data_uv020 _publ_contact_author_name 'Thomas Magauer' _publ_contact_author_address ; Department Chemie Ludwig-Maximilians Universit\"at Butenandtstra\&se 5-13 (Haus F) D-81377 M\"unchen Bundesrepublik Deutschland ; loop_ _publ_author_name _publ_author_address 'Cedric Hugelshofer' ; Department Chemie Ludwig-Maximilians Universit\"at Butenandtstra\&se 5-13 (Haus F) D-81377 M\"unchen Bundesrepublik Deutschland ; 'Thomas Magauer' ; Department Chemie Ludwig-Maximilians Universit\"at Butenandtstra\&se 5-13 (Haus F) D-81377 M\"unchen Bundesrepublik Deutschland ; _publ_contact_author_email 'thomas.magauer@cup.uni-muenchen.de' _publ_contact_author_fax ? _publ_contact_author_phone ? _publ_requested_journal 'J. Am. Chem. Soc.' _publ_section_title ; A Bioinspired Cyclization Sequence Enables the Asymmetric Total Synthesis of Dictyoxetane ; _publ_section_abstract ? _publ_section_comment ? _audit_update_record 17-Feb-16 _chemical_name_common nl-1865p _chemical_compound_source ? _chemical_absolute_configuration 'syn' _exptl_crystal_description rod _exptl_crystal_colour colourless _exptl_crystal_size_max 0.100 #?# in millimeters _exptl_crystal_size_mid 0.050 #?# in millimeters _exptl_crystal_size_min 0.040 #?# in millimeters _exptl_crystal_density_method 'not measured' _exptl_crystal_density_meas ? _exptl_special_details ; ; _audit_author_name 'P. Mayer' #?# X-ray operator _audit_creation_date ? #?# style: 18-Aug-1998 _diffrn_ambient_temperature 100.(2) #?# in K _diffrn_source_type 'Bruker TXS' _diffrn_source_power 2.5 #?# in kW _diffrn_source_voltage 50 #?# in kV _diffrn_source_current 50 #?# in mA _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'rotating anode (TXS)' _diffrn_radiation_monochromator 'focusing mirrors' _diffrn_radiation_collimation ? _diffrn_measurement_device 'fixed-chi three-circle diffractometer' _diffrn_measurement_device_type 'Bruker D8 Venture TXS' _diffrn_measurement_method 'mix of phi and omega scans' _diffrn_measurement_details ? _diffrn_detector_area_resol_mean 7.4074 _diffrn_special_details ? _diffrn_orient_matrix_type ? _diffrn_orient_matrix_UB_11 ? _diffrn_orient_matrix_UB_12 ? _diffrn_orient_matrix_UB_13 ? _diffrn_orient_matrix_UB_21 ? _diffrn_orient_matrix_UB_22 ? _diffrn_orient_matrix_UB_23 ? _diffrn_orient_matrix_UB_31 ? _diffrn_orient_matrix_UB_32 ? _diffrn_orient_matrix_UB_33 ? _cell_length_a 8.5285(6) _cell_length_b 14.0549(9) _cell_length_c 15.1362(10) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 1814.3(2) _cell_measurement_temperature 100.(2) #?# in K _cell_measurement_reflns_used 7352 _cell_measurement_theta_min 2.7413 _cell_measurement_theta_max 25.3364 _cell_special_details ? _exptl_absorpt_coefficient_mu 0.084 _exptl_absorpt_correction_type Multi-Scan _exptl_absorpt_correction_T_min 0.8239 _exptl_absorpt_correction_T_max 0.9580 _shelx_estimated_absorpt_T_min 0.992 _shelx_estimated_absorpt_T_max 0.997 _exptl_absorpt_process_details ; SADABS-2014/5 - Bruker AXS area detector scaling and absorption correction ; _diffrn_reflns_number 7152 #xl _diffrn_reflns_av_R_equivalents 0.0244 #xl _diffrn_reflns_av_unetI/netI 0.0332 #xl _diffrn_reflns_limit_h_min -8 #xl _diffrn_reflns_limit_h_max 10 #xl _diffrn_reflns_limit_k_min -16 #xl _diffrn_reflns_limit_k_max 16 #xl _diffrn_reflns_limit_l_min -17 #xl _diffrn_reflns_limit_l_max 18 #xl _diffrn_reflns_theta_min 3.101 #xl _diffrn_reflns_theta_max 25.364 #xl _diffrn_measured_fraction_theta_max 0.989 #xl _diffrn_reflns_theta_full 25.242 #xl _diffrn_measured_fraction_theta_full 0.989 #xl _diffrn_reflns_Laue_measured_fraction_max 0.989 #xl _diffrn_reflns_Laue_measured_fraction_full 0.989 #xl _diffrn_reflns_point_group_measured_fraction_max 0.973 #xl _diffrn_reflns_point_group_measured_fraction_full 0.977 #xl _space_group_crystal_system orthorhombic _space_group_name_H-M_alt 'P 21 21 21' _space_group_name_Hall 'P 2ac 2ab' _space_group_IT_number 19 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _reflns_number_total 3234 #xl _reflns_number_gt 2889 #xl _reflns_threshold_expression 'I > 2\s(I)' #xl _reflns_Friedel_coverage 0.709 #xl _reflns_Friedel_fraction_max 0.952 #xl _reflns_Friedel_fraction_full 0.961 #xl _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _refine_ls_structure_factor_coef Fsqd #xl _refine_ls_matrix_type full #xl _refine_ls_weighting_scheme calc #xl _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0354P)^2^+0.6797P] where P=(Fo^2^+2Fc^2^)/3' #xl _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none #xl _refine_ls_extinction_coef . #xl _refine_ls_abs_structure_details ; Flack x determined using 1132 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.6(5) #xl _refine_ls_number_reflns 3234 #xl _refine_ls_number_parameters 234 #xl _refine_ls_number_restraints 0 #xl _refine_ls_R_factor_all 0.0466 #xl _refine_ls_R_factor_gt 0.0367 #xl _refine_ls_wR_factor_ref 0.0916 #xl _refine_ls_wR_factor_gt 0.0847 #xl _refine_ls_goodness_of_fit_ref 1.101 #xl _refine_ls_restrained_S_all 1.101 #xl _refine_ls_shift/su_max 0.000 #xl _refine_ls_shift/su_mean 0.000 #xl _refine_diff_density_max 0.143 #xl _refine_diff_density_min -0.212 #xl _refine_diff_density_rms 0.043 #xl _refine_special_details ; C-H: constr O-H: refall ; _computing_data_collection 'APEX3 (Bruker AXS Inc., 2015)' _computing_cell_refinement 'SAINT V8.35A (Bruker AXS Inc., 2015)' _computing_data_reduction 'SAINT V8.35A (Bruker AXS Inc., 2015)' _computing_structure_solution 'XT, VERSION 2014/4' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics 'shelXle (C.B. Huebschle, rev 740)' _computing_publication_material ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.6217(2) 0.14512(14) 0.24308(12) 0.0227(4) Uani 1 1 d . . . . . H1 H 0.622(5) 0.101(3) 0.215(3) 0.063(14) Uiso 1 1 d . . . . . O2 O -0.0980(2) 0.32425(15) 0.36803(13) 0.0253(5) Uani 1 1 d . . . . . H2 H -0.094(5) 0.273(3) 0.394(3) 0.061(13) Uiso 1 1 d . . . . . O3 O 0.3117(3) 0.36201(15) 0.59533(14) 0.0292(5) Uani 1 1 d . . . . . H3 H 0.261(4) 0.365(3) 0.642(3) 0.047(11) Uiso 1 1 d . . . . . O4 O 0.3712(2) 0.46911(12) 0.37799(12) 0.0211(4) Uani 1 1 d . . . . . C1 C 0.5743(3) 0.22703(19) 0.19003(17) 0.0206(6) Uani 1 1 d . . . . . C2 C 0.4768(3) 0.1946(2) 0.10872(18) 0.0251(6) Uani 1 1 d . . . . . H2A H 0.5127 0.2282 0.0549 0.030 Uiso 1 1 calc R U . . . H2B H 0.4891 0.1253 0.0993 0.030 Uiso 1 1 calc R U . . . C3 C 0.3024(3) 0.2189(2) 0.12798(18) 0.0250(6) Uani 1 1 d . . . . . H3A H 0.2707 0.2777 0.0967 0.030 Uiso 1 1 calc R U . . . H3B H 0.2328 0.1662 0.1094 0.030 Uiso 1 1 calc R U . . . C4 C 0.2955(3) 0.2330(2) 0.22829(17) 0.0225(6) Uani 1 1 d . . . . . C5 C 0.1709(3) 0.3019(2) 0.26092(18) 0.0241(6) Uani 1 1 d . . . . . H5A H 0.0661 0.2738 0.2503 0.029 Uiso 1 1 calc R U . . . H5B H 0.1778 0.3615 0.2262 0.029 Uiso 1 1 calc R U . . . C6 C 0.1865(3) 0.32637(19) 0.36078(17) 0.0191(6) Uani 1 1 d . . . . . H6 H 0.1800 0.2639 0.3922 0.023 Uiso 1 1 calc R U . . . C7 C 0.0364(3) 0.38207(19) 0.38936(18) 0.0220(6) Uani 1 1 d . . . . . C8 C 0.0270(3) 0.4019(2) 0.48812(18) 0.0250(6) Uani 1 1 d . . . . . H8A H -0.0820 0.4209 0.5020 0.030 Uiso 1 1 calc R U . . . H8B H 0.0475 0.3414 0.5197 0.030 Uiso 1 1 calc R U . . . C9 C 0.1356(3) 0.4766(2) 0.52562(18) 0.0240(6) Uani 1 1 d . . . . . H9A H 0.1366 0.5317 0.4849 0.029 Uiso 1 1 calc R U . . . H9B H 0.0919 0.4988 0.5826 0.029 Uiso 1 1 calc R U . . . C10 C 0.3026(3) 0.4452(2) 0.54076(18) 0.0224(6) Uani 1 1 d . . . . . H10 H 0.3572 0.4978 0.5729 0.027 Uiso 1 1 calc R U . . . C11 C 0.4034(3) 0.41962(19) 0.46116(17) 0.0200(6) Uani 1 1 d . . . . . C12 C 0.3517(3) 0.36500(19) 0.38159(17) 0.0195(6) Uani 1 1 d . . . . . C13 C 0.4842(3) 0.30857(19) 0.33800(16) 0.0201(6) Uani 1 1 d . . . . . H13A H 0.5819 0.3464 0.3412 0.024 Uiso 1 1 calc R U . . . H13B H 0.5012 0.2492 0.3718 0.024 Uiso 1 1 calc R U . . . C14 C 0.4527(3) 0.28340(19) 0.24270(16) 0.0189(6) Uani 1 1 d . . . . . H14 H 0.4428 0.3457 0.2113 0.023 Uiso 1 1 calc R U . . . C15 C 0.2780(3) 0.1360(2) 0.27460(19) 0.0269(6) Uani 1 1 d . . . . . H15A H 0.3160 0.1409 0.3355 0.040 Uiso 1 1 calc R U . . . H15B H 0.3395 0.0881 0.2428 0.040 Uiso 1 1 calc R U . . . H15C H 0.1673 0.1173 0.2749 0.040 Uiso 1 1 calc R U . . . C16 C 0.0096(3) 0.4722(2) 0.33520(19) 0.0262(6) Uani 1 1 d . . . . . H16A H 0.1060 0.5101 0.3342 0.039 Uiso 1 1 calc R U . . . H16B H -0.0750 0.5096 0.3620 0.039 Uiso 1 1 calc R U . . . H16C H -0.0195 0.4548 0.2747 0.039 Uiso 1 1 calc R U . . . C17 C 0.5751(3) 0.4181(2) 0.48806(19) 0.0255(6) Uani 1 1 d . . . . . H17A H 0.6096 0.3521 0.4955 0.038 Uiso 1 1 calc R U . . . H17B H 0.5881 0.4525 0.5439 0.038 Uiso 1 1 calc R U . . . H17C H 0.6383 0.4488 0.4421 0.038 Uiso 1 1 calc R U . . . C18 C 0.7243(3) 0.2828(2) 0.16875(18) 0.0225(6) Uani 1 1 d . . . . . H18 H 0.7770 0.2966 0.2264 0.027 Uiso 1 1 calc R U . . . C19 C 0.6960(4) 0.3785(2) 0.1236(2) 0.0329(7) Uani 1 1 d . . . . . H19A H 0.7969 0.4077 0.1087 0.049 Uiso 1 1 calc R U . . . H19B H 0.6379 0.4205 0.1636 0.049 Uiso 1 1 calc R U . . . H19C H 0.6350 0.3686 0.0695 0.049 Uiso 1 1 calc R U . . . C20 C 0.8385(3) 0.2233(2) 0.11421(18) 0.0281(7) Uani 1 1 d . . . . . H20A H 0.9347 0.2598 0.1039 0.042 Uiso 1 1 calc R U . . . H20B H 0.7902 0.2072 0.0574 0.042 Uiso 1 1 calc R U . . . H20C H 0.8638 0.1647 0.1463 0.042 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0274(10) 0.0194(11) 0.0212(10) 0.0005(9) -0.0030(9) 0.0046(9) O2 0.0155(10) 0.0292(11) 0.0311(11) 0.0028(10) -0.0026(9) -0.0031(8) O3 0.0319(11) 0.0321(12) 0.0236(10) 0.0058(9) 0.0082(9) 0.0107(10) O4 0.0214(9) 0.0191(9) 0.0228(9) 0.0008(8) -0.0001(8) -0.0008(8) C1 0.0217(13) 0.0206(13) 0.0195(13) 0.0019(11) -0.0009(11) 0.0045(12) C2 0.0246(15) 0.0286(15) 0.0220(14) -0.0031(12) -0.0030(12) 0.0038(12) C3 0.0219(13) 0.0320(15) 0.0212(13) -0.0037(13) -0.0033(12) 0.0000(13) C4 0.0204(13) 0.0262(15) 0.0208(13) -0.0017(12) -0.0033(11) -0.0018(12) C5 0.0187(13) 0.0301(16) 0.0236(14) -0.0024(12) -0.0039(11) -0.0012(12) C6 0.0181(13) 0.0203(13) 0.0188(13) 0.0012(10) -0.0018(11) -0.0003(11) C7 0.0173(13) 0.0219(13) 0.0269(14) 0.0011(12) -0.0008(11) -0.0024(11) C8 0.0174(14) 0.0300(15) 0.0275(14) -0.0007(12) 0.0029(11) 0.0032(12) C9 0.0207(14) 0.0272(15) 0.0242(13) -0.0020(12) 0.0031(12) 0.0050(12) C10 0.0198(13) 0.0247(14) 0.0228(13) -0.0017(12) -0.0005(11) 0.0021(12) C11 0.0188(13) 0.0225(13) 0.0185(13) 0.0018(11) 0.0008(11) -0.0007(12) C12 0.0187(13) 0.0194(13) 0.0205(13) 0.0020(12) 0.0005(11) -0.0009(11) C13 0.0166(13) 0.0221(14) 0.0214(13) 0.0002(11) -0.0029(11) 0.0011(11) C14 0.0167(13) 0.0189(13) 0.0211(13) 0.0005(11) 0.0002(11) -0.0019(11) C15 0.0255(14) 0.0229(15) 0.0324(15) -0.0038(13) 0.0023(12) -0.0038(13) C16 0.0232(14) 0.0231(15) 0.0322(15) 0.0007(12) -0.0018(13) 0.0042(12) C17 0.0198(14) 0.0319(15) 0.0250(14) -0.0039(13) -0.0032(12) 0.0002(13) C18 0.0179(13) 0.0264(15) 0.0232(13) 0.0012(12) 0.0007(11) 0.0033(12) C19 0.0266(15) 0.0303(16) 0.0420(17) 0.0104(15) 0.0090(14) 0.0016(13) C20 0.0254(15) 0.0339(16) 0.0250(14) -0.0019(14) 0.0036(12) 0.0043(13) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C1 1.461(3) . ? O1 H1 0.76(4) . ? O2 C7 1.442(3) . ? O2 H2 0.82(4) . ? O3 C10 1.434(3) . ? O3 H3 0.82(4) . ? O4 C11 1.464(3) . ? O4 C12 1.474(3) . ? C1 C14 1.530(4) . ? C1 C18 1.535(4) . ? C1 C2 1.554(4) . ? C2 C3 1.553(4) . ? C2 H2A 0.9900 . ? C2 H2B 0.9900 . ? C3 C4 1.532(4) . ? C3 H3A 0.9900 . ? C3 H3B 0.9900 . ? C4 C5 1.520(4) . ? C4 C14 1.532(4) . ? C4 C15 1.541(4) . ? C5 C6 1.556(3) . ? C5 H5A 0.9900 . ? C5 H5B 0.9900 . ? C6 C12 1.542(4) . ? C6 C7 1.562(4) . ? C6 H6 1.0000 . ? C7 C8 1.523(4) . ? C7 C16 1.526(4) . ? C8 C9 1.512(4) . ? C8 H8A 0.9900 . ? C8 H8B 0.9900 . ? C9 C10 1.509(4) . ? C9 H9A 0.9900 . ? C9 H9B 0.9900 . ? C10 C11 1.523(4) . ? C10 H10 1.0000 . ? C11 C12 1.495(4) . ? C11 C17 1.521(4) . ? C12 C13 1.530(4) . ? C13 C14 1.509(3) . ? C13 H13A 0.9900 . ? C13 H13B 0.9900 . ? C14 H14 1.0000 . ? C15 H15A 0.9800 . ? C15 H15B 0.9800 . ? C15 H15C 0.9800 . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? C18 C20 1.526(4) . ? C18 C19 1.527(4) . ? C18 H18 1.0000 . ? C19 H19A 0.9800 . ? C19 H19B 0.9800 . ? C19 H19C 0.9800 . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1 O1 H1 110(3) . . ? C7 O2 H2 111(3) . . ? C10 O3 H3 115(3) . . ? C11 O4 C12 61.16(16) . . ? O1 C1 C14 108.0(2) . . ? O1 C1 C18 106.7(2) . . ? C14 C1 C18 114.2(2) . . ? O1 C1 C2 110.6(2) . . ? C14 C1 C2 101.6(2) . . ? C18 C1 C2 115.5(2) . . ? C3 C2 C1 107.4(2) . . ? C3 C2 H2A 110.2 . . ? C1 C2 H2A 110.2 . . ? C3 C2 H2B 110.2 . . ? C1 C2 H2B 110.2 . . ? H2A C2 H2B 108.5 . . ? C4 C3 C2 104.6(2) . . ? C4 C3 H3A 110.8 . . ? C2 C3 H3A 110.8 . . ? C4 C3 H3B 110.8 . . ? C2 C3 H3B 110.8 . . ? H3A C3 H3B 108.9 . . ? C5 C4 C14 105.7(2) . . ? C5 C4 C3 115.6(2) . . ? C14 C4 C3 99.6(2) . . ? C5 C4 C15 110.4(2) . . ? C14 C4 C15 115.4(2) . . ? C3 C4 C15 109.9(2) . . ? C4 C5 C6 113.4(2) . . ? C4 C5 H5A 108.9 . . ? C6 C5 H5A 108.9 . . ? C4 C5 H5B 108.9 . . ? C6 C5 H5B 108.9 . . ? H5A C5 H5B 107.7 . . ? C12 C6 C5 110.8(2) . . ? C12 C6 C7 121.1(2) . . ? C5 C6 C7 108.0(2) . . ? C12 C6 H6 105.2 . . ? C5 C6 H6 105.2 . . ? C7 C6 H6 105.2 . . ? O2 C7 C8 106.3(2) . . ? O2 C7 C16 103.2(2) . . ? C8 C7 C16 111.6(2) . . ? O2 C7 C6 107.9(2) . . ? C8 C7 C6 114.0(2) . . ? C16 C7 C6 113.0(2) . . ? C9 C8 C7 117.6(2) . . ? C9 C8 H8A 107.9 . . ? C7 C8 H8A 107.9 . . ? C9 C8 H8B 107.9 . . ? C7 C8 H8B 107.9 . . ? H8A C8 H8B 107.2 . . ? C10 C9 C8 115.6(2) . . ? C10 C9 H9A 108.4 . . ? C8 C9 H9A 108.4 . . ? C10 C9 H9B 108.4 . . ? C8 C9 H9B 108.4 . . ? H9A C9 H9B 107.4 . . ? O3 C10 C9 112.2(2) . . ? O3 C10 C11 103.5(2) . . ? C9 C10 C11 118.8(2) . . ? O3 C10 H10 107.3 . . ? C9 C10 H10 107.3 . . ? C11 C10 H10 107.3 . . ? O4 C11 C12 59.74(15) . . ? O4 C11 C17 114.7(2) . . ? C12 C11 C17 119.5(2) . . ? O4 C11 C10 117.6(2) . . ? C12 C11 C10 126.3(2) . . ? C17 C11 C10 109.6(2) . . ? O4 C12 C11 59.11(16) . . ? O4 C12 C13 114.6(2) . . ? C11 C12 C13 113.4(2) . . ? O4 C12 C6 116.4(2) . . ? C11 C12 C6 127.9(2) . . ? C13 C12 C6 113.8(2) . . ? C14 C13 C12 113.7(2) . . ? C14 C13 H13A 108.8 . . ? C12 C13 H13A 108.8 . . ? C14 C13 H13B 108.8 . . ? C12 C13 H13B 108.8 . . ? H13A C13 H13B 107.7 . . ? C13 C14 C1 119.9(2) . . ? C13 C14 C4 113.6(2) . . ? C1 C14 C4 106.3(2) . . ? C13 C14 H14 105.3 . . ? C1 C14 H14 105.3 . . ? C4 C14 H14 105.3 . . ? C4 C15 H15A 109.5 . . ? C4 C15 H15B 109.5 . . ? H15A C15 H15B 109.5 . . ? C4 C15 H15C 109.5 . . ? H15A C15 H15C 109.5 . . ? H15B C15 H15C 109.5 . . ? C7 C16 H16A 109.5 . . ? C7 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C7 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C11 C17 H17A 109.5 . . ? C11 C17 H17B 109.5 . . ? H17A C17 H17B 109.5 . . ? C11 C17 H17C 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C20 C18 C19 110.0(2) . . ? C20 C18 C1 111.4(2) . . ? C19 C18 C1 114.3(2) . . ? C20 C18 H18 106.9 . . ? C19 C18 H18 106.9 . . ? C1 C18 H18 106.9 . . ? C18 C19 H19A 109.5 . . ? C18 C19 H19B 109.5 . . ? H19A C19 H19B 109.5 . . ? C18 C19 H19C 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C18 C20 H20A 109.5 . . ? C18 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C18 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1 C1 C2 C3 104.9(3) . . . . ? C14 C1 C2 C3 -9.6(3) . . . . ? C18 C1 C2 C3 -133.8(2) . . . . ? C1 C2 C3 C4 -18.2(3) . . . . ? C2 C3 C4 C5 150.8(2) . . . . ? C2 C3 C4 C14 38.1(3) . . . . ? C2 C3 C4 C15 -83.5(3) . . . . ? C14 C4 C5 C6 -61.4(3) . . . . ? C3 C4 C5 C6 -170.5(2) . . . . ? C15 C4 C5 C6 64.1(3) . . . . ? C4 C5 C6 C12 55.3(3) . . . . ? C4 C5 C6 C7 -170.0(2) . . . . ? C12 C6 C7 O2 -174.8(2) . . . . ? C5 C6 C7 O2 56.1(3) . . . . ? C12 C6 C7 C8 -57.0(3) . . . . ? C5 C6 C7 C8 173.9(2) . . . . ? C12 C6 C7 C16 71.8(3) . . . . ? C5 C6 C7 C16 -57.4(3) . . . . ? O2 C7 C8 C9 -168.4(2) . . . . ? C16 C7 C8 C9 -56.6(3) . . . . ? C6 C7 C8 C9 72.9(3) . . . . ? C7 C8 C9 C10 -78.9(3) . . . . ? C8 C9 C10 O3 -54.9(3) . . . . ? C8 C9 C10 C11 65.8(3) . . . . ? C12 O4 C11 C17 111.1(3) . . . . ? C12 O4 C11 C10 -118.0(3) . . . . ? O3 C10 C11 O4 155.6(2) . . . . ? C9 C10 C11 O4 30.6(4) . . . . ? O3 C10 C11 C12 84.4(3) . . . . ? C9 C10 C11 C12 -40.7(4) . . . . ? O3 C10 C11 C17 -71.2(3) . . . . ? C9 C10 C11 C17 163.8(2) . . . . ? C11 O4 C12 C13 -103.6(2) . . . . ? C11 O4 C12 C6 120.1(2) . . . . ? C17 C11 C12 O4 -103.0(3) . . . . ? C10 C11 C12 O4 103.6(3) . . . . ? O4 C11 C12 C13 105.6(2) . . . . ? C17 C11 C12 C13 2.6(3) . . . . ? C10 C11 C12 C13 -150.8(2) . . . . ? O4 C11 C12 C6 -101.0(3) . . . . ? C17 C11 C12 C6 156.0(3) . . . . ? C10 C11 C12 C6 2.6(4) . . . . ? C5 C6 C12 O4 92.4(3) . . . . ? C7 C6 C12 O4 -35.5(3) . . . . ? C5 C6 C12 C11 162.6(3) . . . . ? C7 C6 C12 C11 34.6(4) . . . . ? C5 C6 C12 C13 -44.2(3) . . . . ? C7 C6 C12 C13 -172.1(2) . . . . ? O4 C12 C13 C14 -93.5(3) . . . . ? C11 C12 C13 C14 -158.8(2) . . . . ? C6 C12 C13 C14 44.0(3) . . . . ? C12 C13 C14 C1 180.0(2) . . . . ? C12 C13 C14 C4 -52.9(3) . . . . ? O1 C1 C14 C13 48.7(3) . . . . ? C18 C1 C14 C13 -69.9(3) . . . . ? C2 C1 C14 C13 165.1(2) . . . . ? O1 C1 C14 C4 -81.8(2) . . . . ? C18 C1 C14 C4 159.7(2) . . . . ? C2 C1 C14 C4 34.7(3) . . . . ? C5 C4 C14 C13 59.8(3) . . . . ? C3 C4 C14 C13 179.9(2) . . . . ? C15 C4 C14 C13 -62.5(3) . . . . ? C5 C4 C14 C1 -166.2(2) . . . . ? C3 C4 C14 C1 -46.1(3) . . . . ? C15 C4 C14 C1 71.5(3) . . . . ? O1 C1 C18 C20 62.2(3) . . . . ? C14 C1 C18 C20 -178.5(2) . . . . ? C2 C1 C18 C20 -61.2(3) . . . . ? O1 C1 C18 C19 -172.4(2) . . . . ? C14 C1 C18 C19 -53.1(3) . . . . ? C2 C1 C18 C19 64.2(3) . . . . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A O1 H1 O4 0.76(4) 2.32(4) 3.079(3) 177(4) 3_645 O2 H2 O3 0.82(4) 2.06(4) 2.785(3) 146(4) 4_456 O3 H3 O1 0.82(4) 2.11(4) 2.936(3) 173(4) 4_456 _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; _audit_block_code C20H34O4_uv020_magauer _audit_creation_method 'APEX3 v2015.9-RC7' _shelxl_version_number ? _chemical_name_systematic ? _chemical_formula_moiety 'C20 H34 O4' _chemical_formula_sum 'C20 H34 O4' _chemical_formula_weight 338.47 #?# (Cohen, 1996) _chemical_melting_point ? #?# in K! _cell_formula_units_Z 4 #?# adjust to _chemical_formula_[] _exptl_crystal_density_diffrn 1.239 _exptl_crystal_F_000 744 #?# check! _shelx_res_file ; uv020_0m.res created by SHELXL-2014/7 TITL uv020_0m_a.res in P2(1)2(1)2(1) REM Old TITL uv020_0m in P2(1)2(1)2(1) REM SHELXT solution in P2(1)2(1)2(1) REM R1 0.130, Rweak 0.018, Alpha 0.002, Orientation as input REM Flack x = -0.562 ( 0.442 ) from Parsons' quotients REM Formula found by SHELXT: C20 O4 CELL 0.71073 8.5285 14.0549 15.1362 90.000 90.000 90.000 ZERR 4.000 0.0006 0.0009 0.0010 0.000 0.000 0.000 LATT -1 SYMM 1/2-X, -Y, 1/2+Z SYMM -X, 1/2+Y, 1/2-Z SYMM 1/2+X, 1/2-Y, -Z SFAC C H O UNIT 80 136 16 OMIT 0 1 1 OMIT 0 2 0 OMIT 0 0 2 OMIT 1 1 0 OMIT 1 0 1 OMIT 0 1 2 OMIT 0 6 6 OMIT 3 3 0 OMIT 6 3 6 OMIT 0 9 3 TEMP -173.15 SIZE 0.04 0.05 0.10 L.S. 10 BOND $H CONF ACTA HTAB EQIV $1 -x+1, y-1/2, -z+1/2 HTAB O1 O4_$1 EQIV $2 x-1/2, -y+1/2, -z+1 HTAB O2 O3_$2 HTAB O3 O1_$2 LIST 4 FMAP 2 PLAN -20 WGHT 0.035400 0.679700 FVAR 0.20796 O1 3 0.621710 0.145116 0.243077 11.00000 0.02741 0.01942 = 0.02121 0.00052 -0.00296 0.00460 H1 2 0.622430 0.100533 0.214711 11.00000 0.06300 O2 3 -0.097950 0.324253 0.368028 11.00000 0.01551 0.02921 = 0.03112 0.00284 -0.00260 -0.00315 H2 2 -0.094317 0.272709 0.393677 11.00000 0.06086 O3 3 0.311731 0.362012 0.595331 11.00000 0.03186 0.03214 = 0.02356 0.00583 0.00818 0.01070 H3 2 0.260585 0.364665 0.641526 11.00000 0.04677 O4 3 0.371228 0.469108 0.377988 11.00000 0.02139 0.01907 = 0.02277 0.00082 -0.00013 -0.00082 C1 1 0.574295 0.227030 0.190033 11.00000 0.02168 0.02063 = 0.01948 0.00192 -0.00092 0.00453 C2 1 0.476762 0.194589 0.108721 11.00000 0.02465 0.02864 = 0.02203 -0.00315 -0.00296 0.00378 AFIX 23 H2A 2 0.512713 0.228181 0.054919 11.00000 -1.20000 H2B 2 0.489150 0.125294 0.099285 11.00000 -1.20000 AFIX 0 C3 1 0.302414 0.218920 0.127976 11.00000 0.02194 0.03201 = 0.02118 -0.00367 -0.00330 -0.00004 AFIX 23 H3A 2 0.270652 0.277681 0.096662 11.00000 -1.20000 H3B 2 0.232826 0.166227 0.109360 11.00000 -1.20000 AFIX 0 C4 1 0.295476 0.233042 0.228288 11.00000 0.02042 0.02622 = 0.02083 -0.00168 -0.00327 -0.00180 C5 1 0.170877 0.301916 0.260921 11.00000 0.01870 0.03008 = 0.02361 -0.00236 -0.00393 -0.00120 AFIX 23 H5A 2 0.066122 0.273824 0.250258 11.00000 -1.20000 H5B 2 0.177824 0.361456 0.226193 11.00000 -1.20000 AFIX 0 C6 1 0.186534 0.326373 0.360784 11.00000 0.01811 0.02028 = 0.01879 0.00122 -0.00182 -0.00034 AFIX 13 H6 2 0.180004 0.263897 0.392182 11.00000 -1.20000 AFIX 0 C7 1 0.036439 0.382070 0.389356 11.00000 0.01725 0.02187 = 0.02686 0.00108 -0.00079 -0.00241 C8 1 0.026979 0.401854 0.488121 11.00000 0.01743 0.02995 = 0.02752 -0.00067 0.00288 0.00321 AFIX 23 H8A 2 -0.082020 0.420927 0.501995 11.00000 -1.20000 H8B 2 0.047450 0.341412 0.519665 11.00000 -1.20000 AFIX 0 C9 1 0.135581 0.476629 0.525624 11.00000 0.02071 0.02719 = 0.02421 -0.00200 0.00308 0.00503 AFIX 23 H9A 2 0.136595 0.531729 0.484882 11.00000 -1.20000 H9B 2 0.091870 0.498800 0.582612 11.00000 -1.20000 AFIX 0 C10 1 0.302618 0.445201 0.540763 11.00000 0.01979 0.02475 = 0.02277 -0.00170 -0.00049 0.00213 AFIX 13 H10 2 0.357204 0.497788 0.572927 11.00000 -1.20000 AFIX 0 C11 1 0.403352 0.419621 0.461156 11.00000 0.01885 0.02254 = 0.01847 0.00175 0.00076 -0.00069 C12 1 0.351732 0.365000 0.381590 11.00000 0.01871 0.01944 = 0.02050 0.00198 0.00054 -0.00090 C13 1 0.484160 0.308568 0.338003 11.00000 0.01662 0.02214 = 0.02141 0.00018 -0.00287 0.00107 AFIX 23 H13A 2 0.581944 0.346369 0.341209 11.00000 -1.20000 H13B 2 0.501175 0.249163 0.371816 11.00000 -1.20000 AFIX 0 C14 1 0.452663 0.283403 0.242704 11.00000 0.01669 0.01885 = 0.02113 0.00049 0.00022 -0.00192 AFIX 13 H14 2 0.442784 0.345734 0.211336 11.00000 -1.20000 AFIX 0 C15 1 0.277991 0.136000 0.274604 11.00000 0.02552 0.02287 = 0.03244 -0.00378 0.00226 -0.00377 AFIX 137 H15A 2 0.316018 0.140946 0.335529 11.00000 -1.50000 H15B 2 0.339522 0.088074 0.242830 11.00000 -1.50000 H15C 2 0.167313 0.117257 0.274912 11.00000 -1.50000 AFIX 0 C16 1 0.009570 0.472208 0.335202 11.00000 0.02318 0.02307 = 0.03221 0.00067 -0.00175 0.00421 AFIX 137 H16A 2 0.106021 0.510092 0.334194 11.00000 -1.50000 H16B 2 -0.075035 0.509567 0.361961 11.00000 -1.50000 H16C 2 -0.019530 0.454842 0.274679 11.00000 -1.50000 AFIX 0 C17 1 0.575122 0.418128 0.488063 11.00000 0.01978 0.03189 = 0.02498 -0.00387 -0.00317 0.00021 AFIX 137 H17A 2 0.609644 0.352109 0.495519 11.00000 -1.50000 H17B 2 0.588134 0.452497 0.543917 11.00000 -1.50000 H17C 2 0.638289 0.448815 0.442092 11.00000 -1.50000 AFIX 0 C18 1 0.724308 0.282818 0.168748 11.00000 0.01788 0.02641 = 0.02317 0.00120 0.00066 0.00333 AFIX 13 H18 2 0.777048 0.296590 0.226352 11.00000 -1.20000 AFIX 0 C19 1 0.695983 0.378483 0.123601 11.00000 0.02658 0.03027 = 0.04199 0.01043 0.00895 0.00160 AFIX 137 H19A 2 0.796886 0.407729 0.108696 11.00000 -1.50000 H19B 2 0.637939 0.420469 0.163631 11.00000 -1.50000 H19C 2 0.634953 0.368628 0.069511 11.00000 -1.50000 AFIX 0 C20 1 0.838451 0.223300 0.114210 11.00000 0.02536 0.03385 = 0.02501 -0.00193 0.00355 0.00430 AFIX 137 H20A 2 0.934659 0.259780 0.103913 11.00000 -1.50000 H20B 2 0.790159 0.207171 0.057401 11.00000 -1.50000 H20C 2 0.863837 0.164728 0.146294 11.00000 -1.50000 REM ##### AFIX 0 HKLF 4 REM uv020_0m_a.res in P2(1)2(1)2(1) REM R1 = 0.0367 for 2889 Fo > 4sig(Fo) and 0.0466 for all 3234 data REM 234 parameters refined using 0 restraints END WGHT 0.0354 0.6797 REM Instructions for potential hydrogen bonds HTAB O1 O4_$1 HTAB O2 O3_$2 HTAB O3 O1_$2 HTAB C2 O4_$1 HTAB C16 O4 EQIV $3 x+1, y, z HTAB C18 O2_$3 REM Highest difference peak 0.143, deepest hole -0.212, 1-sigma level 0.043 Q1 1 0.6576 0.3374 0.4374 11.00000 0.05 0.14 Q2 1 0.3658 0.3757 0.4386 11.00000 0.05 0.14 Q3 1 0.3732 0.4090 0.2427 11.00000 0.05 0.14 Q4 1 0.5862 0.3080 0.3610 11.00000 0.05 0.14 Q5 1 -0.1207 0.1228 0.2651 11.00000 0.05 0.14 Q6 1 0.4719 0.2988 0.2949 11.00000 0.05 0.14 Q7 1 -0.2051 0.2590 0.2970 11.00000 0.05 0.13 Q8 1 0.0344 0.2890 0.5455 11.00000 0.05 0.13 Q9 1 0.3721 0.2602 0.2421 11.00000 0.05 0.13 Q10 1 0.1040 0.5197 0.6237 11.00000 0.05 0.13 Q11 1 -0.0709 0.2178 0.4210 11.00000 0.05 0.13 Q12 1 0.4744 0.2054 0.3904 11.00000 0.05 0.13 Q13 1 0.0550 0.3691 0.0413 11.00000 0.05 0.13 Q14 1 0.7426 0.3064 0.2582 11.00000 0.05 0.12 Q15 1 0.5914 0.3803 0.5591 11.00000 0.05 0.12 Q16 1 0.3861 0.0610 0.2577 11.00000 0.05 0.12 Q17 1 0.3970 0.3444 0.1879 11.00000 0.05 0.12 Q18 1 -0.0317 0.1786 0.2594 11.00000 0.05 0.12 Q19 1 -0.1380 0.3604 0.0003 11.00000 0.05 0.12 Q20 1 0.1487 0.2981 0.5940 11.00000 0.05 0.12 ; _shelx_res_checksum 98904 _shelx_hkl_file ; 5 0 0 -0.01 0.09 6 0 0 29.63 0.80 7 0 0 -0.03 0.13 8 0 0 3.62 0.30 9 0 0 0.01 0.16 10 0 0 12.53 0.55 0 -1 0 -0.01 0.01 1 -1 0 14.25 1.17 2 -1 0 36.70 0.81 3 -1 0 93.14 2.00 4 -1 0 12.63 0.38 5 -1 0 42.42 1.02 6 -1 0 5.00 0.27 6 1 0 5.27 0.29 7 -1 0 7.43 0.37 7 1 0 7.38 0.38 8 -1 0 0.13 0.15 8 1 0 0.13 0.16 9 -1 0 15.70 0.59 9 1 0 16.29 0.62 10 1 0 1.57 0.25 10 -1 0 2.12 0.31 0 -2 0 5.07 1.09 1 2 0 34.53 0.79 1 -2 0 34.07 0.74 -2 2 0 54.33 1.16 2 -2 0 53.40 1.16 3 -2 0 72.18 1.56 4 -2 0 67.36 1.50 5 -2 0 0.04 0.09 6 -2 0 0.34 0.12 7 -2 0 1.32 0.19 8 2 0 23.53 0.77 8 -2 0 24.21 0.72 9 2 0 1.72 0.25 9 -2 0 1.59 0.22 10 -2 0 0.06 0.17 10 2 0 0.20 0.18 0 3 0 0.49 0.10 1 -3 0 8.46 0.24 -1 3 0 8.21 0.24 1 3 0 7.93 0.29 -2 3 0 10.26 0.28 2 -3 0 9.75 0.27 -3 3 0 12.51 0.35 3 -3 0 12.30 0.34 4 -3 0 33.24 0.79 5 -3 0 2.35 0.19 6 -3 0 19.77 0.57 7 -3 0 39.87 1.01 8 -3 0 13.46 0.50 9 -3 0 0.69 0.18 9 3 0 0.69 0.20 10 -3 0 3.15 0.33 10 3 0 3.16 0.35 0 -4 0 15.49 0.44 0 4 0 16.46 0.44 -1 -4 0 86.88 1.89 1 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0.31 5 3 14 1.20 0.29 6 -3 14 0.62 0.32 6 3 -14 0.42 0.27 6 3 14 0.90 0.29 0 -4 14 1.62 0.34 0 4 -14 1.56 0.27 0 4 14 1.71 0.25 -1 4 14 0.30 0.22 1 4 -14 0.05 0.21 1 -4 14 0.33 0.28 -1 4 -14 0.05 0.21 1 4 14 0.11 0.21 -1 -4 14 0.24 0.30 2 -4 14 0.77 0.30 2 4 -14 0.88 0.25 -2 4 14 0.94 0.23 -2 4 -14 0.95 0.25 -2 -4 14 0.49 0.31 2 4 14 0.86 0.24 3 4 -14 5.51 0.44 3 -4 14 5.70 0.51 3 4 14 5.71 0.44 -3 -4 14 5.36 0.52 4 -4 14 5.70 0.52 4 4 -14 5.39 0.46 -4 -4 14 6.36 0.53 4 4 14 6.43 0.48 5 -4 14 0.30 0.29 5 4 -14 0.23 0.27 5 4 14 0.72 0.28 -5 -4 14 1.18 0.31 6 4 -14 -0.07 0.27 6 4 14 0.33 0.28 0 -5 14 9.61 0.60 0 5 -14 9.43 0.52 0 5 14 9.61 0.46 -1 5 14 0.57 0.21 1 -5 14 0.40 0.30 1 5 -14 0.47 0.24 -1 -5 14 0.46 0.31 -1 5 -14 0.71 0.25 1 5 14 0.59 0.22 -2 5 14 1.47 0.23 2 5 -14 1.78 0.30 2 -5 14 1.94 0.35 -2 -5 14 1.53 0.35 2 5 14 1.84 0.27 3 -5 14 1.37 0.33 3 5 -14 1.29 0.30 -3 -5 14 1.43 0.36 3 5 14 1.27 0.26 4 -5 14 4.13 0.49 4 5 -14 3.57 0.44 4 5 14 4.26 0.43 -4 -5 14 4.17 0.49 5 -5 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0.59 -1 -9 14 4.81 0.59 1 9 14 5.83 0.40 2 -9 14 1.75 0.40 2 9 14 2.54 0.36 -2 -9 14 1.98 0.42 3 -9 14 -0.03 0.35 3 9 14 0.68 0.25 -3 -9 14 0.39 0.35 0 10 14 -0.15 0.18 0 -10 14 -0.38 0.33 1 -10 14 1.36 0.40 -1 -10 14 1.81 0.43 1 10 14 1.66 0.26 2 10 14 0.78 0.25 -2 -10 14 0.82 0.38 0 0 15 0.03 0.25 0 0 -15 0.42 0.20 -1 0 -15 7.03 0.45 -1 0 15 6.34 0.49 1 0 15 5.90 0.48 1 0 -15 6.88 0.41 2 0 15 -0.08 0.24 -2 0 15 -0.26 0.25 -2 0 -15 0.17 0.21 2 0 -15 0.28 0.20 3 0 15 0.49 0.27 3 0 -15 0.47 0.20 -3 0 15 0.24 0.26 -4 0 15 8.20 0.49 4 0 15 7.25 0.53 4 0 -15 7.45 0.42 -5 0 15 1.00 0.23 5 0 15 0.24 0.26 5 0 -15 0.27 0.20 0 1 15 0.31 0.25 0 1 -15 0.41 0.21 0 -1 -15 0.67 0.22 0 -1 15 0.32 0.27 -1 1 15 0.26 0.25 1 -1 15 0.61 0.27 1 1 -15 0.73 0.22 -1 -1 -15 1.00 0.23 -1 -1 15 0.42 0.28 -1 1 -15 0.61 0.22 1 -1 -15 0.63 0.21 1 1 15 1.06 0.27 2 -1 15 5.01 0.47 -2 1 15 4.68 0.44 2 1 -15 5.36 0.40 -2 -1 -15 5.76 0.43 2 1 15 4.60 0.44 -2 -1 15 4.15 0.45 -2 1 -15 5.16 0.43 2 -1 -15 5.72 0.37 -3 1 15 1.58 0.29 3 -1 15 1.45 0.31 3 1 -15 1.87 0.27 3 -1 -15 2.03 0.29 3 1 15 1.39 0.30 -3 -1 15 1.71 0.31 4 1 -15 1.21 0.25 -4 1 15 1.36 0.26 4 -1 15 0.66 0.28 -4 -1 15 1.11 0.29 4 -1 -15 1.31 0.21 4 1 15 0.79 0.27 5 1 -15 0.25 0.23 5 -1 15 -0.03 0.27 5 -1 -15 0.20 0.17 5 1 15 0.03 0.25 -5 -1 15 0.68 0.24 0 2 15 0.10 0.23 0 -2 -15 0.41 0.19 0 -2 15 -0.05 0.27 0 2 -15 0.34 0.21 -1 2 15 1.01 0.26 -1 -2 -15 1.43 0.25 1 2 -15 1.34 0.26 1 -2 15 1.11 0.31 1 -2 -15 1.56 0.23 -1 2 -15 1.13 0.25 -1 -2 15 1.11 0.31 1 2 15 0.92 0.26 -2 2 15 3.82 0.40 2 2 -15 3.93 0.38 2 -2 15 4.19 0.46 -2 -2 -15 5.04 0.41 -2 -2 15 3.87 0.46 2 -2 -15 4.82 0.35 2 2 15 3.81 0.41 -3 2 15 2.51 0.37 3 2 -15 3.13 0.37 3 -2 15 2.45 0.36 -3 -2 15 3.13 0.45 3 2 15 2.90 0.40 3 -2 -15 3.28 0.30 4 -2 15 3.29 0.45 -4 2 15 3.50 0.34 4 2 -15 2.84 0.37 4 -2 -15 3.23 0.30 4 2 15 2.28 0.34 -4 -2 15 4.07 0.45 5 -2 15 0.43 0.29 5 2 -15 0.14 0.24 5 2 15 0.52 0.27 -5 -2 15 0.86 0.27 0 -3 15 7.79 0.56 0 3 -15 8.99 0.50 0 3 15 8.14 0.48 0 -3 -15 9.25 0.46 1 -3 15 11.07 0.62 1 3 -15 12.27 0.56 -1 3 15 11.56 0.53 -1 -3 -15 12.94 0.55 -1 -3 15 10.85 0.62 1 -3 -15 13.47 0.52 -1 3 -15 12.19 0.58 1 3 15 11.31 0.55 -2 3 15 3.62 0.38 2 -3 15 3.90 0.47 2 3 -15 4.06 0.40 2 -3 -15 4.62 0.33 -2 -3 15 3.53 0.48 2 3 15 4.02 0.41 -3 3 15 3.84 0.38 3 3 -15 5.37 0.44 3 -3 15 4.72 0.50 -3 -3 15 4.68 0.51 3 3 15 5.01 0.45 3 -3 -15 5.93 0.33 4 3 -15 2.13 0.31 4 -3 15 2.13 0.36 -4 -3 15 2.72 0.36 4 3 15 2.21 0.33 5 3 -15 -0.01 0.25 5 -3 15 0.22 0.28 5 3 15 0.23 0.27 -5 -3 15 0.97 0.29 0 4 -15 1.09 0.27 0 4 15 0.92 0.25 0 -4 15 0.74 0.33 1 -4 15 0.12 0.29 -1 4 15 -0.20 0.21 1 4 -15 0.11 0.22 1 4 15 -0.02 0.22 -1 -4 15 -0.26 0.29 -2 4 15 10.02 0.47 2 -4 15 9.84 0.62 2 4 -15 11.10 0.56 -2 -4 15 10.22 0.62 2 4 15 10.66 0.54 3 4 -15 9.71 0.54 3 -4 15 9.80 0.62 3 4 15 9.33 0.54 -3 -4 15 9.77 0.62 4 -4 15 1.81 0.35 4 4 -15 1.56 0.30 4 4 15 1.69 0.30 -4 -4 15 1.62 0.34 5 4 -15 0.42 0.29 5 -4 15 0.24 0.42 5 4 15 0.49 0.26 0 5 15 0.30 0.22 0 -5 15 -0.22 0.30 -1 5 15 0.66 0.23 1 -5 15 0.67 0.33 -1 -5 15 0.88 0.33 1 5 15 0.74 0.24 -2 5 15 2.45 0.33 2 5 -15 2.86 0.41 2 -5 15 3.05 0.42 2 5 15 3.36 0.39 -2 -5 15 2.72 0.40 3 5 -15 7.05 0.61 3 -5 15 6.77 0.58 -3 -5 15 7.27 0.59 3 5 15 6.94 0.49 4 -5 15 4.07 0.52 -4 -5 15 4.87 0.52 4 5 15 3.84 0.44 -5 -5 15 0.29 0.29 0 -6 15 4.84 0.55 0 6 15 4.93 0.39 1 -6 15 3.61 0.54 -1 6 15 4.71 0.37 -1 -6 15 4.23 0.54 1 6 15 4.92 0.40 2 -6 15 0.76 0.35 2 6 15 0.86 0.25 -2 -6 15 0.98 0.36 3 -6 15 2.55 0.41 3 6 15 3.52 0.41 -3 -6 15 2.51 0.42 4 -6 15 6.02 0.62 -4 -6 15 6.85 0.58 0 7 15 -0.12 0.20 0 -7 15 -0.01 0.33 -1 7 15 0.63 0.22 1 -7 15 0.58 0.35 -1 -7 15 0.55 0.36 1 7 15 0.55 0.23 2 -7 15 0.81 0.37 2 7 15 1.13 0.27 -2 -7 15 1.15 0.38 3 -7 15 3.78 0.56 3 7 15 4.81 0.44 -3 -7 15 3.74 0.48 -4 -7 15 17.37 0.82 0 8 15 4.53 0.37 0 -8 15 4.34 0.58 -1 8 15 1.17 0.23 1 -8 15 1.36 0.39 -1 -8 15 1.56 0.40 1 8 15 1.40 0.26 2 -8 15 -0.60 0.32 2 8 15 0.08 0.23 -2 -8 15 -0.09 0.35 3 8 15 1.61 0.30 -3 -8 15 1.74 0.40 0 9 15 0.49 0.22 0 -9 15 0.50 0.39 1 -9 15 5.04 0.64 1 9 15 5.91 0.43 -1 -9 15 5.23 0.62 -2 -9 15 -0.01 0.36 0 0 16 6.46 0.50 0 0 -16 7.75 0.47 -1 0 -16 8.29 0.50 1 0 -16 7.86 0.46 1 0 16 6.74 0.51 -1 0 16 6.81 0.51 2 0 -16 1.12 0.25 -2 0 16 0.45 0.30 2 0 16 0.77 0.29 3 0 -16 5.51 0.39 3 0 16 4.67 0.49 -3 0 16 4.23 0.46 4 0 -16 14.37 0.57 -4 0 16 14.43 0.61 4 0 16 12.01 0.67 0 1 16 0.39 0.27 0 -1 16 0.43 0.29 0 -1 -16 0.65 0.24 0 1 -16 0.56 0.23 -1 1 16 0.93 0.30 -1 -1 -16 1.28 0.26 1 -1 16 0.77 0.29 1 1 -16 1.11 0.26 1 -1 -16 1.14 0.25 -1 1 -16 1.20 0.27 1 1 16 0.65 0.27 -1 -1 16 0.47 0.30 2 -1 16 2.38 0.36 2 1 -16 3.45 0.37 -2 1 16 2.63 0.34 2 -1 -16 3.49 0.35 -2 -1 16 2.11 0.34 2 1 16 2.10 0.33 3 -1 16 0.31 0.28 3 1 -16 0.31 0.23 -3 1 16 0.48 0.26 3 1 16 0.53 0.28 -3 -1 16 0.23 0.28 3 -1 -16 0.89 0.22 -4 1 16 1.24 0.27 4 -1 16 1.13 0.31 4 1 -16 0.96 0.25 4 1 16 0.55 0.28 -4 -1 16 1.48 0.31 4 -1 -16 1.27 0.23 0 -2 16 6.06 0.53 0 2 -16 7.09 0.47 0 2 16 5.93 0.47 0 -2 -16 8.41 0.47 1 -2 16 3.16 0.46 1 2 -16 2.79 0.38 -1 -2 -16 3.24 0.38 -1 2 16 2.54 0.33 1 -2 -16 3.42 0.35 -1 -2 16 2.49 0.38 1 2 16 2.28 0.33 2 2 -16 0.24 0.24 -2 2 16 -0.30 0.25 2 -2 16 0.09 0.28 2 2 16 -0.11 0.25 -2 -2 16 0.14 0.29 2 -2 -16 0.32 0.19 3 -2 16 3.51 0.48 3 2 -16 3.89 0.42 -3 2 16 3.16 0.40 3 2 16 3.19 0.43 3 -2 -16 4.06 0.35 -3 -2 16 3.48 0.48 4 2 -16 1.07 0.27 -4 2 16 1.36 0.24 4 -2 16 0.64 0.31 -4 -2 16 1.30 0.31 4 2 16 0.74 0.28 4 -2 -16 1.39 0.22 0 -3 16 -0.69 0.28 0 -3 -16 0.36 0.21 0 3 16 -0.13 0.24 1 3 -16 0.15 0.23 1 -3 16 -0.03 0.29 -1 3 16 0.03 0.24 1 3 16 0.31 0.25 -1 -3 16 -0.04 0.31 1 -3 -16 0.61 0.21 2 3 -16 1.66 0.30 2 -3 16 1.34 0.34 -2 3 16 1.01 0.27 -2 -3 16 1.32 0.35 2 -3 -16 2.04 0.30 2 3 16 1.03 0.28 -3 3 16 -0.33 0.22 3 3 -16 -0.05 0.24 3 -3 16 0.08 0.29 -3 -3 16 -0.45 0.29 3 -3 -16 0.17 0.18 3 3 16 0.23 0.26 4 3 -16 0.07 0.25 4 -3 16 0.17 0.30 4 3 16 0.33 0.27 -4 -3 16 0.56 0.30 0 4 16 -0.48 0.22 0 -4 16 -0.61 0.29 -1 4 16 3.49 0.40 1 -4 16 3.71 0.52 1 4 16 4.37 0.42 -1 -4 16 3.43 0.43 2 -4 16 0.14 0.30 -2 4 16 0.21 0.24 2 4 16 0.17 0.24 -2 -4 16 0.28 0.32 3 -4 16 1.60 0.37 -3 -4 16 2.09 0.39 3 4 16 1.81 0.31 4 -4 16 5.23 0.65 -4 -4 16 5.31 0.53 4 4 16 5.39 0.50 0 -5 16 1.43 0.38 0 5 16 1.09 0.26 1 -5 16 0.88 0.36 -1 5 16 0.67 0.25 -1 -5 16 1.02 0.37 1 5 16 1.01 0.27 2 -5 16 2.38 0.41 -2 5 16 2.10 0.28 -2 -5 16 1.94 0.39 2 5 16 2.80 0.39 3 -5 16 0.85 0.36 -3 -5 16 0.43 0.34 3 5 16 0.52 0.27 0 6 16 0.00 0.23 0 -6 16 -0.07 0.33 -1 6 16 0.24 0.22 1 -6 16 0.21 0.34 -1 -6 16 0.21 0.35 1 6 16 0.13 0.23 2 -6 16 0.36 0.36 2 6 16 0.69 0.27 -2 -6 16 0.52 0.36 3 -6 16 -0.67 0.50 -3 -6 16 -0.15 0.34 3 6 16 -0.42 0.23 0 7 16 1.30 0.26 0 -7 16 0.61 0.38 -1 7 16 -0.32 0.20 1 -7 16 -0.39 0.34 -1 -7 16 -0.43 0.33 1 7 16 -0.12 0.23 2 -7 16 5.38 0.71 2 7 16 5.37 0.46 -2 -7 16 5.13 0.61 0 8 16 -0.08 0.22 0 -8 16 0.11 0.37 0 0 17 -0.13 0.26 0 0 -17 0.41 0.25 1 0 17 0.23 0.28 -1 0 17 0.11 0.30 2 0 17 -0.51 0.27 -2 0 17 -0.50 0.26 2 0 -17 -0.07 0.21 3 0 17 1.76 0.36 -3 0 17 2.03 0.34 0 -1 17 8.53 0.59 0 1 17 8.43 0.55 1 1 -17 0.20 0.24 1 -1 17 -0.19 0.29 1 -1 -17 0.20 0.24 -1 -1 17 0.04 0.31 1 1 17 0.01 0.28 2 -1 17 2.36 0.38 -2 1 17 2.39 0.35 2 1 17 2.34 0.36 -2 -1 17 2.84 0.38 -3 1 17 10.45 0.57 3 -1 17 9.25 0.64 3 1 -17 12.01 0.57 -3 -1 17 10.87 0.62 3 -1 -17 13.09 0.54 3 1 17 9.84 0.62 0 -2 17 3.81 0.52 0 2 17 4.50 0.47 0 -2 -17 5.94 0.45 1 -2 17 1.25 0.35 -1 -2 -17 1.88 0.38 -1 2 17 1.19 0.30 1 -2 -17 2.08 0.29 1 2 17 0.82 0.29 -1 -2 17 1.39 0.36 -2 2 17 5.86 0.48 2 -2 17 6.48 0.56 2 2 -17 7.80 0.50 -2 -2 17 6.35 0.56 2 2 17 7.29 0.54 -3 2 17 -0.36 0.25 3 -2 17 -0.28 0.30 3 2 -17 -0.14 0.24 3 2 17 -0.24 0.27 3 -2 -17 0.31 0.20 -3 -2 17 -0.35 0.29 0 -3 17 6.24 0.59 0 3 17 6.52 0.50 0 -3 -17 8.85 0.50 1 -3 17 0.47 0.34 -1 3 17 0.69 0.28 -1 -3 17 0.95 0.36 1 3 17 0.55 0.28 2 -3 17 0.89 0.35 -2 3 17 0.57 0.28 2 -3 -17 1.52 0.25 -2 -3 17 0.77 0.34 2 3 17 0.81 0.30 -3 3 17 -0.02 0.25 3 -3 17 -0.10 0.31 3 3 17 0.17 0.28 -3 -3 17 0.46 0.34 0 4 17 -0.16 0.25 0 -4 17 -0.69 0.31 1 -4 17 0.49 0.36 -1 4 17 0.94 0.28 -1 -4 17 0.85 0.36 1 4 17 0.62 0.28 -2 4 17 0.07 0.26 2 -4 17 0.44 0.34 2 4 17 0.60 0.28 -2 -4 17 0.55 0.35 0 5 17 0.38 0.26 0 -5 17 0.45 0.35 1 -5 17 0.73 0.38 -1 5 17 1.07 0.27 1 5 17 0.68 0.28 -1 -5 17 1.14 0.38 -2 5 17 2.27 0.31 2 -5 17 2.80 0.45 2 5 17 1.68 0.31 -2 -5 17 1.98 0.41 0 -6 17 -0.01 0.36 0 6 17 -0.14 0.24 0 0 18 2.43 0.39 1 0 18 4.25 0.52 -1 0 18 4.17 0.52 0 -1 18 6.94 0.59 0 1 18 7.65 0.56 1 -1 18 3.89 0.52 -1 1 18 4.25 0.50 -1 -1 18 3.81 0.52 1 1 18 4.73 0.51 1 -2 18 0.14 0.34 -1 2 18 0.20 0.30 -1 -2 18 -0.14 0.33 1 2 18 0.11 0.30 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 53090 data_uv033 _audit_update_record 22-Feb-16 _chemical_name_common NL-1882p _chemical_compound_source ? _chemical_absolute_configuration 'syn' _exptl_crystal_description rod _exptl_crystal_colour colourless _exptl_crystal_size_max 0.100 #?# in millimeters _exptl_crystal_size_mid 0.030 #?# in millimeters _exptl_crystal_size_min 0.020 #?# in millimeters _exptl_crystal_density_method 'not measured' _exptl_crystal_density_meas ? _exptl_special_details ; ; _audit_author_name 'P. Mayer' #?# X-ray operator _audit_creation_date ? #?# style: 18-Aug-1998 _diffrn_ambient_temperature 100.(2) #?# in K _diffrn_source_type 'Bruker TXS' _diffrn_source_power 2.5 #?# in kW _diffrn_source_voltage 50 #?# in kV _diffrn_source_current 50 #?# in mA _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'rotating anode (TXS)' _diffrn_radiation_monochromator 'focusing mirrors' _diffrn_radiation_collimation ? _diffrn_measurement_device 'fixed-chi three-circle diffractometer' _diffrn_measurement_device_type 'Bruker D8 Venture TXS' _diffrn_measurement_method 'mix of phi and omega scans' _diffrn_measurement_details ? _diffrn_detector_area_resol_mean 7.4074 _diffrn_special_details ? _diffrn_orient_matrix_type ? _diffrn_orient_matrix_UB_11 ? _diffrn_orient_matrix_UB_12 ? _diffrn_orient_matrix_UB_13 ? _diffrn_orient_matrix_UB_21 ? _diffrn_orient_matrix_UB_22 ? _diffrn_orient_matrix_UB_23 ? _diffrn_orient_matrix_UB_31 ? _diffrn_orient_matrix_UB_32 ? _diffrn_orient_matrix_UB_33 ? _cell_length_a 6.3848(4) _cell_length_b 9.4448(7) _cell_length_c 28.5710(19) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 1722.9(2) _cell_measurement_temperature 100.(2) #?# in K _cell_measurement_reflns_used 9984 _cell_measurement_theta_min 3.0376 _cell_measurement_theta_max 26.3794 _cell_special_details ? _exptl_absorpt_coefficient_mu 0.081 _exptl_absorpt_correction_type Multi-Scan _exptl_absorpt_correction_T_min 0.8980 _exptl_absorpt_correction_T_max 0.9585 _shelx_estimated_absorpt_T_min 0.992 _shelx_estimated_absorpt_T_max 0.998 _exptl_absorpt_process_details ; SADABS-2014/5 - Bruker AXS area detector scaling and absorption correction ; _diffrn_reflns_number 31378 #xl _diffrn_reflns_av_R_equivalents 0.0372 #xl _diffrn_reflns_av_unetI/netI 0.0206 #xl _diffrn_reflns_limit_h_min -7 #xl _diffrn_reflns_limit_h_max 7 #xl _diffrn_reflns_limit_k_min -11 #xl _diffrn_reflns_limit_k_max 11 #xl _diffrn_reflns_limit_l_min -35 #xl _diffrn_reflns_limit_l_max 35 #xl _diffrn_reflns_theta_min 3.038 #xl _diffrn_reflns_theta_max 26.405 #xl _diffrn_measured_fraction_theta_max 0.994 #xl _diffrn_reflns_theta_full 25.242 #xl _diffrn_measured_fraction_theta_full 0.994 #xl _diffrn_reflns_Laue_measured_fraction_max 0.994 #xl _diffrn_reflns_Laue_measured_fraction_full 0.994 #xl _diffrn_reflns_point_group_measured_fraction_max 0.995 #xl _diffrn_reflns_point_group_measured_fraction_full 0.996 #xl _space_group_crystal_system orthorhombic _space_group_name_H-M_alt 'P 21 21 21' _space_group_name_Hall 'P 2ac 2ab' _space_group_IT_number 19 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _reflns_number_total 3507 #xl _reflns_number_gt 3373 #xl _reflns_threshold_expression 'I > 2\s(I)' #xl _reflns_Friedel_coverage 0.714 #xl _reflns_Friedel_fraction_max 0.998 #xl _reflns_Friedel_fraction_full 0.999 #xl _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _refine_ls_structure_factor_coef Fsqd #xl _refine_ls_matrix_type full #xl _refine_ls_weighting_scheme calc #xl _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0383P)^2^+0.6304P] where P=(Fo^2^+2Fc^2^)/3' #xl _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none #xl _refine_ls_extinction_coef . #xl _refine_ls_abs_structure_details ; Flack x determined using 1359 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.1(3) #xl _refine_ls_number_reflns 3507 #xl _refine_ls_number_parameters 217 #xl _refine_ls_number_restraints 0 #xl _refine_ls_R_factor_all 0.0361 #xl _refine_ls_R_factor_gt 0.0338 #xl _refine_ls_wR_factor_ref 0.0856 #xl _refine_ls_wR_factor_gt 0.0843 #xl _refine_ls_goodness_of_fit_ref 1.102 #xl _refine_ls_restrained_S_all 1.102 #xl _refine_ls_shift/su_max 0.000 #xl _refine_ls_shift/su_mean 0.000 #xl _refine_diff_density_max 0.263 #xl _refine_diff_density_min -0.183 #xl _refine_diff_density_rms 0.040 #xl _refine_special_details ; C-H: constr O-H: refall ; _computing_data_collection 'APEX3 (Bruker AXS Inc., 2015)' _computing_cell_refinement 'SAINT V8.35A (Bruker AXS Inc., 2015)' _computing_data_reduction 'SAINT V8.35A (Bruker AXS Inc., 2015)' _computing_structure_solution 'XT, VERSION 2014/4' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics 'shelXle (C.B. Huebschle, rev 740)' _computing_publication_material ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.4406(2) -0.06418(15) 0.36681(5) 0.0189(3) Uani 1 1 d . . . . . H1 H 0.402(5) -0.149(4) 0.3664(11) 0.044(9) Uiso 1 1 d . . . . . O2 O 0.4156(2) 0.60432(14) 0.37790(5) 0.0155(3) Uani 1 1 d . . . . . O3 O 0.8119(2) 0.40881(14) 0.36723(5) 0.0166(3) Uani 1 1 d . . . . . C1 C 0.2625(3) 0.02695(19) 0.35929(7) 0.0139(4) Uani 1 1 d . . . . . C2 C 0.0851(3) -0.0044(2) 0.39543(7) 0.0162(4) Uani 1 1 d . . . . . H2A H -0.0513 -0.0143 0.3793 0.019 Uiso 1 1 calc R U . . . H2B H 0.1149 -0.0933 0.4125 0.019 Uiso 1 1 calc R U . . . C3 C 0.0795(3) 0.1229(2) 0.42988(7) 0.0160(4) Uani 1 1 d . . . . . H3A H -0.0302 0.1916 0.4207 0.019 Uiso 1 1 calc R U . . . H3B H 0.0516 0.0904 0.4622 0.019 Uiso 1 1 calc R U . . . C4 C 0.2982(3) 0.1899(2) 0.42621(6) 0.0138(4) Uani 1 1 d . . . . . C5 C 0.3075(3) 0.3479(2) 0.43815(7) 0.0142(4) Uani 1 1 d . . . . . H5A H 0.2818 0.3605 0.4721 0.017 Uiso 1 1 calc R U . . . H5B H 0.1951 0.3981 0.4210 0.017 Uiso 1 1 calc R U . . . C6 C 0.5210(3) 0.4142(2) 0.42541(6) 0.0136(4) Uani 1 1 d . . . . . H6 H 0.6301 0.3833 0.4483 0.016 Uiso 1 1 calc R U . . . C7 C 0.5106(3) 0.5792(2) 0.42370(7) 0.0154(4) Uani 1 1 d . . . . . C8 C 0.7307(3) 0.6489(2) 0.42439(7) 0.0191(4) Uani 1 1 d . . . . . H8A H 0.7207 0.7431 0.4394 0.023 Uiso 1 1 calc R U . . . H8B H 0.8266 0.5900 0.4434 0.023 Uiso 1 1 calc R U . . . C9 C 0.8220(3) 0.6660(2) 0.37501(7) 0.0201(4) Uani 1 1 d . . . . . H9A H 0.7698 0.7550 0.3609 0.024 Uiso 1 1 calc R U . . . H9B H 0.9766 0.6717 0.3769 0.024 Uiso 1 1 calc R U . . . C10 C 0.7598(3) 0.5422(2) 0.34461(7) 0.0167(4) Uani 1 1 d . . . . . H10 H 0.8146 0.5494 0.3119 0.020 Uiso 1 1 calc R U . . . C11 C 0.5230(3) 0.5101(2) 0.34680(7) 0.0143(4) Uani 1 1 d . . . . . C12 C 0.5902(3) 0.3763(2) 0.37523(7) 0.0141(4) Uani 1 1 d . . . . . C13 C 0.5474(3) 0.2270(2) 0.35831(7) 0.0137(4) Uani 1 1 d . . . . . H13A H 0.5577 0.2241 0.3238 0.016 Uiso 1 1 calc R U . . . H13B H 0.6547 0.1622 0.3712 0.016 Uiso 1 1 calc R U . . . C14 C 0.3324(3) 0.1771(2) 0.37315(6) 0.0134(4) Uani 1 1 d . . . . . H14 H 0.2301 0.2434 0.3582 0.016 Uiso 1 1 calc R U . . . C15 C 0.1986(3) 0.0192(2) 0.30713(7) 0.0159(4) Uani 1 1 d . . . . . H15 H 0.3132 0.0649 0.2887 0.019 Uiso 1 1 calc R U . . . C16 C -0.0039(4) 0.0987(3) 0.29581(8) 0.0289(5) Uani 1 1 d . . . . . H16A H -0.0165 0.1103 0.2618 0.043 Uiso 1 1 calc R U . . . H16B H -0.0008 0.1921 0.3108 0.043 Uiso 1 1 calc R U . . . H16C H -0.1240 0.0448 0.3076 0.043 Uiso 1 1 calc R U . . . C17 C 0.1775(4) -0.1319(2) 0.28935(8) 0.0282(5) Uani 1 1 d . . . . . H17A H 0.1366 -0.1306 0.2563 0.042 Uiso 1 1 calc R U . . . H17B H 0.0702 -0.1816 0.3076 0.042 Uiso 1 1 calc R U . . . H17C H 0.3119 -0.1810 0.2927 0.042 Uiso 1 1 calc R U . . . C18 C 0.4547(3) 0.1070(2) 0.45652(7) 0.0173(4) Uani 1 1 d . . . . . H18A H 0.5978 0.1358 0.4485 0.026 Uiso 1 1 calc R U . . . H18B H 0.4380 0.0054 0.4507 0.026 Uiso 1 1 calc R U . . . H18C H 0.4281 0.1270 0.4896 0.026 Uiso 1 1 calc R U . . . C19 C 0.3704(3) 0.6460(2) 0.46033(7) 0.0189(4) Uani 1 1 d . . . . . H19A H 0.4272 0.6269 0.4916 0.028 Uiso 1 1 calc R U . . . H19B H 0.2293 0.6059 0.4579 0.028 Uiso 1 1 calc R U . . . H19C H 0.3640 0.7485 0.4552 0.028 Uiso 1 1 calc R U . . . C20 C 0.4017(3) 0.4961(2) 0.30181(7) 0.0193(4) Uani 1 1 d . . . . . H20A H 0.4677 0.4242 0.2820 0.029 Uiso 1 1 calc R U . . . H20B H 0.4012 0.5872 0.2854 0.029 Uiso 1 1 calc R U . . . H20C H 0.2574 0.4679 0.3088 0.029 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0174(7) 0.0101(7) 0.0291(8) 0.0008(6) -0.0028(6) 0.0026(6) O2 0.0180(7) 0.0130(6) 0.0157(7) -0.0008(5) -0.0004(5) 0.0024(6) O3 0.0111(7) 0.0145(7) 0.0241(7) 0.0008(6) 0.0030(6) -0.0014(5) C1 0.0142(9) 0.0107(9) 0.0168(10) 0.0007(7) -0.0006(7) -0.0002(7) C2 0.0190(10) 0.0139(9) 0.0156(9) 0.0015(7) -0.0008(7) -0.0032(8) C3 0.0159(10) 0.0164(9) 0.0156(9) 0.0002(7) 0.0006(7) -0.0025(8) C4 0.0151(10) 0.0139(9) 0.0125(9) 0.0008(7) 0.0005(7) -0.0009(7) C5 0.0147(10) 0.0146(9) 0.0133(8) -0.0020(7) 0.0013(7) -0.0012(7) C6 0.0132(10) 0.0126(9) 0.0150(9) -0.0008(7) -0.0014(7) -0.0006(7) C7 0.0190(11) 0.0126(9) 0.0148(9) -0.0007(7) -0.0018(8) -0.0006(8) C8 0.0199(11) 0.0157(10) 0.0218(10) -0.0017(8) -0.0022(8) -0.0039(8) C9 0.0191(10) 0.0149(9) 0.0262(11) -0.0008(8) 0.0007(9) -0.0037(8) C10 0.0171(10) 0.0135(9) 0.0194(10) 0.0016(7) 0.0027(8) -0.0032(8) C11 0.0164(10) 0.0107(9) 0.0159(9) -0.0002(7) 0.0023(7) 0.0006(7) C12 0.0105(9) 0.0147(9) 0.0170(9) 0.0005(7) -0.0006(7) 0.0005(7) C13 0.0153(10) 0.0129(9) 0.0129(9) -0.0017(7) 0.0009(7) 0.0001(7) C14 0.0147(10) 0.0118(8) 0.0138(9) 0.0003(7) -0.0006(7) 0.0013(7) C15 0.0192(10) 0.0126(9) 0.0160(9) -0.0017(7) 0.0017(8) -0.0013(8) C16 0.0351(14) 0.0304(12) 0.0212(11) -0.0076(9) -0.0098(9) 0.0111(11) C17 0.0460(15) 0.0151(10) 0.0233(11) -0.0034(8) -0.0033(11) -0.0032(10) C18 0.0191(10) 0.0157(9) 0.0171(9) 0.0027(8) -0.0027(8) -0.0006(8) C19 0.0244(11) 0.0132(9) 0.0190(10) -0.0035(8) 0.0003(8) 0.0021(8) C20 0.0254(11) 0.0161(10) 0.0163(10) 0.0007(8) -0.0003(8) 0.0015(8) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C1 1.442(2) . ? O1 H1 0.83(4) . ? O2 C11 1.432(2) . ? O2 C7 1.462(2) . ? O3 C10 1.454(2) . ? O3 C12 1.466(2) . ? C1 C14 1.539(2) . ? C1 C15 1.547(3) . ? C1 C2 1.561(3) . ? C2 C3 1.554(3) . ? C2 H2A 0.9900 . ? C2 H2B 0.9900 . ? C3 C4 1.537(3) . ? C3 H3A 0.9900 . ? C3 H3B 0.9900 . ? C4 C5 1.532(3) . ? C4 C14 1.536(2) . ? C4 C18 1.537(3) . ? C5 C6 1.544(3) . ? C5 H5A 0.9900 . ? C5 H5B 0.9900 . ? C6 C12 1.542(3) . ? C6 C7 1.560(3) . ? C6 H6 1.0000 . ? C7 C19 1.515(3) . ? C7 C8 1.552(3) . ? C8 C9 1.535(3) . ? C8 H8A 0.9900 . ? C8 H8B 0.9900 . ? C9 C10 1.509(3) . ? C9 H9A 0.9900 . ? C9 H9B 0.9900 . ? C10 C11 1.544(3) . ? C10 H10 1.0000 . ? C11 C20 1.506(3) . ? C11 C12 1.562(3) . ? C12 C13 1.516(3) . ? C13 C14 1.512(3) . ? C13 H13A 0.9900 . ? C13 H13B 0.9900 . ? C14 H14 1.0000 . ? C15 C17 1.521(3) . ? C15 C16 1.530(3) . ? C15 H15 1.0000 . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? C18 H18A 0.9800 . ? C18 H18B 0.9800 . ? C18 H18C 0.9800 . ? C19 H19A 0.9800 . ? C19 H19B 0.9800 . ? C19 H19C 0.9800 . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1 O1 H1 110(2) . . ? C11 O2 C7 104.83(14) . . ? C10 O3 C12 91.72(13) . . ? O1 C1 C14 106.46(15) . . ? O1 C1 C15 108.85(15) . . ? C14 C1 C15 111.60(15) . . ? O1 C1 C2 111.13(15) . . ? C14 C1 C2 102.41(15) . . ? C15 C1 C2 115.90(16) . . ? C3 C2 C1 106.80(15) . . ? C3 C2 H2A 110.4 . . ? C1 C2 H2A 110.4 . . ? C3 C2 H2B 110.4 . . ? C1 C2 H2B 110.4 . . ? H2A C2 H2B 108.6 . . ? C4 C3 C2 104.74(16) . . ? C4 C3 H3A 110.8 . . ? C2 C3 H3A 110.8 . . ? C4 C3 H3B 110.8 . . ? C2 C3 H3B 110.8 . . ? H3A C3 H3B 108.9 . . ? C5 C4 C14 106.92(15) . . ? C5 C4 C18 110.24(16) . . ? C14 C4 C18 115.07(16) . . ? C5 C4 C3 114.90(16) . . ? C14 C4 C3 99.43(15) . . ? C18 C4 C3 110.03(16) . . ? C4 C5 C6 112.13(16) . . ? C4 C5 H5A 109.2 . . ? C6 C5 H5A 109.2 . . ? C4 C5 H5B 109.2 . . ? C6 C5 H5B 109.2 . . ? H5A C5 H5B 107.9 . . ? C12 C6 C5 112.21(15) . . ? C12 C6 C7 102.41(15) . . ? C5 C6 C7 112.02(17) . . ? C12 C6 H6 110.0 . . ? C5 C6 H6 110.0 . . ? C7 C6 H6 110.0 . . ? O2 C7 C19 107.81(16) . . ? O2 C7 C8 108.54(15) . . ? C19 C7 C8 110.45(16) . . ? O2 C7 C6 102.00(14) . . ? C19 C7 C6 114.82(17) . . ? C8 C7 C6 112.62(17) . . ? C9 C8 C7 112.13(17) . . ? C9 C8 H8A 109.2 . . ? C7 C8 H8A 109.2 . . ? C9 C8 H8B 109.2 . . ? C7 C8 H8B 109.2 . . ? H8A C8 H8B 107.9 . . ? C10 C9 C8 110.36(16) . . ? C10 C9 H9A 109.6 . . ? C8 C9 H9A 109.6 . . ? C10 C9 H9B 109.6 . . ? C8 C9 H9B 109.6 . . ? H9A C9 H9B 108.1 . . ? O3 C10 C9 110.80(16) . . ? O3 C10 C11 92.05(14) . . ? C9 C10 C11 112.73(17) . . ? O3 C10 H10 113.2 . . ? C9 C10 H10 113.2 . . ? C11 C10 H10 113.2 . . ? O2 C11 C20 109.75(16) . . ? O2 C11 C10 111.85(15) . . ? C20 C11 C10 119.08(17) . . ? O2 C11 C12 108.15(15) . . ? C20 C11 C12 120.92(16) . . ? C10 C11 C12 84.89(14) . . ? O3 C12 C13 108.59(15) . . ? O3 C12 C6 111.89(15) . . ? C13 C12 C6 117.44(16) . . ? O3 C12 C11 90.85(14) . . ? C13 C12 C11 122.51(16) . . ? C6 C12 C11 102.52(15) . . ? C14 C13 C12 111.34(16) . . ? C14 C13 H13A 109.4 . . ? C12 C13 H13A 109.4 . . ? C14 C13 H13B 109.4 . . ? C12 C13 H13B 109.4 . . ? H13A C13 H13B 108.0 . . ? C13 C14 C4 112.39(16) . . ? C13 C14 C1 118.57(16) . . ? C4 C14 C1 106.58(15) . . ? C13 C14 H14 106.2 . . ? C4 C14 H14 106.2 . . ? C1 C14 H14 106.2 . . ? C17 C15 C16 108.38(18) . . ? C17 C15 C1 112.94(16) . . ? C16 C15 C1 113.78(16) . . ? C17 C15 H15 107.1 . . ? C16 C15 H15 107.1 . . ? C1 C15 H15 107.1 . . ? C15 C16 H16A 109.5 . . ? C15 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C15 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C15 C17 H17A 109.5 . . ? C15 C17 H17B 109.5 . . ? H17A C17 H17B 109.5 . . ? C15 C17 H17C 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C4 C18 H18A 109.5 . . ? C4 C18 H18B 109.5 . . ? H18A C18 H18B 109.5 . . ? C4 C18 H18C 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C7 C19 H19A 109.5 . . ? C7 C19 H19B 109.5 . . ? H19A C19 H19B 109.5 . . ? C7 C19 H19C 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C11 C20 H20A 109.5 . . ? C11 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C11 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1 C1 C2 C3 108.36(17) . . . . ? C14 C1 C2 C3 -4.97(19) . . . . ? C15 C1 C2 C3 -126.69(17) . . . . ? C1 C2 C3 C4 -22.4(2) . . . . ? C2 C3 C4 C5 153.73(15) . . . . ? C2 C3 C4 C14 40.01(18) . . . . ? C2 C3 C4 C18 -81.17(19) . . . . ? C14 C4 C5 C6 -60.6(2) . . . . ? C18 C4 C5 C6 65.2(2) . . . . ? C3 C4 C5 C6 -169.82(16) . . . . ? C4 C5 C6 C12 48.8(2) . . . . ? C4 C5 C6 C7 163.39(15) . . . . ? C11 O2 C7 C19 -165.74(15) . . . . ? C11 O2 C7 C8 74.60(18) . . . . ? C11 O2 C7 C6 -44.48(18) . . . . ? C12 C6 C7 O2 41.05(18) . . . . ? C5 C6 C7 O2 -79.38(18) . . . . ? C12 C6 C7 C19 157.33(16) . . . . ? C5 C6 C7 C19 36.9(2) . . . . ? C12 C6 C7 C8 -75.10(19) . . . . ? C5 C6 C7 C8 164.48(15) . . . . ? O2 C7 C8 C9 -24.0(2) . . . . ? C19 C7 C8 C9 -142.01(17) . . . . ? C6 C7 C8 C9 88.1(2) . . . . ? C7 C8 C9 C10 -35.7(2) . . . . ? C12 O3 C10 C9 109.74(17) . . . . ? C12 O3 C10 C11 -5.55(15) . . . . ? C8 C9 C10 O3 -52.3(2) . . . . ? C8 C9 C10 C11 49.3(2) . . . . ? C7 O2 C11 C20 164.43(15) . . . . ? C7 O2 C11 C10 -61.11(19) . . . . ? C7 O2 C11 C12 30.62(19) . . . . ? O3 C10 C11 O2 112.75(15) . . . . ? C9 C10 C11 O2 -0.8(2) . . . . ? O3 C10 C11 C20 -117.49(17) . . . . ? C9 C10 C11 C20 128.92(19) . . . . ? O3 C10 C11 C12 5.23(14) . . . . ? C9 C10 C11 C12 -108.36(17) . . . . ? C10 O3 C12 C13 130.38(15) . . . . ? C10 O3 C12 C6 -98.38(16) . . . . ? C10 O3 C12 C11 5.48(15) . . . . ? C5 C6 C12 O3 -165.90(15) . . . . ? C7 C6 C12 O3 73.80(19) . . . . ? C5 C6 C12 C13 -39.3(2) . . . . ? C7 C6 C12 C13 -159.63(17) . . . . ? C5 C6 C12 C11 98.04(18) . . . . ? C7 C6 C12 C11 -22.26(18) . . . . ? O2 C11 C12 O3 -116.52(15) . . . . ? C20 C11 C12 O3 115.83(18) . . . . ? C10 C11 C12 O3 -5.18(14) . . . . ? O2 C11 C12 C13 130.68(18) . . . . ? C20 C11 C12 C13 3.0(3) . . . . ? C10 C11 C12 C13 -117.99(19) . . . . ? O2 C11 C12 C6 -3.86(19) . . . . ? C20 C11 C12 C6 -131.51(18) . . . . ? C10 C11 C12 C6 107.47(15) . . . . ? O3 C12 C13 C14 169.98(15) . . . . ? C6 C12 C13 C14 41.8(2) . . . . ? C11 C12 C13 C14 -86.5(2) . . . . ? C12 C13 C14 C4 -54.4(2) . . . . ? C12 C13 C14 C1 -179.57(16) . . . . ? C5 C4 C14 C13 64.1(2) . . . . ? C18 C4 C14 C13 -58.7(2) . . . . ? C3 C4 C14 C13 -176.16(15) . . . . ? C5 C4 C14 C1 -164.46(16) . . . . ? C18 C4 C14 C1 72.8(2) . . . . ? C3 C4 C14 C1 -44.69(18) . . . . ? O1 C1 C14 C13 42.2(2) . . . . ? C15 C1 C14 C13 -76.4(2) . . . . ? C2 C1 C14 C13 158.96(16) . . . . ? O1 C1 C14 C4 -85.69(18) . . . . ? C15 C1 C14 C4 155.66(16) . . . . ? C2 C1 C14 C4 31.05(19) . . . . ? O1 C1 C15 C17 49.5(2) . . . . ? C14 C1 C15 C17 166.69(18) . . . . ? C2 C1 C15 C17 -76.6(2) . . . . ? O1 C1 C15 C16 173.59(17) . . . . ? C14 C1 C15 C16 -69.2(2) . . . . ? C2 C1 C15 C16 47.5(2) . . . . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A O1 H1 O2 0.83(4) 2.36(4) 3.1510(19) 159(3) 1_545 _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; _audit_block_code C20H32O3_uv033_magauer _audit_creation_method 'APEX3 v2015.9-RC7' _shelxl_version_number ? _chemical_name_systematic ? _chemical_formula_moiety 'C20 H32 O3' _chemical_formula_sum 'C20 H32 O3' _chemical_formula_weight 320.45 #?# (Cohen, 1996) _chemical_melting_point ? #?# in K! _cell_formula_units_Z 4 #?# adjust to _chemical_formula_[] _exptl_crystal_density_diffrn 1.235 _exptl_crystal_F_000 704 #?# check! _shelx_res_file ; uv033_0m.res created by SHELXL-2014/7 TITL uv033_0m_a.res in P2(1)2(1)2(1) REM Old TITL uv033_0m in P2(1)2(1)2(1) REM SHELXT solution in P2(1)2(1)2(1) REM R1 0.181, Rweak 0.041, Alpha 0.014, Orientation as input REM Flack x = 0.295 ( 1.457 ) from Parsons' quotients REM Formula found by SHELXT: C20 O3 CELL 0.71073 6.3848 9.4448 28.5710 90.0000 90.0000 90.0000 ZERR 4.000 0.0004 0.0007 0.0019 0.0000 0.0000 0.0000 LATT -1 SYMM 1/2-X, -Y, 1/2+Z SYMM -X, 1/2+Y, 1/2-Z SYMM 1/2+X, 1/2-Y, -Z SFAC C H O UNIT 80 128 12 TEMP -173.15 OMIT 0 0 2 OMIT 0 0 4 OMIT 0 1 1 OMIT 0 1 2 OMIT 3 3 0 OMIT 3 0 18 OMIT 3 3 12 OMIT 0 6 0 OMIT -3 3 12 OMIT 0 6 9 OMIT 3 0 9 OMIT 0 0 8 SIZE 0.02 0.03 0.10 L.S. 10 BOND $H LIST 4 CONF ACTA HTAB EQIV $1 x, y-1, z HTAB O1 O2_$1 FMAP 2 PLAN -20 WGHT 0.037600 0.655900 FVAR 0.78151 O1 3 0.440629 -0.064178 0.366812 11.00000 0.01744 0.01015 = 0.02909 0.00079 -0.00279 0.00262 H1 2 0.402097 -0.148532 0.366397 11.00000 0.04389 O2 3 0.415596 0.604321 0.377900 11.00000 0.01803 0.01297 = 0.01566 -0.00083 -0.00042 0.00240 O3 3 0.811867 0.408813 0.367228 11.00000 0.01113 0.01453 = 0.02410 0.00079 0.00304 -0.00137 C1 1 0.262525 0.026947 0.359294 11.00000 0.01420 0.01071 = 0.01679 0.00074 -0.00064 -0.00020 C2 1 0.085118 -0.004370 0.395430 11.00000 0.01901 0.01392 = 0.01558 0.00150 -0.00079 -0.00316 AFIX 23 H2A 2 -0.051279 -0.014277 0.379279 11.00000 -1.20000 H2B 2 0.114882 -0.093278 0.412536 11.00000 -1.20000 AFIX 0 C3 1 0.079490 0.122921 0.429878 11.00000 0.01588 0.01638 = 0.01562 0.00026 0.00057 -0.00254 AFIX 23 H3A 2 -0.030224 0.191579 0.420691 11.00000 -1.20000 H3B 2 0.051563 0.090384 0.462220 11.00000 -1.20000 AFIX 0 C4 1 0.298241 0.189941 0.426210 11.00000 0.01507 0.01393 = 0.01253 0.00079 0.00050 -0.00088 C5 1 0.307489 0.347913 0.438150 11.00000 0.01474 0.01457 = 0.01334 -0.00195 0.00127 -0.00120 AFIX 23 H5A 2 0.281775 0.360497 0.472066 11.00000 -1.20000 H5B 2 0.195141 0.398143 0.420986 11.00000 -1.20000 AFIX 0 C6 1 0.520981 0.414232 0.425409 11.00000 0.01317 0.01263 = 0.01504 -0.00084 -0.00141 -0.00064 AFIX 13 H6 2 0.630071 0.383297 0.448347 11.00000 -1.20000 AFIX 0 C7 1 0.510561 0.579182 0.423703 11.00000 0.01897 0.01261 = 0.01475 -0.00067 -0.00183 -0.00055 C8 1 0.730701 0.648914 0.424386 11.00000 0.01997 0.01572 = 0.02177 -0.00174 -0.00219 -0.00391 AFIX 23 H8A 2 0.720724 0.743135 0.439404 11.00000 -1.20000 H8B 2 0.826624 0.589994 0.443407 11.00000 -1.20000 AFIX 0 C9 1 0.821978 0.665949 0.375015 11.00000 0.01912 0.01492 = 0.02624 -0.00077 0.00066 -0.00371 AFIX 23 H9A 2 0.769819 0.754980 0.360922 11.00000 -1.20000 H9B 2 0.976581 0.671650 0.376870 11.00000 -1.20000 AFIX 0 C10 1 0.759819 0.542227 0.344615 11.00000 0.01715 0.01348 = 0.01940 0.00162 0.00271 -0.00316 AFIX 13 H10 2 0.814581 0.549370 0.311908 11.00000 -1.20000 AFIX 0 C11 1 0.522963 0.510125 0.346803 11.00000 0.01642 0.01068 = 0.01595 -0.00023 0.00227 0.00057 C12 1 0.590151 0.376327 0.375229 11.00000 0.01050 0.01472 = 0.01697 0.00048 -0.00065 0.00052 C13 1 0.547417 0.227008 0.358314 11.00000 0.01527 0.01296 = 0.01291 -0.00175 0.00091 0.00015 AFIX 23 H13A 2 0.557744 0.224141 0.323753 11.00000 -1.20000 H13B 2 0.654744 0.162235 0.371233 11.00000 -1.20000 AFIX 0 C14 1 0.332375 0.177141 0.373149 11.00000 0.01472 0.01178 = 0.01385 0.00035 -0.00059 0.00133 AFIX 13 H14 2 0.230104 0.243444 0.358239 11.00000 -1.20000 AFIX 0 C15 1 0.198607 0.019163 0.307127 11.00000 0.01918 0.01259 = 0.01597 -0.00172 0.00172 -0.00126 AFIX 13 H15 2 0.313197 0.064915 0.288673 11.00000 -1.20000 AFIX 0 C16 1 -0.003852 0.098747 0.295806 11.00000 0.03515 0.03041 = 0.02125 -0.00763 -0.00984 0.01114 AFIX 137 H16A 2 -0.016421 0.110311 0.261835 11.00000 -1.50000 H16B 2 -0.000864 0.192094 0.310768 11.00000 -1.50000 H16C 2 -0.123960 0.044813 0.307564 11.00000 -1.50000 AFIX 0 C17 1 0.177451 -0.131909 0.289354 11.00000 0.04601 0.01513 = 0.02332 -0.00338 -0.00330 -0.00322 AFIX 137 H17A 2 0.136682 -0.130560 0.256288 11.00000 -1.50000 H17B 2 0.070195 -0.181544 0.307597 11.00000 -1.50000 H17C 2 0.311839 -0.180992 0.292721 11.00000 -1.50000 AFIX 0 C18 1 0.454691 0.107023 0.456522 11.00000 0.01910 0.01570 = 0.01710 0.00274 -0.00274 -0.00065 AFIX 137 H18A 2 0.597761 0.135792 0.448531 11.00000 -1.50000 H18B 2 0.438034 0.005381 0.450717 11.00000 -1.50000 H18C 2 0.428057 0.127013 0.489649 11.00000 -1.50000 AFIX 0 C19 1 0.370392 0.646010 0.460333 11.00000 0.02441 0.01321 = 0.01901 -0.00348 0.00028 0.00210 AFIX 137 H19A 2 0.427198 0.626832 0.491561 11.00000 -1.50000 H19B 2 0.229248 0.605905 0.457905 11.00000 -1.50000 H19C 2 0.364046 0.748526 0.455231 11.00000 -1.50000 AFIX 0 C20 1 0.401732 0.496129 0.301809 11.00000 0.02539 0.01605 = 0.01634 0.00072 -0.00028 0.00145 AFIX 137 H20A 2 0.467746 0.424195 0.281973 11.00000 -1.50000 H20B 2 0.401188 0.587226 0.285388 11.00000 -1.50000 H20C 2 0.257393 0.467861 0.308793 11.00000 -1.50000 REM ##### AFIX 0 HKLF 4 REM uv033_0m_a.res in P2(1)2(1)2(1) REM R1 = 0.0338 for 3373 Fo > 4sig(Fo) and 0.0361 for all 3507 data REM 217 parameters refined using 0 restraints END WGHT 0.0384 0.6423 REM Instructions for potential hydrogen bonds HTAB O1 O2_$1 REM Highest difference peak 0.263, deepest hole -0.183, 1-sigma level 0.040 Q1 1 0.5153 0.4374 0.3608 11.00000 0.05 0.26 Q2 1 0.3087 0.1059 0.3639 11.00000 0.05 0.25 Q3 1 0.5175 0.4976 0.4292 11.00000 0.05 0.24 Q4 1 0.5632 0.3074 0.3630 11.00000 0.05 0.23 Q5 1 0.4148 0.3828 0.4311 11.00000 0.05 0.23 Q6 1 0.3310 0.1769 0.3991 11.00000 0.05 0.21 Q7 1 0.2025 0.0215 0.3338 11.00000 0.05 0.21 Q8 1 0.4261 0.6158 0.4364 11.00000 0.05 0.20 Q9 1 0.2975 0.2719 0.4328 11.00000 0.05 0.19 Q10 1 0.6176 0.6108 0.4247 11.00000 0.05 0.19 Q11 1 0.1561 0.0121 0.3715 11.00000 0.05 0.19 Q12 1 0.6373 0.5418 0.3411 11.00000 0.05 0.19 Q13 1 0.7527 0.6038 0.3632 11.00000 0.05 0.18 Q14 1 0.3835 0.1476 0.4392 11.00000 0.05 0.18 Q15 1 0.0921 0.1520 0.2896 11.00000 0.05 0.18 Q16 1 0.4344 0.2021 0.3643 11.00000 0.05 0.17 Q17 1 0.1162 0.1964 0.4226 11.00000 0.05 0.16 Q18 1 0.5833 0.1333 0.4604 11.00000 0.05 0.16 Q19 1 0.1889 0.1697 0.4305 11.00000 0.05 0.16 Q20 1 0.1874 0.2176 0.3637 11.00000 0.05 0.16 ; _shelx_res_checksum 19993 _shelx_hkl_file ; -1 0 0 -0.6478 0.91986 2 -1 0 0 -0.1599 0.81012 2 -2 0 0 213.856 8.02275 2 -2 0 0 212.167 7.92614 2 -3 0 0 4.70701 2.08602 2 -3 0 0 3.91994 2.31674 2 -4 0 0 417.538 15.4459 2 -4 0 0 415.572 15.5309 2 -5 0 0 4.31489 2.75224 2 -5 0 0 4.52471 3.20423 2 -6 0 0 40.2521 5.63400 2 -6 0 0 30.6227 4.88793 2 -7 0 0 -1.9010 3.16234 2 0 -1 0 -0.5721 0.35597 3 0 1 0 -0.3194 0.33628 3 0 1 0 -0.1684 0.39826 2 0 -1 0 0.12120 0.36777 2 1 -1 0 9647.49 309.067 1 -1 -1 0 9783.20 313.703 1 -1 1 0 9999.99 309.441 1 -2 -1 0 425.525 13.3184 2 -2 -1 0 375.885 12.1422 3 2 1 0 389.962 13.2586 2 2 1 0 376.515 12.0861 3 -2 1 0 378.032 12.9456 2 2 1 0 365.156 12.0848 3 2 -1 0 378.783 13.1292 2 -2 -1 0 371.445 12.1768 3 3 -1 0 80.6837 5.10651 2 3 1 0 66.3622 4.69683 2 3 1 0 62.6750 2.76042 3 -3 -1 0 63.0024 3.05500 3 -3 -1 0 75.5397 4.90848 2 3 1 0 65.4882 2.75867 3 -3 -1 0 64.9070 3.06301 3 -3 1 0 71.8685 4.60351 2 -4 -1 0 1823.24 58.6819 2 -4 1 0 1739.41 58.1105 2 -4 -1 0 1924.93 58.6667 2 -4 1 0 1863.83 58.4271 2 -5 1 0 587.230 20.7896 2 -5 -1 0 583.485 20.8533 2 -5 1 0 539.338 20.4887 2 -5 -1 0 549.154 21.0127 2 -6 -1 0 92.9864 7.78592 2 -6 1 0 89.0740 7.34881 2 -6 1 0 94.7919 7.29524 2 -6 -1 0 95.1408 7.30363 2 -7 1 0 193.586 11.7404 2 -7 -1 0 153.022 10.0064 2 -7 1 0 160.023 10.1441 2 0 2 0 6517.91 224.896 1 0 -2 0 6465.45 224.831 1 -1 -2 0 15.4189 1.75485 3 -1 -2 0 15.0144 1.78764 3 -1 -2 0 21.3166 2.77467 2 1 -2 0 18.9354 1.76191 3 -1 2 0 15.7282 1.98166 3 -1 2 0 15.3495 1.93283 3 1 -2 0 17.1686 1.92626 3 -1 2 0 19.0925 2.21777 2 1 2 0 18.4470 2.46810 2 1 2 0 19.1432 1.96939 3 1 -2 0 20.2996 2.28666 2 -2 -2 0 751.834 24.2431 2 2 -2 0 739.184 23.0733 3 -2 -2 0 738.746 23.3672 3 -2 -2 0 728.019 23.4158 3 2 2 0 748.410 23.3708 3 2 -2 0 741.533 24.0451 2 -2 2 0 740.953 23.1068 3 -2 2 0 742.195 23.8874 2 2 2 0 731.930 23.3035 3 2 -2 0 753.038 23.1344 3 -2 2 0 763.186 23.1498 3 2 2 0 706.333 24.2397 2 -3 2 0 926.541 30.2957 2 3 -2 0 966.244 30.6844 2 -3 2 0 936.595 28.8597 3 3 2 0 922.075 29.1840 3 -3 -2 0 1001.77 30.8781 2 3 2 0 929.319 30.8370 2 -3 -2 0 928.080 29.3707 3 3 2 0 848.261 29.1211 3 -3 -2 0 915.865 29.2816 3 -3 2 0 968.872 28.8918 3 -4 -2 0 200.990 9.29836 2 -4 2 0 192.950 8.86595 2 -4 -2 0 202.276 7.39233 3 4 2 0 192.479 7.00798 3 4 2 0 222.405 9.59114 2 4 -2 0 201.971 9.42480 2 -4 -2 0 202.580 7.32797 3 4 2 0 201.760 7.04390 3 -5 -2 0 27.3557 2.68696 3 -5 2 0 31.3189 4.62014 2 -5 2 0 33.2282 4.54053 2 -5 -2 0 39.6082 5.30983 2 -5 -2 0 37.5713 5.56038 2 -6 -2 0 131.981 9.41716 2 -6 2 0 140.340 8.96361 2 -6 2 0 127.351 8.39406 2 -6 -2 0 132.850 8.73820 2 -7 2 0 6.03609 3.87840 2 -7 -2 0 5.38836 4.30744 2 0 3 0 3.12388 1.79560 2 0 3 0 0.46355 1.42330 3 0 3 0 2.00519 1.42220 3 0 -3 0 1.84524 1.89054 2 0 -3 0 3.69964 2.62443 3 0 -3 0 1.99012 1.51593 3 1 3 0 67.3616 3.70323 3 -1 -3 0 65.3606 3.62603 3 -1 -3 0 59.4927 3.62557 3 -1 -3 0 64.4388 4.06945 2 1 -3 0 58.3960 3.92834 2 -1 3 0 62.3975 3.89990 2 1 -3 0 52.8182 3.36742 3 -1 3 0 53.9198 3.34249 3 1 3 0 66.7470 3.64411 3 -1 3 0 56.4388 3.44384 3 1 3 0 67.5267 4.04974 2 -2 -3 0 251.755 9.62490 3 2 -3 0 266.218 9.33716 3 -2 -3 0 264.008 9.55181 3 2 3 0 261.248 9.57404 3 -2 3 0 271.797 9.35226 3 -2 3 0 267.272 9.32371 3 2 3 0 258.474 10.0830 3 -2 -3 0 293.699 10.6898 2 2 -3 0 259.856 10.2925 2 2 -3 0 272.544 9.27629 3 -2 3 0 261.533 10.0619 2 2 3 0 263.597 10.4304 2 3 -3 0 163.150 5.65235 3 -3 -3 0 149.072 6.06429 3 -3 -3 0 144.900 6.12013 3 -3 3 0 147.694 5.56882 3 3 3 0 141.051 5.86016 3 3 3 0 121.954 5.75038 3 -3 3 0 139.118 5.52338 3 3 -3 0 138.418 5.45356 3 -4 -3 0 566.372 19.7025 2 -4 3 0 539.913 18.9721 2 -4 3 0 544.825 17.0725 3 4 3 0 515.997 17.4676 3 4 -3 0 536.782 19.4394 2 4 3 0 519.103 19.6892 2 4 3 0 518.269 17.4623 3 -4 3 0 553.367 17.0899 3 -4 -3 0 527.543 17.8061 3 -4 -3 0 522.001 17.6653 3 -5 -3 0 168.274 6.89055 3 5 -3 0 172.119 9.56616 2 -5 -3 0 175.527 9.43377 2 5 3 0 170.545 9.48249 2 5 3 0 163.990 6.40014 3 -5 3 0 157.979 8.81902 2 -5 -3 0 179.307 7.08381 3 5 3 0 162.499 6.40827 3 -6 3 0 63.7704 6.64083 2 -6 3 0 56.0040 6.15497 2 -6 -3 0 60.0220 7.91870 2 -6 -3 0 51.1928 3.71889 3 -6 -3 0 51.8325 6.59772 2 -6 -3 0 49.2908 3.56141 3 -7 -3 0 15.7194 5.06975 2 -7 3 0 12.0280 4.44873 2 0 4 0 3970.57 120.608 3 0 -4 0 3903.74 120.569 3 0 -4 0 3918.98 120.680 3 1 -4 0 254.388 10.0700 2 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9.19056 1.81512 3 -5 1 -6 12.9773 3.89313 2 -5 1 -6 11.2831 3.72520 2 -5 -1 6 9.19607 1.75098 3 -5 -1 6 6.79275 3.56681 2 -6 -1 -6 139.291 10.3735 2 -6 -1 -6 136.588 9.45828 2 -6 1 6 133.435 8.02157 2 -6 1 6 153.091 8.89729 2 -6 -1 6 133.464 8.19117 2 -6 1 -6 137.000 9.62024 2 -6 1 -6 151.048 9.65802 2 -6 -1 6 138.599 9.27351 2 -7 1 6 44.2654 6.00860 2 -7 -1 -6 55.3493 7.39582 2 -7 1 -6 47.2538 7.23765 2 -7 -1 6 39.0955 5.79012 2 0 -2 6 804.403 25.5366 3 0 -2 6 787.324 25.5775 2 0 -2 -6 802.614 25.3832 3 0 2 -6 765.778 25.4529 3 0 2 -6 797.926 25.5923 2 0 -2 -6 841.155 25.3467 2 0 2 6 787.692 25.4345 3 0 2 6 841.484 25.4060 2 0 -2 -6 792.552 25.4263 3 0 2 6 802.444 25.3645 3 0 -2 6 792.344 25.3345 3 -1 2 6 80.4475 3.23574 2 1 2 -6 70.2197 3.94493 3 1 2 -6 70.9079 3.70365 3 1 2 -6 79.7379 3.93720 2 -1 -2 -6 74.8245 4.22572 2 -1 2 6 70.7611 3.55502 3 1 -2 6 73.3611 3.60611 3 -1 -2 -6 74.5285 3.87152 3 1 -2 6 73.4603 4.45450 2 -1 -2 -6 75.8229 3.78473 3 -1 2 6 73.0553 3.90229 3 1 2 6 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114.307 5.12136 3 5 2 -6 94.0021 4.29948 3 5 2 -6 99.6651 6.67434 2 5 2 -6 97.8521 4.30969 3 -5 2 6 97.4118 6.17947 2 -5 2 6 103.675 6.16966 2 -5 -2 -6 95.0982 8.75957 2 -5 -2 -6 100.226 4.75642 3 5 -2 6 95.1777 7.91808 2 -5 -2 -6 89.2258 4.58051 3 -5 -2 -6 103.553 7.52274 2 -5 -2 6 120.378 6.80537 2 -5 -2 6 87.2541 4.70062 3 -5 -2 6 98.6265 4.98860 3 -5 2 -6 103.488 7.70561 2 -6 2 6 38.9999 5.30369 2 -6 -2 -6 26.4746 5.37587 2 -6 2 6 33.3316 4.58670 2 -6 2 -6 26.6111 5.14487 2 -6 -2 6 32.2981 4.82845 2 -6 2 -6 34.1616 5.72341 2 -6 -2 6 30.9325 3.10305 3 -6 -2 6 28.1374 2.85197 3 -6 -2 6 40.4915 6.27788 2 -7 2 6 2.08230 3.45002 2 -7 -2 -6 -0.5740 4.01062 2 -7 -2 6 -1.3384 3.80935 2 -7 2 -6 -1.7544 3.73519 2 0 -3 6 1098.49 35.8783 3 0 -3 -6 1111.51 36.0201 3 0 -3 6 1146.79 36.3337 2 0 3 6 1143.83 36.0468 3 0 3 -6 1125.74 36.2638 2 0 3 -6 1134.43 35.9461 3 0 3 6 1073.58 35.9560 2 0 3 -6 1118.12 36.0816 3 0 -3 -6 1322.87 36.1072 2 1 -3 6 1907.08 59.3123 3 1 3 -6 1937.64 59.7477 2 -1 3 6 2018.11 59.2052 2 -1 3 6 1958.19 59.4787 3 -1 3 6 1899.60 59.3429 3 -1 -3 -6 1906.12 59.5359 3 1 3 -6 1878.11 59.4099 3 1 -3 6 1916.06 60.0296 2 -1 -3 -6 2119.46 60.0880 2 1 3 6 1862.29 59.9669 2 -1 -3 6 1874.63 59.4132 3 -1 3 -6 1919.18 59.9283 2 1 3 6 1928.42 59.4685 3 -1 -3 6 1963.26 59.7580 2 -1 -3 6 1842.57 59.6059 3 1 -3 -6 1757.37 59.2746 3 -1 3 -6 1883.80 59.4754 3 1 -3 -6 2016.78 59.2057 2 -1 3 -6 1875.36 59.3058 3 1 -3 -6 1867.52 59.4071 3 2 3 -6 513.083 17.3172 2 -2 3 6 519.446 16.4704 2 2 -3 6 492.079 17.8191 2 -2 3 6 499.516 16.6148 3 -2 -3 -6 486.940 16.7239 3 2 -3 6 492.739 16.3798 3 -2 -3 -6 507.581 16.8252 3 -2 3 6 512.855 16.5152 3 -2 -3 -6 521.196 17.8813 2 2 3 -6 479.291 16.7996 3 2 -3 6 507.823 16.6429 3 -2 -3 6 499.354 16.7067 3 -2 3 -6 513.320 16.6584 3 2 3 6 491.298 17.7640 2 -2 3 -6 493.061 17.5687 2 2 -3 -6 503.620 16.5064 2 2 3 6 501.879 16.6462 3 -2 3 -6 503.336 16.4494 3 -2 -3 6 475.833 16.8603 3 -2 -3 6 471.089 17.1026 2 2 -3 -6 503.063 16.5716 3 2 -3 -6 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2.06288 3 3 3 10 7.20848 1.87728 3 -3 3 -10 7.89553 3.07989 2 3 3 10 6.24616 2.80056 2 -3 3 -10 10.2772 2.37551 3 4 -3 10 26.5265 5.21876 2 -4 -3 -10 31.0378 3.43972 3 -4 3 10 29.7706 3.54431 3 -4 3 10 27.1213 3.03640 3 -4 -3 -10 31.0318 5.27400 2 4 3 -10 25.0307 2.91857 3 -4 -3 -10 24.5420 4.59519 2 -4 3 10 24.7242 3.00601 2 -4 -3 -10 27.8106 3.12292 3 4 3 -10 27.5189 3.19722 3 -4 3 10 24.7568 3.23757 2 4 3 -10 27.3867 3.80004 2 4 -3 10 29.3083 3.26779 3 4 -3 10 22.7317 2.73766 3 4 -3 -10 24.0655 2.95002 3 -4 -3 10 30.4309 3.76468 3 4 3 10 26.0881 4.64933 2 -4 -3 10 25.7949 3.15810 3 4 3 10 26.8234 2.99564 3 4 -3 -10 24.3113 3.12917 3 -4 3 -10 27.4603 3.03539 3 -4 3 -10 24.1057 3.03614 3 -4 3 -10 29.7156 4.69759 2 4 3 10 29.0915 3.17287 3 -4 -3 10 38.8665 4.78682 2 -5 -3 -10 21.1108 3.09057 3 -5 3 10 23.8014 2.69722 3 -5 3 10 21.8411 3.14124 2 5 3 -10 18.7675 2.86023 3 5 -3 10 22.1960 2.31264 3 -5 -3 -10 17.7727 4.49475 2 5 3 -10 23.5859 4.10913 2 -5 3 10 19.5025 2.66594 3 -5 -3 -10 21.3183 5.54829 2 -5 -3 -10 23.3224 3.33367 3 -5 3 10 19.2624 3.10452 2 5 -3 10 22.7755 5.49258 2 5 3 -10 29.0711 3.15749 3 -5 3 -10 16.7813 4.65470 2 -5 -3 10 22.0072 3.93393 2 5 -3 -10 19.3942 2.34934 3 -5 3 -10 21.0063 2.71052 3 5 3 10 20.3452 2.81698 3 5 3 10 22.4114 2.65232 3 -5 -3 10 22.2296 3.27621 3 5 -3 -10 14.6261 2.43995 3 -5 -3 10 21.7584 3.07401 3 -5 3 -10 23.3033 2.63279 3 6 -3 10 152.533 11.0627 2 -6 -3 -10 149.697 6.93869 3 -6 -3 -10 143.278 10.2365 2 6 3 -10 156.369 6.43638 3 -6 3 10 157.803 7.56360 2 -6 3 10 155.853 6.08997 3 6 3 -10 150.512 8.94221 2 -6 3 10 148.425 6.03430 3 -6 3 10 137.067 7.65447 2 -6 -3 -10 144.768 6.79821 3 6 3 10 143.356 6.09603 3 -6 -3 10 139.295 8.79437 2 -6 3 -10 150.984 10.4747 2 -6 -3 10 144.121 7.04853 3 -6 -3 10 148.056 7.23553 3 -7 -3 -10 2.89285 4.78827 2 -7 -3 -10 3.44258 2.14478 3 -7 3 10 3.53221 3.30871 2 -7 -3 -10 7.39518 2.43232 3 -7 3 -10 9.23533 4.83921 2 -7 -3 10 3.13013 2.23027 3 -7 -3 10 6.33853 2.38344 3 -7 -3 10 4.29243 4.24017 2 0 -4 -10 65.4294 4.75980 3 0 4 10 94.1492 6.71591 3 0 -4 10 71.6678 5.05200 3 0 4 -10 67.2604 5.29248 2 0 -4 10 69.6581 5.52267 2 0 4 -10 93.9989 5.85059 3 0 4 10 68.3042 4.61496 3 0 4 -10 98.1294 6.87687 3 0 4 10 70.0015 4.75365 2 0 -4 10 74.7528 4.70608 3 0 -4 -10 75.2238 4.76347 2 0 -4 -10 70.2277 4.81641 3 1 -4 10 4.29132 2.90905 2 1 4 -10 11.9552 3.23914 3 -1 -4 -10 10.1465 4.09028 3 1 4 -10 12.7008 3.88562 3 -1 4 10 8.84722 2.11446 2 1 -4 10 6.28173 2.30526 3 -1 -4 -10 10.8547 2.77157 2 1 -4 10 7.64145 2.19445 3 -1 4 10 8.69234 2.61372 3 -1 -4 -10 7.76109 2.42422 3 1 4 -10 13.4309 3.03252 2 -1 4 10 5.86701 2.04474 3 -1 -4 10 7.83509 2.97662 3 1 4 10 5.91871 2.57366 3 1 -4 -10 8.34564 2.25866 3 1 -4 -10 8.93509 2.27602 2 -1 -4 10 8.32939 2.97602 2 -1 4 -10 6.51271 3.10629 2 1 -4 -10 6.87812 2.38192 3 -1 4 -10 5.55520 2.36085 3 1 4 10 5.32637 2.02579 3 -1 -4 10 10.4244 3.78772 3 1 4 10 6.78697 2.53365 2 -1 4 -10 9.07673 2.31242 3 2 -4 10 235.202 9.22057 3 -2 -4 -10 237.618 9.59458 3 -2 4 10 247.261 8.84895 2 2 4 -10 239.613 9.46519 3 -2 -4 -10 234.555 9.65218 3 -2 4 10 238.860 9.26251 3 -2 -4 -10 248.014 10.5647 2 2 4 -10 271.474 10.1596 2 2 4 -10 237.415 9.71980 3 2 -4 10 241.995 10.7783 2 -2 4 10 241.544 9.65164 3 -2 -4 10 234.656 9.46802 3 -2 4 -10 227.950 9.46073 3 -2 4 -10 238.208 10.3817 2 -2 -4 10 221.682 9.90182 2 2 4 10 236.914 10.5566 2 -2 4 -10 230.772 9.22242 3 -2 -4 10 224.229 9.78412 3 2 4 10 236.153 9.58324 3 2 -4 -10 230.431 8.77151 2 2 4 10 239.743 9.40213 3 2 -4 -10 227.191 9.39597 3 -3 4 10 30.7410 3.27768 3 -3 4 10 28.1684 3.24916 2 -3 4 10 28.0002 3.32622 3 -3 -4 -10 18.9634 3.09905 3 3 -4 10 23.5762 2.78145 3 -3 -4 -10 29.6404 4.52602 2 3 4 -10 30.8788 4.03857 2 3 -4 10 32.8942 4.99134 2 3 -4 10 31.2405 3.37680 3 3 4 -10 27.2626 3.59074 3 -3 -4 -10 21.9135 3.09860 3 -3 4 -10 28.7032 3.32525 3 -3 -4 10 29.2360 3.98009 2 -3 -4 10 25.4944 3.30088 3 3 4 10 26.4677 3.33306 3 -3 4 -10 31.8820 4.47915 2 3 4 10 29.2384 3.43285 3 -3 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3 -5 -4 -10 111.815 6.24530 3 5 -4 10 111.194 5.40873 3 -5 -4 -10 110.206 6.36300 3 -5 4 10 112.613 6.27435 2 5 4 10 111.648 5.96925 3 -5 4 -10 129.610 8.88963 2 -5 4 -10 112.616 5.68255 3 -5 -4 10 129.328 8.11823 2 5 -4 -10 114.372 5.39938 3 -5 -4 10 110.506 6.52921 3 -5 4 -10 109.036 5.41135 3 -5 -4 10 110.737 6.36700 3 -6 -4 -10 37.2816 4.09417 3 -6 -4 -10 34.6805 6.31576 2 -6 4 10 30.5709 3.24517 3 -6 4 10 32.9707 3.52686 3 6 4 -10 32.6803 5.15386 2 -6 -4 -10 36.7332 4.27509 3 -6 4 10 35.3452 4.89582 2 6 4 -10 36.9124 3.78004 3 -6 4 10 35.0278 4.49888 2 6 -4 10 33.4216 6.82023 2 -6 4 -10 31.3247 2.88453 3 -6 -4 10 35.5269 4.47184 3 6 4 10 34.5789 3.51643 3 -6 4 -10 37.7844 3.22056 3 -6 -4 10 32.2574 5.61902 2 -6 -4 10 34.1217 4.29815 3 -7 -4 -10 8.17605 2.67983 3 -7 4 10 10.5265 3.64587 2 -7 4 10 8.13109 3.59589 2 -7 -4 -10 7.46520 2.64657 3 -7 -4 -10 -1.5854 4.63036 2 -7 -4 10 0.05346 4.55399 2 -7 4 -10 7.09004 4.64027 2 -7 -4 10 2.57737 2.53346 3 -7 -4 10 7.92103 2.85011 3 0 5 10 127.718 6.98877 3 0 -5 -10 96.8222 5.93646 3 0 5 -10 96.8307 6.05173 3 0 5 10 108.688 6.12630 2 0 5 -10 108.193 6.76524 2 0 5 10 107.893 6.17544 3 0 -5 10 110.766 6.39395 3 0 -5 -10 104.442 5.93109 2 0 -5 10 95.7022 5.67842 3 0 5 -10 107.761 5.88042 3 0 -5 10 101.081 6.62029 2 1 5 -10 191.747 8.32485 3 -1 5 10 190.076 8.11075 2 1 -5 10 187.982 9.21563 2 -1 -5 -10 179.902 8.73231 2 -1 -5 -10 185.182 8.47736 3 -1 -5 -10 186.910 8.45623 3 1 5 -10 181.022 8.85121 2 -1 5 10 192.032 8.47036 3 1 -5 10 179.945 8.47408 3 -1 5 10 195.363 8.29300 3 1 -5 10 184.381 8.08415 3 -1 -5 10 189.115 8.81698 2 1 -5 -10 200.824 8.15353 2 1 5 10 186.413 8.53900 3 1 5 10 198.750 8.99741 2 -1 -5 10 177.967 8.65807 3 -1 5 -10 188.006 8.46873 3 1 5 10 179.169 8.15875 3 1 -5 -10 186.306 8.28616 3 -1 5 -10 193.485 9.14459 2 2 -5 10 37.9427 3.81075 3 2 5 -10 31.3633 3.94014 3 -2 -5 -10 33.0583 4.21386 3 -2 5 10 34.3306 3.80878 3 -2 5 10 38.6609 3.92119 2 -2 -5 -10 35.2345 3.98142 3 2 -5 10 35.2125 4.83877 2 -2 -5 -10 38.4773 5.13121 2 -2 5 10 24.2839 3.47969 3 2 5 -10 36.9959 4.09007 3 2 5 -10 38.5199 4.79093 2 -2 -5 10 35.9724 4.87938 2 2 5 10 38.2420 4.75544 2 2 5 10 36.9163 4.03146 3 -2 -5 10 35.5251 4.11358 3 -2 5 -10 30.9165 4.46106 2 2 5 10 39.3548 4.16996 3 2 -5 -10 32.7254 4.08194 3 -2 5 -10 32.0771 3.74299 3 -2 5 -10 36.7633 4.05781 3 -2 -5 10 29.7546 3.25663 3 2 -5 -10 30.8443 3.80280 2 -3 5 10 113.794 5.94291 2 3 -5 10 109.839 5.97417 3 3 5 -10 115.691 7.09110 2 -3 -5 -10 106.920 6.38801 3 3 -5 10 109.085 6.20229 3 -3 -5 -10 115.658 7.67364 2 -3 5 10 106.470 6.27254 3 -3 5 10 105.055 5.84710 3 -3 -5 -10 110.094 6.51454 3 3 5 -10 117.465 6.65163 3 3 -5 10 105.568 7.99811 2 3 -5 -10 115.961 6.10175 3 -3 5 -10 108.003 7.41790 2 -3 -5 10 103.458 6.64932 3 3 5 10 103.153 6.07098 3 -3 -5 10 113.578 7.41844 2 3 -5 -10 113.145 6.08856 2 -3 5 -10 114.043 6.01882 3 -3 5 -10 109.189 6.20648 3 3 5 10 109.734 7.57583 2 3 -5 -10 112.066 6.12931 3 -3 -5 10 107.284 6.28054 3 -4 5 10 336.097 12.7176 2 -4 -5 -10 322.698 13.1667 3 4 -5 10 360.421 15.6350 2 4 5 -10 334.899 12.8691 3 4 5 -10 340.052 14.3683 2 -4 -5 -10 336.339 13.2564 3 4 -5 10 337.057 12.4073 3 -4 5 10 332.640 12.5468 3 -4 5 10 334.675 12.7457 3 -4 -5 -10 326.715 15.0302 2 4 -5 10 341.144 12.7580 3 4 5 -10 327.787 13.1895 3 4 -5 -10 340.640 12.9621 2 4 -5 -10 353.148 12.6552 3 4 5 10 353.329 13.0674 3 4 5 10 338.099 15.2669 2 -4 -5 10 324.751 13.1324 3 -4 5 -10 344.387 12.8237 3 -4 5 -10 353.117 12.6239 3 -4 5 -10 341.027 14.8357 2 -4 -5 10 331.884 13.4652 3 4 5 10 316.841 12.7494 3 -4 -5 10 344.098 14.1525 2 4 -5 -10 332.433 12.6332 3 5 5 -10 19.6822 3.13763 3 -5 -5 -10 14.2963 4.70428 2 -5 -5 -10 14.4178 3.15199 3 5 -5 10 17.8835 2.98976 3 -5 5 10 13.6469 3.63129 2 -5 -5 -10 13.8705 3.43578 3 -5 5 10 15.9242 2.85843 3 5 -5 10 13.8609 5.10526 2 5 5 -10 12.7373 3.97097 2 -5 -5 10 11.4166 4.40757 2 -5 5 -10 13.8295 2.93810 3 -5 -5 10 21.0479 3.77854 3 -5 5 -10 16.0288 2.81644 3 5 5 10 17.3844 3.13623 3 5 -5 -10 20.3608 3.87279 2 -5 -5 10 12.9700 3.26005 3 5 -5 -10 13.4917 2.66938 3 -6 -5 -10 185.959 8.76794 3 6 5 -10 188.630 8.40112 3 -6 -5 -10 176.634 8.79769 3 6 -5 10 185.195 12.4232 2 -6 5 10 180.461 7.86957 3 -6 5 10 184.547 9.22889 2 -6 5 10 183.176 7.70781 3 -6 -5 -10 177.409 11.8119 2 -6 5 10 174.248 9.70740 2 -6 -5 10 190.901 11.5109 2 -6 -5 10 192.371 9.16106 3 -6 5 -10 194.726 7.83945 3 -6 5 -10 180.743 7.46015 3 6 5 10 177.655 8.10177 3 -6 -5 10 195.834 9.05379 3 0 6 -10 122.332 6.87372 3 0 6 10 120.914 7.17720 2 0 -6 10 139.795 7.87632 3 0 -6 10 123.061 7.41780 3 0 6 -10 133.019 7.96919 2 0 6 10 154.885 8.16256 3 0 6 10 153.990 8.97194 3 0 -6 10 122.431 7.61368 2 0 -6 -10 113.555 7.10616 2 0 -6 -10 116.174 7.05560 3 0 6 -10 121.778 7.13746 3 -1 6 10 5.13068 2.75630 3 1 -6 10 -0.6475 3.01703 2 -1 6 10 4.67948 2.49199 3 1 6 -10 7.36973 3.57431 2 1 -6 10 6.45023 2.68618 3 1 6 -10 2.61206 2.79482 3 1 -6 10 2.89187 2.41733 3 -1 6 10 5.05299 2.69604 2 -1 -6 -10 7.22627 3.00640 3 1 6 -10 8.27028 3.39469 3 -1 -6 -10 7.43285 3.14764 2 -1 -6 -10 2.03804 2.72058 3 -1 6 -10 0.86310 3.44541 2 1 -6 -10 6.55481 2.69548 3 1 -6 -10 5.27496 2.90271 2 -1 -6 10 3.17714 2.72839 3 -1 -6 10 8.27913 3.48826 2 1 6 10 6.13904 2.89561 3 1 6 10 8.29690 4.56728 3 1 6 10 8.16435 3.20184 2 -1 6 -10 6.83672 2.87043 3 -1 -6 10 5.92885 3.06770 3 1 -6 -10 3.87275 2.49288 3 -1 6 -10 14.7203 4.34233 3 -2 -6 -10 454.495 18.1982 2 2 6 -10 492.283 18.2703 2 -2 6 10 446.875 16.8914 2 2 -6 10 470.552 17.1052 3 -2 -6 -10 458.854 17.4926 3 -2 6 10 458.422 17.2120 3 2 6 -10 470.183 17.3284 3 2 6 -10 485.733 17.6750 3 2 -6 10 470.436 18.7265 2 -2 6 10 467.445 17.0797 3 -2 -6 -10 468.145 17.5368 3 2 -6 -10 487.686 16.9867 2 -2 6 -10 475.392 18.4753 2 2 6 10 486.240 17.3467 3 -2 -6 10 544.648 17.6384 3 -2 6 -10 476.362 17.1369 3 2 6 10 474.611 18.5608 2 2 6 10 474.594 17.4246 3 2 -6 -10 490.149 17.3059 3 -2 6 -10 440.824 17.1931 3 -2 -6 10 464.861 17.7841 3 2 -6 -10 458.197 17.1835 3 -2 -6 10 489.772 18.1703 2 3 6 -10 149.069 7.67064 3 3 -6 10 147.332 7.34592 3 -3 6 10 146.848 7.68197 2 3 6 -10 151.427 8.81526 2 -3 -6 -10 146.880 8.05893 3 -3 -6 -10 151.670 9.22142 2 -3 6 10 146.419 7.64254 3 -3 6 10 155.903 7.50895 3 -3 -6 -10 149.685 8.05517 3 3 -6 10 150.640 7.66163 3 3 -6 10 142.737 9.29692 2 3 6 -10 150.462 8.01409 3 -3 -6 10 145.362 8.25934 3 3 -6 -10 151.565 7.59058 2 3 -6 -10 136.460 7.48104 3 3 6 10 151.103 7.69454 3 -3 6 -10 153.533 7.70148 3 -3 6 -10 151.291 9.40894 2 3 6 10 139.761 9.23602 2 3 -6 -10 144.621 7.41816 3 -3 -6 10 150.711 8.93800 2 -3 6 -10 142.316 7.25553 3 -3 -6 10 154.669 7.99663 3 3 6 10 144.475 7.68873 3 -4 -6 -10 168.296 8.79401 3 4 6 -10 171.500 9.93662 2 -4 6 10 173.962 8.08638 3 -4 6 10 162.388 8.43809 2 -4 -6 -10 168.953 8.73257 3 -4 -6 -10 168.790 10.3805 2 4 -6 10 177.876 10.9669 2 -4 6 10 177.157 8.35713 3 4 -6 10 175.636 8.35635 3 4 6 -10 173.287 8.39758 3 -4 -6 10 173.440 9.15721 3 -4 6 -10 177.466 8.36743 3 -4 6 -10 186.660 8.26981 3 4 6 10 174.799 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3 -1 3 -32 9.02256 4.05647 3 -1 -3 32 11.4279 4.60213 2 -1 -3 32 13.8986 5.32954 3 1 -3 -32 11.5513 4.03138 3 2 -3 32 69.0824 7.72340 3 2 3 -32 64.3303 6.85040 3 -2 -3 -32 62.4164 7.96468 3 2 -3 32 63.4063 8.64302 2 -2 -3 -32 53.4669 7.69739 2 -2 3 32 62.0710 7.51191 3 -2 3 32 53.4593 7.04433 3 -2 -3 -32 80.4394 9.83718 3 -2 -3 32 74.0418 6.95537 2 -2 3 -32 67.3507 7.44257 3 -2 -3 32 69.5765 8.04930 3 -2 -3 32 68.9748 7.73456 3 2 -3 -32 73.0855 7.32520 3 2 3 32 64.1348 7.80522 3 -2 3 -32 61.1825 7.56081 3 0 4 32 29.3481 5.56629 3 0 -4 32 28.4767 5.28294 3 0 4 -32 41.9020 6.69562 3 0 4 32 31.8691 6.16016 3 0 -4 -32 30.2475 6.46492 3 0 -4 32 29.4624 6.02491 2 0 -4 -32 22.8653 4.38222 3 0 -4 -32 19.3691 4.38424 2 0 -4 32 21.6639 6.28872 3 0 4 -32 36.5537 6.49567 3 1 4 -32 93.5837 8.35614 3 1 4 -32 70.3613 8.18559 2 1 -4 32 96.1980 8.86852 3 1 -4 32 106.118 9.45833 2 -1 -4 -32 88.8619 9.61817 3 -1 -4 -32 88.6009 8.23714 2 -1 4 32 102.286 9.35342 3 -1 -4 32 100.925 9.65480 3 -1 4 -32 92.7294 9.33867 3 -1 -4 32 94.2987 8.56754 3 1 4 32 93.8229 8.82851 3 -1 4 -32 90.2056 8.30112 3 1 -4 -32 94.7031 8.17246 3 -1 -4 32 105.078 8.57344 2 2 -4 32 81.0212 9.35983 2 -2 -4 -32 82.9745 9.39436 3 -2 -4 -32 78.2569 8.16943 3 2 4 -32 74.2323 7.66921 3 2 -4 32 98.0739 8.57064 3 -2 4 32 91.5079 9.61178 3 -2 -4 -32 78.6855 8.50055 2 -2 4 32 76.0356 8.81740 3 -2 -4 32 99.1662 8.31849 2 -2 -4 32 90.7207 8.57585 3 2 4 32 75.2832 7.96485 3 -2 4 -32 89.2951 8.26268 3 -2 -4 32 80.0221 9.00211 3 2 -4 -32 82.5111 7.66201 3 -2 4 -32 74.8377 8.90972 3 0 5 -32 89.2474 12.3318 3 0 -5 32 57.6346 7.60468 3 0 -5 -32 41.5874 5.61124 3 0 -5 32 63.9029 8.04546 2 0 5 -32 52.1260 6.82656 3 0 -5 -32 40.2374 5.18853 2 0 5 32 55.5693 6.83701 3 0 5 32 64.4947 9.15565 3 1 -5 32 10.3142 5.06340 2 -1 5 32 8.52223 4.86906 3 1 5 -32 1.71624 4.45878 3 -1 -5 -32 -1.1390 4.37460 2 1 -5 32 4.56708 4.85350 3 -1 5 32 2.47904 4.24620 3 -1 -5 -32 -1.2260 3.67985 3 -1 -5 -32 15.3136 5.88172 3 -1 5 -32 12.4274 4.95409 3 -1 5 -32 11.1823 4.91839 3 -1 -5 32 20.6717 9.88116 3 -1 -5 32 13.5819 5.15542 2 1 5 32 10.4170 5.25169 3 1 -5 -32 12.6794 4.50317 3 -1 -5 32 17.8452 5.86338 3 0 0 -33 47.2164 6.27865 2 0 0 33 64.9598 8.12067 3 0 0 -33 70.6337 6.24380 2 0 0 -33 102.371 12.6811 3 1 0 -33 24.5547 3.84674 2 1 0 -33 19.4069 3.68449 2 1 0 -33 27.1272 5.25107 3 -1 0 -33 18.1341 4.96738 3 -1 0 33 19.4135 4.67621 3 -1 0 -33 23.7365 5.15832 2 1 0 33 27.0151 5.33260 3 -1 0 33 20.7837 5.50489 3 -1 0 -33 29.3978 6.65912 3 2 0 33 -4.7250 3.86579 3 -2 0 -33 -1.8887 4.02819 3 -2 0 -33 4.66258 5.05204 3 -2 0 33 -1.6374 7.73715 3 2 0 -33 -1.3500 3.60205 3 -2 0 -33 1.67203 4.28956 2 -2 0 33 -2.9839 3.88117 3 -3 0 -33 5.26413 4.28820 3 -3 0 -33 1.33815 4.77305 2 -3 0 33 0.95722 3.58670 3 3 0 -33 6.14585 3.81851 3 -3 0 33 2.17266 4.34838 3 -3 0 -33 0.74743 4.69000 3 3 0 33 9.65926 4.30140 3 0 1 -33 44.6029 6.15025 2 0 -1 -33 57.8195 8.09338 3 0 1 -33 63.6229 6.61075 2 0 -1 33 37.9386 6.11725 3 0 -1 -33 42.6714 5.71069 2 0 -1 33 46.1443 6.41001 3 0 1 -33 65.6559 9.50021 3 0 1 -33 68.9560 9.23192 3 0 -1 -33 42.9948 6.95910 3 0 1 33 44.9874 6.35393 3 0 1 33 38.2801 6.27109 3 -1 1 33 37.0778 8.31969 3 1 -1 33 12.8395 4.73917 3 -1 -1 -33 18.5748 5.34930 3 -1 -1 -33 25.3932 5.35924 2 1 1 -33 23.4128 7.75861 3 1 1 -33 19.2649 3.76074 2 1 1 -33 24.5229 5.29112 3 1 1 -33 15.2433 4.03850 2 -1 -1 -33 16.1134 4.92239 3 -1 1 33 24.5994 5.41296 3 1 -1 -33 21.5754 3.45118 2 -1 1 -33 26.2244 5.31588 2 -1 1 -33 22.2995 6.50235 3 1 -1 -33 22.9459 3.39633 2 1 -1 -33 21.1204 4.86168 3 1 1 33 21.2971 5.63435 3 -1 1 -33 18.7317 4.80132 3 -1 -1 33 22.4297 5.81235 3 -1 -1 33 16.5872 5.07037 3 -2 1 33 10.8133 4.51275 3 2 1 -33 7.63128 4.10918 3 -2 -1 -33 9.99306 5.05227 2 -2 -1 -33 8.90566 4.58104 3 -2 1 33 7.60611 4.57768 3 2 -1 33 10.8384 4.29724 3 -2 -1 -33 13.1966 5.39427 3 -2 -1 33 8.99586 4.30767 3 2 -1 -33 15.8244 4.58937 3 2 1 33 12.0236 4.38783 3 -2 1 -33 9.67880 4.57206 3 -2 1 -33 14.5735 5.14132 2 -2 -1 33 14.1899 5.01797 3 -2 1 -33 7.22098 5.10465 3 3 1 -33 -47.107 70.3965 1 -3 -1 -33 14.8578 44.8220 1 3 -1 -33 29.6695 61.1675 1 -3 1 -33 15.1918 44.3092 1 0 -2 -33 13.7277 3.93227 2 0 -2 33 14.7845 5.07905 3 0 -2 33 11.6203 4.64233 2 0 -2 -33 16.0041 5.08338 3 0 2 -33 13.3393 5.52513 3 0 2 -33 22.7970 4.95928 2 0 2 33 27.8301 8.09339 3 0 -2 33 31.2426 7.12805 3 0 -2 -33 21.8605 9.16625 3 0 2 33 18.5669 4.97954 3 -1 2 33 42.3639 6.44092 3 1 -2 33 60.1399 7.71833 2 -1 -2 -33 53.2965 6.72566 3 1 2 -33 39.4473 5.33025 2 -1 -2 -33 47.0572 6.68288 2 -1 2 33 57.9482 7.25876 3 -1 -2 -33 67.2924 8.44479 3 1 -2 33 64.4959 7.86994 3 -1 2 -33 48.6688 7.14237 3 1 -2 -33 78.3428 9.39854 3 -1 -2 33 47.3708 6.39118 3 -1 -2 33 56.0188 6.50428 2 1 2 33 57.6294 7.48470 3 -1 -2 33 51.7451 7.04991 3 -2 -2 -33 24.1937 5.66635 2 -2 2 33 29.3422 5.56935 3 2 -2 33 26.1197 5.28404 3 -2 -2 -33 40.0180 7.29642 3 -2 2 33 23.8661 5.12476 3 -2 -2 -33 24.0443 5.07643 3 -2 -2 33 27.7269 5.32289 3 -2 -2 33 36.8120 6.12618 3 2 2 33 34.9020 6.00784 3 -2 2 -33 32.8467 6.24888 2 -2 2 -33 29.0047 5.34854 3 -2 2 -33 29.0582 6.26459 3 2 -2 -33 29.6234 4.92015 3 0 -3 33 54.4825 7.44468 2 0 3 33 57.4933 7.13175 3 0 -3 -33 42.1602 5.63291 2 0 -3 -33 41.1320 7.14547 3 0 -3 33 58.8764 9.36621 3 0 3 -33 37.4420 5.30051 3 0 3 -33 40.8105 7.13620 3 0 3 -33 47.7650 7.16413 2 0 3 33 38.8427 5.93527 3 0 -3 33 45.9263 7.33043 3 0 -3 -33 53.1147 6.78533 3 1 3 -33 28.5869 5.40173 2 -1 -3 -33 41.3678 5.85860 2 -1 -3 -33 71.8325 10.3834 3 1 -3 33 44.4158 6.47213 3 1 3 -33 35.1208 5.12677 3 1 -3 33 56.1875 7.73117 2 -1 3 33 53.0895 6.90354 3 -1 3 33 51.5357 7.19991 3 -1 -3 -33 50.4042 7.64051 3 -1 -3 33 35.5188 5.60248 3 -1 3 -33 41.1722 7.02715 3 -1 -3 33 55.0787 6.90214 2 1 3 33 35.5661 5.85322 3 1 -3 -33 54.7689 8.40425 3 -1 3 -33 52.4238 7.90517 3 -1 -3 33 43.1016 6.09731 3 -2 3 33 -0.8702 4.42409 3 -2 3 33 2.95007 4.15871 3 2 -3 33 0.36563 3.76636 3 -2 -3 -33 -0.6351 4.44266 2 2 3 -33 0.18163 4.17815 3 -2 -3 -33 -1.8115 3.56980 3 2 -3 33 6.74046 4.91113 2 -2 -3 -33 2.38410 4.08227 3 2 3 33 -4.5094 3.31090 3 2 -3 -33 8.68067 4.05770 3 -2 -3 33 -0.1756 3.57312 3 -2 -3 33 2.11216 3.82314 2 -2 -3 33 1.87987 4.39276 3 -2 3 -33 1.83827 5.09210 3 0 4 33 76.9336 8.11185 3 0 -4 33 88.1024 9.15939 2 0 -4 33 72.3239 8.71821 3 0 -4 -33 80.4278 7.95553 3 0 4 33 79.9060 8.86770 3 0 4 -33 76.9003 9.40515 3 0 4 -33 84.9677 8.52720 3 0 -4 -33 85.1074 9.92870 3 1 4 -33 108.096 10.8296 3 -1 -4 -33 66.1808 7.86782 3 1 -4 33 65.6747 8.18376 3 -1 4 33 78.6333 7.93684 3 -1 4 33 95.8544 11.3505 3 -1 -4 -33 52.4641 7.35050 2 -1 -4 -33 77.2416 9.19050 3 1 -4 33 83.4400 9.34903 2 -1 -4 33 70.5226 7.69723 2 -1 4 -33 61.3268 7.84278 3 -1 4 -33 72.7271 7.81346 3 -1 -4 33 102.036 11.8686 3 1 4 33 65.8002 8.23557 3 1 -4 -33 87.9473 9.54067 3 0 0 -34 519.440 22.3014 3 0 0 34 480.970 20.6789 3 0 0 34 527.991 21.7344 3 0 0 -34 532.032 21.2652 3 0 0 -34 538.807 20.1864 2 0 0 -34 539.583 19.5502 2 1 0 -34 -1.9721 2.61115 2 -1 0 -34 2.37115 4.23563 3 -1 0 34 0.59499 3.55431 3 -1 0 -34 1.10832 5.22169 3 1 0 -34 2.62788 4.29845 3 1 0 34 1.34296 4.29221 3 -1 0 34 -1.1535 4.61917 3 -1 0 -34 0.11478 4.17727 2 1 0 -34 -6.6940 2.96698 2 -2 0 34 -0.6936 5.81654 3 -2 0 34 8.54379 4.96879 3 -2 0 -34 2.54824 5.03134 3 2 0 34 3.83774 4.38775 3 -2 0 -34 3.06872 4.52768 3 -2 0 -34 -4.9156 4.06924 2 2 0 -34 10.3901 4.15926 3 0 1 -34 121.074 8.51540 2 0 1 34 155.566 13.0628 3 0 1 34 104.437 9.54566 3 0 -1 34 94.9046 9.05755 3 0 -1 -34 100.325 10.3477 3 0 -1 34 114.634 9.88711 3 0 1 -34 120.756 9.44565 3 0 1 -34 133.761 8.36627 2 0 -1 -34 95.7164 7.56730 2 0 -1 -34 144.277 12.0988 3 1 1 -34 180.156 9.02264 2 -1 1 34 150.728 10.5065 3 -1 1 34 207.190 13.8280 3 1 1 -34 183.637 10.8941 3 -1 -1 -34 162.726 10.7533 3 1 1 -34 161.406 8.72918 2 -1 -1 -34 163.846 11.8923 3 -1 -1 -34 168.223 10.4146 2 1 -1 34 178.428 11.2536 3 1 -1 -34 165.801 7.81932 2 -1 -1 34 184.315 12.4429 3 1 1 34 177.651 11.1864 3 1 -1 -34 147.463 7.73200 2 -1 1 -34 175.755 10.9361 2 -1 1 -34 211.616 15.2399 3 -1 1 -34 168.232 10.8224 3 -1 -1 34 188.069 11.9151 3 1 -1 -34 176.234 10.7839 3 -2 -1 -34 12.4382 4.74159 3 -2 1 34 18.2151 7.36125 3 -2 -1 -34 14.0204 5.81256 3 2 1 -34 7.02505 4.25721 3 2 -1 34 1.60351 3.85070 3 -2 1 34 9.69143 6.58194 3 -2 -1 -34 5.01820 4.88889 2 2 -1 -34 31.0981 7.76837 3 -2 -1 34 1.33244 4.54974 3 2 1 34 10.1957 4.41134 3 -2 1 -34 4.16901 4.68561 2 -2 1 -34 10.0281 5.38149 3 -2 1 -34 -4.2934 3.87424 3 -2 -1 34 2.47770 4.42865 3 0 2 34 75.1414 8.43847 3 0 -2 34 69.0195 8.48580 3 0 -2 34 56.8541 8.34496 3 0 2 34 60.1492 7.67767 3 0 -2 34 67.2498 7.54737 2 0 2 -34 67.5251 7.42765 2 0 2 -34 119.443 13.9692 3 0 -2 -34 82.4407 9.53673 3 0 -2 -34 58.6009 6.17184 2 0 -2 -34 67.7321 7.92296 3 -1 -2 -34 137.065 9.67260 3 -1 2 34 136.878 9.71276 3 1 2 -34 100.619 7.93050 2 1 -2 34 106.325 9.50549 2 -1 -2 -34 116.073 10.3368 3 1 -2 34 123.928 9.72544 3 -1 -2 -34 117.014 8.98884 2 -1 2 34 160.306 12.8110 3 -1 -2 34 156.349 12.5643 3 1 2 34 108.602 9.41729 3 1 -2 -34 137.939 9.41038 3 -1 -2 34 113.605 9.63680 3 -1 2 -34 132.950 10.9506 3 2 2 -34 149.367 7.47997 2 -2 2 34 120.443 9.63773 3 -2 -2 -34 144.498 10.9052 3 -2 -2 -34 141.828 10.3632 2 2 -2 34 143.146 10.3126 3 -2 2 34 133.713 10.3687 3 -2 -2 -34 136.741 9.79191 3 -2 2 -34 141.646 10.7858 2 -2 -2 34 128.236 10.4387 3 -2 2 -34 139.126 11.0523 3 2 -2 -34 162.064 9.74989 3 -2 -2 34 139.951 10.1751 3 -2 2 -34 142.486 10.1337 3 0 3 34 12.8724 4.96368 3 0 3 34 7.98131 4.67211 3 0 -3 -34 16.6169 5.80464 3 0 -3 34 13.4891 5.02922 2 0 -3 34 3.58218 3.77302 3 0 -3 -34 4.14046 4.10671 3 0 -3 -34 0.95114 3.49651 2 0 3 -34 6.37265 3.26513 3 0 3 -34 16.4028 5.66630 3 1 -3 34 25.4799 6.02809 3 1 -3 34 20.0264 5.60988 2 -1 -3 -34 16.7118 4.85196 2 -1 3 34 25.1633 5.58015 3 1 3 -34 7.87034 4.82276 2 -1 -3 -34 17.1816 4.75508 3 1 3 -34 8.15457 3.06687 3 -1 -3 -34 29.0526 6.38127 3 -1 3 34 16.9597 5.22851 3 1 3 34 23.9751 5.80384 3 -1 -3 34 17.9247 5.43194 3 -1 3 -34 32.0729 6.76700 3 -1 3 -34 21.0324 4.63065 3 -1 -3 34 18.5873 4.98908 3 1 -3 -34 47.4607 9.20072 3 -1 -3 34 22.1155 5.25957 2 0 0 -35 63.0797 6.73181 2 0 0 35 30.3567 6.44903 3 0 0 -35 42.4534 6.92020 3 1 0 -35 -2.5481 2.54432 2 1 0 -35 -3.7193 3.86693 3 1 0 35 -0.3592 4.51260 3 -1 0 -35 0.71559 4.87536 3 -1 0 -35 0.23129 4.12643 3 -1 0 -35 -0.7336 4.38776 2 -1 0 35 0.25999 4.05192 3 -1 0 35 -2.1942 4.45377 3 0 -1 -35 -0.7054 3.65002 3 0 -1 -35 0.11007 4.58585 3 0 1 35 5.52204 4.59995 3 0 1 35 -0.6524 4.00775 3 0 -1 -35 -4.6664 3.19200 2 0 1 -35 10.5033 5.83892 3 0 -1 35 0.26563 4.23952 3 0 1 -35 4.93308 3.94904 2 0 1 -35 10.6048 4.36377 2 0 1 -35 4.59681 4.54569 3 -1 -1 -35 16.2888 5.61556 3 1 1 -35 14.8014 4.95325 3 -1 -1 -35 8.20137 4.52722 2 1 1 -35 0.06964 3.82821 2 1 -1 35 16.7483 5.41382 3 1 1 -35 12.1760 3.65052 2 -1 1 35 1.98041 4.32481 3 -1 1 35 14.7873 5.12929 3 -1 -1 -35 8.57199 4.72173 3 1 -1 -35 8.49370 3.21566 2 1 -1 -35 11.0661 5.65038 3 1 -1 -35 6.30438 2.82416 2 1 1 35 12.6352 5.52782 3 -1 1 -35 11.2934 5.97554 3 -1 1 -35 18.2939 4.98593 2 -1 -1 35 11.7462 5.19461 3 -1 -1 35 16.3661 6.96029 3 0 2 35 14.4979 5.40193 3 0 2 35 11.5675 7.41692 3 0 -2 -35 3.59600 3.49163 2 0 -2 -35 35.6404 10.6440 3 0 -2 -35 12.7010 4.51811 3 0 -2 35 15.2710 5.23065 3 0 2 -35 12.6914 4.48192 2 0 2 -35 8.78919 4.74506 2 0 2 -35 13.6754 6.06164 3 0 0 0 0.00 0.00 0 _exptl_absorpt_process_details 'SADABS 2014/5' _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_max 0.9585 _exptl_absorpt_correction_T_min 0.8980 _exptl_special_details ) The following wavelength and cell were deduced by SADABS from the direction cosines etc. They are given here for emergency use only: CELL 0.71073 6.388 9.449 28.593 90.005 90.004 89.995 ) ; _shelx_hkl_checksum 48403 data_uv129 # start Validation Reply Form _vrf_PLAT410_uv129 ; PROBLEM: Short Intra H...H Contact H1A .. H11 .. 1.88 Ang. RESPONSE: The mentioned hydrogen atoms have been added by AFIX instructions. We should accept that. ; _vrf_PLAT420_uv129 ; PROBLEM: D-H Without Acceptor O3 -- H3 ... Please Check RESPONSE: There seems to be no acceptor. ; _vrf_PLAT987_uv129 ; PROBLEM: The Flack x is >> 0 - Do a BASF/TWIN Refinement Please Check RESPONSE: According the author the compound is enantiomeric pure. ; # end Validation Reply Form _audit_update_record 30-Mar-16 _chemical_name_common NL-1957p _chemical_compound_source ? _chemical_absolute_configuration 'syn' _exptl_crystal_description block _exptl_crystal_colour colourless _exptl_crystal_size_max 0.070 #?# in millimeters _exptl_crystal_size_mid 0.050 #?# in millimeters _exptl_crystal_size_min 0.030 #?# in millimeters _exptl_crystal_density_method 'not measured' _exptl_crystal_density_meas ? _exptl_special_details ; ; _audit_author_name 'P. Mayer' #?# X-ray operator _audit_creation_date ? #?# style: 18-Aug-1998 _diffrn_ambient_temperature 100.(2) #?# in K _diffrn_source_type 'Bruker TXS' _diffrn_source_power 2.5 #?# in kW _diffrn_source_voltage 50 #?# in kV _diffrn_source_current 50 #?# in mA _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'rotating anode (TXS)' _diffrn_radiation_monochromator 'focusing mirrors' _diffrn_radiation_collimation ? _diffrn_measurement_device 'fixed-chi three-circle diffractometer' _diffrn_measurement_device_type 'Bruker D8 Venture TXS' _diffrn_measurement_method 'mix of phi and omega scans' _diffrn_measurement_details ? _diffrn_detector_area_resol_mean 7.4074 _diffrn_special_details ? _diffrn_orient_matrix_type ? _diffrn_orient_matrix_UB_11 ? _diffrn_orient_matrix_UB_12 ? _diffrn_orient_matrix_UB_13 ? _diffrn_orient_matrix_UB_21 ? _diffrn_orient_matrix_UB_22 ? _diffrn_orient_matrix_UB_23 ? _diffrn_orient_matrix_UB_31 ? _diffrn_orient_matrix_UB_32 ? _diffrn_orient_matrix_UB_33 ? _cell_length_a 7.2444(5) _cell_length_b 10.8801(7) _cell_length_c 23.8676(15) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 1881.2(2) _cell_measurement_temperature 100.(2) #?# in K _cell_measurement_reflns_used 9830 _cell_measurement_theta_min 2.9385 _cell_measurement_theta_max 28.2893 _cell_special_details ? _exptl_absorpt_coefficient_mu 2.200 _exptl_absorpt_correction_type Multi-Scan _exptl_absorpt_correction_T_min 0.6527 _exptl_absorpt_correction_T_max 0.6985 _shelx_estimated_absorpt_T_min 0.861 _shelx_estimated_absorpt_T_max 0.937 _exptl_absorpt_process_details ; SADABS-2014/5 - Bruker AXS area detector scaling and absorption correction ; _diffrn_reflns_number 33734 #xl _diffrn_reflns_av_R_equivalents 0.0687 #xl _diffrn_reflns_av_unetI/netI 0.0441 #xl _diffrn_reflns_limit_h_min -9 #xl _diffrn_reflns_limit_h_max 9 #xl _diffrn_reflns_limit_k_min -14 #xl _diffrn_reflns_limit_k_max 14 #xl _diffrn_reflns_limit_l_min -31 #xl _diffrn_reflns_limit_l_max 31 #xl _diffrn_reflns_theta_min 3.172 #xl _diffrn_reflns_theta_max 28.271 #xl _diffrn_measured_fraction_theta_max 0.997 #xl _diffrn_reflns_theta_full 25.242 #xl _diffrn_measured_fraction_theta_full 0.996 #xl _diffrn_reflns_Laue_measured_fraction_max 0.997 #xl _diffrn_reflns_Laue_measured_fraction_full 0.996 #xl _diffrn_reflns_point_group_measured_fraction_max 0.996 #xl _diffrn_reflns_point_group_measured_fraction_full 0.994 #xl _space_group_crystal_system orthorhombic _space_group_name_H-M_alt 'P 21 21 21' _space_group_name_Hall 'P 2ac 2ab' _space_group_IT_number 19 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Br' 'Br' -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _reflns_number_total 4655 #xl _reflns_number_gt 4453 #xl _reflns_threshold_expression 'I > 2\s(I)' #xl _reflns_Friedel_coverage 0.742 #xl _reflns_Friedel_fraction_max 0.993 #xl _reflns_Friedel_fraction_full 0.992 #xl _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _refine_ls_structure_factor_coef Fsqd #xl _refine_ls_matrix_type full #xl _refine_ls_weighting_scheme calc #xl _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0293P)^2^+0.8784P] where P=(Fo^2^+2Fc^2^)/3' #xl _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none #xl _refine_ls_extinction_coef . #xl _refine_ls_abs_structure_details ; Flack x determined using 1769 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.107(5) #xl _refine_ls_number_reflns 4655 #xl _refine_ls_number_parameters 230 #xl _refine_ls_number_restraints 0 #xl _refine_ls_R_factor_all 0.0317 #xl _refine_ls_R_factor_gt 0.0301 #xl _refine_ls_wR_factor_ref 0.0740 #xl _refine_ls_wR_factor_gt 0.0735 #xl _refine_ls_goodness_of_fit_ref 1.062 #xl _refine_ls_restrained_S_all 1.062 #xl _refine_ls_shift/su_max 0.000 #xl _refine_ls_shift/su_mean 0.000 #xl _refine_diff_density_max 0.337 #xl _refine_diff_density_min -0.499 #xl _refine_diff_density_rms 0.064 #xl _refine_special_details ; C-H: constr O-H: refall ; _computing_data_collection 'APEX3 (Bruker AXS Inc., 2015)' _computing_cell_refinement 'SAINT V8.35A (Bruker AXS Inc., 2015)' _computing_data_reduction 'SAINT V8.35A (Bruker AXS Inc., 2015)' _computing_structure_solution 'XT, VERSION 2014/4' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics 'shelXle (C.B. Huebschle, rev 740)' _computing_publication_material ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Br1 Br 0.57629(4) 0.42256(3) 0.12826(2) 0.02220(10) Uani 1 1 d . . . . . O1 O 0.5593(4) 0.34049(19) 0.25697(9) 0.0163(4) Uani 1 1 d . . . . . H1 H 0.498(7) 0.310(5) 0.233(2) 0.041(14) Uiso 1 1 d . . . . . O2 O 0.6564(3) 0.65920(19) 0.29759(9) 0.0112(4) Uani 1 1 d . . . . . O3 O 0.4083(4) 0.3636(2) 0.45248(10) 0.0201(5) Uani 1 1 d . . . . . H3 H 0.326(7) 0.398(5) 0.436(2) 0.038(14) Uiso 1 1 d . . . . . C1 C 0.6882(4) 0.4937(3) 0.19634(12) 0.0131(6) Uani 1 1 d . . . . . H1A H 0.8046 0.4469 0.2035 0.016 Uiso 1 1 calc R U . . . C2 C 0.5601(4) 0.4701(3) 0.24715(12) 0.0123(5) Uani 1 1 d . . . . . C3 C 0.6417(4) 0.5250(3) 0.30252(12) 0.0098(5) Uani 1 1 d . . . . . C4 C 0.5238(4) 0.4921(3) 0.35337(12) 0.0119(6) Uani 1 1 d . . . . . H4A H 0.4186 0.5498 0.3561 0.014 Uiso 1 1 calc R U . . . H4B H 0.4735 0.4081 0.3487 0.014 Uiso 1 1 calc R U . . . C5 C 0.6368(4) 0.4980(3) 0.40703(12) 0.0114(5) Uani 1 1 d . . . . . H5 H 0.6783 0.5851 0.4114 0.014 Uiso 1 1 calc R U . . . C6 C 0.5386(4) 0.4620(3) 0.46239(12) 0.0143(6) Uani 1 1 d . . . . . C7 C 0.6955(4) 0.4077(3) 0.49910(13) 0.0174(6) Uani 1 1 d . . . . . H7A H 0.7044 0.4527 0.5351 0.021 Uiso 1 1 calc R U . . . H7B H 0.6716 0.3199 0.5072 0.021 Uiso 1 1 calc R U . . . C8 C 0.8746(4) 0.4221(3) 0.46544(12) 0.0162(6) Uani 1 1 d . . . . . H8A H 0.9612 0.3541 0.4737 0.019 Uiso 1 1 calc R U . . . H8B H 0.9357 0.5011 0.4742 0.019 Uiso 1 1 calc R U . . . C9 C 0.8128(4) 0.4185(3) 0.40381(11) 0.0121(5) Uani 1 1 d . . . . . C10 C 0.9466(4) 0.4809(3) 0.36328(12) 0.0134(5) Uani 1 1 d . . . . . H10A H 1.0528 0.4255 0.3566 0.016 Uiso 1 1 calc R U . . . H10B H 0.9945 0.5569 0.3809 0.016 Uiso 1 1 calc R U . . . C11 C 0.8576(4) 0.5141(3) 0.30639(12) 0.0110(5) Uani 1 1 d . . . . . H11 H 0.9066 0.4602 0.2759 0.013 Uiso 1 1 calc R U . . . C12 C 0.8567(4) 0.6518(3) 0.28767(13) 0.0121(6) Uani 1 1 d . . . . . C13 C 0.8962(4) 0.6718(3) 0.22547(13) 0.0151(6) Uani 1 1 d . . . . . H13A H 1.0130 0.6294 0.2159 0.018 Uiso 1 1 calc R U . . . H13B H 0.9153 0.7608 0.2190 0.018 Uiso 1 1 calc R U . . . C14 C 0.7443(4) 0.6263(3) 0.18526(13) 0.0156(6) Uani 1 1 d . . . . . H14A H 0.6345 0.6797 0.1892 0.019 Uiso 1 1 calc R U . . . H14B H 0.7892 0.6334 0.1462 0.019 Uiso 1 1 calc R U . . . C15 C 0.3657(4) 0.5199(3) 0.23831(13) 0.0152(6) Uani 1 1 d . . . . . H15A H 0.2864 0.4936 0.2693 0.023 Uiso 1 1 calc R U . . . H15B H 0.3161 0.4883 0.2029 0.023 Uiso 1 1 calc R U . . . H15C H 0.3695 0.6099 0.2370 0.023 Uiso 1 1 calc R U . . . C16 C 0.4324(5) 0.5699(3) 0.48991(12) 0.0171(5) Uani 1 1 d . . . . . H16 H 0.3328 0.5952 0.4633 0.021 Uiso 1 1 calc R U . . . C17 C 0.5515(5) 0.6837(3) 0.50145(15) 0.0237(7) Uani 1 1 d . . . . . H17A H 0.4789 0.7445 0.5222 0.036 Uiso 1 1 calc R U . . . H17B H 0.5922 0.7194 0.4658 0.036 Uiso 1 1 calc R U . . . H17C H 0.6596 0.6599 0.5236 0.036 Uiso 1 1 calc R U . . . C18 C 0.3381(5) 0.5293(3) 0.54447(14) 0.0225(7) Uani 1 1 d . . . . . H18A H 0.2595 0.5959 0.5584 0.034 Uiso 1 1 calc R U . . . H18B H 0.4323 0.5097 0.5726 0.034 Uiso 1 1 calc R U . . . H18C H 0.2625 0.4563 0.5373 0.034 Uiso 1 1 calc R U . . . C19 C 0.7750(4) 0.2850(3) 0.38523(13) 0.0168(6) Uani 1 1 d . . . . . H19A H 0.8875 0.2359 0.3897 0.025 Uiso 1 1 calc R U . . . H19B H 0.7371 0.2842 0.3458 0.025 Uiso 1 1 calc R U . . . H19C H 0.6763 0.2500 0.4084 0.025 Uiso 1 1 calc R U . . . C20 C 0.9561(4) 0.7452(3) 0.32370(14) 0.0185(6) Uani 1 1 d . . . . . H20A H 1.0897 0.7353 0.3191 0.028 Uiso 1 1 calc R U . . . H20B H 0.9228 0.7325 0.3631 0.028 Uiso 1 1 calc R U . . . H20C H 0.9200 0.8283 0.3122 0.028 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Br1 0.02323(15) 0.03125(17) 0.01212(13) -0.00320(13) -0.00238(12) -0.00329(15) O1 0.0221(11) 0.0113(10) 0.0155(10) 0.0002(8) -0.0042(10) -0.0027(10) O2 0.0084(9) 0.0086(10) 0.0164(10) 0.0011(8) 0.0004(8) -0.0004(8) O3 0.0201(12) 0.0168(11) 0.0233(11) 0.0018(9) 0.0020(11) -0.0055(10) C1 0.0136(13) 0.0160(14) 0.0097(13) -0.0002(11) -0.0022(10) 0.0003(12) C2 0.0106(13) 0.0139(13) 0.0123(12) 0.0004(10) -0.0024(11) -0.0028(12) C3 0.0090(12) 0.0082(12) 0.0124(13) 0.0004(11) 0.0008(10) 0.0008(10) C4 0.0088(12) 0.0133(13) 0.0135(13) 0.0001(11) 0.0006(10) 0.0001(10) C5 0.0124(12) 0.0107(13) 0.0110(13) 0.0005(10) 0.0002(10) -0.0007(11) C6 0.0158(15) 0.0145(13) 0.0125(13) 0.0016(11) 0.0012(11) -0.0016(11) C7 0.0193(14) 0.0184(15) 0.0145(13) 0.0044(13) -0.0003(11) 0.0021(13) C8 0.0168(13) 0.0171(13) 0.0148(13) 0.0024(13) -0.0018(10) 0.0011(13) C9 0.0118(12) 0.0100(12) 0.0144(13) 0.0018(12) 0.0003(10) 0.0007(12) C10 0.0097(12) 0.0166(13) 0.0139(13) 0.0013(11) -0.0012(11) 0.0008(11) C11 0.0098(12) 0.0112(13) 0.0119(13) 0.0000(11) 0.0015(10) 0.0004(11) C12 0.0088(12) 0.0115(14) 0.0160(14) 0.0022(11) -0.0017(11) -0.0023(11) C13 0.0125(14) 0.0153(13) 0.0176(14) 0.0054(11) 0.0015(11) -0.0011(11) C14 0.0144(14) 0.0170(14) 0.0153(14) 0.0048(12) 0.0007(12) 0.0018(12) C15 0.0102(13) 0.0200(15) 0.0153(14) 0.0006(12) -0.0027(10) -0.0011(12) C16 0.0207(13) 0.0166(13) 0.0141(12) 0.0019(12) 0.0040(12) 0.0007(16) C17 0.0285(19) 0.0185(15) 0.0242(16) -0.0025(13) 0.0051(14) 0.0020(14) C18 0.0268(16) 0.0224(16) 0.0183(16) 0.0023(13) 0.0102(13) 0.0016(14) C19 0.0187(14) 0.0110(13) 0.0209(16) 0.0019(11) 0.0018(12) 0.0018(12) C20 0.0161(15) 0.0146(14) 0.0247(16) 0.0014(12) -0.0015(12) -0.0044(12) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Br1 C1 1.974(3) . ? O1 C2 1.430(4) . ? O1 H1 0.80(5) . ? O2 C3 1.469(3) . ? O2 C12 1.473(3) . ? O3 C6 1.446(4) . ? O3 H3 0.80(5) . ? C1 C14 1.522(4) . ? C1 C2 1.549(4) . ? C1 H1A 1.0000 . ? C2 C15 1.524(4) . ? C2 C3 1.566(4) . ? C3 C4 1.526(4) . ? C3 C11 1.572(4) . ? C4 C5 1.521(4) . ? C4 H4A 0.9900 . ? C4 H4B 0.9900 . ? C5 C9 1.543(4) . ? C5 C6 1.551(4) . ? C5 H5 1.0000 . ? C6 C16 1.550(4) . ? C6 C7 1.552(4) . ? C7 C8 1.534(4) . ? C7 H7A 0.9900 . ? C7 H7B 0.9900 . ? C8 C9 1.538(4) . ? C8 H8A 0.9900 . ? C8 H8B 0.9900 . ? C9 C10 1.529(4) . ? C9 C19 1.543(4) . ? C10 C11 1.546(4) . ? C10 H10A 0.9900 . ? C10 H10B 0.9900 . ? C11 C12 1.564(4) . ? C11 H11 1.0000 . ? C12 C20 1.513(4) . ? C12 C13 1.527(4) . ? C13 C14 1.542(4) . ? C13 H13A 0.9900 . ? C13 H13B 0.9900 . ? C14 H14A 0.9900 . ? C14 H14B 0.9900 . ? C15 H15A 0.9800 . ? C15 H15B 0.9800 . ? C15 H15C 0.9800 . ? C16 C17 1.535(5) . ? C16 C18 1.535(4) . ? C16 H16 1.0000 . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? C18 H18A 0.9800 . ? C18 H18B 0.9800 . ? C18 H18C 0.9800 . ? C19 H19A 0.9800 . ? C19 H19B 0.9800 . ? C19 H19C 0.9800 . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C2 O1 H1 107(4) . . ? C3 O2 C12 91.7(2) . . ? C6 O3 H3 103(4) . . ? C14 C1 C2 116.9(2) . . ? C14 C1 Br1 109.8(2) . . ? C2 C1 Br1 109.48(19) . . ? C14 C1 H1A 106.7 . . ? C2 C1 H1A 106.7 . . ? Br1 C1 H1A 106.7 . . ? O1 C2 C15 111.7(3) . . ? O1 C2 C1 107.1(2) . . ? C15 C2 C1 112.8(2) . . ? O1 C2 C3 103.8(2) . . ? C15 C2 C3 109.3(2) . . ? C1 C2 C3 111.8(2) . . ? O2 C3 C4 109.8(2) . . ? O2 C3 C2 109.8(2) . . ? C4 C3 C2 111.7(2) . . ? O2 C3 C11 90.4(2) . . ? C4 C3 C11 119.5(2) . . ? C2 C3 C11 113.3(2) . . ? C5 C4 C3 111.0(2) . . ? C5 C4 H4A 109.4 . . ? C3 C4 H4A 109.4 . . ? C5 C4 H4B 109.4 . . ? C3 C4 H4B 109.4 . . ? H4A C4 H4B 108.0 . . ? C4 C5 C9 112.3(2) . . ? C4 C5 C6 117.4(2) . . ? C9 C5 C6 106.3(2) . . ? C4 C5 H5 106.8 . . ? C9 C5 H5 106.8 . . ? C6 C5 H5 106.8 . . ? O3 C6 C16 107.8(2) . . ? O3 C6 C5 110.3(2) . . ? C16 C6 C5 113.4(2) . . ? O3 C6 C7 106.8(2) . . ? C16 C6 C7 114.4(2) . . ? C5 C6 C7 103.9(2) . . ? C8 C7 C6 106.6(2) . . ? C8 C7 H7A 110.4 . . ? C6 C7 H7A 110.4 . . ? C8 C7 H7B 110.4 . . ? C6 C7 H7B 110.4 . . ? H7A C7 H7B 108.6 . . ? C7 C8 C9 104.6(2) . . ? C7 C8 H8A 110.8 . . ? C9 C8 H8A 110.8 . . ? C7 C8 H8B 110.8 . . ? C9 C8 H8B 110.8 . . ? H8A C8 H8B 108.9 . . ? C10 C9 C8 114.2(2) . . ? C10 C9 C5 107.8(2) . . ? C8 C9 C5 100.3(2) . . ? C10 C9 C19 110.4(2) . . ? C8 C9 C19 110.5(3) . . ? C5 C9 C19 113.3(2) . . ? C9 C10 C11 113.3(2) . . ? C9 C10 H10A 108.9 . . ? C11 C10 H10A 108.9 . . ? C9 C10 H10B 108.9 . . ? C11 C10 H10B 108.9 . . ? H10A C10 H10B 107.7 . . ? C10 C11 C12 118.4(2) . . ? C10 C11 C3 119.0(2) . . ? C12 C11 C3 84.6(2) . . ? C10 C11 H11 110.8 . . ? C12 C11 H11 110.8 . . ? C3 C11 H11 110.8 . . ? O2 C12 C20 109.9(3) . . ? O2 C12 C13 109.4(2) . . ? C20 C12 C13 111.6(3) . . ? O2 C12 C11 90.6(2) . . ? C20 C12 C11 118.6(2) . . ? C13 C12 C11 114.4(2) . . ? C12 C13 C14 115.2(2) . . ? C12 C13 H13A 108.5 . . ? C14 C13 H13A 108.5 . . ? C12 C13 H13B 108.5 . . ? C14 C13 H13B 108.5 . . ? H13A C13 H13B 107.5 . . ? C1 C14 C13 112.8(2) . . ? C1 C14 H14A 109.0 . . ? C13 C14 H14A 109.0 . . ? C1 C14 H14B 109.0 . . ? C13 C14 H14B 109.0 . . ? H14A C14 H14B 107.8 . . ? C2 C15 H15A 109.5 . . ? C2 C15 H15B 109.5 . . ? H15A C15 H15B 109.5 . . ? C2 C15 H15C 109.5 . . ? H15A C15 H15C 109.5 . . ? H15B C15 H15C 109.5 . . ? C17 C16 C18 109.3(3) . . ? C17 C16 C6 114.1(3) . . ? C18 C16 C6 111.2(3) . . ? C17 C16 H16 107.3 . . ? C18 C16 H16 107.3 . . ? C6 C16 H16 107.3 . . ? C16 C17 H17A 109.5 . . ? C16 C17 H17B 109.5 . . ? H17A C17 H17B 109.5 . . ? C16 C17 H17C 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C16 C18 H18A 109.5 . . ? C16 C18 H18B 109.5 . . ? H18A C18 H18B 109.5 . . ? C16 C18 H18C 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C9 C19 H19A 109.5 . . ? C9 C19 H19B 109.5 . . ? H19A C19 H19B 109.5 . . ? C9 C19 H19C 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C12 C20 H20A 109.5 . . ? C12 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C12 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C14 C1 C2 O1 -167.3(2) . . . . ? Br1 C1 C2 O1 67.1(3) . . . . ? C14 C1 C2 C15 69.4(3) . . . . ? Br1 C1 C2 C15 -56.2(3) . . . . ? C14 C1 C2 C3 -54.2(3) . . . . ? Br1 C1 C2 C3 -179.83(19) . . . . ? C12 O2 C3 C4 134.2(2) . . . . ? C12 O2 C3 C2 -102.6(2) . . . . ? C12 O2 C3 C11 12.5(2) . . . . ? O1 C2 C3 O2 178.1(2) . . . . ? C15 C2 C3 O2 -62.6(3) . . . . ? C1 C2 C3 O2 63.0(3) . . . . ? O1 C2 C3 C4 -59.9(3) . . . . ? C15 C2 C3 C4 59.5(3) . . . . ? C1 C2 C3 C4 -175.0(2) . . . . ? O1 C2 C3 C11 78.6(3) . . . . ? C15 C2 C3 C11 -162.0(2) . . . . ? C1 C2 C3 C11 -36.5(3) . . . . ? O2 C3 C4 C5 -81.2(3) . . . . ? C2 C3 C4 C5 156.8(2) . . . . ? C11 C3 C4 C5 21.1(4) . . . . ? C3 C4 C5 C9 -54.1(3) . . . . ? C3 C4 C5 C6 -177.7(2) . . . . ? C4 C5 C6 O3 35.3(4) . . . . ? C9 C5 C6 O3 -91.2(3) . . . . ? C4 C5 C6 C16 -85.7(3) . . . . ? C9 C5 C6 C16 147.7(2) . . . . ? C4 C5 C6 C7 149.5(3) . . . . ? C9 C5 C6 C7 22.9(3) . . . . ? O3 C6 C7 C8 120.0(3) . . . . ? C16 C6 C7 C8 -120.8(3) . . . . ? C5 C6 C7 C8 3.4(3) . . . . ? C6 C7 C8 C9 -28.5(3) . . . . ? C7 C8 C9 C10 156.5(3) . . . . ? C7 C8 C9 C5 41.5(3) . . . . ? C7 C8 C9 C19 -78.3(3) . . . . ? C4 C5 C9 C10 70.9(3) . . . . ? C6 C5 C9 C10 -159.6(2) . . . . ? C4 C5 C9 C8 -169.4(2) . . . . ? C6 C5 C9 C8 -39.9(3) . . . . ? C4 C5 C9 C19 -51.7(3) . . . . ? C6 C5 C9 C19 77.9(3) . . . . ? C8 C9 C10 C11 -161.3(3) . . . . ? C5 C9 C10 C11 -50.8(3) . . . . ? C19 C9 C10 C11 73.5(3) . . . . ? C9 C10 C11 C12 121.0(3) . . . . ? C9 C10 C11 C3 20.7(4) . . . . ? O2 C3 C11 C10 107.9(3) . . . . ? C4 C3 C11 C10 -5.3(4) . . . . ? C2 C3 C11 C10 -140.3(3) . . . . ? O2 C3 C11 C12 -11.8(2) . . . . ? C4 C3 C11 C12 -124.9(3) . . . . ? C2 C3 C11 C12 100.1(2) . . . . ? C3 O2 C12 C20 -133.4(2) . . . . ? C3 O2 C12 C13 103.7(3) . . . . ? C3 O2 C12 C11 -12.5(2) . . . . ? C10 C11 C12 O2 -108.4(3) . . . . ? C3 C11 C12 O2 11.8(2) . . . . ? C10 C11 C12 C20 4.8(4) . . . . ? C3 C11 C12 C20 125.0(3) . . . . ? C10 C11 C12 C13 139.8(3) . . . . ? C3 C11 C12 C13 -100.0(3) . . . . ? O2 C12 C13 C14 -31.5(3) . . . . ? C20 C12 C13 C14 -153.4(3) . . . . ? C11 C12 C13 C14 68.4(3) . . . . ? C2 C1 C14 C13 77.2(3) . . . . ? Br1 C1 C14 C13 -157.3(2) . . . . ? C12 C13 C14 C1 -51.6(4) . . . . ? O3 C6 C16 C17 -178.2(3) . . . . ? C5 C6 C16 C17 -55.8(3) . . . . ? C7 C6 C16 C17 63.2(3) . . . . ? O3 C6 C16 C18 57.6(3) . . . . ? C5 C6 C16 C18 -179.9(3) . . . . ? C7 C6 C16 C18 -61.0(3) . . . . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A O1 H1 Br1 0.80(5) 2.83(5) 3.202(2) 110(4) . O1 H1 O2 0.80(5) 2.11(5) 2.834(3) 149(5) 3_645 _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; _audit_block_code C20H33BrO3_uv129_magauer _audit_creation_method 'APEX3 v2015.9-RC7' _shelxl_version_number ? _chemical_name_systematic ? _chemical_formula_moiety 'C20 H33 Br O3' _chemical_formula_sum 'C20 H33 Br O3' _chemical_formula_weight 401.38 #?# (Cohen, 1996) _chemical_melting_point ? #?# in K! _cell_formula_units_Z 4 #?# adjust to _chemical_formula_[] _exptl_crystal_density_diffrn 1.417 _exptl_crystal_F_000 848 #?# check! _shelx_res_file ; uv129_0m.res created by SHELXL-2014/7 TITL uv129_0m_a.res in P2(1)2(1)2(1) REM Old TITL uv129_0m in P2(1)2(1)2(1) REM SHELXT solution in P2(1)2(1)2(1) REM R1 0.102, Rweak 0.040, Alpha 0.005, Orientation as input REM Flack x = 0.025 ( 0.012 ) from Parsons' quotients REM Formula found by SHELXT: C20 O3 Br CELL 0.71073 7.2444 10.8801 23.8676 90.0000 90.0000 90.0000 ZERR 4.000 0.0005 0.0007 0.0015 0.0000 0.0000 0.0000 LATT -1 SYMM 1/2-X, -Y, 1/2+Z SYMM -X, 1/2+Y, 1/2-Z SYMM 1/2+X, 1/2-Y, -Z SFAC C H O BR UNIT 80 132 12 4 TEMP -173.150 OMIT 0 6 0 OMIT 0 4 0 OMIT 0 3 18 SIZE 0.03 0.05 0.07 L.S. 10 BOND $H LIST 4 CONF SHEL 7.5 0.75 ACTA HTAB FMAP 2 PLAN -20 WGHT 0.059500 0.974900 FVAR 0.52540 BR1 4 0.576286 0.422527 0.128261 11.00000 0.02321 0.03104 = 0.01208 -0.00317 -0.00239 -0.00328 O1 3 0.559250 0.340413 0.256959 11.00000 0.02185 0.01169 = 0.01542 0.00044 -0.00417 -0.00298 H1 2 0.497283 0.310728 0.231376 11.00000 0.04131 O2 3 0.656371 0.659268 0.297580 11.00000 0.00874 0.00818 = 0.01630 0.00081 0.00035 -0.00066 O3 3 0.408105 0.363684 0.452438 11.00000 0.02001 0.01650 = 0.02305 0.00166 0.00216 -0.00559 H3 2 0.325762 0.400768 0.435676 11.00000 0.03826 C1 1 0.688177 0.493567 0.196331 11.00000 0.01389 0.01545 = 0.00980 0.00006 -0.00174 0.00022 AFIX 13 H1A 2 0.804617 0.446772 0.203493 11.00000 -1.20000 AFIX 0 C2 1 0.560073 0.470145 0.247164 11.00000 0.01052 0.01394 = 0.01203 0.00044 -0.00220 -0.00253 C3 1 0.641592 0.525134 0.302488 11.00000 0.00866 0.00836 = 0.01225 0.00041 0.00093 0.00032 C4 1 0.523706 0.491994 0.353338 11.00000 0.00884 0.01375 = 0.01319 0.00017 0.00044 -0.00026 AFIX 23 H4A 2 0.418425 0.549704 0.356040 11.00000 -1.20000 H4B 2 0.473475 0.408010 0.348609 11.00000 -1.20000 AFIX 0 C5 1 0.636862 0.497924 0.407070 11.00000 0.01195 0.01096 = 0.01115 0.00052 0.00011 -0.00087 AFIX 13 H5 2 0.678287 0.585081 0.411405 11.00000 -1.20000 AFIX 0 C6 1 0.538722 0.461976 0.462410 11.00000 0.01582 0.01461 = 0.01264 0.00178 0.00122 -0.00166 C7 1 0.695505 0.407739 0.499126 11.00000 0.01889 0.01869 = 0.01450 0.00439 -0.00009 0.00218 AFIX 23 H7A 2 0.704302 0.452708 0.535086 11.00000 -1.20000 H7B 2 0.671567 0.319925 0.507204 11.00000 -1.20000 AFIX 0 C8 1 0.874686 0.422176 0.465459 11.00000 0.01690 0.01750 = 0.01449 0.00260 -0.00154 0.00140 AFIX 23 H8A 2 0.961386 0.354228 0.473741 11.00000 -1.20000 H8B 2 0.935692 0.501283 0.474247 11.00000 -1.20000 AFIX 0 C9 1 0.812931 0.418411 0.403839 11.00000 0.01176 0.00979 = 0.01444 0.00224 0.00057 0.00110 C10 1 0.946715 0.480898 0.363258 11.00000 0.00932 0.01699 = 0.01356 0.00125 -0.00085 0.00092 AFIX 23 H10A 2 1.052821 0.425497 0.356514 11.00000 -1.20000 H10B 2 0.994664 0.556836 0.380876 11.00000 -1.20000 AFIX 0 C11 1 0.857518 0.514127 0.306414 11.00000 0.00989 0.01092 = 0.01204 -0.00024 0.00131 0.00056 AFIX 13 H11 2 0.906485 0.460282 0.275884 11.00000 -1.20000 AFIX 0 C12 1 0.856678 0.651758 0.287682 11.00000 0.00906 0.01144 = 0.01534 0.00194 -0.00161 -0.00252 C13 1 0.896311 0.671820 0.225413 11.00000 0.01271 0.01523 = 0.01736 0.00552 0.00162 -0.00130 AFIX 23 H13A 2 1.012969 0.629312 0.215861 11.00000 -1.20000 H13B 2 0.915513 0.760786 0.218949 11.00000 -1.20000 AFIX 0 C14 1 0.744164 0.626353 0.185292 11.00000 0.01390 0.01700 = 0.01523 0.00474 0.00037 0.00150 AFIX 23 H14A 2 0.634337 0.679781 0.189303 11.00000 -1.20000 H14B 2 0.788718 0.633687 0.146222 11.00000 -1.20000 AFIX 0 C15 1 0.365661 0.519951 0.238292 11.00000 0.00996 0.02012 = 0.01566 0.00064 -0.00270 -0.00081 AFIX 137 H15A 2 0.286573 0.494247 0.269475 11.00000 -1.50000 H15B 2 0.315697 0.487728 0.203076 11.00000 -1.50000 H15C 2 0.369684 0.609909 0.236619 11.00000 -1.50000 AFIX 0 C16 1 0.432237 0.569911 0.489921 11.00000 0.02071 0.01644 = 0.01421 0.00172 0.00411 0.00095 AFIX 13 H16 2 0.332638 0.595203 0.463301 11.00000 -1.20000 AFIX 0 C17 1 0.551653 0.683795 0.501454 11.00000 0.02870 0.01825 = 0.02399 -0.00240 0.00516 0.00141 AFIX 137 H17A 2 0.479009 0.744690 0.522171 11.00000 -1.50000 H17B 2 0.592581 0.719349 0.465832 11.00000 -1.50000 H17C 2 0.659556 0.660003 0.523717 11.00000 -1.50000 AFIX 0 C18 1 0.338158 0.529164 0.544513 11.00000 0.02676 0.02200 = 0.01868 0.00249 0.00997 0.00218 AFIX 137 H18A 2 0.259092 0.595601 0.558397 11.00000 -1.50000 H18B 2 0.432420 0.509920 0.572626 11.00000 -1.50000 H18C 2 0.262930 0.455971 0.537349 11.00000 -1.50000 AFIX 0 C19 1 0.774851 0.284764 0.385197 11.00000 0.01891 0.01039 = 0.02107 0.00169 0.00169 0.00197 AFIX 137 H19A 2 0.887496 0.235769 0.389449 11.00000 -1.50000 H19B 2 0.736215 0.284146 0.345848 11.00000 -1.50000 H19C 2 0.676693 0.249629 0.408472 11.00000 -1.50000 AFIX 0 C20 1 0.956068 0.745229 0.323674 11.00000 0.01635 0.01447 = 0.02440 0.00107 -0.00146 -0.00444 AFIX 137 H20A 2 1.089696 0.735146 0.319234 11.00000 -1.50000 H20B 2 0.922501 0.732785 0.363043 11.00000 -1.50000 H20C 2 0.920363 0.828282 0.312050 11.00000 -1.50000 AFIX 0 HKLF 4 REM uv129_0m_a.res in P2(1)2(1)2(1) REM R1 = 0.0302 for 4453 Fo > 4sig(Fo) and 0.0318 for all 4655 data REM 230 parameters refined using 0 restraints END WGHT 0.0328 0.7540 REM Instructions for potential hydrogen bonds HTAB O1 Br1 EQIV $1 -x+1, y-1/2, -z+1/2 HTAB O1 O2_$1 EQIV $2 -x+3/2, -y+1, z+1/2 HTAB C7 Br1_$2 EQIV $3 -x+1, y+1/2, -z+1/2 HTAB C14 O1_$3 HTAB C15 Br1 HTAB C15 O1_$3 REM Highest difference peak 0.367, deepest hole -0.511, 1-sigma level 0.064 Q1 1 0.5559 0.4914 0.1247 11.00000 0.05 0.37 Q2 1 0.5592 0.3227 0.1131 11.00000 0.05 0.31 Q3 1 0.8519 0.4190 0.4337 11.00000 0.05 0.31 Q4 1 0.6831 0.3349 0.1334 11.00000 0.05 0.30 Q5 1 0.5852 0.5019 0.3234 11.00000 0.05 0.30 Q6 1 0.8775 0.4414 0.3821 11.00000 0.05 0.29 Q7 1 0.5775 0.4857 0.4313 11.00000 0.05 0.29 Q8 1 0.6040 0.4596 0.2121 11.00000 0.05 0.27 Q9 1 0.5635 0.4874 0.3825 11.00000 0.05 0.26 Q10 1 0.6366 0.3998 0.0964 11.00000 0.05 0.26 Q11 1 0.7373 0.4962 0.3005 11.00000 0.05 0.25 Q12 1 0.9169 0.5209 0.3340 11.00000 0.05 0.24 Q13 1 0.7359 0.4506 0.4036 11.00000 0.05 0.23 Q14 1 0.6439 0.4792 0.1253 11.00000 0.05 0.23 Q15 1 0.8827 0.6601 0.2558 11.00000 0.05 0.23 Q16 1 0.8794 0.5999 0.1459 11.00000 0.05 0.23 Q17 1 0.7910 0.3578 0.3946 11.00000 0.05 0.22 Q18 1 0.5577 0.4981 0.6172 11.00000 0.05 0.22 Q19 1 0.5120 0.4021 0.0978 11.00000 0.05 0.21 Q20 1 1.0053 0.6124 0.1394 11.00000 0.05 0.21 ; _shelx_res_checksum 31507 _shelx_hkl_file ; 1 0 0 -0.6249 0.47856 2 1 0 0 -0.3283 0.69051 3 1 0 0 -0.3048 0.95135 4 -1 0 0 0.30875 1.10115 4 -1 0 0 0.12397 0.74717 3 -2 0 0 2538.70 232.435 1 -2 0 0 2636.43 233.937 1 3 0 0 2.17365 3.24304 3 -3 0 0 0.71988 4.22636 4 -3 0 0 0.11172 2.94858 3 -3 0 0 1.50194 2.24948 2 -3 0 0 0.39438 2.24414 2 3 0 0 -0.0386 4.46639 4 -4 0 0 1995.96 151.795 4 4 0 0 1944.21 151.990 4 4 0 0 1912.88 149.632 3 -4 0 0 1714.95 149.368 3 -4 0 0 1767.16 148.759 2 -5 0 0 4.55359 3.87614 2 -5 0 0 7.44079 5.02617 3 5 0 0 2.38428 5.21070 3 -5 0 0 8.39418 7.27498 4 -5 0 0 6.82738 4.04811 2 5 0 0 7.56555 8.33773 4 -6 0 0 733.482 60.1296 2 6 0 0 719.100 61.9654 3 -6 0 0 659.200 61.3893 3 -6 0 0 752.206 60.3316 2 -6 0 0 731.311 65.1630 4 6 0 0 774.995 66.0169 4 -7 0 0 3.93922 4.65367 2 -7 0 0 0.21068 6.97864 3 7 0 0 -4.5813 7.35109 3 -7 0 0 5.91846 5.02452 2 7 0 0 2.86176 11.2258 4 8 0 0 365.943 45.4096 4 -8 0 0 434.540 37.2315 2 8 0 0 407.848 41.4732 3 -8 0 0 491.375 37.3179 2 9 0 0 5.28700 15.0788 4 9 0 0 -0.9463 11.2607 3 0 -1 0 0.25272 0.52727 4 0 -1 0 -0.1889 0.43114 2 0 1 0 0.63397 0.44184 3 0 1 0 -0.1807 0.52112 4 0 1 0 -0.0579 0.49071 2 -1 1 0 9999.99 803.912 1 -2 -1 0 698.326 56.8226 4 2 1 0 666.391 56.7615 4 -2 -1 0 672.779 56.0098 3 -2 1 0 724.645 55.7354 3 -2 1 0 683.706 56.2797 2 2 -1 0 700.056 55.7041 3 -2 1 0 660.034 56.2813 2 2 -1 0 715.701 57.2989 4 2 1 0 688.623 56.1210 3 -2 1 0 713.995 57.2417 4 -3 -1 0 3745.42 337.091 1 -3 1 0 3670.58 339.469 1 -3 1 0 3873.91 342.205 1 -3 -1 0 3650.49 335.631 1 -4 -1 0 1165.09 89.6963 2 -4 1 0 1124.00 91.5402 2 4 1 0 1172.79 91.9696 3 -4 1 0 1128.85 93.7710 4 -4 1 0 1083.97 91.2551 2 -4 -1 0 1125.07 91.5196 3 -4 -1 0 1156.79 89.7768 2 -4 1 0 1129.42 91.1300 3 4 1 0 1113.64 93.4580 4 4 -1 0 1159.19 91.2991 3 -4 -1 0 1065.10 93.0942 4 4 -1 0 1080.77 93.6741 4 5 1 0 592.247 44.8720 3 -5 1 0 470.083 46.3929 4 5 1 0 453.262 46.1180 4 -5 -1 0 533.014 41.6124 2 -5 -1 0 543.726 41.7248 2 -5 1 0 528.198 43.8388 2 5 -1 0 508.134 43.8830 3 -5 -1 0 511.769 43.9485 3 -5 -1 0 481.973 46.0308 4 5 -1 0 462.119 46.6229 4 -6 1 0 39.1123 12.2364 4 -6 1 0 49.4727 9.34527 2 -6 -1 0 52.3422 10.6444 3 -6 -1 0 38.3135 12.3744 4 6 -1 0 43.5951 13.7835 4 6 -1 0 42.5666 9.72070 3 -6 -1 0 49.8473 6.28809 2 -6 -1 0 46.9947 6.02061 2 6 1 0 38.4373 12.1367 4 6 1 0 47.2675 11.1345 3 -6 1 0 63.7005 10.6970 3 -6 1 0 55.9310 9.48183 2 -7 -1 0 76.7406 7.11121 2 7 1 0 69.2053 13.6446 3 -7 1 0 71.0624 12.1757 3 -7 1 0 81.1436 11.4533 2 7 -1 0 48.8130 16.5389 4 7 -1 0 60.9448 12.8783 3 -7 1 0 68.3048 11.1645 2 7 1 0 49.8982 16.1930 4 -8 1 0 6.43226 6.96061 2 -8 1 0 18.7392 7.48199 2 8 -1 0 18.4579 14.5987 4 8 1 0 7.94557 15.5417 4 8 -1 0 11.9967 9.24177 3 8 1 0 7.52137 9.97040 3 9 1 0 20.9586 15.8162 4 9 -1 0 10.3484 11.8064 3 9 -1 0 14.0487 16.2696 4 -9 1 0 10.8020 6.88111 2 9 1 0 17.3248 12.0493 3 -1 2 0 3407.82 276.998 1 -1 -2 0 3168.92 269.896 1 2 2 0 316.777 27.3434 3 2 -2 0 308.226 26.4801 3 -2 -2 0 355.581 28.0780 4 -2 -2 0 288.189 27.0737 3 -2 2 0 291.967 27.7184 2 -2 2 0 379.627 29.0023 4 -2 2 0 327.861 26.5113 3 -2 2 0 272.547 27.5653 2 2 2 0 358.797 28.1892 4 3 2 0 485.857 40.4865 3 -3 -2 0 444.894 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53.8028 2 7 2 0 592.368 57.8746 4 7 2 0 616.388 54.5744 3 -7 2 0 621.040 53.1172 3 7 -2 0 540.641 57.9520 4 8 2 0 89.3631 21.0293 4 8 -2 0 88.4820 21.7198 4 -8 2 0 76.4928 13.7489 2 -8 2 0 80.2300 14.3065 2 8 -2 0 78.2700 14.5079 3 8 2 0 77.2827 16.4785 3 -9 2 0 7.84909 8.90370 2 9 2 0 1.92485 14.3252 4 9 -2 0 -2.6678 15.3953 4 9 -2 0 2.99268 10.5183 3 9 2 0 -2.7226 11.1204 3 0 -3 0 2.55519 2.15973 3 0 3 0 2.95088 2.27836 3 0 3 0 3.47158 3.29670 4 0 3 0 2.79342 2.71820 2 0 3 0 1.88171 2.76429 2 0 -3 0 3.13022 3.41714 4 1 -3 0 246.659 21.5532 3 1 3 0 263.499 22.1954 2 1 3 0 223.786 22.5312 4 -1 3 0 303.415 23.7015 2 -1 3 0 240.242 21.5136 3 -1 3 0 297.488 23.6491 2 1 3 0 290.722 22.4280 3 1 3 0 279.303 22.3952 3 -1 3 0 215.626 22.9596 4 -1 -3 0 236.912 22.5816 4 1 3 0 276.793 22.1979 2 -2 3 0 1968.67 157.569 2 2 3 0 1974.43 156.543 3 -2 3 0 2057.18 155.592 3 -2 -3 0 1934.27 157.008 4 -2 3 0 1828.49 157.377 2 2 3 0 1966.20 155.312 2 2 -3 0 2046.51 158.108 4 2 3 0 2044.71 156.605 3 2 3 0 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22.3795 4 4 6 0 32.4110 10.8934 4 4 6 0 44.7872 5.68151 2 4 -6 0 27.7586 12.2545 4 4 6 0 46.9221 5.50227 2 4 6 0 35.2348 9.90266 3 -4 6 0 52.9736 12.2492 2 4 -6 0 41.5646 7.48980 3 -4 -6 0 35.5908 10.1070 4 -4 6 0 43.1369 11.4796 2 -4 6 0 46.1766 7.44857 3 4 6 0 39.2357 9.61626 3 -4 6 0 21.3461 11.0250 4 5 6 0 18.2099 9.53056 3 5 -6 0 15.9992 6.43819 3 -5 6 0 16.6508 9.44209 2 -5 6 0 31.9964 10.9356 2 -5 6 0 15.4410 5.93799 3 -5 -6 0 5.86540 8.31560 4 5 6 0 14.8479 11.0932 4 5 -6 0 18.7730 12.3510 4 6 6 0 732.458 65.9562 4 6 -6 0 689.677 68.1897 4 -6 6 0 612.939 60.3240 3 6 6 0 776.185 64.9339 3 -6 6 0 759.054 65.9978 2 6 -6 0 790.497 61.0529 3 7 6 0 30.9037 16.3674 4 7 -6 0 40.0728 17.9985 4 -7 6 0 21.1850 8.14345 3 7 6 0 19.0462 12.0234 3 -7 6 0 8.76948 12.1907 2 7 -6 0 16.2638 8.03224 3 8 6 0 298.970 33.0067 3 -8 6 0 282.153 32.3534 2 8 -6 0 249.873 25.8105 3 8 -6 0 206.233 35.1975 4 8 6 0 206.689 31.5257 4 0 7 0 26.3557 7.77228 2 1 7 0 50.4022 9.71428 2 1 7 0 55.9316 9.28808 3 1 -7 0 84.3108 13.4369 4 1 7 0 86.0344 12.2994 4 -1 7 0 67.4562 8.94185 3 -1 7 0 51.2746 11.5648 2 -1 7 0 53.6998 11.1657 2 1 7 0 44.5607 9.57418 2 1 7 0 66.6847 11.5996 4 1 7 0 58.4122 9.32863 3 1 -7 0 74.5838 8.83104 3 2 7 0 11.6253 6.10130 2 -2 7 0 8.64217 7.38221 2 2 7 0 26.3191 7.27334 3 2 7 0 9.41295 6.22802 3 2 -7 0 31.6776 6.12795 3 -2 7 0 18.7809 5.55234 3 2 7 0 29.7639 9.90496 4 3 7 0 358.322 32.6186 3 -3 7 0 296.880 34.0920 2 3 7 0 358.870 34.1371 4 3 -7 0 299.547 34.4089 4 3 -7 0 349.520 30.2515 3 3 7 0 342.046 30.8245 2 3 7 0 385.316 31.3217 2 3 7 0 375.665 34.5712 4 3 7 0 340.068 32.2467 3 -3 7 0 355.590 35.2667 4 -3 7 0 342.249 30.2284 3 -3 7 0 360.363 35.0868 2 -4 7 0 21.7883 10.1460 2 -4 -7 0 13.1244 8.54451 4 4 7 0 30.6318 9.71380 3 4 7 0 18.1613 5.17530 2 -4 7 0 14.7386 5.86948 3 4 7 0 30.4964 5.68179 2 4 -7 0 19.8866 6.19390 3 -4 7 0 44.3181 12.5293 2 4 7 0 10.6265 9.23617 4 4 -7 0 11.0421 9.28239 4 5 -7 0 279.267 25.8260 3 -5 7 0 298.066 25.9152 3 5 7 0 243.997 30.2814 4 5 7 0 262.523 29.4093 3 5 -7 0 226.916 32.4813 4 -5 7 0 354.390 33.4474 2 -5 -7 0 296.716 30.4059 4 6 -7 0 11.4081 7.15227 3 6 -7 0 7.73998 13.5671 4 -6 7 0 10.9246 11.3038 2 -6 7 0 7.40463 6.36120 3 6 7 0 3.71176 10.0109 3 6 7 0 2.24894 10.6749 4 7 -7 0 82.2555 13.7250 3 7 7 0 69.2440 17.0226 3 -7 7 0 84.9922 18.7910 2 7 7 0 108.923 22.5176 4 7 -7 0 112.869 24.5833 4 -7 7 0 74.1450 12.6855 3 8 -7 0 6.10646 7.88725 3 8 7 0 8.43904 15.8338 4 8 -7 0 8.04893 17.5070 4 8 7 0 4.86184 12.8341 3 -8 7 0 9.38699 13.9132 2 0 8 0 69.8755 12.8007 2 0 8 0 87.5145 11.5881 3 1 8 0 78.1729 10.9811 3 -1 8 0 35.9932 10.3394 4 -1 8 0 50.1623 8.43755 3 1 -8 0 49.1701 8.61313 3 1 8 0 46.8860 11.5935 4 1 8 0 51.7082 9.64179 3 1 8 0 24.2923 9.98875 4 2 8 0 191.387 21.4365 3 2 -8 0 190.102 25.3055 4 -2 8 0 222.465 24.8754 2 -2 8 0 203.454 24.3224 2 2 8 0 202.369 21.9114 2 2 8 0 214.624 22.3275 2 -2 8 0 208.931 20.1440 3 2 -8 0 230.093 20.4864 3 2 8 0 215.610 22.0018 3 -2 8 0 215.194 25.0722 4 2 8 0 230.448 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41.5071 3 4 -4 -1 427.922 43.3955 4 4 4 1 448.609 42.5850 4 -4 -4 1 437.046 41.5353 4 4 -4 -1 500.824 39.8647 3 -4 4 -1 495.701 39.2473 3 -4 4 -1 420.260 43.1071 4 -4 -4 1 561.652 41.7191 3 4 4 1 451.438 40.8787 3 -4 4 -1 505.784 42.9050 2 -5 4 1 214.224 23.8017 2 5 4 -1 199.152 23.2999 3 5 -4 1 211.214 21.0257 3 -5 4 1 218.541 23.9432 2 5 4 -1 244.497 25.2147 4 -5 4 1 201.400 25.5378 4 -5 -4 -1 222.891 24.7157 4 5 -4 1 200.701 26.2666 4 -5 4 1 221.318 21.4212 3 -5 4 -1 230.312 26.2457 4 5 -4 -1 238.044 26.0542 4 -5 -4 1 254.839 24.7935 4 -5 4 -1 237.027 24.7431 2 5 4 1 229.291 23.5576 3 5 -4 -1 265.489 22.0880 3 -5 4 -1 235.965 20.9711 3 5 4 1 231.182 22.9857 3 -5 4 -1 221.408 24.0405 2 -5 -4 1 195.643 22.5199 3 5 4 1 226.646 25.3429 4 -6 4 1 217.581 24.2578 2 -6 4 1 223.072 24.8476 2 6 4 -1 250.847 26.7718 4 -6 4 1 265.694 22.3345 3 6 -4 1 241.525 21.6896 3 -6 -4 -1 256.553 26.5434 4 6 4 -1 256.079 25.2354 3 6 -4 -1 210.866 21.8835 3 -6 4 -1 166.136 23.0008 2 6 -4 -1 238.188 27.1903 4 -6 4 -1 200.736 20.9713 3 6 4 1 201.739 26.2075 4 -6 4 -1 180.165 23.2681 2 -6 -4 1 206.790 24.9084 4 6 4 1 175.433 23.5213 3 7 -4 1 276.879 26.7449 3 -7 4 1 279.816 29.0392 2 -7 4 1 273.540 27.1367 3 7 4 -1 227.072 30.6883 4 7 -4 1 242.135 33.3587 4 7 4 -1 302.070 30.1613 3 -7 4 -1 285.255 29.7409 2 7 -4 -1 294.078 27.3785 3 7 4 1 255.194 29.4255 3 7 -4 -1 257.222 33.6170 4 7 4 1 259.548 32.0859 4 -7 4 -1 275.883 29.7752 2 8 4 -1 171.603 23.1223 3 8 4 -1 138.963 24.2854 4 -8 4 1 149.204 21.5233 2 8 -4 1 150.489 19.2897 3 8 -4 1 135.426 27.0220 4 8 4 1 114.328 24.4014 4 8 4 1 175.065 22.9802 3 8 -4 -1 148.876 19.5767 3 -8 4 -1 166.482 22.1670 2 -8 4 -1 167.736 19.6362 3 8 -4 -1 138.783 24.2871 4 9 -4 1 72.0037 14.5169 3 9 4 -1 95.6121 19.4905 3 9 -4 1 60.9517 19.9240 4 -9 4 1 72.3035 16.2937 2 9 4 -1 87.2918 22.0607 4 9 -4 -1 57.0294 14.2511 3 -9 4 -1 72.0494 16.0890 2 9 4 1 59.2707 17.4914 3 9 -4 -1 72.5092 23.8495 4 9 4 1 51.6377 21.8884 4 0 -5 1 619.659 51.9749 4 0 5 1 672.241 52.5800 4 0 5 -1 596.136 49.9899 3 0 -5 -1 676.793 52.6606 4 0 5 1 553.572 50.0683 3 0 -5 -1 579.916 50.2588 3 0 -5 1 582.758 50.0854 3 -1 -5 -1 2220.45 159.946 3 -1 5 1 2159.08 161.491 2 -1 5 1 1971.68 158.986 3 1 5 -1 2042.91 160.528 4 1 -5 1 1947.95 161.210 4 -1 5 1 1979.03 161.260 2 1 5 -1 1876.49 160.436 4 1 5 -1 2186.08 160.411 2 1 -5 1 2233.00 162.056 2 1 5 -1 2062.81 159.515 3 1 -5 1 2220.71 158.886 3 -1 5 1 1951.86 161.288 4 1 5 -1 1964.74 159.449 3 1 5 -1 2023.01 160.165 2 1 5 1 1762.58 159.305 3 -1 5 -1 2026.52 161.512 2 1 5 1 1913.06 160.945 4 1 5 1 1948.75 159.919 2 1 -5 -1 1964.47 159.001 3 -1 5 -1 1937.43 158.620 3 1 5 1 1932.59 160.722 4 1 -5 -1 1922.52 161.316 4 -1 5 -1 1900.87 161.116 2 -1 5 -1 1743.21 160.699 4 -2 -5 -1 465.137 36.5616 4 -2 5 1 433.198 34.0823 3 -2 5 1 451.540 37.6430 4 2 5 -1 446.265 36.0221 4 -2 5 1 461.200 37.3796 2 -2 5 1 447.556 37.0969 2 2 5 -1 463.599 34.6366 2 2 -5 1 448.067 33.6307 3 2 5 -1 451.556 35.4100 3 2 5 -1 406.202 35.0171 3 2 -5 1 463.454 37.7876 4 -2 5 -1 376.744 36.6198 2 2 -5 -1 365.631 33.7890 3 -2 5 -1 368.648 33.3855 3 2 5 1 356.060 34.2158 2 -2 5 -1 356.464 36.4705 4 -2 -5 1 359.777 35.2082 4 2 5 1 374.161 35.9275 4 -2 5 -1 365.613 36.4244 2 2 5 1 363.120 34.8281 3 2 5 1 340.715 34.6530 3 2 5 1 376.923 34.3338 2 2 -5 -1 379.976 36.8014 4 -3 5 1 391.915 34.7922 4 -3 5 1 355.659 30.5518 3 3 5 -1 360.820 32.0714 3 3 5 -1 335.359 29.9131 2 3 -5 1 378.848 30.1920 3 -3 -5 -1 367.354 33.2134 4 3 -5 1 387.916 35.1750 4 -3 5 1 361.331 33.9568 2 3 5 -1 415.434 33.6634 4 3 5 -1 381.017 32.5664 3 -3 5 -1 289.428 33.1225 2 3 5 1 342.380 32.0300 3 -3 5 -1 337.577 30.0170 3 3 5 1 386.821 33.6413 4 -3 5 -1 351.358 33.9041 4 -3 5 -1 315.682 33.2948 2 3 -5 -1 374.479 30.7465 3 3 5 1 294.843 29.8362 2 3 -5 -1 418.326 35.5982 4 -3 -5 1 382.606 33.0376 4 3 5 1 356.343 32.0943 3 3 5 1 340.945 30.0133 2 4 5 -1 537.866 40.1737 3 4 -5 1 404.426 42.0218 4 4 5 -1 402.601 40.1110 4 -4 5 1 447.107 41.2426 2 -4 5 1 437.272 42.0334 4 4 5 -1 377.613 39.2617 3 -4 5 1 440.001 37.6013 3 -4 -5 -1 410.450 40.2229 4 -4 5 1 455.485 41.0967 2 4 -5 1 431.266 37.0929 3 4 5 1 443.715 41.1579 4 -4 5 -1 498.634 41.7536 2 4 -5 -1 473.357 37.8274 3 4 5 1 404.922 39.4596 3 -4 5 -1 468.769 37.2282 3 -4 5 -1 424.068 41.9099 4 4 5 1 393.954 38.9271 3 4 -5 -1 445.183 42.7481 4 -4 -5 1 477.006 40.6087 4 -4 5 -1 468.528 41.4935 2 -5 -5 -1 193.910 22.4358 4 5 -5 1 218.035 18.5275 3 -5 5 1 199.507 23.2718 2 -5 5 1 219.013 19.1616 3 5 5 -1 174.115 20.2134 3 -5 5 1 220.444 22.9150 2 5 5 -1 205.551 21.6824 3 5 5 -1 203.348 22.6343 4 -5 5 1 205.852 24.4922 4 5 -5 1 187.130 23.2348 4 -5 5 -1 183.930 22.0400 2 -5 5 -1 181.759 18.0539 3 5 5 1 186.068 21.2948 3 5 5 1 142.554 19.7661 3 5 -5 -1 163.429 24.0878 4 5 5 1 154.268 22.0828 4 -5 5 -1 184.638 22.2231 2 -5 5 -1 156.420 23.0456 4 5 -5 -1 177.236 18.5975 3 -5 -5 1 174.193 21.4276 4 -6 5 1 217.322 25.3505 3 6 -5 1 261.087 25.2064 3 -6 5 1 223.455 29.2313 2 6 5 -1 283.644 30.4788 4 -6 5 1 212.464 28.1304 2 6 -5 1 309.759 33.6837 4 -6 5 -1 251.819 28.8125 2 6 -5 -1 285.051 25.9666 3 6 -5 -1 334.793 32.6692 4 6 5 1 313.638 29.2604 3 -6 -5 1 299.680 30.0379 4 6 5 1 331.091 32.9124 4 -6 5 -1 254.797 24.8837 3 7 -5 1 48.7447 18.1221 4 7 5 -1 55.3907 15.8566 4 -7 5 1 47.2679 9.87881 3 7 -5 1 47.8430 10.1997 3 -7 5 1 39.6389 12.8330 2 7 5 -1 44.4523 13.7202 3 7 5 1 23.1545 15.8164 4 7 -5 -1 19.8200 15.5444 4 8 5 -1 122.744 22.3817 3 -8 5 1 132.692 20.9914 2 8 5 -1 121.309 25.3573 4 8 -5 1 145.814 28.1787 4 8 -5 1 147.861 18.4691 3 -8 5 -1 177.805 23.6322 2 8 5 1 140.795 25.1410 4 -8 5 -1 133.543 17.1736 3 8 -5 -1 155.915 19.7680 3 8 5 1 120.650 22.2491 3 8 -5 -1 143.275 27.4525 4 9 -5 1 28.3786 19.3152 4 9 5 -1 28.9029 16.7962 4 -9 5 1 21.0190 13.2641 2 9 5 -1 23.7126 15.7289 3 9 -5 1 24.3035 10.4856 3 9 -5 -1 30.0611 11.6812 3 9 5 1 36.1883 19.4300 4 9 -5 -1 21.2202 18.1715 4 -9 5 -1 42.5685 14.7517 2 9 5 1 7.20899 13.1698 3 0 6 1 309.091 33.4755 2 0 -6 -1 363.275 32.4114 3 0 6 1 363.489 32.2771 3 0 -6 1 382.604 32.2206 3 0 -6 -1 367.954 34.8115 4 0 6 1 450.353 35.5766 4 0 6 1 401.381 34.2632 2 0 6 -1 355.690 34.0354 2 0 6 -1 354.783 32.0584 3 0 6 -1 364.365 34.0196 2 0 6 -1 403.849 34.6751 4 0 -6 1 404.657 34.7776 4 -1 6 1 69.9865 10.7834 4 1 6 -1 67.7043 9.73430 4 1 -6 -1 26.4600 6.15441 3 1 6 1 41.4777 8.23700 2 -1 6 -1 50.3432 9.89253 2 1 6 1 24.7303 8.10144 4 1 6 1 37.6674 8.12474 2 -1 6 -1 50.2564 9.96632 2 1 6 1 31.5309 7.14128 3 -1 6 -1 31.7414 6.25381 3 2 6 -1 1018.98 85.7658 3 2 6 -1 1151.67 85.9602 2 2 -6 1 1157.00 88.9995 4 2 6 -1 965.757 85.2994 2 -2 6 1 1007.71 88.0478 4 -2 6 1 1067.94 88.0036 2 2 6 -1 867.305 86.3869 4 2 -6 1 1074.26 84.3830 3 2 6 -1 1188.80 86.2717 3 2 6 -1 1161.11 87.4012 4 -2 6 1 1039.80 84.6640 3 -2 6 1 1095.72 88.5238 2 2 6 1 978.670 85.7613 3 2 -6 -1 1003.29 84.6339 3 2 6 1 1051.55 87.6204 4 2 6 1 1062.22 85.9580 3 -2 6 -1 1065.50 88.2253 2 2 -6 -1 987.882 88.2879 4 2 6 1 1056.68 85.6809 2 -2 6 -1 978.714 84.1357 3 2 6 1 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11.8249 3 2 6 2 107.078 13.0617 2 2 6 2 110.394 13.7049 3 -3 6 2 1873.04 155.419 2 3 6 -2 1882.07 153.045 3 3 6 -2 1862.96 153.207 3 -3 6 2 1887.46 155.507 4 -3 6 2 2062.29 155.729 2 3 -6 2 1743.00 155.303 4 3 -6 2 1893.92 150.668 3 3 6 -2 1977.15 153.931 4 -3 -6 -2 1927.58 154.583 4 -3 6 2 1899.98 151.646 3 3 6 -2 1931.05 151.589 2 3 6 -2 1717.21 151.182 2 3 -6 -2 1934.94 151.772 3 -3 6 -2 2017.09 150.799 3 3 -6 -2 1727.35 155.540 4 3 6 2 1622.22 151.324 2 -3 6 -2 1931.49 155.493 2 3 6 2 1791.79 154.473 4 -3 6 -2 1933.24 155.554 2 3 6 2 2024.91 151.773 2 3 6 2 2079.67 153.723 3 -3 6 -2 1998.12 155.907 4 3 6 2 1858.82 153.069 3 -3 -6 2 1867.21 153.502 4 4 6 -2 252.862 23.7356 4 -4 6 2 200.809 23.9505 2 4 6 -2 233.850 22.8329 3 -4 6 2 239.343 24.7242 4 4 6 -2 242.014 18.2656 2 4 6 -2 238.681 22.3393 3 4 6 -2 203.480 17.8833 2 4 -6 2 223.712 18.9596 3 -4 6 2 216.497 20.0839 3 -4 6 2 220.463 24.3522 2 4 -6 2 247.671 26.7551 4 -4 -6 -2 237.759 23.9626 4 4 6 2 199.298 23.9565 4 4 6 2 173.788 21.2603 3 4 6 2 192.166 18.1438 2 -4 -6 2 176.191 22.1782 4 -4 6 -2 187.228 18.6973 3 -4 6 -2 182.211 24.1371 4 -4 6 -2 173.681 23.5568 2 4 -6 -2 174.258 19.8227 3 4 6 2 184.384 21.7644 3 -4 6 -2 186.668 23.4746 2 4 -6 -2 212.030 25.8749 4 5 -6 2 180.871 16.8744 3 -5 6 2 207.200 23.0404 2 5 6 -2 187.815 21.0809 3 5 -6 2 142.683 23.7291 4 -5 -6 -2 158.631 21.4562 4 5 6 -2 135.887 20.2937 4 -5 6 2 197.439 23.1043 2 -5 6 2 191.932 18.4317 3 -5 -6 2 142.934 19.9579 4 5 -6 -2 127.330 21.4506 4 5 6 2 184.298 21.2768 3 -5 6 -2 192.795 22.5301 2 5 -6 -2 165.924 18.2954 3 5 6 2 143.327 22.0738 4 -5 6 -2 221.237 23.5532 2 -5 6 -2 171.775 16.5342 3 6 -6 2 58.7553 9.30701 3 -6 6 2 47.9710 14.2137 2 6 -6 2 61.1732 18.5725 4 6 6 -2 46.7144 14.1875 4 -6 6 2 39.7712 9.59445 3 6 6 -2 20.2383 12.0607 3 6 -6 -2 67.0851 11.3538 3 -6 6 -2 49.2682 13.7085 2 6 6 2 56.1037 13.3384 3 6 -6 -2 42.7029 16.6920 4 -6 6 -2 54.0220 8.74383 3 -6 -6 2 75.4502 15.0557 4 6 6 2 50.7331 15.3983 4 7 -6 2 50.6946 18.5439 4 -7 6 2 36.2829 10.4443 3 7 -6 2 44.3217 9.54457 3 7 6 -2 67.3843 15.9946 3 7 6 -2 47.1350 17.0203 4 -7 6 2 30.5119 13.2856 2 7 6 2 74.7419 19.1864 4 7 -6 -2 68.8641 20.3216 4 7 6 2 74.8224 15.6086 3 -7 6 -2 53.5854 9.60823 3 7 -6 -2 62.7019 12.0861 3 -7 6 -2 53.0439 15.4960 2 8 -6 2 29.6879 18.7071 4 8 6 -2 7.84669 13.3347 4 -8 6 2 -2.4620 11.6343 2 8 6 -2 8.18286 13.8955 3 8 -6 2 15.7872 7.64553 3 8 6 2 12.7712 15.1933 4 8 -6 -2 9.17340 16.5528 4 -8 6 -2 -8.1426 11.4923 2 8 6 2 -1.3942 13.4519 3 8 -6 -2 10.7132 9.17594 3 -8 6 -2 4.53266 7.47251 3 0 7 -2 1488.03 116.914 3 0 7 -2 1258.86 118.640 4 0 7 2 1451.23 119.359 2 0 -7 2 1430.02 119.365 4 0 7 2 1464.29 119.459 2 0 7 2 1409.30 117.241 3 0 7 -2 1403.60 119.284 2 0 -7 -2 1474.21 120.450 4 0 7 2 1636.90 120.855 4 0 -7 -2 1637.55 117.921 3 0 7 -2 1439.96 116.872 3 0 7 -2 1319.89 118.984 2 -1 7 2 536.458 49.7749 2 1 -7 2 582.738 50.4320 4 -1 7 2 490.718 46.9838 3 1 7 -2 553.473 47.4489 3 -1 -7 -2 495.607 47.6239 3 1 7 -2 541.951 48.7327 2 1 7 -2 540.633 48.8339 2 1 7 -2 532.177 47.3105 3 1 7 -2 521.962 49.2268 4 1 -7 2 569.798 46.6963 3 -1 7 2 552.748 50.0765 2 1 7 -2 508.448 48.7174 4 -1 7 2 548.154 50.3912 4 1 7 2 565.004 49.0099 2 1 7 2 582.841 48.1015 3 1 7 2 563.144 48.8692 2 -1 7 -2 586.517 50.3700 2 1 -7 -2 564.073 47.4087 3 1 -7 -2 564.155 50.4992 4 1 7 2 643.716 50.9308 4 -1 7 -2 610.072 50.3431 4 -1 7 -2 588.266 46.6829 3 1 7 2 664.645 50.8491 4 2 7 -2 1027.06 84.7844 3 2 7 -2 1100.90 85.0112 3 2 -7 2 1060.91 83.0854 3 2 7 -2 1072.60 86.2394 4 -2 7 2 1010.37 83.7767 3 -2 7 2 1037.63 87.4889 4 2 7 -2 997.586 84.8912 2 -2 7 2 1167.39 87.9719 2 2 7 -2 1196.90 87.0069 4 2 -7 2 1180.18 88.4190 4 -2 7 2 890.691 86.7250 2 2 7 -2 950.959 84.5720 2 2 7 2 1062.98 87.0760 4 -2 7 -2 972.250 87.0191 4 2 7 2 865.152 84.3988 2 2 -7 -2 961.024 87.6028 4 -2 7 -2 1013.03 82.9668 3 -2 7 -2 935.109 87.0705 2 2 7 2 1125.57 85.4721 3 2 7 2 1197.16 88.0217 4 -2 7 -2 884.151 86.6171 2 2 7 2 1036.79 85.1422 2 2 -7 -2 1005.86 83.8320 3 2 7 2 947.361 84.7061 3 -3 7 2 27.9147 10.5512 2 -3 7 2 30.5781 7.12928 3 3 7 -2 37.2312 9.20752 3 -3 7 2 50.4012 12.9362 4 3 -7 2 37.3780 12.6271 4 3 7 -2 44.4712 10.4995 4 3 7 -2 44.2237 10.6888 4 -3 -7 -2 47.9212 11.4564 4 3 7 -2 36.8338 7.36755 2 -3 7 2 31.0322 9.97765 2 3 7 -2 33.1262 7.25831 2 3 -7 2 37.8180 6.45334 3 3 7 -2 36.1026 9.42778 3 3 7 2 36.4780 9.11691 3 3 -7 -2 31.3624 12.5648 4 -3 7 -2 34.1312 11.5174 4 -3 7 -2 27.6885 10.2538 2 -3 7 -2 34.4582 6.10020 3 3 7 2 41.2372 11.5469 4 3 -7 -2 36.4981 7.93750 3 3 7 2 40.5568 7.83031 2 -3 7 -2 33.3824 11.2986 2 3 7 2 26.4316 7.29856 2 3 7 2 33.7343 9.11652 3 -4 7 2 349.010 32.3381 3 -4 7 2 324.584 36.6976 2 4 7 -2 392.937 36.0538 4 -4 -7 -2 370.316 36.2332 4 4 7 -2 312.153 30.9713 2 -4 7 2 327.142 36.5776 2 4 -7 2 401.588 39.1330 4 4 -7 2 367.616 31.2276 3 4 7 -2 315.457 31.0611 2 -4 -7 2 416.927 35.7103 4 4 7 2 379.553 31.5267 2 4 -7 -2 420.624 39.7894 4 -4 7 -2 338.971 36.9692 2 4 7 2 447.818 38.0404 4 -4 7 -2 375.357 37.5575 2 4 7 2 340.828 34.6005 3 4 -7 -2 414.541 33.0713 3 4 7 2 382.943 31.5442 2 -4 7 -2 339.423 31.1112 3 5 7 -2 20.0807 12.1570 4 -5 7 2 46.2557 13.8222 2 -5 7 2 36.7867 8.47215 3 5 -7 2 19.0004 11.9404 4 5 -7 2 32.6809 7.08957 3 5 7 -2 44.0292 11.9375 3 5 -7 -2 51.7455 9.68160 3 -5 -7 2 45.8680 12.8952 4 -5 7 -2 72.7295 15.6739 2 5 -7 -2 20.7771 14.3333 4 -5 7 -2 49.6374 7.64718 3 5 7 2 60.1760 13.3855 3 5 7 2 32.2607 13.1098 4 6 7 -2 259.659 30.9195 4 6 7 -2 229.544 28.8815 3 6 -7 2 254.063 23.9690 3 -6 7 2 222.057 30.4348 2 -6 7 2 230.193 25.2072 3 6 -7 2 259.116 34.0805 4 -6 7 -2 293.281 24.1380 3 6 -7 -2 293.822 34.9134 4 6 7 2 280.770 29.3658 3 6 7 2 283.264 31.9015 4 -6 7 -2 233.356 30.2821 2 6 -7 -2 276.327 26.0970 3 7 7 -2 12.9890 14.4234 4 7 7 -2 15.1344 12.1205 3 7 -7 2 24.8152 7.73949 3 -7 7 2 20.5925 12.7078 2 -7 7 2 12.2145 8.13697 3 7 -7 2 15.4304 16.5604 4 7 7 2 10.4183 11.3067 3 -7 7 -2 13.4422 11.9736 2 7 7 2 11.3636 13.5044 4 7 -7 -2 7.24473 15.6358 4 7 -7 -2 12.3190 8.14726 3 -7 7 -2 14.5117 6.79729 3 8 -7 2 67.1187 23.5302 4 8 7 -2 65.5614 20.0999 4 8 -7 2 97.6169 13.2446 3 8 7 -2 96.4232 20.2629 3 -8 7 2 88.8864 19.8541 2 -8 7 -2 69.7505 19.4356 2 8 7 2 52.6391 17.2647 3 8 7 2 53.9101 18.9497 4 8 -7 -2 51.3785 12.6094 3 8 -7 -2 34.0497 19.5717 4 0 8 2 266.804 26.7390 2 0 -8 -2 252.455 24.6021 3 0 8 -2 297.070 27.2206 2 0 8 -2 238.220 26.0224 2 0 -8 2 208.516 26.1576 4 0 8 -2 232.889 26.0238 4 0 8 2 248.870 26.8685 4 0 8 2 246.870 27.2930 4 0 8 -2 264.513 23.5968 3 0 8 2 253.608 26.3634 2 0 8 2 232.238 23.7123 3 0 8 -2 269.693 23.4183 3 -1 8 2 90.7808 11.8949 3 1 8 -2 89.6346 12.2322 3 1 8 -2 55.9294 12.0925 2 -1 8 2 70.2188 14.1579 2 -1 -8 -2 83.9915 13.2548 3 1 -8 2 84.6665 10.7295 3 1 8 -2 91.6195 13.9677 4 1 -8 2 101.270 15.7744 4 1 8 -2 68.6896 12.2169 2 -1 8 2 114.030 16.1580 4 1 8 -2 92.9621 14.2518 4 1 8 -2 75.2872 12.0552 3 -1 8 2 68.6372 13.8728 2 1 -8 -2 106.492 15.1661 4 1 8 2 105.853 12.4750 3 -1 8 -2 89.8390 10.7838 3 1 -8 -2 94.0637 12.4530 3 -1 8 -2 67.2489 14.5239 2 1 8 2 108.399 15.6669 4 1 8 2 65.0961 12.1738 2 -1 8 -2 56.7636 13.4833 2 1 8 2 73.1504 13.0258 2 -1 8 -2 121.178 15.7138 4 1 8 2 115.872 15.7352 4 2 8 -2 241.953 22.7765 2 2 8 -2 228.486 22.5241 2 -2 8 2 251.945 25.7478 2 -2 8 2 199.059 20.4591 3 2 -8 2 192.934 19.5908 3 2 8 -2 198.425 21.5258 3 2 8 -2 179.469 23.3700 4 2 8 -2 238.044 22.2243 3 -2 8 2 249.864 25.6957 2 2 8 2 251.176 22.7720 3 2 8 2 234.905 22.5797 2 -2 8 -2 206.120 24.5395 2 2 -8 -2 208.943 21.0691 3 2 8 2 179.216 23.8304 4 -2 8 -2 198.072 19.5796 3 2 8 2 185.221 21.6240 3 3 -8 2 971.653 76.5241 3 3 8 -2 921.683 79.0557 3 3 8 -2 771.213 77.5216 2 3 8 -2 1004.07 80.7820 4 3 -8 2 966.990 82.7220 4 3 8 -2 1101.70 81.8543 4 3 8 -2 815.899 77.6929 2 3 8 -2 948.725 79.4619 3 -3 8 2 902.332 77.3149 3 3 8 2 1077.73 82.6463 4 3 8 2 789.920 77.5749 2 3 8 2 850.171 78.0234 2 3 8 2 1036.15 82.1122 4 3 8 2 1062.74 81.8474 3 3 -8 -2 1078.45 84.2906 4 3 8 2 915.263 79.4009 3 3 -8 -2 937.678 77.5035 3 -3 8 -2 899.580 76.3278 3 4 8 -2 141.684 21.6143 4 4 8 -2 210.020 18.6872 2 -4 8 2 194.412 25.0566 2 4 8 -2 208.766 18.4421 2 4 -8 2 157.940 17.3009 3 -4 -8 -2 159.347 22.3296 4 4 8 -2 177.220 21.8708 3 -4 8 2 181.395 18.7464 3 4 8 2 194.237 22.0685 3 4 8 2 199.967 18.5323 2 4 -8 -2 157.124 18.7685 3 -4 8 -2 207.143 25.2846 2 5 8 -2 158.719 21.8461 4 5 -8 2 129.459 13.6942 3 5 -8 2 140.943 24.0320 4 -5 8 2 97.5732 20.8879 2 5 8 -2 125.863 18.9823 3 -5 8 2 118.252 14.9674 3 5 8 2 115.244 11.0583 2 5 -8 -2 140.010 15.6723 3 -5 8 -2 103.428 20.4963 2 -5 8 -2 135.518 13.8934 3 5 8 2 117.959 19.4208 3 -5 -8 2 127.169 18.5005 4 5 8 2 175.456 22.9623 4 5 -8 -2 155.762 22.7029 4 6 -8 2 25.3651 16.5482 4 6 -8 2 36.4566 7.63878 3 -6 8 2 46.5353 9.50745 3 6 8 -2 31.9686 14.5437 4 6 8 -2 30.0451 13.3432 3 -6 8 2 40.9203 16.4729 2 6 -8 -2 39.7274 9.90356 3 -6 8 -2 50.7192 15.9209 2 6 -8 -2 13.4428 15.5238 4 6 8 2 29.1845 12.6633 3 -6 8 -2 26.9575 7.04933 3 6 8 2 18.7308 13.8055 4 7 -8 2 46.2048 8.46280 3 7 -8 2 29.9132 17.9833 4 -7 8 2 37.3933 16.1381 2 7 8 -2 34.2434 16.7930 4 7 8 -2 26.8626 15.6391 3 -7 8 2 16.9298 9.06050 3 7 8 2 50.6227 15.4772 3 7 8 2 27.4058 16.2559 4 7 -8 -2 36.0870 10.3609 3 -7 8 -2 42.6658 16.1294 2 -7 8 -2 29.3192 7.46533 3 7 -8 -2 49.1889 20.1425 4 8 -8 2 83.0410 16.0445 3 8 8 -2 72.3532 19.1685 4 -8 8 2 90.5749 21.7957 2 8 8 2 44.3698 19.4846 3 8 8 2 29.0794 18.1346 4 -8 8 -2 64.4274 19.0431 2 8 -8 -2 66.9266 13.1643 3 0 9 -2 167.157 22.3572 2 0 9 2 191.995 23.0555 2 0 9 -2 206.732 20.3197 3 0 -9 -2 256.536 21.8310 3 0 9 2 178.687 23.0538 2 -1 9 2 941.810 76.9551 3 1 -9 2 981.477 76.3891 3 1 9 -2 944.988 79.3457 2 -1 -9 -2 938.022 77.9426 3 1 9 -2 921.345 77.1648 3 1 -9 2 838.848 80.2501 4 -1 9 2 937.960 81.2240 4 -1 9 2 1041.91 81.5097 2 1 9 -2 945.124 79.5671 4 1 9 -2 1053.46 80.7461 4 1 9 -2 1053.40 79.7312 2 1 9 -2 1017.50 77.5062 3 1 -9 -2 761.570 80.1029 4 1 9 2 899.859 78.9764 2 -1 9 -2 977.663 80.9556 2 -1 9 -2 963.681 80.7441 2 1 9 2 861.463 78.8660 2 -1 9 -2 917.370 76.0726 3 -1 9 -2 818.259 79.6325 4 1 9 2 894.066 80.1050 4 1 9 2 765.085 79.4835 4 1 -9 -2 861.580 76.7824 3 1 9 2 938.691 77.5499 3 2 9 -2 117.816 14.5797 3 2 9 -2 52.8083 12.6075 2 2 9 -2 112.723 15.9537 4 -2 9 2 73.2160 16.4088 2 -2 9 2 112.833 13.0065 3 2 9 -2 83.8977 14.3028 3 2 9 2 102.701 18.5171 4 2 9 2 124.209 17.7639 4 -2 9 -2 96.3751 17.0937 4 -2 9 -2 82.1576 11.2051 3 2 9 2 69.6919 14.1344 2 2 9 2 62.9249 12.9466 3 2 -9 -2 84.3286 12.6140 3 2 9 2 87.2923 13.4934 3 2 9 2 67.2403 12.9884 2 3 9 -2 62.2529 11.9857 2 -3 9 2 64.3257 10.6873 3 3 -9 2 61.4258 9.54196 3 3 9 -2 58.2103 10.9377 2 3 9 -2 58.4516 14.3895 4 -3 9 2 70.2104 16.4294 2 3 9 -2 70.3379 14.0018 4 3 9 -2 80.9443 13.8803 3 3 -9 2 69.6027 17.3560 4 3 9 2 63.3210 17.5501 4 -3 9 -2 59.2166 9.52182 3 3 -9 -2 57.2708 10.6236 3 3 9 2 43.8418 11.8409 3 -3 9 -2 54.3491 15.5498 2 3 9 2 40.5099 10.3734 2 3 9 2 52.7559 14.8750 4 3 9 2 65.9178 11.9480 2 3 -9 -2 43.5780 15.9092 4 -4 9 2 17.0368 7.47117 3 -4 9 2 2.43670 11.6114 2 4 -9 2 14.0270 5.92004 3 4 -9 2 12.6211 13.5310 4 4 9 -2 24.0355 11.1298 4 4 9 -2 19.7388 7.02173 2 4 9 -2 18.6196 7.27003 2 4 9 -2 17.6230 10.5250 3 4 9 -2 25.6665 11.3928 4 4 9 2 39.7000 13.9239 4 -4 9 -2 9.42265 11.8211 2 4 9 2 13.5193 10.0072 3 4 -9 -2 22.9125 7.99121 3 4 9 2 16.8435 6.95473 2 4 9 2 10.5581 6.36065 2 4 -9 -2 27.9438 15.6720 4 -4 9 -2 24.6615 6.37412 3 5 -9 2 176.916 16.4905 3 5 9 -2 184.692 15.2528 2 -5 9 2 173.897 25.7802 2 -5 9 2 163.156 18.2447 3 5 -9 2 156.307 27.4723 4 5 9 -2 157.268 22.8140 4 5 9 -2 168.057 14.8491 2 5 9 -2 181.921 22.8407 3 5 9 2 140.835 14.9202 2 -5 9 -2 169.885 25.0523 2 5 -9 -2 138.780 18.1228 3 5 9 2 133.685 23.7881 4 5 9 2 155.754 15.3446 2 5 9 2 142.841 22.0915 3 -5 9 -2 163.190 16.3415 3 5 -9 -2 116.998 26.3088 4 6 -9 2 38.9052 7.77372 3 6 9 -2 38.8859 14.2231 3 -6 9 2 32.9141 9.65002 3 -6 9 2 21.4312 14.6548 2 6 9 -2 79.1036 18.3866 4 6 -9 2 76.1456 21.7145 4 6 -9 -2 50.6619 10.4169 3 6 9 2 50.6808 16.3461 3 6 -9 -2 71.1022 21.3588 4 -6 9 -2 42.2633 8.09964 3 -6 9 -2 22.5276 14.2504 2 6 9 2 84.1862 19.2880 4 7 -9 2 143.788 26.7625 4 7 -9 2 180.190 16.9268 3 -7 9 2 162.198 27.6570 2 7 9 -2 118.215 25.4625 4 7 9 -2 160.056 25.4163 3 7 9 2 179.666 25.3561 3 7 -9 -2 158.757 19.1593 3 7 9 2 140.515 26.3076 4 7 -9 -2 125.190 29.9614 4 -7 9 -2 188.499 28.5000 2 0 10 2 52.5337 10.8466 3 0 10 -2 44.5833 10.1707 3 0 10 2 48.5897 13.9096 2 0 10 -2 64.2758 11.4605 3 0 10 2 57.8017 15.1349 4 0 -10 -2 55.8652 11.2026 3 0 10 -2 66.8139 14.9036 4 0 10 -2 60.3201 14.4052 4 0 10 -2 35.2419 12.3723 2 1 10 -2 117.138 17.0995 3 1 10 -2 135.293 19.9405 4 1 10 -2 138.318 18.8732 2 1 10 -2 113.921 17.1677 3 1 10 -2 130.526 18.5371 2 -1 10 2 129.837 20.8837 2 1 10 -2 131.818 19.9232 4 -1 10 2 133.312 16.8543 3 1 -10 2 162.047 23.9595 4 -1 10 -2 139.142 20.8331 2 1 10 2 137.775 18.8139 2 1 -10 -2 143.333 17.6851 3 1 10 2 137.434 17.4868 3 -1 10 -2 150.392 16.2842 3 1 10 2 161.866 21.9487 4 1 -10 -2 157.703 23.4314 4 1 10 2 152.270 20.8182 2 -1 10 -2 162.034 16.3273 3 2 10 -2 329.975 33.3137 4 -2 10 2 328.383 29.2316 3 2 -10 2 305.283 34.8147 4 2 10 -2 318.480 30.7078 3 2 -10 2 318.371 27.9077 3 2 10 -2 299.758 32.3737 4 2 10 -2 312.058 30.6924 2 -2 10 2 283.819 33.8987 2 2 10 -2 254.567 30.2660 2 2 -10 -2 284.868 28.9539 3 2 10 2 280.864 30.6674 2 2 10 2 320.423 33.7591 4 2 10 2 310.192 31.4820 2 -2 10 -2 310.787 27.7709 3 2 -10 -2 299.435 35.5423 4 2 10 2 298.146 30.9189 3 -2 10 -2 286.669 33.5029 2 -3 10 2 24.4139 13.0300 2 3 10 -2 12.1960 11.5705 4 3 10 -2 27.4886 9.32194 2 3 10 -2 25.2279 9.31419 2 3 10 -2 10.3706 9.90205 4 3 -10 2 7.14039 5.93957 3 3 10 -2 19.9815 10.3178 3 3 -10 2 18.4569 11.9311 4 -3 10 2 12.4484 7.27395 3 -3 10 -2 18.9183 6.80310 3 3 10 2 22.5562 10.2183 3 3 10 2 37.8298 9.66526 2 3 10 2 14.9852 11.9711 4 3 10 2 39.5454 10.5139 2 3 -10 -2 5.67309 13.6135 4 3 -10 -2 11.2341 7.34419 3 -3 10 -2 47.3324 14.3219 2 -4 10 2 245.644 31.4694 2 -4 10 2 212.180 23.8613 3 4 10 -2 236.453 29.4149 4 4 10 -2 255.662 28.9624 3 4 -10 2 228.790 22.2976 3 4 10 -2 252.157 24.3294 2 4 -10 2 203.529 31.6670 4 4 10 -2 273.649 24.7890 2 4 10 2 239.482 24.3000 2 -4 10 -2 186.706 21.9537 3 4 -10 -2 223.272 23.9797 3 4 10 2 290.864 25.4279 2 4 10 2 219.255 29.6278 4 4 10 2 263.380 28.7000 3 4 -10 -2 186.614 31.7461 4 -4 10 -2 261.052 31.4005 2 5 -10 2 85.1474 11.8435 3 5 -10 2 87.2905 23.1927 4 5 10 -2 82.5353 19.6185 4 -5 10 2 81.9483 13.6271 3 5 10 -2 75.4374 17.2106 3 5 10 -2 108.955 11.3939 2 5 10 -2 110.083 12.0494 2 -5 10 2 99.2115 22.4394 2 5 -10 -2 88.1281 13.8746 3 5 10 2 87.1517 11.2167 2 5 10 2 94.0387 18.3782 3 -5 10 -2 91.3574 20.5023 2 5 10 2 89.7430 11.8642 2 5 -10 -2 98.9920 23.8638 4 -5 10 -2 72.3753 11.3717 3 5 10 2 93.9003 20.9404 4 6 -10 2 7.85240 17.1481 4 -6 10 2 0.59028 7.56301 3 6 10 -2 16.7455 13.2087 3 6 10 -2 10.2373 14.5035 4 6 -10 2 9.58873 5.69214 3 -6 10 2 9.43677 14.6007 2 6 -10 -2 16.4219 17.4311 4 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736.695 68.6312 4 -3 3 -3 709.962 65.1447 3 -3 -3 3 744.166 64.9047 2 -3 3 -3 756.541 67.9264 2 3 3 3 824.677 65.2600 2 -3 -3 3 755.434 67.0856 4 3 3 3 728.837 66.8116 3 3 -3 -3 783.719 66.4448 3 -3 -3 3 763.111 66.9318 3 -4 3 3 394.977 35.1436 2 -4 3 3 388.927 36.3498 4 4 -3 3 338.674 34.6760 2 4 -3 3 376.851 32.0480 3 4 3 -3 383.877 34.4668 3 4 3 -3 408.682 35.0351 4 4 -3 3 382.882 36.2054 4 -4 3 3 366.121 33.0019 3 -4 -3 -3 392.295 35.9217 4 -4 3 3 349.598 34.8006 2 4 3 3 399.081 36.2458 4 4 3 3 389.537 33.9475 3 -4 3 -3 355.216 34.5868 2 -4 3 -3 408.564 36.3260 4 -4 3 -3 387.453 32.0609 3 -4 -3 3 356.395 33.7197 3 4 -3 -3 415.046 36.8971 4 -4 -3 3 401.340 34.6275 4 4 3 3 392.990 34.2284 3 4 -3 -3 368.357 33.2798 3 5 3 -3 89.6665 15.5738 4 -5 3 3 87.3739 12.0856 3 -5 3 3 106.144 13.8863 2 -5 -3 -3 86.4690 13.7650 4 -5 3 3 90.7086 15.7157 4 5 -3 3 83.0295 16.5026 4 5 3 -3 96.9350 14.2595 3 5 -3 3 85.4207 11.2908 3 -5 3 3 96.0424 14.4070 2 -5 3 -3 131.619 15.6443 2 5 3 3 107.651 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180.102 19.0518 3 -3 -6 -3 191.701 20.3409 4 -3 6 3 143.265 19.9536 2 3 6 -3 138.492 16.3558 2 -3 6 3 185.985 17.3967 3 -3 6 3 159.208 20.4715 2 3 6 3 159.989 16.8199 2 3 -6 -3 193.981 17.7254 3 3 6 3 215.000 19.1710 3 3 6 3 164.135 16.6201 2 -3 6 -3 143.130 19.7613 2 3 6 3 161.362 18.4704 3 -3 -6 3 199.221 19.1985 4 -4 6 3 362.658 34.4146 2 4 6 -3 278.582 30.8477 3 4 6 -3 369.459 32.3239 3 4 6 -3 309.441 32.2841 4 -4 6 3 316.170 29.8640 3 -4 6 3 305.656 34.2108 4 -4 -6 -3 341.950 33.4084 4 4 -6 3 331.833 28.2176 3 4 6 -3 349.191 28.1041 2 4 6 -3 380.949 28.2924 2 -4 6 3 369.464 34.4749 2 4 -6 3 316.707 34.0503 4 4 6 3 369.746 28.5699 2 4 -6 -3 298.799 34.7162 4 -4 6 -3 339.878 34.3409 2 4 6 3 308.638 33.6395 4 -4 6 -3 371.481 34.3449 2 -4 6 -3 316.717 28.1963 3 4 6 3 346.803 31.9419 3 -4 -6 3 299.339 31.6329 4 -4 6 -3 314.343 34.3069 4 4 -6 -3 355.755 30.4131 3 4 6 3 277.218 30.9716 3 4 6 3 351.491 28.3833 2 5 6 -3 127.886 17.1907 3 -5 -6 -3 103.801 17.4315 4 -5 6 3 95.1317 17.6930 2 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19.3250 4 8 -6 3 33.1708 8.89761 3 8 6 -3 35.2201 15.2286 3 -8 6 3 19.3280 13.0672 2 8 -6 -3 45.1594 12.2852 3 8 -6 -3 40.9458 19.3565 4 8 6 3 42.0647 18.1153 4 -8 6 -3 38.3242 14.4927 2 8 6 3 28.8306 15.0676 3 0 7 -3 52.2283 11.1718 4 0 7 -3 78.6323 9.83476 3 0 -7 -3 90.8263 11.7932 3 0 7 3 92.6675 13.7337 4 0 7 3 94.8986 10.7835 3 0 7 3 58.8139 12.6542 4 -1 7 3 734.674 67.2181 2 1 -7 3 809.354 63.8309 3 1 7 -3 837.657 66.6852 2 1 7 -3 791.465 64.6797 3 1 -7 3 714.925 67.4305 2 -1 -7 -3 729.328 65.1757 3 1 7 -3 711.636 66.0391 4 -1 7 3 768.487 64.6168 3 1 -7 3 799.240 67.4239 4 1 7 -3 739.922 65.9575 2 1 7 -3 777.774 66.2197 4 -1 7 3 803.262 67.7184 2 -1 7 3 875.760 68.5425 4 1 7 -3 750.334 64.5807 3 -1 -7 3 792.459 66.5770 2 1 -7 -3 751.112 64.7434 3 -1 7 -3 805.944 67.1830 4 1 7 3 860.584 66.9341 2 -1 7 -3 788.407 63.7171 3 1 7 3 787.699 66.4036 2 1 7 3 838.477 65.3794 3 1 -7 -3 769.541 68.1570 4 -1 7 -3 810.436 67.6582 2 1 7 3 757.178 66.9498 4 1 7 3 701.408 67.0691 4 -2 -7 -3 415.342 34.7446 3 2 7 -3 408.371 33.9317 3 -2 7 3 394.581 32.9494 3 2 -7 3 416.398 37.4061 4 2 7 -3 416.814 35.0925 4 2 7 -3 329.847 33.4831 3 2 7 -3 401.150 35.2661 4 -2 7 3 453.102 37.6220 2 -2 7 3 458.584 37.7089 2 2 -7 3 437.922 37.9395 2 2 -7 3 406.504 31.8427 3 -2 7 3 393.282 37.0432 4 2 7 3 414.073 34.5809 2 2 -7 -3 316.341 36.4690 4 -2 7 -3 345.656 36.2321 2 2 7 3 325.740 33.5718 3 -2 7 -3 334.786 35.5957 4 2 7 3 314.398 35.4442 4 2 7 3 344.948 33.8400 3 -2 7 -3 322.436 31.4163 3 2 7 3 322.772 33.4546 2 2 -7 -3 358.165 32.8210 3 -2 7 -3 349.366 35.7028 2 3 7 -3 104.090 14.8836 4 3 7 -3 110.885 12.9403 2 3 7 -3 93.4566 15.1629 4 3 7 -3 130.893 13.2241 2 -3 -7 -3 96.6363 15.6274 4 3 -7 3 104.869 17.8208 4 3 -7 3 93.2982 10.8999 3 -3 7 3 88.0322 15.2448 4 -3 7 3 112.900 16.2005 2 -3 7 3 89.9060 12.7188 3 3 7 -3 112.032 15.0143 3 3 7 -3 94.0885 13.7406 3 -3 7 3 118.760 17.0183 2 -3 7 -3 114.827 11.2525 3 3 -7 -3 115.873 13.5237 3 3 7 3 104.748 14.1716 3 3 7 3 124.827 15.2623 3 -3 7 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3 6 7 -3 122.600 21.0738 4 6 -7 3 141.300 26.4583 4 -6 7 3 181.682 24.6987 2 6 -7 3 179.105 16.5085 3 -6 7 -3 166.986 16.3594 3 6 7 3 134.335 23.9477 4 6 7 3 139.864 22.1145 3 -6 7 -3 196.848 24.9104 2 6 -7 -3 138.553 23.6940 4 6 -7 -3 173.658 19.1204 3 7 -7 3 189.606 32.2477 4 -7 7 3 219.795 28.8013 2 7 -7 3 208.618 20.6748 3 7 7 -3 209.138 27.6708 4 7 7 -3 211.922 27.7472 3 7 -7 -3 231.446 33.0117 4 7 7 3 197.261 26.7661 3 -7 7 -3 214.755 29.4058 2 7 -7 -3 237.977 24.0250 3 7 7 3 191.445 29.2348 4 -7 7 -3 215.460 20.5310 3 8 7 -3 89.7871 20.9044 4 8 -7 3 123.831 28.0505 4 8 7 -3 167.295 25.6434 3 8 -7 3 138.781 14.8741 3 -8 7 3 120.381 22.7941 2 8 7 3 102.804 23.9405 4 8 -7 -3 95.6569 26.6851 4 8 7 3 86.2107 20.4188 3 8 -7 -3 113.195 17.7878 3 -8 7 -3 91.6362 21.8993 2 0 8 3 58.6831 10.6421 3 0 8 -3 85.6200 10.0380 3 0 8 3 67.0627 13.9328 4 0 8 -3 80.4935 13.1483 2 0 8 3 76.9899 12.8840 2 0 -8 -3 58.1336 10.9275 3 0 8 3 89.4375 14.0704 2 0 8 -3 57.5009 10.0008 3 1 8 -3 85.0799 11.0603 3 -1 8 3 69.5452 14.1030 2 1 8 -3 61.0131 11.5873 2 -1 8 3 81.0044 13.9128 2 -1 -8 -3 108.587 12.9399 3 1 8 -3 57.9807 12.2304 2 1 8 3 75.3608 12.0759 3 -1 8 -3 40.7916 12.6806 2 1 -8 -3 90.3053 12.1068 3 -1 8 -3 64.4252 13.6520 2 1 8 3 61.1049 12.5901 2 -1 8 -3 61.5205 9.24470 3 -1 8 -3 85.1121 10.3073 3 1 8 3 108.156 15.3501 4 1 8 3 88.9080 14.8355 4 1 8 3 60.9523 12.2433 2 2 8 -3 127.533 18.7422 4 -2 8 3 122.391 19.3928 2 -2 8 3 143.419 16.6894 3 2 8 -3 132.333 17.5075 2 2 8 -3 194.272 18.9075 3 -2 8 3 163.303 21.2359 4 2 8 -3 138.069 17.6146 2 2 -8 3 154.780 15.2359 3 -2 8 3 141.133 20.3813 2 2 -8 3 160.375 21.3345 4 2 8 -3 148.075 17.1687 3 2 8 -3 154.215 19.3698 4 2 8 3 160.151 17.9776 2 -2 8 -3 182.417 20.9986 4 -2 8 -3 161.138 15.1946 3 2 8 3 187.180 21.4627 4 -2 8 -3 148.558 20.5986 2 -2 8 -3 152.604 20.1084 2 2 -8 -3 160.078 20.6554 4 2 -8 -3 178.065 17.5005 3 2 8 3 167.012 18.0144 3 2 8 3 178.288 18.3087 3 2 8 3 125.695 17.6779 2 2 8 3 165.060 20.7872 4 3 -8 3 258.739 33.9428 4 3 -8 3 327.419 27.9091 3 3 8 -3 265.851 31.3610 4 -3 8 3 348.174 29.8361 3 3 8 -3 355.706 31.3488 3 3 8 3 296.164 33.3618 4 3 8 3 405.514 32.5404 3 3 -8 -3 256.828 34.1598 4 3 8 3 388.395 30.7139 2 -3 8 -3 323.826 27.9881 3 3 -8 -3 330.821 29.8146 3 -4 8 3 238.373 24.2639 3 4 -8 3 244.639 22.2976 3 4 8 -3 220.570 26.6537 3 4 8 -3 272.241 27.8770 4 4 8 -3 207.371 23.3174 2 -4 8 3 193.990 27.8776 2 4 -8 3 291.570 31.8545 4 4 8 -3 274.541 27.8411 4 -4 8 -3 264.993 29.3009 2 4 8 3 271.836 24.1209 2 4 8 3 288.067 24.0873 2 4 8 3 301.616 27.7831 3 5 -8 3 453.032 44.6944 4 5 8 -3 461.059 40.5283 3 -5 8 3 403.697 35.8770 3 5 8 -3 370.393 39.1074 4 5 -8 3 412.300 33.6751 3 -5 8 3 421.497 42.4337 2 -5 8 -3 380.176 33.6387 3 5 -8 -3 400.295 36.3324 3 -5 8 -3 444.687 42.4243 2 5 8 3 420.121 32.7604 2 5 8 3 376.195 32.4978 2 5 -8 -3 351.627 43.2309 4 -5 -8 3 358.791 38.6997 4 5 8 3 323.105 40.5708 4 5 8 3 416.993 39.5009 3 6 -8 3 204.249 31.7634 4 6 8 -3 191.853 26.8186 4 6 8 -3 293.059 29.3730 3 6 -8 3 239.959 20.9287 3 -6 8 3 254.614 30.8679 2 -6 8 3 213.131 23.5066 3 -6 8 -3 229.746 20.9167 3 -6 8 -3 265.019 30.6672 2 6 8 3 193.115 30.9713 4 6 -8 -3 233.205 24.2065 3 6 -8 -3 190.176 31.5962 4 -7 8 3 99.3432 22.4856 2 7 -8 3 140.138 27.7575 4 7 -8 3 118.064 13.2025 3 7 8 -3 99.6422 20.4386 3 7 8 -3 136.628 23.5530 4 7 -8 -3 144.702 27.9927 4 -7 8 -3 139.932 25.1468 2 7 -8 -3 116.537 17.0889 3 -7 8 -3 98.8678 12.6933 3 7 8 3 79.7004 18.7641 3 7 8 3 133.158 24.4100 4 8 8 -3 112.621 24.6922 4 -8 8 3 141.910 25.7007 2 8 8 3 128.706 35.9932 3 8 -8 -3 145.777 19.2658 3 0 9 -3 82.0396 12.0235 3 0 9 3 84.2661 16.8689 4 0 9 3 78.6661 17.0667 4 0 9 -3 103.676 12.6415 3 0 9 -3 87.2702 14.8686 2 0 9 3 76.9603 12.4252 3 0 9 3 93.6244 15.2284 2 0 9 3 96.3503 15.9637 2 0 9 -3 86.0967 15.1329 4 0 9 -3 104.885 15.9164 2 0 -9 -3 74.8848 12.9552 3 0 -9 3 77.2938 16.1904 4 1 9 -3 270.309 26.2822 4 -1 9 3 194.194 25.2629 2 1 9 -3 255.097 23.1093 3 -1 9 3 206.858 25.8817 2 1 9 -3 169.464 23.1868 2 1 9 -3 208.765 23.9802 2 -1 -9 -3 267.590 24.1367 3 -1 9 3 240.828 22.8349 3 1 9 -3 187.223 22.1695 3 1 9 -3 279.000 26.0107 4 1 9 3 229.951 23.1917 3 -1 9 -3 244.147 26.1039 4 1 9 3 211.810 24.1594 2 -1 9 -3 187.204 24.8210 2 1 9 3 273.959 27.4233 4 -1 9 -3 199.732 20.8734 3 1 9 3 192.150 24.6633 2 -1 9 -3 195.259 25.4482 2 1 -9 -3 238.864 22.7801 3 -1 9 -3 210.649 21.2845 3 1 9 3 242.623 26.6116 4 2 -9 3 20.8754 6.34608 3 -2 9 3 36.9378 12.7940 2 2 -9 3 12.5729 11.1528 4 -2 9 3 28.4950 8.11792 3 2 9 -3 27.9390 8.96156 3 2 9 -3 53.3479 10.8189 3 2 9 -3 42.0926 9.51889 2 2 9 -3 7.48399 8.44669 4 2 9 -3 17.3645 10.1753 4 2 9 3 23.2125 8.92957 3 2 9 3 22.9576 8.52602 2 2 9 3 7.74737 10.5804 4 2 9 3 16.8683 8.97796 2 2 9 3 15.6051 10.5642 4 -2 9 -3 15.5370 5.81965 3 2 -9 -3 19.4222 7.77482 3 2 -9 -3 17.5174 12.7606 4 -2 9 -3 37.6157 12.4680 2 -2 9 -3 12.4485 10.3835 4 3 -9 3 503.511 49.9696 4 -3 9 3 442.900 48.5959 2 3 9 -3 452.907 44.3170 2 3 -9 3 500.324 42.2149 3 3 9 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443.684 48.3623 4 -6 -6 4 462.912 44.6082 4 -6 6 -4 414.196 39.0996 3 -6 6 -4 482.378 46.8501 2 6 6 4 488.819 47.5154 4 6 -6 -4 465.637 42.0827 3 7 -6 4 4.58768 5.87832 3 -7 6 4 19.2892 12.8925 2 7 6 -4 5.68142 11.0688 3 7 6 -4 4.01964 10.7175 4 7 -6 4 9.08637 14.5835 4 7 -6 -4 3.35994 8.36871 3 7 -6 -4 6.23092 14.4054 4 7 6 4 8.17472 10.8224 3 -7 6 -4 8.74889 5.62125 3 -7 6 -4 11.0973 10.7759 2 7 6 4 7.21785 13.7997 4 8 6 -4 143.607 25.9834 4 8 6 -4 165.050 25.0778 3 8 -6 4 195.688 18.5584 3 -8 6 4 194.017 26.9966 2 8 -6 4 152.451 30.1106 4 8 -6 -4 155.064 29.7782 4 8 6 4 158.579 24.7163 3 8 -6 -4 173.524 22.3950 3 8 6 4 132.537 28.1144 4 -8 6 -4 175.299 26.0991 2 0 7 4 93.8088 13.3776 4 0 7 4 82.8714 11.3637 3 0 7 4 90.8892 13.0861 4 0 -7 -4 84.2047 11.9062 3 0 -7 4 82.9178 13.7286 2 0 7 4 90.7351 13.6297 2 0 7 4 97.5394 13.5530 2 0 7 -4 86.6438 10.5263 3 0 7 -4 90.0348 10.6384 3 0 7 -4 92.4965 13.1992 2 0 -7 4 72.4112 12.7467 4 0 7 -4 102.224 13.1391 4 -1 7 4 485.686 45.9596 3 -1 7 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102.067 16.8628 2 2 10 -5 77.6777 15.3498 3 2 10 -5 100.015 16.5838 2 2 10 -5 112.231 18.3448 4 2 10 -5 110.384 18.2788 4 2 -10 5 127.406 20.9959 4 -2 10 5 108.108 15.5902 3 2 10 5 137.012 21.7662 4 -2 10 -5 104.068 12.5674 3 -2 10 -5 113.106 12.5668 3 2 10 5 95.0057 17.4595 2 2 -10 -5 125.275 22.7279 4 2 10 5 115.462 16.7984 3 -2 10 -5 95.0042 19.5150 2 2 10 5 117.481 17.2876 2 2 -10 -5 109.885 16.2597 3 -3 10 5 424.339 45.8645 2 3 10 -5 472.858 43.1841 4 3 10 -5 500.454 41.6369 2 3 10 -5 477.745 41.5976 2 -3 10 5 451.067 40.4789 3 3 10 -5 420.791 42.8714 4 3 -10 5 474.036 46.5918 4 -3 10 -5 418.570 45.5997 2 3 10 5 441.609 42.1350 3 3 10 5 407.303 40.8597 2 3 -10 -5 421.213 40.0670 3 3 -10 -5 409.881 45.5975 4 -3 10 -5 425.545 37.0362 3 3 10 5 411.995 45.1387 4 -3 10 -5 455.861 37.3186 3 4 10 -5 55.8117 11.3233 2 4 10 -5 47.5581 10.7317 2 -4 10 5 46.7013 11.4152 3 4 10 -5 46.5421 14.4045 4 4 -10 5 42.9922 18.0096 4 -4 10 5 64.9673 18.0920 2 4 10 -5 29.1999 12.5244 3 4 10 -5 44.6280 14.4174 4 4 10 5 59.2041 14.4230 3 4 10 5 56.1371 18.0994 4 -4 10 -5 72.9715 18.6133 2 4 10 5 60.9444 11.8840 2 4 -10 -5 52.3492 19.1585 4 4 10 5 67.2649 13.1849 2 -4 10 -5 55.0241 7.24074 3 -4 10 -5 59.0139 7.25360 3 4 -10 -5 56.4550 12.0752 3 -5 10 5 27.0497 15.6377 2 5 10 -5 25.0795 7.05092 2 5 10 -5 30.6466 7.50765 2 5 10 -5 21.6681 13.3065 4 5 -10 5 15.6271 16.8305 4 5 10 -5 36.7551 13.9084 3 -5 10 -5 50.3895 17.1723 2 5 10 5 31.9537 13.3544 3 5 10 5 21.5759 15.8963 4 5 -10 -5 28.6958 17.8949 4 5 10 5 29.3317 7.36775 2 5 10 5 38.1329 8.65777 2 5 -10 -5 35.6836 11.1257 3 6 10 -5 169.622 27.5398 3 6 10 -5 171.228 25.2431 4 -6 10 5 144.396 27.9536 2 6 -10 5 141.456 30.5315 4 6 -10 -5 187.708 21.8703 3 6 10 5 202.983 30.2382 4 6 -10 -5 215.270 33.4407 4 6 10 5 199.959 26.6888 3 -6 10 -5 164.293 28.2644 2 0 11 -5 68.0411 16.8523 2 0 -11 -5 74.7112 14.1830 3 0 11 -5 77.3278 16.5020 4 0 11 -5 85.1006 13.2118 3 0 11 -5 60.0577 11.9010 3 0 11 5 92.5748 19.8301 4 0 11 5 61.9958 16.3796 2 -1 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57.5793 2 -2 3 9 674.694 57.1370 4 2 3 -9 650.409 53.0131 4 -2 -3 -9 578.516 55.5334 3 -2 -3 -9 626.911 57.2195 4 2 3 -9 761.168 56.0961 3 2 -3 9 671.399 57.7358 2 -2 -3 -9 682.687 56.3003 2 2 3 -9 681.347 53.0280 4 -2 3 9 696.992 56.0360 3 2 -3 9 635.674 56.6760 4 2 3 9 673.840 56.2870 2 2 3 9 657.654 55.6521 3 -2 -3 9 661.652 56.2028 2 2 -3 -9 705.984 57.4369 4 -2 -3 9 751.492 55.9232 3 2 -3 -9 680.470 56.0965 3 2 3 9 716.784 57.9717 4 -2 3 -9 604.193 56.4198 4 -2 3 -9 571.330 56.9080 2 2 -3 -9 693.443 57.5185 2 -3 -3 -9 2384.97 171.015 3 3 -3 9 2070.13 172.384 2 3 3 -9 2006.32 170.649 3 -3 3 9 2258.40 172.428 4 3 3 -9 2074.49 170.162 2 -3 3 9 2202.07 170.853 3 3 3 -9 2187.39 169.022 4 3 -3 9 2051.34 172.332 4 -3 3 9 2178.79 172.340 2 -3 -3 -9 2262.23 173.091 4 -3 -3 9 2291.34 170.928 3 -3 -3 9 2082.43 168.815 4 3 3 9 2101.33 170.569 2 3 3 9 2110.15 172.987 4 -3 3 -9 2109.91 172.310 2 -3 3 -9 2187.96 172.497 4 3 -3 -9 1966.92 171.755 2 3 -3 -9 2135.30 172.364 4 3 -3 -9 1980.11 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181.733 24.0223 4 7 -4 9 181.418 18.1998 3 7 -4 9 177.239 28.7552 4 7 -4 9 174.681 24.1689 2 7 -4 9 184.411 17.8527 3 -7 -4 9 198.399 23.8080 4 7 -4 -9 200.405 28.2474 4 7 -4 -9 215.416 23.8351 3 7 4 9 213.869 23.9047 3 7 4 9 188.377 29.0633 4 8 4 -9 53.0022 16.1261 4 8 -4 9 56.3137 20.7115 4 -8 4 9 57.1801 15.2313 2 8 4 -9 43.3078 15.5949 3 8 -4 9 49.3474 9.35735 3 8 -4 9 43.9686 9.41596 3 8 -4 -9 98.9686 17.1741 3 8 4 9 81.9190 16.3550 3 8 4 9 78.1339 21.5310 4 8 -4 -9 82.3590 22.0247 4 -8 4 -9 94.3908 18.6641 2 0 -5 -9 9.48484 5.89222 2 0 5 9 6.52482 5.16291 3 0 5 -9 1.01069 3.42019 3 0 -5 9 7.81334 3.43184 3 0 5 -9 3.33050 3.87257 4 0 -5 9 6.32642 4.49318 4 0 -5 9 6.10289 6.38512 2 0 5 9 7.68822 6.25045 2 0 -5 -9 2.18094 5.22130 3 0 5 9 2.69342 6.49733 4 0 5 9 7.42188 6.74466 4 0 5 -9 7.19053 5.86929 2 1 5 -9 266.552 25.3418 4 1 5 -9 313.615 28.4102 2 1 -5 9 271.187 27.3892 4 -1 -5 -9 304.072 28.4114 2 1 5 -9 272.397 26.1941 3 -1 5 9 243.417 28.7409 4 -1 -5 -9 267.589 27.3763 3 -1 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239.756 22.5848 4 4 6 -10 221.082 22.8333 2 4 -6 10 229.444 28.0714 2 -4 6 10 218.718 27.2397 2 4 6 -10 213.586 24.7635 3 -4 -6 -10 211.134 22.9501 2 4 6 -10 207.063 22.2729 4 -4 6 10 211.070 23.7969 3 4 -6 10 202.242 27.4736 4 4 6 10 244.523 29.0056 4 4 -6 -10 298.937 29.9905 4 -4 -6 10 255.023 23.5888 2 4 6 10 254.789 25.3824 3 -4 6 -10 272.852 28.1909 4 4 -6 -10 262.708 25.8806 3 4 6 10 258.077 24.0502 2 -5 -6 -10 509.869 43.6791 2 5 6 -10 497.103 42.9918 2 -5 6 10 428.119 48.1959 2 5 6 -10 476.686 44.4392 4 5 -6 10 525.939 50.0434 2 5 6 -10 436.738 46.3963 3 5 6 10 538.517 46.8969 3 5 6 10 571.497 44.2728 2 -5 -6 10 575.367 43.6024 2 -5 -6 10 514.463 44.2599 4 5 -6 -10 500.622 50.6364 4 5 6 10 436.209 49.6555 4 5 -6 -10 524.740 46.5165 3 6 -6 10 27.5082 13.5216 2 6 6 -10 15.5565 11.7487 3 6 -6 10 31.9744 15.9482 4 -6 6 10 21.2874 12.5654 2 6 6 -10 35.8707 11.0483 4 -6 -6 -10 21.9472 5.62679 2 6 6 10 16.5197 14.4131 4 -6 -6 10 14.7815 8.48003 4 6 6 10 13.3768 5.16456 2 6 -6 -10 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208.175 24.2068 2 3 -7 11 142.434 21.4390 4 -3 -7 -11 190.879 21.2080 3 3 7 11 121.979 20.5395 4 -3 7 -11 151.040 20.5872 4 3 -7 -11 157.060 19.6735 3 3 -7 -11 123.704 22.9057 4 -3 -7 11 182.277 18.6792 3 4 -7 11 471.865 46.5533 2 4 7 -11 462.432 40.7744 2 4 7 -11 439.831 39.2042 4 4 7 -11 482.030 39.4438 4 4 -7 11 454.116 45.3964 4 -4 7 11 471.596 46.0638 2 4 7 -11 410.697 42.4031 3 4 -7 -11 435.022 41.8952 3 4 7 11 447.425 46.4755 4 4 -7 -11 454.426 46.4503 4 4 7 11 444.795 41.2419 2 -4 -7 11 450.573 41.0369 2 5 7 -11 232.346 26.0657 3 5 -7 11 207.267 28.7261 2 -5 -7 -11 197.012 21.8390 2 5 -7 11 241.101 29.7915 4 5 7 -11 260.177 22.8424 4 5 7 -11 195.174 21.1070 2 -5 7 11 222.093 28.6188 2 5 7 -11 244.572 22.9172 4 5 -7 -11 212.117 29.9341 4 5 7 11 245.642 30.8825 4 5 7 11 187.231 21.9779 2 5 7 11 187.366 24.9068 3 5 -7 -11 202.231 24.4305 3 -5 -7 11 191.900 21.5246 2 6 7 -11 67.1909 16.9170 3 6 7 -11 73.0183 8.60758 2 6 7 -11 93.7336 8.38032 2 -6 7 11 79.8996 19.1378 2 6 -7 11 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464.875 34.2397 3 -1 -8 11 426.577 40.1754 2 -2 8 11 70.9237 17.0481 2 2 -8 11 112.340 17.9293 4 2 8 -11 80.5372 11.8364 4 -2 -8 -11 89.4617 15.9201 3 -2 -8 -11 75.9319 13.6456 2 2 8 -11 72.8825 11.9609 3 2 8 -11 104.050 14.4685 3 2 8 -11 79.6533 14.9165 2 2 -8 11 70.1473 17.2275 2 2 8 -11 109.019 12.2623 4 2 8 11 76.1247 14.6787 2 -2 8 -11 84.2004 14.7113 4 2 8 11 94.4459 18.8191 4 2 -8 -11 113.010 18.0956 4 -2 -8 11 85.5721 16.1717 2 2 -8 -11 75.2026 14.5880 3 3 -8 11 300.736 34.6771 4 -3 8 11 361.914 36.5195 2 3 8 -11 382.948 32.6899 3 -3 -8 -11 337.647 33.0468 3 3 8 -11 257.615 28.2579 4 3 -8 11 374.496 36.3868 2 3 8 11 256.659 34.8335 4 -3 -8 11 365.779 32.7603 2 3 -8 -11 311.524 32.2982 3 3 -8 -11 263.949 35.4645 4 4 8 -11 240.559 23.6385 3 4 8 -11 175.232 20.2768 2 4 -8 11 166.601 26.1347 2 -4 -8 -11 180.578 20.6492 2 -4 8 11 164.324 25.7668 2 4 -8 -11 180.750 23.0176 3 4 8 11 221.708 28.2889 4 4 8 11 162.440 22.3995 3 4 8 11 142.261 20.2428 2 4 -8 -11 216.824 28.8313 4 -4 -8 11 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90.8434 21.0836 4 8 -2 -14 76.2681 18.4044 3 8 2 14 83.6456 16.2737 3 0 -3 -14 239.545 25.1027 2 0 -3 -14 300.070 24.4465 3 0 3 14 214.377 24.9795 2 0 3 -14 240.909 21.9414 3 0 3 14 291.755 23.8701 3 0 3 -14 217.174 24.3747 2 0 -3 14 246.713 21.8859 3 0 -3 14 215.637 25.1020 2 -1 3 14 795.599 69.3640 2 -1 3 14 808.396 68.2656 4 1 -3 14 767.248 69.2254 2 1 -3 14 840.667 65.1375 3 -1 -3 -14 848.760 69.1231 2 1 3 -14 807.970 66.3258 3 1 3 -14 743.485 68.3766 2 -1 3 14 818.669 68.0931 4 -1 3 14 714.097 66.8524 3 -1 -3 -14 788.608 67.1522 3 -1 -3 -14 801.584 68.5669 4 -1 3 -14 792.786 65.0951 3 -1 3 -14 814.780 69.4575 2 1 3 14 819.901 67.0114 3 1 3 14 840.037 69.2184 2 -1 -3 14 742.922 68.6576 2 -1 -3 14 849.364 66.4768 3 1 -3 -14 782.891 67.4482 3 -1 3 -14 805.774 66.5155 4 1 -3 -14 826.017 69.4098 2 1 3 14 855.107 69.0619 4 -2 3 14 204.331 22.9376 2 2 -3 14 193.307 17.1820 3 -2 -3 -14 224.323 20.9344 3 -2 -3 -14 192.839 22.0917 4 -2 3 14 178.608 21.4134 4 2 -3 14 201.505 23.1493 2 -2 -3 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3 4 3 -14 74.3332 12.4996 2 4 -3 14 69.4913 7.55410 3 4 3 -14 78.3683 14.1017 3 -4 3 14 79.1458 14.9353 4 -4 3 14 76.0016 15.0027 2 4 -3 14 82.2076 15.7380 2 4 3 -14 74.7852 8.51512 4 4 -3 14 60.5671 7.63967 3 -4 -3 14 95.9881 8.60746 4 4 -3 -14 96.0063 14.6880 3 -4 3 -14 112.191 15.8222 2 4 -3 -14 100.449 16.6160 4 -4 -3 14 92.8379 13.7197 3 -4 3 -14 93.4853 15.7395 4 4 3 14 80.2399 17.4472 4 4 -3 -14 88.3827 14.6114 2 4 3 14 115.173 14.8603 2 4 3 14 93.9766 13.1056 3 -4 -3 14 98.8650 14.1244 2 -5 -3 -14 478.780 45.5174 2 5 3 -14 430.688 44.6394 2 5 3 -14 481.496 43.3217 4 5 -3 14 488.178 49.7253 4 -5 3 14 549.135 48.4893 4 5 -3 14 492.052 41.3496 3 -5 3 14 457.516 47.3874 2 5 3 -14 509.563 47.1680 3 5 -3 14 475.838 48.3270 2 5 3 14 519.421 46.0836 2 5 -3 -14 503.834 46.9420 3 5 3 14 534.490 45.9573 3 5 -3 -14 491.384 47.6813 2 -5 3 -14 532.280 51.3438 2 5 -3 -14 611.574 49.8262 4 5 3 14 573.618 51.3633 4 -5 -3 14 539.343 43.4572 4 -5 -3 14 501.010 45.5470 2 5 3 14 578.585 45.8699 3 6 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26.1615 17.2669 4 8 3 14 20.5126 7.77838 2 8 3 14 32.6734 12.4686 3 8 -3 -14 23.5056 14.0260 3 8 3 14 28.1557 19.2202 4 0 4 14 144.574 17.6600 3 0 4 14 141.653 19.4146 4 0 -4 -14 177.365 18.8125 3 0 -4 14 177.134 20.5436 2 0 4 14 184.271 20.8053 2 0 -4 -14 215.655 20.6016 2 0 -4 14 153.410 15.7661 4 0 4 14 152.358 19.4218 4 0 4 -14 173.842 16.2940 3 0 4 -14 159.770 15.5120 4 0 4 -14 196.022 20.6550 2 0 -4 14 193.146 16.6504 3 -1 4 14 190.947 21.8779 2 -1 4 14 154.267 18.8616 3 -1 -4 -14 189.511 19.8331 3 1 4 -14 209.103 18.3100 3 -1 -4 -14 185.346 20.8174 2 -1 4 14 175.290 20.6318 4 -1 4 14 187.513 20.7307 4 1 4 -14 187.091 20.7217 2 1 -4 14 202.961 21.8230 2 1 -4 14 167.236 18.4623 4 -1 4 -14 172.582 16.4494 3 1 4 14 171.954 21.1581 4 1 -4 -14 193.131 19.9627 3 1 4 14 178.695 18.9250 3 -1 -4 14 169.738 20.7789 2 -1 -4 14 141.813 17.5985 3 -1 4 -14 200.876 21.7383 2 -1 4 -14 183.138 18.2564 4 1 4 14 208.855 21.6674 2 1 4 14 173.649 21.1142 4 1 -4 -14 212.306 21.8923 2 -2 4 14 605.200 51.6538 4 2 -4 14 495.564 51.5651 2 -2 -4 -14 469.141 49.9544 2 2 -4 14 662.515 51.0109 4 -2 -4 -14 507.504 51.0468 4 -2 4 14 510.197 51.4807 2 -2 4 14 565.350 49.6673 3 -2 -4 -14 637.249 50.4638 3 -2 4 -14 578.723 45.7856 3 2 4 14 583.353 49.4032 3 2 -4 -14 646.752 52.3408 4 2 4 14 584.177 52.1637 4 -2 4 -14 528.592 51.5884 2 -2 -4 14 612.981 49.2709 3 2 4 14 641.856 51.5172 2 -2 -4 14 506.304 50.3351 2 2 -4 -14 560.449 51.6182 2 2 -4 -14 602.287 50.2928 3 3 4 -14 214.561 21.4441 3 -3 -4 -14 195.211 21.4235 3 -3 4 14 162.498 22.4110 4 -3 -4 -14 242.381 22.8412 2 -3 4 14 191.564 21.3790 3 -3 -4 -14 174.940 22.1108 4 3 -4 14 155.459 22.0672 4 -3 -4 14 245.363 21.4961 3 3 4 14 198.944 22.4057 2 3 -4 -14 168.587 21.3808 3 -3 -4 14 213.148 22.4506 2 -3 4 -14 202.287 23.5589 2 3 -4 -14 233.128 23.7830 2 3 4 14 169.760 20.0667 3 4 4 -14 974.508 80.4576 3 -4 4 14 875.027 82.1618 2 4 4 -14 821.009 79.1564 2 -4 -4 -14 1002.75 80.4194 3 4 -4 14 981.808 83.0450 4 -4 4 14 931.653 81.6974 4 4 -4 14 858.027 82.3714 2 -4 -4 -14 1014.69 80.5637 2 4 4 14 921.327 80.1966 2 4 4 14 904.737 79.4014 3 4 -4 -14 885.099 81.7773 2 4 -4 -14 1057.55 83.1891 4 -4 -4 14 909.751 79.8445 2 4 4 14 972.038 83.9501 4 4 -4 -14 967.205 80.6364 3 -4 4 -14 1123.25 83.4306 4 5 4 -14 124.634 19.0792 3 -5 -4 -14 152.775 17.5851 2 5 4 -14 144.651 17.0745 2 -5 4 14 144.288 20.5695 2 -5 4 14 94.8504 19.6698 4 5 -4 14 98.7048 21.4120 4 5 -4 14 155.943 21.6959 2 5 -4 -14 106.581 19.8821 4 5 4 14 119.667 22.5047 4 5 -4 -14 139.915 20.2562 3 5 4 14 167.325 18.6748 2 -5 -4 14 128.498 13.6576 4 5 4 14 142.113 18.7742 3 -5 -4 14 152.203 17.1136 2 6 4 -14 25.1085 8.33665 4 6 -4 14 28.7941 16.0150 4 6 4 -14 14.5866 11.1941 3 6 4 -14 33.4038 8.45057 2 -6 -4 -14 23.3730 9.03564 2 6 -4 14 23.9564 12.4206 2 -6 4 14 20.6688 11.5573 2 -6 -4 14 11.2455 7.01153 4 6 4 14 12.7229 14.2087 4 6 -4 -14 16.6741 14.1162 4 -6 -4 14 19.3414 7.95392 2 6 4 14 13.0157 8.63697 2 6 -4 -14 18.5757 11.9768 3 6 4 14 15.0727 9.34581 3 7 4 -14 20.9102 6.07474 2 -7 -4 -14 35.4412 9.47688 2 -7 4 14 23.3584 12.9519 2 7 -4 14 39.7826 18.2900 4 7 4 -14 25.3627 9.91027 4 7 4 -14 26.1562 13.3771 3 7 -4 14 39.2605 14.2836 2 7 -4 -14 23.9630 14.9327 4 7 4 14 21.7327 8.37045 2 7 -4 -14 14.2577 12.9344 3 -7 -4 14 23.1811 9.94347 4 7 4 14 14.5188 11.7247 3 -7 -4 14 16.4756 6.63059 2 7 4 14 26.7539 17.2317 4 8 -4 14 85.9022 20.2897 2 -8 4 14 106.260 21.5863 2 8 -4 14 144.693 28.4393 4 8 4 -14 95.8809 22.2186 3 8 4 14 114.686 27.2958 4 8 -4 -14 152.908 25.9784 4 8 -4 -14 109.065 20.8374 3 8 4 14 85.3533 18.6594 3 0 5 14 1039.73 103.388 4 0 -5 -14 1337.00 103.068 3 0 -5 -14 1373.28 105.190 2 0 -5 14 1311.81 105.067 2 0 -5 14 1181.18 100.088 4 0 5 -14 1223.24 104.366 2 0 5 14 1222.68 102.313 3 0 5 -14 1297.79 100.343 3 0 5 14 1397.74 105.337 2 0 5 14 1073.62 103.805 4 1 5 -14 359.982 35.2008 2 1 -5 14 325.710 35.9841 2 -1 5 14 342.598 33.4185 3 -1 -5 -14 395.120 34.4687 3 -1 5 14 425.567 36.4390 4 1 -5 14 367.795 30.3112 3 -1 5 14 303.365 35.3840 2 -1 5 -14 353.600 35.7846 2 -1 -5 14 316.559 34.8597 2 -1 5 -14 381.527 30.4587 3 -1 -5 14 354.995 32.2293 3 1 5 14 429.237 36.9982 4 1 5 14 376.950 33.6860 3 1 -5 -14 372.661 34.2736 3 2 -5 14 148.805 20.1131 2 -2 -5 -14 155.219 18.4210 2 -2 5 14 103.401 17.2309 4 -2 -5 -14 108.694 16.4823 3 2 5 -14 152.658 15.8323 3 2 5 -14 147.956 17.8730 2 -2 5 14 144.714 19.5229 2 -2 -5 -14 109.912 17.7735 4 -2 5 14 110.882 15.7077 3 -2 -5 14 159.096 16.3637 3 2 -5 -14 90.6115 18.3185 4 -2 -5 14 139.064 17.4588 2 2 5 14 141.893 18.2461 4 2 5 14 134.155 16.0461 3 -2 5 -14 112.130 16.0302 4 2 -5 -14 138.083 17.3287 3 -3 -5 -14 22.8611 9.36511 3 3 5 -14 31.2997 9.36571 2 3 -5 14 35.6599 12.2750 2 -3 5 14 24.3458 11.2717 2 3 5 -14 31.0090 9.26296 3 3 -5 14 20.7876 11.0047 4 -3 -5 -14 29.2974 9.61238 2 -3 5 14 27.1242 10.7074 4 -3 -5 14 21.9507 8.57308 3 3 5 14 15.1270 8.36646 2 -3 -5 14 22.6024 9.10522 2 3 5 14 12.9647 10.8084 4 3 5 14 17.7343 8.06460 3 3 -5 -14 12.4115 8.99708 3 3 -5 -14 17.9113 11.0066 4 -3 5 -14 17.2545 9.70153 4 4 -5 14 108.885 19.9375 4 -4 5 14 100.421 18.4065 2 4 5 -14 97.5693 14.2072 2 4 -5 14 110.542 18.8863 2 -4 5 14 94.6304 17.0698 4 -4 -5 -14 103.765 15.1174 2 -4 -5 -14 106.156 16.2114 3 4 5 -14 145.563 17.0228 3 -4 5 -14 96.8497 16.8779 4 4 -5 -14 70.6707 15.2008 3 4 5 14 90.5018 15.2224 2 -4 -5 14 96.5757 14.7758 2 4 -5 -14 91.5728 19.1758 4 4 5 14 91.8121 19.7443 4 5 5 -14 190.961 22.8003 2 5 -5 14 215.604 28.0801 2 -5 5 14 193.396 27.9659 2 5 5 -14 210.388 25.4817 3 -5 -5 -14 218.655 23.8655 2 5 5 14 218.437 23.9375 2 5 -5 -14 269.872 26.4165 3 5 5 14 244.766 25.1212 3 -5 -5 14 236.363 23.4986 2 6 5 -14 237.430 30.3304 3 6 5 -14 275.261 25.8579 4 -6 -5 -14 281.714 27.3267 2 -6 5 14 314.795 32.8743 2 6 5 -14 284.291 26.2605 2 6 -5 14 222.245 33.2898 4 6 -5 14 285.086 34.2310 2 -6 -5 14 267.453 25.3448 4 6 5 14 290.055 27.5909 2 6 5 14 263.928 34.9366 4 6 5 14 290.822 29.6945 3 -6 -5 14 283.346 26.6635 2 6 -5 -14 251.929 29.8696 3 6 -5 -14 211.256 31.9981 4 -7 -5 -14 124.313 15.7413 2 -7 5 14 100.259 20.7211 2 7 5 -14 92.2247 11.3913 2 7 5 -14 151.060 17.7060 4 7 -5 14 109.740 22.8905 2 7 5 -14 110.493 20.9534 3 7 -5 14 134.362 26.8536 4 7 -5 -14 126.121 21.3834 3 7 -5 -14 140.627 24.8788 4 7 5 14 114.706 14.7885 2 7 5 14 120.470 19.6900 3 7 5 14 130.988 26.5189 4 -7 -5 14 137.832 17.0583 4 -7 -5 14 119.015 12.7425 2 -8 5 14 63.4545 16.8522 2 8 5 -14 48.6452 12.8689 4 8 -5 14 68.8954 17.9339 2 8 -5 14 35.2354 20.5808 4 8 -5 -14 40.3309 20.8721 4 8 -5 -14 48.8129 15.7463 3 8 5 14 39.0776 14.5683 3 0 6 14 4.64074 8.85203 4 0 6 14 0.23507 6.05930 3 0 6 -14 5.27637 4.97902 4 0 -6 -14 6.25684 7.65285 3 0 -6 14 8.89833 9.08142 2 0 6 14 9.87523 8.93795 2 0 -6 14 8.67975 4.69904 3 0 -6 -14 5.15033 7.53645 2 0 6 -14 1.65037 4.75425 3 0 -6 14 4.87769 4.95339 4 0 6 -14 1.50599 7.53947 2 0 6 14 3.15534 8.70965 4 1 -6 14 367.371 34.4993 4 -1 6 14 360.745 37.7907 4 -1 -6 -14 413.252 36.2871 3 1 -6 14 412.294 38.9064 2 -1 6 14 435.860 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683.357 60.1567 3 -3 6 -14 700.110 61.8753 4 3 -6 -14 637.819 63.3370 4 3 6 14 760.437 62.0729 2 -3 -6 14 675.936 61.3670 2 3 6 14 633.448 63.0241 4 3 -6 -14 652.464 60.8062 3 -4 -6 -14 14.5222 9.98326 3 4 -6 14 10.7261 11.1036 2 4 6 -14 11.4911 9.12984 3 4 6 -14 1.72000 7.20067 2 -4 -6 -14 9.40545 7.84711 2 -4 6 14 1.51506 9.82106 2 4 -6 14 41.3482 14.8017 4 4 -6 -14 39.3985 15.6345 4 4 6 14 33.3477 14.8257 4 -4 -6 14 8.07284 8.20634 2 4 6 14 4.28423 7.94099 2 4 -6 -14 22.1340 10.4117 3 5 -6 14 31.1489 15.3580 4 5 6 -14 34.9068 12.7594 3 5 6 -14 41.1797 6.35462 4 5 -6 14 39.7280 14.9455 2 5 6 -14 37.2356 6.45822 4 5 6 -14 50.8009 10.5707 2 -5 -6 -14 58.1444 11.8765 2 -5 6 14 42.7719 14.8616 2 5 6 14 44.8958 12.6265 3 5 6 14 65.8666 12.4429 2 5 -6 -14 32.3639 12.0101 3 5 -6 -14 27.2582 15.0247 4 5 6 14 30.9005 15.7041 4 -5 -6 14 58.5849 11.3402 2 6 6 -14 112.762 20.6066 3 6 6 -14 123.870 13.8027 4 6 6 -14 116.682 13.6284 4 6 -6 14 118.613 24.7656 4 6 -6 14 105.197 21.8819 2 6 6 -14 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46.6030 11.5910 3 -1 7 -14 37.9215 6.17514 3 -1 7 -14 38.3528 5.93824 3 -2 -7 -14 502.906 46.5002 2 -2 -7 -14 492.997 45.8855 3 2 -7 14 463.750 45.6798 4 2 7 -14 467.825 45.7428 2 2 7 -14 427.905 43.6125 3 -2 7 14 481.296 48.3209 2 2 -7 14 471.022 48.5071 2 -2 7 14 440.221 47.1384 4 2 7 14 573.711 47.4180 2 -2 -7 14 569.499 47.7972 2 2 7 14 604.854 50.2959 4 -2 -7 14 543.329 43.9137 3 2 -7 -14 531.358 46.0400 3 -2 7 -14 412.113 44.6573 4 3 7 -14 12.6312 8.75307 2 3 7 -14 13.0559 9.65205 3 -3 7 14 15.9114 11.9885 2 3 -7 14 9.76602 11.4176 2 -3 -7 -14 8.47946 7.59720 2 3 -7 14 7.67545 9.80722 4 -3 -7 -14 10.2633 10.0024 3 3 7 14 20.0781 13.0156 4 3 7 14 32.3810 11.2592 2 3 -7 -14 17.2061 13.4651 4 -3 -7 14 27.6442 10.8175 2 3 -7 -14 21.6759 10.1851 3 -3 7 -14 23.8157 10.6071 4 -4 7 14 333.997 36.4987 2 4 -7 14 322.119 36.8328 2 4 7 -14 308.446 31.4365 2 4 7 -14 326.537 33.6362 3 -4 -7 -14 347.700 32.6419 2 -4 -7 -14 358.615 34.1466 3 4 -7 14 315.727 35.3090 4 4 7 14 237.178 35.5841 4 -4 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123.190 18.8870 2 3 -8 14 126.828 23.1016 2 -3 8 14 124.756 22.7299 2 3 8 -14 171.186 20.2556 3 -3 -8 -14 163.583 21.5641 3 -3 -8 -14 125.020 19.1896 2 3 8 14 118.219 18.6661 2 3 -8 -14 174.513 25.8248 4 3 8 14 139.909 24.2531 4 -3 -8 14 126.161 19.7878 2 3 -8 -14 142.354 20.1227 3 4 8 -14 259.071 29.1840 3 -4 -8 -14 200.757 29.3885 3 -4 -8 -14 289.029 28.8827 2 -4 8 14 283.242 33.8969 2 4 8 -14 275.632 28.2078 2 4 -8 14 289.473 34.8440 2 -4 -8 14 298.155 29.1202 2 4 -8 -14 219.582 29.7347 3 4 8 14 256.087 28.6539 2 5 8 -14 67.8265 15.8737 3 5 8 -14 39.1667 10.6637 2 5 8 -14 61.3274 6.83050 4 -5 8 14 38.0452 16.9668 2 5 8 -14 66.2024 7.11001 4 5 -8 14 47.0319 18.1124 2 5 -8 14 71.4414 19.3632 4 -5 -8 -14 55.2543 12.0939 2 5 8 14 35.5210 13.5492 3 5 -8 -14 60.8403 20.4753 4 -5 -8 14 45.1958 11.7831 2 5 -8 -14 47.7452 14.5625 3 5 8 14 58.0345 20.2647 4 5 8 14 30.4566 11.4805 2 6 -8 14 67.9992 20.6445 4 6 8 -14 30.8940 14.9513 3 6 -8 14 45.1290 18.4894 2 -6 8 14 60.1715 19.0005 2 6 8 -14 54.0462 9.01541 4 -6 -8 14 46.9535 9.87386 2 6 8 14 36.1017 14.3749 3 6 8 14 42.9314 19.7975 4 6 -8 -14 52.0321 16.1010 3 6 -8 -14 50.6427 20.4327 4 6 8 14 45.2653 10.6396 2 0 9 14 33.0567 14.6972 4 0 9 14 15.3918 11.6173 2 0 -9 -14 40.8408 13.1473 3 0 9 -14 44.0331 10.1288 4 0 9 -14 27.2005 7.32545 3 0 -9 14 10.0977 11.8350 2 0 9 -14 22.1607 7.30133 3 0 -9 14 51.6264 11.4726 4 -1 -9 -14 220.120 24.9646 3 -1 9 14 205.837 27.7450 4 1 9 -14 198.628 20.7448 3 1 9 -14 179.120 19.8053 4 1 -9 14 254.223 28.8068 2 1 9 -14 199.050 20.0086 4 1 -9 14 170.972 23.3399 4 -1 9 14 160.492 25.8317 2 1 9 14 174.603 27.0581 4 -1 9 -14 147.968 21.2926 4 1 9 14 238.132 26.6120 2 -1 9 -14 185.082 17.6869 3 -1 -9 14 216.748 26.4268 2 1 -9 -14 174.115 23.8135 3 -1 9 -14 208.454 17.7738 3 2 9 -14 297.811 29.4498 3 -2 -9 -14 290.389 32.6743 3 2 9 -14 340.844 27.4207 4 2 9 -14 290.006 26.9442 4 2 -9 14 287.398 35.9294 2 -2 9 14 288.997 35.4608 4 2 -9 14 341.206 33.8422 4 -2 9 14 243.688 33.2034 2 2 -9 -14 276.896 32.7189 3 -2 9 -14 338.261 32.7636 4 2 9 14 326.308 36.6427 4 -2 -9 14 279.569 33.4869 2 2 9 14 310.402 33.1985 2 -3 9 14 68.5428 16.8285 2 3 9 -14 23.2279 5.61107 4 -3 -9 -14 33.9095 13.3808 3 3 -9 14 22.9508 14.0950 4 3 9 -14 26.1018 5.64114 4 3 9 -14 45.3203 11.8219 3 3 -9 -14 55.0697 15.0313 3 3 9 14 26.4301 15.9149 4 3 -9 -14 34.3689 17.3484 4 4 9 -14 47.1801 6.22801 4 -4 -9 -14 49.8711 13.1529 2 4 9 -14 45.9455 12.1102 2 4 9 -14 57.9721 15.3213 3 4 -9 14 46.7874 17.8087 4 -4 -9 -14 46.6264 15.1320 3 4 -9 14 50.0815 18.0495 2 -4 9 14 42.6063 16.6725 2 4 9 -14 42.7189 6.09696 4 4 9 14 40.5850 18.2186 4 -4 -9 14 40.4103 12.6941 2 4 9 14 47.4107 14.5045 3 4 -9 -14 50.5257 15.0699 3 4 -9 -14 37.5897 18.7795 4 4 9 14 28.0872 11.6140 2 5 9 -14 164.565 16.2921 4 5 -9 14 182.280 30.0736 2 -5 -9 -14 235.954 24.2212 2 5 9 -14 214.783 22.4635 2 5 9 -14 171.688 16.3114 4 -5 9 14 211.104 30.3343 2 5 -9 14 184.224 31.0610 4 5 -9 -14 143.215 30.0956 4 5 -9 -14 170.083 24.4036 3 5 9 14 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24.2087 4 2 10 -14 282.403 27.2588 3 -2 -10 -14 240.786 30.8974 3 2 10 -14 273.140 24.5894 4 -2 10 14 293.496 34.0589 2 2 -10 14 273.078 34.0554 2 -2 10 14 260.993 33.3282 4 2 10 14 191.579 28.4836 2 -2 -10 14 230.463 29.7366 2 2 -10 -14 204.134 28.2299 3 2 10 14 183.521 31.6973 4 3 -10 14 14.2273 14.6508 2 3 10 -14 8.33010 9.26062 3 3 10 -14 5.30019 5.93851 4 3 10 -14 6.94250 5.53347 4 -3 10 14 31.1456 16.1393 2 -3 -10 -14 2.14820 11.8455 3 3 -10 14 17.0146 12.9744 4 3 10 14 15.8495 15.8485 4 3 -10 -14 20.9611 17.1654 4 -3 -10 14 12.4231 11.1162 2 3 -10 -14 6.60884 12.1807 3 3 10 14 24.0029 12.6712 2 4 10 -14 366.888 35.9634 3 4 -10 14 321.702 38.5079 4 4 -10 14 411.669 42.8419 2 4 10 -14 344.460 28.1249 4 4 10 -14 319.481 27.8150 4 4 10 14 324.748 35.8850 3 -4 -10 14 315.830 34.5340 2 4 10 14 312.326 34.2898 2 4 -10 -14 305.033 35.8184 3 4 10 14 258.152 39.1421 4 4 -10 -14 261.994 40.1174 4 5 -10 14 87.0669 21.6963 4 5 -10 14 59.2170 20.7153 2 5 10 -14 60.5653 16.8513 3 -5 10 14 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335.229 30.2382 2 4 -4 15 305.539 32.5572 2 4 -4 15 229.736 30.8219 4 -4 -4 -15 271.508 29.0321 3 4 4 -15 313.626 30.0434 3 -4 4 15 256.677 30.7142 4 4 4 -15 344.650 29.7403 2 -4 4 15 349.595 33.0428 2 4 4 15 283.469 28.3446 3 -4 -4 15 305.770 29.6009 2 4 -4 -15 262.718 29.5291 3 4 4 15 310.326 30.1094 2 4 -4 -15 217.762 30.7657 4 5 -4 15 105.041 20.5063 2 -5 4 15 109.888 19.6425 4 5 4 -15 99.9216 14.7276 2 -5 -4 -15 101.224 14.9821 2 5 4 -15 92.1630 9.74919 4 -5 4 15 100.483 17.8975 2 5 4 -15 68.3969 15.7573 3 5 -4 15 129.477 21.0330 4 -5 -4 15 81.1631 9.54121 4 5 4 15 78.6670 14.6562 2 5 -4 -15 104.878 17.9586 3 5 4 15 90.3836 20.9913 4 -5 -4 15 71.6679 13.7554 2 5 4 15 88.3649 14.8875 3 5 -4 -15 94.1816 18.1160 4 6 -4 15 107.579 20.1409 2 6 4 -15 122.461 20.0969 3 6 4 -15 128.137 14.3522 4 -6 -4 -15 109.405 16.2729 2 -6 4 15 118.562 21.5350 2 6 -4 15 110.912 23.3863 4 6 4 -15 105.085 15.3623 2 6 4 15 96.2361 22.5285 4 -6 -4 15 109.415 15.8142 2 6 4 15 98.7810 16.1641 2 6 -4 -15 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32.7617 20.2915 4 0 9 -15 292.188 29.6536 4 0 -9 15 291.067 30.1705 4 0 -9 -15 362.950 34.2766 3 0 -9 15 343.324 36.4864 2 0 9 -15 312.176 28.4661 3 0 9 15 355.961 36.3704 2 0 9 -15 304.496 28.3722 3 0 9 15 280.908 34.2779 4 1 -9 15 63.0405 18.1925 2 1 9 -15 73.3550 11.9310 3 1 9 -15 85.1327 11.1655 4 -1 9 15 62.6565 17.9250 4 1 9 -15 63.8910 11.6675 3 1 -9 15 82.9804 15.6947 4 -1 -9 -15 93.7841 17.0552 3 -1 9 15 67.6486 17.8779 2 1 9 15 51.1753 15.3810 2 1 9 15 60.9025 18.5359 4 -1 9 -15 58.4823 13.1538 4 -1 -9 15 44.8018 14.9938 2 1 -9 -15 53.9176 15.7212 3 -1 9 -15 62.8405 8.59263 3 -1 9 -15 53.1372 8.35483 3 -2 9 15 371.670 41.0636 4 2 -9 15 391.992 43.4210 2 2 9 -15 389.208 32.8294 4 -2 -9 -15 331.523 38.9058 3 2 9 -15 371.289 32.7090 4 2 9 -15 332.232 36.3014 3 2 -9 15 370.858 39.5440 4 2 9 15 443.188 44.3595 4 -2 9 -15 357.037 38.4115 4 2 9 15 462.155 42.0952 2 2 -9 -15 475.888 40.5162 3 -2 -9 15 477.668 42.6422 2 -3 9 15 92.6814 21.7784 2 3 -9 15 102.409 22.6339 2 3 -9 15 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20 39.1349 13.1239 3 6 -4 -20 34.3976 14.4161 3 6 4 20 44.1422 13.2599 2 -6 -4 20 35.5749 12.9075 2 6 4 20 33.3871 18.5754 4 7 -4 20 191.855 31.8122 4 -7 4 20 155.665 26.2523 2 7 -4 -20 181.104 28.8350 3 7 4 20 169.275 23.9775 3 -7 -4 20 158.116 22.8494 2 0 -5 -20 134.705 19.6237 3 0 -5 20 146.113 15.9273 3 0 -5 20 111.830 12.5789 4 0 -5 20 166.999 23.1100 2 0 5 20 187.032 23.6522 2 0 5 -20 137.307 12.4362 4 0 5 -20 163.899 16.0727 3 0 5 20 142.915 20.8934 4 -1 -5 -20 213.672 24.2438 3 1 5 -20 247.867 22.1428 3 1 -5 20 188.217 18.9365 3 -1 5 20 193.490 25.9825 4 -1 5 20 264.386 28.8876 2 1 -5 20 216.197 21.2561 4 -1 5 20 210.105 25.0579 4 1 -5 20 214.289 27.3848 2 -1 5 -20 186.318 19.3261 3 1 -5 -20 186.301 25.0482 3 1 5 20 187.945 25.5819 4 -1 5 -20 156.839 19.9108 4 -1 -5 20 217.459 26.7358 2 1 5 20 201.253 26.4082 2 -1 -5 20 198.973 21.0889 3 2 -5 20 166.228 14.1234 3 2 -5 20 206.003 25.6109 2 -2 5 20 198.649 25.0993 2 -2 -5 20 137.636 18.1587 3 -2 5 -20 136.787 14.0931 3 -2 5 -20 143.401 18.6001 4 2 -5 -20 164.388 21.3300 3 -2 -5 20 135.712 21.7546 2 2 5 20 123.289 22.5016 4 2 5 20 131.438 21.6760 2 -3 5 20 621.997 57.8392 4 3 -5 20 545.245 56.4660 4 -3 5 20 578.740 59.8933 2 3 5 -20 651.207 56.4931 3 3 -5 20 689.202 61.8218 2 -3 -5 -20 734.264 57.8670 3 -3 -5 20 661.497 59.3217 2 3 5 20 577.079 59.9175 4 3 5 20 654.129 58.9946 2 -3 5 -20 604.227 56.9269 4 3 -5 -20 643.326 57.6909 3 -4 5 20 159.264 25.6616 2 4 5 -20 202.062 23.1591 3 -4 -5 -20 162.608 23.7077 3 4 -5 20 208.943 26.4137 4 4 -5 20 157.826 26.2718 2 -4 5 20 186.384 23.6358 4 4 5 20 194.042 27.7189 4 4 -5 -20 173.528 23.4959 3 4 5 20 123.337 21.6053 2 -4 -5 20 125.508 21.5421 2 5 -5 20 93.8854 22.3405 2 -5 -5 -20 79.4762 17.1346 3 5 5 -20 86.1836 18.1365 3 5 -5 20 105.332 22.2028 4 -5 5 20 131.199 23.0370 2 -5 -5 20 109.080 18.6009 2 5 -5 -20 58.8346 19.3541 4 5 -5 -20 103.433 19.6455 3 5 5 20 115.804 19.1497 2 5 5 20 67.6030 21.5494 4 6 -5 20 86.8326 24.2183 4 6 -5 20 82.8403 20.6991 2 6 5 -20 77.0946 18.8150 3 -6 5 20 89.5813 21.1789 2 6 -5 -20 59.3288 19.9154 4 6 5 20 71.0969 22.5488 4 -6 -5 20 83.6395 16.4014 2 6 5 20 88.4082 17.1990 2 6 -5 -20 89.6332 19.0904 3 6 5 20 85.2677 16.8675 3 0 -6 20 1524.19 124.637 2 0 -6 20 1371.27 115.137 4 0 6 20 1519.30 124.473 2 0 6 -20 1393.91 117.324 3 0 6 20 1374.19 122.730 4 0 -6 -20 1508.60 121.328 3 0 6 -20 1480.14 114.997 4 -1 -6 -20 153.936 19.3914 3 1 -6 20 77.7943 18.8576 2 1 -6 20 96.2945 11.0343 3 -1 6 20 85.0699 19.4734 2 1 6 -20 102.900 14.4544 3 1 6 20 75.8711 18.0352 2 -1 6 -20 105.788 11.8858 3 -1 -6 20 73.3579 18.0609 2 1 -6 -20 99.7112 17.5807 3 -2 -6 -20 290.326 33.7921 3 2 -6 20 318.757 33.2247 4 2 6 -20 359.540 32.7827 3 -2 6 20 353.032 37.1089 4 -2 6 20 369.894 38.5763 2 2 -6 20 371.330 39.1017 2 -2 -6 20 337.330 37.0077 2 2 6 20 344.842 37.7108 4 -2 6 -20 310.141 32.2380 4 2 -6 -20 323.643 34.7160 3 2 6 20 311.264 35.8522 2 -2 -6 20 296.515 33.9285 3 -3 -6 -20 139.183 23.1106 3 3 6 -20 123.128 19.2725 3 3 -6 20 150.446 22.3716 4 -3 6 20 153.544 22.6375 4 -3 6 20 146.910 24.9800 2 3 -6 20 124.593 24.6350 2 -3 -6 20 160.878 23.5830 2 3 6 20 165.964 25.8970 4 3 -6 -20 132.969 21.7052 3 3 6 20 182.479 24.5219 2 -3 6 -20 158.534 21.4534 4 4 -6 20 133.847 22.8801 4 4 -6 20 103.038 22.8142 2 -4 -6 -20 101.642 20.2050 3 4 6 -20 114.959 18.7726 3 -4 6 20 105.231 21.5409 4 -4 6 20 117.736 22.8622 2 -4 -6 20 88.6834 18.6432 2 4 -6 -20 98.7684 19.6826 3 4 6 20 119.059 20.8767 2 4 6 20 109.317 24.4062 4 -5 -6 -20 100.326 19.6156 3 -5 6 20 76.0656 21.3374 2 5 -6 20 76.3869 22.0510 2 5 6 -20 74.6119 17.5302 3 5 -6 20 93.7652 21.1390 4 5 6 20 92.6348 23.6882 4 -5 -6 20 78.5402 16.8027 2 5 -6 -20 86.4365 20.7456 4 5 -6 -20 81.9085 18.5770 3 5 6 20 95.6404 18.0202 3 5 6 20 68.6940 16.8994 2 6 -6 20 96.0364 24.0947 4 6 -6 20 85.4780 23.5312 2 6 6 -20 141.858 22.9552 3 -6 6 20 93.4014 22.8892 2 6 -6 -20 65.5056 22.0582 4 6 6 20 94.1073 19.7608 3 6 6 20 88.1400 24.4648 4 6 6 20 105.403 18.1019 2 6 -6 -20 90.1962 20.0699 3 -6 -6 20 106.644 18.3201 2 0 7 20 139.800 22.9753 4 0 -7 20 117.340 14.0931 3 0 -7 -20 125.148 20.2570 3 0 7 -20 123.742 15.0574 3 0 -7 20 116.899 22.5020 2 0 7 20 146.764 22.9698 2 0 7 -20 116.922 11.2196 4 1 -7 20 258.198 24.6396 4 1 -7 20 266.833 32.1892 2 -1 -7 -20 234.990 28.3722 3 -1 7 20 290.982 31.3622 2 1 7 -20 209.443 24.0677 3 -1 7 20 265.167 30.9020 4 -1 7 -20 241.050 23.9153 4 1 7 20 215.266 30.3308 4 -1 -7 20 237.050 31.7312 2 1 7 20 234.100 30.5158 2 -1 -7 20 218.013 23.9018 3 1 -7 -20 215.448 27.8365 3 -1 7 -20 235.089 21.6724 3 -2 -7 -20 181.724 24.3204 3 -2 7 20 167.170 25.2866 4 2 -7 20 190.799 28.0654 2 2 7 -20 139.029 20.6858 3 2 -7 20 170.910 22.5286 4 -2 7 20 161.960 26.4265 2 2 -7 -20 172.213 24.0198 3 2 7 20 156.190 26.6863 4 2 7 20 225.472 26.7138 2 -2 -7 20 195.693 25.7619 2 3 -7 20 483.920 47.2790 4 3 -7 20 480.991 51.3906 2 -3 -7 -20 434.190 46.6310 3 -3 7 20 401.055 49.3431 2 -3 7 20 492.329 49.0592 4 3 7 20 537.345 51.9045 4 3 -7 -20 460.034 47.2239 3 -3 -7 20 512.561 48.6482 2 -3 7 -20 570.261 47.6000 4 3 7 20 468.085 48.7826 2 -4 -7 -20 49.0990 16.9365 3 4 -7 20 88.1950 21.5741 2 -4 7 20 53.3248 17.3660 4 -4 7 20 82.8824 20.5434 2 4 -7 20 53.0114 17.5629 4 4 7 -20 65.5007 15.3879 3 4 7 20 47.3836 20.1622 4 -4 -7 20 71.3931 16.9685 2 4 -7 -20 50.4757 15.5841 3 4 7 20 64.9410 16.6261 2 -5 7 20 65.2709 19.8216 2 5 7 -20 68.6028 16.8966 3 -5 -7 -20 61.0327 17.0923 3 5 -7 20 54.2114 18.8887 4 5 -7 20 55.7118 19.8321 2 5 -7 -20 45.3649 17.6421 3 5 7 20 33.8394 15.0223 3 5 -7 -20 62.2565 21.3075 4 5 7 20 59.6700 15.9595 2 -5 -7 20 54.5208 15.6188 2 5 7 20 53.9384 21.5831 4 0 -8 -20 357.794 39.5725 3 0 8 -20 411.764 32.1743 4 0 8 20 443.368 43.8971 4 0 8 -20 365.452 34.0097 3 0 -8 20 336.135 41.7751 2 0 8 -20 379.800 32.0846 4 1 -8 20 196.375 28.5597 2 -1 8 20 228.931 28.9136 2 -1 -8 -20 184.909 24.8601 3 -1 8 20 133.796 25.4069 4 1 8 -20 180.862 19.7880 3 -1 8 -20 170.845 16.2794 3 1 8 20 137.497 23.8590 4 -1 8 -20 165.938 16.3966 3 1 -8 -20 167.571 24.1864 3 -1 -8 20 195.159 19.4401 3 2 8 -20 65.1433 13.7735 3 2 -8 20 73.1615 15.3378 4 2 -8 20 73.4298 20.0091 2 -2 8 20 60.9211 18.4118 4 -2 -8 -20 68.9291 17.2386 3 -2 8 20 76.2883 20.0556 2 2 8 20 82.8453 21.2502 4 -2 -8 20 90.0064 19.6257 2 -2 8 -20 75.7259 14.9635 4 2 8 20 52.1059 17.7935 2 2 -8 -20 82.6737 18.2059 3 -3 -8 -20 107.901 21.1052 3 3 -8 20 110.763 20.9552 4 3 -8 20 111.830 24.3917 2 -3 8 20 96.4453 23.2035 2 3 8 -20 111.409 19.2051 3 -3 8 20 100.878 22.6805 4 3 8 20 151.760 22.4012 2 3 -8 -20 132.122 21.9370 3 3 8 20 119.236 25.5320 4 -3 -8 20 150.230 23.8064 2 4 -8 20 174.125 29.9648 2 -4 8 20 168.407 27.3254 4 -4 -8 -20 191.928 26.6765 3 4 8 -20 145.853 23.0024 3 4 -8 20 191.559 28.0591 4 -4 8 20 171.926 31.2850 2 -4 -8 20 160.246 25.1384 2 4 -8 -20 205.316 26.8217 3 4 8 20 192.175 26.2328 2 4 8 20 161.511 30.3848 4 5 -8 20 73.1245 22.9668 2 5 8 -20 69.2262 18.3027 3 -5 8 20 103.028 23.5671 2 5 -8 20 54.5617 19.6350 4 -5 -8 20 53.9993 15.5714 2 5 -8 -20 52.1419 17.1710 3 5 8 20 51.9664 21.4541 4 5 8 20 44.6263 15.5427 3 5 8 20 50.2648 15.7185 2 5 -8 -20 33.9356 19.0483 4 0 9 -20 3.42467 6.67426 3 0 9 20 4.62508 13.4563 2 0 -9 20 4.31782 12.9923 2 0 9 -20 0.83911 4.62212 4 0 9 -20 8.88507 5.13202 4 0 9 20 4.82575 13.5822 4 0 -9 -20 -1.6921 11.9781 3 0 9 -20 5.05854 6.29062 3 -1 9 20 124.383 25.2382 2 1 9 -20 125.067 16.1902 3 1 -9 20 132.585 18.0637 4 -1 -9 -20 134.169 23.4109 3 1 -9 20 124.535 25.1870 2 -1 9 20 116.612 24.6084 4 1 9 -20 126.113 17.0795 3 1 -9 -20 158.728 23.1390 3 -1 -9 20 141.275 26.2798 2 -1 9 -20 120.170 12.5219 3 -1 9 -20 127.850 12.6553 3 -1 9 -20 118.253 16.8095 4 1 9 20 124.835 25.6384 4 1 9 20 159.026 24.8373 2 2 -9 20 164.181 28.4624 2 -2 9 20 173.091 27.4647 4 -2 9 20 152.004 27.4815 2 2 -9 20 146.253 21.8182 4 -2 -9 -20 133.083 23.8393 3 -2 9 -20 134.519 20.5316 4 -2 -9 20 183.543 28.0340 2 2 9 20 177.478 25.8998 2 2 -9 -20 164.259 24.6025 3 2 9 20 130.957 27.4157 4 3 -9 20 73.3194 17.7557 4 3 -9 20 19.2290 16.7171 2 -3 9 20 34.6607 17.7668 4 -3 -9 -20 67.1852 17.5590 3 -3 9 20 16.0288 15.8731 2 3 9 -20 24.7454 12.3801 3 -3 -9 20 44.2894 16.1454 2 3 9 20 80.6246 22.0574 4 3 -9 -20 49.4366 17.3955 3 3 9 20 30.8157 14.3069 2 -4 9 20 205.289 31.5159 4 4 -9 20 201.151 28.4440 4 -4 -9 -20 184.042 26.7272 3 4 -9 -20 132.517 25.0623 3 4 9 20 132.158 29.8720 4 4 9 20 147.128 24.9932 2 -4 -9 20 162.085 25.3340 2 0 10 20 11.2456 14.1037 2 0 10 -20 7.19498 6.97905 3 0 -10 20 10.7263 14.1187 2 0 -10 -20 15.6447 14.0827 3 0 10 20 13.9924 15.4282 4 0 10 -20 9.62132 6.15749 4 -1 -10 -20 330.416 38.2465 3 1 10 -20 408.974 40.9413 3 -1 10 20 333.002 41.5283 2 1 -10 20 354.372 42.4982 2 1 10 -20 353.120 32.8062 3 -1 10 20 360.703 42.0972 4 1 -10 20 345.223 33.7573 4 -1 -10 20 342.267 40.2858 2 1 10 20 337.440 41.7776 4 -1 10 -20 292.092 27.7353 3 1 -10 -20 323.954 38.0228 3 1 10 20 391.536 42.5845 2 -2 10 20 22.7944 17.0162 4 2 -10 20 34.8799 18.7293 2 2 -10 20 37.3032 13.5288 4 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21 143.526 20.1407 2 -1 0 21 93.8253 13.2379 4 1 0 -21 111.594 16.5010 3 1 0 21 85.7936 15.0985 4 1 0 21 115.115 18.8800 2 -1 0 -21 111.803 15.1390 3 1 0 21 130.202 14.7256 3 -1 0 -21 115.499 15.1460 4 -1 0 21 93.4345 15.1940 3 -2 0 21 198.086 18.2729 4 -2 0 21 146.050 23.3409 2 -2 0 21 202.251 18.6374 4 2 0 21 147.086 18.5616 3 2 0 21 160.928 23.8093 2 -2 0 -21 179.140 21.2176 4 -2 0 -21 164.510 19.7103 3 2 0 21 227.630 22.8643 4 2 0 -21 163.071 21.2809 3 -3 0 -21 55.8957 13.7461 4 -3 0 21 56.8306 9.41329 4 3 0 21 59.2931 10.4543 3 3 0 -21 71.3172 14.1392 3 -3 0 21 60.3096 15.3169 2 3 0 21 51.4609 14.7258 2 -3 0 -21 56.4586 11.0405 3 -3 0 21 54.8166 9.60791 4 3 0 21 60.8383 14.7809 4 -4 0 21 110.143 19.4398 2 4 0 21 118.532 20.6772 4 -4 0 21 104.476 13.4701 4 4 0 21 94.2531 13.0867 3 -4 0 -21 88.2678 14.7786 3 4 0 -21 110.160 18.3298 3 4 0 21 90.2043 19.0370 2 -4 0 21 102.236 12.9966 4 -5 0 21 149.563 17.4899 4 5 0 21 143.389 25.0182 4 5 0 21 165.217 17.1921 3 -5 0 21 140.971 16.9260 4 5 0 21 134.710 17.1033 3 -5 0 21 136.400 22.0644 2 5 0 -21 158.267 22.4978 3 5 0 21 135.193 22.2577 2 6 0 -21 9.46170 9.49293 4 6 0 21 4.20473 14.8248 4 -6 0 21 -2.3571 8.03283 4 -6 0 21 3.93040 10.6411 2 6 0 21 3.35119 7.02192 3 6 0 21 4.22056 10.9262 2 6 0 21 -5.8798 7.00499 3 6 0 -21 -6.2447 10.6164 3 7 0 21 189.946 21.3297 3 7 0 -21 191.552 27.7881 3 -7 0 21 224.578 28.2581 2 7 0 -21 174.107 23.5743 4 7 0 21 181.706 32.0256 4 0 1 21 175.743 19.8858 3 0 -1 21 169.575 23.4632 2 0 -1 21 168.097 19.1794 3 0 1 -21 183.815 20.0277 3 0 -1 -21 166.736 19.9886 3 0 1 21 164.560 23.4156 2 0 -1 21 178.442 18.6491 4 0 1 21 183.061 20.2454 4 0 -1 21 164.353 18.3197 4 -1 1 21 305.847 32.9097 2 1 1 -21 335.757 29.3851 3 -1 1 21 319.599 28.7787 4 -1 1 21 303.283 28.6642 4 1 -1 21 294.176 33.0030 2 -1 -1 -21 290.603 28.6972 3 1 -1 21 312.414 29.2157 4 -1 1 21 329.876 29.5178 3 -1 -1 -21 285.582 29.5902 4 -1 1 -21 273.430 28.3811 4 -1 -1 21 286.154 26.3477 4 1 1 21 312.404 28.6386 3 -1 -1 21 251.305 28.3533 3 -1 -1 21 258.608 31.9660 2 1 -1 -21 298.462 30.2178 3 1 1 21 280.043 32.3174 2 -1 -1 21 326.590 26.5264 4 1 1 21 264.592 29.8047 4 -1 1 -21 252.901 27.6797 3 -2 1 21 212.174 27.3900 2 2 -1 21 217.101 21.8378 3 2 -1 21 232.900 25.3996 4 2 1 -21 219.243 24.0928 3 -2 -1 -21 212.547 25.0735 4 -2 1 21 235.419 22.5949 4 -2 -1 -21 235.755 23.7371 3 2 1 21 233.831 22.4691 3 -2 1 -21 195.316 23.8889 4 -2 -1 21 222.193 19.3923 4 2 1 21 165.904 25.7885 2 2 -1 -21 211.791 24.4626 3 2 1 21 205.778 25.1497 4 -2 1 -21 225.235 22.1437 3 -2 -1 21 195.447 26.6129 2 -2 -1 21 248.661 19.6708 4 -3 1 21 107.956 14.6059 4 3 1 -21 117.141 17.7320 3 -3 1 21 105.234 14.4301 4 -3 -1 -21 114.370 16.0148 3 -3 1 21 115.345 20.2376 2 3 -1 21 115.925 13.6981 3 3 -1 21 119.034 20.0840 2 3 -1 21 115.380 19.5445 4 -3 1 -21 110.909 14.3426 3 -3 -1 21 105.160 10.0672 4 3 1 21 109.080 19.5563 2 3 1 21 97.7121 20.1060 4 3 1 21 113.963 14.4241 3 -3 -1 21 102.957 10.1913 4 3 -1 -21 140.511 18.6554 3 -3 1 -21 104.657 18.0386 4 -3 -1 21 109.189 20.7586 2 4 1 -21 428.184 39.7482 3 -4 -1 -21 413.646 37.2385 3 -4 1 21 425.651 36.7370 4 -4 1 21 409.494 41.7632 2 4 -1 21 392.133 41.4914 4 -4 1 21 373.250 36.9255 4 4 -1 21 378.790 34.9873 3 4 -1 21 412.766 41.9201 2 4 1 21 415.895 42.2551 4 -4 -1 21 352.581 32.6743 4 -4 1 -21 388.227 35.5484 3 4 1 21 416.551 36.4895 3 4 1 21 436.234 41.7266 2 4 -1 -21 428.708 39.8900 3 -4 -1 21 376.859 40.6255 2 5 -1 21 44.5332 18.7140 4 5 1 -21 44.1753 14.8499 3 5 -1 21 36.8882 15.0509 2 5 1 21 67.0278 16.3043 2 -5 -1 21 74.6937 9.15176 4 -5 -1 21 59.1786 15.9107 2 5 1 21 64.6680 11.6228 3 -5 -1 21 73.1585 9.80380 4 5 1 21 73.9983 19.3923 4 5 -1 -21 79.5693 17.1195 3 5 1 21 73.8637 12.7351 3 6 -1 21 55.3707 16.1469 2 6 1 -21 35.6251 16.0225 3 -6 1 21 42.9932 15.5346 2 6 -1 21 61.0816 10.5677 3 -6 1 21 41.8672 13.1198 4 6 -1 21 41.6965 18.7517 4 6 -1 21 44.9571 9.25060 3 6 -1 -21 31.7817 14.1980 3 6 1 21 66.5776 20.7063 4 -6 -1 21 28.4191 8.83698 4 6 -1 -21 40.5536 13.1989 4 -6 -1 21 39.2528 14.6408 2 6 1 21 48.9627 11.4885 3 6 1 21 49.8801 15.7708 2 7 -1 21 3.26429 7.71905 3 7 1 -21 -3.1575 12.5065 3 7 -1 21 -2.0636 16.6408 4 -7 1 21 2.16517 12.5849 2 7 1 -21 9.18297 8.63778 4 7 -1 21 12.0093 12.2004 2 7 -1 -21 -1.0519 14.3116 3 7 1 21 3.69301 16.0406 4 7 1 21 7.21010 12.1773 2 -7 -1 21 0.89274 11.1121 2 7 -1 -21 13.0287 12.1068 4 7 1 21 11.3851 9.86943 3 0 2 21 674.677 62.2256 4 0 -2 21 801.655 66.0905 2 0 -2 21 711.966 60.2477 3 0 2 -21 684.579 60.3546 3 0 2 21 771.197 65.7264 2 0 -2 21 729.570 59.3682 4 0 2 21 612.209 61.4702 4 0 -2 21 677.082 59.1953 4 0 2 21 716.143 61.2923 3 0 -2 -21 771.884 62.3176 3 1 -2 21 266.980 25.3685 4 -1 -2 -21 288.317 27.2923 4 -1 2 21 274.880 30.1177 2 -1 2 21 268.100 26.3702 4 -1 -2 -21 259.472 26.2022 3 1 -2 21 230.631 23.9511 3 1 2 21 275.182 28.3381 4 -1 2 -21 212.875 23.9368 3 -1 -2 21 246.337 21.2344 4 -1 -2 21 231.256 24.8335 3 -1 2 -21 293.231 25.1186 4 1 -2 -21 251.242 27.5443 3 1 2 21 224.746 29.0314 2 1 2 21 238.104 25.0900 3 -1 -2 21 233.640 21.1899 4 -1 -2 21 226.908 28.0542 2 -2 2 21 288.904 29.4957 2 2 2 -21 204.705 23.7792 3 2 -2 21 223.714 21.5156 3 -2 2 21 223.924 24.0066 4 -2 -2 -21 220.448 25.4278 4 -2 -2 -21 218.995 23.6545 3 2 -2 21 213.161 24.7843 4 2 -2 21 255.100 28.8950 2 -2 2 21 218.017 24.2288 4 -2 -2 21 221.476 27.3728 2 2 2 21 214.490 26.0230 4 2 2 21 209.033 23.0467 3 2 2 21 251.642 28.0601 2 -2 2 -21 196.857 23.6706 4 -2 2 -21 189.141 21.1707 3 2 -2 -21 243.428 25.5095 3 -3 -2 -21 22.0572 9.80919 3 3 -2 21 19.4018 11.8750 4 -3 2 21 25.7038 12.9676 2 -3 2 21 28.0288 9.98051 4 3 2 -21 20.4542 11.3243 3 3 -2 21 21.3132 6.80778 3 3 -2 21 22.9412 12.6729 2 -3 2 21 27.0524 9.52029 4 3 2 21 38.7633 9.70593 3 -3 -2 21 35.8402 12.9043 2 3 2 21 40.2737 14.3443 4 3 -2 -21 50.9345 13.0354 3 -3 2 -21 47.7544 13.3763 4 3 2 21 42.4851 13.2385 2 -3 2 -21 45.6171 8.21103 3 4 -2 21 182.942 26.6287 4 -4 2 21 196.442 22.7335 4 4 2 -21 155.768 23.0307 3 4 -2 21 177.396 18.0156 3 -4 -2 -21 188.809 22.3777 3 4 -2 21 170.005 25.5804 2 -4 2 21 193.230 26.0380 2 -4 2 21 196.780 21.8207 4 4 -2 -21 189.834 24.2759 3 4 2 21 178.863 26.2668 4 4 2 21 215.161 26.9083 2 -4 -2 21 197.191 25.0838 2 5 -2 21 109.158 22.4149 4 -5 2 21 104.702 21.8154 2 5 -2 21 111.028 12.8801 3 5 2 -21 106.991 19.3411 3 5 -2 21 103.354 21.3871 2 -5 2 21 121.091 18.7113 4 5 -2 -21 142.445 20.4082 4 5 2 21 117.161 20.9259 2 5 -2 -21 103.228 19.3640 3 5 2 21 124.368 23.6405 4 5 2 21 118.254 17.5039 3 -5 -2 21 87.0073 19.3616 2 -6 2 21 95.2815 21.2409 2 6 -2 21 92.6134 23.6714 4 6 -2 21 104.327 22.6987 2 6 -2 21 89.5396 12.3751 3 6 -2 21 117.251 12.6652 3 6 2 -21 87.3979 19.1634 3 -6 2 21 60.8774 17.2933 4 -6 -2 21 146.497 21.3209 2 6 -2 -21 143.370 20.8933 4 6 -2 -21 138.695 21.9661 3 6 2 21 149.000 26.9343 4 -7 2 21 22.4583 14.5411 2 7 -2 21 22.9084 14.9814 2 7 2 -21 21.8707 14.6902 3 7 -2 21 44.5633 20.0385 4 7 2 21 41.4094 20.3732 4 7 2 21 45.1676 14.9836 2 7 2 21 51.3187 13.3380 3 -7 -2 21 48.7242 14.9325 2 7 -2 -21 39.2580 16.6380 3 7 -2 -21 50.9108 16.3548 4 0 -3 21 398.114 44.2028 2 0 3 21 465.629 45.3983 2 0 3 -21 480.017 40.0578 3 0 3 21 471.586 43.1882 4 0 3 21 442.310 42.9661 4 0 -3 -21 465.680 41.9612 3 0 -3 21 428.201 38.0153 4 -1 -3 -21 249.647 29.7110 3 -1 3 21 236.309 28.9767 4 1 3 -21 301.211 28.5220 3 1 -3 21 277.817 26.6687 3 -1 3 21 276.533 32.7679 2 1 -3 21 269.646 32.8670 2 -1 3 21 249.095 29.4470 4 1 -3 21 261.998 27.4957 4 1 3 21 299.472 31.6478 4 -1 3 -21 287.437 27.2061 4 -1 -3 21 338.118 33.6738 2 -1 -3 21 327.581 28.6892 3 1 3 21 312.157 32.9792 2 1 3 21 320.976 31.5826 4 1 -3 -21 348.780 30.9160 3 -1 3 -21 317.863 27.2711 3 -2 3 21 41.6362 14.5321 2 2 -3 21 40.9306 7.72325 3 -2 3 21 50.2050 12.0014 4 -2 -3 -21 38.1429 11.4377 3 2 -3 21 57.6944 12.8092 4 2 3 -21 48.6632 11.9266 3 2 -3 21 30.6220 13.7886 2 -2 -3 21 28.1165 12.4214 2 2 -3 -21 29.0881 11.6279 3 2 3 21 45.2148 13.6285 4 2 3 21 19.6524 12.0251 2 -2 3 -21 25.8624 7.30663 3 -2 3 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147.859 22.7008 2 5 -3 -21 117.654 22.1515 3 6 -3 21 77.0458 19.5687 2 6 -3 21 62.8573 20.2346 4 6 3 -21 62.9831 17.1515 3 -6 3 21 61.7297 17.7520 2 6 -3 -21 64.3228 17.5188 3 -6 -3 21 72.7922 16.5226 2 6 3 21 49.1564 15.5294 2 6 3 21 58.7158 21.0369 4 6 3 21 72.2482 14.7656 3 6 -3 -21 64.9811 17.6753 4 0 4 21 1317.40 109.133 2 0 -4 21 1135.35 108.063 2 0 -4 21 1255.79 101.022 4 0 -4 -21 1339.65 105.992 3 0 4 21 1217.54 106.856 4 0 4 21 1310.06 107.414 4 1 -4 21 144.430 17.9864 4 1 -4 21 130.571 16.7427 3 -1 -4 -21 179.187 21.1760 3 -1 4 21 146.878 20.8869 4 1 -4 21 204.297 25.4143 2 -1 4 21 131.130 21.5706 4 -1 -4 21 184.773 19.0552 3 -1 4 -21 177.523 17.4302 3 -1 4 -21 183.215 17.8793 4 1 -4 -21 208.801 22.4034 3 1 4 21 129.454 21.4116 4 2 4 -21 407.716 36.1705 3 -2 4 21 379.121 38.3975 4 2 -4 21 367.302 36.8531 4 -2 4 21 350.051 40.5892 2 -2 4 21 375.360 37.9665 4 -2 -4 -21 351.228 36.9225 3 2 -4 21 409.133 41.6082 2 -2 -4 21 377.747 39.6534 2 -2 4 -21 346.879 32.6501 3 2 4 21 425.695 40.5235 2 2 -4 -21 419.830 38.5232 3 2 4 21 396.554 40.0111 4 -3 4 21 66.1181 14.9708 4 3 -4 21 50.6084 16.1460 2 -3 4 21 43.9861 15.4639 2 -3 -4 -21 47.7358 12.8599 3 3 -4 21 56.0220 15.1187 4 3 -4 21 51.4765 6.53707 3 -3 4 21 58.0859 14.5994 4 3 4 -21 47.5471 12.7740 3 3 4 21 38.7595 13.7350 2 3 4 21 42.6190 15.4655 4 -3 -4 21 46.1706 13.9035 2 3 -4 -21 37.7529 13.3437 3 -3 4 -21 35.6621 5.94019 3 -3 4 -21 33.4301 12.5705 4 4 -4 21 117.810 21.5906 4 -4 -4 -21 104.206 18.0949 3 4 4 -21 76.0125 15.7300 3 -4 4 21 72.3243 18.6513 2 4 -4 21 89.0464 20.3901 2 -4 4 21 104.978 18.0105 4 -4 -4 21 60.8552 16.5506 2 4 -4 -21 65.3505 16.3903 3 4 4 21 102.526 22.0298 4 4 4 21 64.7975 16.9199 2 5 -4 21 104.545 23.3597 2 5 -4 21 101.711 21.8109 4 -5 -4 -21 82.0546 16.8787 3 -5 4 21 102.816 21.1470 2 5 4 -21 101.069 18.7715 3 -5 -4 21 68.9090 16.7925 2 5 4 21 80.7902 17.5912 2 5 4 21 73.5249 21.1424 4 5 -4 -21 63.7059 16.6929 3 5 -4 -21 61.4475 17.8734 4 6 -4 21 357.937 43.9814 2 6 4 -21 337.340 41.2905 3 -6 -4 21 426.879 41.6431 2 6 4 21 471.096 48.7010 4 6 -4 -21 426.755 43.7650 4 6 4 21 375.407 40.8931 2 6 -4 -21 420.579 42.6722 3 0 5 21 3.54831 11.5379 2 0 -5 21 5.77783 11.2402 2 0 5 21 2.34412 9.96750 4 0 -5 -21 3.35358 9.65674 3 0 -5 21 2.67754 2.20775 4 0 5 -21 3.74937 6.73600 3 0 -5 21 -1.3634 5.67406 3 -1 -5 -21 76.2121 15.0547 3 1 -5 21 59.2868 9.29558 3 -1 5 21 64.3590 15.3537 4 1 5 -21 49.8014 11.2879 3 1 -5 21 64.0197 15.8220 2 -1 5 21 53.7711 16.6042 2 1 -5 21 69.3180 11.6767 4 -1 5 -21 73.3745 10.5413 3 1 5 21 70.7377 16.9609 4 1 -5 -21 74.8419 15.5427 3 -1 -5 21 43.1507 16.0936 2 -1 5 -21 57.2859 10.6286 4 -1 -5 21 62.1250 11.3645 3 1 5 21 53.7370 15.6990 2 -2 5 21 407.681 42.0379 4 2 -5 21 447.798 40.1840 4 2 5 -21 417.039 38.7633 3 -2 5 21 459.508 44.2790 2 2 -5 21 479.218 45.7984 2 2 -5 21 448.807 35.0177 3 -2 -5 -21 406.349 40.6550 3 -2 5 -21 389.485 38.6659 4 2 -5 -21 416.764 41.2682 3 2 5 21 467.928 43.9825 2 -2 -5 21 387.728 42.5220 2 -2 5 -21 388.922 34.9565 3 2 5 21 352.402 42.1994 4 3 5 -21 219.860 27.4597 3 3 -5 21 317.715 31.0249 4 3 -5 21 243.652 33.0471 2 -3 5 21 301.334 31.6941 4 -3 -5 -21 298.213 31.0853 3 -3 5 21 280.443 33.5729 2 -3 5 -21 272.364 29.3626 4 -3 -5 21 213.611 30.6944 2 3 -5 -21 264.195 30.2202 3 3 5 21 209.375 29.8441 2 3 5 21 314.723 34.6841 4 -4 5 21 354.562 38.8099 4 4 -5 21 315.128 38.9647 4 4 -5 21 382.474 42.0989 2 4 5 -21 392.051 38.4197 3 -4 5 21 409.853 42.2627 2 4 -5 -21 332.818 37.7840 3 4 5 21 382.286 39.4329 2 -4 -5 21 365.707 39.1149 2 5 -5 21 166.328 27.1256 2 -5 5 21 129.071 25.0680 2 -5 -5 -21 142.245 23.2482 3 5 5 -21 171.006 23.6622 3 5 -5 21 177.077 26.0497 4 5 5 21 118.985 22.3315 2 -5 -5 21 148.986 22.6978 2 5 5 21 136.839 27.0221 4 5 -5 -21 146.165 24.2883 4 5 -5 -21 146.332 23.3407 3 -6 5 21 65.2540 19.1180 2 6 -5 21 74.5355 22.6276 4 6 5 -21 54.9038 17.2427 3 6 -5 21 70.0278 20.6343 2 -6 -5 21 71.7696 16.0546 2 6 5 21 27.8714 19.2036 4 6 -5 -21 40.4708 18.0348 4 6 5 21 53.7106 14.9911 2 6 5 21 47.4021 14.9011 3 6 -5 -21 52.0520 16.8265 3 0 6 21 137.429 21.6553 4 0 6 -21 109.927 14.9349 3 0 -6 -21 121.966 19.8248 3 -1 6 21 678.594 57.1793 4 -1 6 21 567.334 57.1874 2 1 -6 21 621.058 58.1980 2 -1 -6 -21 698.952 55.2130 3 1 -6 21 611.421 50.6123 4 -1 6 -21 544.460 48.8148 3 1 -6 -21 558.754 54.0207 3 -1 -6 21 530.913 55.9464 2 1 6 21 541.100 56.1125 2 1 6 21 530.848 55.8757 4 -2 6 21 16.1894 13.5464 2 2 6 -21 28.3677 10.4733 3 -2 6 21 27.7282 14.0169 4 -2 -6 -21 20.0224 11.8895 3 2 -6 21 40.8069 11.8975 4 2 -6 21 18.8836 14.2790 2 2 6 21 43.4024 16.2400 4 -2 6 -21 56.2136 12.4034 4 2 6 21 26.6582 13.5557 2 -2 6 -21 36.0733 4.84021 3 -2 -6 21 23.5501 12.9919 2 2 -6 -21 43.8481 13.5690 3 -3 6 21 36.2638 16.4912 2 3 6 -21 44.8781 13.2487 3 3 -6 21 58.4010 15.1868 4 -3 6 21 58.1196 16.5822 4 -3 -6 -21 43.9309 14.3756 3 3 -6 21 32.9698 16.2131 2 3 6 21 60.3977 16.2046 2 3 -6 -21 51.1857 16.4545 3 -3 6 -21 59.0795 14.9902 4 -3 -6 21 43.7199 14.5126 2 4 6 -21 1.70917 10.4515 3 4 -6 21 10.2730 13.3149 4 -4 6 21 10.6790 15.2494 2 4 -6 21 13.0260 14.0386 2 -4 -6 -21 6.15229 11.8252 3 -4 6 21 6.27913 11.7618 4 -4 -6 21 3.39381 11.6702 2 4 -6 -21 15.8968 12.8977 3 4 6 21 0.56461 14.3155 4 4 6 21 10.4627 12.4247 2 -5 -6 -21 92.4367 19.4169 3 5 6 -21 112.113 20.3694 3 5 -6 21 110.241 23.3421 4 5 -6 21 89.5177 22.3431 2 -5 6 21 112.827 23.6614 2 5 6 21 97.1504 25.5322 4 5 -6 -21 100.946 23.9973 4 5 -6 -21 121.213 22.0615 3 5 6 21 91.0491 18.8873 2 -5 -6 21 106.122 19.9019 2 6 6 -21 2.75116 13.3413 3 6 -6 21 5.40344 14.6830 4 6 -6 21 6.94153 14.3422 2 -6 6 21 8.26925 16.0892 2 -6 -6 21 12.1617 10.7800 2 6 -6 -21 20.2352 14.9181 3 6 -6 -21 14.3710 15.1566 4 6 6 21 -5.5279 10.5370 3 6 6 21 3.52389 10.3209 2 0 7 21 64.2919 17.8765 2 0 -7 21 50.8495 9.37093 3 0 7 21 47.0200 16.1027 4 0 -7 21 72.9883 18.8741 2 0 -7 -21 49.6296 14.7280 3 0 7 -21 50.2932 9.84338 3 -1 -7 -21 18.7120 12.6900 3 1 7 -21 17.3176 8.84193 3 1 -7 21 14.4273 13.6749 2 -1 7 21 17.5991 14.6849 4 -1 7 21 22.9046 14.1488 2 1 -7 21 13.3002 5.07542 3 1 -7 21 18.9951 8.21247 4 1 -7 -21 12.8863 11.7951 3 1 7 21 4.81979 13.2317 4 -1 -7 21 16.4553 8.02834 3 -1 7 -21 9.05291 6.64422 4 -1 -7 21 9.13463 12.5852 2 -1 7 -21 12.2603 5.74369 3 1 7 21 12.2898 12.7880 2 2 7 -21 472.596 41.5822 3 2 -7 21 510.014 49.2080 2 -2 7 21 451.314 47.5773 2 2 -7 21 474.989 42.3429 4 -2 -7 -21 458.930 44.2233 3 2 7 21 436.480 45.8604 2 -2 -7 21 409.448 45.3677 2 2 -7 -21 364.000 43.1952 3 -2 7 -21 388.832 40.9177 4 2 7 21 472.664 47.9151 4 -3 -7 -21 50.2870 15.4697 3 3 -7 21 62.0114 19.1328 2 3 -7 21 26.6416 13.3489 4 -3 7 21 60.6334 18.1017 4 -3 7 21 104.724 21.9056 2 3 7 -21 55.4800 13.9110 3 -3 -7 21 77.1552 18.1903 2 3 7 21 84.0955 17.6741 2 3 -7 -21 48.8890 15.5678 3 -3 7 -21 37.7275 13.8103 4 3 7 21 21.1326 15.8864 4 -4 7 21 372.927 40.5921 4 4 -7 21 380.101 39.4836 4 -4 7 21 301.452 39.8246 2 4 7 -21 345.975 35.5887 3 4 -7 21 362.685 42.0344 2 4 7 21 288.002 37.0433 2 4 -7 -21 328.884 37.3025 3 -4 -7 21 312.388 37.3443 2 4 7 21 376.308 43.0110 4 -5 7 21 19.5339 15.2006 2 5 -7 21 15.8614 15.3462 2 5 -7 21 6.89490 15.5188 4 -5 -7 -21 23.7681 15.4690 3 5 7 -21 10.5904 13.5532 3 5 -7 -21 -2.4563 16.5192 4 -5 -7 21 17.3135 12.8646 2 5 7 21 21.1786 12.9633 3 5 7 21 -1.8314 16.4710 4 5 -7 -21 6.74465 13.2856 3 5 7 21 23.4780 13.1116 2 0 8 -21 94.4408 14.2180 3 0 -8 21 129.341 24.6120 2 0 8 21 129.525 23.5984 2 0 -8 -21 93.0988 19.4081 3 0 -8 21 129.531 14.0154 3 0 8 21 84.0905 21.4751 4 -1 8 21 208.683 28.0759 4 -1 8 21 179.694 28.1785 2 1 -8 21 165.986 28.0751 2 1 8 -21 201.206 20.8173 3 -1 -8 -21 206.329 27.6436 3 1 8 21 179.062 28.3010 4 -1 8 -21 167.857 16.5926 3 -1 8 -21 170.966 16.4155 3 -1 -8 21 141.984 27.7196 2 1 8 21 156.586 28.2177 2 -1 -8 21 145.063 19.0589 3 1 -8 -21 201.900 25.6509 3 2 8 -21 203.899 22.0520 3 -2 -8 -21 198.229 26.2596 3 -2 8 21 181.000 27.0109 4 2 -8 21 165.338 22.7419 4 2 -8 21 172.450 28.8450 2 -2 8 21 197.761 28.8459 2 2 8 21 172.706 28.2441 2 2 8 21 134.070 27.5342 4 2 -8 -21 171.463 25.6110 3 -2 8 -21 148.924 21.4341 4 -2 -8 21 195.833 27.0696 2 -3 8 21 35.7622 16.9182 4 3 -8 21 32.2853 16.3231 2 -3 -8 -21 41.2734 15.4101 3 3 -8 21 41.9017 14.6173 4 -3 8 21 36.2052 17.2803 2 3 8 -21 33.1854 13.2455 3 3 8 21 45.7020 18.7039 4 3 -8 -21 39.1803 15.4472 3 3 8 21 44.7608 16.8602 2 -3 -8 21 56.4089 17.5373 2 4 -8 21 53.4727 20.3819 2 -4 8 21 56.7895 18.8411 4 -4 -8 -21 62.5277 19.0329 3 4 -8 21 72.9698 19.2779 4 4 8 -21 73.3104 17.1249 3 -4 8 21 64.8337 20.4086 2 4 -8 -21 56.0362 17.2407 3 4 8 21 59.1875 22.6869 4 4 8 21 71.9241 17.3909 2 -4 -8 21 57.6529 16.6413 2 0 -9 21 13.5482 14.3347 2 0 -9 -21 1.15624 12.3044 3 0 9 -21 5.33723 6.67787 3 0 9 21 22.7638 16.3987 4 0 9 21 12.9186 14.4746 2 0 9 -21 5.02587 6.91969 3 1 9 -21 74.8453 13.0691 3 1 -9 21 88.2096 14.4125 4 1 9 -21 89.6633 13.8715 3 -1 -9 -21 90.5645 18.6513 3 -1 9 21 79.9108 21.0534 2 -1 9 21 84.2992 21.2085 4 1 -9 21 65.7594 20.5318 2 1 9 21 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130.803 22.7154 3 4 1 23 162.974 25.4238 4 -4 1 -23 144.381 18.5270 3 4 1 23 163.335 19.8161 3 4 1 23 135.864 24.0569 2 5 -1 23 241.864 25.2522 3 -5 1 23 219.681 33.2755 2 -5 1 23 286.139 28.2135 4 5 1 -23 235.704 30.9477 3 5 -1 23 298.100 25.7366 3 -5 1 23 257.606 26.9825 4 5 -1 23 295.391 34.5500 4 5 -1 23 227.240 33.5263 2 5 -1 -23 334.829 32.6485 3 -5 -1 23 246.818 31.7145 2 5 1 23 266.440 27.5094 3 5 1 23 256.742 32.0475 2 5 1 23 296.381 35.4012 4 -6 1 23 169.431 26.3477 2 6 -1 23 161.371 29.9035 4 -6 1 23 158.301 19.3868 4 6 -1 23 180.217 25.8427 2 6 1 -23 172.439 24.6097 3 6 1 23 114.398 23.4977 2 -6 -1 23 124.259 23.8201 2 6 1 23 118.376 18.2289 3 6 1 23 81.8516 24.7245 4 6 -1 -23 107.062 22.1339 3 0 -2 -23 94.0967 16.2525 3 0 -2 23 101.940 13.0450 4 0 2 -23 112.602 15.6537 3 0 -2 23 106.102 14.4727 3 0 2 23 80.2741 15.9965 4 0 -2 23 108.104 18.3725 2 0 2 23 114.427 20.7385 2 0 -2 23 87.5977 12.3055 4 0 2 23 100.640 16.6480 4 -1 2 23 63.9440 13.7711 4 1 -2 23 93.6302 13.9257 4 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159.680 25.8506 2 -6 -2 23 167.338 25.6628 2 6 -2 -23 133.725 25.4696 3 6 2 23 154.426 29.5331 4 0 -3 23 303.241 27.0571 4 0 3 23 336.283 35.9814 2 0 -3 23 286.106 28.8649 3 0 3 23 269.997 31.8908 4 0 -3 23 308.144 26.9405 4 0 -3 23 341.098 35.8745 2 0 3 23 278.216 32.0732 4 0 3 -23 332.391 29.8345 3 0 -3 -23 306.946 31.7106 3 -1 3 23 13.0616 10.1473 4 1 -3 23 15.6266 7.89400 4 1 3 -23 7.47430 8.72542 3 1 -3 23 19.3738 13.0112 2 1 -3 23 12.0577 7.04010 3 -1 -3 -23 16.2565 10.3046 3 -1 3 23 26.5675 13.3890 2 -1 3 23 7.69794 9.72617 4 1 3 23 12.4642 11.7122 4 1 3 23 13.0525 10.4402 4 1 3 23 15.8262 12.6276 2 -1 3 -23 15.8221 7.67948 3 -1 -3 23 13.6158 8.72424 3 -1 3 -23 7.88032 6.93105 4 -1 -3 23 4.78754 11.1697 2 1 -3 -23 15.9539 10.7083 3 2 3 -23 208.761 23.9734 3 2 -3 23 204.537 24.4905 4 -2 -3 -23 227.733 24.9409 3 -2 3 23 237.485 25.3789 4 -2 3 23 209.896 25.1668 4 2 -3 23 186.805 20.6123 3 2 -3 23 233.760 29.7527 2 -2 3 23 237.085 29.8163 2 -2 -3 23 272.020 29.8238 2 -2 3 -23 231.408 21.4450 3 2 3 23 167.852 26.1470 4 2 -3 -23 204.363 25.8496 3 -2 3 -23 188.402 23.2874 4 2 3 23 228.603 28.6811 2 3 -3 23 223.595 26.6835 4 -3 3 23 234.704 25.2949 4 3 -3 23 179.921 28.0598 2 -3 3 23 177.411 27.6617 2 3 3 -23 159.535 23.6611 3 3 -3 23 160.011 19.0998 3 -3 -3 -23 164.928 24.3105 3 -3 3 23 180.938 23.5675 4 -3 3 -23 231.926 26.0679 4 -3 3 -23 222.308 20.1923 3 3 -3 -23 243.577 26.6769 3 -3 -3 23 229.571 28.4452 2 3 3 23 264.859 29.6470 4 3 3 23 250.145 28.7084 2 4 -3 23 62.8272 17.1596 4 -4 -3 -23 69.6208 15.3810 3 -4 3 23 77.9511 15.3769 4 4 -3 23 64.0544 18.5861 2 -4 3 23 56.4797 17.7795 2 4 -3 23 70.0496 9.10235 3 -4 3 23 75.5682 16.2042 4 4 3 -23 74.0766 16.2310 3 4 -3 23 66.6676 8.75875 3 -4 -3 23 59.0549 16.7072 2 4 -3 -23 70.2477 16.4444 3 4 3 23 62.4496 18.4598 4 4 3 23 85.7449 19.5440 2 5 -3 23 18.4966 3.89796 3 -5 3 23 23.2247 11.5658 4 5 -3 23 9.01523 14.3844 2 -5 -3 -23 7.91190 10.8129 3 -5 3 23 22.9342 13.8473 4 -5 3 23 11.5381 13.6346 2 5 3 -23 19.5246 13.0789 3 5 -3 23 24.1436 16.3811 4 5 -3 -23 27.3504 14.0344 3 5 3 23 17.9163 12.4714 2 -5 -3 23 33.6606 15.0708 2 5 3 23 7.69157 15.5287 4 -6 3 23 250.635 33.0098 2 6 -3 23 224.571 31.6666 2 6 -3 23 290.994 36.3502 4 6 3 23 203.908 29.0050 2 6 3 23 186.950 33.1627 4 6 3 23 216.358 26.0940 3 6 -3 -23 215.397 29.8670 3 -6 -3 23 200.546 28.8079 2 0 -4 23 126.032 11.5613 4 0 -4 -23 146.784 20.0860 3 0 4 23 106.719 19.0167 4 0 -4 23 126.290 11.5315 4 0 4 -23 124.789 16.0193 3 0 -4 23 107.672 15.9537 3 0 -4 23 125.375 22.4625 2 0 4 23 113.577 22.4151 2 1 4 -23 12.9094 8.87278 3 -1 4 23 19.4660 10.9979 4 -1 -4 -23 11.1215 10.5282 3 1 -4 23 15.5954 7.92279 4 1 -4 23 4.85564 11.7176 2 -1 4 23 -1.2775 11.5043 2 -1 4 23 12.9714 9.89484 4 1 -4 23 4.12093 6.21241 3 1 4 23 -3.9054 11.1181 4 1 -4 -23 -3.6827 11.1026 3 -1 -4 23 5.42121 7.98331 3 1 4 23 2.96712 11.2244 2 -1 -4 23 2.82399 11.3356 2 -1 4 -23 1.51627 6.58953 3 -1 4 -23 7.22073 6.65767 4 2 -4 23 142.800 22.1245 4 -2 4 23 177.939 24.2140 4 2 -4 23 161.238 18.1165 3 -2 -4 -23 170.889 23.3955 3 -2 4 23 224.308 27.3622 2 -2 4 23 216.977 25.1196 4 2 -4 23 218.271 28.4083 2 2 4 23 167.908 25.7748 4 -2 4 -23 200.820 18.9849 3 2 4 23 208.956 27.4048 2 2 -4 -23 187.272 24.4503 3 -2 -4 23 226.880 27.5895 2 -2 4 -23 175.552 21.7258 4 -3 4 23 239.325 32.9778 2 -3 4 23 244.708 32.4871 4 3 -4 23 272.492 22.8713 3 3 4 -23 325.970 30.4557 3 3 -4 23 265.490 33.8183 2 -3 -4 -23 264.010 29.1823 3 -3 4 23 297.399 30.5406 4 -3 -4 23 219.783 30.6930 2 -3 4 -23 246.499 22.7962 3 3 4 23 232.123 31.2248 2 3 -4 -23 283.548 30.8852 3 -3 4 -23 285.262 29.8382 4 3 4 23 230.049 32.1366 4 4 -4 23 69.7770 19.9996 2 4 4 -23 68.6802 17.0521 3 -4 4 23 64.6082 19.2442 2 -4 -4 -23 69.7373 15.8024 3 4 -4 23 76.6921 18.4832 4 -4 4 23 70.6516 16.5390 4 4 -4 -23 76.1408 17.4690 3 -4 -4 23 76.6225 17.7153 2 4 4 23 85.6711 21.4662 4 4 4 23 88.3310 18.4713 2 -5 4 23 93.7616 19.3132 4 5 -4 23 109.767 24.1290 4 -5 -4 -23 91.8407 17.5917 3 5 4 -23 113.303 20.4834 3 5 -4 23 79.3753 21.3344 2 -5 4 23 62.1930 20.1997 2 -5 -4 23 109.460 21.1259 2 5 4 23 99.8113 20.9887 2 5 -4 -23 137.881 22.1939 3 5 4 23 92.8148 23.5622 4 -6 4 23 30.2693 16.3810 2 6 4 -23 30.2944 15.3564 3 6 -4 23 22.6975 16.3686 2 6 -4 23 5.67120 17.0366 4 6 -4 -23 25.9440 17.1520 3 -6 -4 23 34.1257 13.7719 2 6 4 23 26.3264 12.6743 3 6 -4 -23 39.2859 16.7351 4 6 4 23 14.9813 18.6666 4 6 4 23 41.3867 15.0445 2 0 5 -23 184.531 20.2731 3 0 5 23 164.143 26.6123 2 0 -5 -23 166.113 23.7151 3 0 5 23 217.260 26.0254 4 0 -5 23 208.014 20.3297 3 0 -5 23 137.584 25.5354 2 1 -5 23 348.831 31.2817 3 -1 5 23 369.235 40.3013 2 1 5 -23 380.399 33.8324 3 1 -5 23 379.133 40.4852 2 -1 -5 -23 365.246 36.2464 3 -1 5 23 359.161 37.2486 4 1 -5 23 314.056 31.8678 4 -1 5 -23 327.928 31.4459 4 -1 -5 23 318.072 32.9110 3 1 -5 -23 338.952 36.4054 3 -1 5 -23 350.804 31.6196 3 1 5 23 380.027 39.9683 2 -1 -5 23 370.833 39.6967 2 2 -5 23 60.9811 8.47909 3 -2 -5 -23 47.5848 14.4761 3 2 -5 23 52.5516 12.9649 4 2 -5 23 41.6696 16.5665 2 -2 5 23 56.8387 17.9293 2 2 5 -23 54.3064 12.4576 3 -2 5 23 62.2013 16.3492 4 2 5 23 46.3071 16.6881 4 -2 5 -23 55.0067 8.38071 3 2 5 23 52.7067 16.9050 2 -2 -5 23 53.3937 16.5660 2 2 -5 -23 54.1924 16.5768 3 -2 5 -23 70.3305 13.3296 4 3 5 -23 43.5288 14.2942 3 -3 -5 -23 22.1095 12.8998 3 3 -5 23 38.5839 14.1836 4 -3 5 23 48.4698 14.6546 4 3 -5 23 40.3258 17.4634 2 -3 5 23 45.0079 17.2163 2 3 5 23 53.1238 16.0342 2 3 -5 -23 66.8636 16.4958 3 -3 -5 23 56.7009 15.9892 2 3 5 23 65.2701 19.1874 4 -3 5 -23 78.5277 15.8879 4 4 5 -23 27.9993 13.0727 3 -4 5 23 12.8030 14.1646 2 -4 -5 -23 23.4112 13.8047 3 4 -5 23 23.7062 15.5734 2 4 -5 23 34.3640 14.0591 4 -4 5 23 32.8252 14.1712 4 4 -5 -23 35.2212 14.3183 3 4 5 23 6.60512 12.8575 2 -4 -5 23 14.4832 13.5644 2 4 5 23 29.2518 16.9220 4 -5 -5 -23 98.8098 19.8609 3 5 5 -23 121.185 22.4942 3 5 -5 23 116.312 25.0517 4 -5 5 23 107.671 24.3122 2 -5 5 23 117.062 22.3207 4 5 -5 23 104.820 25.3083 2 5 -5 -23 137.046 24.4534 3 5 5 23 136.240 28.1654 4 -5 -5 23 145.561 22.8869 2 5 5 23 137.102 23.4575 2 0 -6 23 76.0584 12.4969 3 0 -6 -23 58.3201 16.1013 3 0 6 23 73.1570 19.5785 2 0 6 23 87.7900 19.2438 4 0 -6 23 78.2330 19.8004 2 0 6 -23 89.2802 13.6901 3 -1 6 23 18.2813 14.5129 2 -1 6 23 1.47901 12.9694 4 1 6 -23 11.7276 9.26072 3 1 -6 23 21.7588 14.7882 2 1 -6 23 16.1770 6.34448 3 -1 -6 -23 24.8060 12.9589 3 1 -6 -23 29.9706 13.3094 3 1 6 23 33.1160 15.6293 2 -1 6 -23 26.7077 7.45370 4 -1 -6 23 31.1848 14.8100 2 1 6 23 15.9058 13.7349 4 -1 -6 23 20.9838 9.39148 3 -1 6 -23 29.5953 7.33889 3 2 -6 23 250.145 32.8975 2 -2 6 23 265.173 32.9766 2 2 -6 23 258.719 26.3870 4 2 6 -23 280.632 26.6960 3 -2 6 23 251.845 29.6086 4 -2 6 -23 183.370 24.3883 4 -2 -6 23 225.513 30.1463 2 2 -6 -23 240.090 28.9235 3 -2 6 -23 210.271 19.5813 3 2 6 23 190.897 29.8722 4 2 6 23 233.578 30.6329 2 3 -6 23 10.5762 12.0316 4 -3 6 23 9.01207 11.7171 4 -3 -6 -23 5.10741 12.0492 3 3 6 -23 8.78089 11.3443 3 -3 6 23 24.9168 15.3539 2 3 -6 23 34.6909 17.1024 2 3 -6 -23 14.9975 12.7808 3 -3 -6 23 16.6173 14.4182 2 3 6 23 24.1097 16.1930 4 3 6 23 31.5692 15.8644 2 -3 6 -23 6.96550 10.6415 4 -4 6 23 273.420 34.3543 4 4 -6 23 281.158 34.3026 4 4 -6 23 303.564 39.0932 2 -4 -6 -23 252.616 34.4037 3 -4 6 23 348.333 40.9325 2 4 6 -23 262.446 32.3800 3 -4 -6 23 344.771 35.5917 2 4 6 23 332.889 36.8685 2 4 6 23 315.046 39.4345 4 4 -6 -23 315.737 35.2706 3 -5 6 23 27.9125 18.5677 2 -5 -6 -23 26.2811 13.9899 3 5 -6 23 47.7658 18.7592 4 5 6 -23 22.1910 15.3483 3 -5 6 23 41.3602 16.9182 4 5 -6 23 33.9495 19.5576 2 5 -6 -23 65.9469 19.0402 3 -5 -6 23 49.9386 15.9967 2 5 6 23 64.8312 22.2474 4 5 6 23 45.7277 16.4477 2 0 -7 -23 49.1413 16.3522 3 0 7 -23 56.8275 10.8616 3 0 7 23 75.8208 19.4781 2 0 7 23 40.8529 18.0211 4 0 -7 23 66.7730 19.3156 2 0 -7 23 55.2773 9.84034 3 -1 -7 -23 265.371 31.9385 3 1 7 -23 255.627 27.5490 3 1 -7 23 266.035 35.3701 2 -1 7 23 322.054 35.5501 2 1 -7 23 289.211 24.3555 3 1 -7 23 252.718 25.7993 4 -1 7 23 269.438 33.6744 4 -1 7 -23 266.838 24.7447 3 -1 -7 23 278.861 34.7985 2 1 7 23 322.812 35.8174 2 -1 7 -23 249.967 25.0547 4 -1 -7 23 251.357 27.0826 3 1 -7 -23 274.686 32.2463 3 1 7 23 286.864 35.1262 4 2 -7 23 33.8636 17.4290 2 2 7 -23 38.1378 11.7955 3 2 -7 23 36.7731 12.2123 4 -2 7 23 34.2329 15.1695 4 -2 -7 -23 37.3330 14.8287 3 -2 7 23 43.8574 17.1450 2 -2 7 -23 13.4771 9.72233 4 2 7 23 18.0157 15.4589 4 2 7 23 41.3428 16.2125 2 2 -7 -23 31.8411 14.2439 3 -2 -7 23 25.5083 15.5567 2 -3 7 23 17.0609 13.8794 4 -3 -7 -23 5.62427 12.3947 3 -3 7 23 13.7618 15.3304 2 3 -7 23 9.91403 14.4136 2 3 7 -23 8.23883 11.2938 3 3 -7 23 25.7437 13.5411 4 3 7 23 13.8050 15.7975 4 3 7 23 8.71870 13.0285 2 -3 -7 23 15.8503 14.5732 2 3 -7 -23 32.8503 14.5660 3 -4 7 23 20.6603 16.0599 2 -4 -7 -23 17.5555 15.2058 3 4 -7 23 33.8552 18.1140 2 4 -7 23 18.0159 15.4456 4 -4 7 23 22.3925 15.0432 4 4 7 -23 16.5794 12.2483 3 4 7 23 12.2330 17.4107 4 4 7 23 17.8313 13.3549 2 -4 -7 23 31.6619 15.4528 2 4 -7 -23 13.2474 13.7776 3 0 8 -23 34.5854 9.22049 3 0 -8 -23 31.4430 14.5574 3 0 -8 23 29.0591 18.0248 2 0 8 23 30.4404 16.1848 2 0 -8 23 35.8220 8.66645 3 0 8 23 13.8755 16.6175 4 1 -8 23 127.677 16.7116 4 1 -8 23 157.418 27.9243 2 -1 -8 -23 134.979 23.6948 3 -1 8 23 192.891 28.7700 2 1 8 -23 166.789 19.6218 3 -1 8 23 156.865 26.7738 4 -1 -8 23 161.438 19.0747 3 1 8 23 181.531 27.9125 2 1 8 23 140.898 26.9869 4 -1 8 -23 155.339 16.5875 4 -1 8 -23 150.268 15.2996 3 -1 -8 23 152.298 26.7080 2 1 -8 -23 162.999 24.4833 3 -1 8 -23 147.150 15.0763 3 2 8 -23 83.0236 15.8070 3 -2 8 23 81.2640 21.9275 2 2 -8 23 118.155 18.0535 4 -2 -8 -23 82.1559 18.9312 3 2 -8 23 57.2298 20.5045 2 -2 8 23 95.7786 21.5098 4 2 8 23 38.1594 17.6502 2 2 8 23 94.4243 23.2097 4 2 -8 -23 64.9653 19.0789 3 3 8 -23 143.965 24.0227 3 -3 8 23 182.900 28.9238 4 3 -8 23 197.077 32.1206 2 -3 8 23 226.332 32.7425 2 -3 -8 -23 176.899 27.5925 3 3 -8 -23 226.803 30.7804 3 3 8 23 242.900 31.4395 2 3 8 23 141.161 30.7829 4 -3 -8 23 249.341 31.1718 2 4 8 -23 44.9666 15.3634 3 4 -8 23 47.2635 17.4536 4 -4 -8 -23 45.2438 17.3399 3 -4 8 23 39.0273 18.7178 4 4 8 23 14.7503 14.7969 2 4 8 23 9.15113 20.1267 4 0 -9 23 318.585 37.9862 2 0 -9 -23 250.578 33.2049 3 0 9 -23 260.953 25.7362 3 0 9 23 253.544 36.1922 4 -1 9 23 24.8670 17.6142 2 -1 -9 -23 41.5897 16.4395 3 1 9 -23 50.1290 11.5950 3 1 -9 23 34.6534 18.5204 2 -1 9 23 36.9042 17.8304 4 1 -9 -23 28.2166 15.5301 3 1 9 23 41.4891 19.2626 2 -1 -9 23 22.7887 17.8856 2 1 9 23 66.4169 21.0131 4 2 -9 23 180.283 31.6071 2 2 -9 23 154.636 22.9954 4 -2 -9 -23 177.991 27.8798 3 -2 9 23 169.655 30.9296 2 2 9 23 193.475 31.9863 4 2 -9 -23 200.829 28.2776 3 2 9 23 239.708 30.7908 2 0 10 -23 11.7712 8.68278 3 0 10 23 20.5785 17.3398 4 0 -10 23 18.3901 16.6453 2 0 10 23 30.7096 19.8760 2 0 0 -24 1166.12 100.159 3 0 0 24 1162.02 104.591 2 0 0 24 1267.44 100.189 4 -1 0 24 169.821 18.3677 4 1 0 -24 175.569 21.2021 3 1 0 24 150.688 20.4097 4 1 0 24 143.656 24.4812 2 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30.1710 2 6 0 24 203.445 32.0956 4 6 0 24 210.080 22.1148 3 0 -1 24 50.9429 11.1870 4 0 1 24 77.6939 18.1435 2 0 1 24 60.5164 12.9281 4 0 -1 24 58.2679 11.4768 4 0 -1 24 61.2716 12.4229 3 0 -1 -24 62.7642 13.3635 3 0 1 -24 57.4192 12.4721 3 0 -1 24 75.9646 18.6168 2 0 1 24 78.4459 14.1903 4 1 -1 24 116.980 21.6955 2 1 -1 24 83.3053 15.1360 3 1 -1 24 131.361 17.9746 4 -1 1 24 95.7875 18.9867 2 1 1 -24 130.960 18.6946 3 -1 -1 -24 101.240 17.5915 3 -1 1 24 124.967 16.7937 4 1 1 24 119.293 18.6447 4 -1 -1 24 127.139 13.8203 4 -1 -1 24 99.2892 21.1026 2 1 1 24 111.440 21.4237 2 -1 1 -24 124.621 16.7519 3 -1 1 -24 110.663 16.3167 4 1 1 24 117.907 18.1264 4 1 -1 -24 149.133 19.0848 3 2 -1 24 126.807 19.5992 4 -2 1 24 137.219 23.4657 2 2 -1 24 127.218 22.7904 2 2 1 -24 130.460 19.0279 3 -2 -1 -24 132.100 17.5104 3 -2 1 24 120.083 17.0155 4 -2 -1 -24 110.442 18.4881 4 2 -1 24 110.007 15.8334 3 -2 1 24 127.744 16.2972 4 -2 -1 24 138.019 12.3077 4 -2 1 -24 141.506 17.1791 3 -2 1 -24 127.056 18.5730 4 2 -1 -24 100.377 18.8727 3 -2 -1 24 134.177 23.0541 2 2 1 24 139.342 22.9450 2 2 1 24 141.539 20.0261 4 -3 -1 -24 624.943 52.8357 3 3 -1 24 547.459 57.2478 2 -3 1 24 608.216 58.0794 2 3 -1 24 567.603 50.6777 3 3 1 -24 600.982 54.1283 3 -3 1 24 664.316 51.5843 4 -3 1 24 643.324 51.8586 4 3 -1 24 507.601 55.0122 4 3 -1 -24 572.058 54.4126 3 -3 1 -24 555.961 51.0826 3 3 1 24 587.644 56.0012 4 -3 -1 24 534.994 57.4174 2 3 1 24 629.278 58.0181 2 4 -1 24 46.8131 16.1921 2 4 -1 24 47.7539 9.78637 3 -4 1 24 53.9305 16.9146 2 4 1 -24 32.4316 13.7155 3 -4 1 24 57.1913 10.8733 4 4 -1 24 41.2445 17.2294 4 -4 1 24 36.7610 10.8048 4 -4 -1 -24 47.4690 12.5961 3 4 -1 -24 34.6417 13.7961 3 4 1 24 26.1518 17.1946 4 4 1 24 45.7858 16.5652 2 -4 1 -24 32.0351 9.69857 3 -4 -1 24 38.6613 15.1317 2 -5 1 24 127.410 24.3851 2 5 -1 24 136.143 24.6618 2 5 -1 24 134.510 25.2670 4 -5 1 24 166.714 20.4177 4 5 -1 24 148.200 17.4251 3 5 -1 24 149.558 17.6471 3 5 1 -24 164.942 24.0957 3 -5 1 24 149.635 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2 -24 436.348 37.8890 3 1 2 24 394.788 40.3215 4 -1 -2 24 408.057 33.5725 4 -1 -2 24 428.039 44.1196 2 -2 2 24 108.908 16.4198 4 2 -2 24 102.652 21.1073 2 2 2 -24 70.2504 15.2273 3 -2 2 24 99.6733 20.9319 2 -2 -2 -24 106.208 17.1655 3 2 -2 24 96.2858 16.7203 4 -2 2 24 91.7932 15.1949 4 2 -2 24 87.0854 13.1993 3 -2 -2 24 92.5327 20.0423 2 2 2 24 100.049 18.4171 4 -2 2 -24 81.3152 14.0281 3 2 2 24 95.2547 20.1809 2 -2 2 -24 77.5909 15.3964 4 2 -2 -24 80.0952 17.8736 3 3 -2 24 119.310 22.5278 2 -3 2 24 114.286 16.8799 4 3 -2 24 90.1819 13.7813 3 -3 2 24 105.726 16.8573 4 3 2 -24 116.458 18.6417 3 3 -2 24 106.658 18.5495 4 -3 2 24 103.554 21.8045 2 -3 -2 -24 122.689 18.4649 3 3 -2 -24 131.984 19.8978 3 3 2 24 104.828 21.0727 2 -3 -2 24 110.205 21.4324 2 -3 2 -24 98.5609 14.3373 3 3 2 24 96.8022 20.0621 4 4 -2 24 187.617 27.4862 2 -4 2 24 186.046 29.0704 2 -4 2 24 175.762 21.5665 4 4 -2 24 167.480 24.9827 4 -4 -2 -24 152.634 21.9059 3 4 2 -24 189.413 24.3462 3 4 -2 24 138.759 17.3879 3 -4 2 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47.5586 2 2 1 25 512.073 46.0129 4 -2 1 -25 415.444 43.0310 4 2 -1 -25 470.413 44.2941 3 -2 -1 25 415.781 37.0938 4 -2 -1 25 435.868 37.2116 4 2 1 25 439.065 47.4909 2 -2 -1 25 486.305 48.2983 2 -2 1 -25 417.193 41.4624 3 -3 1 25 113.698 23.1794 2 3 -1 25 118.745 21.8367 4 -3 -1 -25 106.882 18.1186 3 3 -1 25 132.282 23.7391 2 -3 1 25 115.677 15.7762 4 -3 1 25 112.599 15.6446 4 3 1 -25 98.8479 18.9718 3 3 -1 25 115.189 15.6398 3 -3 -1 25 125.518 24.1294 2 3 -1 -25 121.930 19.9814 3 3 1 25 148.547 23.9775 2 3 1 25 125.433 21.4662 4 -3 1 -25 115.823 16.6457 3 4 -1 25 230.123 25.0785 3 -4 -1 -25 270.442 27.9481 3 4 -1 25 291.083 34.4149 2 -4 1 25 284.788 26.9397 4 -4 1 25 255.169 25.7525 4 4 1 -25 253.595 30.1270 3 4 -1 25 281.697 33.9866 4 -4 1 25 252.132 33.3367 2 4 1 25 253.781 32.6694 2 4 1 25 255.495 34.4183 4 -4 -1 25 280.090 33.5024 2 4 -1 -25 235.015 30.4778 3 -4 1 -25 226.697 25.7081 3 5 -1 25 164.411 27.2619 2 -5 1 25 161.850 28.7708 2 5 -1 25 193.853 28.3388 4 -5 1 25 188.151 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17.6576 2 -3 -5 -27 39.8498 14.8148 3 -3 5 27 41.6158 16.4975 4 -3 5 27 18.0423 17.1457 2 3 -5 27 46.1210 14.2738 4 3 -5 -27 47.1158 16.2383 3 3 5 27 35.8514 16.1767 2 -3 -5 27 36.4848 17.2281 2 3 5 27 58.4318 21.2637 4 0 6 27 29.9632 17.5948 2 0 -6 27 47.9110 18.6308 2 0 6 -27 34.6474 10.7627 3 0 -6 -27 35.6448 15.6259 3 0 6 27 38.1546 16.4813 4 1 -6 27 36.6236 18.4100 2 -1 -6 -27 48.2792 16.8168 3 1 6 -27 57.9143 13.7304 3 -1 6 27 44.9968 19.7351 2 -1 6 27 50.7091 18.6784 4 1 -6 -27 72.0772 19.4301 3 -1 6 -27 66.6005 11.0482 3 1 6 27 64.7676 19.1635 4 1 6 27 54.7999 19.0473 2 -1 -6 27 70.7422 20.4934 2 2 6 -27 318.119 35.2459 3 -2 6 27 326.753 43.0099 2 -2 -6 -27 313.264 38.8707 3 2 -6 27 351.331 44.0298 2 2 -6 27 383.975 34.9476 4 -2 6 27 330.699 38.9217 4 2 6 27 362.572 44.0635 2 -2 -6 27 362.315 41.9267 2 2 -6 -27 384.031 40.0710 3 -3 6 27 58.0628 17.8893 4 -3 -6 -27 26.6655 16.5133 3 3 -6 27 64.5019 16.1720 4 3 6 -27 75.6297 16.6841 3 3 6 27 27.7206 16.7121 2 -3 -6 27 36.5681 17.8765 2 3 6 27 101.153 24.4447 4 0 7 27 8.67406 16.2400 4 0 -7 -27 30.8683 15.7402 3 0 -7 27 42.0176 19.6423 2 0 7 -27 38.1411 10.3138 3 0 7 27 51.6924 21.6312 2 -1 -7 -27 235.498 32.1798 3 -1 7 27 241.809 31.7974 4 1 -7 27 221.648 34.4399 2 -1 7 27 240.343 34.6863 2 1 7 27 203.544 33.0532 2 -1 7 -27 235.049 21.8907 3 1 7 27 149.667 30.3533 4 -1 -7 27 217.694 35.3535 2 1 -7 -27 211.216 31.6028 3 -2 -7 -27 7.93569 14.2342 3 2 7 -27 16.9229 12.0557 3 -2 7 27 1.40534 15.2454 4 2 7 27 12.4364 15.1457 2 2 7 27 17.7275 16.3556 4 -2 -7 27 18.3039 15.8419 2 0 0 -28 232.728 27.8098 3 0 0 28 234.607 32.9711 2 -1 0 28 17.8539 14.8423 2 -1 0 28 21.1977 8.81382 4 1 0 28 20.3066 11.0281 4 1 0 28 29.7394 16.4348 2 -1 0 28 14.1950 8.39647 4 1 0 -28 15.1980 11.2772 3 -1 0 -28 25.0626 11.4858 3 1 0 28 10.7516 11.5983 4 -2 0 -28 7.14109 9.83648 3 2 0 28 8.03741 11.9699 4 2 0 -28 0.89425 12.1035 3 -2 0 28 17.3392 14.7155 2 2 0 28 2.52236 14.2709 2 -2 0 28 5.81470 6.42507 4 -2 0 28 7.02458 6.27909 4 3 0 28 14.4544 13.0292 4 3 0 28 8.12296 13.8395 2 -3 0 28 1.99213 13.5189 2 -3 0 28 2.99158 3.89056 4 -3 0 -28 14.3221 10.8054 3 3 0 -28 14.9525 12.9200 3 -4 0 28 269.561 36.1087 2 -4 0 -28 256.935 28.9558 3 4 0 28 299.265 35.4014 4 4 0 28 260.042 37.5632 2 4 0 -28 280.437 34.4918 3 0 -1 -28 76.3066 16.7203 3 0 1 28 67.2832 14.1625 4 0 1 28 63.4091 14.6585 4 0 -1 28 72.9888 20.6470 2 0 1 28 51.3161 18.7025 2 0 -1 28 69.2054 12.8715 4 0 1 -28 56.4935 14.3403 3 0 -1 28 55.8658 12.2843 4 1 1 -28 85.4806 18.0248 3 -1 -1 -28 85.4166 17.5075 3 -1 1 28 83.8410 16.0931 4 1 -1 28 65.6946 20.3769 2 -1 1 28 77.9037 21.4745 2 -1 1 28 106.120 17.1702 4 1 -1 28 96.7336 17.8076 4 1 -1 28 106.205 17.0991 4 -1 1 -28 117.147 18.1466 3 1 1 28 103.479 18.6546 4 -1 -1 28 104.193 12.6490 4 1 1 28 104.433 22.8192 2 -1 -1 28 106.833 23.6488 2 -1 -1 28 106.191 12.4579 4 1 -1 -28 91.0052 18.0402 3 -2 1 28 140.188 19.1901 4 -2 1 28 121.316 18.4977 4 -2 -1 -28 160.976 20.9323 3 2 -1 28 140.738 22.2354 4 -2 1 28 155.301 27.5805 2 2 -1 28 144.754 26.7831 2 2 1 -28 140.787 22.0062 3 -2 -1 28 169.715 27.7778 2 2 1 28 166.585 27.6766 2 -2 1 -28 209.266 21.1607 3 2 -1 -28 186.382 24.0962 3 2 1 28 149.641 24.1762 4 -3 1 28 72.8374 14.0264 4 3 1 -28 83.7144 17.8626 3 -3 -1 -28 110.765 18.2645 3 3 -1 28 72.1411 21.2067 2 -3 1 28 103.818 24.3030 2 3 -1 28 102.153 20.9322 4 3 1 28 88.8786 22.8327 2 3 -1 -28 110.151 20.6975 3 -3 -1 28 136.305 24.5803 2 3 1 28 116.652 22.8005 4 -4 1 28 58.2493 15.9558 4 -4 -1 -28 59.9986 14.8093 3 -4 1 28 54.3668 20.8473 2 4 -1 28 73.6048 21.2617 2 4 1 -28 48.5019 16.3559 3 4 -1 28 42.7933 18.5295 4 -4 -1 28 66.6560 19.4428 2 4 1 28 55.9134 18.7263 4 -4 1 -28 49.6787 11.7572 3 4 1 28 61.3336 19.5837 2 4 -1 -28 71.3453 17.8738 3 0 2 28 234.111 28.9917 4 0 -2 -28 223.711 28.9096 3 0 -2 28 265.436 24.4736 4 0 2 28 206.111 32.9849 2 0 2 28 255.516 29.5962 4 0 -2 28 265.440 24.3260 4 0 -2 28 299.604 35.7935 2 0 2 -28 252.005 27.8365 3 1 -2 28 145.285 18.8816 4 1 -2 28 132.984 25.8427 2 -1 2 28 141.314 20.4024 4 -1 2 28 146.792 26.9018 2 -1 -2 -28 145.110 22.9598 3 -1 2 28 161.942 20.9066 4 1 -2 28 141.529 19.6997 4 1 2 -28 130.388 21.5951 3 -1 -2 28 182.039 28.4478 2 1 2 28 164.056 27.4920 2 1 -2 -28 123.549 22.3141 3 -1 2 -28 143.866 20.5059 3 1 2 28 129.801 22.9694 4 -2 2 28 64.1622 22.1204 2 2 -2 28 51.2193 12.4743 3 -2 2 28 61.1275 14.5740 4 -2 -2 -28 49.9662 15.2878 3 -2 2 28 68.6728 14.4100 4 2 -2 28 58.5986 15.9476 4 2 -2 28 66.2055 20.7492 2 2 2 -28 53.0401 14.7118 3 -2 2 -28 101.380 17.4440 4 2 2 28 99.9564 22.1564 2 2 -2 -28 112.453 19.2691 3 2 2 28 91.3541 20.1284 4 -2 -2 28 109.043 23.1097 2 -2 2 -28 100.853 15.5507 3 -3 2 28 83.2908 15.9800 4 3 2 -28 87.2867 19.2382 3 3 -2 28 72.8546 21.5789 2 -3 2 28 72.1386 21.7918 2 3 -2 28 66.8191 18.2650 4 -3 -2 -28 89.7547 17.9242 3 3 2 28 103.494 21.6362 4 -3 2 -28 103.305 15.0395 3 3 -2 -28 88.5426 19.6966 3 3 2 28 81.2554 22.0138 2 -4 2 28 102.243 25.8295 2 4 -2 28 112.151 26.7824 2 4 -2 28 106.015 24.2605 4 -4 -2 -28 81.2488 18.0217 3 4 2 -28 107.383 20.6273 3 -4 2 28 109.673 17.8866 4 4 -2 -28 122.135 22.6259 3 -4 -2 28 161.285 26.9681 2 -4 2 -28 146.546 16.4348 3 4 2 28 147.646 25.5130 2 4 2 28 155.404 28.2397 4 0 -3 28 76.2434 7.88159 4 0 -3 28 82.0254 8.05604 4 0 3 -28 56.7503 13.7460 3 0 3 28 49.9144 19.0080 2 0 -3 28 39.5876 18.2602 2 0 -3 -28 52.4882 16.8597 3 0 3 28 53.9440 16.4222 4 -1 -3 -28 262.730 30.9409 3 1 -3 28 269.374 27.7050 4 1 -3 28 230.396 27.1206 4 -1 3 28 268.032 36.6869 2 1 -3 28 297.246 35.7822 2 1 3 -28 281.196 29.5814 3 -1 3 28 225.448 29.9769 4 1 3 28 326.291 37.7172 2 1 3 28 295.792 33.9389 4 -1 -3 28 303.843 36.7284 2 -1 3 -28 287.850 28.8973 3 1 -3 -28 343.658 34.5525 3 2 3 -28 186.820 24.9734 3 2 -3 28 172.201 21.6367 3 2 -3 28 198.488 23.5372 4 -2 3 28 182.773 29.9081 2 -2 3 28 179.565 27.6933 4 -2 -3 -28 143.911 24.9292 3 2 -3 28 177.516 29.7990 2 -2 3 28 141.700 23.5471 4 -2 3 -28 222.559 21.1268 3 2 3 28 170.062 26.3042 4 -2 -3 28 177.314 29.0449 2 -2 3 -28 174.263 23.3663 4 2 3 28 167.076 28.6048 2 2 -3 -28 188.477 26.2536 3 -3 3 28 15.0895 15.6861 2 -3 -3 -28 5.43780 12.5006 3 3 -3 28 13.4673 14.4729 2 -3 3 28 4.67755 10.9954 4 3 3 -28 8.15658 11.5118 3 3 -3 28 -0.0697 11.7426 4 -3 -3 28 2.36542 13.8574 2 3 -3 -28 2.96643 13.2249 3 3 3 28 11.1830 14.6286 2 -3 3 -28 14.1339 7.73188 3 3 3 28 5.04788 13.0743 4 -4 3 28 293.036 37.3107 2 4 -3 28 231.590 32.3696 4 4 -3 28 260.276 36.2925 2 4 3 -28 248.153 30.3751 3 -4 3 28 245.285 28.8855 4 4 -3 -28 305.770 44.4911 3 4 3 28 211.747 35.1692 4 4 3 28 259.099 34.1707 2 -4 -3 28 215.852 32.9441 2 0 4 28 9.49610 14.5170 2 0 -4 -28 12.6763 12.9929 3 0 -4 28 3.10605 13.8134 2 0 4 28 6.66684 11.8191 4 0 4 -28 3.78027 8.96794 3 -1 -4 -28 185.918 24.2039 3 -1 4 28 158.387 23.8900 4 1 -4 28 147.563 27.8814 2 1 -4 28 181.553 17.9472 4 1 -4 28 173.994 19.8132 3 -1 4 28 191.536 29.5394 2 1 4 -28 187.100 22.8653 3 -1 4 -28 119.618 18.7620 3 1 4 28 114.810 24.6721 4 1 -4 -28 107.937 21.7515 3 -1 -4 28 99.4387 24.5920 2 1 4 28 115.059 25.6943 2 2 -4 28 397.954 45.1432 2 -2 4 28 355.882 39.1460 4 2 4 -28 371.349 38.3474 3 2 -4 28 314.915 36.2182 4 -2 4 28 409.661 45.5109 2 2 4 28 372.696 43.6531 2 2 -4 -28 382.862 40.3543 3 -2 4 -28 360.941 33.7540 3 -2 -4 28 415.164 44.5407 2 2 4 28 368.496 41.6242 4 3 4 -28 21.8931 12.4962 3 3 -4 28 12.5659 12.5394 4 -3 4 28 15.2137 13.0933 4 -3 4 28 12.7470 17.7176 2 3 -4 28 15.4269 17.9553 2 -3 -4 -28 21.0930 14.3636 3 -3 -4 28 25.5104 15.7906 2 -3 4 -28 17.4894 6.88578 3 3 4 28 23.4106 16.5757 4 3 4 28 27.9816 15.9980 2 3 -4 -28 35.7761 15.8378 3 0 5 28 123.863 25.9661 2 0 5 -28 102.887 16.7860 3 0 5 28 78.0630 20.7491 4 0 -5 -28 83.9832 19.9806 3 0 -5 28 114.409 24.9949 2 1 5 -28 41.9921 12.8819 3 1 -5 28 64.1753 9.75872 4 -1 5 28 73.0419 18.6201 4 1 -5 28 50.7081 19.2953 2 -1 5 28 39.7716 19.1536 2 -1 -5 -28 33.5109 15.2441 3 -1 5 -28 89.1880 13.4101 3 -1 -5 28 84.4981 22.1275 2 1 5 28 62.9656 20.3874 2 1 -5 -28 96.5158 19.2107 3 1 5 28 52.7718 17.9351 4 -2 -5 -28 219.529 29.1803 3 2 -5 28 203.807 33.9197 2 2 -5 28 277.707 26.7901 4 -2 5 28 194.578 33.5479 2 2 5 -28 272.827 28.3569 3 -2 5 28 236.777 30.7039 4 -2 -5 28 217.258 32.9550 2 2 5 28 196.287 34.3881 2 -2 5 -28 209.728 22.0944 3 2 5 28 218.043 33.8037 4 2 -5 -28 225.985 30.2163 3 -3 5 28 236.854 38.2141 2 -3 -5 -28 200.969 28.5819 3 3 -5 28 181.595 25.3675 4 3 5 -28 179.395 25.8681 3 -3 5 28 164.949 26.3461 4 3 5 28 148.801 29.3284 4 3 -5 -28 195.555 31.7961 3 3 5 28 188.583 31.9001 2 0 6 28 61.3105 18.7215 4 0 6 28 61.1712 20.7348 2 0 -6 -28 73.5800 19.9793 3 0 6 -28 94.9097 15.1899 3 0 -6 28 73.4126 21.1849 2 -1 6 28 45.1811 18.3204 4 -1 -6 -28 53.5237 18.7186 3 1 -6 28 40.1892 19.3248 2 1 6 -28 62.4206 14.1594 3 -1 6 28 69.0166 21.5358 2 1 6 28 72.3825 21.5792 4 -1 -6 28 64.5829 20.7240 2 1 -6 -28 75.6384 19.2597 3 1 6 28 68.3469 21.6912 2 -1 6 -28 83.5818 13.0113 3 -2 6 28 222.964 30.6120 4 2 -6 28 185.665 23.8308 4 -2 -6 -28 210.201 28.5683 3 2 6 -28 188.760 25.5722 3 -2 -6 28 181.753 30.6988 2 2 6 28 197.137 31.7882 4 2 6 28 232.408 32.9900 2 2 -6 -28 255.270 44.5402 3 0 0 29 9.98501 10.2345 4 0 0 29 10.0229 9.22668 4 0 0 29 11.4583 15.1427 2 0 0 -29 6.28690 11.6717 3 1 0 -29 306.460 34.6779 3 1 0 29 330.372 40.0569 2 -1 0 29 332.962 30.6159 4 -1 0 -29 309.719 32.5823 3 -1 0 29 349.565 40.1780 2 -1 0 29 321.120 30.9381 4 1 0 29 300.381 33.6402 4 1 0 29 267.942 32.6402 4 -2 0 -29 56.4855 14.4639 3 2 0 29 44.0288 15.6216 4 -2 0 29 54.4491 20.6563 2 2 0 29 48.7196 19.1470 2 2 0 -29 43.8808 15.2946 3 -2 0 29 54.9312 9.66101 4 -3 0 -29 101.902 16.9392 3 3 0 29 91.9240 22.6807 2 3 0 29 89.0150 20.7011 4 -3 0 29 66.4799 20.8963 2 3 0 -29 69.0035 18.8414 3 0 1 29 7.04156 10.6801 4 0 -1 29 7.00011 14.9886 2 0 -1 29 13.3449 8.84656 4 0 -1 29 14.3264 9.00556 4 0 1 -29 7.21686 11.5141 3 0 1 29 -3.6107 9.66848 4 0 1 29 13.0163 15.0785 2 0 -1 -29 2.43439 10.3762 3 1 1 -29 20.0050 12.9580 3 1 -1 29 14.5998 15.4349 2 -1 1 29 13.4358 9.73693 4 -1 -1 -29 25.9328 13.5416 3 1 -1 29 15.0205 10.7904 4 -1 1 29 14.8968 10.2650 4 1 -1 29 13.5456 10.6357 4 -1 1 29 11.8533 15.0691 2 1 1 29 35.5434 16.9682 2 1 1 29 15.9043 13.0908 4 1 -1 -29 26.4172 12.7478 3 -1 1 -29 41.3763 13.0935 3 -1 -1 29 29.0751 7.47803 4 -1 -1 29 15.9507 15.2254 2 -1 -1 29 23.8412 6.67169 4 -2 1 29 301.283 37.2011 2 2 -1 29 260.584 35.7798 2 2 1 -29 281.373 32.4173 3 -2 1 29 242.319 26.9897 4 -2 -1 -29 272.224 30.1516 3 2 -1 29 250.487 30.5175 4 2 -1 -29 294.451 33.3085 3 -2 -1 29 255.053 36.0814 2 2 1 29 305.828 37.1948 2 2 1 29 255.862 32.2713 4 -2 1 -29 247.251 28.7160 3 3 -1 29 64.9898 18.4019 4 -3 1 29 98.0877 23.2312 2 -3 1 29 59.8375 12.1961 4 -3 -1 -29 106.310 17.8808 3 3 1 -29 99.1282 19.1601 3 3 -1 29 98.3975 23.2220 2 3 -1 -29 57.7764 17.6719 3 3 1 29 106.263 25.0100 2 -3 -1 29 73.6976 21.2983 2 -3 1 -29 71.2491 14.5251 3 3 1 29 60.7671 19.9526 4 0 -2 29 245.231 26.1390 4 0 2 29 279.870 30.4524 4 0 -2 29 217.618 23.4240 4 0 -2 29 271.453 35.5268 2 0 2 -29 252.696 28.1320 3 0 -2 -29 245.104 29.4665 3 -1 -2 -29 27.7704 14.5625 3 -1 2 29 42.8090 18.8418 2 1 -2 29 48.0532 12.7343 4 -1 2 29 63.1393 15.2429 4 1 -2 29 39.8250 18.4169 2 1 2 -29 41.0056 13.4738 3 -1 2 29 58.8012 14.7305 4 -1 -2 29 26.4144 17.5669 2 1 2 29 63.6551 19.7776 2 1 2 29 59.4619 17.3215 4 1 -2 -29 50.3684 15.4951 3 -1 2 -29 46.4825 12.7913 3 -2 2 29 34.7516 12.4538 4 2 -2 29 45.9551 18.5749 2 2 -2 29 57.4828 15.2260 4 -2 2 29 61.0037 21.3647 2 2 2 -29 62.3676 15.5591 3 -2 -2 -29 60.2591 15.9817 3 -2 2 -29 73.5030 13.6618 3 2 2 29 73.8452 20.9881 2 -2 -2 29 64.6053 20.2896 2 2 -2 -29 82.5087 19.5154 3 2 2 29 65.8318 17.5098 4 -3 2 29 74.9320 14.2809 4 -3 -2 -29 77.7157 16.6377 3 3 2 -29 49.5173 16.7401 3 3 -2 29 97.0714 20.0736 4 -3 2 29 78.8862 22.7592 2 3 -2 29 55.8702 19.4343 2 -3 2 -29 56.6164 12.4757 3 3 2 29 35.6136 17.9478 4 3 -2 -29 39.7189 16.6396 3 -3 -2 29 50.6103 19.5755 2 3 2 29 60.8368 19.8972 2 0 3 -29 151.019 22.1994 3 0 -3 -29 183.696 26.5687 3 0 3 29 159.252 24.7763 4 0 3 29 143.589 28.7560 2 0 -3 29 164.355 28.9369 2 1 -3 29 153.510 20.2506 4 -1 -3 -29 160.590 25.9048 3 1 3 -29 166.945 23.4531 3 1 -3 29 177.851 29.8958 2 -1 3 29 170.918 29.7848 2 -1 3 29 143.458 24.3028 4 1 3 29 147.461 26.0590 4 1 -3 -29 172.123 26.9098 3 -1 -3 29 190.354 29.9016 2 -1 3 -29 196.839 22.0604 3 1 3 29 225.215 31.0959 2 -2 -3 -29 9.82065 11.6841 3 2 -3 29 6.27815 11.0229 4 -2 3 29 5.10230 10.9467 4 -2 3 29 9.23400 17.5709 2 2 -3 29 27.9033 17.4367 2 2 3 -29 16.3087 12.5191 3 2 3 29 4.07435 14.8553 4 2 -3 -29 18.2268 13.6868 3 2 3 29 26.9519 17.9999 2 -2 3 -29 6.41014 8.66637 3 -2 -3 29 21.3298 15.8441 2 -3 3 29 157.689 23.4345 4 -3 -3 -29 156.527 25.5412 3 3 -3 29 166.158 30.1474 2 3 -3 29 173.511 26.1553 4 3 3 -29 161.174 24.6162 3 3 -3 -29 194.225 27.3690 3 3 3 29 179.830 29.8313 2 -3 3 -29 183.222 20.0509 3 3 3 29 218.904 29.1594 4 -3 -3 29 180.558 29.4285 2 0 4 -29 403.960 38.8821 3 0 -4 29 408.843 47.3655 2 0 -4 -29 424.735 42.9391 3 0 4 29 392.596 47.2787 2 1 4 -29 67.9430 15.9070 3 -1 4 29 69.6867 18.1821 4 -1 -4 -29 63.0519 18.3257 3 -1 4 29 89.9493 22.7728 2 1 -4 29 80.4067 13.0345 4 1 -4 29 64.9573 21.6493 2 1 -4 -29 74.3238 18.6001 3 1 4 29 101.756 21.9614 4 -1 -4 29 126.452 25.7437 2 1 4 29 140.970 26.2917 2 -1 4 -29 95.3293 15.7862 3 -2 4 29 86.2665 18.4494 4 -2 -4 -29 58.4873 17.4508 3 2 -4 29 63.4753 21.0223 2 2 4 -29 64.2573 16.3958 3 -2 4 29 56.4744 20.4599 2 2 -4 29 88.2609 16.7947 4 2 -4 -29 73.7332 18.8368 3 -2 -4 29 64.6118 20.5388 2 2 4 29 64.3614 20.5218 4 2 4 29 63.2459 21.9293 2 -2 4 -29 72.2211 12.2178 3 0 5 -29 176.393 22.1253 3 0 5 29 182.241 28.2512 4 0 5 29 187.973 30.8148 2 0 -5 -29 141.863 26.3521 3 0 -5 29 187.088 31.3135 2 1 -5 29 11.1931 15.6904 2 -1 -5 -29 12.2202 14.8320 3 1 5 -29 23.1440 11.4343 3 -1 5 29 18.4851 16.8917 2 -1 5 29 23.2028 15.2357 4 -1 5 -29 19.4661 9.47276 3 1 5 29 20.4694 15.5411 4 1 5 29 8.92246 15.4480 2 1 -5 -29 11.2269 14.4232 3 -1 -5 29 18.7133 16.5898 2 -2 -5 -29 151.314 24.4294 3 2 5 -29 109.654 19.8167 3 -2 5 29 93.1345 21.4601 4 2 5 29 108.129 24.6240 4 2 5 29 129.696 26.8576 2 -2 -5 29 114.305 24.6166 2 2 -5 -29 86.5735 21.1546 3 0 0 30 319.067 33.3444 4 0 0 -30 336.505 35.4818 3 0 0 30 329.041 41.3416 2 1 0 -30 136.087 21.6834 3 1 0 30 144.935 27.7963 2 -1 0 -30 140.667 20.6581 3 1 0 30 175.264 22.5232 4 -1 0 30 123.940 17.6063 4 -1 0 30 121.957 26.3625 2 2 0 -30 19.7721 14.5719 3 -2 0 30 20.1335 15.5480 2 -2 0 -30 15.8174 11.8617 3 2 0 30 6.45468 12.6133 4 2 0 30 17.4306 16.1648 2 -3 0 -30 283.102 31.1729 3 3 0 -30 286.195 33.5752 3 3 0 30 254.832 37.2581 2 -3 0 30 300.518 40.5834 2 0 1 -30 297.701 32.0199 3 0 -1 30 319.314 30.0342 4 0 1 30 256.886 37.7992 2 0 1 30 345.837 32.9675 4 0 -1 30 248.968 37.9776 2 0 -1 -30 295.947 33.0952 3 -1 1 30 326.805 40.3068 2 -1 1 30 331.925 31.5614 4 1 -1 30 395.851 41.9374 2 1 1 -30 337.331 34.7680 3 1 -1 30 327.635 32.7655 4 -1 -1 -30 276.645 33.6182 3 -1 -1 30 286.265 27.3260 4 -1 1 -30 276.467 32.4819 3 -1 -1 30 283.943 39.2478 2 1 1 30 248.218 32.9758 4 1 1 30 311.245 39.7890 2 1 -1 -30 314.018 35.1872 3 -2 -1 -30 208.427 26.1260 3 -2 1 30 197.094 22.5239 4 2 -1 30 249.181 33.6007 2 2 -1 30 216.548 27.2369 4 -2 1 30 216.333 32.7263 2 2 1 -30 224.297 27.2750 3 -2 -1 30 156.157 30.7172 2 2 -1 -30 188.639 27.3362 3 2 1 30 159.618 30.6691 2 2 1 30 204.646 28.4360 4 -2 1 -30 185.188 24.5486 3 3 1 -30 169.709 27.0285 3 3 -1 30 167.205 29.9756 2 -3 1 30 178.855 30.4338 2 3 -1 30 160.214 26.0963 4 -3 -1 -30 141.335 23.9568 3 -3 1 -30 168.384 21.9521 3 3 -1 -30 174.829 28.3558 3 3 1 30 174.047 29.9689 2 -3 -1 30 167.780 29.8704 2 0 2 -30 230.679 26.9581 3 0 -2 -30 210.972 28.1432 3 0 -2 30 217.980 21.6715 4 0 2 30 267.280 29.4281 4 0 -2 30 190.909 32.3284 2 0 2 30 205.079 33.1219 2 1 -2 30 17.5885 10.3559 4 1 -2 30 17.6956 15.6575 2 -1 2 30 4.61635 15.1019 2 -1 -2 -30 13.5270 13.3386 3 -1 2 30 5.25030 10.6145 4 1 2 -30 19.8431 13.0624 3 1 2 30 -0.4378 12.1961 4 -1 2 -30 9.77382 10.4913 3 1 2 30 17.3674 15.6219 2 1 -2 -30 7.09829 12.5206 3 -1 -2 30 21.4841 18.1820 2 2 2 -30 238.126 28.8550 3 2 -2 30 238.414 33.8613 2 2 -2 30 251.055 27.6585 4 -2 2 30 212.671 33.4712 2 -2 2 30 229.559 25.4855 4 -2 -2 -30 241.942 28.3670 3 -2 2 -30 209.650 24.1348 3 2 2 30 149.244 30.6889 2 2 -2 -30 163.133 28.7907 3 2 2 30 156.251 28.5165 4 -2 -2 30 188.751 32.3677 2 0 3 -30 81.6988 16.2971 3 0 3 30 90.8373 23.0927 2 0 3 30 73.9926 18.5130 4 0 -3 30 83.7910 22.7319 2 0 -3 -30 60.6346 18.1022 3 1 -3 30 218.095 33.6135 2 1 3 -30 239.159 27.3607 3 1 -3 30 244.500 23.9180 4 -1 3 30 267.255 35.7676 2 -1 -3 30 191.366 32.0566 2 1 3 30 191.497 29.3238 4 1 3 30 179.268 32.1908 2 1 -3 -30 190.109 29.8822 3 -1 3 -30 191.483 25.0777 3 2 3 -30 73.7562 17.2670 3 -2 3 30 57.5481 21.2859 2 2 -3 30 78.4345 15.9180 4 -2 -3 -30 65.8872 17.7641 3 2 -3 30 50.3703 20.6603 2 -2 3 30 66.5336 15.7489 4 -2 -3 30 31.8979 18.0950 2 2 3 30 49.5592 18.7405 4 -2 3 -30 31.2949 10.9572 3 2 -3 -30 37.6642 16.2160 3 2 3 30 45.0625 20.4420 2 0 -4 -30 12.8344 12.8133 3 0 4 30 0.01368 11.7620 4 0 4 30 -0.5345 17.2879 2 0 4 -30 1.41142 9.70375 3 0 -4 30 4.73973 15.6961 2 -1 -4 -30 88.4930 19.5441 3 -1 4 30 126.807 23.2025 4 1 -4 30 115.308 26.5886 2 -1 4 30 135.296 32.3991 2 1 4 -30 104.043 19.0785 3 1 -4 -30 99.3196 21.4448 3 -1 4 -30 128.471 18.4277 3 1 4 30 103.425 22.6827 4 1 4 30 106.714 25.3286 2 -1 -4 30 89.4162 23.7588 2 0 0 31 11.6653 16.2595 2 0 0 -31 25.0466 12.4526 3 0 0 31 6.89329 10.2698 4 -1 0 31 6.82795 15.4349 2 -1 0 -31 -4.5062 10.6800 3 1 0 31 -6.7165 13.9799 2 1 0 31 5.03368 11.3377 4 -1 0 31 9.76377 9.63385 4 1 0 -31 5.55680 12.8447 3 2 0 31 121.383 30.2459 2 2 0 -31 149.065 23.7339 3 2 0 31 139.092 23.6408 4 -2 0 31 167.890 29.5602 2 0 -1 31 72.9009 14.1259 4 0 1 31 66.2161 15.8745 4 0 -1 31 66.4586 22.2353 2 0 1 -31 62.4901 16.0684 3 0 1 31 60.7895 20.3572 2 0 -1 -31 48.8888 15.5110 3 -1 -1 -31 296.636 35.3064 3 1 -1 31 330.270 34.0658 4 -1 1 31 340.536 33.3082 4 -1 1 31 336.918 42.2971 2 1 -1 31 339.282 42.3202 2 -1 -1 31 337.255 42.5530 2 1 1 31 312.339 35.4245 4 -1 1 -31 330.521 34.5563 3 1 -1 -31 313.839 36.9587 3 -2 1 31 65.9743 25.7569 2 -2 -1 -31 53.1325 15.2223 3 2 1 -31 56.5826 17.5239 3 2 -1 31 53.8471 15.7782 4 2 1 31 55.8727 24.0163 2 -2 1 -31 60.6952 15.2060 3 -2 -1 31 61.4998 21.2689 2 2 -1 -31 60.3913 17.1776 3 0 -2 -31 3.36275 11.8559 3 0 2 -31 5.35921 11.7291 3 0 2 31 7.22771 15.6217 2 0 2 31 -0.3946 12.0356 4 0 -2 31 -2.7584 14.0788 2 -1 -2 -31 9.37635 11.9561 3 1 -2 31 25.0783 11.0480 4 1 2 -31 22.4667 13.0737 3 -1 2 31 34.0820 18.6056 2 -1 2 31 26.0231 12.6594 4 1 -2 31 33.4000 21.2271 2 1 2 31 11.0264 13.2122 4 -1 -2 31 7.90955 15.3996 2 -1 2 -31 26.3470 12.3041 3 1 -2 -31 22.3666 13.9691 3 1 2 31 27.9074 17.6916 2 0 3 31 203.677 29.0777 4 0 3 -31 239.799 26.6819 3 0 0 0 0.00 0.00 0 _exptl_absorpt_process_details 'SADABS 2014/5' _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_max 0.6985 _exptl_absorpt_correction_T_min 0.6527 _exptl_special_details ) The following wavelength and cell were deduced by SADABS from the direction cosines etc. They are given here for emergency use only: CELL 0.71073 7.242 10.879 23.844 89.997 90.010 90.002 ) ; _shelx_hkl_checksum 74745