data_cb9block _audit_creation_method SHELXL-2014 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C30 H22 Fe N6, 2(Cl O4), H2 O' _chemical_formula_sum 'C30 H24 Cl2 Fe N6 O9' _chemical_formula_weight 739.30 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0040 0.0020 'WGCromer Program in WinGX L.J. Farrugia, J.Appl.Cryst. 2012,45,849-854' 'H' 'H' 0.0000 0.0000 'WGCromer Program in WinGX L.J. Farrugia, J.Appl.Cryst. 2012,45,849-854' 'N' 'N' 0.0076 0.0040 'WGCromer Program in WinGX L.J. Farrugia, J.Appl.Cryst. 2012,45,849-854' 'O' 'O' 0.0133 0.0073 'WGCromer Program in WinGX L.J. Farrugia, J.Appl.Cryst. 2012,45,849-854' 'Cl' 'Cl' 0.1704 0.1889 'WGCromer Program in WinGX L.J. Farrugia, J.Appl.Cryst. 2012,45,849-854' 'Fe' 'Fe' 0.3584 0.9913 'WGCromer Program in WinGX L.J. Farrugia, J.Appl.Cryst. 2012,45,849-854' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/n' _space_group_name_Hall '-P 2yn' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 8.7293(4) _cell_length_b 8.7613(5) _cell_length_c 38.725(2) _cell_angle_alpha 90 _cell_angle_beta 91.950(3) _cell_angle_gamma 90 _cell_volume 2960.0(3) _cell_formula_units_Z 4 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 9914 _cell_measurement_theta_min 2.29 _cell_measurement_theta_max 33.83 _exptl_crystal_description block _exptl_crystal_colour 'dark red' _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.659 _exptl_crystal_F_000 1512 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.100 _exptl_crystal_size_mid 0.090 _exptl_crystal_size_min 0.080 _exptl_absorpt_coefficient_mu 0.898 _shelx_estimated_absorpt_T_min 0.916 _shelx_estimated_absorpt_T_max 0.932 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.645 _exptl_absorpt_correction_T_max 0.747 _exptl_absorpt_process_details 'SADABS-2014/4' _exptl_special_details ; ? ; _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.7749 _diffrn_radiation_source 'Advanced Light Source station 11.3.1' _diffrn_radiation_monochromator 'silicon 111' _diffrn_measurement_device_type 'Bruker D8 with PHOTON 100 detector' _diffrn_measurement_method 'shutterless /f and /w scans' _diffrn_detector_area_resol_mean 10.42 _diffrn_reflns_number 45305 _diffrn_reflns_av_unetI/netI 0.0408 _diffrn_reflns_av_R_equivalents 0.0475 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_l_min -54 _diffrn_reflns_limit_l_max 54 _diffrn_reflns_theta_min 2.295 _diffrn_reflns_theta_max 33.072 _diffrn_reflns_theta_full 33.050 _diffrn_measured_fraction_theta_max 0.994 _diffrn_measured_fraction_theta_full 0.994 _diffrn_reflns_Laue_measured_fraction_max 0.994 _diffrn_reflns_Laue_measured_fraction_full 0.994 _diffrn_reflns_point_group_measured_fraction_max 0.994 _diffrn_reflns_point_group_measured_fraction_full 0.994 _reflns_number_total 8630 _reflns_number_gt 7493 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Bruker APEX 2' _computing_cell_refinement 'Bruker SAINT' _computing_data_reduction 'Bruker SAINT' _computing_structure_solution 'SHELXT (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2014 (Sheldrick, 2014)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ; All non-hydrogens were refined anisotropically. Hydrogens were placed geometrically on their carrier atom and refined with a riding model except those on the lattice water oxygen O1W that could no be found nor fixed and are omitted in the structural model. ; _vrf_PLAT306_cb9block ; PROBLEM: Isolated Oxygen Atom (H-atoms Missing ?) ....... O1W RESPONSE: Hydrogens on the lattice oxygen O1W could not be found nor fixed. The presence of these hydrogens is clearly indicated by short contact of O1W with O2 and O3, corresponding to hydrogen bonds. However refinement of hydrogen atoms at the corresponding approximate coordinates with distance restraints did not converge and these hydrogens are thus omitted in the structural model, although taken into account in the formula. ; _vrf_PLAT430_cb9block ; PROBLEM: Short Inter D...A Contact O1W .. O3 .. 2.69 Ang. RESPONSE: Hydrogens on the lattice oxygen O1W could not be found nor fixed. The presence of these hydrogens is clearly indicated by short contact of O1W with O2 and O3, corresponding to hydrogen bonds. However refinement of hydrogen atoms at the corresponding approximate coordinates with distance restraints did not converge and these hydrogens are thus omitted in the structural model, although taken into account in the formula. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0228P)^2^+19.2178P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 8630 _refine_ls_number_parameters 433 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0878 _refine_ls_R_factor_gt 0.0785 _refine_ls_wR_factor_ref 0.1800 _refine_ls_wR_factor_gt 0.1769 _refine_ls_goodness_of_fit_ref 1.231 _refine_ls_restrained_S_all 1.231 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Fe1 Fe 0.65865(6) 0.34030(6) 0.37252(2) 0.01022(12) Uani 1 1 d . . . . . N1 N 0.4494(3) 0.2568(4) 0.36648(8) 0.0119(6) Uani 1 1 d . . . . . N2 N 0.6296(4) 0.3704(4) 0.32462(8) 0.0124(6) Uani 1 1 d . . . . . N3 N 0.8627(3) 0.4254(4) 0.36227(9) 0.0135(6) Uani 1 1 d . . . . . N4 N 0.5799(3) 0.5400(4) 0.38820(8) 0.0120(6) Uani 1 1 d . . . . . N5 N 0.6921(3) 0.3164(4) 0.42057(8) 0.0119(6) Uani 1 1 d . . . . . N6 N 0.7411(3) 0.1299(4) 0.37291(8) 0.0122(6) Uani 1 1 d . . . . . C1 C 0.3643(4) 0.1925(4) 0.39085(10) 0.0137(7) Uani 1 1 d . . . . . H1A H 0.4010 0.1951 0.4142 0.016 Uiso 1 1 calc R U . . . C2 C 0.2239(4) 0.1220(5) 0.38301(11) 0.0171(8) Uani 1 1 d . . . . . H2A H 0.1656 0.0781 0.4008 0.021 Uiso 1 1 calc R U . . . C3 C 0.1710(4) 0.1173(5) 0.34888(11) 0.0188(8) Uani 1 1 d . . . . . H3A H 0.0773 0.0673 0.3429 0.023 Uiso 1 1 calc R U . . . C4 C 0.2554(4) 0.1858(5) 0.32361(11) 0.0178(8) Uani 1 1 d . . . . . H4A H 0.2194 0.1855 0.3002 0.021 Uiso 1 1 calc R U . . . C5 C 0.3934(4) 0.2550(4) 0.33303(10) 0.0145(7) Uani 1 1 d . . . . . C6 C 0.4957(4) 0.3282(4) 0.30884(10) 0.0142(7) Uani 1 1 d . . . . . C7 C 0.4666(5) 0.3594(5) 0.27382(11) 0.0202(8) Uani 1 1 d . . . . . H7A H 0.3711 0.3329 0.2629 0.024 Uiso 1 1 calc R U . . . C8 C 0.5796(5) 0.4294(5) 0.25539(11) 0.0231(9) Uani 1 1 d . . . . . H8A H 0.5627 0.4494 0.2315 0.028 Uiso 1 1 calc R U . . . C9 C 0.7181(5) 0.4710(5) 0.27167(11) 0.0212(8) Uani 1 1 d . . . . . H9A H 0.7956 0.5201 0.2591 0.025 Uiso 1 1 calc R U . . . C10 C 0.7410(4) 0.4395(5) 0.30651(10) 0.0155(7) Uani 1 1 d . . . . . C11 C 0.8773(4) 0.4703(4) 0.32874(11) 0.0152(7) Uani 1 1 d . . . . . C12 C 1.0107(5) 0.5376(5) 0.31731(12) 0.0203(8) Uani 1 1 d . . . . . H12A H 1.0180 0.5696 0.2940 0.024 Uiso 1 1 calc R U . . . C13 C 1.1331(5) 0.5570(5) 0.34074(13) 0.0227(9) Uani 1 1 d . . . . . H13A H 1.2251 0.6035 0.3336 0.027 Uiso 1 1 calc R U . . . C14 C 1.1205(4) 0.5087(5) 0.37430(12) 0.0202(8) Uani 1 1 d . . . . . H14A H 1.2042 0.5199 0.3904 0.024 Uiso 1 1 calc R U . . . C15 C 0.9834(4) 0.4429(4) 0.38434(11) 0.0159(7) Uani 1 1 d . . . . . H15A H 0.9752 0.4095 0.4075 0.019 Uiso 1 1 calc R U . . . C16 C 0.5163(4) 0.6512(5) 0.36852(10) 0.0151(7) Uani 1 1 d . . . . . H16A H 0.5122 0.6385 0.3441 0.018 Uiso 1 1 calc R U . . . C17 C 0.4565(4) 0.7835(5) 0.38234(11) 0.0168(7) Uani 1 1 d . . . . . H17A H 0.4128 0.8600 0.3677 0.020 Uiso 1 1 calc R U . . . C18 C 0.4613(5) 0.8028(5) 0.41799(11) 0.0190(8) Uani 1 1 d . . . . . H18A H 0.4185 0.8913 0.4280 0.023 Uiso 1 1 calc R U . . . C19 C 0.5294(5) 0.6907(5) 0.43872(11) 0.0174(7) Uani 1 1 d . . . . . H19A H 0.5374 0.7031 0.4631 0.021 Uiso 1 1 calc R U . . . C20 C 0.5856(4) 0.5606(5) 0.42324(10) 0.0139(7) Uani 1 1 d . . . . . C21 C 0.6565(4) 0.4310(4) 0.44217(10) 0.0131(7) Uani 1 1 d . . . . . C22 C 0.6870(5) 0.4194(5) 0.47756(10) 0.0183(8) Uani 1 1 d . . . . . H22A H 0.6613 0.5001 0.4927 0.022 Uiso 1 1 calc R U . . . C23 C 0.7556(5) 0.2879(5) 0.49021(11) 0.0210(8) Uani 1 1 d . . . . . H23A H 0.7782 0.2785 0.5143 0.025 Uiso 1 1 calc R U . . . C24 C 0.7921(5) 0.1685(5) 0.46798(11) 0.0190(8) Uani 1 1 d . . . . . H24A H 0.8379 0.0771 0.4766 0.023 Uiso 1 1 calc R U . . . C25 C 0.7593(4) 0.1880(4) 0.43283(10) 0.0134(7) Uani 1 1 d . . . . . C26 C 0.7878(4) 0.0801(4) 0.40498(10) 0.0134(7) Uani 1 1 d . . . . . C27 C 0.8547(4) -0.0635(5) 0.40985(11) 0.0170(7) Uani 1 1 d . . . . . H27A H 0.8885 -0.0960 0.4322 0.020 Uiso 1 1 calc R U . . . C28 C 0.8709(5) -0.1575(5) 0.38154(12) 0.0203(8) Uani 1 1 d . . . . . H28A H 0.9180 -0.2547 0.3842 0.024 Uiso 1 1 calc R U . . . C29 C 0.8178(4) -0.1089(5) 0.34917(12) 0.0191(8) Uani 1 1 d . . . . . H29A H 0.8252 -0.1736 0.3296 0.023 Uiso 1 1 calc R U . . . C30 C 0.7536(4) 0.0357(4) 0.34575(11) 0.0147(7) Uani 1 1 d . . . . . H30A H 0.7175 0.0689 0.3236 0.018 Uiso 1 1 calc R U . . . Cl1 Cl 0.78637(11) 0.79889(12) 0.52302(2) 0.0188(2) Uani 1 1 d . . . . . Cl2 Cl 0.44925(12) 0.84726(12) 0.27615(3) 0.0216(2) Uani 1 1 d . . . . . O1 O 0.6233(4) 0.7776(6) 0.52236(9) 0.0402(10) Uani 1 1 d . . . . . O2 O 0.8558(4) 0.6828(4) 0.54459(9) 0.0303(8) Uani 1 1 d . . . . . O3 O 0.8395(4) 0.7856(4) 0.48839(8) 0.0294(7) Uani 1 1 d . . . . . O4 O 0.8258(5) 0.9467(4) 0.53662(9) 0.0362(9) Uani 1 1 d . . . . . O5 O 0.4649(5) 1.0105(4) 0.27301(11) 0.0390(10) Uani 1 1 d . . . . . O6 O 0.3130(5) 0.8123(5) 0.29503(11) 0.0474(11) Uani 1 1 d . . . . . O7 O 0.4396(5) 0.7810(5) 0.24255(9) 0.0390(9) Uani 1 1 d . . . . . O8 O 0.5820(4) 0.7889(5) 0.29489(9) 0.0369(9) Uani 1 1 d . . . . . O1W O 0.9812(14) 0.3848(18) 0.5514(3) 0.195(5) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Fe1 0.0065(2) 0.0092(2) 0.0150(2) 0.00169(19) 0.00070(17) 0.00049(18) N1 0.0076(13) 0.0108(14) 0.0172(15) -0.0001(12) 0.0007(11) 0.0022(11) N2 0.0102(13) 0.0098(14) 0.0174(15) 0.0017(11) 0.0026(11) 0.0010(11) N3 0.0075(13) 0.0097(14) 0.0235(16) 0.0017(12) 0.0014(11) 0.0014(11) N4 0.0050(12) 0.0127(15) 0.0182(15) 0.0026(12) 0.0005(11) -0.0008(11) N5 0.0078(13) 0.0109(14) 0.0171(14) 0.0007(12) 0.0016(11) -0.0014(11) N6 0.0076(13) 0.0081(14) 0.0209(15) -0.0002(11) 0.0014(11) -0.0013(10) C1 0.0105(15) 0.0107(16) 0.0200(17) 0.0010(14) 0.0010(13) 0.0025(13) C2 0.0121(16) 0.0124(17) 0.027(2) 0.0004(15) 0.0037(14) 0.0027(13) C3 0.0073(16) 0.0164(18) 0.033(2) -0.0035(16) -0.0002(15) -0.0014(13) C4 0.0120(16) 0.0182(19) 0.0230(19) -0.0033(15) -0.0033(14) 0.0012(14) C5 0.0120(16) 0.0134(17) 0.0180(17) -0.0018(14) -0.0008(13) 0.0034(13) C6 0.0119(16) 0.0131(17) 0.0178(17) 0.0003(14) 0.0006(13) 0.0017(13) C7 0.0205(19) 0.021(2) 0.0188(19) -0.0008(15) -0.0021(15) 0.0023(16) C8 0.028(2) 0.025(2) 0.0162(18) 0.0040(16) 0.0032(16) 0.0051(18) C9 0.023(2) 0.020(2) 0.022(2) 0.0049(16) 0.0079(16) 0.0042(16) C10 0.0123(16) 0.0133(17) 0.0212(18) 0.0012(14) 0.0055(14) 0.0032(14) C11 0.0086(15) 0.0130(17) 0.0242(19) 0.0013(14) 0.0061(13) 0.0019(13) C12 0.0152(18) 0.0169(19) 0.030(2) 0.0023(16) 0.0112(15) -0.0013(15) C13 0.0109(17) 0.0153(19) 0.042(3) 0.0008(18) 0.0097(16) -0.0023(14) C14 0.0065(15) 0.0110(17) 0.043(3) 0.0002(17) 0.0013(15) 0.0007(13) C15 0.0088(15) 0.0091(16) 0.030(2) 0.0029(15) 0.0009(14) 0.0023(13) C16 0.0117(16) 0.0147(17) 0.0187(17) 0.0038(14) -0.0007(13) 0.0005(14) C17 0.0128(16) 0.0120(17) 0.025(2) 0.0022(15) -0.0007(14) 0.0035(14) C18 0.0158(17) 0.0136(18) 0.028(2) -0.0032(15) 0.0021(15) 0.0034(14) C19 0.0162(17) 0.0164(19) 0.0195(18) -0.0019(15) 0.0009(14) 0.0023(14) C20 0.0074(15) 0.0154(17) 0.0188(17) 0.0012(14) 0.0005(13) -0.0018(13) C21 0.0079(15) 0.0121(16) 0.0193(17) 0.0000(14) -0.0005(12) 0.0015(13) C22 0.0170(18) 0.021(2) 0.0174(18) 0.0004(15) 0.0007(14) 0.0032(15) C23 0.0213(19) 0.026(2) 0.0155(18) 0.0037(16) 0.0009(15) 0.0043(17) C24 0.0182(18) 0.0177(19) 0.0210(19) 0.0069(16) 0.0000(14) 0.0031(15) C25 0.0097(15) 0.0112(17) 0.0194(17) 0.0022(14) 0.0011(13) -0.0001(13) C26 0.0087(15) 0.0109(17) 0.0209(18) 0.0030(14) 0.0029(13) -0.0013(13) C27 0.0124(16) 0.0112(17) 0.027(2) 0.0065(15) 0.0026(14) 0.0009(14) C28 0.0153(17) 0.0107(17) 0.035(2) 0.0033(16) 0.0032(16) -0.0007(14) C29 0.0096(16) 0.0184(19) 0.029(2) -0.0040(16) 0.0006(14) 0.0003(14) C30 0.0081(15) 0.0130(17) 0.0231(19) -0.0012(14) 0.0014(13) -0.0004(13) Cl1 0.0167(4) 0.0211(5) 0.0185(4) 0.0040(4) -0.0013(3) -0.0010(4) Cl2 0.0227(5) 0.0198(5) 0.0222(5) 0.0049(4) -0.0017(4) -0.0052(4) O1 0.0134(15) 0.078(3) 0.0296(18) -0.0042(19) -0.0001(13) -0.0039(17) O2 0.0362(19) 0.0277(18) 0.0268(16) 0.0093(14) -0.0037(14) 0.0091(15) O3 0.0324(18) 0.037(2) 0.0191(15) 0.0060(14) 0.0040(13) -0.0051(15) O4 0.057(3) 0.0195(17) 0.0317(19) -0.0001(14) -0.0037(17) -0.0106(17) O5 0.050(2) 0.0151(16) 0.054(2) 0.0034(16) 0.0302(19) 0.0002(16) O6 0.034(2) 0.054(3) 0.054(3) 0.022(2) 0.0122(18) -0.0123(19) O7 0.054(2) 0.038(2) 0.0240(17) -0.0034(16) -0.0137(16) -0.0122(19) O8 0.0343(19) 0.049(2) 0.0267(17) 0.0063(16) -0.0140(15) 0.0005(17) O1W 0.152(10) 0.235(15) 0.198(12) -0.028(11) 0.001(9) -0.007(10) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Fe1 N2 1.882(3) . ? Fe1 N5 1.885(3) . ? Fe1 N1 1.974(3) . ? Fe1 N6 1.979(3) . ? Fe1 N4 1.983(3) . ? Fe1 N3 1.984(3) . ? N1 C1 1.344(5) . ? N1 C5 1.369(5) . ? N2 C6 1.352(5) . ? N2 C10 1.360(5) . ? N3 C15 1.342(5) . ? N3 C11 1.367(5) . ? N4 C16 1.345(5) . ? N4 C20 1.368(5) . ? N5 C25 1.347(5) . ? N5 C21 1.350(5) . ? N6 C30 1.345(5) . ? N6 C26 1.365(5) . ? C1 C2 1.397(5) . ? C1 H1A 0.9500 . ? C2 C3 1.385(6) . ? C2 H2A 0.9500 . ? C3 C4 1.382(6) . ? C3 H3A 0.9500 . ? C4 C5 1.386(5) . ? C4 H4A 0.9500 . ? C5 C6 1.464(5) . ? C6 C7 1.398(5) . ? C7 C8 1.381(6) . ? C7 H7A 0.9500 . ? C8 C9 1.393(6) . ? C8 H8A 0.9500 . ? C9 C10 1.385(6) . ? C9 H9A 0.9500 . ? C10 C11 1.470(6) . ? C11 C12 1.392(5) . ? C12 C13 1.388(6) . ? C12 H12A 0.9500 . ? C13 C14 1.375(7) . ? C13 H13A 0.9500 . ? C14 C15 1.395(5) . ? C14 H14A 0.9500 . ? C15 H15A 0.9500 . ? C16 C17 1.387(6) . ? C16 H16A 0.9500 . ? C17 C18 1.390(6) . ? C17 H17A 0.9500 . ? C18 C19 1.389(6) . ? C18 H18A 0.9500 . ? C19 C20 1.386(6) . ? C19 H19A 0.9500 . ? C20 C21 1.476(5) . ? C21 C22 1.391(5) . ? C22 C23 1.380(6) . ? C22 H22A 0.9500 . ? C23 C24 1.398(6) . ? C23 H23A 0.9500 . ? C24 C25 1.392(5) . ? C24 H24A 0.9500 . ? C25 C26 1.462(5) . ? C26 C27 1.398(5) . ? C27 C28 1.382(6) . ? C27 H27A 0.9500 . ? C28 C29 1.389(6) . ? C28 H28A 0.9500 . ? C29 C30 1.389(6) . ? C29 H29A 0.9500 . ? C30 H30A 0.9500 . ? Cl1 O1 1.435(3) . ? Cl1 O4 1.436(4) . ? Cl1 O2 1.437(3) . ? Cl1 O3 1.439(3) . ? Cl2 O7 1.424(4) . ? Cl2 O8 1.440(4) . ? Cl2 O5 1.442(4) . ? Cl2 O6 1.450(4) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N2 Fe1 N5 177.96(14) . . ? N2 Fe1 N1 80.92(14) . . ? N5 Fe1 N1 100.81(13) . . ? N2 Fe1 N6 100.08(14) . . ? N5 Fe1 N6 81.08(14) . . ? N1 Fe1 N6 89.47(13) . . ? N2 Fe1 N4 98.14(13) . . ? N5 Fe1 N4 80.75(14) . . ? N1 Fe1 N4 91.95(13) . . ? N6 Fe1 N4 161.72(14) . . ? N2 Fe1 N3 80.91(14) . . ? N5 Fe1 N3 97.41(13) . . ? N1 Fe1 N3 161.66(14) . . ? N6 Fe1 N3 91.30(13) . . ? N4 Fe1 N3 93.03(13) . . ? C1 N1 C5 118.1(3) . . ? C1 N1 Fe1 127.1(3) . . ? C5 N1 Fe1 114.6(3) . . ? C6 N2 C10 120.7(3) . . ? C6 N2 Fe1 119.5(3) . . ? C10 N2 Fe1 119.7(3) . . ? C15 N3 C11 118.4(3) . . ? C15 N3 Fe1 127.3(3) . . ? C11 N3 Fe1 114.3(2) . . ? C16 N4 C20 117.9(3) . . ? C16 N4 Fe1 127.3(3) . . ? C20 N4 Fe1 114.7(3) . . ? C25 N5 C21 120.6(3) . . ? C25 N5 Fe1 119.4(3) . . ? C21 N5 Fe1 119.9(3) . . ? C30 N6 C26 119.1(3) . . ? C30 N6 Fe1 127.2(3) . . ? C26 N6 Fe1 113.7(3) . . ? N1 C1 C2 122.3(4) . . ? N1 C1 H1A 118.8 . . ? C2 C1 H1A 118.8 . . ? C3 C2 C1 118.8(4) . . ? C3 C2 H2A 120.6 . . ? C1 C2 H2A 120.6 . . ? C4 C3 C2 119.6(4) . . ? C4 C3 H3A 120.2 . . ? C2 C3 H3A 120.2 . . ? C3 C4 C5 118.9(4) . . ? C3 C4 H4A 120.6 . . ? C5 C4 H4A 120.6 . . ? N1 C5 C4 122.2(4) . . ? N1 C5 C6 113.2(3) . . ? C4 C5 C6 124.5(4) . . ? N2 C6 C7 120.7(4) . . ? N2 C6 C5 111.6(3) . . ? C7 C6 C5 127.7(4) . . ? C8 C7 C6 118.6(4) . . ? C8 C7 H7A 120.7 . . ? C6 C7 H7A 120.7 . . ? C7 C8 C9 120.4(4) . . ? C7 C8 H8A 119.8 . . ? C9 C8 H8A 119.8 . . ? C10 C9 C8 118.9(4) . . ? C10 C9 H9A 120.6 . . ? C8 C9 H9A 120.6 . . ? N2 C10 C9 120.6(4) . . ? N2 C10 C11 111.0(3) . . ? C9 C10 C11 128.4(4) . . ? N3 C11 C12 122.0(4) . . ? N3 C11 C10 113.8(3) . . ? C12 C11 C10 124.2(4) . . ? C13 C12 C11 118.5(4) . . ? C13 C12 H12A 120.7 . . ? C11 C12 H12A 120.7 . . ? C14 C13 C12 119.7(4) . . ? C14 C13 H13A 120.1 . . ? C12 C13 H13A 120.1 . . ? C13 C14 C15 119.2(4) . . ? C13 C14 H14A 120.4 . . ? C15 C14 H14A 120.4 . . ? N3 C15 C14 122.1(4) . . ? N3 C15 H15A 118.9 . . ? C14 C15 H15A 118.9 . . ? N4 C16 C17 122.7(4) . . ? N4 C16 H16A 118.6 . . ? C17 C16 H16A 118.6 . . ? C16 C17 C18 119.1(4) . . ? C16 C17 H17A 120.5 . . ? C18 C17 H17A 120.5 . . ? C19 C18 C17 119.1(4) . . ? C19 C18 H18A 120.5 . . ? C17 C18 H18A 120.5 . . ? C20 C19 C18 118.9(4) . . ? C20 C19 H19A 120.6 . . ? C18 C19 H19A 120.6 . . ? N4 C20 C19 122.4(4) . . ? N4 C20 C21 113.1(3) . . ? C19 C20 C21 124.5(4) . . ? N5 C21 C22 121.0(4) . . ? N5 C21 C20 111.5(3) . . ? C22 C21 C20 127.5(4) . . ? C23 C22 C21 118.5(4) . . ? C23 C22 H22A 120.7 . . ? C21 C22 H22A 120.7 . . ? C22 C23 C24 120.7(4) . . ? C22 C23 H23A 119.6 . . ? C24 C23 H23A 119.6 . . ? C25 C24 C23 117.8(4) . . ? C25 C24 H24A 121.1 . . ? C23 C24 H24A 121.1 . . ? N5 C25 C24 121.3(4) . . ? N5 C25 C26 111.3(3) . . ? C24 C25 C26 127.4(4) . . ? N6 C26 C27 121.4(4) . . ? N6 C26 C25 114.3(3) . . ? C27 C26 C25 124.3(4) . . ? C28 C27 C26 118.9(4) . . ? C28 C27 H27A 120.6 . . ? C26 C27 H27A 120.6 . . ? C27 C28 C29 119.6(4) . . ? C27 C28 H28A 120.2 . . ? C29 C28 H28A 120.2 . . ? C28 C29 C30 119.1(4) . . ? C28 C29 H29A 120.4 . . ? C30 C29 H29A 120.4 . . ? N6 C30 C29 121.9(4) . . ? N6 C30 H30A 119.1 . . ? C29 C30 H30A 119.1 . . ? O1 Cl1 O4 110.4(3) . . ? O1 Cl1 O2 108.5(2) . . ? O4 Cl1 O2 109.5(2) . . ? O1 Cl1 O3 108.9(2) . . ? O4 Cl1 O3 109.5(2) . . ? O2 Cl1 O3 110.0(2) . . ? O7 Cl2 O8 109.7(3) . . ? O7 Cl2 O5 109.3(2) . . ? O8 Cl2 O5 108.5(3) . . ? O7 Cl2 O6 110.5(3) . . ? O8 Cl2 O6 109.3(2) . . ? O5 Cl2 O6 109.5(3) . . ? _refine_diff_density_max 1.946 _refine_diff_density_min -1.321 _refine_diff_density_rms 0.128 _shelxl_version_number 2014-3 _shelx_res_file ; REM Solution 1 R1 0.163 Rweak 0.019, Alpha = 0.0641 in P2(1)/n REM Formula: C30 N3 O12 Cl2 Fe TITL cb9block in P2/n CELL 0.7749 8.7293 8.7613 38.725 90.000 91.950 90.000 ZERR 4.00 0.0004 0.0005 0.002 0.000 0.003 0.000 LATT 1 SYMM 1/2-X, 1/2+Y, 1/2-Z SFAC C H N O CL FE DISP Fe 0.35840 0.99131 4329.23 DISP Cl 0.17039 0.18886 824.77 DISP O 0.01328 0.00733 32.03 DISP N 0.00764 0.00400 17.46 DISP C 0.00399 0.00196 8.55 DISP H 0.00000 0.00000 0.67 UNIT 120 96 24 36 8 4 TEMP -173 SIZE 0.10 0.09 0.08 REM piece of dark red block REM data to 0.71 angstrom REM inconsistent equivalents OMIT 0 1 1 OMIT 0 2 2 OMIT 2 0 4 OMIT 2 1 4 OMIT -1 3 5 OMIT -3 1 7 OMIT -1 3 7 OMIT 2 1 8 OMIT -9 0 9 OMIT 1 3 16 REM most disagreeable zero Fo2 OMIT -1 0 3 OMIT 0 2 1 OMIT -2 0 2 OMIT 0 0 20 OMIT 3 1 0 OMIT 1 2 0 OMIT -3 0 1 OMIT -3 1 1 OMIT 2 1 1 OMIT 2 1 2 OMIT 1 1 3 OMIT -1 2 3 OMIT 1 2 3 OMIT -1 1 5 OMIT 0 0 8 OMIT 0 1 8 OMIT 2 1 0 OMIT -2 1 3 OMIT -1 2 4 OMIT -2 0 6 OMIT 2 0 6 OMIT -1 3 6 OMIT 1 0 7 OMIT -1 0 9 OMIT 0 2 0 OMIT -1 2 1 OMIT 2 0 2 OMIT -2 1 2 OMIT 1 1 2 OMIT -1 2 6 OMIT 1 2 4 OMIT -5 3 1 OMIT -2 5 3 L.S. 12 BOND $H ACTA 66.1 FMAP 2 PLAN 10 WGHT 0.022800 19.217800 FVAR 0.57370 FE1 6 0.658648 0.340301 0.372517 11.00000 0.00655 0.00915 = 0.01498 0.00169 0.00070 0.00049 N1 3 0.449423 0.256828 0.366478 11.00000 0.00757 0.01082 = 0.01725 -0.00013 0.00065 0.00221 N2 3 0.629611 0.370408 0.324622 11.00000 0.01023 0.00976 = 0.01740 0.00168 0.00262 0.00101 N3 3 0.862735 0.425409 0.362272 11.00000 0.00749 0.00970 = 0.02346 0.00171 0.00139 0.00141 N4 3 0.579852 0.540034 0.388201 11.00000 0.00501 0.01274 = 0.01822 0.00258 0.00047 -0.00085 N5 3 0.692134 0.316441 0.420565 11.00000 0.00782 0.01094 = 0.01713 0.00069 0.00156 -0.00141 N6 3 0.741114 0.129928 0.372914 11.00000 0.00756 0.00815 = 0.02090 -0.00020 0.00136 -0.00131 C1 1 0.364336 0.192538 0.390851 11.00000 0.01051 0.01072 = 0.01997 0.00102 0.00097 0.00251 AFIX 43 H1A 2 0.401014 0.195129 0.414224 11.00000 -1.20000 AFIX 0 C2 1 0.223851 0.122047 0.383009 11.00000 0.01206 0.01243 = 0.02706 0.00042 0.00374 0.00270 AFIX 43 H2A 2 0.165615 0.078140 0.400756 11.00000 -1.20000 AFIX 0 C3 1 0.171013 0.117339 0.348881 11.00000 0.00726 0.01637 = 0.03258 -0.00351 -0.00024 -0.00141 AFIX 43 H3A 2 0.077298 0.067283 0.342889 11.00000 -1.20000 AFIX 0 C4 1 0.255365 0.185846 0.323608 11.00000 0.01197 0.01821 = 0.02302 -0.00333 -0.00326 0.00121 AFIX 43 H4A 2 0.219398 0.185542 0.300178 11.00000 -1.20000 AFIX 0 C5 1 0.393355 0.255022 0.333026 11.00000 0.01203 0.01343 = 0.01798 -0.00180 -0.00084 0.00336 C6 1 0.495687 0.328187 0.308837 11.00000 0.01188 0.01305 = 0.01781 0.00028 0.00059 0.00167 C7 1 0.466580 0.359378 0.273816 11.00000 0.02049 0.02104 = 0.01882 -0.00077 -0.00209 0.00233 AFIX 43 H7A 2 0.371075 0.332948 0.262929 11.00000 -1.20000 AFIX 0 C8 1 0.579579 0.429401 0.255392 11.00000 0.02811 0.02526 = 0.01620 0.00405 0.00318 0.00509 AFIX 43 H8A 2 0.562742 0.449375 0.231450 11.00000 -1.20000 AFIX 0 C9 1 0.718121 0.470963 0.271674 11.00000 0.02252 0.01956 = 0.02208 0.00491 0.00790 0.00419 AFIX 43 H9A 2 0.795611 0.520064 0.259091 11.00000 -1.20000 AFIX 0 C10 1 0.740955 0.439485 0.306512 11.00000 0.01225 0.01331 = 0.02123 0.00122 0.00553 0.00323 C11 1 0.877259 0.470320 0.328744 11.00000 0.00855 0.01304 = 0.02425 0.00130 0.00606 0.00187 C12 1 1.010735 0.537642 0.317312 11.00000 0.01524 0.01690 = 0.02957 0.00230 0.01117 -0.00134 AFIX 43 H12A 2 1.017967 0.569643 0.293985 11.00000 -1.20000 AFIX 0 C13 1 1.133059 0.556999 0.340743 11.00000 0.01089 0.01527 = 0.04250 0.00083 0.00974 -0.00234 AFIX 43 H13A 2 1.225093 0.603478 0.333617 11.00000 -1.20000 AFIX 0 C14 1 1.120535 0.508663 0.374297 11.00000 0.00649 0.01100 = 0.04322 0.00015 0.00126 0.00069 AFIX 43 H14A 2 1.204157 0.519867 0.390446 11.00000 -1.20000 AFIX 0 C15 1 0.983412 0.442922 0.384338 11.00000 0.00876 0.00912 = 0.02991 0.00290 0.00090 0.00226 AFIX 43 H15A 2 0.975197 0.409480 0.407537 11.00000 -1.20000 AFIX 0 C16 1 0.516267 0.651165 0.368521 11.00000 0.01173 0.01468 = 0.01872 0.00377 -0.00067 0.00054 AFIX 43 H16A 2 0.512153 0.638479 0.344144 11.00000 -1.20000 AFIX 0 C17 1 0.456457 0.783517 0.382342 11.00000 0.01279 0.01202 = 0.02545 0.00224 -0.00073 0.00355 AFIX 43 H17A 2 0.412804 0.859954 0.367653 11.00000 -1.20000 AFIX 0 C18 1 0.461267 0.802783 0.417992 11.00000 0.01584 0.01358 = 0.02775 -0.00320 0.00214 0.00339 AFIX 43 H18A 2 0.418542 0.891347 0.428042 11.00000 -1.20000 AFIX 0 C19 1 0.529426 0.690719 0.438718 11.00000 0.01621 0.01645 = 0.01952 -0.00187 0.00091 0.00230 AFIX 43 H19A 2 0.537368 0.703099 0.463084 11.00000 -1.20000 AFIX 0 C20 1 0.585634 0.560564 0.423244 11.00000 0.00737 0.01540 = 0.01882 0.00120 0.00053 -0.00177 C21 1 0.656456 0.430988 0.442171 11.00000 0.00786 0.01215 = 0.01926 -0.00005 -0.00054 0.00150 C22 1 0.687034 0.419352 0.477557 11.00000 0.01696 0.02060 = 0.01740 0.00044 0.00071 0.00322 AFIX 43 H22A 2 0.661297 0.500073 0.492678 11.00000 -1.20000 AFIX 0 C23 1 0.755596 0.287920 0.490206 11.00000 0.02135 0.02628 = 0.01549 0.00367 0.00091 0.00429 AFIX 43 H23A 2 0.778222 0.278456 0.514280 11.00000 -1.20000 AFIX 0 C24 1 0.792148 0.168492 0.467985 11.00000 0.01818 0.01770 = 0.02100 0.00687 0.00000 0.00309 AFIX 43 H24A 2 0.837876 0.077095 0.476589 11.00000 -1.20000 AFIX 0 C25 1 0.759268 0.188042 0.432829 11.00000 0.00965 0.01116 = 0.01941 0.00219 0.00114 -0.00013 C26 1 0.787771 0.080121 0.404979 11.00000 0.00872 0.01085 = 0.02093 0.00297 0.00291 -0.00127 C27 1 0.854720 -0.063514 0.409850 11.00000 0.01243 0.01118 = 0.02746 0.00653 0.00257 0.00088 AFIX 43 H27A 2 0.888539 -0.095999 0.432240 11.00000 -1.20000 AFIX 0 C28 1 0.870889 -0.157481 0.381544 11.00000 0.01534 0.01072 = 0.03494 0.00327 0.00316 -0.00071 AFIX 43 H28A 2 0.918037 -0.254688 0.384214 11.00000 -1.20000 AFIX 0 C29 1 0.817751 -0.108862 0.349167 11.00000 0.00956 0.01839 = 0.02929 -0.00403 0.00059 0.00030 AFIX 43 H29A 2 0.825184 -0.173602 0.329616 11.00000 -1.20000 AFIX 0 C30 1 0.753583 0.035692 0.345748 11.00000 0.00810 0.01303 = 0.02313 -0.00118 0.00144 -0.00041 AFIX 43 H30A 2 0.717480 0.068910 0.323580 11.00000 -1.20000 AFIX 0 CL1 5 0.786372 0.798887 0.523022 11.00000 0.01668 0.02111 = 0.01854 0.00401 -0.00126 -0.00105 CL2 5 0.449247 0.847264 0.276149 11.00000 0.02271 0.01978 = 0.02215 0.00495 -0.00166 -0.00525 O1 4 0.623270 0.777645 0.522364 11.00000 0.01338 0.07758 = 0.02959 -0.00417 -0.00013 -0.00394 O2 4 0.855797 0.682830 0.544594 11.00000 0.03622 0.02772 = 0.02675 0.00929 -0.00366 0.00909 O3 4 0.839532 0.785581 0.488393 11.00000 0.03237 0.03682 = 0.01910 0.00597 0.00405 -0.00505 O4 4 0.825779 0.946737 0.536622 11.00000 0.05701 0.01946 = 0.03168 -0.00013 -0.00373 -0.01057 O5 4 0.464914 1.010479 0.273009 11.00000 0.05024 0.01511 = 0.05362 0.00336 0.03017 0.00018 O6 4 0.313040 0.812256 0.295028 11.00000 0.03399 0.05441 = 0.05439 0.02182 0.01218 -0.01234 O7 4 0.439612 0.781039 0.242553 11.00000 0.05442 0.03766 = 0.02402 -0.00336 -0.01373 -0.01216 O8 4 0.582040 0.788918 0.294890 11.00000 0.03431 0.04868 = 0.02672 0.00635 -0.01396 0.00047 O1W 4 0.981192 0.384850 0.551355 11.00000 0.15213 0.23522 = 0.19837 -0.02768 0.00113 -0.00727 HKLF 4 REM cb9block in P2/n REM R1 = 0.0785 for 7493 Fo > 4sig(Fo) and 0.0878 for all 8630 data REM 433 parameters refined using 0 restraints END WGHT 0.0223 19.2684 REM Highest difference peak 1.946, deepest hole -1.321, 1-sigma level 0.128 Q1 1 0.6463 0.3505 0.3480 11.00000 0.05 1.10 Q2 1 0.6648 0.3411 0.3968 11.00000 0.05 0.96 Q3 1 0.4453 0.8353 0.2549 11.00000 0.05 0.72 Q4 1 0.7816 0.7987 0.5017 11.00000 0.05 0.65 Q5 1 0.3346 0.7408 0.2818 11.00000 0.05 0.60 Q6 1 0.6633 0.4102 0.4602 11.00000 0.05 0.58 Q7 1 0.3894 0.9773 0.2613 11.00000 0.05 0.55 Q8 1 0.8007 0.7966 0.5455 11.00000 0.05 0.55 Q9 1 0.5806 0.5647 0.4063 11.00000 0.05 0.54 Q10 1 0.5115 0.7556 0.2366 11.00000 0.05 0.51 ; 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4 -9 2307.87 60.39 9 -4 -9 625.44 33.30 9 4 -9 520.35 34.50 -9 4 9 578.14 42.50 -8 -4 9 629.54 48.90 8 -4 -9 601.54 45.30 8 -4 -9 620.64 32.40 -8 4 9 621.14 34.60 -8 4 9 695.93 43.60 7 -4 -9 84.89 27.10 -7 -4 9 49.80 22.90 -7 -4 9 32.60 15.60 7 -4 -9 41.70 16.20 7 -4 -9 36.80 13.50 -7 4 9 57.09 24.50 -7 4 9 46.70 15.00 7 4 -9 59.79 17.90 -6 -4 9 202.88 20.50 6 -4 -9 207.68 17.30 -6 -4 9 236.68 29.30 6 -4 -9 232.38 30.70 6 -4 -9 208.58 19.70 6 4 -9 216.18 17.00 -6 4 9 212.48 18.40 6 4 -9 222.48 20.20 -6 4 9 241.18 27.90 5 -4 -9 285.07 20.10 -5 -4 9 300.57 22.90 5 -4 -9 268.47 16.40 5 -4 -9 331.57 31.10 -5 -4 9 322.07 22.90 -5 -4 9 304.97 28.20 5 4 -9 269.07 19.90 -5 4 9 278.17 26.30 -5 4 9 266.47 17.90 4 -4 -9 593.24 33.70 4 -4 -9 582.64 22.40 -4 -4 9 642.84 28.30 -4 -4 9 613.54 27.90 4 4 -9 647.74 28.10 4 4 -9 618.74 26.00 -4 4 9 570.44 30.20 4 4 -9 551.94 23.50 -4 4 9 589.34 21.10 3 -4 -9 527.25 17.80 3 -4 -9 520.65 30.90 3 -4 -9 512.65 14.70 -3 -4 9 526.95 24.40 -3 -4 9 497.85 24.20 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23.50 -11 -5 9 483.35 60.79 11 -5 -9 503.55 43.60 -11 5 9 714.03 50.99 -10 -5 9 70.99 33.30 10 5 -9 76.39 21.10 -10 5 9 54.99 25.70 -9 -5 9 38.90 30.10 9 -5 -9 29.80 17.10 -9 5 9 47.80 24.40 8 -5 -9 23.10 13.70 8 -5 -9 23.30 17.70 -8 -5 9 28.40 23.20 8 5 -9 21.30 14.70 -8 5 9 24.30 14.60 -8 5 9 48.90 23.10 7 -5 -9 1444.56 75.39 7 -5 -9 1467.55 48.10 -7 -5 9 1300.07 60.69 7 -5 -9 1531.55 44.40 7 5 -9 1451.05 46.60 -7 5 9 1416.46 56.39 -7 5 9 1514.25 46.60 -6 -5 9 150.98 19.70 6 -5 -9 110.59 18.70 6 -5 -9 119.19 15.20 6 -5 -9 96.39 30.20 -6 -5 9 167.48 22.00 6 5 -9 157.38 19.60 -6 5 9 121.49 26.60 6 5 -9 159.68 18.70 -6 5 9 129.19 16.50 5 -5 -9 12.60 8.80 5 -5 -9 19.90 11.00 -5 -5 9 22.60 14.50 5 -5 -9 16.70 15.30 -5 -5 9 12.40 12.60 -5 5 9 17.30 9.90 5 5 -9 21.20 11.30 5 5 -9 17.40 12.80 -5 5 9 27.30 16.50 4 -5 -9 20.50 9.10 4 -5 -9 16.20 14.50 -4 -5 9 18.20 11.40 4 -5 -9 9.30 6.90 -4 -5 9 22.70 13.20 -4 5 9 27.70 14.40 -4 5 9 14.20 7.90 4 5 -9 37.20 15.00 4 5 -9 20.20 10.90 3 -5 -9 86.69 9.90 3 -5 -9 77.59 7.80 -3 -5 9 84.29 14.10 3 -5 -9 96.09 22.10 -3 -5 9 93.89 15.40 3 5 -9 83.69 14.00 3 5 -9 83.49 14.20 -3 5 9 79.59 8.10 3 5 -9 94.19 15.80 -2 -5 9 2542.25 49.20 2 -5 -9 2656.83 66.79 2 -5 -9 2554.94 25.00 2 -5 -9 2480.05 20.60 -2 -5 9 2603.84 51.39 2 5 -9 2545.55 43.40 -2 5 9 2396.96 22.50 2 5 -9 2663.83 54.39 -2 5 9 2349.06 49.60 2 5 -9 2500.45 44.00 1 -5 -9 501.65 32.70 -1 -5 9 505.35 22.80 1 5 -9 522.85 20.10 1 5 -9 538.65 28.10 1 5 -9 557.24 24.00 -1 5 9 481.55 23.70 1 5 -9 524.05 20.50 0 -5 9 161.28 12.50 0 -5 9 156.48 14.60 0 -5 -9 132.79 22.50 0 5 -9 164.08 12.30 0 5 -9 178.08 19.80 0 5 -9 157.48 14.60 0 5 9 142.49 15.80 -1 -5 -9 611.04 15.30 1 -5 9 636.34 23.60 1 -5 9 639.54 20.30 -1 -5 -9 625.84 34.40 -1 -5 -9 657.63 16.00 -1 5 -9 636.24 20.90 -1 5 -9 614.54 24.20 -1 5 -9 624.84 30.30 1 5 9 591.64 26.10 1 5 9 632.44 13.60 2 -5 9 130.89 11.90 -2 -5 -9 146.69 23.00 -2 -5 -9 115.99 10.90 2 -5 9 99.19 13.10 2 5 9 132.59 10.20 -2 5 -9 107.89 14.00 -3 -5 -9 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6 -9 180.48 37.60 10 6 9 230.78 25.90 -9 -7 9 39.40 34.20 -9 7 9 93.29 30.20 9 7 -9 53.19 20.00 8 -7 -9 137.89 42.50 -8 -7 9 101.39 40.80 8 7 -9 80.29 19.80 -8 7 9 58.89 23.40 -7 -7 9 717.13 62.49 -7 7 9 823.62 46.30 7 7 -9 822.92 38.10 6 -7 -9 189.58 38.70 6 7 -9 268.07 23.80 6 7 -9 244.68 31.80 -6 7 9 255.77 29.90 -5 -7 9 261.27 24.30 -5 -7 9 234.18 25.10 5 -7 -9 217.08 37.20 5 -7 -9 316.57 23.50 5 7 -9 293.97 22.50 5 7 -9 255.97 28.80 4 -7 -9 9.90 16.60 -4 -7 9 20.00 13.40 4 -7 -9 11.50 10.10 -4 -7 9 23.30 13.90 4 7 -9 18.70 12.90 -4 7 9 25.00 16.20 -3 -7 9 113.89 17.90 3 -7 -9 185.58 30.30 -3 -7 9 126.89 18.70 3 -7 -9 154.18 11.40 3 7 -9 133.49 20.70 -3 7 9 138.59 9.90 3 7 -9 106.89 21.40 3 7 -9 123.49 16.50 -2 -7 9 1551.64 45.00 2 -7 -9 1543.15 59.49 -2 -7 9 1618.44 46.40 2 7 -9 1556.54 40.20 -2 7 9 1413.96 44.50 2 7 -9 1519.15 44.70 2 7 -9 1585.34 50.79 1 -7 -9 88.59 26.90 1 7 -9 85.79 19.80 0 -7 9 80.69 14.60 0 -7 9 73.79 12.30 0 -7 -9 107.39 26.70 0 7 -9 98.79 19.40 0 7 -9 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1352.86 47.90 -10 -2 21 1056.79 79.39 10 2 -21 1370.66 47.80 -10 2 21 1214.78 62.59 9 -2 -21 21.80 18.90 -9 -2 21 9.10 22.90 -9 2 21 22.80 23.90 -8 -2 21 256.07 39.90 8 -2 -21 281.27 23.70 -8 2 21 266.47 34.80 8 2 -21 334.97 27.50 -8 2 21 289.37 26.60 7 -2 -21 77.59 16.20 -7 -2 21 94.29 27.80 7 -2 -21 67.69 28.10 -7 2 21 110.19 30.10 -7 2 21 91.59 17.70 6 -2 -21 9.20 10.90 6 -2 -21 15.30 23.80 -6 -2 21 6.10 12.20 -6 -2 21 7.90 14.70 -6 -2 21 24.40 17.60 -6 2 21 8.40 13.00 -6 2 21 14.60 12.60 -6 2 21 13.60 17.00 6 2 -21 5.60 12.70 6 2 -21 21.70 13.50 -5 -2 21 56.79 15.60 5 -2 -21 52.99 23.80 5 -2 -21 48.20 12.30 -5 -2 21 70.59 20.00 5 2 -21 45.60 17.60 -5 2 21 46.30 13.40 -5 2 21 53.59 13.80 -4 -2 21 1962.30 47.90 4 -2 -21 1987.10 64.19 -4 -2 21 1863.31 47.10 -4 -2 21 1804.52 46.60 4 -2 -21 1945.51 36.80 -4 2 21 1961.10 51.39 4 2 -21 1831.42 51.29 -4 2 21 1919.51 42.20 -4 2 21 2011.60 44.30 4 2 -21 1892.91 41.70 -3 -2 21 43.50 13.20 3 -2 -21 25.80 7.90 -3 -2 21 37.50 12.70 3 -2 -21 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2132.29 83.89 -3 -4 28 2173.48 56.59 -3 -4 28 2290.67 56.59 3 4 -28 2356.66 51.89 3 4 -28 2171.58 66.39 -3 4 28 2365.46 41.90 -3 4 28 2103.09 55.49 -3 4 28 2312.27 38.20 -2 -4 28 253.37 21.80 2 -4 -28 285.97 45.20 2 4 -28 247.98 29.30 -2 4 28 271.27 13.00 2 4 -28 265.67 22.30 -2 4 28 214.88 22.30 -2 4 28 264.67 14.10 1 -4 -28 33.70 26.20 -1 -4 28 21.00 11.80 -1 -4 28 18.30 13.00 -1 4 28 13.90 7.30 1 4 -28 22.40 15.80 -1 4 28 21.80 7.40 -1 4 28 22.80 13.70 1 4 -28 16.20 13.10 0 -4 28 90.49 16.70 0 -4 -28 98.89 10.90 0 -4 -28 131.99 39.30 0 -4 28 108.99 14.90 0 4 -28 92.89 17.90 0 4 28 93.49 10.40 0 4 28 116.79 18.70 0 4 28 101.59 13.40 0 4 -28 119.89 25.90 1 -4 28 967.70 35.00 1 -4 28 933.91 30.80 -1 -4 -28 947.81 59.99 -1 -4 -28 1003.10 28.10 1 4 28 1007.10 28.40 -1 4 -28 945.71 36.50 -1 4 -28 938.21 47.60 1 4 28 1008.40 24.60 1 4 28 850.31 34.40 2 -4 28 284.67 20.50 2 -4 28 297.87 22.60 -2 -4 -28 337.97 44.90 -2 -4 -28 294.77 18.60 2 4 28 299.67 16.70 2 4 28 280.67 23.40 -2 4 -28 325.37 32.00 2 4 28 300.07 19.20 -2 4 -28 333.17 26.30 -3 -4 -28 928.81 61.99 -3 -4 -28 942.21 32.20 3 -4 28 901.11 36.40 3 -4 28 963.90 32.90 -3 4 -28 985.60 39.50 -3 4 -28 878.31 47.60 3 4 28 960.00 29.90 3 4 28 924.21 37.80 -4 -4 -28 119.49 37.90 4 -4 28 151.78 18.00 -4 -4 -28 153.28 17.10 4 4 28 164.48 19.60 4 4 28 158.58 22.60 -4 4 -28 137.89 27.80 4 4 28 167.48 16.80 5 -4 28 189.48 20.10 -5 -4 -28 159.78 38.20 -5 -4 -28 199.48 20.60 5 4 28 212.68 20.00 -5 4 -28 163.18 28.20 5 4 28 178.78 25.20 5 4 28 195.88 22.90 6 -4 28 106.49 19.90 -6 -4 -28 79.89 29.40 -6 -4 -28 102.39 17.90 6 4 28 105.59 25.10 6 4 28 98.69 18.20 6 4 28 82.19 21.50 -6 4 -28 88.69 27.70 7 -4 28 9.10 15.30 7 4 28 1.60 14.10 -7 4 -28 8.90 17.90 7 4 28 11.80 18.50 8 -4 28 60.09 20.00 -8 4 -28 27.80 22.00 8 4 28 35.90 22.60 8 4 28 56.89 20.20 -9 -4 -28 96.99 37.30 9 -4 28 119.09 21.60 9 4 28 100.49 23.30 -9 -5 28 11.10 37.50 9 5 -28 16.20 19.60 -9 5 28 21.20 27.00 8 -5 -28 41.40 48.60 -8 5 28 116.19 32.70 8 5 -28 99.19 24.40 7 -5 -28 16.20 36.60 -7 5 28 58.49 26.50 7 5 -28 51.09 20.60 6 -5 -28 56.89 38.20 6 5 -28 64.39 19.10 6 5 -28 63.79 24.00 -6 5 28 71.79 26.10 5 -5 -28 212.88 53.39 -5 5 28 273.77 30.50 5 5 -28 240.88 24.80 5 5 -28 219.48 29.00 4 5 -28 99.09 18.10 4 5 -28 113.39 25.50 -4 5 28 94.79 23.30 3 -5 -28 21.30 25.30 3 5 -28 36.70 18.50 3 5 -28 49.40 20.80 -3 5 28 27.30 15.80 2 -5 -28 62.69 31.50 2 5 -28 48.90 15.50 2 5 -28 32.80 18.50 -2 5 28 46.70 19.80 1 -5 -28 23.60 26.60 -1 -5 28 15.40 13.00 -1 -5 28 38.00 13.80 1 5 -28 38.80 14.90 -1 5 28 21.70 14.30 1 5 -28 32.10 19.10 0 -5 28 29.50 14.10 0 -5 28 30.70 12.70 0 -5 -28 26.10 27.10 0 5 -28 32.60 15.60 0 5 -28 30.90 18.70 0 5 28 37.00 16.70 1 -5 28 198.58 19.20 -1 -5 -28 185.28 11.70 -1 -5 -28 222.48 44.10 1 -5 28 174.88 19.80 1 5 28 173.28 21.50 -1 5 -28 177.18 20.00 -1 5 -28 164.08 27.70 1 5 28 186.78 11.50 -2 -5 -28 575.74 56.29 -2 -5 -28 554.54 22.80 2 -5 28 549.25 26.50 2 5 28 521.35 30.80 -2 5 -28 565.84 31.60 -2 5 -28 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6 -28 509.95 31.20 3 -6 -28 77.79 37.70 3 6 -28 70.59 17.90 -3 6 28 100.89 21.80 -2 -6 28 114.09 17.20 2 -6 -28 96.09 36.70 2 6 -28 146.79 41.50 -2 6 28 101.29 22.20 -1 -6 28 454.15 24.80 1 -6 -28 459.45 50.99 -1 6 28 436.96 30.00 1 6 -28 428.46 36.90 0 -6 28 325.27 22.70 0 -6 -28 330.77 48.70 0 6 28 374.46 34.40 0 6 -28 314.77 32.90 -1 -6 -28 20.90 25.70 1 -6 28 18.00 13.30 1 6 28 33.20 16.80 2 -6 28 506.95 27.70 -2 -6 -28 452.55 57.09 -2 6 -28 461.95 38.10 2 6 28 475.75 31.70 -3 -6 -28 0.70 24.70 3 -6 28 11.90 12.90 3 6 28 8.50 17.10 -3 6 -28 19.10 18.00 -4 -6 -28 1.20 26.90 4 -6 28 19.90 13.40 -4 6 -28 11.40 17.80 4 6 28 35.40 19.50 5 -6 28 11.80 13.40 -5 -6 -28 -19.80 29.50 5 6 28 7.40 16.90 -5 6 -28 19.30 19.30 6 -6 28 346.57 26.30 6 6 28 346.57 33.60 7 -6 28 35.80 17.20 7 6 28 46.10 25.40 -7 6 -28 40.40 22.70 7 6 28 24.70 17.30 8 -6 28 51.69 19.30 -8 6 -28 46.30 25.40 8 6 28 58.89 22.90 8 6 28 71.99 28.90 8 -7 -28 -3.00 53.99 -8 7 28 17.50 23.90 8 7 -28 33.20 19.90 7 -7 -28 90.89 43.40 7 7 -28 155.08 24.00 -7 7 28 117.19 29.30 6 -7 -28 8.00 29.70 -6 7 28 15.80 18.80 6 7 -28 8.00 21.20 6 7 -28 4.40 17.60 5 -7 -28 13.20 28.40 5 7 -28 21.40 18.80 5 7 -28 34.00 18.70 4 -7 -28 165.28 50.49 -4 7 28 170.98 27.30 4 7 -28 185.28 25.30 4 7 -28 175.18 29.70 3 -7 -28 31.80 31.70 3 7 -28 22.30 19.30 -2 -7 28 279.17 23.10 2 7 -28 285.57 33.70 -2 7 28 274.47 28.20 -1 -7 28 43.20 14.80 1 -7 -28 17.20 26.70 1 7 -28 53.79 21.80 -1 7 28 40.90 17.50 0 -7 28 8.60 12.90 0 -7 -28 18.10 24.30 0 7 -28 21.20 17.70 -1 -7 -28 14.20 33.00 1 -7 28 7.60 11.90 1 7 28 7.70 16.70 -1 7 -28 19.30 19.00 -2 -7 -28 696.13 74.49 2 -7 28 643.64 30.40 2 7 28 581.34 35.70 -2 7 -28 583.84 40.40 -3 -7 -28 42.50 34.70 3 -7 28 47.20 15.30 -3 7 -28 49.30 21.50 3 7 28 52.49 22.10 4 -7 28 24.10 14.60 -4 -7 -28 8.60 30.40 4 7 28 22.30 18.10 -4 7 -28 32.20 21.10 5 -7 28 17.00 14.90 -5 -7 -28 -2.10 31.60 -5 7 -28 10.80 18.90 5 7 28 24.90 21.60 6 -7 28 26.30 17.10 -6 -7 -28 -3.30 38.90 -6 7 -28 14.00 17.60 6 7 28 22.70 22.30 7 -7 28 43.30 19.20 -7 7 -28 20.40 19.00 7 7 28 56.19 26.40 7 -8 -28 139.99 49.60 -7 8 28 162.68 31.40 7 8 -28 187.68 28.50 6 -8 -28 37.40 43.50 -6 8 28 23.80 20.00 6 8 -28 30.60 21.50 6 8 -28 26.80 19.00 5 -8 -28 610.34 65.69 -5 8 28 501.85 36.70 5 8 -28 561.34 33.70 5 8 -28 413.66 41.00 4 -8 -28 22.60 38.00 -4 8 28 25.70 19.10 4 8 -28 22.20 18.30 3 -8 -28 9.40 27.00 -3 -8 28 12.20 14.90 3 8 -28 12.20 18.20 -3 8 28 -3.20 15.10 -2 -8 28 31.00 15.40 -2 8 28 36.60 19.00 2 8 -28 30.90 18.90 -1 -8 28 2.10 12.60 1 -8 -28 17.20 34.80 -1 8 28 3.20 15.50 1 8 -28 22.10 19.90 0 -8 28 17.10 14.00 0 -8 -28 2.00 38.10 0 8 28 6.90 17.00 -1 -8 -28 298.97 48.80 1 -8 28 294.37 23.20 -1 8 -28 302.77 34.60 1 8 28 286.47 29.60 -2 -8 -28 8.80 31.20 2 -8 28 7.60 12.70 2 8 28 28.20 19.00 -2 8 -28 10.70 17.90 3 -8 28 196.38 22.50 -3 -8 -28 208.08 64.89 -3 8 -28 192.58 31.70 3 8 28 185.98 28.00 4 -8 28 3.30 14.50 -4 -8 -28 -7.50 36.10 -4 8 -28 5.30 18.60 4 8 28 6.10 19.50 5 -8 28 48.00 18.40 -5 -8 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-2 30 41.20 14.00 -3 -2 -30 39.40 13.40 -3 -2 -30 45.80 26.70 3 2 30 45.10 14.20 3 2 30 42.80 12.50 -3 2 -30 53.49 17.10 -3 2 -30 62.99 24.20 3 2 30 48.40 16.20 -4 -2 -30 461.45 43.50 4 -2 30 408.46 27.00 -4 -2 -30 445.16 25.40 4 -2 30 472.35 25.80 -4 2 -30 429.76 37.30 4 2 30 438.96 27.00 4 2 30 446.16 29.20 -4 2 -30 435.16 26.80 4 2 30 433.96 24.20 -5 -2 -30 41.20 24.20 5 -2 30 38.20 14.70 -5 -2 -30 48.40 15.20 5 2 30 54.39 18.00 5 2 30 34.90 16.70 -5 2 -30 43.70 20.40 5 2 30 33.40 13.60 -6 -2 -30 104.69 33.00 6 -2 30 101.39 18.10 6 2 30 106.39 25.20 -6 2 -30 88.69 27.40 7 -2 30 3.40 12.80 -7 2 -30 5.40 18.70 7 2 30 6.90 13.30 8 -2 30 5.30 15.30 -8 -2 -30 7.20 25.20 8 2 30 2.90 15.50 9 -2 30 89.69 21.90 -9 -2 -30 82.99 35.60 9 2 30 101.19 20.80 10 -3 -30 53.59 22.90 10 3 -30 40.80 20.20 -10 3 30 38.40 30.70 9 -3 -30 71.29 24.10 -9 -3 30 127.99 49.20 9 3 -30 90.99 27.50 -9 3 30 76.69 32.40 -8 -3 30 17.90 26.90 8 -3 -30 7.00 17.50 8 3 -30 14.40 16.70 -8 3 30 6.50 23.40 -7 -3 30 536.05 47.20 7 -3 -30 385.46 49.20 7 -3 -30 476.55 28.90 -7 3 30 397.06 40.40 7 3 -30 451.75 29.60 6 -3 -30 253.27 22.30 -6 -3 30 272.47 37.60 6 -3 -30 237.18 47.00 -6 3 30 271.17 26.30 6 3 -30 255.17 23.40 -6 3 30 233.78 29.80 6 3 -30 219.48 30.40 -6 3 30 286.57 25.80 5 -3 -30 512.55 53.39 5 -3 -30 446.96 24.40 -5 -3 30 420.36 32.20 -5 3 30 426.36 26.20 -5 3 30 450.55 35.50 5 3 -30 428.36 35.60 -5 3 30 500.75 28.90 5 3 -30 442.16 26.90 -4 -3 30 22.90 15.90 -4 -3 30 35.50 16.50 4 -3 -30 57.89 32.00 -4 -3 30 33.30 16.60 4 -3 -30 23.00 11.60 4 3 -30 37.30 15.30 -4 3 30 44.50 14.70 -4 3 30 28.40 16.60 4 3 -30 37.80 20.10 3 -3 -30 779.22 56.39 -3 -3 30 757.22 35.00 -3 -3 30 699.23 32.00 -3 -3 30 770.82 34.40 3 3 -30 740.93 30.30 -3 3 30 732.83 27.00 -3 3 30 723.13 22.70 3 3 -30 770.92 43.00 -3 3 30 704.23 35.20 -3 3 30 805.42 30.70 -2 -3 30 113.99 18.00 2 -3 -30 149.69 41.30 2 3 -30 119.19 18.30 2 3 -30 111.69 25.70 -2 3 30 114.59 12.70 -2 3 30 114.99 19.60 -2 3 30 111.39 10.70 -2 3 30 122.09 14.70 -1 -3 30 1949.70 42.80 -1 -3 30 2059.59 50.09 1 -3 -30 2015.50 77.39 1 3 -30 1884.71 49.90 1 3 -30 1839.32 61.79 -1 3 30 1942.11 32.60 -1 3 30 1888.51 48.00 -1 3 30 2018.30 38.70 0 -3 -30 6.00 27.00 0 -3 30 1.30 13.90 0 -3 -30 3.80 8.80 0 -3 30 7.50 10.80 0 3 30 1.40 6.20 0 3 30 -0.20 7.40 0 3 -30 2.30 17.20 0 3 -30 -2.40 11.60 0 3 30 4.30 10.10 -1 -3 -30 259.17 42.10 -1 -3 -30 233.98 17.60 1 -3 30 247.38 19.30 1 -3 30 241.58 20.80 -1 3 -30 248.28 22.40 1 3 30 227.58 14.60 1 3 30 228.68 17.00 -1 3 -30 213.18 29.60 1 3 30 229.68 20.50 -2 -3 -30 4.80 25.70 -2 -3 -30 2.20 10.00 2 -3 30 5.50 12.90 2 -3 30 3.80 10.60 2 3 30 0.10 10.90 2 3 30 6.30 8.40 -2 3 -30 -3.90 15.90 -2 3 -30 9.30 13.30 -3 -3 -30 428.76 24.00 -3 -3 -30 434.96 46.70 3 -3 30 404.56 23.20 3 -3 30 423.26 25.90 -3 3 -30 409.16 36.10 -3 3 -30 410.66 26.60 3 3 30 446.46 22.70 3 3 30 420.86 26.80 3 3 30 452.55 26.00 -4 -3 -30 571.14 49.70 -4 -3 -30 644.14 30.10 4 3 30 604.04 33.40 -4 3 -30 589.34 41.00 4 3 30 627.04 28.20 4 3 30 628.84 31.50 -5 -3 -30 15.60 21.90 -5 -3 -30 30.70 14.70 5 -3 30 34.20 14.60 5 3 30 48.70 19.90 5 3 30 38.60 16.90 5 3 30 37.70 14.40 -5 3 -30 32.10 18.90 -6 -3 -30 18.60 15.60 6 -3 30 9.60 13.70 -6 -3 -30 15.50 23.30 6 3 30 19.30 13.70 6 3 30 12.20 18.50 7 -3 30 69.79 19.40 -7 3 -30 75.99 28.50 7 3 30 80.89 19.30 7 3 30 62.39 26.90 8 -3 30 10.00 14.90 -8 3 -30 5.90 20.70 8 3 30 15.60 15.80 -9 -3 -30 40.60 28.30 9 -3 30 60.39 19.20 9 3 30 75.39 22.30 -9 -4 30 105.89 44.70 -9 4 30 156.08 37.50 9 4 -30 190.88 25.90 8 -4 -30 133.29 52.09 -8 -4 30 135.89 39.00 8 4 -30 165.68 23.80 -8 4 30 149.88 33.60 7 -4 -30 41.30 37.70 7 4 -30 76.89 19.90 -7 4 30 47.50 22.50 6 -4 -30 -4.70 33.80 6 4 -30 9.40 16.40 -6 4 30 5.70 18.50 6 4 -30 3.90 14.70 5 -4 -30 284.67 54.29 -5 4 30 313.27 31.30 5 4 -30 324.27 33.60 5 4 -30 335.97 26.60 4 -4 -30 24.10 29.60 -4 4 30 47.00 21.70 4 4 -30 48.50 16.20 -4 4 30 37.00 17.80 4 4 -30 38.40 18.60 -4 4 30 44.30 20.20 3 -4 -30 445.66 54.49 -3 -4 30 407.06 28.20 -3 4 30 467.95 19.50 -3 4 30 485.95 22.00 -3 4 30 436.56 29.90 3 4 -30 459.25 26.50 3 4 -30 449.36 37.20 -2 -4 30 6.10 12.80 2 -4 -30 16.60 28.00 -2 -4 30 1.50 11.10 -2 4 30 4.30 12.80 -2 4 30 5.70 7.70 2 4 -30 -1.60 11.60 -2 4 30 11.00 7.20 2 4 -30 14.50 18.00 -1 -4 30 789.72 33.70 -1 -4 30 798.82 30.50 1 -4 -30 819.32 60.89 -1 4 30 839.22 22.70 -1 4 30 843.72 24.60 1 4 -30 758.42 43.40 -1 4 30 737.43 34.40 1 4 -30 778.22 35.00 0 -4 30 5.00 12.60 0 -4 -30 20.80 25.30 0 -4 30 11.20 11.40 0 -4 -30 8.00 8.10 0 4 30 20.10 13.80 0 4 30 8.00 7.80 0 4 -30 5.90 12.30 0 4 -30 13.20 17.80 1 -4 30 9.10 11.60 -1 -4 -30 7.30 9.00 1 -4 30 10.90 11.00 -1 -4 -30 19.80 29.10 1 4 30 10.90 11.30 -1 4 -30 11.40 13.40 -1 4 -30 12.40 17.80 1 4 30 5.80 8.70 2 -4 30 51.79 16.70 -2 -4 -30 44.60 28.10 -2 -4 -30 43.60 12.40 2 -4 30 58.99 16.10 2 4 30 50.49 11.40 -2 4 -30 47.50 17.30 2 4 30 50.99 12.90 2 4 30 41.50 17.00 -2 4 -30 47.50 18.90 -3 -4 -30 20.50 28.10 3 4 30 16.00 14.00 3 4 30 20.40 12.50 3 4 30 10.30 9.60 -3 4 -30 8.60 17.10 -4 -4 -30 180.28 40.80 4 -4 30 190.38 19.40 -4 -4 -30 201.28 21.40 4 4 30 210.98 19.30 4 4 30 211.38 22.10 4 4 30 204.88 25.10 -5 -4 -30 43.80 26.80 -5 -4 -30 58.89 16.00 5 -4 30 64.19 16.20 5 4 30 72.49 16.60 5 4 30 63.89 22.20 5 4 30 74.89 19.60 -5 4 -30 70.89 24.40 -6 -4 -30 154.68 39.00 -6 -4 -30 158.78 20.80 6 -4 30 148.29 20.30 -6 4 -30 134.19 30.90 6 4 30 150.98 27.50 6 4 30 161.98 20.90 7 -4 30 275.37 24.90 7 4 30 274.97 33.60 7 4 30 288.57 27.50 -7 4 -30 254.47 34.90 8 -4 30 8.60 15.50 8 4 30 16.90 22.90 8 4 30 16.80 17.00 -8 4 -30 19.50 23.00 9 -4 30 80.19 22.30 -9 -4 -30 108.29 37.30 9 4 30 72.89 22.80 -9 -5 30 -3.20 33.30 -9 5 30 10.50 22.60 9 5 -30 26.40 21.00 8 5 -30 -0.70 16.30 -8 5 30 8.60 23.00 7 -5 -30 73.29 44.30 7 5 -30 135.49 22.60 -7 5 30 120.69 30.40 6 -5 -30 806.22 70.19 -6 5 30 962.20 48.30 6 5 -30 1075.59 44.10 6 5 -30 957.40 49.00 5 -5 -30 20.10 34.90 5 5 -30 20.90 15.60 5 5 -30 34.90 19.50 -5 5 30 34.90 19.90 4 -5 -30 116.59 38.90 -4 5 30 111.89 23.60 4 5 -30 105.49 19.20 4 5 -30 114.39 26.30 3 -5 -30 12.30 27.70 -3 5 30 23.90 17.80 3 5 -30 22.70 19.70 3 5 -30 17.50 14.30 2 -5 -30 297.67 58.69 -2 -5 30 301.97 21.80 -2 5 30 278.07 25.80 2 5 -30 251.37 31.40 -1 5 30 541.25 31.00 1 5 -30 533.55 39.10 0 -5 30 2.40 12.30 0 -5 -30 5.70 29.70 0 5 -30 -2.40 17.00 0 5 30 1.00 13.50 -1 -5 -30 72.99 32.80 1 5 30 67.79 19.00 2 -5 30 13.80 13.30 -2 -5 -30 18.50 31.40 -2 5 -30 4.10 16.00 2 5 30 13.30 13.50 3 -5 30 84.39 17.20 -3 5 -30 78.79 26.80 3 5 30 77.79 20.90 -4 -5 -30 194.18 64.89 4 -5 30 230.68 20.80 -4 5 -30 253.47 33.00 4 5 30 221.68 27.10 -5 -5 -30 -20.90 25.20 5 -5 30 4.90 12.40 -5 5 -30 4.40 16.70 5 5 30 -8.00 15.70 -6 -5 -30 127.29 44.50 6 -5 30 145.99 20.70 6 5 30 155.48 28.60 -6 5 -30 158.38 31.20 6 5 30 167.78 22.60 -7 -5 -30 5.10 31.40 7 -5 30 -3.00 14.20 7 5 30 -3.20 15.40 7 5 30 4.10 21.30 -7 5 -30 9.80 18.70 8 -5 30 98.79 20.60 -8 5 -30 105.29 34.00 8 5 30 100.59 29.70 8 5 30 130.79 24.40 8 -6 -30 -46.70 41.50 8 6 -30 24.00 20.50 -8 6 30 14.80 25.40 7 -6 -30 -25.80 43.80 -7 6 30 17.30 23.60 7 6 -30 7.60 18.30 6 -6 -30 -13.50 36.10 6 6 -30 0.80 15.40 6 6 -30 5.90 17.20 -6 6 30 22.30 18.40 5 -6 -30 -8.40 28.30 5 6 -30 17.40 17.00 5 6 -30 25.10 18.90 -5 6 30 6.50 18.00 4 -6 -30 258.97 56.89 4 6 -30 254.97 32.20 -4 6 30 254.97 28.20 4 6 -30 257.07 25.90 3 -6 -30 347.97 57.59 3 6 -30 340.47 35.90 -3 6 30 305.07 29.40 -2 -6 30 56.49 16.80 2 -6 -30 31.70 30.90 -2 6 30 66.89 21.70 2 6 -30 75.89 26.30 1 -6 -30 23.60 33.20 -1 -6 30 19.20 12.90 -1 6 30 14.60 15.70 1 6 -30 19.60 18.80 0 -6 30 100.89 17.60 0 -6 -30 98.39 39.20 0 6 -30 105.39 26.60 0 6 30 104.59 21.30 -1 -6 -30 39.00 31.10 1 -6 30 30.20 13.50 -1 6 -30 28.30 19.80 1 6 30 48.00 20.70 -2 -6 -30 225.08 47.00 2 -6 30 304.27 22.60 -2 6 -30 297.67 34.40 2 6 30 293.47 28.20 -3 -6 -30 93.59 36.70 3 -6 30 79.69 16.00 3 6 30 76.69 22.90 -3 6 -30 76.79 26.20 -4 -6 -30 278.07 52.89 4 -6 30 276.87 22.50 -4 6 -30 257.07 32.20 4 6 30 289.87 30.10 5 -6 30 18.30 15.00 -5 -6 -30 -17.60 29.00 5 6 30 17.30 20.10 -5 6 -30 23.30 21.30 6 -6 30 286.67 24.90 -6 -6 -30 252.77 53.49 6 6 30 275.37 31.90 -6 6 -30 253.97 35.70 7 -6 30 82.39 19.90 7 6 30 71.19 26.40 8 -6 30 11.50 17.50 8 6 30 -0.50 23.10 -8 6 -30 9.80 22.60 7 -7 -30 262.17 85.99 -7 7 30 158.08 31.30 7 7 -30 179.58 28.80 6 -7 -30 4.40 44.20 -6 7 30 16.80 20.70 6 7 -30 21.60 20.70 6 7 -30 10.10 16.70 5 -7 -30 29.80 47.00 5 7 -30 27.00 18.60 5 7 -30 20.00 19.10 -5 7 30 37.60 21.40 4 -7 -30 9.20 27.50 4 7 -30 22.40 17.20 4 7 -30 32.60 20.50 -4 7 30 27.80 17.10 3 -7 -30 19.60 28.30 -3 -7 30 21.90 15.10 -3 7 30 42.50 20.70 3 7 -30 28.10 19.70 2 -7 -30 261.87 45.10 -2 -7 30 291.87 23.00 -2 7 30 277.27 28.60 2 7 -30 244.58 32.70 1 -7 -30 28.20 26.90 -1 -7 30 61.39 16.70 -1 7 30 66.29 21.40 1 7 -30 61.09 22.30 0 -7 30 84.09 17.20 0 -7 -30 65.99 33.80 0 7 30 74.29 21.90 0 7 -30 85.09 27.00 -1 -7 -30 16.50 32.50 1 -7 30 19.00 13.20 1 7 30 21.80 17.60 2 -7 30 18.30 13.60 -2 -7 -30 1.50 34.70 -2 7 -30 15.80 19.90 2 7 30 22.80 18.20 3 -7 30 372.56 26.40 -3 7 -30 259.47 34.60 3 7 30 339.47 31.60 4 -7 30 5.60 13.20 -4 -7 -30 -17.90 36.30 -4 7 -30 4.80 16.70 4 7 30 13.40 19.90 5 -7 30 84.59 18.80 -5 -7 -30 63.49 47.40 5 7 30 82.49 26.10 -5 7 -30 89.49 26.60 -6 -7 -30 -11.40 37.60 6 -7 30 19.10 16.30 -6 7 -30 18.40 18.60 6 7 30 25.70 21.10 7 -7 30 48.50 20.00 -7 7 -30 73.49 26.90 7 7 30 71.69 27.60 6 -8 -30 25.80 37.10 -6 8 30 62.09 25.50 6 8 -30 49.70 22.20 6 8 -30 30.50 22.00 5 -8 -30 7.90 32.90 5 8 -30 4.30 19.70 5 8 -30 1.60 17.90 -5 8 30 9.60 17.80 -4 8 30 81.09 25.50 4 8 -30 85.69 27.80 -3 -8 30 0.80 14.90 3 8 -30 6.50 17.80 -3 8 30 11.10 16.40 -2 -8 30 27.20 17.10 2 -8 -30 33.50 28.70 2 8 -30 29.20 18.60 -2 8 30 20.30 18.50 -1 -8 30 14.90 14.00 1 -8 -30 18.30 41.10 -1 8 30 14.50 16.80 1 8 -30 26.40 19.30 0 -8 30 20.80 15.40 0 -8 -30 6.80 25.90 0 8 -30 15.60 17.00 1 -8 30 1052.69 39.10 -1 8 -30 809.22 47.20 1 8 30 888.11 42.40 2 -8 30 302.47 24.70 2 8 30 289.77 30.80 3 -8 30 44.70 17.40 -3 -8 -30 24.90 31.40 3 8 30 47.80 20.90 -3 8 -30 61.09 24.20 4 -8 30 35.60 16.90 -4 -8 -30 12.90 42.30 -4 8 -30 30.20 22.40 4 8 30 31.50 21.50 5 -8 30 106.89 21.00 -5 -8 -30 93.39 53.49 -5 8 -30 73.99 27.80 5 8 30 109.29 27.80 -6 -8 -30 -21.60 39.40 6 -8 30 11.10 16.80 6 8 30 16.70 22.50 -6 8 -30 12.70 19.20 5 -9 -30 70.99 44.10 -5 9 30 68.19 25.70 -4 -9 30 50.59 19.10 -4 9 30 65.49 24.60 4 9 -30 41.30 21.00 -3 -9 30 118.09 20.80 3 9 -30 88.29 28.10 -3 9 30 112.59 25.10 -2 -9 30 31.90 17.40 2 -9 -30 30.60 32.70 -2 9 30 22.00 17.50 2 9 -30 23.50 20.20 -1 -9 30 118.19 21.10 1 9 -30 81.59 28.00 -1 9 30 134.99 26.40 0 -9 -30 2.90 27.40 0 -9 30 9.00 15.00 0 9 -30 8.90 19.80 0 9 30 4.00 19.40 1 -9 30 4.10 15.60 -1 9 -30 14.80 18.00 1 9 30 6.00 18.40 2 -9 30 16.10 15.60 -2 -9 -30 9.50 43.80 -2 9 -30 5.10 19.50 2 9 30 1.30 18.80 -3 -9 -30 47.70 44.90 3 -9 30 72.39 20.90 3 9 30 48.40 21.20 -3 9 -30 80.09 25.40 4 -9 30 113.39 23.00 -4 -9 -30 110.29 46.10 4 9 30 109.99 27.90 -4 9 -30 130.19 31.00 -2 -10 30 96.09 20.20 2 -10 -30 87.09 36.90 -2 10 30 97.69 26.10 -1 -10 30 56.89 19.90 -1 10 30 63.79 25.00 0 -10 -30 179.28 54.39 0 -10 30 154.78 21.90 0 10 30 149.79 28.20 0 10 -30 139.29 30.50 1 -10 30 82.99 21.70 -1 -10 -30 55.19 33.60 1 10 30 87.79 26.80 2 -10 30 15.60 16.70 -2 -10 -30 35.00 40.30 2 10 30 9.30 19.50 -2 10 -30 24.10 21.20 10 0 -31 -0.40 16.70 -10 0 31 -20.90 28.50 -9 0 31 221.48 40.00 9 0 -31 230.88 26.80 -8 0 31 -1.40 20.00 8 0 -31 4.60 15.10 -7 0 31 858.81 49.10 7 0 -31 835.52 37.30 -6 0 31 15.90 14.40 -6 0 31 11.00 18.30 -6 0 31 8.90 15.80 6 0 -31 16.80 13.70 6 0 -31 3.50 20.90 5 0 -31 37.50 23.60 -5 0 31 46.40 16.50 -5 0 31 40.40 19.90 5 0 -31 44.80 15.40 -5 0 31 58.59 18.40 4 0 -31 11.00 10.80 -4 0 31 15.40 13.60 -4 0 31 19.40 13.90 4 0 -31 24.90 19.50 -4 0 31 7.60 12.30 -3 0 31 60.29 15.90 -3 0 31 66.59 16.60 3 0 -31 115.39 30.70 3 0 -31 74.99 14.50 -3 0 31 71.19 16.00 2 0 -31 1.00 10.00 -2 0 31 2.60 8.90 -2 0 31 1.00 10.10 2 0 -31 1.80 19.20 -2 0 31 0.40 8.40 1 0 -31 809.72 49.00 -1 0 31 715.13 24.60 -1 0 31 791.12 25.60 -1 0 31 791.42 30.10 1 0 -31 810.22 32.00 0 0 31 2.40 9.60 0 0 -31 2.90 10.70 0 0 31 -2.90 7.90 0 0 31 1.20 6.60 0 0 -31 6.70 17.80 -1 0 -31 1671.93 44.40 1 0 31 1667.43 37.40 1 0 31 1624.74 35.00 -1 0 -31 1664.63 63.19 1 0 31 1689.63 42.80 2 0 31 -0.70 8.60 2 0 31 6.30 11.00 2 0 31 2.10 8.80 -2 0 -31 -5.40 17.70 -2 0 -31 -0.90 10.10 -3 0 -31 53.59 22.20 3 0 31 62.09 12.70 -3 0 -31 47.00 14.00 3 0 31 60.69 14.90 3 0 31 61.69 15.00 4 0 31 7.70 10.60 -4 0 -31 5.30 12.20 -4 0 -31 7.80 18.60 4 0 31 8.50 12.20 4 0 31 11.80 12.70 -5 0 -31 1793.02 67.69 5 0 31 1872.91 47.50 -6 0 -31 6.70 19.20 6 0 31 5.00 12.50 -6 0 -31 10.30 19.60 -7 0 -31 106.79 32.20 -7 0 -31 105.89 29.60 7 0 31 101.39 20.10 8 0 31 -1.60 13.90 -8 0 -31 3.00 24.40 -9 0 -31 433.06 47.50 9 0 31 455.65 31.00 -10 -1 31 72.09 37.70 10 1 -31 66.69 21.40 -10 1 31 36.60 26.40 9 -1 -31 78.59 25.20 -9 -1 31 47.10 27.50 -9 1 31 90.19 37.20 9 1 -31 104.09 24.30 8 -1 -31 467.55 30.80 -8 -1 31 428.86 41.20 -8 1 31 376.56 41.00 8 1 -31 443.56 29.80 7 -1 -31 501.85 47.10 7 -1 -31 459.45 30.60 7 1 -31 482.15 29.40 -7 1 31 459.35 41.20 6 -1 -31 41.30 24.20 6 -1 -31 44.60 15.50 -6 -1 31 41.60 22.40 -6 1 31 40.10 17.90 -6 1 31 52.99 18.80 6 1 -31 47.10 23.30 6 1 -31 46.70 16.60 -6 1 31 40.60 21.00 -5 -1 31 1.10 12.90 -5 -1 31 9.30 13.30 5 -1 -31 6.50 11.20 -5 -1 31 2.40 15.60 5 -1 -31 -8.20 20.00 -5 1 31 10.10 13.60 5 1 -31 7.10 12.40 -5 1 31 7.60 12.80 5 1 -31 15.60 18.60 -5 1 31 8.60 15.80 -4 -1 31 98.39 21.30 -4 -1 31 96.49 18.30 4 -1 -31 102.69 15.70 -4 -1 31 92.09 18.50 4 -1 -31 97.59 34.50 4 1 -31 111.09 29.90 -4 1 31 110.79 18.50 -4 1 31 96.09 17.90 -4 1 31 95.79 21.10 4 1 -31 90.59 16.40 -3 -1 31 39.40 13.50 3 -1 -31 37.90 13.20 3 -1 -31 34.90 24.60 -3 -1 31 48.20 17.00 -3 -1 31 38.60 15.10 3 1 -31 33.80 20.00 -3 1 31 48.20 16.00 -3 1 31 39.20 14.20 3 1 -31 42.30 14.40 -3 1 31 56.39 17.00 -2 -1 31 7.50 8.60 2 -1 -31 11.00 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