data_compound_4.CHCl3 _audit_creation_date 09-02-01 _audit_creation_method 'from The Personal SDP version 2.1.1' _chemical_formula_sum 'C37 H31 Cl4 N O3 P2 Pt' _chemical_formula_weight 936.51 _computing_data_collection 'APEX II (Bruker)' _computing_cell_refinement 'APEX II (Bruker)' _computing_data_reduction 'SAINT (Bruker)' _computing_structure_solution ; SHELXS-86 (Sheldrick, 1986) as implemented in The Personal SDP ; _computing_structure_refinement ; Full-matrix least-squares (The Personal SDP, 1991) ; _cell_length_a 11.1572(5) _cell_length_b 11.6921(5) _cell_length_c 14.6755(7) _cell_angle_alpha 92.144(1) _cell_angle_beta 96.166(1) _cell_angle_gamma 106.110(1) _cell_volume 1824.1(1) _cell_formula_units_Z 2 _cell_measurement_temperature 296 _cell_measurement_reflns_used 9467 _cell_measurement_theta_min 3 _cell_measurement_theta_max 29 _symmetry_cell_setting 'triclinic' _symmetry_space_group_name_H-M 'P -1' loop_ _symmetry_equiv_pos_as_xyz '+x,+y,+z' '-x,-y,-z' _exptl_crystal_description 'bipyramid' _exptl_crystal_colour 'colourless' _exptl_crystal_size_max 0.250 _exptl_crystal_size_mid 0.200 _exptl_crystal_size_min 0.120 _exptl_crystal_density_diffrn 1.705 _exptl_crystal_F_000 920 _exptl_absorpt_coefficient_mu 4.304 _exptl_absorpt_correction_type 'empirical' _exptl_absorpt_process_details ; SADABS ; _exptl_absorpt_correction_T_min 0.594 _exptl_absorpt_correction_T_max 1.000 _diffrn_ambient_temperature 296 _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type 'Mo-K\a' _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_monochromator 'graphite' _diffrn_radiation_detector 'APEX II CCD area detector' _diffrn_measurement_device 'APEX II (Bruker)' _diffrn_measurement_method 'omega' _diffrn_standards_number 175 _diffrn_standards_decay_% 0.00 _diffrn_reflns_number_total 60430 _diffrn_reflns_number_independent 11538 _R_int 0.0246 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_theta_min 3.00 _diffrn_reflns_theta_max 29.00 _total_number_of_frames 3013 _time_per_frame_seconds 20 _frame_width_degrees 0.50 _detector_sample_distance_cm 5.00 _diffrn_reflns_reduction_process 'SAINT' loop_ _atom_type_symbol _atom_type_oxidation_number _atom_type_number_in_cell _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Pt 0 2 -2.3520 8.3880 'International Tables Vol IV Table 2.2A' Cl 0 8 0.1320 0.1590 'International Tables Vol IV Table 2.2A' P 0 4 0.0900 0.0950 'International Tables Vol IV Table 2.2A' O 0 6 0.0080 0.0060 'International Tables Vol IV Table 2.2A' N 0 2 0.0040 0.0030 'International Tables Vol IV Table 2.2A' C 0 74 0.0020 0.0020 'International Tables Vol IV Table 2.2A' H 0 62 0.0000 0.0000 'International Tables Vol IV Table 2.2A' loop_ _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_occupancy _atom_site_U_iso_or_equiv _atom_site_thermal_displace_type _atom_site_type_symbol Pt 0.293639(6) -.035970(6) 0.253098(5) 1.00 0.03032(2) Uani Pt Cl1 0.14073(5) 0.06817(5) 0.25934(5) 1.00 0.0548(2) Uani Cl Cl2 0.24580(7) 0.63825(7) 0.57966(5) 1.00 0.0755(3) Uani Cl Cl3 0.2762(2) 0.5285(2) 0.7479(1) 0.50 0.0987(8) Uani Cl Cl4 0.4386(2) 0.5196(2) 0.5930(2) 0.50 0.116(1) Uani Cl Cl5 0.2346(4) 0.5503(3) 0.7554(2) 0.25 0.110(2) Uani Cl Cl6 0.3967(4) 0.4968(3) 0.6291(4) 0.25 0.138(2) Uani Cl Cl7 0.3089(4) 0.5093(3) 0.7360(3) 0.25 0.106(2) Uani Cl Cl8 0.4625(3) 0.5463(3) 0.6329(3) 0.25 0.097(2) Uani Cl P1 0.45258(4) -0.11723(4) 0.24068(3) 1.00 0.0305(2) Uani P P2 0.14099(4) -0.20312(4) 0.26793(3) 1.00 0.0329(2) Uani P O1 0.4184(1) 0.1352(1) 0.24683(9) 1.00 0.0394(5) Uani O O2 0.3664(2) 0.1040(2) 0.1002(1) 1.00 0.0748(9) Uani O O3 0.4645(2) 0.2799(2) 0.1610(1) 1.00 0.091(1) Uani O N 0.4152(2) 0.1724(2) 0.1687(1) 1.00 0.0489(8) Uani N C1 0.3541(3) 0.6064(2) 0.6630(2) 1.00 0.076(1) Uani C C111 0.5922(2) -0.0154(2) 0.2023(1) 1.00 0.0355(7) Uani C C112 0.6659(2) 0.0777(2) 0.2635(2) 1.00 0.0482(9) Uani C C113 0.7774(2) 0.1512(2) 0.2405(2) 1.00 0.057(1) Uani C C114 0.8170(2) 0.1316(2) 0.1574(2) 1.00 0.058(1) Uani C C115 0.7444(2) 0.0406(2) 0.0963(2) 1.00 0.0543(9) Uani C C116 0.6318(2) -0.0324(2) 0.1179(1) 1.00 0.0437(8) Uani C C121 0.5218(2) -0.1555(2) 0.3492(1) 1.00 0.0363(7) Uani C C122 0.6337(2) -0.1860(2) 0.3530(2) 1.00 0.0517(9) Uani C C123 0.6924(2) -0.2061(2) 0.4359(2) 1.00 0.065(1) Uani C C124 0.6413(3) -0.1935(2) 0.5161(2) 1.00 0.064(1) Uani C C125 0.5323(2) -0.1611(2) 0.5132(2) 1.00 0.055(1) Uani C C126 0.4708(2) -0.1423(2) 0.4301(1) 1.00 0.0429(8) Uani C C131 0.4135(2) -0.2443(2) 0.1571(1) 1.00 0.0346(7) Uani C C132 0.4425(2) -0.3503(2) 0.1739(2) 1.00 0.0422(8) Uani C C133 0.4150(2) -0.4405(2) 0.1040(2) 1.00 0.057(1) Uani C C134 0.3615(3) -0.4241(2) 0.0182(2) 1.00 0.064(1) Uani C C135 0.3320(2) -0.3193(2) 0.0015(2) 1.00 0.059(1) Uani C C136 0.3570(2) -0.2296(2) 0.0708(1) 1.00 0.0448(8) Uani C C211 0.1620(2) -0.3519(2) 0.2537(1) 1.00 0.0380(7) Uani C C212 0.2260(2) -0.3946(2) 0.3260(2) 1.00 0.0476(8) Uani C C213 0.2343(2) -0.5105(2) 0.3194(2) 1.00 0.065(1) Uani C C214 0.1793(3) -0.5849(2) 0.2423(2) 1.00 0.077(1) Uani C C215 0.1184(3) -0.5433(2) 0.1708(2) 1.00 0.075(1) Uani C C216 0.1085(2) -0.4272(2) 0.1758(2) 1.00 0.053(1) Uani C C221 0.0850(2) -0.2080(2) 0.3809(1) 1.00 0.0365(7) Uani C C222 0.0080(2) -0.3141(2) 0.4071(1) 1.00 0.0420(8) Uani C C223 -0.0355(2) -0.3184(2) 0.4926(2) 1.00 0.0491(9) Uani C C224 -0.0018(2) -0.2175(2) 0.5523(2) 1.00 0.0541(9) Uani C C225 0.0750(2) -0.1135(2) 0.5275(2) 1.00 0.0550(9) Uani C C226 0.1196(2) -0.1074(2) 0.4417(2) 1.00 0.0467(9) Uani C C231 0.0093(2) -0.2093(2) 0.1813(1) 1.00 0.0362(7) Uani C C232 -0.1143(2) -0.2556(2) 0.1973(2) 1.00 0.0463(8) Uani C C233 -0.2120(2) -0.2667(2) 0.1265(2) 1.00 0.058(1) Uani C C234 -0.1870(2) -0.2315(2) 0.0416(2) 1.00 0.058(1) Uani C C235 -0.0647(2) -0.1827(2) 0.0257(2) 1.00 0.061(1) Uani C C236 0.0337(2) -0.1710(2) 0.0949(2) 1.00 0.054(1) Uani C H1 0.6390 0.0911 0.3227 1.00 0.0531 Uiso H H2 0.8276 0.2166 0.2831 1.00 0.0624 Uiso H H3 0.8960 0.1819 0.1419 1.00 0.0638 Uiso H H4 0.7722 0.0274 0.0375 1.00 0.0598 Uiso H H5 0.5806 -0.0956 0.0739 1.00 0.0481 Uiso H H6 0.6708 -0.1933 0.2970 1.00 0.0568 Uiso H H7 0.7697 -0.2291 0.4380 1.00 0.0710 Uiso H H8 0.6827 -0.2076 0.5744 1.00 0.0709 Uiso H H9 0.4975 -0.1512 0.5698 1.00 0.0606 Uiso H H10 0.3931 -0.1202 0.4285 1.00 0.0472 Uiso H H11 0.4816 -0.3612 0.2340 1.00 0.0464 Uiso H H12 0.4334 -0.5153 0.1157 1.00 0.0631 Uiso H H13 0.3446 -0.4867 -0.0307 1.00 0.0709 Uiso H H14 0.2938 -0.3085 -0.0590 1.00 0.0653 Uiso H H15 0.3350 -0.1564 0.0593 1.00 0.0494 Uiso H H16 0.2645 -0.3430 0.3808 1.00 0.0523 Uiso H H17 0.2792 -0.5395 0.3695 1.00 0.0709 Uiso H H18 0.1838 -0.6666 0.2387 1.00 0.0850 Uiso H H19 0.0816 -0.5953 0.1159 1.00 0.0821 Uiso H H20 0.0642 -0.3990 0.1249 1.00 0.0587 Uiso H H21 -0.0153 -0.3853 0.3656 1.00 0.0462 Uiso H H22 -0.0897 -0.3923 0.5103 1.00 0.0540 Uiso H H23 -0.0325 -0.2204 0.6118 1.00 0.0594 Uiso H H24 0.0988 -0.0429 0.5698 1.00 0.0604 Uiso H H25 0.1744 -0.0332 0.4249 1.00 0.0514 Uiso H H26 -0.1332 -0.2805 0.2578 1.00 0.0510 Uiso H H27 -0.2984 -0.2998 0.1380 1.00 0.0635 Uiso H H28 -0.2553 -0.2406 -0.0074 1.00 0.0637 Uiso H H29 -0.0471 -0.1563 -0.0346 1.00 0.0673 Uiso H H30 0.1196 -0.1360 0.0830 1.00 0.0593 Uiso H loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 _atom_site_aniso_type_symbol Pt 0.02974(3) 0.02764(3) 0.03328(3) 0.00824(2) 0.00291(2) 0.00048(3) Pt Cl1 0.0494(2) 0.0473(2) 0.0745(4) 0.0248(2) 0.0081(2) -0.0003(3) Cl Cl2 0.0869(4) 0.0789(4) 0.0591(4) 0.0279(3) -0.0098(3) 0.0049(3) Cl Cl3 0.084(1) 0.116(1) 0.0677(8) -0.0185(9) -0.0028(8) 0.0361(7) Cl Cl4 0.098(1) 0.0737(9) 0.181(2) 0.0345(8) 0.008(1) -0.010(1) Cl Cl5 0.155(3) 0.077(2) 0.060(2) -0.030(2) 0.005(2) 0.008(2) Cl Cl6 0.123(2) 0.099(2) 0.207(5) 0.070(1) -0.026(3) 0.014(2) Cl Cl7 0.094(2) 0.092(2) 0.117(2) 0.004(2) -0.002(2) 0.050(2) Cl Cl8 0.101(2) 0.076(2) 0.126(3) 0.044(1) 0.023(2) 0.013(2) Cl P1 0.0302(2) 0.0329(2) 0.0292(2) 0.0104(2) 0.0034(2) 0.0005(2) P P2 0.0313(2) 0.0320(2) 0.0348(2) 0.0075(2) 0.0053(2) 0.0008(2) P O1 0.0415(7) 0.0321(6) 0.0393(7) 0.0047(5) -0.0019(6) -0.0007(6) O O2 0.098(1) 0.068(1) 0.0453(9) 0.008(1) -0.007(1) 0.0062(9) O O3 0.114(2) 0.051(1) 0.088(1) -0.007(1) -0.002(1) 0.0265(9) O N 0.0466(9) 0.0375(8) 0.056(1) 0.0050(7) -0.0018(9) -0.0001(8) N C1 0.085(2) 0.055(1) 0.073(2) 0.005(1) -0.019(1) 0.018(1) C C111 0.0335(8) 0.0364(8) 0.0366(9) 0.0106(6) 0.0038(7) 0.0032(8) C C112 0.040(1) 0.052(1) 0.047(1) 0.0050(9) 0.0076(9) -0.007(1) C C113 0.043(1) 0.056(1) 0.062(1) 0.000(1) 0.004(1) -0.005(1) C C114 0.047(1) 0.056(1) 0.066(1) 0.002(1) 0.017(1) 0.009(1) C C115 0.058(1) 0.054(1) 0.051(1) 0.010(1) 0.0226(9) 0.011(1) C C116 0.048(1) 0.043(1) 0.039(1) 0.0090(8) 0.0114(8) 0.0038(9) C C121 0.0374(8) 0.0349(8) 0.0354(9) 0.0100(7) 0.0004(8) 0.0015(8) C C122 0.047(1) 0.061(1) 0.051(1) 0.0262(8) -0.0031(9) -0.001(1) C C123 0.061(1) 0.064(1) 0.069(2) 0.0298(9) -0.020(1) 0.001(1) C C124 0.081(2) 0.049(1) 0.052(1) 0.013(1) -0.025(1) 0.004(1) C C125 0.071(1) 0.053(1) 0.034(1) 0.006(1) -0.001(1) 0.005(1) C C126 0.048(1) 0.042(1) 0.035(1) 0.0080(8) 0.0039(9) 0.0022(9) C C131 0.0337(8) 0.0355(8) 0.0352(9) 0.0095(6) 0.0079(7) 0.0004(8) C C132 0.0406(9) 0.0380(9) 0.050(1) 0.0126(7) 0.0129(8) 0.0016(9) C C133 0.061(1) 0.039(1) 0.075(2) 0.0153(9) 0.019(1) -0.006(1) C C134 0.076(2) 0.055(1) 0.056(1) 0.011(1) 0.011(1) -0.019(1) C C135 0.069(1) 0.063(1) 0.040(1) 0.012(1) 0.003(1) -0.009(1) C C136 0.049(1) 0.045(1) 0.039(1) 0.0119(8) 0.0014(9) -0.0033(9) C C211 0.0376(8) 0.0317(8) 0.045(1) 0.0068(7) 0.0132(8) 0.0040(8) C C212 0.046(1) 0.045(1) 0.056(1) 0.0155(8) 0.0159(9) 0.0118(9) C C213 0.070(1) 0.052(1) 0.085(2) 0.0276(9) 0.033(1) 0.027(1) C C214 0.092(2) 0.039(1) 0.112(2) 0.025(1) 0.043(1) 0.014(1) C C215 0.084(2) 0.042(1) 0.093(2) 0.009(1) 0.019(1) -0.016(1) C C216 0.057(1) 0.043(1) 0.058(1) 0.0115(9) 0.009(1) -0.008(1) C C221 0.0348(8) 0.0411(9) 0.0348(9) 0.0126(7) 0.0046(7) 0.0019(8) C C222 0.0359(9) 0.048(1) 0.042(1) 0.0095(8) 0.0060(8) 0.0043(9) C C223 0.0390(9) 0.065(1) 0.045(1) 0.0146(9) 0.0091(9) 0.012(1) C C224 0.048(1) 0.082(1) 0.039(1) 0.0280(9) 0.0096(9) 0.006(1) C C225 0.063(1) 0.064(1) 0.041(1) 0.0257(9) 0.004(1) -0.007(1) C C226 0.052(1) 0.044(1) 0.043(1) 0.0133(8) 0.0042(9) -0.0030(9) C C231 0.0359(8) 0.0352(8) 0.037(1) 0.0104(7) 0.0030(8) 0.0003(8) C C232 0.0375(9) 0.054(1) 0.048(1) 0.0124(8) 0.0065(9) 0.008(1) C C233 0.037(1) 0.070(1) 0.065(1) 0.0154(9) -0.002(1) 0.004(1) C C234 0.055(1) 0.069(1) 0.052(1) 0.0275(9) -0.010(1) 0.000(1) C C235 0.066(1) 0.079(1) 0.041(1) 0.025(1) 0.001(1) 0.008(1) C C236 0.046(1) 0.071(1) 0.043(1) 0.012(1) 0.0084(9) 0.009(1) C _refine_special_details ;weight = (4*F~o~^2^)/[\s^2^(F~o~^2^)] (refinement on F^2^) \s(F~o~^2^) = [\s^2^(F~o~^2^) + (P*F~o~^2^)^2^]^(1/2)^ P = 0.0200 ; _refine_ls_structure_factor_coef 'Fsqd' _refine_ls_matrix_type 'full' _refine_ls_weighting_scheme 'calc' _refine_ls_hydrogen_treatment 'noref' _refine_ls_number_reflns 11538 _refine_ls_number_parameters 469 _refine_ls_number_constraints 0 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.031 _refine_ls_R_factor_obs 0.031 _refine_ls_wR_factor_obs 0.048 _conventional_R1_(I>2\s(I)) 0.022 _reflections_with_I>2\s(I) 9926 _refine_ls_shift/esd_max 0.010 _refine_ls_shift/esd_mean 0.000 _refine_ls_goodness_of_fit_all 1.012 _refine_ls_goodness_of_fit_obs 1.012 _refine_diff_density_max 1.705 _refine_diff_density_min -1.331 _refine_diff_density_esd 0.175 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_publ_flag Pt Cl1 2.362(1) 1_555 1_555 yes Pt P1 2.252(1) 1_555 1_555 yes Pt P2 2.243(1) 1_555 1_555 yes Pt O1 2.109(1) 1_555 1_555 yes Cl2 C1 1.749(3) 1_555 1_555 yes Cl3 Cl5 0.606(5) 1_555 1_555 yes Cl3 Cl7 0.519(5) 1_555 1_555 yes Cl3 C1 1.737(3) 1_555 1_555 yes Cl4 Cl6 0.753(6) 1_555 1_555 yes Cl4 Cl8 0.646(4) 1_555 1_555 yes Cl4 C1 1.907(4) 1_555 1_555 yes Cl5 Cl7 1.121(7) 1_555 1_555 yes Cl5 C1 2.004(5) 1_555 1_555 yes Cl6 Cl7 1.958(7) 1_555 1_555 yes Cl6 Cl8 0.794(5) 1_555 1_555 yes Cl6 C1 1.567(6) 1_555 1_555 yes Cl7 Cl8 2.370(6) 1_555 1_555 yes Cl7 C1 1.607(5) 1_555 1_555 yes Cl8 C1 1.648(5) 1_555 1_555 yes P1 C111 1.836(2) 1_555 1_555 yes P1 C121 1.821(2) 1_555 1_555 yes P1 C131 1.815(2) 1_555 1_555 yes P2 C211 1.825(2) 1_555 1_555 yes P2 C221 1.831(2) 1_555 1_555 yes P2 C231 1.820(2) 1_555 1_555 yes O1 N 1.242(2) 1_555 1_555 yes O2 N 1.236(2) 1_555 1_555 yes O3 N 1.239(2) 1_555 1_555 yes C111 C112 1.393(3) 1_555 1_555 yes C111 C116 1.384(3) 1_555 1_555 yes C112 C113 1.385(3) 1_555 1_555 yes C112 H1 0.970 1_555 1_555 yes C113 C114 1.373(4) 1_555 1_555 yes C113 H2 0.970 1_555 1_555 yes C114 C115 1.373(3) 1_555 1_555 yes C114 H3 0.970 1_555 1_555 yes C115 C116 1.385(3) 1_555 1_555 yes C115 H4 0.970 1_555 1_555 yes C116 H5 0.970 1_555 1_555 yes C121 C122 1.386(3) 1_555 1_555 yes C121 C126 1.392(3) 1_555 1_555 yes C122 C123 1.379(4) 1_555 1_555 yes C122 H6 0.970 1_555 1_555 yes C123 C124 1.381(4) 1_555 1_555 yes C123 H7 0.970 1_555 1_555 yes C124 C125 1.367(4) 1_555 1_555 yes C124 H8 0.970 1_555 1_555 yes C125 C126 1.390(3) 1_555 1_555 yes C125 H9 0.970 1_555 1_555 yes C126 H10 0.970 1_555 1_555 yes C131 C132 1.389(3) 1_555 1_555 yes C131 C136 1.391(3) 1_555 1_555 yes C132 C133 1.389(3) 1_555 1_555 yes C132 H11 0.970 1_555 1_555 yes C133 C134 1.377(4) 1_555 1_555 yes C133 H12 0.970 1_555 1_555 yes C134 C135 1.378(4) 1_555 1_555 yes C134 H13 0.970 1_555 1_555 yes C135 C136 1.382(3) 1_555 1_555 yes C135 H14 0.970 1_555 1_555 yes C136 H15 0.970 1_555 1_555 yes C211 C212 1.400(3) 1_555 1_555 yes C211 C216 1.388(3) 1_555 1_555 yes C212 C213 1.384(4) 1_555 1_555 yes C212 H16 0.970 1_555 1_555 yes C213 C214 1.376(4) 1_555 1_555 yes C213 H17 0.970 1_555 1_555 yes C214 C215 1.367(4) 1_555 1_555 yes C214 H18 0.970 1_555 1_555 yes C215 C216 1.392(4) 1_555 1_555 yes C215 H19 0.970 1_555 1_555 yes C216 H20 0.970 1_555 1_555 yes C221 C222 1.392(3) 1_555 1_555 yes C221 C226 1.388(3) 1_555 1_555 yes C222 C223 1.391(3) 1_555 1_555 yes C222 H21 0.970 1_555 1_555 yes C223 C224 1.380(3) 1_555 1_555 yes C223 H22 0.970 1_555 1_555 yes C224 C225 1.367(3) 1_555 1_555 yes C224 H23 0.970 1_555 1_555 yes C225 C226 1.399(3) 1_555 1_555 yes C225 H24 0.970 1_555 1_555 yes C226 H25 0.970 1_555 1_555 yes C231 C232 1.384(3) 1_555 1_555 yes C231 C236 1.391(3) 1_555 1_555 yes C232 C233 1.398(3) 1_555 1_555 yes C232 H26 0.970 1_555 1_555 yes C233 C234 1.359(4) 1_555 1_555 yes C233 H27 0.970 1_555 1_555 yes C234 C235 1.374(3) 1_555 1_555 yes C234 H28 0.970 1_555 1_555 yes C235 C236 1.387(3) 1_555 1_555 yes C235 H29 0.970 1_555 1_555 yes C236 H30 0.970 1_555 1_555 yes loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_2 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Cl1 Pt P1 173.6(1) 1_555 1_555 1_555 yes Cl1 Pt P2 87.3(1) 1_555 1_555 1_555 yes Cl1 Pt O1 84.3(1) 1_555 1_555 1_555 yes P1 Pt P2 98.8(1) 1_555 1_555 1_555 yes P1 Pt O1 89.7(1) 1_555 1_555 1_555 yes P2 Pt O1 171.2(1) 1_555 1_555 1_555 yes Cl5 Cl3 Cl7 170.8(6) 1_555 1_555 1_555 yes Cl5 Cl3 C1 107.5(4) 1_555 1_555 1_555 yes Cl7 Cl3 C1 67.0(5) 1_555 1_555 1_555 yes Cl6 Cl4 Cl8 68.7(5) 1_555 1_555 1_555 yes Cl6 Cl4 C1 52.5(4) 1_555 1_555 1_555 yes Cl8 Cl4 C1 57.1(4) 1_555 1_555 1_555 yes Cl3 Cl5 Cl7 4.2(3) 1_555 1_555 1_555 yes Cl3 Cl5 C1 55.8(3) 1_555 1_555 1_555 yes Cl7 Cl5 C1 53.2(3) 1_555 1_555 1_555 yes Cl4 Cl6 Cl7 156.0(4) 1_555 1_555 1_555 yes Cl4 Cl6 Cl8 49.3(4) 1_555 1_555 1_555 yes Cl4 Cl6 C1 105.1(4) 1_555 1_555 1_555 yes Cl7 Cl6 Cl8 111.7(6) 1_555 1_555 1_555 yes Cl7 Cl6 C1 52.8(2) 1_555 1_555 1_555 yes Cl8 Cl6 C1 81.5(4) 1_555 1_555 1_555 yes Cl3 Cl7 Cl5 4.9(3) 1_555 1_555 1_555 yes Cl3 Cl7 Cl6 142.3(6) 1_555 1_555 1_555 yes Cl3 Cl7 Cl8 139.5(6) 1_555 1_555 1_555 yes Cl3 Cl7 C1 95.7(5) 1_555 1_555 1_555 yes Cl5 Cl7 Cl6 138.0(4) 1_555 1_555 1_555 yes Cl5 Cl7 Cl8 136.8(3) 1_555 1_555 1_555 yes Cl5 Cl7 C1 92.8(3) 1_555 1_555 1_555 yes Cl6 Cl7 Cl8 18.1(1) 1_555 1_555 1_555 yes Cl6 Cl7 C1 51.0(2) 1_555 1_555 1_555 yes Cl8 Cl7 C1 44.0(2) 1_555 1_555 1_555 yes Cl4 Cl8 Cl6 62.0(5) 1_555 1_555 1_555 yes Cl4 Cl8 Cl7 110.3(4) 1_555 1_555 1_555 yes Cl4 Cl8 C1 103.6(4) 1_555 1_555 1_555 yes Cl6 Cl8 Cl7 50.2(5) 1_555 1_555 1_555 yes Cl6 Cl8 C1 70.1(4) 1_555 1_555 1_555 yes Cl7 Cl8 C1 42.6(2) 1_555 1_555 1_555 yes Pt P1 C111 114.0(1) 1_555 1_555 1_555 yes Pt P1 C121 114.4(1) 1_555 1_555 1_555 yes Pt P1 C131 113.8(1) 1_555 1_555 1_555 yes C111 P1 C121 100.1(1) 1_555 1_555 1_555 yes C111 P1 C131 103.3(1) 1_555 1_555 1_555 yes C121 P1 C131 109.8(1) 1_555 1_555 1_555 yes Pt P2 C211 122.8(1) 1_555 1_555 1_555 yes Pt P2 C221 113.1(1) 1_555 1_555 1_555 yes Pt P2 C231 107.8(1) 1_555 1_555 1_555 yes C211 P2 C221 101.0(1) 1_555 1_555 1_555 yes C211 P2 C231 102.9(1) 1_555 1_555 1_555 yes C221 P2 C231 108.2(1) 1_555 1_555 1_555 yes Pt O1 N 113.3(1) 1_555 1_555 1_555 yes O1 N O2 121.1(2) 1_555 1_555 1_555 yes O1 N O3 118.1(2) 1_555 1_555 1_555 yes O2 N O3 120.7(2) 1_555 1_555 1_555 yes Cl2 C1 Cl3 110.0(2) 1_555 1_555 1_555 yes Cl2 C1 Cl4 102.8(2) 1_555 1_555 1_555 yes Cl2 C1 Cl5 96.9(2) 1_555 1_555 1_555 yes Cl2 C1 Cl6 110.9(2) 1_555 1_555 1_555 yes Cl2 C1 Cl7 121.0(2) 1_555 1_555 1_555 yes Cl2 C1 Cl8 120.6(2) 1_555 1_555 1_555 yes Cl3 C1 Cl4 114.8(2) 1_555 1_555 1_555 yes Cl3 C1 Cl5 16.8(1) 1_555 1_555 1_555 yes Cl3 C1 Cl6 92.5(2) 1_555 1_555 1_555 yes Cl3 C1 Cl7 17.3(2) 1_555 1_555 1_555 yes Cl3 C1 Cl8 110.7(2) 1_555 1_555 1_555 yes Cl4 C1 Cl5 129.8(2) 1_555 1_555 1_555 yes Cl4 C1 Cl6 22.4(2) 1_555 1_555 1_555 yes Cl4 C1 Cl7 98.2(2) 1_555 1_555 1_555 yes Cl4 C1 Cl8 19.2(1) 1_555 1_555 1_555 yes Cl5 C1 Cl6 107.4(3) 1_555 1_555 1_555 yes Cl5 C1 Cl7 34.0(2) 1_555 1_555 1_555 yes Cl5 C1 Cl8 127.4(2) 1_555 1_555 1_555 yes Cl6 C1 Cl7 76.2(3) 1_555 1_555 1_555 yes Cl6 C1 Cl8 28.5(2) 1_555 1_555 1_555 yes Cl7 C1 Cl8 93.4(3) 1_555 1_555 1_555 yes P1 C111 C112 118.3(2) 1_555 1_555 1_555 yes P1 C111 C116 122.7(1) 1_555 1_555 1_555 yes C112 C111 C116 118.8(2) 1_555 1_555 1_555 yes C111 C112 C113 120.4(2) 1_555 1_555 1_555 yes C111 C112 H1 119.8 1_555 1_555 1_555 yes C113 C112 H1 119.8 1_555 1_555 1_555 yes C112 C113 C114 120.1(2) 1_555 1_555 1_555 yes C112 C113 H2 119.9 1_555 1_555 1_555 yes C114 C113 H2 119.9 1_555 1_555 1_555 yes C113 C114 C115 119.8(2) 1_555 1_555 1_555 yes C113 C114 H3 120.1 1_555 1_555 1_555 yes C115 C114 H3 120.1 1_555 1_555 1_555 yes C114 C115 C116 120.7(2) 1_555 1_555 1_555 yes C114 C115 H4 119.7 1_555 1_555 1_555 yes C116 C115 H4 119.7 1_555 1_555 1_555 yes C111 C116 C115 120.1(2) 1_555 1_555 1_555 yes C111 C116 H5 119.9 1_555 1_555 1_555 yes C115 C116 H5 119.9 1_555 1_555 1_555 yes P1 C121 C122 119.6(2) 1_555 1_555 1_555 yes P1 C121 C126 120.5(2) 1_555 1_555 1_555 yes C122 C121 C126 119.5(2) 1_555 1_555 1_555 yes C121 C122 C123 120.3(2) 1_555 1_555 1_555 yes C121 C122 H6 119.9 1_555 1_555 1_555 yes C123 C122 H6 119.9 1_555 1_555 1_555 yes C122 C123 C124 120.1(3) 1_555 1_555 1_555 yes C122 C123 H7 119.9 1_555 1_555 1_555 yes C124 C123 H7 119.9 1_555 1_555 1_555 yes C123 C124 C125 120.0(2) 1_555 1_555 1_555 yes C123 C124 H8 120.0 1_555 1_555 1_555 yes C125 C124 H8 120.0 1_555 1_555 1_555 yes C124 C125 C126 120.7(2) 1_555 1_555 1_555 yes C124 C125 H9 119.6 1_555 1_555 1_555 yes C126 C125 H9 119.6 1_555 1_555 1_555 yes C121 C126 C125 119.4(2) 1_555 1_555 1_555 yes C121 C126 H10 120.3 1_555 1_555 1_555 yes C125 C126 H10 120.3 1_555 1_555 1_555 yes P1 C131 C132 123.5(1) 1_555 1_555 1_555 yes P1 C131 C136 116.6(2) 1_555 1_555 1_555 yes C132 C131 C136 119.9(2) 1_555 1_555 1_555 yes C131 C132 C133 119.4(2) 1_555 1_555 1_555 yes C131 C132 H11 120.3 1_555 1_555 1_555 yes C133 C132 H11 120.3 1_555 1_555 1_555 yes C132 C133 C134 120.3(2) 1_555 1_555 1_555 yes C132 C133 H12 119.8 1_555 1_555 1_555 yes C134 C133 H12 119.8 1_555 1_555 1_555 yes C133 C134 C135 120.4(2) 1_555 1_555 1_555 yes C133 C134 H13 119.8 1_555 1_555 1_555 yes C135 C134 H13 119.8 1_555 1_555 1_555 yes C134 C135 C136 119.9(2) 1_555 1_555 1_555 yes C134 C135 H14 120.0 1_555 1_555 1_555 yes C136 C135 H14 120.0 1_555 1_555 1_555 yes C131 C136 C135 120.1(2) 1_555 1_555 1_555 yes C131 C136 H15 120.0 1_555 1_555 1_555 yes C135 C136 H15 120.0 1_555 1_555 1_555 yes P2 C211 C212 119.2(1) 1_555 1_555 1_555 yes P2 C211 C216 121.8(2) 1_555 1_555 1_555 yes C212 C211 C216 118.9(2) 1_555 1_555 1_555 yes C211 C212 C213 120.0(2) 1_555 1_555 1_555 yes C211 C212 H16 120.0 1_555 1_555 1_555 yes C213 C212 H16 120.0 1_555 1_555 1_555 yes C212 C213 C214 120.5(3) 1_555 1_555 1_555 yes C212 C213 H17 119.7 1_555 1_555 1_555 yes C214 C213 H17 119.7 1_555 1_555 1_555 yes C213 C214 C215 119.8(3) 1_555 1_555 1_555 yes C213 C214 H18 120.1 1_555 1_555 1_555 yes C215 C214 H18 120.1 1_555 1_555 1_555 yes C214 C215 C216 120.8(3) 1_555 1_555 1_555 yes C214 C215 H19 119.6 1_555 1_555 1_555 yes C216 C215 H19 119.6 1_555 1_555 1_555 yes C211 C216 C215 119.9(2) 1_555 1_555 1_555 yes C211 C216 H20 120.0 1_555 1_555 1_555 yes C215 C216 H20 120.0 1_555 1_555 1_555 yes P2 C221 C222 120.0(2) 1_555 1_555 1_555 yes P2 C221 C226 120.8(1) 1_555 1_555 1_555 yes C222 C221 C226 119.2(2) 1_555 1_555 1_555 yes C221 C222 C223 120.4(2) 1_555 1_555 1_555 yes C221 C222 H21 119.8 1_555 1_555 1_555 yes C223 C222 H21 119.8 1_555 1_555 1_555 yes C222 C223 C224 120.1(2) 1_555 1_555 1_555 yes C222 C223 H22 120.0 1_555 1_555 1_555 yes C224 C223 H22 120.0 1_555 1_555 1_555 yes C223 C224 C225 119.9(2) 1_555 1_555 1_555 yes C223 C224 H23 120.0 1_555 1_555 1_555 yes C225 C224 H23 120.0 1_555 1_555 1_555 yes C224 C225 C226 120.8(2) 1_555 1_555 1_555 yes C224 C225 H24 119.6 1_555 1_555 1_555 yes C226 C225 H24 119.6 1_555 1_555 1_555 yes C221 C226 C225 119.6(2) 1_555 1_555 1_555 yes C221 C226 H25 120.2 1_555 1_555 1_555 yes C225 C226 H25 120.2 1_555 1_555 1_555 yes P2 C231 C232 122.2(2) 1_555 1_555 1_555 yes P2 C231 C236 118.9(1) 1_555 1_555 1_555 yes C232 C231 C236 118.9(2) 1_555 1_555 1_555 yes C231 C232 C233 120.0(2) 1_555 1_555 1_555 yes C231 C232 H26 120.0 1_555 1_555 1_555 yes C233 C232 H26 120.0 1_555 1_555 1_555 yes C232 C233 C234 120.7(2) 1_555 1_555 1_555 yes C232 C233 H27 119.7 1_555 1_555 1_555 yes C234 C233 H27 119.7 1_555 1_555 1_555 yes C233 C234 C235 119.7(2) 1_555 1_555 1_555 yes C233 C234 H28 120.1 1_555 1_555 1_555 yes C235 C234 H28 120.1 1_555 1_555 1_555 yes C234 C235 C236 120.6(2) 1_555 1_555 1_555 yes C234 C235 H29 119.7 1_555 1_555 1_555 yes C236 C235 H29 119.7 1_555 1_555 1_555 yes C231 C236 C235 120.1(2) 1_555 1_555 1_555 yes C231 C236 H30 120.0 1_555 1_555 1_555 yes C235 C236 H30 120.0 1_555 1_555 1_555 yes