ja909129b_si_003.txt

48 hrs
HPLC output

x: Elution time (min)
 y: CAD detector signal (mV)

    10.00000	      1.8908
    10.00267	      1.9073
    10.00533	      1.9242
    10.00800	      1.9382
    10.01067	      1.9471
    10.01333	      1.9430
    10.01600	      1.9284
    10.01867	      1.9056
    10.02133	      1.8823
    10.02400	      1.8661
    10.02667	      1.8540
    10.02933	      1.8364
    10.03200	      1.8123
    10.03467	      1.7868
    10.03733	      1.7680
    10.04000	      1.7624
    10.04267	      1.7676
    10.04533	      1.7820
    10.04800	      1.7978
    10.05067	      1.8118
    10.05333	      1.8229
    10.05600	      1.8325
    10.05867	      1.8360
    10.06133	      1.8376
    10.06400	      1.8436
    10.06667	      1.8515
    10.06933	      1.8550
    10.07200	      1.8543
    10.07467	      1.8519
    10.07733	      1.8506
    10.08000	      1.8512
    10.08267	      1.8542
    10.08533	      1.8604
    10.08800	      1.8698
    10.09067	      1.8843
    10.09333	      1.8971
    10.09600	      1.9057
    10.09867	      1.9033
    10.10133	      1.8902
    10.10400	      1.8699
    10.10667	      1.8455
    10.10933	      1.8147
    10.11200	      1.7866
    10.11467	      1.7634
    10.11733	      1.7448
    10.12000	      1.7339
    10.12267	      1.7312
    10.12533	      1.7400
    10.12800	      1.7527
    10.13067	      1.7616
    10.13333	      1.7694
    10.13600	      1.7820
    10.13867	      1.7981
    10.14133	      1.8190
    10.14400	      1.8416
    10.14667	      1.8582
    10.14933	      1.8686
    10.15200	      1.8747
    10.15467	      1.8771
    10.15733	      1.8771
    10.16000	      1.8743
    10.16267	      1.8685
    10.16533	      1.8594
    10.16800	      1.8515
    10.17067	      1.8504
    10.17333	      1.8574
    10.17600	      1.8746
    10.17867	      1.8948
    10.18133	      1.9144
    10.18400	      1.9275
    10.18667	      1.9334
    10.18933	      1.9366
    10.19200	      1.9415
    10.19467	      1.9483
    10.19733	      1.9559
    10.20000	      1.9634
    10.20267	      1.9692
    10.20533	      1.9737
    10.20800	      1.9784
    10.21067	      1.9889
    10.21333	      2.0027
    10.21600	      2.0170
    10.21867	      2.0260
    10.22133	      2.0239
    10.22400	      2.0136
    10.22667	      1.9979
    10.22933	      1.9793
    10.23200	      1.9568
    10.23467	      1.9349
    10.23733	      1.9129
    10.24000	      1.8959
    10.24267	      1.8832
    10.24533	      1.8719
    10.24800	      1.8610
    10.25067	      1.8546
    10.25333	      1.8533
    10.25600	      1.8564
    10.25867	      1.8618
    10.26133	      1.8716
    10.26400	      1.8832
    10.26667	      1.8950
    10.26933	      1.9038
    10.27200	      1.9072
    10.27467	      1.9068
    10.27733	      1.9041
    10.28000	      1.9011
    10.28267	      1.8990
    10.28533	      1.8983
    10.28800	      1.8995
    10.29067	      1.9036
    10.29333	      1.9106
    10.29600	      1.9169
    10.29867	      1.9217
    10.30133	      1.9279
    10.30400	      1.9366
    10.30667	      1.9470
    10.30933	      1.9550
    10.31200	      1.9552
    10.31467	      1.9488
    10.31733	      1.9363
    10.32000	      1.9249
    10.32267	      1.9214
    10.32533	      1.9224
    10.32800	      1.9269
    10.33067	      1.9284
    10.33333	      1.9233
    10.33600	      1.9166
    10.33867	      1.9100
    10.34133	      1.9087
    10.34400	      1.9139
    10.34667	      1.9264
    10.34933	      1.9442
    10.35200	      1.9659
    10.35467	      1.9877
    10.35733	      2.0064
    10.36000	      2.0203
    10.36267	      2.0292
    10.36533	      2.0327
    10.36800	      2.0289
    10.37067	      2.0228
    10.37333	      2.0173
    10.37600	      2.0142
    10.37867	      2.0136
    10.38133	      2.0143
    10.38400	      2.0155
    10.38667	      2.0173
    10.38933	      2.0203
    10.39200	      2.0254
    10.39467	      2.0321
    10.39733	      2.0432
    10.40000	      2.0568
    10.40267	      2.0696
    10.40533	      2.0808
    10.40800	      2.0935
    10.41067	      2.1070
    10.41333	      2.1230
    10.41600	      2.1391
    10.41867	      2.1565
    10.42133	      2.1742
    10.42400	      2.1924
    10.42667	      2.2076
    10.42933	      2.2201
    10.43200	      2.2247
    10.43467	      2.2216
    10.43733	      2.2137
    10.44000	      2.2049
    10.44267	      2.2009
    10.44533	      2.2030
    10.44800	      2.2155
    10.45067	      2.2352
    10.45333	      2.2601
    10.45600	      2.2863
    10.45867	      2.3136
    10.46133	      2.3389
    10.46400	      2.3638
    10.46667	      2.3817
    10.46933	      2.3918
    10.47200	      2.4030
    10.47467	      2.4210
    10.47733	      2.4417
    10.48000	      2.4636
    10.48267	      2.4858
    10.48533	      2.5088
    10.48800	      2.5222
    10.49067	      2.5263
    10.49333	      2.5265
    10.49600	      2.5254
    10.49867	      2.5228
    10.50133	      2.5180
    10.50400	      2.5085
    10.50667	      2.4995
    10.50933	      2.4956
    10.51200	      2.4956
    10.51467	      2.4964
    10.51733	      2.4976
    10.52000	      2.4992
    10.52267	      2.5012
    10.52533	      2.5049
    10.52800	      2.5146
    10.53067	      2.5320
    10.53333	      2.5558
    10.53600	      2.5845
    10.53867	      2.6204
    10.54133	      2.6628
    10.54400	      2.7166
    10.54667	      2.7820
    10.54933	      2.8735
    10.55200	      2.9778
    10.55467	      3.1117
    10.55733	      3.2660
    10.56000	      3.4682
    10.56267	      3.7010
    10.56533	      3.9932
    10.56800	      4.3179
    10.57067	      4.6979
    10.57333	      5.1017
    10.57600	      5.5431
    10.57867	      6.0113
    10.58133	      6.5134
    10.58400	      7.0772
    10.58667	      7.6890
    10.58933	      8.3782
    10.59200	      9.0981
    10.59467	      9.8835
    10.59733	     10.6643
    10.60000	     11.4876
    10.60267	     12.2856
    10.60533	     13.1369
    10.60800	     13.9493
    10.61067	     14.7824
    10.61333	     15.5558
    10.61600	     16.3214
    10.61867	     17.0271
    10.62133	     17.7152
    10.62400	     18.3277
    10.62667	     18.8944
    10.62933	     19.3782
    10.63200	     19.7873
    10.63467	     20.0982
    10.63733	     20.3194
    10.64000	     20.4614
    10.64267	     20.5320
    10.64533	     20.5213
    10.64800	     20.4392
    10.65067	     20.2549
    10.65333	     20.0005
    10.65600	     19.6421
    10.65867	     19.2404
    10.66133	     18.7764
    10.66400	     18.2901
    10.66667	     17.7501
    10.66933	     17.1790
    10.67200	     16.5614
    10.67467	     15.9326
    10.67733	     15.2941
    10.68000	     14.6618
    10.68267	     14.0493
    10.68533	     13.4239
    10.68800	     12.8098
    10.69067	     12.1801
    10.69333	     11.5788
    10.69600	     10.9594
    10.69867	     10.3822
    10.70133	      9.8164
    10.70400	      9.3146
    10.70667	      8.8419
    10.70933	      8.4373
    10.71200	      8.0696
    10.71467	      7.7656
    10.71733	      7.5009
    10.72000	      7.2826
    10.72267	      7.0916
    10.72533	      6.9472
    10.72800	      6.8401
    10.73067	      6.7760
    10.73333	      6.7478
    10.73600	      6.7626
    10.73867	      6.8103
    10.74133	      6.9034
    10.74400	      7.0281
    10.74667	      7.2052
    10.74933	      7.4083
    10.75200	      7.6562
    10.75467	      7.9401
    10.75733	      8.2959
    10.76000	      8.7088
    10.76267	      9.2083
    10.76533	      9.7485
    10.76800	     10.3351
    10.77067	     10.9452
    10.77333	     11.5758
    10.77600	     12.2240
    10.77867	     12.8642
    10.78133	     13.4969
    10.78400	     14.0910
    10.78667	     14.6963
    10.78933	     15.2761
    10.79200	     15.8632
    10.79467	     16.3954
    10.79733	     16.8912
    10.80000	     17.3071
    10.80267	     17.6698
    10.80533	     17.9476
    10.80800	     18.1650
    10.81067	     18.3105
    10.81333	     18.3952
    10.81600	     18.3864
    10.81867	     18.2904
    10.82133	     18.1070
    10.82400	     17.8620
    10.82667	     17.5384
    10.82933	     17.1648
    10.83200	     16.7130
    10.83467	     16.2360
    10.83733	     15.7154
    10.84000	     15.2004
    10.84267	     14.6420
    10.84533	     14.0978
    10.84800	     13.5194
    10.85067	     12.9466
    10.85333	     12.3340
    10.85600	     11.7452
    10.85867	     11.1555
    10.86133	     10.6010
    10.86400	     10.0595
    10.86667	      9.5591
    10.86933	      9.0925
    10.87200	      8.6685
    10.87467	      8.2840
    10.87733	      7.9128
    10.88000	      7.5641
    10.88267	      7.2111
    10.88533	      6.8800
    10.88800	      6.5546
    10.89067	      6.2649
    10.89333	      5.9848
    10.89600	      5.7322
    10.89867	      5.4890
    10.90133	      5.2726
    10.90400	      5.0665
    10.90667	      4.8909
    10.90933	      4.7283
    10.91200	      4.5903
    10.91467	      4.4699
    10.91733	      4.3681
    10.92000	      4.2793
    10.92267	      4.2140
    10.92533	      4.1750
    10.92800	      4.1603
    10.93067	      4.1611
    10.93333	      4.1728
    10.93600	      4.1877
    10.93867	      4.2045
    10.94133	      4.2239
    10.94400	      4.2517
    10.94667	      4.2906
    10.94933	      4.3371
    10.95200	      4.3979
    10.95467	      4.4827
    10.95733	      4.5781
    10.96000	      4.6775
    10.96267	      4.7718
    10.96533	      4.8533
    10.96800	      4.9148
    10.97067	      4.9622
    10.97333	      4.9992
    10.97600	      5.0309
    10.97867	      5.0671
    10.98133	      5.1022
    10.98400	      5.1288
    10.98667	      5.1470
    10.98933	      5.1603
    10.99200	      5.1677
    10.99467	      5.1679
    10.99733	      5.1655
    11.00000	      5.1637
    11.00267	      5.1679
    11.00533	      5.1790
    11.00800	      5.1892
    11.01067	      5.1978
    11.01333	      5.2150
    11.01600	      5.2433
    11.01867	      5.2853
    11.02133	      5.3309
    11.02400	      5.3944
    11.02667	      5.4725
    11.02933	      5.5791
    11.03200	      5.7013
    11.03467	      5.8493
    11.03733	      6.0029
    11.04000	      6.1819
    11.04267	      6.3770
    11.04533	      6.6096
    11.04800	      6.8676
    11.05067	      7.1591
    11.05333	      7.4731
    11.05600	      7.8097
    11.05867	      8.1554
    11.06133	      8.5028
    11.06400	      8.8483
    11.06667	      9.1854
    11.06933	      9.5387
    11.07200	      9.8850
    11.07467	     10.2371
    11.07733	     10.5599
    11.08000	     10.8747
    11.08267	     11.1587
    11.08533	     11.4346
    11.08800	     11.6765
    11.09067	     11.8981
    11.09333	     12.0816
    11.09600	     12.2370
    11.09867	     12.3499
    11.10133	     12.4329
    11.10400	     12.4778
    11.10667	     12.4909
    11.10933	     12.4641
    11.11200	     12.4057
    11.11467	     12.3110
    11.11733	     12.1908
    11.12000	     12.0233
    11.12267	     11.8370
    11.12533	     11.6134
    11.12800	     11.3803
    11.13067	     11.1169
    11.13333	     10.8607
    11.13600	     10.5995
    11.13867	     10.3542
    11.14133	     10.1009
    11.14400	      9.8544
    11.14667	      9.5958
    11.14933	      9.3357
    11.15200	      9.0657
    11.15467	      8.7987
    11.15733	      8.5361
    11.16000	      8.2822
    11.16267	      8.0404
    11.16533	      7.8009
    11.16800	      7.5732
    11.17067	      7.3534
    11.17333	      7.1476
    11.17600	      6.9420
    11.17867	      6.7617
    11.18133	      6.6021
    11.18400	      6.4786
    11.18667	      6.3747
    11.18933	      6.2837
    11.19200	      6.1908
    11.19467	      6.1014
    11.19733	      6.0129
    11.20000	      5.9326
    11.20267	      5.8615
    11.20533	      5.8055
    11.20800	      5.7641
    11.21067	      5.7393
    11.21333	      5.7355
    11.21600	      5.7557
    11.21867	      5.7828
    11.22133	      5.8153
    11.22400	      5.8529
    11.22667	      5.9037
    11.22933	      5.9687
    11.23200	      6.0590
    11.23467	      6.1609
    11.23733	      6.2786
    11.24000	      6.4124
    11.24267	      6.5736
    11.24533	      6.7748
    11.24800	      7.0123
    11.25067	      7.2828
    11.25333	      7.5717
    11.25600	      7.8952
    11.25867	      8.2356
    11.26133	      8.6172
    11.26400	      9.0080
    11.26667	      9.4397
    11.26933	      9.8743
    11.27200	     10.3584
    11.27467	     10.8376
    11.27733	     11.3460
    11.28000	     11.8299
    11.28267	     12.3237
    11.28533	     12.7903
    11.28800	     13.2573
    11.29067	     13.6910
    11.29333	     14.1050
    11.29600	     14.4871
    11.29867	     14.8492
    11.30133	     15.2090
    11.30400	     15.5568
    11.30667	     15.8842
    11.30933	     16.1733
    11.31200	     16.4250
    11.31467	     16.6368
    11.31733	     16.8218
    11.32000	     16.9687
    11.32267	     17.0797
    11.32533	     17.1524
    11.32800	     17.2067
    11.33067	     17.2549
    11.33333	     17.3093
    11.33600	     17.3719
    11.33867	     17.4496
    11.34133	     17.5549
    11.34400	     17.6832
    11.34667	     17.8497
    11.34933	     18.0507
    11.35200	     18.3249
    11.35467	     18.6647
    11.35733	     19.1346
    11.36000	     19.6902
    11.36267	     20.4071
    11.36533	     21.2236
    11.36800	     22.2547
    11.37067	     23.4404
    11.37333	     24.9428
    11.37600	     26.6626
    11.37867	     28.7881
    11.38133	     31.1893
    11.38400	     33.9872
    11.38667	     37.1067
    11.38933	     40.6064
    11.39200	     44.4999
    11.39467	     48.7110
    11.39733	     53.3493
    11.40000	     58.1843
    11.40267	     63.4156
    11.40533	     68.6534
    11.40800	     74.2456
    11.41067	     79.7327
    11.41333	     85.6246
    11.41600	     91.3656
    11.41867	     97.4448
    11.42133	    103.2548
    11.42400	    109.2106
    11.42667	    114.7442
    11.42933	    120.1774
    11.43200	    125.0517
    11.43467	    129.5511
    11.43733	    133.4094
    11.44000	    136.7465
    11.44267	    139.4294
    11.44533	    141.5375
    11.44800	    143.0076
    11.45067	    143.9145
    11.45333	    144.2254
    11.45600	    144.0306
    11.45867	    143.2166
    11.46133	    141.9650
    11.46400	    140.1217
    11.46667	    137.9853
    11.46933	    135.4063
    11.47200	    132.6755
    11.47467	    129.6280
    11.47733	    126.5016
    11.48000	    123.1663
    11.48267	    119.8249
    11.48533	    116.4521
    11.48800	    113.2165
    11.49067	    110.1670
    11.49333	    107.3994
    11.49600	    104.9805
    11.49867	    102.8998
    11.50133	    101.2336
    11.50400	     99.9987
    11.50667	     99.2374
    11.50933	     99.0042
    11.51200	     99.2417
    11.51467	     99.9968
    11.51733	    101.1308
    11.52000	    102.7262
    11.52267	    104.6176
    11.52533	    106.8708
    11.52800	    109.1734
    11.53067	    111.5102
    11.53333	    113.7735
    11.53600	    116.0011
    11.53867	    118.2523
    11.54133	    120.4664
    11.54400	    122.6144
    11.54667	    124.5373
    11.54933	    126.1871
    11.55200	    127.4364
    11.55467	    128.2513
    11.55733	    128.6016
    11.56000	    128.4061
    11.56267	    127.7724
    11.56533	    126.6469
    11.56800	    125.1388
    11.57067	    123.1560
    11.57333	    120.8149
    11.57600	    118.0434
    11.57867	    114.9176
    11.58133	    111.4340
    11.58400	    107.6043
    11.58667	    103.5582
    11.58933	     99.2562
    11.59200	     94.9520
    11.59467	     90.4547
    11.59733	     86.0901
    11.60000	     81.5485
    11.60267	     77.2266
    11.60533	     72.7999
    11.60800	     68.6747
    11.61067	     64.5196
    11.61333	     60.6671
    11.61600	     56.8010
    11.61867	     53.2162
    11.62133	     49.6976
    11.62400	     46.4456
    11.62667	     43.3286
    11.62933	     40.4395
    11.63200	     37.7321
    11.63467	     35.2141
    11.63733	     32.9070
    11.64000	     30.7508
    11.64267	     28.8121
    11.64533	     26.9766
    11.64800	     25.3479
    11.65067	     23.7899
    11.65333	     22.4189
    11.65600	     21.1401
    11.65867	     20.0365
    11.66133	     19.0142
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    19.98133	      5.8828
    19.98400	      5.8766
    19.98667	      5.8642
    19.98933	      5.8457
    19.99200	      5.8274
    19.99467	      5.8112
    19.99733	      5.8000
    20.00000	      5.7925
    20.00267	      5.7836
    20.00533	      5.7688
    20.00800	      5.7499