data_mo_LizLaAuBi2square_0m _audit_creation_method SHELXL-2013 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'Au3 Bi4 La3' _chemical_formula_weight 1843.55 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'La' 'La' -0.2871 2.4523 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Au' 'Au' -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Bi' 'Bi' -4.1077 10.2566 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system cubic _space_group_IT_number 220 _space_group_name_H-M_alt 'I -4 3 d' _space_group_name_Hall 'I -4bd 2c 3' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' 'z, x, y' 'z+1/2, -x+1/2, -y' '-z+1/2, -x, y+1/2' '-z, x+1/2, -y+1/2' 'y, z, x' '-y, z+1/2, -x+1/2' 'y+1/2, -z+1/2, -x' '-y+1/2, -z, x+1/2' 'y+1/4, x+1/4, z+1/4' '-y+1/4, -x+3/4, z+3/4' 'y+3/4, -x+1/4, -z+3/4' '-y+3/4, x+3/4, -z+1/4' 'x+1/4, z+1/4, y+1/4' '-x+3/4, z+3/4, -y+1/4' '-x+1/4, -z+3/4, y+3/4' 'x+3/4, -z+1/4, -y+3/4' 'z+1/4, y+1/4, x+1/4' 'z+3/4, -y+1/4, -x+3/4' '-z+3/4, y+3/4, -x+1/4' '-z+1/4, -y+3/4, x+3/4' 'x+1/2, y+1/2, z+1/2' '-x+1, -y+1/2, z+1' '-x+1/2, y+1, -z+1' 'x+1, -y+1, -z+1/2' 'z+1/2, x+1/2, y+1/2' 'z+1, -x+1, -y+1/2' '-z+1, -x+1/2, y+1' '-z+1/2, x+1, -y+1' 'y+1/2, z+1/2, x+1/2' '-y+1/2, z+1, -x+1' 'y+1, -z+1, -x+1/2' '-y+1, -z+1/2, x+1' 'y+3/4, x+3/4, z+3/4' '-y+3/4, -x+5/4, z+5/4' 'y+5/4, -x+3/4, -z+5/4' '-y+5/4, x+5/4, -z+3/4' 'x+3/4, z+3/4, y+3/4' '-x+5/4, z+5/4, -y+3/4' '-x+3/4, -z+5/4, y+5/4' 'x+5/4, -z+3/4, -y+5/4' 'z+3/4, y+3/4, x+3/4' 'z+5/4, -y+3/4, -x+5/4' '-z+5/4, y+5/4, -x+3/4' '-z+3/4, -y+5/4, x+5/4' _cell_length_a 10.327(2) _cell_length_b 10.327(2) _cell_length_c 10.327(2) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 1101(1) _cell_formula_units_Z 4 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 2308 _cell_measurement_theta_min 4.84 _cell_measurement_theta_max 27.66 _exptl_crystal_description Irregular _exptl_crystal_colour Metallic _exptl_crystal_density_meas None _exptl_crystal_density_method 'Not measured' _exptl_crystal_density_diffrn 11.119 _exptl_crystal_F_000 2960 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.020 _exptl_crystal_size_mid 0.015 _exptl_crystal_size_min 0.010 _exptl_absorpt_coefficient_mu 114.743 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type Numerical _exptl_absorpt_correction_T_min 0.2660 _exptl_absorpt_correction_T_max 0.7457 _exptl_absorpt_process_details ? _exptl_special_details ; ? ; _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source ? _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 2241 _diffrn_reflns_av_unetI/netI 0.0360 _diffrn_reflns_av_R_equivalents 0.0509 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_l_min -9 _diffrn_reflns_limit_l_max 13 _diffrn_reflns_theta_min 4.835 _diffrn_reflns_theta_max 27.990 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.992 _diffrn_measured_fraction_theta_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.992 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.991 _diffrn_reflns_point_group_measured_fraction_full 1.000 _reflns_number_total 224 _reflns_number_gt 217 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.725 _reflns_Friedel_fraction_max 0.990 _reflns_Friedel_fraction_full 1.000 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Bruker APEX2' _computing_cell_refinement 'Bruker SAINT' _computing_data_reduction 'Bruker SAINT' _computing_structure_solution 'SHELXS-97 (Sheldrick 2008)' _computing_structure_refinement 'SHELXL-2013 (Sheldrick, 2013)' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _refine_special_details ; Refined as a 2-component inversion twin. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0318P)^2^+92.1057P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens . _refine_ls_hydrogen_treatment undef _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_abs_structure_details ; Refined as an inversion twin. ; _refine_ls_abs_structure_Flack 0.93(4) _chemical_absolute_configuration ? _refine_ls_number_reflns 224 _refine_ls_number_parameters 9 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0314 _refine_ls_R_factor_gt 0.0302 _refine_ls_wR_factor_ref 0.0717 _refine_ls_wR_factor_gt 0.0712 _refine_ls_goodness_of_fit_ref 1.279 _refine_ls_restrained_S_all 1.279 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Au1 Au 0.8750 0.0000 0.2500 0.0084(5) Uani 1 4 d S T P . . Bi2 Bi 0.08643(8) 0.08643(8) 0.08643(8) 0.0042(4) Uani 1 3 d S T P . . La3 La 0.3750 0.0000 0.2500 0.0062(6) Uani 1 4 d S T P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Au1 0.0096(6) 0.0096(6) 0.0060(9) 0.000 0.000 0.000 Bi2 0.0042(4) 0.0042(4) 0.0042(4) 0.0003(3) -0.0003(3) -0.0003(3) La3 0.0073(13) 0.0056(8) 0.0056(8) 0.000 0.000 0.000 _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Au1 Bi2 2.901(3) . ? Au1 Bi2 2.901(3) 26_554 ? Au1 Bi2 2.901(3) 39_454 ? Au1 Bi2 2.901(3) 16_545 ? Au1 La3 3.1620(6) . ? Au1 La3 3.1620(6) 30_455 ? Au1 La3 3.1620(6) 26_554 ? Au1 La3 3.1620(6) 29_544 ? Bi2 Au1 2.901(3) 33_554 ? Bi2 Au1 2.901(3) 7_564 ? Bi2 La3 3.540(4) 9_554 ? Bi2 La3 3.540(4) 2_664 ? Bi2 La3 3.540(4) 29_544 ? Bi2 La3 3.609(4) . ? Bi2 La3 3.609(4) 30_455 ? Bi2 La3 3.609(4) 10_655 ? La3 Au1 3.1620(6) 11_556 ? La3 Au1 3.1620(6) 3_655 ? La3 Au1 3.1620(6) 33_554 ? La3 Bi2 3.540(4) 2_665 ? La3 Bi2 3.540(4) 16_545 ? La3 Bi2 3.540(4) 38_554 ? La3 Bi2 3.540(4) 27_644 ? La3 Bi2 3.609(4) 28_455 ? La3 Bi2 3.609(4) 13 ? La3 Bi2 3.609(4) 39_454 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Bi2 Au1 Bi2 82.37(3) . 26_554 ? Bi2 Au1 Bi2 124.50(2) . 39_454 ? Bi2 Au1 Bi2 124.50(2) 26_554 39_454 ? Bi2 Au1 Bi2 124.50(2) . 16_545 ? Bi2 Au1 Bi2 124.50(2) 26_554 16_545 ? Bi2 Au1 Bi2 82.37(3) 39_454 16_545 ? Bi2 Au1 La3 72.918(17) . . ? Bi2 Au1 La3 155.259(18) 26_554 . ? Bi2 Au1 La3 72.919(17) 39_454 . ? Bi2 Au1 La3 71.29(3) 16_545 . ? Bi2 Au1 La3 72.918(17) . 30_455 ? Bi2 Au1 La3 71.29(3) 26_554 30_455 ? Bi2 Au1 La3 155.259(18) 39_454 30_455 ? Bi2 Au1 La3 72.919(17) 16_545 30_455 ? La3 Au1 La3 99.594(1) . 30_455 ? Bi2 Au1 La3 155.260(18) . 26_554 ? Bi2 Au1 La3 72.919(17) 26_554 26_554 ? Bi2 Au1 La3 71.29(3) 39_454 26_554 ? Bi2 Au1 La3 72.919(17) 16_545 26_554 ? La3 Au1 La3 131.8 . 26_554 ? La3 Au1 La3 99.6 30_455 26_554 ? Bi2 Au1 La3 71.29(3) . 29_544 ? Bi2 Au1 La3 72.919(17) 26_554 29_544 ? Bi2 Au1 La3 72.919(17) 39_454 29_544 ? Bi2 Au1 La3 155.259(18) 16_545 29_544 ? La3 Au1 La3 99.6 . 29_544 ? La3 Au1 La3 131.8 30_455 29_544 ? La3 Au1 La3 99.6 26_554 29_544 ? Au1 Bi2 Au1 112.69(2) 33_554 7_564 ? Au1 Bi2 Au1 112.69(2) 33_554 . ? Au1 Bi2 Au1 112.69(2) 7_564 . ? Au1 Bi2 La3 139.90(3) 33_554 9_554 ? Au1 Bi2 La3 57.785(9) 7_564 9_554 ? Au1 Bi2 La3 106.151(14) . 9_554 ? Au1 Bi2 La3 57.785(9) 33_554 2_664 ? Au1 Bi2 La3 106.151(14) 7_564 2_664 ? Au1 Bi2 La3 139.90(3) . 2_664 ? La3 Bi2 La3 86.04(3) 9_554 2_664 ? Au1 Bi2 La3 106.151(14) 33_554 29_544 ? Au1 Bi2 La3 139.90(3) 7_564 29_544 ? Au1 Bi2 La3 57.785(9) . 29_544 ? La3 Bi2 La3 86.04(3) 9_554 29_544 ? La3 Bi2 La3 86.04(3) 2_664 29_544 ? Au1 Bi2 La3 56.871(15) 33_554 . ? Au1 Bi2 La3 124.57(5) 7_564 . ? Au1 Bi2 La3 56.871(15) . . ? La3 Bi2 La3 162.986(3) 9_554 . ? La3 Bi2 La3 107.703(1) 2_664 . ? La3 Bi2 La3 84.998(1) 29_544 . ? Au1 Bi2 La3 124.57(5) 33_554 30_455 ? Au1 Bi2 La3 56.871(15) 7_564 30_455 ? Au1 Bi2 La3 56.871(15) . 30_455 ? La3 Bi2 La3 84.998(1) 9_554 30_455 ? La3 Bi2 La3 162.986(3) 2_664 30_455 ? La3 Bi2 La3 107.703(1) 29_544 30_455 ? La3 Bi2 La3 84.00(3) . 30_455 ? Au1 Bi2 La3 56.871(15) 33_554 10_655 ? Au1 Bi2 La3 56.871(15) 7_564 10_655 ? Au1 Bi2 La3 124.57(5) . 10_655 ? La3 Bi2 La3 107.704(1) 9_554 10_655 ? La3 Bi2 La3 84.998(1) 2_664 10_655 ? La3 Bi2 La3 162.986(3) 29_544 10_655 ? La3 Bi2 La3 84.00(3) . 10_655 ? La3 Bi2 La3 84.00(3) 30_455 10_655 ? Au1 La3 Au1 99.594(1) . 11_556 ? Au1 La3 Au1 131.8 . 3_655 ? Au1 La3 Au1 99.6 11_556 3_655 ? Au1 La3 Au1 99.6 . 33_554 ? Au1 La3 Au1 131.8 11_556 33_554 ? Au1 La3 Au1 99.6 3_655 33_554 ? Au1 La3 Bi2 138.106(17) . 2_665 ? Au1 La3 Bi2 50.923(18) 11_556 2_665 ? Au1 La3 Bi2 86.732(12) 3_655 2_665 ? Au1 La3 Bi2 86.732(13) 33_554 2_665 ? Au1 La3 Bi2 50.923(18) . 16_545 ? Au1 La3 Bi2 86.732(12) 11_556 16_545 ? Au1 La3 Bi2 86.732(12) 3_655 16_545 ? Au1 La3 Bi2 138.106(17) 33_554 16_545 ? Bi2 La3 Bi2 135.130(3) 2_665 16_545 ? Au1 La3 Bi2 86.732(12) . 38_554 ? Au1 La3 Bi2 138.106(17) 11_556 38_554 ? Au1 La3 Bi2 50.923(18) 3_655 38_554 ? Au1 La3 Bi2 86.732(12) 33_554 38_554 ? Bi2 La3 Bi2 135.130(3) 2_665 38_554 ? Bi2 La3 Bi2 65.328(5) 16_545 38_554 ? Au1 La3 Bi2 86.732(12) . 27_644 ? Au1 La3 Bi2 86.732(12) 11_556 27_644 ? Au1 La3 Bi2 138.106(17) 3_655 27_644 ? Au1 La3 Bi2 50.923(18) 33_554 27_644 ? Bi2 La3 Bi2 65.328(5) 2_665 27_644 ? Bi2 La3 Bi2 135.130(3) 16_545 27_644 ? Bi2 La3 Bi2 135.130(3) 38_554 27_644 ? Au1 La3 Bi2 50.210(2) . . ? Au1 La3 Bi2 136.893(16) 11_556 . ? Au1 La3 Bi2 123.358(17) 3_655 . ? Au1 La3 Bi2 50.210(2) 33_554 . ? Bi2 La3 Bi2 127.924(17) 2_665 . ? Bi2 La3 Bi2 91.82(3) 16_545 . ? Bi2 La3 Bi2 77.430(1) 38_554 . ? Bi2 La3 Bi2 64.608(15) 27_644 . ? Au1 La3 Bi2 123.358(17) . 28_455 ? Au1 La3 Bi2 50.210(2) 11_556 28_455 ? Au1 La3 Bi2 50.210(2) 3_655 28_455 ? Au1 La3 Bi2 136.892(16) 33_554 28_455 ? Bi2 La3 Bi2 64.608(15) 2_665 28_455 ? Bi2 La3 Bi2 77.431(1) 16_545 28_455 ? Bi2 La3 Bi2 91.82(3) 38_554 28_455 ? Bi2 La3 Bi2 127.924(17) 27_644 28_455 ? Bi2 La3 Bi2 167.33(3) . 28_455 ? Au1 La3 Bi2 136.892(16) . 13 ? Au1 La3 Bi2 123.358(17) 11_556 13 ? Au1 La3 Bi2 50.210(2) 3_655 13 ? Au1 La3 Bi2 50.210(2) 33_554 13 ? Bi2 La3 Bi2 77.431(1) 2_665 13 ? Bi2 La3 Bi2 127.924(17) 16_545 13 ? Bi2 La3 Bi2 64.608(15) 38_554 13 ? Bi2 La3 Bi2 91.82(3) 27_644 13 ? Bi2 La3 Bi2 90.698(4) . 13 ? Bi2 La3 Bi2 90.698(3) 28_455 13 ? Au1 La3 Bi2 50.210(2) . 39_454 ? Au1 La3 Bi2 50.210(2) 11_556 39_454 ? Au1 La3 Bi2 136.892(16) 3_655 39_454 ? Au1 La3 Bi2 123.358(17) 33_554 39_454 ? Bi2 La3 Bi2 91.82(3) 2_665 39_454 ? Bi2 La3 Bi2 64.608(15) 16_545 39_454 ? Bi2 La3 Bi2 127.924(17) 38_554 39_454 ? Bi2 La3 Bi2 77.431(1) 27_644 39_454 ? Bi2 La3 Bi2 90.698(3) . 39_454 ? Bi2 La3 Bi2 90.698(3) 28_455 39_454 ? Bi2 La3 Bi2 167.33(3) 13 39_454 ? _refine_diff_density_max 2.204 _refine_diff_density_min -3.839 _refine_diff_density_rms 0.768 _shelxl_version_number 2013-4 _shelx_res_file ; TITL mo_LizLaAuBi2square_0m in I-43d CELL 0.71073 10.32670 10.32670 10.32670 90.0000 90.0000 90.0000 ZERR 4.00 0.01180 0.01180 0.01180 0.0000 0.0000 0.0000 LATT -2 SYMM 0.5-X, -Y, 0.5+Z SYMM -X, 0.5+Y, 0.5-Z SYMM 0.5+X, 0.5-Y, -Z SYMM Z, X, Y SYMM 0.5+Z, 0.5-X, -Y SYMM 0.5-Z, -X, 0.5+Y SYMM -Z, 0.5+X, 0.5-Y SYMM Y, Z, X SYMM -Y, 0.5+Z, 0.5-X SYMM 0.5+Y, 0.5-Z, -X SYMM 0.5-Y, -Z, 0.5+X SYMM 0.25+Y, 0.25+X, 0.25+Z SYMM 0.25-Y, 0.75-X, 0.75+Z SYMM 0.75+Y, 0.25-X, 0.75-Z SYMM 0.75-Y, 0.75+X, 0.25-Z SYMM 0.25+X, 0.25+Z, 0.25+Y SYMM 0.75-X, 0.75+Z, 0.25-Y SYMM 0.25-X, 0.75-Z, 0.75+Y SYMM 0.75+X, 0.25-Z, 0.75-Y SYMM 0.25+Z, 0.25+Y, 0.25+X SYMM 0.75+Z, 0.25-Y, 0.75-X SYMM 0.75-Z, 0.75+Y, 0.25-X SYMM 0.25-Z, 0.75-Y, 0.75+X SFAC LA AU BI UNIT 12 12 16 TEMP 23.000 L.S. 10 ACTA TWIN WGHT 0.031800 92.105698 BASF 0.92903 FVAR 0.02547 MOLE 1 AU1 2 0.500000 0.250000 0.125000 10.25000 0.00956 0.00956 = 0.00600 0.00000 0.00000 0.00000 BI2 3 0.586431 0.413569 -0.086431 10.33333 0.00423 0.00423 = 0.00423 0.00030 -0.00030 -0.00030 LA3 1 0.625000 0.500000 0.250000 10.25000 0.00733 0.00563 = 0.00563 0.00000 0.00000 0.00000 HKLF 4 REM mo_LizLaAuBi2square_0m in I-43d REM R1 = 0.0302 for 217 Fo > 4sig(Fo) and 0.0314 for all 224 data REM 9 parameters refined using 0 restraints END WGHT 0.0317 92.9658 REM Highest difference peak 2.204, deepest hole -3.839, 1-sigma level 0.768 Q1 1 0.5580 0.6518 0.1605 11.00000 0.05 2.20 Q2 1 0.4300 0.3161 -0.1231 11.00000 0.05 2.02 Q3 1 0.6208 0.6579 0.2376 11.00000 0.05 1.82 Q4 1 0.6519 0.5435 -0.1463 11.00000 0.05 1.61 Q5 1 0.6590 0.5470 0.3926 11.00000 0.05 1.58 Q6 1 0.5000 0.2500 -0.0320 10.50000 0.05 1.49 Q7 1 0.6319 0.3402 -0.0006 11.00000 0.05 1.43 Q8 1 0.5663 0.4076 -0.2292 11.00000 0.05 1.40 Q9 1 0.4880 0.3294 -0.1840 11.00000 0.05 1.26 Q10 1 0.5411 0.1197 0.1044 11.00000 0.05 1.25 Q11 1 0.6333 0.5189 0.0979 11.00000 0.05 1.22 Q12 1 0.5972 0.2917 0.1815 11.00000 0.05 1.05 Q13 1 0.5441 0.3930 0.1066 11.00000 0.05 0.94 Q14 1 0.4484 0.5238 0.3012 11.00000 0.05 0.92 Q15 1 0.6629 0.4170 -0.0367 11.00000 0.05 0.83 Q16 1 0.4642 0.5000 0.2500 10.50000 0.05 0.83 Q17 1 0.5276 0.5625 0.1678 11.00000 0.05 0.78 Q18 1 0.4807 0.4890 -0.0616 11.00000 0.05 0.74 Q19 1 0.5577 0.5454 0.1574 11.00000 0.05 0.70 Q20 1 0.5141 0.4724 0.0271 11.00000 0.05 0.69 ; _shelx_res_checksum 90902 _shelx_hkl_file ; -1 -1 0 0.15 0.33 -1 -1 0 0.22 0.45 -1 0 1 1.13 0.33 -1 0 1 0.37 0.17 -1 1 0 0.23 0.18 0 -1 -1 0.61 0.31 0 -1 1 0.63 0.37 1 -1 0 0.56 0.17 -2 0 0 0.22 0.42 0 -2 0 0.55 0.37 0 0 -2 0.57 0.34 0 0 2 1.04 0.65 2 0 0 0.85 0.21 -2 -1 -1 72.75 6.33 1 -1 2 76.50 6.45 -2 1 1 76.32 6.29 -1 -2 -1 69.97 6.28 1 -2 1 71.64 6.37 -1 -1 2 79.76 6.33 -1 2 -1 94.00 6.30 1 -2 -1 95.97 6.33 1 1 2 97.43 6.39 -1 -1 2 72.89 6.74 -2 0 2 38.20 2.93 -2 2 0 34.86 2.68 0 -2 -2 32.92 2.86 0 -2 2 29.22 2.58 2 -2 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