data_shelx _audit_creation_method SHELXL-2014 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C24 H26 Fe2 S2' _chemical_formula_sum 'C24 H26 Fe2 S2' _chemical_formula_weight 490.27 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Fe' 'Fe' 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 5.794(13) _cell_length_b 12.06(3) _cell_length_c 16.07(4) _cell_angle_alpha 111.24(12) _cell_angle_beta 92.08(9) _cell_angle_gamma 93.43(11) _cell_volume 1043(5) _cell_formula_units_Z 2 _cell_measurement_temperature 150(2) _cell_measurement_reflns_used 9836 _cell_measurement_theta_min 2.63 _cell_measurement_theta_max 30.47 _exptl_crystal_description 'plate' _exptl_crystal_colour 'yellow' _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.562 _exptl_crystal_F_000 508 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.628 _exptl_crystal_size_mid 0.319 _exptl_crystal_size_min 0.122 _exptl_absorpt_coefficient_mu 1.599 _shelx_estimated_absorpt_T_min 0.433 _shelx_estimated_absorpt_T_max 0.829 _exptl_absorpt_correction_type 'multi-scan' _exptl_absorpt_correction_T_min 0.6383 _exptl_absorpt_correction_T_max 0.7461 _exptl_absorpt_process_details SADABS _exptl_special_details ; ? ; _diffrn_ambient_temperature 150(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_source 'I\ms micro focus' _diffrn_radiation_monochromator 'Quazar multi-layer optics' _diffrn_measurement_device_type 'Bruker kappa Proton CMOS' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 41547 _diffrn_reflns_av_unetI/netI 0.0186 _diffrn_reflns_av_R_equivalents 0.0427 _diffrn_reflns_limit_h_min -7 _diffrn_reflns_limit_h_max 7 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_theta_min 2.640 _diffrn_reflns_theta_max 25.681 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measured_fraction_theta_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_point_group_measured_fraction_full 0.999 _reflns_number_total 3946 _reflns_number_gt 3626 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Bruker APEX2' _computing_cell_refinement 'Bruker SAINT' _computing_data_reduction 'Bruker SAINT' _computing_structure_solution 'SHELXTS-2013 (Sheldrick, 2013)' _computing_structure_refinement 'SHELXTL-2013, SHELXL-2013 (Sheldrick, 2013)' _computing_molecular_graphics ; ORTEP-3 for Windows (Farrugia, 1997), Mercury (Macrae et al., 2008) _computing_publication_material 'SHELXL-2013' _refine_special_details Only one of the four five-membered (Cp) rings in the asymmetric unit displayed larger thermal motion for three of its five carbon atoms (C20, C21, C24). This five-membered ring had to be refined using the EADP instruction to model the anisotropic thermal parameters of these three atoms (C20, C21, C24) and also C22 in this ring, on that of C23. As a result of this model, the Hirshfeld test flagged these warnings. Unrestricted refinement (without EADP instruction) of this Cp ring resulted in large librations for these three atoms. This seemed chemically and physically unsatisfactory as there is no apparent reason for three out of five carbon ring atoms of this Cp ring to behave as such. Hence the EADP instruction and subsequent Hirshfeld test alerts. Alerts related to the high difference electron density peak refer to the peak directly related to the modelling of the thermal motion of these atoms in this five membered ring. This peak appears close to C20 and C24. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0897P)^2^+4.4155P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 3946 _refine_ls_number_parameters 229 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0588 _refine_ls_R_factor_gt 0.0553 _refine_ls_wR_factor_ref 0.1497 _refine_ls_wR_factor_gt 0.1464 _refine_ls_goodness_of_fit_ref 1.035 _refine_ls_restrained_S_all 1.035 _refine_ls_shift/su_max 0.003 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Fe1 Fe 0.00761(9) 0.39761(5) 0.21104(3) 0.01381(18) Uani 1 1 d . . . . . Fe2 Fe 0.47304(9) 0.13936(5) 0.82927(3) 0.01474(18) Uani 1 1 d . . . . . S1 S 0.02836(19) 0.15561(10) 0.46574(7) 0.0250(3) Uani 1 1 d . . . . . S2 S 0.3751(2) 0.14217(10) 0.46657(7) 0.0261(3) Uani 1 1 d . . . . . C1 C -0.0044(8) 0.2922(4) 0.4467(3) 0.0231(9) Uani 1 1 d . . . . . H1A H -0.1697 0.3091 0.4496 0.028 Uiso 1 1 calc R U . . . H1B H 0.0847 0.3587 0.4949 0.028 Uiso 1 1 calc R U . . . C2 C 0.0779(8) 0.2867(4) 0.3572(3) 0.0203(8) Uani 1 1 d . . . . . H2A H 0.2491 0.2883 0.3590 0.024 Uiso 1 1 calc R U . . . H2B H 0.0154 0.2106 0.3103 0.024 Uiso 1 1 calc R U . . . C3 C 0.0027(7) 0.3883(3) 0.3337(2) 0.0164(8) Uani 1 1 d . . . . . C4 C -0.2245(7) 0.3973(4) 0.3029(3) 0.0200(8) Uani 1 1 d . . . . . H4 H -0.3535 0.3411 0.2945 0.024 Uiso 1 1 calc R U . . . C5 C -0.2253(7) 0.5041(4) 0.2869(3) 0.0232(9) Uani 1 1 d . . . . . H5 H -0.3553 0.5327 0.2655 0.028 Uiso 1 1 calc R U . . . C6 C 0.0013(8) 0.5623(4) 0.3082(3) 0.0218(9) Uani 1 1 d . . . . . H6 H 0.0498 0.6362 0.3033 0.026 Uiso 1 1 calc R U . . . C7 C 0.1411(7) 0.4908(4) 0.3379(3) 0.0187(8) Uani 1 1 d . . . . . H7 H 0.3004 0.5085 0.3574 0.022 Uiso 1 1 calc R U . . . C8 C -0.1247(8) 0.3069(5) 0.0840(3) 0.0315(11) Uani 1 1 d . . . . . H8 H -0.2845 0.2931 0.0649 0.038 Uiso 1 1 calc R U . . . C9 C 0.0064(9) 0.2334(4) 0.1136(3) 0.0313(11) Uani 1 1 d . . . . . H9 H -0.0488 0.1602 0.1182 0.038 Uiso 1 1 calc R U . . . C10 C 0.2334(8) 0.2862(5) 0.1351(3) 0.0313(11) Uani 1 1 d . . . . . H10 H 0.3587 0.2549 0.1570 0.038 Uiso 1 1 calc R U . . . C11 C 0.2443(8) 0.3922(4) 0.1193(3) 0.0322(11) Uani 1 1 d . . . . . H11 H 0.3777 0.4460 0.1283 0.039 Uiso 1 1 calc R U . . . C12 C 0.0250(10) 0.4055(4) 0.0876(3) 0.0332(11) Uani 1 1 d . . . . . H12 H -0.0170 0.4702 0.0713 0.040 Uiso 1 1 calc R U . . . C13 C 0.4715(7) 0.2189(4) 0.5826(3) 0.0207(8) Uani 1 1 d . . . . . H13A H 0.6429 0.2239 0.5884 0.025 Uiso 1 1 calc R U . . . H13B H 0.4227 0.3013 0.6029 0.025 Uiso 1 1 calc R U . . . C14 C 0.3763(8) 0.1577(4) 0.6424(3) 0.0220(9) Uani 1 1 d . . . . . H14A H 0.2063 0.1622 0.6432 0.026 Uiso 1 1 calc R U . . . H14B H 0.4077 0.0724 0.6180 0.026 Uiso 1 1 calc R U . . . C15 C 0.4818(7) 0.2136(3) 0.7355(3) 0.0178(8) Uani 1 1 d . . . . . C16 C 0.3742(7) 0.2881(4) 0.8118(3) 0.0200(8) Uani 1 1 d . . . . . H16 H 0.2213 0.3128 0.8123 0.024 Uiso 1 1 calc R U . . . C17 C 0.5343(8) 0.3193(4) 0.8867(3) 0.0233(9) Uani 1 1 d . . . . . H17 H 0.5072 0.3674 0.9465 0.028 Uiso 1 1 calc R U . . . C18 C 0.7411(8) 0.2664(4) 0.8571(3) 0.0247(9) Uani 1 1 d . . . . . H18 H 0.8780 0.2731 0.8935 0.030 Uiso 1 1 calc R U . . . C19 C 0.7106(7) 0.2016(4) 0.7640(3) 0.0213(8) Uani 1 1 d . . . . . H19 H 0.8235 0.1578 0.7270 0.026 Uiso 1 1 calc R U . . . C20 C 0.1884(13) 0.0361(5) 0.8299(5) 0.0528(7) Uani 1 1 d . . . . . H20 H 0.0339 0.0542 0.8217 0.063 Uiso 1 1 calc R U . . . C21 C 0.3289(12) -0.0289(5) 0.7668(5) 0.0528(7) Uani 1 1 d . . . . . H21 H 0.2840 -0.0661 0.7049 0.063 Uiso 1 1 calc R U . . . C22 C 0.5323(12) -0.0334(5) 0.8023(5) 0.0528(7) Uani 1 1 d . . . . . H22 H 0.6559 -0.0728 0.7695 0.063 Uiso 1 1 calc R U . . . C23 C 0.5441(12) 0.0240(5) 0.8897(5) 0.0528(7) Uani 1 1 d . . . . . H23 H 0.6767 0.0305 0.9283 0.063 Uiso 1 1 calc R U . . . C24 C 0.3407(12) 0.0730(5) 0.9177(5) 0.0528(7) Uani 1 1 d . . . . . H24 H 0.3026 0.1187 0.9767 0.063 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Fe1 0.0181(3) 0.0137(3) 0.0100(3) 0.0048(2) 0.0011(2) 0.0014(2) Fe2 0.0197(3) 0.0135(3) 0.0132(3) 0.0077(2) -0.0003(2) 0.0003(2) S1 0.0275(6) 0.0304(6) 0.0238(5) 0.0192(5) -0.0040(4) -0.0034(4) S2 0.0325(6) 0.0349(6) 0.0121(5) 0.0078(4) 0.0046(4) 0.0149(5) C1 0.028(2) 0.029(2) 0.020(2) 0.0168(18) 0.0059(17) 0.0085(17) C2 0.030(2) 0.0188(19) 0.0142(19) 0.0081(16) 0.0033(16) 0.0035(16) C3 0.023(2) 0.0166(18) 0.0090(17) 0.0033(14) 0.0017(14) 0.0016(15) C4 0.020(2) 0.023(2) 0.0168(19) 0.0062(16) 0.0031(15) 0.0014(15) C5 0.025(2) 0.029(2) 0.018(2) 0.0090(17) 0.0043(16) 0.0118(17) C6 0.037(2) 0.0130(18) 0.0154(19) 0.0043(15) 0.0044(17) 0.0046(16) C7 0.023(2) 0.0193(19) 0.0120(18) 0.0039(15) -0.0003(15) 0.0000(15) C8 0.024(2) 0.049(3) 0.013(2) 0.0008(19) -0.0017(16) 0.003(2) C9 0.059(3) 0.017(2) 0.014(2) 0.0008(16) 0.011(2) -0.001(2) C10 0.033(3) 0.043(3) 0.016(2) 0.0055(19) 0.0044(18) 0.019(2) C11 0.032(2) 0.035(3) 0.020(2) -0.0002(19) 0.0117(18) -0.0097(19) C12 0.063(3) 0.029(2) 0.012(2) 0.0100(18) 0.007(2) 0.013(2) C13 0.021(2) 0.029(2) 0.0138(19) 0.0090(17) 0.0009(15) 0.0023(16) C14 0.034(2) 0.0179(19) 0.015(2) 0.0085(16) -0.0037(16) 0.0013(16) C15 0.023(2) 0.0156(18) 0.0174(19) 0.0099(16) 0.0012(15) -0.0001(15) C16 0.025(2) 0.0175(19) 0.020(2) 0.0103(16) 0.0037(16) 0.0024(16) C17 0.036(2) 0.018(2) 0.017(2) 0.0077(16) 0.0031(17) -0.0008(17) C18 0.026(2) 0.028(2) 0.024(2) 0.0167(18) -0.0047(17) -0.0070(17) C19 0.022(2) 0.024(2) 0.022(2) 0.0131(17) 0.0025(16) 0.0019(16) C20 0.0696(18) 0.0343(13) 0.0672(18) 0.0345(13) 0.0113(14) -0.0065(12) C21 0.0696(18) 0.0343(13) 0.0672(18) 0.0345(13) 0.0113(14) -0.0065(12) C22 0.0696(18) 0.0343(13) 0.0672(18) 0.0345(13) 0.0113(14) -0.0065(12) C23 0.0696(18) 0.0343(13) 0.0672(18) 0.0345(13) 0.0113(14) -0.0065(12) C24 0.0696(18) 0.0343(13) 0.0672(18) 0.0345(13) 0.0113(14) -0.0065(12) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Fe1 C3 2.015(6) . ? Fe1 C12 2.025(6) . ? Fe1 C8 2.030(6) . ? Fe1 C9 2.031(7) . ? Fe1 C7 2.035(6) . ? Fe1 C4 2.033(6) . ? Fe1 C10 2.035(6) . ? Fe1 C5 2.037(6) . ? Fe1 C6 2.037(6) . ? Fe1 C11 2.037(6) . ? Fe2 C20 2.009(7) . ? Fe2 C15 2.012(6) . ? Fe2 C24 2.018(7) . ? Fe2 C23 2.016(7) . ? Fe2 C22 2.022(8) . ? Fe2 C21 2.021(8) . ? Fe2 C16 2.026(6) . ? Fe2 C17 2.029(7) . ? Fe2 C18 2.032(6) . ? Fe2 C19 2.028(5) . ? S1 C1 1.800(6) . ? S1 S2 2.025(5) . ? S2 C13 1.805(6) . ? C1 C2 1.513(6) . ? C1 H1A 0.9900 . ? C1 H1B 0.9900 . ? C2 C3 1.490(6) . ? C2 H2A 0.9900 . ? C2 H2B 0.9900 . ? C3 C4 1.413(6) . ? C3 C7 1.412(6) . ? C4 C5 1.402(7) . ? C4 H4 0.9500 . ? C5 C6 1.420(7) . ? C5 H5 0.9500 . ? C6 C7 1.408(6) . ? C6 H6 0.9500 . ? C7 H7 0.9500 . ? C8 C9 1.396(8) . ? C8 C12 1.412(8) . ? C8 H8 0.9500 . ? C9 C10 1.401(8) . ? C9 H9 0.9500 . ? C10 C11 1.390(8) . ? C10 H10 0.9500 . ? C11 C12 1.391(8) . ? C11 H11 0.9500 . ? C12 H12 0.9500 . ? C13 C14 1.508(6) . ? C13 H13A 0.9900 . ? C13 H13B 0.9900 . ? C14 C15 1.490(7) . ? C14 H14A 0.9900 . ? C14 H14B 0.9900 . ? C15 C19 1.419(6) . ? C15 C16 1.422(6) . ? C16 C17 1.414(7) . ? C16 H16 0.9500 . ? C17 C18 1.408(7) . ? C17 H17 0.9500 . ? C18 C19 1.413(7) . ? C18 H18 0.9500 . ? C19 H19 0.9500 . ? C20 C21 1.366(10) . ? C20 C24 1.540(10) . ? C20 H20 0.9500 . ? C21 C22 1.303(10) . ? C21 H21 0.9500 . ? C22 C23 1.319(10) . ? C22 H22 0.9500 . ? C23 C24 1.367(10) . ? C23 H23 0.9500 . ? C24 H24 0.9500 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C3 Fe1 C12 177.88(19) . . ? C3 Fe1 C8 140.0(2) . . ? C12 Fe1 C8 40.7(2) . . ? C3 Fe1 C9 111.8(2) . . ? C12 Fe1 C9 67.6(3) . . ? C8 Fe1 C9 40.2(2) . . ? C3 Fe1 C7 40.8(2) . . ? C12 Fe1 C7 138.4(2) . . ? C8 Fe1 C7 179.12(19) . . ? C9 Fe1 C7 140.5(2) . . ? C3 Fe1 C4 40.87(19) . . ? C12 Fe1 C4 141.2(2) . . ? C8 Fe1 C4 112.0(2) . . ? C9 Fe1 C4 110.9(2) . . ? C7 Fe1 C4 68.5(2) . . ? C3 Fe1 C10 111.0(2) . . ? C12 Fe1 C10 67.2(2) . . ? C8 Fe1 C10 67.7(2) . . ? C9 Fe1 C10 40.3(2) . . ? C7 Fe1 C10 112.5(2) . . ? C4 Fe1 C10 138.0(2) . . ? C3 Fe1 C5 68.3(2) . . ? C12 Fe1 C5 113.6(2) . . ? C8 Fe1 C5 111.6(2) . . ? C9 Fe1 C5 138.0(2) . . ? C7 Fe1 C5 68.2(2) . . ? C4 Fe1 C5 40.3(2) . . ? C10 Fe1 C5 178.0(2) . . ? C3 Fe1 C6 68.5(2) . . ? C12 Fe1 C6 112.2(2) . . ? C8 Fe1 C6 138.9(2) . . ? C9 Fe1 C6 178.7(2) . . ? C7 Fe1 C6 40.45(19) . . ? C4 Fe1 C6 68.4(2) . . ? C10 Fe1 C6 140.9(2) . . ? C5 Fe1 C6 40.8(2) . . ? C3 Fe1 C11 137.8(2) . . ? C12 Fe1 C11 40.1(2) . . ? C8 Fe1 C11 68.0(3) . . ? C9 Fe1 C11 67.6(2) . . ? C7 Fe1 C11 111.5(2) . . ? C4 Fe1 C11 177.87(19) . . ? C10 Fe1 C11 39.9(2) . . ? C5 Fe1 C11 141.8(2) . . ? C6 Fe1 C11 113.1(2) . . ? C20 Fe2 C15 117.9(3) . . ? C20 Fe2 C24 45.0(3) . . ? C15 Fe2 C24 159.0(2) . . ? C20 Fe2 C23 68.9(3) . . ? C15 Fe2 C23 157.9(2) . . ? C24 Fe2 C23 39.6(3) . . ? C20 Fe2 C22 66.4(3) . . ? C15 Fe2 C22 122.5(3) . . ? C24 Fe2 C22 66.5(3) . . ? C23 Fe2 C22 38.1(3) . . ? C20 Fe2 C21 39.6(3) . . ? C15 Fe2 C21 106.0(3) . . ? C24 Fe2 C21 68.8(3) . . ? C23 Fe2 C21 64.8(3) . . ? C22 Fe2 C21 37.6(3) . . ? C20 Fe2 C16 108.7(3) . . ? C15 Fe2 C16 41.25(18) . . ? C24 Fe2 C16 124.6(3) . . ? C23 Fe2 C16 160.3(2) . . ? C22 Fe2 C16 160.4(2) . . ? C21 Fe2 C16 126.7(3) . . ? C20 Fe2 C17 129.1(3) . . ? C15 Fe2 C17 69.3(2) . . ? C24 Fe2 C17 110.3(3) . . ? C23 Fe2 C17 124.6(3) . . ? C22 Fe2 C17 156.6(3) . . ? C21 Fe2 C17 165.3(2) . . ? C16 Fe2 C17 40.8(2) . . ? C20 Fe2 C18 166.9(2) . . ? C15 Fe2 C18 69.0(2) . . ? C24 Fe2 C18 125.2(3) . . ? C23 Fe2 C18 109.1(3) . . ? C22 Fe2 C18 120.6(3) . . ? C21 Fe2 C18 152.3(2) . . ? C16 Fe2 C18 68.5(2) . . ? C17 Fe2 C18 40.6(2) . . ? C20 Fe2 C19 151.5(2) . . ? C15 Fe2 C19 41.14(19) . . ? C24 Fe2 C19 159.6(2) . . ? C23 Fe2 C19 123.0(3) . . ? C22 Fe2 C19 105.9(3) . . ? C21 Fe2 C19 117.6(3) . . ? C16 Fe2 C19 68.9(2) . . ? C17 Fe2 C19 68.7(2) . . ? C18 Fe2 C19 40.7(2) . . ? C1 S1 S2 103.58(18) . . ? C13 S2 S1 103.59(19) . . ? C2 C1 S1 112.4(3) . . ? C2 C1 H1A 109.1 . . ? S1 C1 H1A 109.1 . . ? C2 C1 H1B 109.1 . . ? S1 C1 H1B 109.1 . . ? H1A C1 H1B 107.9 . . ? C3 C2 C1 111.6(4) . . ? C3 C2 H2A 109.3 . . ? C1 C2 H2A 109.3 . . ? C3 C2 H2B 109.3 . . ? C1 C2 H2B 109.3 . . ? H2A C2 H2B 108.0 . . ? C4 C3 C7 108.3(4) . . ? C4 C3 C2 124.8(4) . . ? C7 C3 C2 126.9(4) . . ? C4 C3 Fe1 70.3(2) . . ? C7 C3 Fe1 70.3(3) . . ? C2 C3 Fe1 125.1(3) . . ? C5 C4 C3 107.7(4) . . ? C5 C4 Fe1 70.0(3) . . ? C3 C4 Fe1 68.9(3) . . ? C5 C4 H4 126.1 . . ? C3 C4 H4 126.1 . . ? Fe1 C4 H4 126.6 . . ? C4 C5 C6 108.4(4) . . ? C4 C5 Fe1 69.7(3) . . ? C6 C5 Fe1 69.6(3) . . ? C4 C5 H5 125.8 . . ? C6 C5 H5 125.8 . . ? Fe1 C5 H5 126.4 . . ? C7 C6 C5 107.7(4) . . ? C7 C6 Fe1 69.7(3) . . ? C5 C6 Fe1 69.6(3) . . ? C7 C6 H6 126.2 . . ? C5 C6 H6 126.2 . . ? Fe1 C6 H6 126.1 . . ? C6 C7 C3 107.9(4) . . ? C6 C7 Fe1 69.9(3) . . ? C3 C7 Fe1 68.9(3) . . ? C6 C7 H7 126.0 . . ? C3 C7 H7 126.0 . . ? Fe1 C7 H7 126.8 . . ? C9 C8 C12 107.1(5) . . ? C9 C8 Fe1 70.0(3) . . ? C12 C8 Fe1 69.4(3) . . ? C9 C8 H8 126.5 . . ? C12 C8 H8 126.5 . . ? Fe1 C8 H8 125.7 . . ? C8 C9 C10 108.2(5) . . ? C8 C9 Fe1 69.9(3) . . ? C10 C9 Fe1 70.0(3) . . ? C8 C9 H9 125.9 . . ? C10 C9 H9 125.9 . . ? Fe1 C9 H9 125.8 . . ? C11 C10 C9 108.4(4) . . ? C11 C10 Fe1 70.1(3) . . ? C9 C10 Fe1 69.7(3) . . ? C11 C10 H10 125.8 . . ? C9 C10 H10 125.8 . . ? Fe1 C10 H10 126.0 . . ? C10 C11 C12 107.8(4) . . ? C10 C11 Fe1 70.0(3) . . ? C12 C11 Fe1 69.5(3) . . ? C10 C11 H11 126.1 . . ? C12 C11 H11 126.1 . . ? Fe1 C11 H11 126.0 . . ? C11 C12 C8 108.5(5) . . ? C11 C12 Fe1 70.4(3) . . ? C8 C12 Fe1 69.8(3) . . ? C11 C12 H12 125.7 . . ? C8 C12 H12 125.7 . . ? Fe1 C12 H12 125.6 . . ? C14 C13 S2 112.7(3) . . ? C14 C13 H13A 109.0 . . ? S2 C13 H13A 109.0 . . ? C14 C13 H13B 109.0 . . ? S2 C13 H13B 109.0 . . ? H13A C13 H13B 107.8 . . ? C15 C14 C13 111.6(4) . . ? C15 C14 H14A 109.3 . . ? C13 C14 H14A 109.3 . . ? C15 C14 H14B 109.3 . . ? C13 C14 H14B 109.3 . . ? H14A C14 H14B 108.0 . . ? C19 C15 C16 107.5(4) . . ? C19 C15 C14 125.7(4) . . ? C16 C15 C14 126.9(4) . . ? C19 C15 Fe2 70.0(2) . . ? C16 C15 Fe2 69.9(3) . . ? C14 C15 Fe2 125.5(3) . . ? C17 C16 C15 108.1(4) . . ? C17 C16 Fe2 69.7(3) . . ? C15 C16 Fe2 68.9(3) . . ? C17 C16 H16 125.9 . . ? C15 C16 H16 125.9 . . ? Fe2 C16 H16 127.0 . . ? C16 C17 C18 108.0(4) . . ? C16 C17 Fe2 69.4(3) . . ? C18 C17 Fe2 69.8(3) . . ? C16 C17 H17 126.0 . . ? C18 C17 H17 126.0 . . ? Fe2 C17 H17 126.3 . . ? C17 C18 C19 108.4(4) . . ? C17 C18 Fe2 69.6(3) . . ? C19 C18 Fe2 69.5(3) . . ? C17 C18 H18 125.8 . . ? C19 C18 H18 125.8 . . ? Fe2 C18 H18 126.7 . . ? C18 C19 C15 108.0(4) . . ? C18 C19 Fe2 69.8(3) . . ? C15 C19 Fe2 68.9(3) . . ? C18 C19 H19 126.0 . . ? C15 C19 H19 126.0 . . ? Fe2 C19 H19 126.9 . . ? C21 C20 C24 103.3(7) . . ? C21 C20 Fe2 70.7(4) . . ? C24 C20 Fe2 67.8(4) . . ? C21 C20 H20 128.3 . . ? C24 C20 H20 128.3 . . ? Fe2 C20 H20 124.8 . . ? C22 C21 C20 111.4(7) . . ? C22 C21 Fe2 71.3(4) . . ? C20 C21 Fe2 69.7(4) . . ? C22 C21 H21 124.3 . . ? C20 C21 H21 124.3 . . ? Fe2 C21 H21 126.4 . . ? C21 C22 C23 111.1(7) . . ? C21 C22 Fe2 71.1(4) . . ? C23 C22 Fe2 70.7(4) . . ? C21 C22 H22 124.5 . . ? C23 C22 H22 124.5 . . ? Fe2 C22 H22 125.3 . . ? C22 C23 C24 111.2(7) . . ? C22 C23 Fe2 71.2(4) . . ? C24 C23 Fe2 70.3(4) . . ? C22 C23 H23 124.4 . . ? C24 C23 H23 124.4 . . ? Fe2 C23 H23 125.8 . . ? C23 C24 C20 103.0(6) . . ? C23 C24 Fe2 70.1(4) . . ? C20 C24 Fe2 67.2(4) . . ? C23 C24 H24 128.5 . . ? C20 C24 H24 128.5 . . ? Fe2 C24 H24 125.7 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag S2 S1 C1 C2 62.8(3) . . . . ? S1 C1 C2 C3 167.4(3) . . . . ? C1 C2 C3 C4 -76.0(5) . . . . ? C1 C2 C3 C7 104.0(5) . . . . ? C1 C2 C3 Fe1 -165.2(3) . . . . ? C7 C3 C4 C5 0.9(4) . . . . ? C2 C3 C4 C5 -179.1(4) . . . . ? Fe1 C3 C4 C5 -59.4(3) . . . . ? C7 C3 C4 Fe1 60.3(3) . . . . ? C2 C3 C4 Fe1 -119.7(4) . . . . ? C3 C4 C5 C6 -0.3(5) . . . . ? Fe1 C4 C5 C6 -59.1(3) . . . . ? C3 C4 C5 Fe1 58.7(3) . . . . ? C4 C5 C6 C7 -0.4(5) . . . . ? Fe1 C5 C6 C7 -59.5(3) . . . . ? C4 C5 C6 Fe1 59.1(3) . . . . ? C5 C6 C7 C3 0.9(4) . . . . ? Fe1 C6 C7 C3 -58.5(3) . . . . ? C5 C6 C7 Fe1 59.4(3) . . . . ? C4 C3 C7 C6 -1.1(4) . . . . ? C2 C3 C7 C6 178.9(4) . . . . ? Fe1 C3 C7 C6 59.2(3) . . . . ? C4 C3 C7 Fe1 -60.3(3) . . . . ? C2 C3 C7 Fe1 119.7(4) . . . . ? C12 C8 C9 C10 0.0(5) . . . . ? Fe1 C8 C9 C10 -59.8(3) . . . . ? C12 C8 C9 Fe1 59.8(3) . . . . ? C8 C9 C10 C11 0.1(5) . . . . ? Fe1 C9 C10 C11 -59.6(4) . . . . ? C8 C9 C10 Fe1 59.7(4) . . . . ? C9 C10 C11 C12 -0.1(5) . . . . ? Fe1 C10 C11 C12 -59.5(3) . . . . ? C9 C10 C11 Fe1 59.4(3) . . . . ? C10 C11 C12 C8 0.1(5) . . . . ? Fe1 C11 C12 C8 -59.6(3) . . . . ? C10 C11 C12 Fe1 59.8(3) . . . . ? C9 C8 C12 C11 -0.1(5) . . . . ? Fe1 C8 C12 C11 60.0(3) . . . . ? C9 C8 C12 Fe1 -60.1(3) . . . . ? S1 S2 C13 C14 64.5(3) . . . . ? S2 C13 C14 C15 172.7(3) . . . . ? C13 C14 C15 C19 -73.6(5) . . . . ? C13 C14 C15 C16 106.3(5) . . . . ? C13 C14 C15 Fe2 -163.3(3) . . . . ? C19 C15 C16 C17 -1.3(5) . . . . ? C14 C15 C16 C17 178.7(4) . . . . ? Fe2 C15 C16 C17 58.9(3) . . . . ? C19 C15 C16 Fe2 -60.2(3) . . . . ? C14 C15 C16 Fe2 119.9(4) . . . . ? C15 C16 C17 C18 1.0(5) . . . . ? Fe2 C16 C17 C18 59.4(3) . . . . ? C15 C16 C17 Fe2 -58.3(3) . . . . ? C16 C17 C18 C19 -0.4(5) . . . . ? Fe2 C17 C18 C19 58.8(3) . . . . ? C16 C17 C18 Fe2 -59.1(3) . . . . ? C17 C18 C19 C15 -0.5(5) . . . . ? Fe2 C18 C19 C15 58.4(3) . . . . ? C17 C18 C19 Fe2 -58.9(3) . . . . ? C16 C15 C19 C18 1.1(5) . . . . ? C14 C15 C19 C18 -179.0(4) . . . . ? Fe2 C15 C19 C18 -59.0(3) . . . . ? C16 C15 C19 Fe2 60.1(3) . . . . ? C14 C15 C19 Fe2 -120.0(4) . . . . ? C24 C20 C21 C22 -1.3(6) . . . . ? Fe2 C20 C21 C22 59.1(4) . . . . ? C24 C20 C21 Fe2 -60.4(4) . . . . ? C20 C21 C22 C23 1.4(7) . . . . ? Fe2 C21 C22 C23 59.6(4) . . . . ? C20 C21 C22 Fe2 -58.2(4) . . . . ? C21 C22 C23 C24 -0.8(7) . . . . ? Fe2 C22 C23 C24 59.0(4) . . . . ? C21 C22 C23 Fe2 -59.9(4) . . . . ? C22 C23 C24 C20 0.0(6) . . . . ? Fe2 C23 C24 C20 59.6(4) . . . . ? C22 C23 C24 Fe2 -59.6(4) . . . . ? C21 C20 C24 C23 0.7(5) . . . . ? Fe2 C20 C24 C23 -61.6(4) . . . . ? C21 C20 C24 Fe2 62.3(4) . . . . ? _refine_diff_density_max 2.873 _refine_diff_density_min -1.197 _refine_diff_density_rms 0.142 _shelxl_version_number 2014-3 _shelx_res_file ; TITL mo_MLJS08x4 2015-11-29 18:24 CELL 0.71073 5.7937 12.0602 16.0671 111.236 92.085 93.431 ZERR 2.00 0.0129 0.0329 0.0392 0.119 0.094 0.105 LATT 1 SFAC C H S FE UNIT 48 52 4 4 MERG 2 EADP C23 C24 C20 C21 C22 SHEL 99 0.82 ACTA FMAP 2 PLAN 20 BOND $H CONF L.S. 10 SIZE 0.122 0.319 0.628 TEMP -123.15 WGHT 0.089700 4.415501 FVAR 0.61692 FE1 4 0.007610 0.397608 0.211044 11.00000 0.01814 0.01370 = 0.01003 0.00480 0.00112 0.00140 FE2 4 0.473038 0.139356 0.829270 11.00000 0.01974 0.01346 = 0.01320 0.00775 -0.00032 0.00030 S1 3 0.028363 0.155613 0.465737 11.00000 0.02749 0.03037 = 0.02383 0.01924 -0.00400 -0.00344 S2 3 0.375147 0.142174 0.466570 11.00000 0.03246 0.03493 = 0.01214 0.00779 0.00465 0.01486 C1 1 -0.004430 0.292218 0.446736 11.00000 0.02752 0.02932 = 0.02001 0.01678 0.00585 0.00850 AFIX 23 H1A 2 -0.169714 0.309060 0.449603 11.00000 -1.20000 H1B 2 0.084710 0.358730 0.494863 11.00000 -1.20000 AFIX 0 C2 1 0.077948 0.286652 0.357153 11.00000 0.02999 0.01876 = 0.01418 0.00812 0.00326 0.00351 AFIX 23 H2A 2 0.249144 0.288317 0.359011 11.00000 -1.20000 H2B 2 0.015442 0.210572 0.310273 11.00000 -1.20000 AFIX 0 C3 1 0.002675 0.388276 0.333689 11.00000 0.02265 0.01656 = 0.00899 0.00334 0.00167 0.00161 C4 1 -0.224515 0.397294 0.302892 11.00000 0.01979 0.02274 = 0.01681 0.00615 0.00310 0.00144 AFIX 43 H4 2 -0.353528 0.341072 0.294522 11.00000 -1.20000 AFIX 0 C5 1 -0.225268 0.504109 0.286916 11.00000 0.02491 0.02915 = 0.01755 0.00902 0.00435 0.01179 AFIX 43 H5 2 -0.355258 0.532680 0.265494 11.00000 -1.20000 AFIX 0 C6 1 0.001295 0.562320 0.308198 11.00000 0.03689 0.01304 = 0.01540 0.00435 0.00442 0.00461 AFIX 43 H6 2 0.049813 0.636214 0.303251 11.00000 -1.20000 AFIX 0 C7 1 0.141086 0.490843 0.337947 11.00000 0.02284 0.01930 = 0.01204 0.00390 -0.00026 0.00004 AFIX 43 H7 2 0.300396 0.508490 0.357444 11.00000 -1.20000 AFIX 0 C8 1 -0.124681 0.306874 0.083959 11.00000 0.02367 0.04860 = 0.01312 0.00082 -0.00168 0.00258 AFIX 43 H8 2 -0.284483 0.293103 0.064925 11.00000 -1.20000 AFIX 0 C9 1 0.006378 0.233390 0.113551 11.00000 0.05890 0.01694 = 0.01418 0.00081 0.01148 -0.00105 AFIX 43 H9 2 -0.048799 0.160229 0.118237 11.00000 -1.20000 AFIX 0 C10 1 0.233395 0.286198 0.135149 11.00000 0.03349 0.04271 = 0.01579 0.00555 0.00441 0.01876 AFIX 43 H10 2 0.358652 0.254868 0.156962 11.00000 -1.20000 AFIX 0 C11 1 0.244298 0.392199 0.119251 11.00000 0.03220 0.03525 = 0.01972 -0.00016 0.01173 -0.00973 AFIX 43 H11 2 0.377724 0.445964 0.128348 11.00000 -1.20000 AFIX 0 C12 1 0.024972 0.405519 0.087644 11.00000 0.06299 0.02861 = 0.01192 0.01004 0.00748 0.01273 AFIX 43 H12 2 -0.017041 0.470155 0.071284 11.00000 -1.20000 AFIX 0 C13 1 0.471475 0.218878 0.582646 11.00000 0.02088 0.02855 = 0.01382 0.00901 0.00088 0.00229 AFIX 23 H13A 2 0.642850 0.223870 0.588351 11.00000 -1.20000 H13B 2 0.422709 0.301314 0.602896 11.00000 -1.20000 AFIX 0 C14 1 0.376324 0.157724 0.642441 11.00000 0.03442 0.01789 = 0.01536 0.00851 -0.00368 0.00130 AFIX 23 H14A 2 0.206304 0.162170 0.643241 11.00000 -1.20000 H14B 2 0.407697 0.072442 0.617982 11.00000 -1.20000 AFIX 0 C15 1 0.481774 0.213598 0.735536 11.00000 0.02329 0.01560 = 0.01744 0.00991 0.00115 -0.00012 C16 1 0.374177 0.288147 0.811814 11.00000 0.02534 0.01747 = 0.02035 0.01026 0.00366 0.00237 AFIX 43 H16 2 0.221332 0.312756 0.812348 11.00000 -1.20000 AFIX 0 C17 1 0.534344 0.319258 0.886724 11.00000 0.03617 0.01798 = 0.01674 0.00767 0.00308 -0.00077 AFIX 43 H17 2 0.507163 0.367376 0.946514 11.00000 -1.20000 AFIX 0 C18 1 0.741147 0.266368 0.857092 11.00000 0.02636 0.02802 = 0.02412 0.01667 -0.00465 -0.00704 AFIX 43 H18 2 0.878036 0.273066 0.893526 11.00000 -1.20000 AFIX 0 C19 1 0.710647 0.201636 0.763988 11.00000 0.02153 0.02419 = 0.02226 0.01311 0.00248 0.00194 AFIX 43 H19 2 0.823474 0.157818 0.726953 11.00000 -1.20000 AFIX 0 C20 1 0.188379 0.036129 0.829915 11.00000 0.06957 0.03430 = 0.06720 0.03448 0.01125 -0.00647 AFIX 43 H20 2 0.033855 0.054231 0.821657 11.00000 -1.20000 AFIX 0 C21 1 0.328885 -0.028899 0.766823 11.00000 0.06957 0.03430 = 0.06720 0.03448 0.01125 -0.00647 AFIX 43 H21 2 0.283986 -0.066140 0.704909 11.00000 -1.20000 AFIX 0 C22 1 0.532328 -0.033390 0.802311 11.00000 0.06957 0.03430 = 0.06720 0.03448 0.01125 -0.00647 AFIX 43 H22 2 0.655862 -0.072827 0.769536 11.00000 -1.20000 AFIX 0 C23 1 0.544114 0.024028 0.889719 11.00000 0.06957 0.03430 = 0.06720 0.03448 0.01125 -0.00647 AFIX 43 H23 2 0.676670 0.030488 0.928253 11.00000 -1.20000 AFIX 0 C24 1 0.340688 0.073050 0.917656 11.00000 0.06957 0.03430 = 0.06720 0.03448 0.01125 -0.00647 AFIX 43 H24 2 0.302649 0.118672 0.976685 11.00000 -1.20000 AFIX 0 HKLF 4 REM mo_MLJS08x4 2015-11-29 18:24 REM R1 = 0.0553 for 3626 Fo > 4sig(Fo) and 0.0588 for all 3946 data REM 229 parameters refined using 0 restraints END WGHT 0.0881 4.5410 REM Highest difference peak 2.873, deepest hole 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4 0 1582.79 58.3166 1 -2 4 0 1564.06 58.6205 6 -2 4 0 1726.67 57.6759 3 1 -4 0 42.2909 2.90927 8 1 -4 0 44.3077 3.31680 6 1 -4 0 45.5699 2.73240 8 1 -4 0 39.1784 3.69313 1 1 -4 0 46.2626 3.31550 1 1 -4 0 51.0225 3.32799 5 1 -4 0 45.1058 3.57177 7 -1 4 0 46.5117 3.46387 6 -1 4 0 52.1122 2.52691 3 -1 4 0 46.9120 2.84856 8 -1 4 0 44.3091 3.19135 1 -1 4 0 47.4504 3.58510 7 -1 4 0 47.3663 3.18852 8 -1 4 0 43.2445 3.48748 1 0 -4 0 1655.56 61.4214 6 0 -4 0 1759.88 61.3569 8 0 -4 0 1848.60 62.7330 1 0 -4 0 1667.60 61.4440 8 0 -4 0 1596.61 61.8936 1 0 -4 0 1932.55 62.5060 5 0 4 0 1723.14 61.7142 8 0 4 0 1737.07 62.5750 7 0 4 0 1753.07 61.6462 6 0 4 0 1708.12 61.8740 1 0 4 0 1627.71 61.3128 8 0 4 0 1836.08 62.4679 1 -1 -4 0 16.0825 1.47449 8 -1 -4 0 17.0336 2.31972 5 -1 -4 0 22.7123 4.19735 2 -1 -4 0 13.5970 3.91733 1 -1 -4 0 14.5130 1.29267 8 -1 -4 0 15.2458 1.18111 9 1 4 0 14.5705 1.69785 8 1 4 0 16.6763 1.58690 8 1 4 0 19.4234 1.99897 1 1 4 0 16.8688 1.64845 6 1 4 0 15.3133 1.13320 4 -2 -4 0 2121.85 73.0526 1 -2 -4 0 1980.10 76.7656 1 -2 -4 0 2097.80 77.1650 2 -2 -4 0 2071.88 73.1632 9 -2 -4 0 2214.18 74.6439 5 2 4 0 1997.83 72.7597 8 2 4 0 2012.31 72.7892 9 2 4 0 2023.09 73.3593 4 2 4 0 2051.98 74.0104 1 2 4 0 2122.77 73.2047 1 2 4 0 2071.06 72.9724 8 -3 -4 0 3.90444 5.84350 2 -3 -4 0 -0.2377 1.77869 1 -3 -4 0 -0.3842 1.34028 9 -3 -4 0 0.18150 0.86380 1 -3 -4 0 -1.9119 2.12750 5 3 4 0 1.37392 2.51231 1 3 4 0 -2.1282 2.15875 4 3 4 0 0.57959 1.13372 8 3 4 0 -0.2759 1.13167 9 3 4 0 -1.4148 1.86519 1 3 4 0 0.76680 1.27126 6 3 4 0 -1.9265 0.78172 8 -4 -4 0 383.211 16.0364 5 -4 -4 0 357.995 22.6226 2 4 4 0 368.190 17.0274 1 4 4 0 392.196 16.8522 4 4 4 0 357.906 14.7985 8 4 4 0 384.862 13.9837 8 4 4 0 371.887 14.7754 6 4 4 0 384.154 15.4828 9 4 4 0 393.906 14.4949 1 -5 -4 0 23.1480 3.85123 5 -5 -4 0 18.4764 9.45886 2 5 4 0 21.7839 4.14833 1 5 4 0 14.1379 3.07160 6 5 4 0 18.5807 1.89295 8 5 4 0 18.2077 3.38753 9 5 4 0 21.2822 5.97457 4 5 4 0 18.1006 2.14842 1 5 4 0 18.3935 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110.147 7.24992 8 5 -6 0 101.235 8.95692 9 5 -6 0 92.6618 7.21510 8 5 -6 0 105.089 9.46326 6 5 -6 0 114.942 10.6335 1 -5 6 0 97.6274 7.39478 1 -5 6 0 135.037 16.4770 2 -5 6 0 101.131 7.72655 8 -5 6 0 101.082 7.35565 3 -5 6 0 111.935 8.55142 8 4 -6 0 91.3925 8.51600 1 4 -6 0 79.6107 5.94606 8 4 -6 0 82.3001 6.13056 7 4 -6 0 74.7061 6.97090 9 4 -6 0 88.8270 7.16268 1 4 -6 0 92.3975 7.87756 6 4 -6 0 91.1830 5.87288 8 -4 6 0 83.3089 6.76959 8 -4 6 0 86.2408 6.74114 1 -4 6 0 80.7513 8.15261 6 -4 6 0 85.5484 6.73717 1 -4 6 0 90.8246 5.97311 3 -4 6 0 84.7164 6.74819 8 3 -6 0 865.625 30.4441 5 3 -6 0 818.840 31.2714 8 3 -6 0 830.736 32.1408 1 3 -6 0 797.244 32.9453 1 3 -6 0 821.396 30.9276 8 3 -6 0 800.860 31.1746 7 3 -6 0 808.916 32.2896 6 -3 6 0 813.077 31.4066 8 -3 6 0 825.932 31.8352 1 -3 6 0 842.165 31.9843 1 -3 6 0 800.898 31.6596 8 -3 6 0 811.474 43.8480 7 -3 6 0 878.912 30.9569 3 2 -6 0 263.980 13.5378 1 2 -6 0 275.851 11.5475 8 2 -6 0 277.027 12.5625 1 2 -6 0 275.631 11.9498 8 2 -6 0 273.317 12.6143 7 2 -6 0 291.099 11.8424 5 2 -6 0 274.663 12.5316 6 -2 6 0 286.310 12.6746 1 -2 6 0 263.744 12.2950 1 -2 6 0 296.550 11.2292 3 -2 6 0 268.126 11.7469 8 -2 6 0 281.757 12.3464 8 -2 6 0 283.766 14.7374 7 -2 6 0 260.431 12.6737 6 1 -6 0 1974.95 72.1712 1 1 -6 0 1968.73 69.4608 8 1 -6 0 1918.58 69.7216 8 1 -6 0 1910.35 70.2805 1 1 -6 0 1938.00 70.1070 6 1 -6 0 2046.23 70.3617 5 -1 6 0 1962.94 70.7068 1 -1 6 0 1860.20 69.4970 8 -1 6 0 1982.48 70.3636 1 -1 6 0 2014.20 70.3432 6 -1 6 0 1889.70 70.5941 7 -1 6 0 1926.03 70.1150 8 0 -6 0 73.3626 6.16669 5 0 -6 0 71.0934 4.09408 8 0 -6 0 77.1785 4.91578 1 0 -6 0 78.6922 4.18401 8 0 -6 0 73.5346 4.34550 6 0 -6 0 80.0155 6.29398 1 0 6 0 72.1219 5.33137 1 0 6 0 74.8459 4.72500 6 0 6 0 74.4617 4.18883 8 0 6 0 70.6592 4.82334 1 0 6 0 78.5150 5.83723 7 0 6 0 71.7718 4.75458 8 -1 -6 0 243.341 11.3844 5 -1 -6 0 239.411 9.42349 8 -1 -6 0 222.035 9.13960 8 -1 -6 0 234.190 8.73715 9 -1 -6 0 247.210 14.7281 1 1 6 0 230.550 9.53895 8 1 6 0 236.573 9.61347 6 1 6 0 224.362 10.0660 8 1 6 0 233.620 10.1733 1 1 6 0 221.243 12.3263 7 1 6 0 221.755 10.7643 1 -2 -6 0 204.076 12.7730 2 -2 -6 0 220.726 10.9330 5 -2 -6 0 214.135 8.54760 9 -2 -6 0 212.811 9.17753 1 -2 -6 0 222.765 17.1368 1 2 6 0 215.792 8.81111 8 2 6 0 199.068 12.9403 7 2 6 0 208.364 8.27916 4 2 6 0 208.898 8.14822 9 2 6 0 209.493 9.34433 1 2 6 0 210.335 8.50955 6 2 6 0 204.082 10.1667 1 2 6 0 216.575 9.40184 8 -3 -6 0 58.7488 4.05843 9 -3 -6 0 56.6767 3.69413 1 -3 -6 0 49.3305 5.34716 5 -3 -6 0 72.1083 10.4285 2 3 6 0 59.0375 4.22010 1 3 6 0 56.3245 3.10173 6 3 6 0 54.2151 3.39752 6 3 6 0 52.4190 4.40542 4 3 6 0 57.3176 5.66185 1 3 6 0 56.8911 3.74637 8 3 6 0 60.0925 3.26747 9 3 6 0 59.0800 4.54086 8 -4 -6 0 130.656 15.4567 2 -4 -6 0 136.212 8.79462 5 4 6 0 132.597 6.56291 9 4 6 0 153.121 7.09712 1 4 6 0 122.024 9.86886 4 4 6 0 130.720 7.69296 8 4 6 0 142.937 6.62022 8 -5 -6 0 54.0272 13.0991 2 -5 -6 0 51.9862 6.21848 5 5 6 0 48.6322 4.96442 9 5 6 0 66.8564 7.47566 4 5 6 0 50.6172 4.46952 8 5 6 0 51.7808 4.20947 1 5 6 0 40.8572 5.06270 1 5 6 0 46.6462 5.85376 8 -6 -6 0 10.7736 4.37827 5 -6 -6 0 6.06764 11.7272 2 6 6 0 10.4116 3.16120 8 6 6 0 14.9687 12.7029 7 6 6 0 6.35673 3.67223 9 6 6 0 7.37309 7.41801 8 -7 -6 0 22.7561 5.83592 5 -7 -6 0 15.3905 14.0650 2 7 6 0 15.9497 15.5201 7 7 6 0 15.5946 5.78282 9 7 -7 0 35.8131 9.01399 1 7 -7 0 42.0890 9.75437 6 7 -7 0 45.6018 6.33153 8 7 -7 0 42.2207 9.01280 9 -7 7 0 58.1382 21.7161 2 -7 7 0 34.0615 5.92598 3 6 -7 0 35.9270 11.3768 4 6 -7 0 51.9190 6.52311 8 6 -7 0 63.7505 11.0366 1 6 -7 0 55.6257 8.46698 6 6 -7 0 48.2986 5.89154 8 6 -7 0 60.9176 8.37988 1 6 -7 0 64.8816 8.38200 9 -6 7 0 66.6236 17.4284 2 -6 7 0 57.4704 6.58291 8 -6 7 0 65.0958 6.43491 8 -6 7 0 69.7810 10.6723 6 -6 7 0 68.8251 6.87394 3 -6 7 0 71.4489 8.57132 1 5 -7 0 11.8573 4.76188 9 5 -7 0 15.7656 3.68992 8 5 -7 0 16.5816 4.64999 7 5 -7 0 12.9511 4.01930 8 5 -7 0 12.7146 6.75544 1 -5 7 0 18.7814 3.94632 3 -5 7 0 19.6001 4.89672 8 -5 7 0 23.9625 6.50479 6 -5 7 0 18.3811 4.45469 1 -5 7 0 13.1590 4.85644 8 -5 7 0 15.9155 4.39940 1 4 -7 0 13.0983 3.67475 1 4 -7 0 10.2205 2.93012 8 4 -7 0 22.8062 3.15688 5 4 -7 0 12.4887 3.74466 9 4 -7 0 20.5468 4.30629 7 4 -7 0 16.4392 4.88508 6 4 -7 0 19.0090 3.33685 8 4 -7 0 20.0010 5.66659 1 -4 7 0 51.0759 28.7980 7 -4 7 0 15.0208 3.75316 1 -4 7 0 15.1440 4.21938 8 -4 7 0 23.1197 4.22144 1 -4 7 0 18.9307 3.42091 3 -4 7 0 22.1649 4.06718 8 3 -7 0 2.94788 3.78568 1 3 -7 0 6.77942 2.27762 8 3 -7 0 4.37793 3.65795 7 3 -7 0 5.33386 2.22956 5 3 -7 0 4.26815 2.14394 8 3 -7 0 4.33224 2.87229 1 3 -7 0 3.05456 2.94014 6 -3 7 0 8.73208 2.31433 3 -3 7 0 5.44554 3.48743 1 -3 7 0 10.3612 3.29437 8 -3 7 0 2.51101 3.84182 6 -3 7 0 4.10523 2.51972 1 -3 7 0 -0.9539 12.5650 7 -3 7 0 2.02639 2.34168 8 2 -7 0 810.295 32.1754 5 2 -7 0 845.679 30.9470 8 2 -7 0 817.876 31.2295 8 2 -7 0 795.940 31.7756 6 2 -7 0 765.715 32.3392 7 2 -7 0 769.892 33.5694 1 2 -7 0 881.416 32.2970 1 -2 7 0 831.755 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2071.67 71.7212 1 -3 -1 3 1990.16 71.9192 1 -3 -1 3 1998.87 72.5269 9 2 1 -3 559.853 19.7093 8 2 1 -3 556.896 19.9021 6 2 1 -3 535.249 20.3681 9 2 1 -3 535.659 21.0388 8 2 1 -3 519.877 21.9523 1 2 1 -3 554.558 20.2702 1 -2 -1 3 550.745 20.9356 1 -2 -1 3 542.101 20.5735 9 -2 -1 3 527.781 20.5994 8 -2 -1 3 547.219 20.0407 6 -2 -1 3 544.272 19.6274 8 1 1 -3 1521.88 55.4947 1 1 1 -3 1532.34 53.6321 1 1 1 -3 1571.32 54.4021 8 1 1 -3 1417.02 53.3541 9 -1 -1 3 1580.50 53.6919 1 -1 -1 3 1465.08 53.4959 9 -1 -1 3 1566.48 54.3371 8 -1 -1 3 1474.58 53.1817 6 -1 -1 3 1485.62 53.1549 8 -1 -1 3 1511.01 54.7289 1 0 1 -3 817.269 27.2963 8 0 1 -3 840.343 34.4730 7 0 1 -3 864.353 29.8492 1 0 1 -3 705.978 26.6348 1 0 1 -3 658.670 26.2790 9 0 1 -3 738.219 26.4646 8 0 -1 3 644.322 26.6612 1 0 -1 3 656.314 26.2777 9 0 -1 3 820.031 29.0684 1 0 -1 3 793.999 27.3756 8 0 -1 3 713.667 26.4133 8 -1 1 -3 786.034 27.1269 8 -1 1 -3 768.095 27.5347 7 -1 1 -3 756.102 27.9949 4 -1 1 -3 882.228 27.7579 3 -1 1 -3 715.690 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38.6701 9.52317 2 1 9 -5 581.657 23.3662 1 1 9 -5 569.978 24.6313 8 1 9 -5 564.051 22.4974 8 1 9 -5 568.114 25.7018 1 -1 -9 5 586.996 23.5219 1 -1 -9 5 565.583 21.6317 9 -1 -9 5 609.734 22.4322 8 -1 -9 5 581.837 22.7897 8 -1 -9 5 585.171 21.6284 6 -1 -9 5 565.423 25.4944 5 -1 -9 5 552.846 25.0329 2 -1 -9 5 534.988 35.4726 1 0 9 -5 326.471 16.5466 1 0 9 -5 318.040 13.5752 8 0 9 -5 304.042 14.5928 1 0 9 -5 317.281 13.6179 6 0 9 -5 334.506 15.9385 8 0 -9 5 338.506 13.8412 8 0 -9 5 317.317 14.6111 1 0 -9 5 309.859 12.6561 9 0 -9 5 331.221 16.4097 5 0 -9 5 329.279 14.2611 8 0 -9 5 301.253 13.6482 6 0 -9 5 332.464 26.0696 1 -1 9 -5 929.464 35.2120 8 -1 9 -5 932.434 35.8704 6 -1 9 -5 953.905 37.4468 8 -1 9 -5 889.184 36.8129 7 -1 9 -5 947.954 38.0385 1 -1 9 -5 934.148 36.2411 1 1 -9 5 970.798 36.3276 8 1 -9 5 977.373 35.5150 8 1 -9 5 951.356 36.4567 1 1 -9 5 977.073 37.9577 5 1 -9 5 944.757 33.8561 4 1 -9 5 937.118 36.0251 6 1 -9 5 900.140 44.3130 1 -2 9 -5 291.203 14.0144 6 -2 9 -5 285.892 13.0160 7 -2 9 -5 284.806 14.9929 8 -2 9 -5 280.991 12.5419 8 -2 9 -5 286.160 14.9947 1 2 -9 5 287.105 13.8560 1 2 -9 5 291.768 12.7119 8 2 -9 5 265.023 22.6231 1 2 -9 5 292.202 14.1866 6 2 -9 5 291.000 14.3261 5 2 -9 5 267.828 12.1469 4 2 -9 5 293.627 13.7622 8 -3 9 -5 65.3813 6.69114 1 -3 9 -5 69.4150 5.52350 8 -3 9 -5 77.1322 8.20075 8 -3 9 -5 87.5800 8.95041 7 -3 9 -5 66.1139 5.52680 3 -3 9 -5 70.5959 7.45318 1 -3 9 -5 66.3259 8.51523 6 3 -9 5 71.0752 6.83052 1 3 -9 5 63.8162 12.3190 1 3 -9 5 79.9563 5.77162 8 3 -9 5 59.3349 6.94205 6 3 -9 5 61.2580 6.57230 4 3 -9 5 63.6269 6.55226 8 3 -9 5 59.8098 6.54404 5 -4 9 -5 69.7969 8.04948 8 -4 9 -5 71.6894 7.76093 1 -4 9 -5 48.9411 5.61912 3 -4 9 -5 65.0665 6.08068 8 4 -9 5 68.8056 12.3775 1 4 -9 5 65.7311 8.06511 6 4 -9 5 65.8819 6.30127 8 4 -9 5 49.8837 5.71283 5 4 -9 5 57.2839 6.92281 1 4 -9 5 73.9098 8.42268 4 4 -9 5 56.8020 6.48848 8 -5 9 -5 8.62813 4.45089 1 -5 9 -5 4.74966 6.89215 6 -5 9 -5 4.72779 3.76354 8 -5 9 -5 6.02848 3.41008 3 -5 9 -5 16.9016 4.78745 1 -5 9 -5 1.44687 5.60919 8 5 -9 5 6.49095 3.90151 8 5 -9 5 -1.2320 12.2188 1 5 -9 5 19.0476 7.78740 4 5 -9 5 14.6123 4.70454 1 5 -9 5 3.82967 5.49571 6 5 -9 5 5.04370 5.10285 8 -6 9 -5 115.315 9.51297 3 -6 9 -5 89.1559 10.5275 1 6 -9 5 136.527 10.6038 8 6 -9 5 116.429 11.3015 1 6 -9 5 129.747 15.6203 8 6 -9 5 142.404 12.8447 9 6 -9 5 115.155 14.1717 6 6 -9 5 102.873 22.5122 1 -7 9 -5 17.0051 5.34321 3 7 -9 5 27.0416 7.07596 8 7 -9 5 41.7832 11.4848 6 7 -9 5 28.8754 7.97280 1 7 -9 5 28.6573 8.71536 9 7 8 -5 25.0517 7.46245 8 7 8 -5 15.3622 9.65768 1 7 8 -5 17.6065 5.84238 9 -7 -8 5 49.4254 19.1259 2 -7 -8 5 17.7102 6.35636 5 6 8 -5 213.723 13.4843 1 6 8 -5 230.968 12.7892 8 6 8 -5 212.308 11.6769 9 6 8 -5 245.504 28.3794 8 6 8 -5 230.776 22.5231 1 -6 -8 5 201.977 26.0318 2 -6 -8 5 235.584 14.8396 5 5 8 -5 22.3305 11.2158 1 5 8 -5 6.29027 2.81647 9 5 8 -5 13.8158 6.56278 4 5 8 -5 6.44881 8.13566 8 5 8 -5 1.80298 4.20988 1 5 8 -5 15.3652 3.75377 8 -5 -8 5 0.73420 5.66449 1 -5 -8 5 1.88987 4.70781 9 -5 -8 5 7.16823 4.87920 5 -5 -8 5 21.4368 12.7767 2 -5 -8 5 6.47921 3.32847 1 4 8 -5 347.113 13.9080 9 4 8 -5 330.917 18.4290 8 4 8 -5 345.057 15.5178 1 4 8 -5 347.395 14.7556 8 4 8 -5 314.042 24.1319 1 -4 -8 5 342.441 14.7443 1 -4 -8 5 334.576 17.9476 5 -4 -8 5 334.726 15.4960 9 -4 -8 5 286.216 23.6748 2 3 8 -5 158.176 7.02453 9 3 8 -5 148.324 11.2518 8 3 8 -5 151.676 8.13183 8 3 8 -5 148.417 8.63616 1 3 8 -5 143.492 17.4774 1 -3 -8 5 158.109 8.37614 9 -3 -8 5 150.622 6.11556 8 -3 -8 5 141.942 9.09078 1 -3 -8 5 161.472 20.7424 1 -3 -8 5 149.540 11.1366 5 -3 -8 5 126.913 15.9235 2 -3 -8 5 145.286 6.39278 8 2 8 -5 854.534 32.1369 1 2 8 -5 843.445 33.4130 8 2 8 -5 780.441 36.9935 1 2 8 -5 828.094 31.4371 8 -2 -8 5 816.365 36.4100 2 -2 -8 5 852.256 31.1620 9 -2 -8 5 871.492 34.7891 5 -2 -8 5 813.291 30.5743 8 -2 -8 5 761.818 43.4882 1 -2 -8 5 878.311 32.1844 1 -2 -8 5 836.447 31.0793 8 1 8 -5 170.147 12.1017 1 1 8 -5 177.044 8.53399 8 1 8 -5 196.302 10.7521 8 1 8 -5 156.325 7.33910 4 1 8 -5 191.644 9.55545 1 -1 -8 5 176.472 12.2129 2 -1 -8 5 181.336 8.94309 8 -1 -8 5 185.680 21.6855 1 -1 -8 5 190.796 8.54195 8 -1 -8 5 181.169 7.87908 9 -1 -8 5 185.121 7.82048 6 -1 -8 5 180.966 11.1705 5 -1 -8 5 186.759 9.39030 1 0 8 -5 2990.19 106.943 1 0 8 -5 2949.27 104.121 8 0 8 -5 3077.08 106.126 8 0 8 -5 2850.37 104.859 1 0 8 -5 2783.93 103.842 6 0 -8 5 3012.42 104.189 8 0 -8 5 2858.14 104.795 8 0 -8 5 2835.47 104.084 6 0 -8 5 2727.17 104.777 1 0 -8 5 3423.56 114.991 1 0 -8 5 3031.10 106.746 5 0 -8 5 2710.37 103.169 9 -1 8 -5 4.10487 2.19442 1 -1 8 -5 0.24997 3.71164 1 -1 8 -5 1.74343 1.46687 8 -1 8 -5 2.32208 3.46798 7 -1 8 -5 6.74973 3.43392 8 -1 8 -5 5.30200 2.62270 6 1 -8 5 2.91090 1.74798 8 1 -8 5 4.29603 3.15365 5 1 -8 5 2.17432 1.86007 1 1 -8 5 4.61769 2.36511 6 1 -8 5 5.59246 1.47303 4 1 -8 5 0.93952 2.30840 8 1 -8 5 13.5517 8.48736 1 -2 8 -5 1955.36 73.1906 1 -2 8 -5 2037.41 72.1321 1 -2 8 -5 1984.11 71.0079 8 -2 8 -5 1954.71 71.0042 7 -2 8 -5 2079.92 73.2243 8 -2 8 -5 1988.32 72.2659 6 2 -8 5 1698.92 71.7406 8 2 -8 5 2041.29 71.1685 4 2 -8 5 2079.63 72.8032 5 2 -8 5 1962.95 72.1907 8 2 -8 5 1992.52 72.2703 1 2 -8 5 1926.64 78.5448 1 2 -8 5 2007.05 72.5821 6 -3 8 -5 7.47911 2.26991 8 -3 8 -5 9.96211 2.85677 3 -3 8 -5 6.68346 3.46268 1 -3 8 -5 1.37195 3.85131 6 -3 8 -5 11.4573 4.23416 8 -3 8 -5 6.90458 2.93208 1 3 -8 5 -1.5691 7.38791 1 3 -8 5 9.01014 3.59417 4 3 -8 5 6.93597 2.61037 8 3 -8 5 13.9349 3.54561 5 3 -8 5 9.21249 3.27777 8 3 -8 5 6.06835 3.62540 6 3 -8 5 6.20494 2.96639 1 -4 8 -5 277.326 12.3972 8 -4 8 -5 259.746 14.1729 1 -4 8 -5 255.211 14.0338 8 -4 8 -5 264.834 12.8977 3 4 -8 5 256.282 20.3318 1 4 -8 5 267.346 13.4162 8 4 -8 5 274.806 14.4567 4 4 -8 5 292.789 12.1282 5 4 -8 5 272.998 14.8155 6 4 -8 5 266.228 13.5026 1 4 -8 5 271.740 12.4634 8 -5 8 -5 10.5676 3.66484 3 -5 8 -5 12.0804 4.60172 8 -5 8 -5 21.7132 3.81852 8 -5 8 -5 4.10660 6.17857 6 5 -8 5 22.3528 10.7676 1 5 -8 5 16.0721 4.17860 8 5 -8 5 23.6344 5.81554 6 5 -8 5 16.2535 4.35292 1 5 -8 5 20.4703 4.20229 8 5 -8 5 29.2362 7.71569 4 -6 8 -5 173.688 11.5054 3 -6 8 -5 200.902 11.6604 1 6 -8 5 175.709 15.5125 6 6 -8 5 182.407 12.6796 8 6 -8 5 164.407 11.3762 8 6 -8 5 177.267 12.4022 1 6 -8 5 165.992 22.3358 1 6 -8 5 199.456 14.1395 9 -7 8 -5 12.2227 5.25203 3 7 -8 5 26.6384 6.64358 8 7 -8 5 9.59649 8.31857 9 7 -8 5 21.7195 7.20201 1 7 -8 5 16.8903 9.31826 6 7 7 -5 34.0433 6.33512 9 7 7 -5 11.0112 14.7808 1 7 7 -5 35.3877 6.76291 8 -7 -7 5 30.2309 17.4492 2 -7 -7 5 26.8793 6.44367 5 6 7 -5 51.5320 6.62691 1 6 7 -5 54.6462 14.1199 1 6 7 -5 67.6431 6.31824 8 6 7 -5 68.5366 12.4061 8 6 7 -5 57.7887 6.91103 9 -6 -7 5 73.6210 9.48661 5 -6 -7 5 60.5871 17.1853 2 5 7 -5 39.4311 8.50567 8 5 7 -5 33.2423 4.22050 8 5 7 -5 35.8454 12.4162 1 5 7 -5 40.3624 4.87231 9 5 7 -5 32.0986 4.82889 1 -5 -7 5 25.1372 5.51988 1 -5 -7 5 34.3904 4.12632 1 -5 -7 5 28.4210 6.15001 5 -5 -7 5 47.1919 12.8990 2 -5 -7 5 28.2914 5.46490 9 4 7 -5 2.95819 2.34920 8 4 7 -5 3.93017 3.01629 1 4 7 -5 5.19207 1.95145 9 4 7 -5 0.44101 9.32387 1 4 7 -5 6.10220 6.10153 8 -4 -7 5 3.38982 3.15868 9 -4 -7 5 -2.3852 9.63363 2 -4 -7 5 0.97190 6.09722 1 -4 -7 5 2.19655 4.06639 5 -4 -7 5 2.22026 2.46132 1 3 7 -5 73.7168 11.9481 1 3 7 -5 79.5115 4.47225 9 3 7 -5 69.9285 8.00850 8 3 7 -5 74.3514 5.24556 8 3 7 -5 75.8880 5.88313 1 -3 -7 5 66.6118 5.68315 1 -3 -7 5 78.8956 3.95376 8 -3 -7 5 62.2014 7.82110 5 -3 -7 5 76.2081 11.3337 1 -3 -7 5 78.5971 3.60375 8 -3 -7 5 77.6999 5.69369 9 -3 -7 5 77.9428 12.4300 2 2 7 -5 8.41499 3.49034 8 2 7 -5 9.60395 1.60015 9 2 7 -5 9.66186 2.17033 8 2 7 -5 9.60637 2.45405 1 2 7 -5 7.66581 6.66753 1 -2 -7 5 9.17359 2.04208 9 -2 -7 5 10.8023 1.65630 8 -2 -7 5 6.86902 7.11955 2 -2 -7 5 6.88002 2.18051 1 -2 -7 5 10.1048 2.12434 8 -2 -7 5 -6.0912 9.38361 1 1 7 -5 11.6746 1.42004 4 1 7 -5 14.2805 3.44210 8 1 7 -5 9.65659 2.45678 1 1 7 -5 11.9442 6.01965 1 1 7 -5 7.84047 2.13206 8 -1 -7 5 11.3446 2.15051 8 -1 -7 5 13.3822 10.1054 1 -1 -7 5 7.43388 2.17376 1 -1 -7 5 10.2378 5.83926 2 -1 -7 5 9.24381 2.30987 8 -1 -7 5 10.5458 1.62191 9 -1 -7 5 8.15355 1.80028 6 0 7 -5 300.485 12.0882 4 0 7 -5 320.924 12.8734 8 0 7 -5 300.270 13.4360 1 0 7 -5 299.035 12.7560 6 0 7 -5 327.625 15.7859 1 0 7 -5 325.700 14.6365 8 0 -7 5 312.779 13.0802 6 0 -7 5 300.134 12.1320 9 0 -7 5 329.465 12.9975 8 0 -7 5 317.758 13.7279 8 0 -7 5 305.747 13.5813 1 0 -7 5 383.540 23.6930 1 -1 7 -5 206.323 9.88630 6 -1 7 -5 210.942 11.0060 8 -1 7 -5 212.422 11.5579 1 -1 7 -5 204.479 9.12332 8 -1 7 -5 210.963 10.0291 1 1 -7 5 211.218 10.0832 6 1 -7 5 206.948 16.9407 1 1 -7 5 214.915 10.1192 1 1 -7 5 204.125 9.28436 8 1 -7 5 211.084 10.2828 8 1 -7 5 207.340 8.57806 4 -2 7 -5 324.741 13.2326 7 -2 7 -5 325.867 15.3868 1 -2 7 -5 338.632 15.4402 8 -2 7 -5 320.573 14.2258 1 -2 7 -5 328.903 14.7549 6 -2 7 -5 319.325 13.3297 8 2 -7 5 338.139 13.8797 4 2 -7 5 332.195 14.6773 8 2 -7 5 332.824 13.5820 8 2 -7 5 323.833 14.4419 1 2 -7 5 343.731 15.0921 6 2 -7 5 338.233 20.8561 1 -3 7 -5 623.307 23.8782 8 -3 7 -5 639.415 25.6603 8 -3 7 -5 613.978 24.7600 1 -3 7 -5 654.152 25.6884 1 -3 7 -5 628.474 25.7493 6 -3 7 -5 629.282 24.5988 3 3 -7 5 669.131 24.8869 5 3 -7 5 630.248 25.1171 4 3 -7 5 639.967 26.2738 6 3 -7 5 611.114 25.0818 8 3 -7 5 583.944 30.3502 1 3 -7 5 620.749 25.0197 1 3 -7 5 581.511 24.8125 8 -4 7 -5 42.7650 4.27450 8 -4 7 -5 38.6451 4.74711 3 -4 7 -5 52.1892 5.62522 8 4 -7 5 36.8611 4.59237 5 4 -7 5 43.6337 5.09562 8 4 -7 5 36.2511 4.36992 8 4 -7 5 50.2265 6.95125 4 4 -7 5 27.5702 5.35146 6 4 -7 5 38.3283 4.56853 1 4 -7 5 33.9043 8.48622 1 -5 7 -5 24.2352 6.15210 6 -5 7 -5 47.7555 5.81527 3 -5 7 -5 48.2386 5.99120 1 5 -7 5 50.3011 5.41168 8 5 -7 5 42.5874 5.36996 8 5 -7 5 30.9476 9.55314 1 -6 7 -5 5.54448 4.06414 3 -6 7 -5 14.7162 4.80366 1 -6 7 -5 6.55781 4.25854 1 6 -7 5 0.00928 14.8523 1 6 -7 5 -4.1687 5.26544 9 6 -7 5 13.4065 4.33877 8 6 -7 5 8.95272 4.45433 1 6 -7 5 14.1710 6.40784 6 6 -7 5 3.17345 3.91268 8 -7 7 -5 114.409 10.2501 3 7 -7 5 129.906 11.6337 8 7 -7 5 116.228 11.9933 1 7 -7 5 112.826 10.9624 8 7 -7 5 144.143 14.4132 6 7 -7 5 112.493 12.6711 9 7 6 -5 20.2020 5.70119 1 7 6 -5 27.9554 14.5496 8 7 6 -5 28.0894 5.60133 8 7 6 -5 5.24954 16.0415 1 7 6 -5 17.1047 5.32205 9 -7 -6 5 58.8028 19.1569 2 -7 -6 5 14.0205 5.65440 5 6 6 -5 134.982 9.88939 1 6 6 -5 167.356 9.54730 9 6 6 -5 155.625 17.6598 8 6 6 -5 150.128 8.84184 8 6 6 -5 132.558 19.9464 1 -6 -6 5 143.107 7.95520 1 -6 -6 5 153.509 11.1020 5 -6 -6 5 134.576 23.2893 2 -6 -6 5 136.319 8.88096 1 5 6 -5 5.70572 2.81208 9 5 6 -5 14.2228 3.99757 1 5 6 -5 20.7393 6.68484 8 5 6 -5 30.7437 19.3561 1 5 6 -5 7.21354 2.51700 8 -5 -6 5 -1.5122 3.82074 9 -5 -6 5 4.58017 4.20924 5 -5 -6 5 2.22954 2.65973 1 -5 -6 5 -8.1069 10.4088 2 4 6 -5 128.912 17.2296 1 4 6 -5 151.239 7.60073 8 4 6 -5 144.545 8.59740 1 4 6 -5 152.602 11.1992 8 4 6 -5 144.870 7.52014 9 -4 -6 5 158.012 10.3976 5 -4 -6 5 167.449 8.06799 1 -4 -6 5 140.409 11.3999 1 -4 -6 5 141.336 8.72284 9 -4 -6 5 151.943 18.8976 2 3 6 -5 0.78893 1.55337 8 3 6 -5 1.55590 1.28360 9 3 6 -5 0.23300 1.91595 1 3 6 -5 -2.3383 8.95272 1 3 6 -5 9.16737 3.93168 8 -3 -6 5 1.74209 0.88744 8 -3 -6 5 -0.4014 1.24733 8 -3 -6 5 7.75635 7.35269 2 -3 -6 5 0.66304 1.94942 1 -3 -6 5 2.31903 2.16337 9 -3 -6 5 8.28771 6.21227 1 2 6 -5 1870.10 66.5363 8 2 6 -5 1752.91 64.0091 9 2 6 -5 1780.39 65.0580 1 2 6 -5 1822.34 64.6922 8 2 6 -5 1722.21 71.3882 1 -2 -6 5 1783.14 72.6071 1 -2 -6 5 1817.90 63.9815 8 -2 -6 5 1877.05 65.2204 1 -2 -6 5 1784.75 64.6224 9 -2 -6 5 1806.82 69.6933 2 -2 -6 5 1819.10 64.7168 8 1 6 -5 325.835 13.7397 1 1 6 -5 287.448 19.0319 1 1 6 -5 338.048 14.9047 8 1 6 -5 332.010 13.2919 8 -1 -6 5 312.793 23.1419 1 -1 -6 5 317.858 13.7381 8 -1 -6 5 326.294 12.5250 6 -1 -6 5 343.239 13.8634 1 -1 -6 5 311.745 16.6612 2 -1 -6 5 341.496 13.0679 8 -1 -6 5 337.751 12.8663 9 0 6 -5 2148.22 73.2742 8 0 6 -5 1894.47 71.9003 1 0 6 -5 1929.75 70.8375 4 0 6 -5 2020.65 71.4643 8 0 -6 5 1998.93 72.3789 8 0 -6 5 2018.00 71.5077 8 0 -6 5 1985.61 72.1489 1 0 -6 5 1904.49 71.4625 6 0 -6 5 2323.70 80.2141 1 0 -6 5 1896.30 70.8314 9 -1 6 -5 4.89050 1.94249 4 -1 6 -5 2.46926 2.54849 8 -1 6 -5 6.41158 1.39727 8 -1 6 -5 5.77851 2.06718 6 -1 6 -5 9.23050 2.21922 1 -1 6 -5 1.86823 2.30647 1 1 -6 5 6.58663 1.84381 1 1 -6 5 3.68309 1.80249 6 1 -6 5 7.03818 2.21913 8 1 -6 5 7.47777 1.58570 4 1 -6 5 8.52712 1.57451 8 1 -6 5 10.8951 6.70394 1 -2 6 -5 301.323 13.1902 6 -2 6 -5 292.597 11.7973 8 -2 6 -5 292.796 12.6415 1 -2 6 -5 278.991 11.3741 7 -2 6 -5 313.030 12.3338 3 -2 6 -5 292.171 13.6020 8 -2 6 -5 296.506 13.8207 1 2 -6 5 297.903 13.4404 6 2 -6 5 291.442 12.4788 4 2 -6 5 292.124 13.0657 8 2 -6 5 296.646 11.9654 8 2 -6 5 270.423 17.8488 1 2 -6 5 279.290 12.6253 1 -3 6 -5 406.140 16.8498 8 -3 6 -5 380.804 15.0917 8 -3 6 -5 387.907 16.0012 3 -3 6 -5 377.561 16.9144 1 -3 6 -5 396.950 16.6403 1 3 -6 5 398.258 16.5673 8 3 -6 5 380.978 17.3952 6 3 -6 5 397.960 16.7275 4 3 -6 5 398.895 15.3871 8 3 -6 5 305.009 20.7785 1 3 -6 5 384.026 16.1710 1 -4 6 -5 73.5264 5.63661 1 -4 6 -5 67.9794 6.32604 1 -4 6 -5 68.6647 5.82124 8 -4 6 -5 75.9518 5.66772 3 -4 6 -5 74.6559 4.58535 8 -4 6 -5 73.3760 7.77619 6 4 -6 5 63.9956 4.83290 8 4 -6 5 76.9102 7.87430 6 4 -6 5 68.2192 9.38083 1 4 -6 5 69.7088 7.62997 4 4 -6 5 59.6714 5.77587 8 4 -6 5 65.5256 4.65340 5 4 -6 5 70.5957 5.75946 1 -5 6 -5 139.185 8.14896 1 -5 6 -5 133.140 8.79825 3 5 -6 5 169.026 15.9634 1 5 -6 5 143.448 8.71847 8 5 -6 5 138.559 7.70053 8 5 -6 5 136.553 8.62023 1 5 -6 5 114.024 10.8248 6 -6 6 -5 16.9141 4.12887 1 -6 6 -5 19.6354 4.60264 3 -6 6 -5 7.17719 11.2897 2 -6 6 -5 30.7500 4.39313 1 6 -6 5 9.46641 8.75580 4 6 -6 5 22.4393 4.62283 8 6 -6 5 11.5513 6.32431 6 6 -6 5 29.2369 4.46438 8 6 -6 5 23.5858 5.68840 9 6 -6 5 23.4251 4.73366 1 6 -6 5 19.7063 13.7761 1 -7 6 -5 35.9904 6.17983 1 -7 6 -5 45.1710 14.4955 2 -7 6 -5 37.2987 6.72730 3 7 -6 5 33.3841 6.93417 1 7 -6 5 40.2468 9.78708 6 7 -6 5 32.1697 5.97521 8 7 -6 5 33.7670 6.15636 8 7 -6 5 42.7115 8.82451 9 7 -6 5 24.4020 19.4255 1 7 5 -5 173.845 24.4835 1 7 5 -5 137.041 9.39655 8 7 5 -5 128.827 10.8625 9 7 5 -5 122.353 10.8054 1 7 5 -5 122.290 15.3676 8 -7 -5 5 106.758 21.1886 2 -7 -5 5 108.344 10.8523 5 6 5 -5 0.12861 3.66121 9 6 5 -5 5.30316 3.80681 1 6 5 -5 2.49643 2.77846 8 6 5 -5 4.37628 8.41592 8 6 5 -5 5.68488 16.0707 1 -6 -5 5 3.52260 4.65577 5 -6 -5 5 9.71274 3.16866 1 -6 -5 5 4.85317 2.99910 1 -6 -5 5 7.29530 15.7489 2 5 5 -5 93.5390 9.90544 8 5 5 -5 96.6044 18.5920 1 5 5 -5 91.7315 7.20498 1 5 5 -5 101.725 5.82247 8 5 5 -5 96.3129 6.74410 9 -5 -5 5 102.105 8.62229 9 -5 -5 5 60.3494 14.3272 2 -5 -5 5 100.281 6.22418 1 -5 -5 5 87.0850 8.85612 5 4 5 -5 11.9888 2.16144 8 4 5 -5 7.30300 4.65611 8 4 5 -5 9.80905 11.6171 1 4 5 -5 11.1665 2.34765 9 4 5 -5 8.99015 2.73565 1 -4 -5 5 13.2335 9.63759 2 -4 -5 5 8.95174 4.00376 1 -4 -5 5 12.4655 3.25806 9 -4 -5 5 9.21064 2.41048 1 -4 -5 5 7.56282 4.00726 5 3 5 -5 74.7181 7.19138 8 3 5 -5 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20.8111 1 -5 -2 6 514.774 20.4751 1 -5 -2 6 483.081 30.3309 2 -5 -2 6 416.367 20.3514 1 -5 -2 6 544.033 20.6394 6 -5 -2 6 510.212 22.3200 9 4 2 -6 21.1330 3.16383 9 4 2 -6 20.0807 2.50583 8 4 2 -6 21.4676 4.62162 8 4 2 -6 28.1252 8.34421 1 4 2 -6 16.9023 3.38303 1 -4 -2 6 6.30082 7.64115 2 -4 -2 6 18.1972 3.52222 9 -4 -2 6 16.6806 3.12779 6 -4 -2 6 19.4133 3.74236 1 -4 -2 6 19.9655 2.17193 8 -4 -2 6 25.3155 3.43440 8 3 2 -6 2299.15 88.6346 1 3 2 -6 2258.08 83.2505 9 3 2 -6 2375.71 83.7069 1 3 2 -6 2366.46 85.1374 8 -3 -2 6 2232.39 84.0763 8 -3 -2 6 2488.42 83.6966 1 -3 -2 6 2312.16 82.3910 8 -3 -2 6 2297.44 82.9198 6 -3 -2 6 2354.32 84.0607 9 -3 -2 6 2339.48 84.8435 1 2 2 -6 747.357 28.9859 8 2 2 -6 697.624 26.9591 9 2 2 -6 774.891 27.7661 1 2 2 -6 731.474 26.7519 8 2 2 -6 705.006 32.1050 1 -2 -2 6 748.890 26.6799 8 -2 -2 6 763.196 27.7328 1 -2 -2 6 703.410 26.7909 6 -2 -2 6 710.230 28.6630 8 -2 -2 6 739.301 27.5773 9 -2 -2 6 731.666 29.4849 1 1 2 -6 155.632 8.56242 8 1 2 -6 167.876 6.81581 9 1 2 -6 161.952 6.92769 8 1 2 -6 197.276 26.9896 7 1 2 -6 164.294 12.8521 1 1 2 -6 163.079 7.57271 1 -1 -2 6 163.910 7.10968 9 -1 -2 6 174.640 7.70346 1 -1 -2 6 166.797 10.2536 1 -1 -2 6 161.425 8.82525 8 0 2 -6 2507.92 95.6036 1 0 2 -6 3153.17 102.459 1 0 2 -6 2576.72 95.2051 8 0 2 -6 2844.07 96.6063 8 0 2 -6 3149.82 108.609 7 0 -2 6 2380.70 94.9132 9 0 -2 6 2919.08 99.5053 1 0 -2 6 2441.78 95.5683 1 0 -2 6 2794.15 96.9233 8 0 -2 6 2428.11 95.0399 8 -1 2 -6 419.639 15.2348 8 -1 2 -6 413.498 16.1554 4 -1 2 -6 408.796 18.5288 7 -1 2 -6 421.011 16.0158 8 -1 2 -6 423.079 15.8205 1 1 -2 6 370.201 26.6276 7 1 -2 6 420.256 15.6117 4 1 -2 6 413.736 15.4593 8 1 -2 6 411.332 15.8425 1 1 -2 6 415.562 20.5608 1 1 -2 6 415.073 16.9357 8 -2 2 -6 2013.93 69.9261 1 -2 2 -6 2068.91 71.8144 1 -2 2 -6 2096.59 70.6465 3 -2 2 -6 1945.14 71.3852 4 -2 2 -6 1959.96 70.0913 7 2 -2 6 1879.65 74.8332 1 2 -2 6 1969.76 74.9043 7 2 -2 6 1917.86 70.6370 4 2 -2 6 1943.31 69.5598 8 2 -2 6 2013.26 70.9654 8 2 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17.1818 1 0 6 -10 421.648 16.6128 8 0 6 -10 443.823 19.7496 8 0 6 -10 400.344 16.3116 4 0 -6 10 453.206 29.1028 1 0 -6 10 418.523 18.9643 8 0 -6 10 385.505 17.2986 1 0 -6 10 396.182 16.2572 8 0 -6 10 366.833 15.7874 9 -1 6 -10 318.332 14.5227 4 -1 6 -10 332.846 14.6223 1 -1 6 -10 339.539 16.5326 8 -1 6 -10 317.866 35.9339 7 -1 6 -10 299.324 22.2227 1 -1 6 -10 327.144 13.6910 8 1 -6 10 340.000 14.7799 1 1 -6 10 359.643 13.4670 9 1 -6 10 365.095 27.9352 1 1 -6 10 318.558 16.2799 8 1 -6 10 348.961 15.1260 6 1 -6 10 333.570 13.9905 8 -2 6 -10 332.943 15.6908 4 -2 6 -10 317.409 20.0335 7 -2 6 -10 348.047 13.6012 8 -2 6 -10 329.007 14.7559 1 -2 6 -10 345.164 15.9061 8 2 -6 10 353.910 15.0957 1 2 -6 10 343.555 16.6856 8 2 -6 10 339.046 15.8224 6 2 -6 10 350.278 14.2982 8 2 -6 10 291.342 28.1323 1 -3 6 -10 220.423 10.4714 1 -3 6 -10 208.252 10.7036 3 -3 6 -10 217.621 9.98107 8 -3 6 -10 212.044 12.4122 4 -3 6 -10 218.126 8.64909 8 3 -6 10 186.637 12.0048 6 3 -6 10 212.867 10.6762 1 3 -6 10 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466.860 18.4261 1 3 -5 11 434.138 30.9485 1 3 -5 11 430.607 18.8341 8 3 -5 11 452.226 20.6459 6 3 -5 11 444.797 20.8332 8 3 -5 11 448.716 18.6753 4 3 -5 11 455.449 18.8729 1 -4 5 -11 49.2557 8.12091 4 -4 5 -11 36.4797 5.34953 3 -4 5 -11 49.8612 6.05080 1 4 -5 11 48.5735 5.35574 1 4 -5 11 37.5244 4.31500 8 4 -5 11 65.0196 22.4847 1 4 -5 11 45.9810 6.56257 6 4 -5 11 46.1466 6.72329 8 -5 5 -11 99.7481 8.29287 3 -5 5 -11 110.248 6.25737 1 -5 5 -11 94.9952 6.10925 1 5 -5 11 97.9670 7.22989 1 5 -5 11 119.716 11.4186 4 5 -5 11 120.603 20.1107 1 5 -5 11 94.6621 7.56030 8 5 -5 11 112.774 12.6565 6 5 -5 11 113.323 10.0787 8 -6 5 -11 136.729 10.8641 3 6 -5 11 157.250 10.3081 8 6 -5 11 170.804 23.4708 1 6 -5 11 169.474 17.9373 6 6 -5 11 144.301 9.22779 1 6 -5 11 153.744 12.6227 8 7 -5 11 24.0040 18.3520 1 7 -5 11 22.7759 11.3593 6 7 -5 11 28.2058 10.7276 9 7 -5 11 26.1011 5.25432 1 7 4 -11 7.44683 5.42615 8 7 4 -11 -44.523 36.5946 1 7 4 -11 2.95657 6.27764 9 -7 -4 11 -7.1845 19.5130 2 6 4 -11 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5.03246 3 4 -9 12 47.3769 8.68550 6 4 -9 12 23.3665 6.59421 8 4 -9 12 89.3175 26.6017 1 4 -9 12 33.1682 6.73719 4 4 -9 12 17.4503 4.91388 1 4 -9 12 28.0290 5.45840 8 -5 9 -12 163.095 11.5401 3 -5 9 -12 159.860 12.8845 1 5 -9 12 161.908 11.8317 1 5 -9 12 165.016 14.3300 8 5 -9 12 168.978 12.4670 8 5 -9 12 153.717 36.4925 1 5 -9 12 188.238 17.2631 6 -6 9 -12 130.305 11.1370 3 6 -9 12 135.123 12.8980 8 6 -9 12 106.303 13.7486 6 6 -9 12 123.382 12.0524 1 6 8 -12 -4.2126 32.1760 1 6 8 -12 29.6426 7.27686 8 6 8 -12 38.7317 5.99440 9 -6 -8 12 19.6318 18.2436 2 5 8 -12 218.482 11.2086 9 5 8 -12 199.930 15.7710 1 5 8 -12 228.208 36.5600 1 5 8 -12 207.005 12.8667 8 -5 -8 12 206.959 9.75338 8 -5 -8 12 218.587 13.7456 1 -5 -8 12 213.723 11.1610 8 -5 -8 12 153.793 25.1879 2 4 8 -12 172.089 10.7337 8 4 8 -12 170.120 9.20743 9 4 8 -12 173.088 30.2319 1 4 8 -12 175.596 12.8030 1 4 8 -12 190.563 19.6866 8 -4 -8 12 171.153 9.09042 8 -4 -8 12 191.550 23.3603 2 -4 -8 12 150.332 16.8541 1 -4 -8 12 168.864 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239.952 15.7026 1 0 -8 12 300.453 16.0014 8 0 -8 12 297.453 13.0870 8 0 -8 12 279.744 12.4668 9 0 -8 12 290.899 13.8044 6 0 -8 12 272.156 14.1777 1 0 -8 12 331.589 31.2307 1 -1 8 -12 123.299 33.9167 7 -1 8 -12 148.471 12.2752 8 -1 8 -12 134.749 17.5732 1 -1 8 -12 143.541 8.02451 8 -1 8 -12 141.723 9.42359 1 -1 8 -12 144.668 9.19986 4 1 -8 12 157.562 22.6002 1 1 -8 12 147.243 9.57415 6 1 -8 12 151.583 9.49953 1 1 -8 12 160.543 8.64379 8 1 -8 12 140.515 10.9870 8 -2 8 -12 -12.828 15.4710 7 -2 8 -12 -1.7361 5.15845 8 -2 8 -12 11.1712 2.54539 8 -2 8 -12 13.5479 4.57747 4 -2 8 -12 6.04219 3.24106 1 -2 8 -12 14.8489 6.80424 1 2 -8 12 -8.9236 16.9463 1 2 -8 12 5.15857 3.01569 1 2 -8 12 8.35796 4.30268 6 2 -8 12 9.99124 5.02542 8 2 -8 12 8.01847 3.12166 8 -3 8 -12 429.925 22.0189 1 -3 8 -12 431.419 21.2487 4 -3 8 -12 451.433 17.4786 8 -3 8 -12 460.367 20.0222 8 -3 8 -12 417.279 19.5304 3 3 -8 12 440.046 19.7432 1 3 -8 12 484.176 19.6533 4 3 -8 12 420.908 18.7481 8 3 -8 12 406.965 41.7671 1 3 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12 39.8436 11.4419 1 -4 -7 12 49.0404 6.29502 1 -4 -7 12 57.6750 5.32047 8 -4 -7 12 64.4650 5.47509 6 -4 -7 12 64.0195 16.3763 2 -4 -7 12 62.7702 7.29672 8 3 7 -12 559.473 24.0308 1 3 7 -12 541.581 45.5984 1 3 7 -12 546.061 21.5225 9 3 7 -12 543.827 27.7258 8 3 7 -12 549.961 22.7846 8 -3 -7 12 523.319 24.5246 8 -3 -7 12 529.953 30.6692 1 -3 -7 12 574.344 21.7406 6 -3 -7 12 559.585 21.7048 8 -3 -7 12 558.820 23.6598 1 -3 -7 12 499.198 30.5969 2 2 7 -12 70.1146 4.89122 9 2 7 -12 79.8386 6.37790 8 2 7 -12 75.6100 7.67952 1 2 7 -12 66.7832 20.0734 1 -2 -7 12 72.3844 6.90658 1 -2 -7 12 86.7698 14.1112 1 -2 -7 12 85.1467 5.67101 8 -2 -7 12 69.1963 6.28081 9 -2 -7 12 69.9211 7.99254 8 1 7 -12 256.588 13.5361 1 1 7 -12 262.596 12.3849 8 1 7 -12 253.948 16.3316 8 1 7 -12 226.447 29.7676 1 -1 -7 12 272.681 15.2626 8 -1 -7 12 283.070 12.1257 9 -1 -7 12 275.736 25.0213 1 -1 -7 12 258.353 11.7310 8 -1 -7 12 261.270 13.3432 1 0 7 -12 176.456 11.4163 1 0 7 -12 206.687 13.7001 8 0 7 -12 194.209 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31.2829 3.86929 8 -5 -6 12 37.6631 19.5451 2 4 6 -12 2.01628 2.51963 9 4 6 -12 0.01814 8.06533 8 4 6 -12 6.26149 4.73252 1 4 6 -12 25.5608 67.3291 7 4 6 -12 3.54580 23.5321 1 4 6 -12 3.96331 3.24956 8 -4 -6 12 -2.7022 3.09037 6 -4 -6 12 5.40209 2.68323 8 -4 -6 12 3.45723 4.02524 1 -4 -6 12 2.36686 4.70655 9 -4 -6 12 2.27124 8.15302 1 -4 -6 12 1.33079 4.73154 8 -4 -6 12 12.5683 11.6252 2 3 6 -12 62.0600 5.73969 8 3 6 -12 59.5156 4.78710 9 3 6 -12 65.3913 20.3842 1 3 6 -12 56.9734 8.99977 8 3 6 -12 63.7820 7.18794 1 -3 -6 12 61.3356 5.39681 6 -3 -6 12 66.4461 5.19794 8 -3 -6 12 60.7689 10.9050 1 -3 -6 12 55.5049 7.72904 8 -3 -6 12 59.3081 6.86650 1 2 6 -12 31.8504 3.56630 9 2 6 -12 -3.1796 41.9804 7 2 6 -12 32.9300 17.8647 1 2 6 -12 31.3105 6.99008 8 2 6 -12 36.8817 5.31024 1 2 6 -12 39.3092 4.67605 8 -2 -6 12 32.6943 9.18878 1 -2 -6 12 33.5299 6.58111 8 -2 -6 12 49.0995 5.89371 1 -2 -6 12 27.0851 4.04327 9 1 6 -12 160.519 12.1707 8 1 6 -12 148.780 9.46480 1 1 6 -12 126.694 49.0835 7 1 6 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8.53085 9 4 9 -14 136.230 10.8163 8 4 9 -14 157.264 14.3048 1 4 9 -14 104.867 30.0378 1 -4 -9 14 112.872 21.8632 2 -4 -9 14 123.610 12.1419 1 -4 -9 14 145.381 12.3137 8 -4 -9 14 124.286 9.01562 8 -4 -9 14 139.064 7.05523 6 3 9 -14 109.889 11.5456 1 3 9 -14 99.4649 14.6854 8 3 9 -14 110.955 9.26285 8 3 9 -14 75.5286 25.7365 1 3 9 -14 105.219 7.20235 9 -3 -9 14 102.356 19.7183 2 -3 -9 14 108.190 10.5454 1 -3 -9 14 122.645 19.8024 1 -3 -9 14 111.608 7.17616 6 -3 -9 14 100.204 7.64309 6 -3 -9 14 114.647 11.2995 8 -3 -9 14 93.3877 11.0589 9 2 9 -14 305.675 34.3510 1 2 9 -14 313.046 15.2561 8 2 9 -14 318.081 21.1407 1 -2 -9 14 297.700 24.6871 2 -2 -9 14 286.257 17.7390 8 -2 -9 14 321.826 16.5437 1 -2 -9 14 292.104 31.5922 1 -2 -9 14 318.233 14.5632 6 1 9 -14 166.367 11.8807 1 1 9 -14 155.926 24.6732 1 1 9 -14 167.178 8.99502 4 1 9 -14 154.645 9.73878 8 -1 -9 14 167.118 11.3672 1 -1 -9 14 175.188 24.8826 1 -1 -9 14 160.305 10.1201 6 -1 -9 14 153.468 18.2178 2 -1 -9 14 137.015 12.7693 8 0 9 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8 -4 -8 14 13.6394 4.25381 6 -4 -8 14 10.7436 3.98295 8 3 8 -14 217.667 14.3472 1 3 8 -14 219.041 19.8054 8 3 8 -14 186.420 77.6878 7 3 8 -14 207.872 12.2820 8 3 8 -14 215.826 33.3732 1 3 8 -14 218.679 10.7611 9 -3 -8 14 235.031 11.4786 8 -3 -8 14 229.629 13.7594 1 -3 -8 14 191.169 22.7316 2 -3 -8 14 217.539 13.9176 9 -3 -8 14 242.353 15.6664 8 -3 -8 14 219.121 10.9722 6 -3 -8 14 252.896 24.4249 1 2 8 -14 336.285 15.6167 8 2 8 -14 320.743 41.4332 1 -2 -8 14 320.570 18.4973 8 -2 -8 14 263.123 27.0425 1 -2 -8 14 346.650 16.8211 1 1 8 -14 422.017 27.5778 8 1 8 -14 383.243 37.8692 1 1 8 -14 435.579 20.1436 1 1 8 -14 449.098 17.6139 4 1 8 -14 489.377 68.5504 7 1 8 -14 400.153 18.3730 8 -1 -8 14 416.618 19.6738 1 -1 -8 14 408.625 33.1483 1 -1 -8 14 399.694 21.4873 8 0 8 -14 264.963 48.9967 7 0 8 -14 203.936 10.5864 8 0 8 -14 188.723 10.9014 4 0 8 -14 175.291 11.8814 1 0 8 -14 236.350 15.9224 8 0 8 -14 271.344 27.5051 1 0 -8 14 182.256 13.9351 8 0 -8 14 218.986 24.3652 1 0 -8 14 183.301 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9.96817 7.18023 6 4 -8 14 5.61929 4.66240 8 4 -8 14 14.3553 4.71224 1 4 -8 14 -6.7216 23.1100 1 4 -8 14 16.5567 6.27690 4 -5 8 -14 28.2517 5.86760 3 5 -8 14 43.3746 10.7064 6 5 -8 14 43.9246 6.60523 1 5 -8 14 34.1424 7.00558 8 5 -8 14 35.5200 9.04193 8 5 -8 14 25.2492 31.3331 1 -6 8 -14 18.9203 7.58487 3 6 -8 14 36.6452 13.7846 6 6 -8 14 31.8974 7.13559 1 6 -8 14 29.0000 10.8344 8 6 7 -14 52.0762 8.80778 8 6 7 -14 58.5716 41.3022 1 6 7 -14 79.0361 9.48351 9 -6 -7 14 90.7341 24.5849 2 5 7 -14 -11.424 30.0018 1 5 7 -14 20.0743 4.46073 9 5 7 -14 28.4866 5.99960 8 5 7 -14 21.5939 8.74828 1 -5 -7 14 19.9860 16.6793 2 -5 -7 14 23.7768 6.61558 1 -5 -7 14 33.2916 5.05977 8 -5 -7 14 19.4920 7.17651 8 -5 -7 14 19.8077 5.39480 6 4 7 -14 117.316 31.0203 1 4 7 -14 100.363 11.8583 1 4 7 -14 -43.377 92.6435 7 4 7 -14 65.5696 12.8197 8 4 7 -14 78.2591 6.46636 9 -4 -7 14 61.8788 17.0226 2 -4 -7 14 98.6685 11.8471 8 -4 -7 14 81.1277 7.15330 8 -4 -7 14 101.897 10.1815 1 -4 -7 14 90.8492 14.3840 1 -4 -7 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