 83.9291 1 -10 -4 1 196.735 133.105 1 -9 -4 1 9737.33 721.799 1 -9 4 1 10144.2 604.189 3 -9 4 1 9163.27 673.036 1 -8 4 1 1089.96 203.169 3 -8 -4 1 1048.87 245.372 1 -8 4 1 934.539 190.519 1 -7 4 1 4240.64 394.376 1 -7 -4 1 4262.67 416.995 1 -7 4 1 4059.03 349.438 3 -6 -4 1 1020.97 183.204 1 -6 4 1 759.642 155.574 1 -6 4 1 947.148 165.103 3 5 -4 -1 11067.7 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6270.10 505.429 1 6 -14 -2 5953.05 376.045 2 -5 -14 2-50.7219 75.1870 2 5 -14 -2 32.2213 41.0873 2 -5 -14 2 49.6563 49.2165 1 -4 -14 2 19180.1 988.058 2 4 -14 -2 18429.9 725.580 2 -4 -14 2 19258.6 739.407 1 3 -14 -2 7.08886 20.5350 2 -3 -14 2 77.9032 61.4470 1 -3 -14 2-54.2434 92.9084 2 -2 -14 2 27100.1 672.588 1 2 -14 -2 26767.5 945.065 2 -2 -14 2 26481.3 1107.51 2 -1 -14 2 47.4693 29.2545 1 1 -14 -2 65.6416 27.1264 2 -1 -14 2 68.5140 48.2228 2 0 -14 2 25556.6 1036.68 2 1 -14 2 2480.67 337.408 2 2 -14 2 57201.5 1521.92 2 3 -14 2 5432.73 466.865 2 4 -14 2 19981.3 947.693 2 5 -14 2 1367.63 247.696 2 -6 14 -2 461.248 97.3157 1 -6 -14 -2 445.854 158.945 1 6 -14 2 496.542 183.564 2 7 -14 2 163.377 112.512 2 -7 14 -2 123.276 52.9934 1 -7 -14 -2 118.356 47.5555 1 8 -14 2 5315.11 537.345 2 -8 -14 -2 5473.61 601.544 1 -9 -14 -2-35.4178 69.6271 1 -10 -14 -2 1161.52 302.139 1 10 -14 2-88.5219 327.586 2 -11 -14 -2-50.1456 35.1194 1 -12 -14 -2 313.438 166.247 1 -13 -14 -2 1210.96 384.971 1 -14 -14 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292.917 2 -4 3 -3 79.3993 38.3200 1 5 -3 3 27631.2 1087.78 2 -5 3 -3 28505.7 964.962 1 -6 3 -3 13366.6 733.491 1 -6 -3 -3 13475.9 803.611 1 6 -3 3 13870.0 821.392 2 7 -3 3 58825.8 1728.50 2 -7 -3 -3 58822.8 1708.63 1 -7 3 -3 58274.1 1597.73 1 -8 -3 -3 8784.74 715.919 1 -8 3 -3 8688.31 664.527 1 8 -3 3 8650.95 707.531 2 -9 3 -3 7989.66 673.959 1 -9 -3 -3 9060.17 730.632 1 -10 3 -3 4103.12 509.012 1 -10 -3 -3 4293.04 549.267 1 -11 3 -3 2430.54 387.411 1 -11 -3 -3 2318.16 419.384 1 -12 3 -3 179.899 140.144 1 -12 -3 -3 166.070 117.100 1 -13 -3 -3 1262.08 348.145 1 -13 3 -3 1143.56 304.536 1 -14 3 -3 87.1005 117.830 1 -14 -3 -3 410.007 221.936 1 -15 -3 -3 958.574 313.101 1 -15 3 -3 971.097 293.455 1 -16 -3 -3 116.376 167.536 1 -16 3 -3 99.6001 99.0438 1 -17 3 -3 26.6859 21.8830 1 -17 -3 -3 9.69635 73.4714 1 -18 -3 -3 73.6956 97.0739 1 -18 3 -3 127.343 114.840 1 -20 4 3 107.547 139.742 1 -19 -4 3-50.4275 139.109 1 -19 4 3-24.1315 45.1990 1 -18 4 3 391.220 207.364 1 -18 -4 3 312.924 193.012 1 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1009.03 152.117 2 -3 4 3 82401.5 1522.01 3 -3 -4 3 80900.3 1296.36 2 -2 4 3 46.8294 28.3892 3 -2 -4 3 45.5913 29.7603 2 -1 4 3 104639. 1487.94 3 -1 -4 3 103626. 1498.29 2 0 4 3 20.7511 11.9237 3 0 -4 3 425.720 134.289 2 1 -4 3 40339.6 1039.57 2 1 4 3 39663.7 799.078 3 2 -4 3 5217.68 394.671 2 3 -4 3 142369. 2175.28 2 -4 4 -3 5614.15 402.069 1 4 -4 3 5403.42 450.669 2 5 -4 3 36172.9 1243.51 2 -5 4 -3 36162.2 1072.76 1 6 -4 3 2607.87 367.945 2 -6 4 -3 2760.33 326.599 1 -6 -4 -3 2542.89 347.074 1 -7 4 -3 2414.82 318.702 1 -7 -4 -3 2137.96 329.082 1 7 -4 3 2239.79 333.017 2 -8 4 -3 2090.22 342.803 1 -8 -4 -3 1537.32 318.887 1 8 -4 3 1501.98 302.310 2 -9 4 -3 7759.73 634.652 1 9 -4 3 8295.24 681.838 2 -9 -4 -3 7953.21 704.339 1 -10 4 -3 3774.57 478.520 1 -10 -4 -3 4124.19 553.729 1 -11 -4 -3 14574.8 1028.50 1 -11 4 -3 14969.8 989.674 1 -12 -4 -3 1214.33 301.594 1 -12 4 -3 1325.68 311.714 1 -13 -4 -3 273.507 158.266 1 -13 4 -3 308.705 155.613 1 -14 -4 -3 1536.26 395.515 1 -14 4 -3 1461.49 357.874 1 -15 -4 -3 545.463 251.943 1 -15 4 -3 479.181 220.258 1 -16 -4 -3 272.610 172.373 1 -16 4 -3 238.771 139.623 1 -17 -4 -3 57.1538 16.4034 1 -17 4 -3-32.7932 132.121 1 -18 4 -3 307.174 164.676 1 -18 -4 -3 265.134 210.989 1 -20 5 3-17.6726 79.4005 1 -19 -5 3 2.62920 94.5919 1 -19 5 3-89.2367 110.538 1 -18 5 3-106.622 120.781 1 -18 -5 3-94.4453 121.091 1 -17 5 3 689.151 268.337 1 -17 -5 3 577.875 212.335 1 -16 5 3-112.909 132.289 1 -16 -5 3-156.215 199.329 1 -15 -5 3 2966.44 520.675 1 -15 5 3 2905.45 512.566 1 -14 5 3 10.7263 40.9494 1 -14 -5 3-198.256 183.529 1 -13 5 3 3736.24 529.862 1 -13 5 3 3601.38 459.356 3 -13 -5 3 3326.56 492.706 1 -12 5 3 81.5923 101.420 1 -12 5 3-48.7609 78.2034 3 -12 -5 3 45.6481 54.4550 1 -11 5 3 8333.93 716.322 1 -11 -5 3 8580.62 742.761 1 -11 5 3 8167.80 656.870 3 -10 5 3 8.09744 39.6529 3 -10 5 3-72.2733 94.7206 1 -10 -5 3-94.5955 89.0585 1 -9 5 3 2186.61 315.927 3 -9 5 3 2028.89 326.816 1 -9 -5 3 2155.42 319.968 1 -8 -5 3 8.82612 31.3270 2 -8 5 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940.478 259.867 1 -12 6 3 1517.41 326.541 1 -12 -6 3 1639.17 348.765 1 -12 6 3 1303.31 283.292 3 -11 6 3 22.3579 39.0305 1 -11 6 3 6.50949 36.9856 3 -11 -6 3-89.4316 152.651 1 -10 6 3-75.7978 92.8490 1 -10 6 3-7.16498 60.4212 3 -10 -6 3-74.1881 98.9368 1 -9 6 3 295.934 127.213 3 -9 6 3 181.000 82.7842 1 -9 -6 3 106.952 32.2930 1 -8 6 3 172.219 87.9100 3 -8 -6 3 22.6941 94.4828 1 -8 -6 3 149.272 76.4137 2 -7 -6 3 5.14858 28.8558 2 -7 6 3 50.7689 12.9354 3 -7 -6 3-49.0151 65.8429 1 -6 6 3 702.205 166.578 3 -6 -6 3 518.349 147.946 1 -6 -6 3 619.038 147.361 2 -5 -6 3 79822.2 1568.48 1 -5 6 3 81687.9 1705.10 3 -5 -6 3 80154.6 1541.54 2 -4 -6 3 156.295 77.4927 2 -4 6 3 146.535 80.9660 3 -4 -6 3 97.6345 53.5987 1 -3 -6 3 33419.0 816.262 1 -3 6 3 33598.1 1009.02 3 -3 -6 3 32518.1 934.086 2 -2 6 3-6.91531 28.9555 3 -2 -6 3 53.0693 48.6210 2 -1 -6 3 56037.3 1180.28 2 -1 6 3 53633.1 1168.99 3 0 -6 3 1607.80 140.716 2 0 6 3 1902.62 219.861 3 1 -6 3 129875. 1985.23 2 1 6 3 122083. 1598.96 3 2 -6 3 2558.70 294.166 2 3 -6 3 43065.3 1212.82 2 -3 6 -3 46129.6 942.155 1 -4 6 -3 4285.34 334.373 1 4 -6 3 4434.70 426.474 2 -5 6 -3 97970.1 1700.31 1 5 -6 3 100688. 2092.78 2 6 -6 3 520.135 92.3048 2 -6 -6 -3 718.242 104.190 1 -7 -6 -3 29789.2 1276.64 1 -7 6 -3 31641.1 1120.04 1 7 -6 3 31833.7 1285.59 2 8 -6 3 117.132 64.2973 2 -8 -6 -3 33.3538 57.1257 1 -8 6 -3 41.6200 41.4364 1 -9 6 -3 3604.48 417.829 1 -9 -6 -3 3453.47 468.875 1 9 -6 3 3407.28 459.172 2 -10 -6 -3-36.5840 37.4002 1 -10 6 -3-58.8011 105.236 1 10 -6 3-7.44675 55.3352 2 -11 -6 -3 391.293 165.426 1 -11 6 -3 396.847 140.052 1 -12 -6 -3 71.2208 7.51441 1 -12 6 -3-6.48335 44.8738 1 -13 6 -3-21.0277 81.1307 1 -13 -6 -3-24.4770 65.6303 1 -14 -6 -3 179.340 137.477 1 -14 6 -3 13.9533 32.1765 1 -15 6 -3 259.310 134.691 1 -15 -6 -3 316.009 204.721 1 -16 6 -3-55.5878 85.3945 1 -16 -6 -3 90.3697 120.980 1 -17 -6 -3 4.67355 46.8277 1 -17 6 -3-27.1332 84.6556 1 -18 6 -3 13.6562 60.1969 1 -19 6 -3 7.40541 103.625 1 -20 7 3-39.9127 35.9580 1 -19 -7 3 266.610 218.493 1 -19 7 3 107.087 106.544 1 -18 7 3 9.51067 41.9899 1 -18 -7 3 48.3929 52.1583 1 -17 7 3 85.7176 90.6259 1 -17 -7 3-88.7145 152.648 1 -16 7 3 58.7586 58.8043 1 -16 -7 3-73.9378 174.649 1 -15 7 3 1009.94 300.360 1 -15 -7 3 721.085 223.607 1 -14 7 3 268.040 140.286 1 -14 -7 3 105.263 78.2952 1 -13 7 3-11.8708 58.9440 3 -13 7 3 30.6962 83.6949 1 -13 -7 3-128.179 149.661 1 -12 7 3 670.191 191.433 3 -12 -7 3 554.220 209.088 1 -12 7 3 639.046 216.098 1 -11 7 3 96.2591 59.7661 1 -11 -7 3 217.292 96.6881 1 -11 7 3 124.456 41.3435 3 -10 -7 3 25.8019 84.8598 1 -10 7 3 132.704 51.4011 1 -10 7 3 263.233 118.590 3 -9 -7 3 1795.04 299.911 1 -9 7 3 1791.89 302.135 3 -8 -7 3 784.527 182.020 2 -8 7 3 946.558 217.729 3 -8 -7 3 751.584 179.841 1 -7 -7 3 21007.2 894.357 2 -7 -7 3 22571.0 977.095 1 -7 7 3 23085.5 996.898 3 -6 -7 3 1515.11 238.243 2 -6 -7 3 1259.02 219.072 1 -6 7 3 1366.96 244.370 3 -5 7 3 32357.6 1096.34 3 -5 -7 3 32454.9 995.161 1 -5 -7 3 32291.0 1028.72 2 -4 -7 3 911.773 156.708 1 -4 7 3 898.056 181.457 3 4 -7 -3 885.033 85.9259 2 -4 -7 3 1003.21 185.421 2 -3 -7 3 11233.9 469.771 1 -3 7 3 11274.9 599.683 3 -3 -7 3 11430.6 570.111 2 -2 7 3 1531.71 215.860 3 -2 -7 3 1775.87 227.968 2 -1 7 3 87640.5 1552.98 3 -1 -7 3 85205.7 1535.61 2 0 -7 3 1673.76 228.309 2 0 7 3 1541.01 204.037 3 1 -7 3 98933.6 1783.11 2 2 -7 3 2541.71 304.607 2 3 -7 3 2454.46 314.112 2 -3 7 -3 2158.35 198.616 1 4 -7 3 33.2308 59.0273 2 -4 7 -3 20.4818 21.7160 1 -5 7 -3 20970.8 762.724 1 5 -7 3 22887.8 1003.81 2 -6 -7 -3 227.285 110.984 1 6 -7 3-60.7525 167.937 2 -7 7 -3 9544.04 610.920 1 7 -7 3 9479.90 695.296 2 -7 -7 -3 9139.90 697.856 1 -8 7 -3-35.6482 73.6152 1 -8 -7 -3 55.4655 40.4303 1 8 -7 3 57.9156 47.3427 2 -9 7 -3 745.838 187.346 1 -9 -7 -3 727.652 210.558 1 9 -7 3 853.644 223.724 2 -10 7 -3 55.6882 64.6263 1 -10 -7 -3 65.7081 58.1137 1 10 -7 3 32.2666 40.7605 2 -11 7 -3-62.0304 74.9484 1 -11 -7 -3-11.9769 61.0023 1 -12 -7 -3 314.244 121.914 1 -12 7 -3 272.027 127.126 1 -13 -7 -3 9.51848 83.0319 1 -13 7 -3 35.9116 20.8142 1 -14 7 -3 115.676 65.2022 1 -14 -7 -3 311.984 173.616 1 -15 7 -3 267.646 92.1513 1 -15 -7 -3 305.595 167.556 1 -16 7 -3 718.578 278.049 1 -16 -7 -3 754.157 297.699 1 -17 -7 -3 511.116 227.803 1 -17 7 -3 601.691 244.494 1 -18 7 -3 172.846 136.012 1 -20 8 3-178.581 177.847 1 -19 8 3 552.848 263.750 1 -19 -8 3 364.681 189.145 1 -18 8 3 200.293 155.758 1 -18 -8 3 71.9172 55.4147 1 -17 -8 3 411.382 186.781 1 -17 8 3 909.032 307.419 1 -16 8 3 79.1338 25.1552 1 -16 -8 3-131.964 170.117 1 -15 8 3 1495.08 368.815 1 -15 -8 3 1325.02 336.640 1 -14 8 3-51.8402 117.534 1 -14 -8 3-25.6610 27.9734 1 -13 8 3 9.02197 59.9661 1 -13 8 3 19.9780 26.4252 3 -13 -8 3-39.7409 112.012 1 -12 8 3 220.983 108.500 3 -12 8 3 135.729 76.0699 1 -12 -8 3 175.523 102.225 1 -11 8 3 1155.72 252.846 1 -11 8 3 1388.51 265.590 3 -11 -8 3 1349.82 282.357 1 -10 -8 3 258.691 112.850 1 -10 8 3 285.160 104.568 3 -9 -8 3 14791.9 890.104 1 -9 8 3 14577.8 850.589 3 -9 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3 701.173 187.308 2 -7 -8 -3 1429.15 245.726 1 -7 8 -3 1666.16 248.079 1 -8 -8 -3-286.695 171.431 1 -8 8 -3 5.87173 38.0323 1 -9 -8 -3 9.45892 67.9418 1 -9 8 -3-12.4487 13.9680 1 9 -8 3-30.5170 80.8611 2 -10 -8 -3 1447.13 333.740 1 10 -8 3 1713.92 346.802 2 -10 8 -3 1470.98 287.664 1 -11 8 -3 96.0369 39.3783 1 -11 -8 -3 188.922 84.4254 1 11 -8 3 166.855 120.781 2 -12 -8 -3 578.661 196.424 1 -12 8 -3 599.606 195.657 1 -13 -8 -3 213.305 130.129 1 -13 8 -3 102.591 75.7892 1 -14 8 -3 6.98366 76.9143 1 -14 -8 -3 130.444 129.886 1 -15 8 -3 188.916 106.258 1 -15 -8 -3 381.717 204.393 1 -16 -8 -3 40.9080 109.824 1 -16 8 -3 45.6095 60.9790 1 -17 -8 -3 1203.98 372.914 1 -17 8 -3 915.393 312.834 1 -19 9 3 100.713 102.284 1 -19 -9 3 218.458 124.191 1 -18 9 3 44.9711 67.6518 1 -18 -9 3-13.1428 123.218 1 -17 -9 3-85.3499 164.316 1 -17 9 3 114.860 62.3539 1 -16 9 3-60.6889 114.947 1 -16 -9 3-26.1451 104.451 1 -15 9 3 2793.75 500.971 1 -15 -9 3 2922.71 535.061 1 -14 9 3-102.912 101.319 1 -14 -9 3-74.9949 108.557 1 -13 9 3 1881.95 346.213 3 -13 -9 3 1790.89 373.303 1 -13 9 3 1860.96 375.041 1 -12 -9 3 18.8183 72.9531 1 -12 9 3 15.3211 21.1862 3 -11 -9 3 36.5491 8.26558 1 -11 9 3 3.11707 41.0330 3 -10 -9 3-139.954 129.955 1 -10 -9 3-78.6307 79.1630 2 -10 9 3 99.4112 62.2634 3 -9 -9 3 9187.29 681.892 2 -9 9 3 9790.70 706.069 3 -9 -9 3 9897.05 745.078 1 -8 -9 3 148.350 74.8340 2 -8 9 3 98.3282 49.8453 3 -8 -9 3 66.8195 53.5848 1 -7 -9 3 1006.24 208.260 2 -7 -9 3 980.896 197.263 1 -7 9 3 971.038 200.692 3 6 -9 -3 4633.08 206.243 2 -6 -9 3 5366.10 484.348 2 -6 -9 3 4647.52 433.555 1 -6 9 3 5132.79 480.324 3 -5 -9 3 1163.24 195.791 1 5 -9 -3 1078.91 104.873 2 -5 9 3 1263.74 229.086 3 -5 -9 3 1274.10 225.038 2 -4 -9 3 4074.41 331.611 1 -4 9 3 4340.34 416.682 3 -4 -9 3 4453.40 413.677 2 4 -9 -3 4669.81 250.920 2 -3 9 3 1850.25 251.758 3 -3 -9 3 1607.77 176.124 1 -3 -9 3 1642.51 234.456 2 -2 -9 3 2658.03 198.001 1 -2 -9 3 3037.33 321.449 2 -2 9 3 2748.20 319.419 3 -1 -9 3 49379.2 1271.16 2 -1 9 3 50771.5 1263.10 3 0 -9 3 3303.70 337.053 2 -2 9 -3 371.061 64.9109 1 2 -9 3 164.495 153.809 2 3 -9 3 297.223 109.457 2 -3 9 -3 758.210 117.300 1 -4 9 -3 35.4166 38.6394 1 4 -9 3 132.103 103.808 2 5 -9 3 911.151 257.063 2 -5 9 -3 742.325 145.466 1 6 -9 3 366.938 113.625 2 -6 9 -3 415.869 136.825 1 -6 -9 -3 334.591 114.044 1 -7 -9 -3-36.8120 77.0612 1 -7 9 -3 3.44567 13.4172 1 -8 -9 -3 43.9075 80.7139 1 -8 9 -3 162.393 54.9339 1 9 -9 3 4793.60 601.996 2 -9 -9 -3 4171.82 555.042 1 -9 9 -3 3885.86 448.087 1 -10 -9 -3 244.415 42.5737 1 -10 9 -3 396.468 132.842 1 10 -9 3 314.319 143.317 2 -11 9 -3 86.6269 15.1001 1 -11 -9 -3 157.230 116.445 1 11 -9 3 126.308 99.4243 2 -12 -9 -3 520.730 232.579 1 -12 9 -3 291.015 112.220 1 -13 -9 -3 1354.75 357.658 1 -13 9 -3 1380.82 309.070 1 -14 9 -3-15.1758 94.0059 1 -14 -9 -3 93.1371 116.970 1 -15 9 -3 259.166 121.755 1 -15 -9 -3 392.568 214.271 1 -16 -9 -3 205.206 170.980 1 -17 -9 -3 113.510 160.534 1 -19 -10 3 491.141 245.721 1 -18 -10 3 492.212 238.130 1 -17 -10 3-170.908 185.958 1 -16 -10 3 1083.25 345.456 1 -15 -10 3 235.437 130.517 1 -14 -10 3 2004.72 446.440 1 -13 10 3 4099.00 512.953 3 -13 -10 3 4199.57 584.642 1 -12 -10 3 921.528 258.991 1 -12 10 3 948.647 256.999 3 -11 -10 3 947.324 215.352 1 -11 10 3 866.180 220.490 3 -11 -10 3 757.438 196.641 2 -10 -10 3 477.392 154.004 2 -10 -10 3 567.446 162.340 1 -10 10 3 601.213 186.889 3 -9 -10 3 6434.29 582.707 2 -9 -10 3 6763.83 601.479 1 -9 10 3 6342.31 581.579 3 -8 -10 3 635.919 163.604 1 -8 -10 3 761.836 194.587 2 -8 10 3 661.734 179.989 3 8 -10 -3 409.186 65.5119 2 -7 -10 3 7608.25 588.985 2 -7 10 3 8130.59 615.589 3 7 -10 -3 6418.95 257.672 2 -7 -10 3 7564.51 568.969 1 -6 -10 3 359.248 139.265 2 6 -10 -3 54.4933 48.3342 2 -6 10 3 301.451 118.249 3 -6 -10 3 358.473 121.919 1 5 -10 -3 136936. 1322.80 2 -5 10 3 136525. 2406.72 3 -5 -10 3 131105. 2344.39 2 -5 -10 3 135685. 2079.75 1 4 -10 -3 1799.77 170.643 2 -4 -10 3 1479.99 197.960 1 -4 -10 3 1624.78 261.630 2 -4 10 3 1546.39 261.716 3 -3 -10 3 109236. 1465.75 1 -3 -10 3 102545. 1958.82 2 -3 10 3 102686. 1964.79 3 -2 -10 3 6420.79 306.621 1 -2 -10 3 7600.57 532.520 2 -2 10 3 6706.20 504.845 3 -1 -10 3 19453.0 823.144 2 -1 10 3 19210.4 822.606 3 0 -10 3 3974.90 383.832 2 1 -10 3 23645.1 922.789 2 -2 10 -3 2142.98 133.804 1 2 -10 3 1611.89 106.781 2 -3 10 -3 59131.7 884.597 1 3 -10 3 55906.9 1539.84 2 4 -10 3 3637.27 411.910 2 -4 10 -3 3025.98 243.598 1 5 -10 3 60635.1 1650.46 2 -5 10 -3 61332.1 1222.30 1 -6 -10 -3 3490.70 457.396 1 -6 10 -3 3247.82 337.242 1 7 -10 3 1191.05 186.141 2 -7 10 -3 2067.29 276.718 1 -7 -10 -3 1906.73 316.765 1 -8 10 -3 58.5309 45.1768 1 -8 -10 -3 18.6184 45.7469 1 -9 10 -3 90.6071 21.0317 1 -9 -10 -3 162.618 100.148 1 -10 -10 -3-80.7622 117.452 1 -10 10 -3-103.850 87.7257 1 10 -10 3-35.7449 65.5290 2 -11 -10 -3 921.870 256.457 1 -11 10 -3 824.255 220.705 1 11 -10 3 982.034 270.989 2 -12 10 -3-102.476 102.824 1 -12 -10 -3 35.3750 102.339 1 -13 -10 -3 323.962 199.371 1 -13 10 -3 256.852 115.526 1 -14 -10 -3 242.389 155.641 1 -14 10 -3 6.16559 59.1130 1 -15 -10 -3 598.883 276.869 1 -16 -10 -3 354.414 198.911 1 -17 -10 -3 252.943 231.251 1 -19 -11 3 62.3624 101.480 1 -18 -11 3-0.76759 78.8041 1 -17 -11 3 182.019 109.809 1 -16 -11 3-62.0116 166.847 1 -15 -11 3 2049.12 428.281 1 -14 -11 3 468.070 228.375 1 -14 -11 3 532.587 225.889 2 -13 -11 3 8287.91 760.022 2 -13 11 3 9066.46 769.413 3 -13 -11 3 8828.08 867.716 1 -12 -11 3 39.7879 64.4548 1 -12 -11 3-34.3480 96.4661 2 -12 11 3 41.3578 13.4215 3 -11 -11 3 3.88759 84.3758 2 -11 11 3 4.74819 53.6422 3 -11 -11 3 5.50383 85.3942 1 -10 -11 3 48.6966 73.8959 1 -10 -11 3 100.837 69.1215 2 -10 11 3 75.5007 52.3282 3 -9 11 3 408.620 143.224 3 -9 -11 3 508.032 157.188 1 -9 -11 3 408.774 152.276 2 -8 -11 3-60.0644 95.6468 1 -8 11 3 38.7367 31.3042 3 -8 -11 3 13.9415 45.8121 2 -7 11 3 29718.2 1216.47 3 -7 -11 3 28798.0 1134.90 1 7 -11 -3 27537.2 579.554 2 -7 -11 3 28348.7 1189.61 2 6 -11 -3 1513.44 127.540 2 -6 11 3 1760.79 304.013 3 -6 -11 3 1636.54 251.276 1 -6 -11 3 1908.07 306.685 2 -5 -11 3 116365. 1957.01 1 -5 11 3 114578. 2268.48 3 -5 -11 3 114260. 2267.89 2 -4 -11 3 747.712 141.115 1 -4 -11 3 815.407 193.535 2 -4 11 3 809.837 194.874 3 4 -11 -3 835.729 127.957 2 3 -11 -3 144001. 1787.51 2 -3 -11 3 147825. 1732.04 1 -3 -11 3 145445. 2429.42 2 -3 11 3 149972. 2440.93 3 -2 -11 3 1644.40 153.011 1 -2 -11 3 1836.15 276.821 2 -2 11 3 1958.03 286.799 3 -1 -11 3 68511.8 1604.80 2 0 -11 3 23.9024 42.0564 2 1 -11 3 1646.02 242.989 2 3 -11 3-74.5326 196.293 2 -3 11 -3 355.933 69.2693 1 4 -11 3-26.4062 68.9698 2 -4 11 -3 38.8332 33.0227 1 5 -11 3 14678.8 838.391 2 -5 11 -3 12544.0 560.810 1 6 -11 3 1703.99 351.500 2 -6 11 -3 745.664 155.474 1 7 -11 3 5868.73 554.894 2 -7 11 -3 6173.07 468.383 1 -7 -11 -3 5523.93 578.492 1 -8 -11 -3 2730.47 430.816 1 -8 11 -3 2505.40 333.679 1 8 -11 3 1894.54 301.380 2 -9 -11 -3 6591.86 683.290 1 -9 11 -3 6631.73 554.029 1 9 -11 3 5087.13 500.571 2 10 -11 3-84.6865 102.078 2 -10 11 -3-40.5926 91.6580 1 -10 -11 -3-10.2626 131.104 1 -11 11 -3 2178.85 352.123 1 -11 -11 -3 1976.26 418.245 1 11 -11 3 2210.39 393.729 2 -12 -11 -3 954.641 294.618 1 -12 11 -3 1127.44 277.161 1 -13 -11 -3 3948.39 610.427 1 -14 -11 -3 1942.83 473.604 1 -15 -11 -3 1478.85 407.004 1 -16 -11 -3 1363.74 435.304 1 -17 -11 -3 123.832 142.217 1 -19 -12 3 1229.37 418.881 1 -18 -12 3 899.882 345.894 1 -17 -12 3 2101.99 502.979 1 -16 -12 3 825.225 297.544 1 -15 -12 3 2940.21 484.256 2 -15 -12 3 3133.02 550.745 1 -14 -12 3 1069.14 283.959 2 -14 -12 3 1200.88 331.098 1 -13 12 3 10449.6 840.233 3 -13 -12 3 9739.18 843.544 2 -13 -12 3 10515.6 937.893 1 -12 -12 3 355.048 141.211 2 -12 -12 3 459.100 177.493 1 -12 12 3 472.814 177.529 3 -11 -12 3 1829.64 330.640 2 -11 12 3 1858.57 337.072 3 -11 -12 3 2142.21 370.246 1 -10 -12 3 543.462 182.660 1 -10 12 3 500.519 176.865 3 -10 -12 3 531.529 170.328 2 -9 -12 3 103.279 74.2031 2 -9 -12 3 155.625 72.6709 1 -9 12 3 104.958 64.5100 3 -8 -12 3 286.031 124.350 1 -8 -12 3 278.038 120.179 2 -8 12 3 215.994 125.038 3 -7 12 3 399.080 131.633 3 -7 -12 3 415.510 156.408 2 -7 -12 3 405.670 128.795 1 7 -12 -3 425.288 90.9730 2 6 -12 -3 2039.54 183.804 2 -6 -12 3 1940.22 284.006 1 -6 12 3 1975.48 332.082 3 -6 -12 3 2217.66 348.815 2 -5 12 3 736.665 188.801 3 -5 -12 3 693.189 149.686 1 5 -12 -3 767.610 122.421 2 -5 -12 3 834.450 201.886 2 -4 12 3 5422.78 504.215 3 4 -12 -3 5510.55 353.793 2 -4 -12 3 5389.39 385.726 1 -4 -12 3 5674.77 517.328 2 -3 -12 3 76522.9 1836.36 2 -3 12 3 81676.6 1858.51 3 -3 -12 3 81931.7 1291.03 1 3 -12 -3 79887.9 1413.26 2 -2 -12 3 160.990 104.108 2 -2 -12 3 53.6726 29.7812 1 -1 -12 3 68100.7 1660.63 2 0 -12 3 5942.97 504.642 2 1 -12 3 31771.6 1117.05 2 2 -12 3 3839.71 332.018 2 -3 12 -3 40895.8 657.734 1 3 -12 3 40875.2 1363.02 2 4 -12 3 9646.76 707.031 2 -4 12 -3 8625.20 392.100 1 -5 12 -3 62387.2 1220.21 1 5 -12 3 67247.4 1800.64 2 6 -12 3 11853.6 804.835 2 -6 12 -3 9546.39 545.503 1 7 -12 3 16562.5 955.501 2 -7 -12 -3 16869.3 1023.70 1 -7 12 -3 17480.4 780.081 1 -8 12 -3 5217.96 480.587 1 -8 -12 -3 5545.45 628.026 1 8 -12 3 5083.35 549.155 2 -9 -12 -3 1980.88 393.899 1 -9 12 -3 1778.45 301.686 1 -10 12 -3 110.058 59.5227 1 -10 -12 -3 151.787 71.5975 1 -11 -12 -3 243.129 157.021 1 11 -12 3 160.298 97.8954 2 -12 -12 -3 118.930 128.334 1 -13 -12 -3 66.8785 63.4756 1 -14 -12 -3 82.6178 111.693 1 -15 -12 -3 395.961 211.972 1 -16 -12 -3 177.816 191.261 1 -17 -12 -3 299.682 240.568 1 -18 -13 3-61.3536 76.0269 1 -17 -13 3 84.9262 99.2850 1 -16 -13 3 19.4419 52.6609 1 -15 -13 3-93.6365 167.053 2 -15 -13 3-89.7000 127.810 1 -14 -13 3-22.8411 83.9384 1 -14 -13 3 30.6363 54.0576 2 -13 13 3 597.493 211.056 3 -13 -13 3 560.801 207.912 2 -13 -13 3 674.478 251.981 1 -12 -13 3-67.9898 93.6205 1 -12 -13 3 10.8492 35.4749 2 -12 13 3-39.0263 44.1808 3 -11 -13 3-67.6282 107.647 2 -11 13 3-9.73863 19.8740 3 -11 -13 3-70.5808 91.2932 1 -10 -13 3 532.924 179.780 1 -10 13 3 642.160 203.951 3 -10 -13 3 701.311 207.496 2 -9 13 3 178.850 101.592 3 -9 -13 3 85.4858 40.3938 1 -9 -13 3 143.924 69.5257 2 -8 -13 3 259.004 107.038 1 -8 -13 3 256.213 124.456 2 -8 13 3 217.367 101.968 3 7 -13 -3 8565.06 400.528 2 -7 13 3 8332.95 665.130 3 -7 -13 3 8522.40 616.145 1 -7 -13 3 8293.45 678.086 2 6 -13 -3 1075.28 144.139 2 -6 13 3 985.903 237.614 3 -6 -13 3 934.613 197.723 1 -6 -13 3 1207.39 262.372 2 5 -13 -3 8609.00 434.663 2 -5 13 3 8584.21 639.612 3 -5 -13 3 8026.50 643.764 2 -5 -13 3 8242.78 522.726 1 4 -13 -3 118.622 55.3212 2 -4 13 3 134.210 93.5524 3 -4 -13 3 155.303 82.8705 2 -4 -13 3 96.9323 36.3959 1 -3 -13 3 263.648 118.896 2 3 -13 -3 273.053 92.2994 2 -3 13 3 429.631 143.314 3 -3 -13 3 355.698 85.2124 1 -2 -13 3 6759.53 572.857 2 -2 -13 3 6111.77 299.322 1 -1 -13 3 43764.6 1370.16 2 0 -13 3 7917.56 602.870 2 1 -13 3 93332.8 1986.62 2 2 -13 3 3717.29 355.758 2 3 -13 3 4658.83 455.438 2 4 -13 3 1937.87 297.294 2 -4 13 -3 1998.58 179.304 1 5 -13 3 1940.33 390.945 2 -5 13 -3 936.130 140.992 1 6 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4 119306. 1384.15 2 -3 0 4 122.720 50.5414 2 -2 0 4 64894.0 1132.25 2 -1 0 4 3161.17 310.653 2 0 0 4 40405.4 1051.90 2 1 0 4 3770.90 320.620 2 2 0 4 6794.71 462.112 2 3 0 4 5154.44 208.655 3 3 0 4 6080.25 521.106 2 4 0 4 21531.8 1002.08 2 5 0 4 3702.08 440.241 2 -6 0 -4 12057.6 747.281 1 6 0 4 12558.3 811.213 2 -7 0 -4 2979.15 404.146 1 -8 0 -4 15545.7 930.831 1 -9 0 -4 16055.0 1006.37 1 -10 0 -4 4569.76 552.354 1 -11 0 -4 3931.93 544.766 1 -12 0 -4 848.708 262.102 1 -13 0 -4 5446.41 705.915 1 -14 0 -4 5654.91 733.285 1 -15 0 -4 3057.69 581.661 1 -16 0 -4 560.892 265.620 1 -17 0 -4 887.969 328.360 1 -18 0 -4 197.764 148.133 1 -20 1 4 81.4040 78.3189 1 -20 -1 4 179.951 144.127 1 -19 1 4-142.779 163.247 1 -19 -1 4-3.86792 83.6888 1 -18 -1 4 35.9564 13.4208 1 -18 1 4-51.0400 135.599 1 -17 1 4 456.269 205.773 1 -17 -1 4 677.069 295.101 1 -16 1 4 310.695 171.844 1 -16 -1 4 326.713 157.621 1 -15 -1 4-18.4105 146.430 1 -15 1 4 26.2313 85.7141 1 -14 -1 4 794.017 257.483 1 -14 -1 4 1156.79 293.056 3 -14 1 4 726.973 268.141 1 -14 1 4 734.505 205.091 3 -13 1 4 132.000 115.777 1 -13 -1 4 201.995 142.269 1 -13 1 4 243.190 157.317 3 -12 1 4 2903.36 468.720 1 -12 -1 4 2886.08 461.543 1 -12 1 4 3050.78 450.678 3 -11 1 4 91.7546 106.561 1 -11 -1 4 140.363 121.110 1 -11 1 4 276.157 173.908 3 -10 1 4 2116.45 214.646 2 -10 -1 4 2489.26 277.620 2 -10 -1 4 2299.82 391.712 1 -10 1 4 1879.58 349.355 1 -9 1 4 19.9922 25.2022 2 -9 1 4-23.4320 37.8976 1 -9 -1 4 15.5330 17.8011 2 -9 -1 4 57.3065 94.2224 1 -8 1 4 9825.13 685.974 1 -8 -1 4 10269.0 699.434 1 -8 1 4 9769.26 388.983 2 -8 -1 4 9804.32 467.309 2 -7 -1 4 634.047 164.390 1 -7 1 4 543.887 87.1243 2 -7 -1 4 531.202 113.083 2 -6 -1 4 26151.4 688.204 2 -6 1 4 24709.9 540.315 2 -5 -1 4 150.776 48.8231 2 -4 1 4 107081. 1215.97 2 -4 -1 4 104990. 1358.08 2 -3 1 4 547.430 97.9120 2 -3 -1 4 189.954 86.7449 2 -2 1 4 76153.0 1212.94 2 -2 -1 4 73949.2 1267.37 2 -1 -1 4 8538.31 495.508 2 -1 1 4 3920.42 309.851 2 0 -1 4 7546.83 441.785 2 0 1 4 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847.149 328.735 1 -18 1 -4 622.632 286.957 1 -18 -1 -4 242.923 151.475 1 -20 -2 4-83.0864 128.184 1 -20 2 4-68.4703 68.9338 1 -19 -2 4 208.497 134.456 1 -19 2 4 171.513 103.036 1 -18 -2 4 275.220 168.191 1 -18 2 4 246.619 167.165 1 -17 2 4 2.85897 80.7001 1 -17 -2 4 211.872 170.236 1 -16 -2 4-71.2125 121.039 1 -16 2 4 131.084 124.469 1 -15 -2 4 264.123 167.768 1 -15 2 4 260.565 155.253 1 -14 2 4 318.068 131.493 3 -14 2 4 325.991 137.126 1 -14 -2 4 231.976 127.175 1 -13 -2 4 2170.39 435.787 1 -13 2 4 2335.33 430.720 1 -13 2 4 2240.59 395.340 3 -12 2 4 18946.5 1156.97 1 -12 -2 4 19243.0 1200.23 1 -12 2 4 18650.3 1084.84 3 -11 -2 4 1056.77 199.079 2 -11 2 4 1324.10 290.298 3 -11 2 4 1221.56 281.537 1 -11 -2 4 1242.24 293.239 1 -10 -2 4 32813.0 1000.95 2 -10 2 4 32374.7 1378.78 1 -10 -2 4 32503.9 1403.65 1 -10 2 4 32031.5 1340.34 3 -9 2 4 75.8375 35.9414 2 -9 -2 4 63.1185 31.5991 2 -9 2 4 64.8563 48.8839 1 -9 2 4 214.539 157.035 3 -9 -2 4-5.34827 6.77961 1 -8 2 4 6301.48 545.582 1 -8 -2 4 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3 4 37.5322 30.7605 1 -13 -3 4-87.2174 115.373 1 -12 3 4 1442.92 313.557 1 -12 -3 4 1602.61 351.525 1 -12 3 4 1471.56 298.153 3 -11 -3 4 10.8811 37.6026 2 -11 3 4 34.7639 46.3361 3 -11 3 4 27.2761 60.7143 1 -11 -3 4 114.903 110.529 1 -10 3 4 4329.32 486.574 3 -10 3 4 4272.06 507.088 1 -10 -3 4 5046.86 590.548 1 -10 -3 4 4505.60 394.532 2 -9 3 4 211.022 53.7066 2 -9 -3 4 228.963 89.1306 2 -9 3 4 137.402 87.0903 1 -9 -3 4 182.273 106.482 1 -9 3 4 171.317 83.3262 3 -8 3 4 5936.16 232.217 2 -8 -3 4 6038.11 543.166 1 -8 -3 4 6032.50 410.358 2 -8 3 4 5938.61 533.748 3 -7 -3 4 28.4291 29.7807 2 -7 3 4 29.6713 15.0639 2 -7 -3 4-4.99503 39.1461 1 -7 3 4-8.63862 69.4793 3 -6 -3 4 190.539 148.652 1 -6 -3 4 120.282 67.4660 2 -6 3 4 43.3193 28.3177 3 -5 3 4 1424.52 249.025 3 -5 3 4 1253.27 98.9670 2 -5 -3 4 1576.85 193.789 2 -4 -3 4 52032.3 1055.69 2 -4 3 4 51129.2 1338.83 3 -4 3 4 52720.1 776.320 2 -3 -3 4 610.469 122.526 2 -3 3 4 231.576 48.2550 2 -3 3 4 477.427 134.105 3 -2 -3 4 62076.2 1248.85 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133.159 119.660 1 -16 3 -4 80.3205 79.6949 1 -16 -3 -4 162.524 146.490 1 -17 3 -4 52.6267 64.9789 1 -17 -3 -4 193.828 156.386 1 -18 3 -4 138.682 123.139 1 -20 4 4 962.363 359.360 1 -19 4 4 316.310 210.508 1 -19 -4 4 336.536 159.962 1 -18 4 4 2550.78 543.025 1 -18 -4 4 2676.20 562.040 1 -17 -4 4 559.939 240.435 1 -17 4 4 468.621 231.277 1 -16 4 4 4080.92 622.801 1 -16 -4 4 4095.67 642.218 1 -15 4 4 227.473 159.536 1 -15 -4 4 90.1604 48.2325 1 -14 -4 4 704.341 310.156 1 -14 4 4 1089.94 289.043 1 -14 4 4 1139.43 276.414 3 -13 4 4-41.8578 96.2590 1 -13 -4 4-86.3861 107.824 1 -13 4 4-46.2178 83.2420 3 -12 -4 4 507.338 210.963 1 -12 -4 4 342.103 112.797 2 -12 4 4 464.437 159.736 3 -12 4 4 234.276 115.246 1 -11 4 4-63.4258 95.1170 1 -11 -4 4 56.4792 48.8077 1 -11 4 4-17.9361 39.9576 3 -11 -4 4-67.1501 86.0060 2 -10 -4 4 17894.1 814.556 2 -10 4 4 18680.3 1053.62 1 -10 4 4 18810.9 1030.62 3 -10 -4 4 17167.9 1064.35 1 -9 -4 4 1032.55 243.366 1 -9 4 4 874.206 219.617 3 -9 -4 4 969.817 184.030 2 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3263.00 443.826 1 8 -4 4 3182.05 452.959 2 -9 4 -4 86.5163 82.1272 1 -9 -4 -4-52.0216 106.471 1 9 -4 4-14.5372 75.2005 2 -10 4 -4 4507.89 522.255 1 -10 -4 -4 4591.64 571.984 1 -11 -4 -4 765.475 238.808 1 -11 4 -4 657.997 216.397 1 -12 4 -4 3515.87 515.631 1 -12 -4 -4 3320.23 524.677 1 -13 4 -4 1535.50 355.752 1 -13 -4 -4 1329.36 345.661 1 -14 4 -4 1545.94 361.596 1 -14 -4 -4 1535.40 389.305 1 -15 4 -4 234.142 145.280 1 -15 -4 -4 470.965 223.148 1 -16 4 -4 721.020 264.845 1 -16 -4 -4 726.407 285.154 1 -17 4 -4 61.7670 21.9657 1 -17 -4 -4 200.184 158.407 1 -18 4 -4-12.3202 88.0135 1 -20 5 4 56.7508 52.3674 1 -19 5 4 21.6298 37.5478 1 -19 -5 4 61.6087 55.2144 1 -18 5 4-195.757 153.969 1 -18 -5 4-141.828 114.879 1 -17 -5 4 2.00194 89.6465 1 -17 5 4 34.7746 77.4345 1 -16 5 4 1031.40 337.524 1 -16 -5 4 824.337 297.654 1 -15 5 4-128.055 160.851 1 -15 -5 4-115.490 145.014 1 -14 -5 4 228.314 114.379 1 -14 5 4 278.172 121.394 3 -14 5 4 143.558 37.8684 1 -13 5 4 9.37669 53.8535 1 -13 -5 4-52.7300 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4 2104.44 277.053 2 -4 6 4 18411.1 830.964 3 -4 -6 4 17632.0 721.246 2 -3 -6 4 593.979 135.065 2 -3 6 4 562.495 150.523 3 -2 6 4 43053.3 1162.96 3 -2 -6 4 42249.2 1117.80 2 -1 -6 4 1459.86 129.383 2 -1 6 4 1951.54 245.587 3 0 -6 4 19700.9 822.423 2 0 6 4 19309.7 707.282 3 1 6 4 624.234 130.095 3 1 -6 4 597.678 146.844 2 2 -6 4 4099.53 393.065 2 3 -6 4 78.3534 111.444 2 4 -6 4 21279.9 988.951 2 -4 6 -4 21941.3 796.730 1 5 -6 4-171.556 213.949 2 -5 6 -4 316.969 102.182 1 -6 6 -4 258.899 93.8086 1 6 -6 4-318.212 321.462 2 7 -6 4 155.770 235.152 2 -7 6 -4 130.923 79.2162 1 -7 -6 -4 45.6541 100.810 1 -8 6 -4 85.0583 17.4446 1 -8 -6 -4 87.6722 19.8261 1 8 -6 4 123.904 31.0888 2 -9 6 -4 908.152 227.073 1 -9 -6 -4 899.814 261.724 1 9 -6 4 877.082 246.201 2 -10 -6 -4 2162.57 405.822 1 -10 6 -4 2314.10 371.956 1 10 -6 4 2417.10 424.996 2 -11 6 -4 3297.74 478.934 1 -11 -6 -4 3334.50 520.349 1 -12 -6 -4 3687.15 561.604 1 -12 6 -4 3950.50 533.676 1 -13 6 -4 2181.35 430.661 1 -13 -6 -4 2078.68 446.951 1 -14 6 -4 613.054 223.002 1 -14 -6 -4 493.356 234.457 1 -15 6 -4 1021.08 304.862 1 -15 -6 -4 1146.99 352.597 1 -16 -6 -4 42.7929 56.9546 1 -16 6 -4-217.523 156.980 1 -17 6 -4 50.6585 41.4219 1 -17 -6 -4 83.2740 97.7898 1 -18 6 -4-74.8266 87.1848 1 -19 -7 4 93.9995 137.996 1 -18 7 4 52.1644 82.2168 1 -18 -7 4 488.258 237.795 1 -17 7 4 76.8430 87.9585 1 -17 -7 4 68.0128 78.4605 1 -16 7 4-63.4285 83.5081 1 -16 -7 4 83.8190 72.4857 1 -15 7 4 2434.09 487.632 1 -15 -7 4 2105.01 465.978 1 -14 -7 4 4643.80 629.088 1 -14 7 4 4886.83 590.270 3 -14 7 4 4738.17 632.668 1 -13 -7 4 689.412 199.317 2 -13 7 4 998.510 274.423 3 -13 -7 4 812.580 273.985 1 -12 -7 4 592.489 153.975 2 -12 -7 4 844.571 241.027 1 -12 7 4 764.220 261.439 3 -11 -7 4 576.447 208.668 1 -11 -7 4 608.807 167.904 2 -11 7 4 573.458 192.643 3 -10 -7 4 6349.01 538.329 2 -10 -7 4 6897.86 643.926 1 -10 7 4 6997.93 624.292 3 -9 -7 4 1203.94 255.682 1 -9 7 4 1399.72 285.962 3 -9 -7 4 1353.21 251.694 2 -8 -7 4 8284.73 639.086 1 -8 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4-11.5738 54.3321 3 -9 -8 4-53.6429 92.3989 1 -8 -8 4 2928.90 376.317 1 -8 8 4 3202.76 414.140 3 -8 -8 4 2988.57 360.632 2 -7 -8 4 15.8645 37.1450 2 -7 8 4-5.25253 48.3500 3 -7 -8 4 23.6325 41.2313 1 -6 -8 4 9554.11 595.794 1 -6 8 4 9404.08 653.597 3 -6 -8 4 9368.92 599.862 2 5 -8 -4 2.99274 8.03406 2 -5 -8 4 33.4047 58.4056 1 -5 -8 4 23.9625 56.9718 2 -5 8 4-67.7132 102.383 3 -4 -8 4 145778. 2230.26 2 -4 -8 4 142204. 1953.53 1 -4 8 4 146702. 2427.73 3 -3 8 4 193.638 78.0760 3 -3 -8 4 217.812 90.7732 2 -2 -8 4 70283.1 1547.50 2 -2 8 4 69783.1 1564.33 3 -1 8 4 1144.95 205.674 3 -1 -8 4 1276.20 211.276 2 0 8 4 13130.2 629.517 3 0 -8 4 12701.0 655.125 2 1 8 4 1719.22 229.045 3 1 -8 4 1600.44 225.913 2 2 -8 4 94558.0 2020.34 2 3 -8 4 684.875 171.622 2 -3 8 -4 659.299 122.245 1 4 -8 4 7886.27 610.536 2 -4 8 -4 7610.19 446.640 1 5 -8 4 2931.89 386.450 2 -5 8 -4 3266.98 331.113 1 -6 8 -4 8282.55 543.801 1 6 -8 4 6852.52 598.252 2 -7 -8 -4 1387.04 301.181 1 -7 8 -4 1331.90 241.170 1 -8 8 -4 3404.81 403.437 1 -8 -8 -4 3689.02 487.741 1 8 -8 4 2529.11 378.224 2 -9 8 -4 1932.36 327.884 1 -9 -8 -4 1807.36 374.243 1 9 -8 4 1870.51 370.364 2 -10 -8 -4 457.096 212.234 1 -10 8 -4 595.774 216.764 1 10 -8 4 403.682 179.194 2 -11 8 -4 531.704 187.106 1 -11 -8 -4 467.410 177.235 1 11 -8 4 459.101 202.577 2 -12 8 -4 187.581 94.2583 1 -12 -8 -4 306.814 165.940 1 -13 -8 -4 413.929 160.645 1 -13 8 -4 269.035 141.218 1 -14 -8 -4 168.399 125.062 1 -14 8 -4 42.3667 114.977 1 -15 -8 -4 224.346 196.021 1 -15 8 -4-49.4459 129.777 1 -16 -8 -4 80.6471 142.321 1 -17 -8 -4 716.137 307.648 1 -19 -9 4 109.843 140.232 1 -18 -9 4 286.759 204.270 1 -17 -9 4 529.665 272.875 1 -16 -9 4 1781.37 443.678 1 -15 -9 4 2516.55 519.584 1 -14 -9 4 7181.63 801.655 1 -14 9 4 6717.35 680.801 3 -13 -9 4 3447.27 486.501 2 -13 -9 4 3678.92 560.281 1 -13 9 4 3670.79 514.624 3 -12 -9 4 12887.4 867.474 2 -12 -9 4 13794.9 998.570 1 -12 9 4 13235.1 925.146 3 -11 -9 4 2884.90 408.139 2 -11 9 4 3003.16 438.242 3 -11 -9 4 2677.14 451.837 1 -10 9 4 21356.5 1125.06 3 -10 -9 4 21145.2 1137.91 1 -10 -9 4 20100.6 1033.20 2 -9 -9 4 1825.25 322.417 1 -9 9 4 1883.29 341.683 3 -9 -9 4 2076.73 331.082 2 -8 9 4 21272.5 1056.01 3 -8 -9 4 20768.9 973.585 2 -8 -9 4 20341.5 1012.40 1 -7 -9 4 294.064 114.671 2 -7 -9 4 224.219 90.0526 1 -7 9 4 224.200 72.0196 3 -6 -9 4 5701.19 459.149 1 -6 9 4 5386.04 501.376 3 -6 -9 4 5342.87 466.558 2 -5 -9 4 2557.53 300.784 1 -5 -9 4 2873.35 346.488 2 -5 9 4 2618.11 359.597 3 5 -9 -4 2597.15 167.755 2 -4 -9 4 3144.87 290.969 1 -4 9 4 2883.39 336.543 3 -4 -9 4 3624.05 373.825 2 -3 9 4 83.0563 63.0370 3 -3 -9 4 43.2900 48.6731 2 -2 9 4 1035.93 192.836 3 -2 -9 4 882.988 180.483 2 -1 9 4 290.696 104.639 3 -1 -9 4 248.971 88.1503 2 0 -9 4-154.020 253.503 2 0 9 4 389.579 117.425 3 2 -9 4-155.463 180.368 2 -3 9 -4 910.371 138.581 1 3 -9 4 914.906 231.378 2 4 -9 4 19677.9 980.584 2 -4 9 -4 18988.6 678.857 1 -5 9 -4 2765.13 293.865 1 5 -9 4 3581.64 448.256 2 -6 9 -4 13630.6 669.770 1 6 -9 4 13267.6 850.173 2 -7 9 -4 4221.07 421.790 1 -7 -9 -4 4231.80 525.600 1 7 -9 4 3544.18 411.187 2 -8 9 -4 22074.2 998.002 1 -8 -9 -4 22372.6 1246.60 1 8 -9 4 20173.7 1154.27 2 -9 9 -4 4319.84 476.170 1 -9 -9 -4 4605.38 590.176 1 9 -9 4 4022.21 568.186 2 -10 -9 -4 15205.5 1073.63 1 10 -9 4 14196.5 1052.31 2 -10 9 -4 14790.8 915.054 1 -11 -9 -4 455.784 207.169 1 11 -9 4 613.713 228.983 2 -11 9 -4 616.204 185.369 1 -12 -9 -4-120.925 128.578 1 -12 9 -4 16.3386 49.8869 1 12 -9 4 52.2365 72.2855 2 -13 9 -4-133.156 117.475 1 -13 -9 -4-95.4811 139.156 1 -14 -9 -4-52.1120 108.278 1 -14 9 -4 7.85571 36.3634 1 -15 -9 -4 65.1225 100.465 1 -16 -9 -4 175.391 140.827 1 -17 -9 -4 149.309 142.827 1 -19 -10 4 872.582 370.837 1 -18 -10 4 2879.04 609.234 1 -17 -10 4 874.935 354.986 1 -16 -10 4 4284.02 677.327 1 -15 -10 4 287.732 211.850 1 -14 -10 4 7785.55 835.817 1 -14 10 4 7323.91 726.417 3 -13 -10 4 18.8013 36.1572 2 -13 10 4 48.3751 65.9521 3 -13 -10 4 96.4233 97.1092 1 -12 -10 4 1622.70 306.527 2 -12 10 4 1773.29 347.110 3 -12 -10 4 1792.08 364.200 1 -11 -10 4 65.1530 17.6635 2 -11 10 4 79.2967 36.7970 3 -11 -10 4 130.677 101.325 1 -10 -10 4 141.531 82.2728 2 -10 -10 4 205.872 132.147 1 -10 10 4 181.781 82.5898 3 -9 -10 4 298.077 117.756 1 -9 -10 4 321.203 121.171 2 -9 10 4 386.545 158.334 3 -8 -10 4 17270.0 927.728 1 -8 10 4 17289.8 972.969 3 -8 -10 4 16784.4 910.082 2 -7 -10 4 112.986 25.0604 1 -7 10 4 124.186 42.6105 3 -7 -10 4 193.739 93.5556 2 -6 -10 4 28861.7 1045.63 1 6 -10 -4 24880.0 442.125 2 -6 10 4 29061.3 1199.98 3 -6 -10 4 28250.0 1117.08 2 -5 -10 4 859.501 175.481 1 -5 10 4 830.463 200.613 3 -5 -10 4 957.779 210.910 2 5 -10 -4 965.023 114.542 2 -4 10 4 149705. 2594.57 3 -4 -10 4 158239. 2535.09 2 -4 -10 4 149891. 1990.42 1 -3 10 4 946.439 211.292 3 -3 -10 4 1317.08 243.563 2 -2 -10 4 184462. 2687.27 2 -2 10 4 179721. 2684.05 3 -1 -10 4 2022.77 289.920 2 -1 10 4 1766.46 267.862 3 0 -10 4 82347.2 1811.91 2 0 10 4 79986.5 1698.00 3 1 -10 4 1464.79 155.064 2 2 -10 4 16451.2 861.196 2 -2 10 -4 16966.5 475.846 1 -3 10 -4 1877.95 187.871 1 3 -10 4 2606.24 381.567 2 -4 10 -4 84196.8 1359.87 1 4 -10 4 78085.5 1961.15 2 5 -10 4 4952.31 550.460 2 -5 10 -4 4072.43 342.171 1 6 -10 4 15832.6 941.990 2 -6 10 -4 17729.3 762.219 1 -7 -10 -4 3828.29 509.295 1 -7 10 -4 3985.83 398.698 1 7 -10 4 3492.28 442.674 2 -8 10 -4 5041.49 471.843 1 -8 -10 -4 4894.25 573.733 1 -9 -10 -4 768.653 231.563 1 -9 10 -4 842.918 202.608 1 -10 10 -4 759.987 212.359 1 -10 -10 -4 701.340 241.713 1 10 -10 4 795.095 266.473 2 -11 10 -4 48.7555 49.2329 1 -11 -10 -4-118.226 141.072 1 11 -10 4 64.2481 64.5166 2 -12 10 -4-26.2683 18.7933 1 -12 -10 -4 56.9826 47.1774 1 12 -10 4 39.5339 66.0680 2 -13 -10 -4-42.8562 81.8581 1 -14 -10 -4 13.5485 38.0955 1 -15 -10 -4 54.6136 5.21475 1 -16 -10 -4 255.399 188.824 1 -19 -11 4 40.7402 102.112 1 -18 -11 4 114.230 193.096 1 -17 -11 4 536.331 247.253 1 -16 -11 4 375.589 186.084 1 -15 -11 4 47.1443 117.397 1 -14 -11 4 251.759 135.967 2 -14 -11 4 332.628 148.958 1 -14 11 4 377.334 170.710 3 -13 -11 4 131.236 92.5776 2 -13 -11 4 195.696 140.435 1 -13 11 4 97.4709 111.612 3 -12 11 4-17.9257 72.2765 3 -12 -11 4 52.5395 13.9619 2 -12 -11 4 68.0846 70.3820 1 -11 -11 4 542.876 179.797 2 -11 11 4 570.981 201.557 3 -11 -11 4 555.621 188.686 1 -10 11 4 1632.90 307.787 3 -10 -11 4 1462.29 283.876 2 -10 -11 4 1695.24 319.572 1 -9 -11 4 233.970 103.154 2 -9 11 4 236.881 114.306 3 -9 -11 4 265.368 117.563 1 -8 -11 4 10332.5 721.522 1 -8 11 4 10015.8 754.479 3 -8 -11 4 10321.1 740.435 2 -7 -11 4 472.521 138.434 1 -7 -11 4 524.287 151.992 2 -7 11 4 426.519 153.790 3 -6 -11 4 1109.95 208.982 1 6 -11 -4 820.772 96.2968 2 -6 -11 4 990.403 216.628 2 -6 11 4 922.329 213.468 3 -5 -11 4 2648.99 299.523 1 -5 11 4 2650.83 374.916 3 -5 -11 4 3186.82 393.278 2 5 -11 -4 3055.22 223.199 2 -4 11 4 1951.78 299.728 3 -4 -11 4 2025.27 232.018 1 -4 -11 4 2286.13 328.662 2 -3 11 4 2011.05 321.827 3 -3 -11 4 2434.99 333.666 2 -2 -11 4 8838.80 609.251 2 -2 11 4 9267.50 615.664 3 -1 11 4 1019.96 213.871 3 -1 -11 4 1219.03 235.843 2 0 -11 4 45179.7 1374.92 2 1 -11 4 1336.10 142.080 2 -2 11 -4 749.812 90.8885 1 2 -11 4 231.441 166.181 2 3 -11 4 1322.56 280.464 2 -3 11 -4 1263.74 142.541 1 4 -11 4 84828.8 2091.16 2 -4 11 -4 83864.8 1314.94 1 5 -11 4 594.043 212.023 2 -5 11 -4 278.307 90.9651 1 6 -11 4 13894.4 885.679 2 -6 11 -4 14175.5 664.214 1 -7 -11 -4-19.4651 103.718 1 -7 11 -4 37.6780 55.5154 1 -8 -11 -4 1347.83 294.280 1 -8 11 -4 1306.88 234.487 1 -9 11 -4 92.0690 63.5627 1 -9 -11 -4 47.3944 30.6863 1 10 -11 4 119.130 11.0654 2 -10 11 -4 152.199 87.6477 1 -10 -11 -4 35.2205 51.2846 1 -11 -11 -4 283.505 206.081 1 11 -11 4 276.730 169.393 2 12 -11 4 275.601 139.057 2 -12 -11 -4 430.318 208.184 1 -13 -11 -4 133.998 83.8433 1 -14 -11 -4-128.117 141.386 1 -15 -11 -4 98.9752 133.492 1 -16 -11 -4 19.9775 87.0169 1 -19 -12 4 183.964 188.682 1 -18 -12 4 223.626 186.567 1 -17 -12 4 433.227 253.293 1 -16 -12 4-84.9369 116.761 1 -15 -12 4 326.523 180.959 1 -14 -12 4 245.060 150.818 1 -14 -12 4 319.440 148.991 2 -14 12 4 196.127 113.070 3 -13 -12 4 1293.07 315.521 2 -13 12 4 1635.61 354.206 3 -13 -12 4 1542.93 382.106 1 -12 -12 4 3097.60 462.856 2 -12 -12 4 3289.67 504.550 1 -12 12 4 3490.61 487.011 3 -11 -12 4 208.449 97.0980 2 -11 12 4 86.6245 55.9244 3 -11 -12 4 136.421 118.712 1 -10 12 4 3452.84 469.024 3 -10 -12 4 3337.40 458.322 1 -10 -12 4 3143.05 441.672 2 -9 -12 4-42.4423 65.2465 2 -9 12 4 5.98673 73.6251 3 -9 -12 4-72.2434 84.1572 1 -8 -12 4 1899.98 301.968 1 -8 -12 4 2062.81 333.058 2 -8 12 4 2070.20 338.910 3 -7 12 4-9.62451 72.9780 3 -7 -12 4 29.8389 48.3378 2 7 -12 -4-87.7243 52.3980 2 -7 -12 4-24.8908 56.3523 1 -6 12 4 27996.9 1222.17 3 -6 -12 4 28419.0 1044.13 1 6 -12 -4 26711.4 612.865 2 -6 -12 4 28291.5 1199.16 2 5 -12 -4 24.3607 27.7587 2 -5 -12 4 3.96389 9.55202 1 -5 12 4-3.63413 52.4637 3 -5 -12 4 27.5251 44.1698 2 4 -12 -4 5225.15 338.004 2 -4 -12 4 5536.30 379.454 1 -4 12 4 5717.59 516.663 3 -4 -12 4 5552.38 516.899 2 -3 12 4 67.7613 98.6670 3 -3 -12 4 78.6708 103.395 2 -2 12 4 1992.13 293.507 3 -2 -12 4 1880.27 288.974 2 -1 -12 4 54.1343 41.6447 2 -1 12 4 70.0143 49.4538 3 0 -12 4 4237.19 428.478 2 -2 12 -4 8404.30 258.237 1 2 -12 4 7879.33 585.925 2 -3 12 -4 111.205 57.4379 1 3 -12 4 138.561 158.511 2 4 -12 4 28202.5 1248.89 2 -4 12 -4 26854.9 709.548 1 -5 12 -4 259.966 78.0815 1 5 -12 4 482.759 188.292 2 6 -12 4 3883.07 484.327 2 -6 12 -4 3780.21 345.255 1 7 -12 4-180.414 160.139 2 -7 -12 -4-27.7712 107.670 1 -7 12 -4 24.5637 43.6645 1 -8 -12 -4-53.7748 77.0028 1 -9 -12 -4 517.080 196.302 1 10 -12 4-48.5443 338.371 2 -10 -12 -4 153.551 120.980 1 11 -12 4 542.491 225.145 2 -11 -12 -4 418.928 191.120 1 -12 -12 -4 1270.13 344.416 1 -13 -12 -4-122.827 141.418 1 -14 -12 -4 122.202 15.2468 1 -15 -12 -4 8.22623 79.2599 1 -16 -12 -4 432.857 259.884 1 -19 -13 4 44.0942 92.8926 1 -18 -13 4 32.9403 74.2348 1 -17 -13 4 187.908 182.531 1 -16 -13 4 2183.93 484.551 1 -15 -13 4 1204.23 354.214 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605.543 3 -3 -13 4 7687.42 623.710 2 -2 13 4 8930.37 633.410 3 -2 -13 4 8815.03 643.658 2 -1 -13 4 1183.94 244.720 2 0 -13 4 16135.3 865.051 2 1 -13 4 59.3712 243.898 2 2 -13 4 71.7560 239.712 2 3 -13 4 5147.33 537.915 2 -3 13 -4 3647.59 212.089 1 4 -13 4 1107.36 322.285 2 -4 13 -4 549.199 106.564 1 5 -13 4 5089.93 554.551 2 6 -13 4 735.469 241.747 2 7 -13 4 2391.63 386.943 2 -7 -13 -4 2402.59 418.754 1 -8 -13 -4 4878.80 593.144 1 8 -13 4 3772.73 472.876 2 9 -13 4 186.039 321.471 2 -9 -13 -4 1677.23 377.937 1 -10 -13 -4 584.581 230.366 1 -11 -13 -4 77.5677 59.7836 1 11 -13 4 133.962 89.9308 2 -12 -13 -4 127.932 63.1740 1 -13 -13 -4-52.8671 119.242 1 -14 -13 -4-194.083 185.495 1 -15 -13 -4 148.541 142.041 1 -16 -13 -4 35.1597 27.4323 1 -18 -14 4 1484.39 434.064 1 -17 -14 4 1360.20 415.295 1 -16 -14 4 708.344 279.073 1 -15 -14 4 789.391 281.959 2 -15 -14 4 802.556 283.814 1 -14 -14 4 837.306 266.540 2 -14 -14 4 814.062 281.230 1 -14 14 4 755.653 245.156 3 -13 -14 4 593.880 218.186 2 -13 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521.408 3 -7 -16 4 17.5004 32.4421 2 -7 16 4 127.914 111.493 3 -7 -16 4 98.1446 47.8350 1 6 -16 -4 2508.82 252.022 2 -6 -16 4 2457.35 311.406 1 -6 16 4 2626.48 393.214 3 -6 -16 4 2509.33 400.745 2 -5 16 4 1114.46 270.013 3 -5 -16 4 1021.91 187.525 1 5 -16 -4 1046.21 182.371 2 -5 -16 4 1209.22 288.425 2 -4 -16 4 92168.7 1609.53 1 -4 -16 4 93250.4 2359.52 2 4 -16 -4 86985.4 1730.45 2 3 -16 -4 2330.19 321.660 2 -3 -16 4 1930.41 204.277 1 -3 -16 4 2367.83 381.478 2 -2 -16 4 62606.7 1855.12 2 -1 -16 4-4.36562 50.2902 2 0 -16 4 2060.55 336.534 2 1 -16 4 343.197 151.754 2 2 -16 4 23176.2 1144.80 2 3 -16 4 504.426 197.888 2 4 -16 4 12108.2 884.950 2 5 -16 4 7827.70 740.533 2 6 -16 4 14812.0 1003.58 2 7 -16 4 5863.47 649.586 2 -7 -16 -4 4533.12 587.465 1 8 -16 4 98.6383 25.5379 2 -8 -16 -4 312.402 138.345 1 9 -16 4 1439.22 252.530 2 -9 -16 -4 2046.08 443.026 1 10 -16 4 1969.17 165.021 2 -10 -16 -4 3357.18 552.684 1 -11 -16 -4 1538.52 398.470 1 -12 -16 -4 1127.66 339.509 1 -13 -16 -4 1093.07 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377.951 2 7 -18 4 2037.80 409.278 2 -7 -18 -4 1455.91 348.627 1 -8 -18 -4 2520.05 452.464 1 8 -18 4 2586.20 442.093 2 9 -18 4 1417.89 307.305 2 -9 -18 -4 1656.44 381.387 1 -10 -18 -4 1958.95 419.627 1 -11 -18 -4 1839.22 452.338 1 -12 -18 -4 3605.97 617.018 1 -13 -18 -4 2126.33 493.545 1 -14 -18 -4 2518.18 553.364 1 -15 -18 -4 1075.82 381.886 1 -18 -19 4-52.6474 113.875 1 -17 -19 4-20.4185 106.262 1 -16 -19 4 448.020 191.194 2 -16 -19 4 229.444 98.7764 1 -15 -19 4 104.867 27.6345 2 -15 -19 4 117.118 107.381 1 -14 19 4 2135.78 442.687 3 -14 -19 4 2116.59 447.079 1 -14 -19 4 2137.80 467.872 2 -13 -19 4-89.0190 134.102 2 -13 19 4 101.324 135.091 3 -13 -19 4-87.8063 146.231 1 -12 -19 4 1573.06 362.503 1 -12 19 4 1528.60 387.389 3 -12 -19 4 1799.84 408.540 2 -11 -19 4 246.721 193.946 2 -11 -19 4 458.570 221.381 1 -11 19 4 333.027 191.108 3 -10 -19 4 3714.83 492.149 1 -10 19 4 3703.02 564.180 3 -10 -19 4 3658.57 572.005 2 -9 -19 4 855.646 287.077 2 -9 -19 4 639.585 191.449 1 -8 -19 4 1197.23 257.299 1 -8 -19 4 1295.54 333.641 2 -7 -19 4 1061.94 232.281 1 -7 -19 4 1211.32 320.266 2 -6 -19 4 1705.20 372.572 2 -6 -19 4 1792.71 270.194 1 5 -19 -4 4441.83 431.132 2 -5 -19 4 4744.22 598.122 2 -4 -19 4 11577.2 885.757 2 4 -19 -4 11422.1 702.525 2 3 -19 -4 2597.89 364.052 2 -3 -19 4 3030.03 461.006 2 2 -19 -4 56027.5 1674.00 2 -2 -19 4 59780.8 1978.95 2 -1 -19 4-3.03772 76.6390 2 0 -19 4 4373.31 524.413 2 1 -19 4 182.853 122.530 2 4 -19 4-27.5383 207.244 2 5 -19 4 103.821 112.656 2 6 -19 4 4135.28 592.891 2 -7 -19 -4 1254.10 298.468 1 7 -19 4 1743.50 378.564 2 8 -19 4 254.056 132.845 2 -8 -19 -4 53.3935 63.3069 1 9 -19 4 1912.72 395.003 2 -9 -19 -4 1711.33 396.966 1 -10 -19 -4 337.291 205.421 1 -11 -19 -4 393.345 206.787 1 -12 -19 -4 1564.02 405.221 1 -13 -19 -4 108.215 122.798 1 -14 -19 -4 2045.50 506.534 1 -15 -19 -4 307.128 227.209 1 -18 -20 4-98.1399 157.470 1 -17 -20 4-155.465 171.341 1 -16 -20 4-19.0924 63.3748 2 -16 -20 4-208.171 215.658 1 -15 -20 4 59.9476 43.8670 2 -15 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1622.65 323.356 2 -2 -22 4 1949.76 379.418 2 1 -22 -4 414.383 173.064 2 -1 -22 4 425.519 158.142 2 0 -22 4 482.011 189.753 2 1 -22 4 61.3943 57.9381 2 2 -22 4 404.230 139.103 2 4 -22 4 1386.62 127.505 2 5 -22 4-264.387 275.977 2 -6 -22 -4-123.518 186.546 1 6 -22 4 149.149 113.896 2 -7 -22 -4-195.076 187.352 1 7 -22 4 81.4679 132.106 2 -8 -22 -4 549.418 174.829 1 8 -22 4 623.717 253.523 2 -9 -22 -4 1648.08 431.676 1 -10 -22 -4 6000.54 789.068 1 -11 -22 -4 1878.06 462.989 1 -12 -22 -4 4867.75 759.128 1 -13 -22 -4 666.236 307.480 1 -14 -22 -4 1212.45 429.094 1 -17 -23 4-146.108 192.507 2 -16 -23 4 181.075 190.002 2 -15 -23 4 109.635 104.624 2 -14 -23 4 239.225 182.884 2 -13 -23 4 68.6893 78.9477 2 -12 -23 4 986.353 330.606 2 -11 -23 4 139.404 164.859 2 -10 -23 4 802.193 304.461 2 -9 -23 4 217.161 173.335 2 -8 -23 4 4117.31 626.326 2 -7 -23 4 635.608 273.667 2 -6 -23 4 17818.9 1248.47 2 -5 -23 4 292.067 205.612 2 -4 -23 4 44074.9 1911.43 2 4 -23 -4 40683.9 1482.09 2 3 -23 -4 843.584 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5 349.820 98.6517 2 -10 3 5 379.064 143.445 3 -9 -3 5 497.766 156.470 1 -9 3 5 472.682 148.220 3 -9 -3 5 493.752 117.104 2 -8 3 5 586.668 73.9798 2 -8 -3 5 825.583 206.419 1 -8 3 5 1063.53 247.552 3 -8 -3 5 933.511 172.471 2 -7 3 5 35521.0 579.063 2 -7 -3 5 38998.2 1018.99 2 -7 3 5 38500.6 1399.83 3 -6 -3 5 1827.81 226.366 2 -6 3 5 1817.53 319.711 3 -6 3 5 1791.49 144.273 2 -5 -3 5 49850.3 1123.10 2 -5 3 5 49835.8 1480.21 3 -5 3 5 53033.1 880.420 2 -4 -3 5-160.677 137.100 2 -4 3 5 97.1715 84.3678 3 -3 -3 5 69358.7 1417.59 2 -3 3 5 66921.7 1580.61 3 -3 3 5 69771.6 1236.60 2 -2 -3 5 1999.67 252.598 2 -2 3 5 1978.52 268.565 3 -2 3 5 1878.05 229.647 2 -1 3 5 246639. 2708.48 3 -1 -3 5 237936. 2797.21 2 -1 3 5 242109. 2726.25 2 0 -3 5 12404.0 674.131 2 0 3 5 10990.6 555.471 3 0 3 5 11202.1 639.584 2 1 -3 5 98090.8 1968.05 2 1 3 5 99578.9 1490.68 3 1 3 5 101622. 1978.13 2 2 3 5 12359.0 487.321 3 2 3 5 12435.1 750.995 2 2 -3 5 12074.7 743.335 2 3 3 5 23554.3 595.934 3 3 -3 5 22412.9 1029.02 2 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462.169 193.021 3 -15 4 5 989.971 341.307 1 -14 4 5 84.1465 82.5856 1 -14 -4 5 94.8490 94.2453 1 -14 4 5 26.3516 48.4642 3 -13 -4 5 88.4849 94.1366 1 -13 4 5-74.6536 113.911 3 -12 -4 5 1553.73 355.910 1 -12 4 5 1415.43 314.193 3 -11 4 5 1686.53 313.645 3 -11 -4 5 1961.26 362.979 1 -11 -4 5 1885.04 275.129 2 -10 -4 5 1283.29 297.172 1 -10 4 5 1407.51 306.453 3 -10 -4 5 1307.21 221.226 2 -9 -4 5 460.520 173.924 1 -9 -4 5 476.345 152.884 2 -9 4 5 276.625 80.7477 3 -8 -4 5 724.504 201.932 1 -8 -4 5 891.419 178.476 2 -8 4 5 839.820 217.145 3 -7 -4 5 573.544 129.297 2 -7 4 5 454.890 142.319 3 -6 -4 5 124.652 77.2834 2 -6 4 5 40.2438 51.1658 3 -6 4 5 37.5893 21.9297 2 -5 -4 5 1866.91 227.952 2 -5 4 5 2182.69 305.425 3 -5 4 5 1850.46 156.416 2 -4 -4 5 919.649 166.306 2 -4 4 5 866.679 187.456 3 -4 4 5 812.542 123.315 2 -3 -4 5 7169.24 427.013 2 -3 4 5 7904.51 540.658 3 -3 4 5 7755.95 406.722 2 -2 4 5-38.9563 56.8668 3 -2 4 5-31.0698 36.4308 2 -1 -4 5 7694.52 520.684 2 -1 4 5 7816.58 486.648 3 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364.109 3 -1 6 5 5209.89 413.204 3 -1 -6 5 5097.49 428.135 2 0 -6 5 242.822 143.507 2 0 6 5 47.3617 26.7690 3 1 -6 5 9507.59 643.267 2 1 6 5 9869.82 511.860 3 2 -6 5 1283.13 257.750 2 2 6 5 682.475 134.823 3 3 -6 5 23991.7 1070.23 2 4 -6 5 1668.07 287.889 2 5 -6 5-492.127 324.577 2 -5 6 -5 454.334 136.602 1 6 -6 5 128.710 344.630 2 -6 6 -5 977.954 214.203 1 -7 6 -5 2957.98 373.787 1 7 -6 5 3200.03 461.392 2 -8 -6 -5 1017.17 278.482 1 -8 6 -5 1116.49 244.368 1 8 -6 5 1087.31 272.329 2 -9 6 -5 8595.57 695.443 1 -9 -6 -5 8410.76 798.523 1 9 -6 5 8498.51 819.971 2 -10 6 -5-2.37504 42.8542 1 -10 -6 -5-16.1430 13.5556 1 10 -6 5-97.1494 67.3199 2 -11 -6 -5 1467.79 341.038 1 -11 6 -5 1408.14 315.567 1 -12 6 -5 1227.40 323.800 1 -12 -6 -5 1310.83 380.744 1 -13 6 -5 2071.95 422.771 1 -13 -6 -5 2055.38 456.369 1 -14 -6 -5 811.383 273.825 1 -14 6 -5 650.133 257.709 1 -15 6 -5 592.067 229.691 1 -15 -6 -5 681.488 287.663 1 -16 6 -5 5.19331 64.7213 1 -16 -6 -5 282.189 208.087 1 -17 -6 -5 206.811 191.615 1 -19 -7 5 118.033 75.2365 1 -18 -7 5 151.535 157.510 1 -17 -7 5 739.577 280.883 1 -16 -7 5 195.486 126.808 1 -15 7 5 1448.68 333.155 3 -15 -7 5 1485.63 375.798 1 -14 -7 5 1572.73 392.091 1 -14 7 5 1512.52 361.776 3 -13 -7 5 16303.6 1183.42 1 -13 7 5 16105.8 1073.94 3 -12 -7 5 2823.06 389.989 2 -12 -7 5 2460.21 468.534 1 -12 7 5 3091.95 480.700 3 -11 -7 5 77665.8 2308.41 1 -11 7 5 73580.9 2212.33 3 -11 -7 5 71023.5 1876.22 2 -10 -7 5 281.537 122.516 2 -10 7 5 226.513 124.845 3 -10 -7 5 262.637 148.462 1 -9 -7 5 23565.1 1154.48 1 -9 7 5 22941.8 1180.06 3 -9 -7 5 23059.9 990.156 2 -8 -7 5 33.5311 61.1543 1 -8 -7 5 82.1487 84.8889 2 -8 7 5 15.5739 42.5209 3 -7 -7 5 2381.67 336.198 1 -7 7 5 2460.82 366.359 3 -7 -7 5 2279.46 296.462 2 -6 -7 5 1970.26 276.326 2 -6 7 5 1767.06 304.930 3 -5 -7 5 773.863 163.852 2 -5 7 5 865.234 196.262 3 -4 7 5 28.6169 5.67065 3 -4 -7 5 45.2095 39.5109 2 -3 7 5 13761.9 735.743 3 -3 -7 5 13130.6 685.426 2 -2 7 5 2092.86 282.428 3 -2 -7 5 1425.06 142.978 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362.690 243.878 2 -1 8 5 1128.00 198.733 3 0 8 5 47.4577 48.5614 3 1 -8 5 15411.2 854.196 2 1 8 5 15217.3 683.354 3 2 -8 5 374.529 157.102 2 3 -8 5 326.075 140.507 2 4 -8 5 961.116 236.267 2 -4 8 -5 838.380 160.545 1 -5 8 -5 7721.68 515.708 1 5 -8 5 6887.79 616.167 2 -6 8 -5 2307.42 309.905 1 6 -8 5 2176.89 343.313 2 7 -8 5 532.807 133.136 2 -7 8 -5 2128.79 319.417 1 8 -8 5 1341.12 40.3901 2 -8 -8 -5 1376.85 320.409 1 -8 8 -5 1429.14 271.824 1 -9 -8 -5 134.070 73.0760 1 9 -8 5 174.392 111.155 2 -9 8 -5 69.6527 56.7976 1 -10 -8 -5 307.282 172.280 1 -10 8 -5 453.436 203.203 1 10 -8 5 362.668 157.756 2 -11 -8 -5 5409.32 682.521 1 -11 8 -5 5991.86 621.142 1 11 -8 5 5718.92 713.321 2 -12 -8 -5 1243.13 363.694 1 -12 8 -5 1348.14 316.339 1 -13 -8 -5 3090.39 543.563 1 -13 8 -5 3095.16 493.157 1 -14 -8 -5 859.154 282.424 1 -15 -8 -5 176.510 72.0788 1 -16 -8 -5 227.685 154.301 1 -19 -9 5 15.6682 37.5029 1 -18 -9 5-55.5917 56.2342 1 -17 -9 5-59.3732 119.102 1 -16 -9 5-83.7915 99.8475 1 -15 -9 5 3130.60 571.845 1 -15 9 5 2338.49 425.672 3 -14 9 5 196.590 56.3365 3 -14 -9 5 393.609 191.421 1 -13 -9 5 93.2921 46.9979 2 -13 -9 5 110.915 36.7506 1 -13 9 5-26.2648 91.2783 3 -12 -9 5 1100.80 305.537 1 -12 9 5 970.325 271.832 3 -12 -9 5 1066.15 253.971 2 -11 -9 5 1233.41 272.543 2 -11 -9 5 1488.38 322.192 1 -11 9 5 1380.03 294.767 3 -10 -9 5 2069.10 388.698 1 -10 9 5 2002.05 371.880 3 -10 -9 5 2170.39 347.424 2 -9 -9 5 441.407 171.454 1 -9 9 5 250.603 105.386 3 -9 -9 5 363.043 126.579 2 -8 -9 5 3763.85 453.918 1 -8 -9 5 4118.29 454.493 2 -8 9 5 3944.46 496.750 3 -7 -9 5 1186.84 233.831 1 -7 9 5 1306.71 261.653 3 -7 -9 5 1404.98 259.421 2 -6 -9 5 3764.15 416.283 2 -6 9 5 3564.03 441.780 3 -6 -9 5 3324.88 383.232 1 6 -9 -5 3098.72 150.659 2 -5 9 5 2941.37 359.765 3 -5 -9 5 3016.26 342.859 2 -4 9 5-137.632 115.397 3 -4 -9 5-41.8019 36.7601 2 -3 -9 5 1429.06 239.318 2 -3 9 5 1401.00 245.136 3 -2 -9 5 3098.75 364.453 2 -2 9 5 2586.83 343.218 3 -1 -9 5 10335.5 618.388 2 -1 9 5 12023.7 672.966 3 0 -9 5 176.217 248.923 2 0 9 5 1002.00 197.378 3 1 -9 5 12284.1 759.652 2 1 9 5 12231.2 645.882 3 2 -9 5 379.129 141.197 2 3 -9 5 6978.15 611.424 2 4 -9 5 1591.96 316.482 2 -4 9 -5 1281.31 197.160 1 5 -9 5 463.199 186.146 2 -5 9 -5 531.407 126.796 1 6 -9 5 966.695 235.999 2 -6 9 -5 878.970 193.811 1 7 -9 5 2407.15 212.827 2 -7 9 -5 3688.65 395.739 1 -8 9 -5 473.368 161.847 1 -8 -9 -5 634.130 201.605 1 9 -9 5 779.537 257.470 2 -9 -9 -5 640.510 227.761 1 -9 9 -5 731.198 206.058 1 -10 9 -5 215.704 125.541 1 -10 -9 -5 212.242 135.221 1 10 -9 5 176.367 130.422 2 -11 9 -5 384.335 163.435 1 -11 -9 -5 205.585 145.296 1 11 -9 5 327.743 156.030 2 -12 9 -5 353.151 170.453 1 -12 -9 -5 350.291 192.154 1 12 -9 5 324.696 185.062 2 -13 -9 -5 123.395 58.3790 1 -14 -9 -5 85.9531 28.1201 1 -15 -9 -5 131.602 51.1474 1 -16 -9 -5 118.542 127.182 1 -19 -10 5 695.876 307.600 1 -18 -10 5 398.538 247.306 1 -17 -10 5 475.659 258.039 1 -16 -10 5 522.865 245.960 1 -15 10 5 2352.49 440.747 3 -15 -10 5 2617.90 516.605 1 -14 10 5 448.111 202.580 3 -14 -10 5 580.733 254.559 1 -13 -10 5 663.166 226.465 2 -13 10 5 709.256 220.812 3 -13 -10 5 521.442 223.742 1 -12 -10 5 32.8664 71.9321 2 -12 -10 5 53.8604 124.372 1 -12 10 5 13.1119 56.6108 3 -11 -10 5 8234.47 754.501 1 -11 10 5 7996.78 746.956 3 -11 -10 5 7804.73 679.651 2 -10 -10 5 210.084 152.958 2 -10 -10 5 231.018 173.224 1 -10 10 5 37.2893 85.6939 3 -9 -10 5 8681.64 721.074 1 -9 10 5 8691.22 736.309 3 -9 -10 5 8812.89 680.836 2 -8 -10 5 76.8825 60.0511 1 -8 10 5 207.472 121.597 3 -8 -10 5 221.244 115.530 2 -7 -10 5 31605.9 1203.96 1 -7 -10 5 31273.1 1220.98 2 -7 10 5 30528.1 1323.44 3 -6 -10 5 943.608 194.425 1 -6 10 5 1001.39 237.601 3 -6 -10 5 1179.39 237.818 2 6 -10 -5 981.027 97.0454 2 -5 10 5 2214.66 331.557 3 -5 -10 5 2141.77 305.137 2 -4 -10 5 617.960 167.872 2 -4 10 5 499.889 151.762 3 -3 10 5 316.602 114.288 3 -3 -10 5 237.244 95.0276 2 -2 10 5 942.866 212.398 3 -2 -10 5 1128.40 223.127 2 -1 10 5 226.017 93.0626 3 0 10 5 184.806 90.7092 3 1 -10 5 81.9721 189.425 2 2 -10 5 2522.20 408.478 2 -3 10 -5 36786.6 920.540 1 3 -10 5 35838.9 1386.96 2 4 -10 5 1572.64 315.865 2 -4 10 -5 943.240 162.773 1 5 -10 5 30294.6 1355.74 2 -5 10 -5 31464.8 999.673 1 6 -10 5 330.035 191.421 2 -6 10 -5 228.753 100.990 1 7 -10 5 1521.85 78.9186 2 -7 10 -5 3815.50 414.737 1 -8 10 -5 318.256 161.258 1 -8 -10 -5 61.3363 88.6755 1 9 -10 5 2155.22 297.640 2 -9 10 -5 2827.02 388.030 1 -9 -10 -5 2865.67 493.401 1 -10 -10 -5 209.750 145.613 1 -10 10 -5 321.382 160.794 1 10 -10 5 226.652 166.782 2 -11 -10 -5 641.503 263.615 1 11 -10 5 303.331 174.746 2 -12 -10 -5 626.992 255.646 1 12 -10 5 520.396 217.593 2 -13 -10 -5 327.021 165.851 1 -14 -10 -5 54.3730 81.5645 1 -15 -10 -5-38.9149 161.956 1 -16 -10 -5 134.116 167.896 1 -19 -11 5 175.242 140.296 1 -18 -11 5 315.531 198.537 1 -17 -11 5 2552.92 560.917 1 -16 -11 5 2171.79 502.336 1 -15 11 5 11807.2 1000.70 3 -15 -11 5 12829.8 1116.15 1 -14 11 5 4148.76 594.265 3 -14 -11 5 4015.20 653.037 1 -13 -11 5 25718.5 1545.66 1 -13 11 5 26830.6 1446.28 3 -13 -11 5 27189.6 1352.97 2 -12 -11 5 2656.85 487.865 1 -12 11 5 2807.02 472.898 3 -12 -11 5 2824.40 455.763 2 -11 -11 5 31144.3 1524.70 1 -11 11 5 32410.6 1514.68 3 -11 -11 5 31897.0 1401.85 2 -10 -11 5 1784.34 337.381 1 -10 -11 5 1763.74 338.994 2 -10 11 5 1602.25 349.803 3 -9 -11 5 35397.9 1434.14 1 -9 11 5 35701.4 1516.48 3 -9 -11 5 34743.6 1391.76 2 -8 -11 5 2344.18 361.227 1 -8 11 5 2419.50 400.774 3 -8 -11 5 2612.02 387.191 2 -7 -11 5 16845.2 875.008 1 -7 11 5 16548.1 992.412 3 -7 -11 5 17074.4 935.824 2 6 -11 -5 17.4046 16.8131 2 -6 -11 5-19.1290 61.5281 1 -6 11 5-69.0459 91.3099 3 -6 -11 5-25.0538 64.2651 2 -5 -11 5 3457.90 394.989 2 -5 11 5 3668.59 433.095 3 -4 11 5 303.816 127.592 3 -4 -11 5 297.130 119.965 2 -3 11 5 638.242 161.291 3 -3 -11 5 563.601 156.732 2 -2 11 5 152.984 72.5198 3 -2 -11 5 114.557 60.4057 2 -1 -11 5 1.70370 61.4679 2 -1 11 5 25.9314 4.03635 3 0 11 5 296.655 124.029 3 1 -11 5 647.899 163.407 2 2 -11 5-46.6200 122.456 2 3 -11 5 2623.19 488.943 2 -3 11 -5 865.946 128.314 1 4 -11 5 4019.61 497.624 2 -4 11 -5 3078.61 288.324 1 5 -11 5 39846.2 1560.70 2 -5 11 -5 40476.8 1097.66 1 6 -11 5 12919.0 951.423 2 -6 11 -5 11480.7 641.754 1 -7 11 -5 32129.1 1134.48 1 7 -11 5 31061.1 1493.13 2 -8 11 -5 11827.8 743.706 1 -8 -11 -5 12085.8 997.825 1 8 -11 5 10909.3 918.216 2 -9 -11 -5 19199.8 1245.62 1 9 -11 5 15664.5 1116.65 2 -10 -11 -5 4639.44 680.790 1 10 -11 5 4569.65 658.799 2 -11 -11 -5 3880.91 599.030 1 11 -11 5 3546.65 571.137 2 12 -11 5 3072.53 549.460 2 -12 -11 -5 3340.88 602.800 1 -13 -11 -5 444.528 209.325 1 -14 -11 -5 791.958 297.026 1 -15 -11 -5-134.296 207.347 1 -16 -11 -5 299.569 235.767 1 -19 -12 5 1505.46 464.051 1 -18 -12 5 857.310 368.601 1 -17 -12 5 5456.89 801.949 1 -16 -12 5 104.452 144.063 1 -15 12 5 1234.56 328.278 3 -15 -12 5 1358.54 401.394 1 -14 -12 5 64.5869 109.480 2 -14 12 5 104.291 126.192 3 -14 -12 5 241.414 193.904 1 -13 -12 5 774.427 248.158 2 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5 35647.5 1453.03 2 -3 12 -5 34026.4 787.797 1 4 -12 5 4626.61 558.758 2 -4 12 -5 4110.67 312.842 1 5 -12 5 37381.9 1529.13 2 -5 12 -5 36419.3 1002.12 1 6 -12 5 1395.33 309.776 2 7 -12 5 6.10719 210.847 2 -8 -12 -5 227.168 150.728 1 -9 -12 -5 609.514 238.880 1 10 -12 5-6.84771 47.6102 2 -10 -12 -5 6.48386 11.6545 1 -11 -12 -5-146.739 139.183 1 11 -12 5 8.80627 75.6672 2 12 -12 5 230.905 152.497 2 -12 -12 -5 183.803 159.394 1 -13 -12 -5 1749.60 442.639 1 -14 -12 -5 408.747 249.866 1 -15 -12 -5 268.317 185.513 1 -16 -12 -5 432.204 259.871 1 -19 -13 5 209.186 151.852 1 -18 -13 5 998.517 367.878 1 -17 -13 5 174.742 160.449 1 -16 -13 5 1391.40 415.203 1 -15 -13 5 906.748 348.404 1 -15 13 5 1049.43 300.863 3 -14 -13 5 2115.16 479.880 1 -14 -13 5 2391.82 451.816 2 -14 13 5 2238.80 456.707 3 -13 -13 5 3777.35 581.768 1 -13 13 5 3956.96 553.574 3 -13 -13 5 3951.03 540.532 2 -12 -13 5 488.472 205.395 2 -12 13 5 383.393 171.676 3 -12 -13 5 426.900 206.025 1 -11 -13 5 12931.6 973.381 1 -11 -13 5 12962.2 946.854 2 -11 13 5 12757.1 969.526 3 -10 -13 5-21.6045 39.3850 2 -10 -13 5 37.4400 67.5597 1 -10 13 5 29.9472 51.1161 3 -9 -13 5 23914.4 1177.07 1 -9 13 5 24449.7 1278.92 3 -9 -13 5 23527.4 1201.86 2 -8 13 5 16.8980 66.8933 3 -8 -13 5 25.0815 29.0067 1 -8 -13 5 70.3502 85.1221 2 -7 -13 5 17152.3 886.853 1 -7 13 5 17035.3 1030.57 3 -7 -13 5 17224.5 998.105 2 -6 -13 5 51.0329 36.6979 1 -6 13 5 40.6694 41.2316 3 -6 -13 5-18.5144 75.5154 2 6 -13 -5 61.9210 27.3170 2 5 -13 -5 9470.56 459.960 2 -5 -13 5 9073.18 545.597 1 -5 13 5 9067.54 713.335 3 -5 -13 5 9324.75 697.047 2 -4 13 5 375.647 139.393 3 -4 -13 5 505.897 163.720 2 -3 -13 5 9346.44 685.353 2 -3 13 5 9425.00 685.573 3 -2 13 5 480.697 164.434 3 -2 -13 5 566.897 173.204 2 -1 -13 5 62908.2 1787.54 2 -1 13 5 62573.4 1720.85 3 0 -13 5-347.442 276.050 2 1 -13 5 26433.6 1222.76 2 2 -13 5-374.826 255.214 2 3 -13 5 46266.0 1697.28 2 4 -13 5 4226.56 546.765 2 5 -13 5 83435.8 2315.90 2 6 -13 5 6399.81 669.845 2 7 -13 5 19216.3 1166.64 2 -8 -13 -5 3289.06 527.612 1 8 -13 5 2560.58 398.042 2 -9 -13 -5 229.445 95.4304 1 -10 -13 -5 559.837 215.630 1 -11 -13 -5 294.189 131.384 1 11 -13 5 71.4642 30.1251 2 -12 -13 -5 1740.26 440.196 1 -13 -13 -5 1390.20 385.589 1 -14 -13 -5 928.053 336.158 1 -15 -13 -5-25.1998 11.5458 1 -19 -14 5-104.285 160.216 1 -18 -14 5 104.469 133.734 1 -17 -14 5 834.350 318.660 1 -16 -14 5 187.019 141.129 1 -15 -14 5 778.457 283.950 1 -15 14 5 733.514 260.225 3 -14 -14 5 844.250 289.059 2 -14 -14 5 865.835 297.298 1 -14 14 5 791.437 269.712 3 -13 -14 5 120.905 108.753 2 -13 -14 5 144.786 128.411 1 -13 14 5 101.554 89.2729 3 -12 -14 5 513.112 206.071 2 -12 14 5 386.992 161.938 3 -12 -14 5 475.842 202.860 1 -11 -14 5 609.057 225.603 2 -11 -14 5 588.488 231.518 1 -11 14 5 596.792 205.516 3 -10 -14 5 911.919 256.988 2 -10 14 5 870.968 258.786 3 -10 -14 5 863.334 246.257 1 -9 14 5 5378.64 616.804 3 -9 -14 5 4891.11 552.924 1 -9 -14 5 5382.61 600.984 2 -8 -14 5 395.671 156.833 1 -8 14 5 499.262 186.355 3 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148.945 3 -4 -15 5 96.3950 110.175 2 -3 -15 5 67444.4 1953.70 2 -3 15 5 66957.0 1939.17 3 -2 -15 5-9.65994 67.9015 2 -1 -15 5 17048.6 980.815 2 0 -15 5 77.8545 77.3585 2 1 -15 5 19825.3 1075.96 2 2 -15 5-415.251 325.034 2 3 -15 5 11355.8 861.051 2 4 -15 5 818.014 254.023 2 5 -15 5 1414.22 382.539 2 6 -15 5 441.412 201.465 2 7 -15 5 384.357 158.667 2 -8 -15 -5 195.879 105.423 1 8 -15 5-29.2116 145.074 2 9 -15 5 272.986 377.754 2 -9 -15 -5 1366.83 340.697 1 -10 -15 -5-57.8406 91.6581 1 11 -15 5-204.723 362.914 2 -11 -15 -5 10.3116 19.4878 1 -12 -15 -5-119.113 128.083 1 -13 -15 -5 121.425 92.5476 1 -14 -15 -5 62.6871 85.7111 1 -15 -15 -5 39.5360 71.1719 1 -18 -16 5 126.398 157.418 1 -17 -16 5 568.862 257.923 1 -16 -16 5 194.635 140.428 1 -15 -16 5 99.8804 107.123 2 -15 16 5 180.209 151.510 3 -15 -16 5 140.502 145.256 1 -14 -16 5 26.3838 63.2095 2 -14 16 5 49.4007 92.9978 3 -14 -16 5-62.7238 73.9512 1 -13 -16 5 42.7331 48.1970 2 -13 16 5-3.23634 20.4043 3 -13 -16 5 22.0198 76.7609 1 -12 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7824.30 790.312 2 6 -16 5 550.909 224.877 2 7 -16 5 2401.36 431.833 2 8 -16 5-87.6802 191.517 2 -8 -16 -5 93.6053 58.5266 1 -9 -16 -5 87.2072 58.7785 1 -10 -16 -5-99.8577 138.027 1 -11 -16 -5 95.2802 85.9465 1 -12 -16 -5 469.163 246.588 1 -13 -16 -5 419.939 223.864 1 -14 -16 -5 653.335 264.830 1 -15 -16 -5 817.436 343.457 1 -18 -17 5 184.749 161.426 1 -17 -17 5 95.0336 89.8842 1 -16 -17 5 419.276 232.733 1 -15 -17 5 1476.55 377.687 2 -15 17 5 1500.26 384.977 3 -15 -17 5 1338.27 379.125 1 -14 -17 5 1338.56 373.741 2 -14 -17 5 1352.40 364.327 1 -14 17 5 1146.58 336.296 3 -13 -17 5 911.739 281.522 2 -13 17 5 823.912 260.182 3 -13 -17 5 878.841 258.642 1 -12 -17 5 719.108 245.824 2 -12 17 5 706.587 249.313 3 -12 -17 5 763.228 245.198 1 -11 -17 5 11486.3 931.745 1 -11 17 5 11131.4 948.839 3 -11 -17 5 11534.0 970.428 2 -10 -17 5 112.590 83.9052 1 -10 17 5 114.311 111.120 3 -10 -17 5 107.644 79.2248 2 -9 -17 5 10672.3 791.051 1 -9 17 5 10057.3 884.137 3 -9 -17 5 10805.1 904.494 2 -8 -17 5 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-9 9 17 312.322 301.784 3 -8 9 17 495.618 293.033 3 -7 9 17 267.349 246.803 3 -6 -9 17-591.823 333.744 2 -6 9 17-125.923 161.455 3 -5 -9 17-891.277 503.666 2 -5 9 17-197.926 186.244 3 -10 10 17 416.947 291.013 3 -9 10 17 3645.87 715.321 3 -8 10 17 114.727 123.359 3 -7 10 17 1388.61 374.721 3 -6 -10 17-322.820 346.073 2 -6 10 17 24.4290 158.512 3 -5 -10 17-218.161 330.463 2 -5 10 17 464.647 165.009 3 -3 -10 17-559.720 539.138 2 -10 11 17 171.232 124.502 3 -9 11 17 643.965 265.477 3 -8 11 17 14.1623 118.819 3 -7 11 17-83.6505 164.280 3 -6 -11 17-270.814 252.966 2 -6 11 17-198.794 214.324 3 -5 -11 17-1180.81 472.472 2 -5 11 17-53.9507 84.6783 3 -4 -11 17-954.763 527.219 2 -10 12 17 100.347 107.827 3 -9 12 17 3440.38 673.562 3 -8 12 17 278.175 123.092 3 -7 -12 17 2814.80 598.774 2 -7 12 17 2528.18 540.672 3 -6 -12 17 1160.13 358.744 2 -6 12 17 902.767 329.541 3 -5 -12 17 2213.20 480.639 2 -4 -12 17 32.1461 238.039 2 -3 -12 17-1101.88 498.967 2 -9 13 17-145.290 217.397 3 -8 13 17-135.864 181.037 3 -7 -13 17 124.308 190.895 2 -7 13 17 77.7573 61.1663 3 -6 -13 17-84.6623 94.5008 2 -6 13 17-103.059 166.853 3 -5 -13 17 155.513 23.7242 2 -4 -13 17-506.993 323.677 2 -3 -13 17-1043.79 492.287 2 -9 14 17 227.534 116.873 3 -8 14 17 174.278 101.563 3 -7 -14 17 1286.06 433.955 2 -7 14 17 725.926 281.270 3 -6 -14 17 912.690 387.726 2 -6 14 17 559.326 251.447 3 -5 -14 17 881.413 348.954 2 -4 -14 17-454.850 330.547 2 -3 -14 17-329.784 331.903 2 -8 15 17 260.590 184.863 3 -7 -15 17 1095.58 420.163 2 -7 15 17 476.751 235.693 3 -6 -15 17 1986.48 551.256 2 -6 15 17 892.046 343.145 3 -5 -15 17 1193.01 412.304 2 -4 -15 17 515.110 200.934 2 -8 -16 17 501.656 317.280 2 -8 16 17 118.197 127.928 3 -7 -16 17 1156.05 430.922 2 -7 16 17 960.101 354.075 3 -6 -16 17 702.602 364.133 2 -6 16 17-25.9659 115.961 3 -5 -16 17 495.850 328.335 2 -8 -17 17 880.242 395.398 2 -7 -17 17 790.824 388.581 2 -7 17 17 130.729 72.9469 3 -6 17 17 489.047 257.981 3 -6 18 17 850.614 339.758 3 -10 0 18-231.226 245.002 3 -9 0 18-153.149 201.913 3 -8 0 18 479.840 242.345 3 -7 0 18-151.227 171.399 3 -2 0 18 2294.70 581.168 2 -1 0 18 2482.32 627.653 2 0 0 18 3281.36 717.927 2 -10 1 18 0.88070 175.416 3 -10 -1 18 502.660 205.558 3 -9 1 18-250.530 237.348 3 -9 -1 18-377.815 274.311 3 -8 1 18-274.241 256.546 3 -8 -1 18-304.012 232.773 3 -7 1 18 48.4309 37.1397 3 -7 -1 18-176.812 192.029 3 -3 -1 18 208.877 157.209 2 -2 1 18 146.321 140.559 2 -2 -1 18 21.9037 113.499 2 -1 1 18 225.573 192.442 2 -1 -1 18 24.1215 44.2114 2 0 1 18 388.628 220.848 2 0 -1 18 190.058 157.611 2 -10 2 18 339.177 173.891 3 -10 -2 18 609.507 246.267 3 -9 2 18-23.6955 134.663 3 -9 -2 18-155.508 187.984 3 -8 2 18-91.3232 189.832 3 -8 -2 18-46.3722 138.557 3 -7 2 18 47.0969 97.7076 3 -7 -2 18-102.398 136.556 3 -3 -2 18 9.78200 110.599 2 -2 2 18 80.9583 85.7530 2 -2 -2 18 13.9774 82.5134 2 -1 2 18 308.687 237.604 2 -1 -2 18 198.207 81.8636 2 0 -2 18 95.7586 93.2017 2 -10 3 18 140.281 119.895 3 -10 -3 18 205.448 76.3019 3 -9 3 18-139.123 190.886 3 -9 -3 18 42.8882 45.5811 3 -8 3 18-23.7657 120.030 3 -8 -3 18 40.5218 54.6112 3 -7 3 18-87.6517 145.402 3 -7 -3 18 22.9065 38.1968 3 -3 -3 18 363.278 267.646 2 -2 -3 18 60.1978 110.798 2 -1 -3 18 66.0310 110.838 2 0 -3 18 465.173 287.863 2 -10 4 18 833.600 335.243 3 -10 -4 18 1252.35 443.863 3 -9 4 18 261.322 161.649 3 -9 -4 18 446.421 311.577 3 -8 4 18 688.401 289.514 3 -8 -4 18 688.717 330.266 3 -7 4 18 134.262 152.810 3 -7 -4 18 188.256 157.313 3 -4 -4 18 161.419 168.673 2 -3 -4 18 219.522 100.717 2 -2 -4 18 917.772 373.984 2 -1 -4 18 412.467 213.813 2 -10 5 18 246.617 187.402 3 -10 -5 18 393.889 304.507 3 -9 5 18 38.4890 99.4251 3 -9 -5 18 407.068 328.058 3 -8 5 18 371.651 217.611 3 -8 -5 18 879.883 388.648 3 -7 5 18 121.541 141.705 3 -7 -5 18 396.420 305.464 3 -3 -5 18-100.703 180.131 2 -2 -5 18-116.952 235.784 2 -1 -5 18-100.109 207.631 2 -10 6 18 202.635 205.152 3 -9 6 18 118.603 162.052 3 -8 6 18 90.5276 131.462 3 -7 6 18 156.552 154.028 3 -2 -6 18-12.5323 120.718 2 -1 -6 18 60.3257 130.910 2 -9 7 18 416.014 299.976 3 -8 7 18 997.828 396.379 3 -7 7 18 464.671 285.625 3 -4 -7 18-685.892 688.577 2 -9 8 18 1005.47 427.736 3 -8 8 18 4140.88 766.721 3 -7 8 18 574.148 321.787 3 -9 9 18 695.801 371.702 3 -8 9 18 2656.88 603.618 3 -7 9 18 691.504 299.630 3 -5 -9 18-499.958 532.323 2 -8 10 18 1845.31 487.647 3 -7 10 18 619.156 277.682 3 -5 -10 18-1203.97 612.698 2 -8 11 18-123.321 167.626 3 -7 11 18-191.623 213.144 3 -6 -11 18-942.472 476.309 2 -4 -11 18-1014.54 607.888 2 -8 12 18-199.689 218.170 3 -7 12 18 39.1237 116.764 3 -6 -12 18-587.191 387.997 2 -5 -12 18-1235.84 588.223 2 -7 13 18 344.062 212.373 3 -6 -13 18 302.897 87.7240 2 -7 14 18 73.5873 117.907 3 -8 0 19-354.751 300.381 3 -2 0 19-275.912 249.796 2 -8 1 19-150.112 205.932 3 -8 -1 19-290.845 277.625 3 -8 2 19-11.2180 163.431 3 -8 -2 19-234.748 296.877 3 -8 3 19-72.5730 99.6896 3 -8 -3 19 238.681 193.901 3 -3 -3 19-171.637 209.630 2 -8 4 19 493.416 283.266 3 -8 -4 19 398.304 239.341 3 -3 -4 19 121.936 85.9051 2 -8 5 19 614.401 308.857 3 -8 -5 19 434.943 264.749 3 -8 6 19 333.079 247.729 3 -8 -6 19 482.893 293.369 3 0 0 0 0.00 0.00 0 TITL SBL_96_RT_MO in P2/c REM P2/c (#13 in standard setting) CELL 0.71073 16.011568 29.374226 14.572627 90.0000 105.5616 90.0000 ZERR 92.00 0.000685 0.001032 0.000607 0.0000 0.0046 0.0000 LATT 1 SYMM -x, y,-z+1/2 SFAC C H N O Zn UNIT 92.00 92.00 92.00 92.00 92.00 TREF HKLF 4 END ; _shelx_hkl_checksum 22249