data_sa4178 _audit_creation_date 2015-06-12 _audit_creation_method ; Olex2 1.2 (compiled 2015.01.26 svn.r3150 for OlexSys, GUI svn.r4998) ; _publ_contact_author_address ? _publ_contact_author_email ? _publ_contact_author_name '' _publ_contact_author_phone ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2008). Acta Cryst. A64, 112-122. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C17 H13 Br F3 N O4 S' _chemical_formula_sum 'C17 H13 Br F3 N O4 S' _chemical_formula_weight 464.25 _chemical_absolute_configuration ad _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Br' 'Br' -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'F' 'F' 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'orthorhombic' _space_group_IT_number 19 _space_group_name_H-M_alt 'P 21 21 21' _space_group_name_Hall 'P 2ac 2ab' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' _cell_length_a 14.600(4) _cell_length_b 14.941(4) _cell_length_c 16.318(4) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 3559.6(15) _cell_formula_units_Z 8 _cell_measurement_reflns_used 12678 _cell_measurement_temperature 173.1500 _cell_measurement_theta_max 31.5152 _cell_measurement_theta_min 1.8481 _shelx_estimated_absorpt_T_max ? _shelx_estimated_absorpt_T_min ? _exptl_absorpt_coefficient_mu 2.481 _exptl_absorpt_correction_T_max 1.0000 _exptl_absorpt_correction_T_min 0.7607 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'CrystalClear (Rigaku Inc., 2007)' _exptl_absorpt_special_details ? _exptl_crystal_colour Colorless _exptl_crystal_density_diffrn 1.733 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description block _exptl_crystal_F_000 1856 _exptl_crystal_size_max 0.29 _exptl_crystal_size_mid 0.14 _exptl_crystal_size_min 0.09 _exptl_special_details ; ? ; _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0624 _diffrn_reflns_av_unetI/netI 0.0570 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_k_max 19 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_number 28297 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_theta_full 26.000 _diffrn_reflns_theta_max 27.503 _diffrn_reflns_theta_min 1.872 _diffrn_ambient_temperature 173.1500 _diffrn_detector_area_resol_mean 28.5714 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_details ; scan: Number of images: 360 Slice: -110.0000 - 70.0000 Image width: 0.5000 Exp time: 15.0000 Rotation axis: Omega Omega: 0.0000 Chi: 45.0000 Phi: 0.0000 XTD: 45.1005 2theta: -20.1287 scan: Number of images: 360 Slice: -110.0000 - 70.0000 Image width: 0.5000 Exp time: 15.0000 Rotation axis: Omega Omega: 0.0000 Chi: 45.0000 Phi: 180.0000 XTD: 45.1005 2theta: -20.1287 ; _diffrn_measurement_device ; Saturn724+ (2x2 bin mode) ; _diffrn_measurement_device_details ; AFC10: Fixed Chi 2 circle ; _diffrn_measurement_device_type 'Saturn724+ CCD' _diffrn_measurement_method '\w scans at fixed \c = 45\%' _diffrn_number_total 4565 _diffrn_orient_matrix_type d*Trek _diffrn_orient_matrix_UB_11 0.0272 _diffrn_orient_matrix_UB_12 0.0444 _diffrn_orient_matrix_UB_13 0.0444 _diffrn_orient_matrix_UB_21 0.0015 _diffrn_orient_matrix_UB_22 -0.0478 _diffrn_orient_matrix_UB_23 0.0468 _diffrn_orient_matrix_UB_31 0.0562 _diffrn_orient_matrix_UB_32 -0.0162 _diffrn_orient_matrix_UB_33 -0.0183 _diffrn_radiation_detector CCD _diffrn_radiation_monochromator 'Graphite Monochromator' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_source 'Sealed Tube' _diffrn_source_current 30.0000 _diffrn_source_power 1.5000 _diffrn_source_voltage 50.0000 _diffrn_special_details ; ? ; _reflns_Friedel_coverage 0.802 _reflns_Friedel_fraction_full 0.998 _reflns_Friedel_fraction_max 0.998 _reflns_number_gt 7342 _reflns_number_total 8164 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'CrystalClear (Rigaku Inc., 2007)' _computing_data_collection 'CrystalClear (Rigaku Inc., 2007)' _computing_data_reduction 'CrystalClear (Rigaku Inc., 2007)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'CIFTAB (Sheldrick, 2013)' _computing_structure_refinement 'SHELXL (Sheldrick, 2014)' _computing_structure_solution ; 'SHELXT (Sheldrick, 2014)' ; _refine_diff_density_max 0.470 _refine_diff_density_min -0.592 _refine_diff_density_rms 0.092 _refine_ls_abs_structure_details ; Flack x determined using 2407 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.003(6) _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.120 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 489 _refine_ls_number_reflns 8164 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0669 _refine_ls_R_factor_gt 0.0588 _refine_ls_restrained_S_all 1.120 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0318P)^2^+6.6530P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1141 _refine_ls_wR_factor_ref 0.1206 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C1(H1), C2(H2), C1A(H1A), C2A(H2A) 2.b Secondary CH2 refined with riding coordinates: C3(H3A,H3B), C3A(H3AA,H3AB) 2.c Aromatic/amide H refined with riding coordinates: C7(H7), C9(H9), C12(H12), C13(H13), C15(H15), C16(H16), C7A(H7A), C9A(H9A), C12A(H12A), C13A(H13A), C15A(H15A), C16A(H16A) 2.d Idealised Me refined as rotating group: C17(H17A,H17B,H17C), C17A(H17D,H17E,H17F) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Br1 Br 0.69980(6) 0.18339(5) 0.44838(5) 0.0421(2) Uani 1 1 d . . . . . S1 S 0.45406(13) 0.34837(12) 0.46855(12) 0.0326(4) Uani 1 1 d . . . . . F1 F 0.6194(4) 0.3070(3) 0.6991(3) 0.0491(12) Uani 1 1 d . . . . . F2 F 0.6374(4) 0.6112(4) 0.7665(3) 0.0558(14) Uani 1 1 d . . . . . F3 F 0.6450(4) 0.5243(3) 0.4922(3) 0.0477(12) Uani 1 1 d . . . . . O1 O 0.6949(4) 0.3865(3) 0.3750(3) 0.0339(11) Uani 1 1 d . . . . . O2 O 0.5553(4) 0.4150(4) 0.3307(3) 0.0371(12) Uani 1 1 d . . . . . O3 O 0.4149(4) 0.4360(3) 0.4619(4) 0.0405(13) Uani 1 1 d . . . . . O4 O 0.4420(4) 0.2996(4) 0.5440(3) 0.0383(12) Uani 1 1 d . . . . . N1 N 0.5680(4) 0.3565(4) 0.4595(3) 0.0288(12) Uani 1 1 d . . . . . C1 C 0.6253(5) 0.3336(5) 0.5308(4) 0.0315(16) Uani 1 1 d . . . . . H1 H 0.5956 0.2837 0.5594 0.038 Uiso 1 1 calc R . . . . C2 C 0.7172(5) 0.3006(4) 0.5006(5) 0.0334(16) Uani 1 1 d . . . . . H2 H 0.7587 0.2939 0.5474 0.040 Uiso 1 1 calc R . . . . C3 C 0.7587(5) 0.3648(6) 0.4403(5) 0.0393(18) Uani 1 1 d . . . . . H3A H 0.7764 0.4192 0.4685 0.047 Uiso 1 1 calc R . . . . H3B H 0.8135 0.3384 0.4168 0.047 Uiso 1 1 calc R . . . . C4 C 0.6040(5) 0.3884(5) 0.3857(5) 0.0321(16) Uani 1 1 d . . . . . C5 C 0.6326(5) 0.4108(5) 0.5911(4) 0.0318(16) Uani 1 1 d . . . . . C6 C 0.6402(6) 0.5006(5) 0.5722(4) 0.0343(17) Uani 1 1 d . . . . . C7 C 0.6427(6) 0.5681(6) 0.6285(5) 0.043(2) Uani 1 1 d . . . . . H7 H 0.6479 0.6276 0.6124 0.051 Uiso 1 1 calc R . . . . C8 C 0.6371(6) 0.5450(6) 0.7096(5) 0.042(2) Uani 1 1 d . . . . . C9 C 0.6296(6) 0.4580(6) 0.7358(5) 0.042(2) Uani 1 1 d . . . . . H9 H 0.6259 0.4434 0.7911 0.050 Uiso 1 1 calc R . . . . C10 C 0.6277(5) 0.3932(5) 0.6751(5) 0.0337(16) Uani 1 1 d . . . . . C11 C 0.4195(5) 0.2814(5) 0.3864(5) 0.0322(16) Uani 1 1 d . . . . . C12 C 0.3739(6) 0.3206(6) 0.3208(5) 0.043(2) Uani 1 1 d . . . . . H12 H 0.3637 0.3820 0.3198 0.051 Uiso 1 1 calc R . . . . C13 C 0.3436(6) 0.2668(6) 0.2569(6) 0.046(2) Uani 1 1 d . . . . . H13 H 0.3132 0.2924 0.2127 0.055 Uiso 1 1 calc R . . . . C14 C 0.3586(5) 0.1743(5) 0.2585(5) 0.0358(17) Uani 1 1 d . . . . . C15 C 0.4021(5) 0.1375(5) 0.3261(5) 0.0353(17) Uani 1 1 d . . . . . H15 H 0.4110 0.0759 0.3284 0.042 Uiso 1 1 calc R . . . . C16 C 0.4322(5) 0.1902(5) 0.3899(5) 0.0340(16) Uani 1 1 d . . . . . H16 H 0.4609 0.1644 0.4350 0.041 Uiso 1 1 calc R . . . . C17 C 0.3306(6) 0.1171(6) 0.1870(5) 0.045(2) Uani 1 1 d . . . . . H17A H 0.2708 0.1348 0.1686 0.067 Uiso 1 1 calc GR . . . . H17B H 0.3292 0.0554 0.2035 0.067 Uiso 1 1 calc GR . . . . H17C H 0.3738 0.1245 0.1432 0.067 Uiso 1 1 calc GR . . . . Br1A Br 0.69877(6) 0.76509(5) 0.48270(5) 0.03856(19) Uani 1 1 d . . . . . S1A S 0.43093(13) 0.89305(13) 0.50800(12) 0.0353(4) Uani 1 1 d . . . . . F1A F 0.6264(4) 0.8185(3) 0.7367(3) 0.0519(13) Uani 1 1 d . . . . . F2A F 0.6025(4) 1.0937(4) 0.8720(3) 0.0692(17) Uani 1 1 d . . . . . F3A F 0.5650(4) 1.0800(3) 0.5882(3) 0.0531(14) Uani 1 1 d . . . . . O1A O 0.6740(3) 0.9710(3) 0.4429(3) 0.0357(12) Uani 1 1 d . . . . . O2A O 0.5395(4) 0.9681(4) 0.3811(4) 0.0436(14) Uani 1 1 d . . . . . O3A O 0.3825(4) 0.9703(4) 0.4799(4) 0.0496(15) Uani 1 1 d . . . . . O4A O 0.4125(4) 0.8575(4) 0.5877(3) 0.0465(15) Uani 1 1 d . . . . . N1A N 0.5436(4) 0.9175(4) 0.5122(4) 0.0291(12) Uani 1 1 d . . . . . C1A C 0.5971(5) 0.8842(5) 0.5830(4) 0.0331(16) Uani 1 1 d . . . . . H1A H 0.5716 0.8262 0.5992 0.040 Uiso 1 1 calc R . . . . C2A C 0.6949(5) 0.8693(5) 0.5560(5) 0.0337(15) Uani 1 1 d . . . . . H2A H 0.7331 0.8575 0.6042 0.040 Uiso 1 1 calc R . . . . C3A C 0.7307(5) 0.9499(5) 0.5122(5) 0.0362(17) Uani 1 1 d . . . . . H3AA H 0.7320 1.0005 0.5495 0.043 Uiso 1 1 calc R . . . . H3AB H 0.7928 0.9386 0.4939 0.043 Uiso 1 1 calc R . . . . C4A C 0.5839(5) 0.9531(5) 0.4418(5) 0.0330(16) Uani 1 1 d . . . . . C5A C 0.5951(5) 0.9456(5) 0.6581(4) 0.0312(16) Uani 1 1 d . . . . . C6A C 0.5822(6) 1.0371(6) 0.6597(5) 0.0392(18) Uani 1 1 d . . . . . C7A C 0.5842(7) 1.0891(6) 0.7296(5) 0.048(2) Uani 1 1 d . . . . . H7A H 0.5747 1.1507 0.7280 0.057 Uiso 1 1 calc R . . . . C8A C 0.6012(6) 1.0441(7) 0.8021(5) 0.048(2) Uani 1 1 d . . . . . C9A C 0.6151(6) 0.9542(6) 0.8064(5) 0.044(2) Uani 1 1 d . . . . . H9A H 0.6265 0.9260 0.8562 0.053 Uiso 1 1 calc R . . . . C10A C 0.6117(6) 0.9075(5) 0.7353(5) 0.0380(18) Uani 1 1 d . . . . . C11A C 0.4225(5) 0.8059(5) 0.4361(4) 0.0311(15) Uani 1 1 d . . . . . C12A C 0.3900(5) 0.8230(5) 0.3577(5) 0.0348(16) Uani 1 1 d . . . . . H12A H 0.3762 0.8811 0.3412 0.042 Uiso 1 1 calc R . . . . C13A C 0.3786(6) 0.7514(6) 0.3044(5) 0.0415(19) Uani 1 1 d . . . . . H13A H 0.3560 0.7617 0.2520 0.050 Uiso 1 1 calc R . . . . C14A C 0.4003(5) 0.6646(5) 0.3279(5) 0.0336(16) Uani 1 1 d . . . . . C15A C 0.4354(5) 0.6513(5) 0.4063(5) 0.0357(17) Uani 1 1 d . . . . . H15A H 0.4528 0.5939 0.4219 0.043 Uiso 1 1 calc R . . . . C16A C 0.4451(5) 0.7198(5) 0.4609(5) 0.0339(16) Uani 1 1 d . . . . . H16A H 0.4665 0.7090 0.5137 0.041 Uiso 1 1 calc R . . . . C17A C 0.3870(6) 0.5860(6) 0.2712(6) 0.049(2) Uani 1 1 d . . . . . H17D H 0.3278 0.5601 0.2805 0.073 Uiso 1 1 calc GR . . . . H17E H 0.4336 0.5421 0.2815 0.073 Uiso 1 1 calc GR . . . . H17F H 0.3912 0.6060 0.2153 0.073 Uiso 1 1 calc GR . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Br1 0.0390(4) 0.0293(3) 0.0580(5) -0.0025(3) 0.0035(4) 0.0016(4) S1 0.0311(9) 0.0286(8) 0.0381(11) -0.0035(8) 0.0006(7) 0.0011(7) F1 0.069(3) 0.041(3) 0.038(3) 0.016(2) 0.000(2) -0.002(3) F2 0.073(4) 0.057(3) 0.037(3) -0.017(2) -0.008(3) -0.004(3) F3 0.088(4) 0.030(2) 0.025(2) 0.0042(18) -0.002(2) -0.006(2) O1 0.028(3) 0.038(3) 0.035(3) 0.006(2) 0.003(2) -0.002(2) O2 0.040(3) 0.040(3) 0.031(3) 0.004(2) -0.006(2) -0.002(3) O3 0.033(3) 0.032(3) 0.057(4) -0.009(3) 0.002(3) 0.010(2) O4 0.041(3) 0.040(3) 0.035(3) 0.002(2) 0.004(2) -0.001(2) N1 0.027(3) 0.031(3) 0.028(3) -0.001(3) -0.001(2) -0.003(2) C1 0.027(3) 0.032(4) 0.035(4) 0.006(3) -0.006(3) -0.002(3) C2 0.035(4) 0.026(3) 0.039(4) 0.004(3) -0.007(3) 0.004(3) C3 0.031(4) 0.044(4) 0.043(4) 0.005(4) -0.003(3) -0.006(3) C4 0.038(4) 0.026(3) 0.033(4) -0.003(3) 0.001(3) -0.002(3) C5 0.036(4) 0.030(4) 0.030(4) 0.002(3) -0.003(3) 0.000(3) C6 0.050(5) 0.029(4) 0.024(4) 0.003(3) -0.002(3) -0.010(3) C7 0.061(6) 0.037(4) 0.030(4) -0.005(3) -0.008(4) -0.003(4) C8 0.049(5) 0.046(5) 0.030(4) -0.010(4) -0.007(4) -0.003(4) C9 0.046(5) 0.056(5) 0.023(4) 0.005(4) -0.004(3) 0.003(4) C10 0.034(4) 0.032(4) 0.036(4) 0.007(3) -0.007(3) -0.003(3) C11 0.031(4) 0.027(4) 0.039(4) 0.005(3) 0.004(3) -0.001(3) C12 0.046(5) 0.027(4) 0.055(5) 0.001(4) -0.013(4) -0.001(4) C13 0.053(5) 0.033(4) 0.051(5) -0.003(4) -0.021(4) 0.001(4) C14 0.034(4) 0.033(4) 0.040(4) -0.004(3) 0.002(3) 0.000(3) C15 0.030(4) 0.032(4) 0.044(4) -0.004(3) 0.003(3) 0.001(3) C16 0.028(4) 0.034(4) 0.040(4) -0.002(3) -0.002(3) -0.002(3) C17 0.046(5) 0.047(5) 0.041(5) -0.008(4) -0.005(4) -0.009(4) Br1A 0.0404(4) 0.0338(4) 0.0414(4) -0.0026(3) -0.0003(4) 0.0055(3) S1A 0.0319(9) 0.0401(10) 0.0338(10) -0.0093(8) -0.0004(8) 0.0030(8) F1A 0.073(4) 0.047(3) 0.036(3) 0.008(2) -0.003(2) 0.014(3) F2A 0.089(4) 0.079(4) 0.039(3) -0.028(3) -0.011(3) -0.006(4) F3A 0.094(4) 0.030(2) 0.035(3) 0.006(2) 0.002(3) -0.001(3) O1A 0.035(3) 0.034(3) 0.038(3) 0.008(2) -0.001(2) -0.008(2) O2A 0.049(3) 0.042(3) 0.040(3) 0.011(3) -0.009(3) -0.005(3) O3A 0.044(3) 0.042(3) 0.063(4) -0.020(3) -0.014(3) 0.021(3) O4A 0.040(3) 0.068(4) 0.032(3) -0.011(3) 0.009(2) -0.011(3) N1A 0.031(3) 0.030(3) 0.026(3) 0.005(3) 0.000(2) 0.003(2) C1A 0.038(4) 0.031(4) 0.030(4) 0.006(3) -0.003(3) -0.006(3) C2A 0.029(3) 0.037(4) 0.034(4) 0.001(3) -0.001(3) -0.003(3) C3A 0.031(4) 0.038(4) 0.040(4) 0.002(4) -0.004(3) -0.005(3) C4A 0.034(4) 0.028(4) 0.037(4) 0.006(3) -0.005(3) -0.001(3) C5A 0.037(4) 0.029(4) 0.028(4) -0.001(3) 0.001(3) -0.001(3) C6A 0.052(5) 0.035(4) 0.030(4) -0.002(3) -0.001(4) -0.007(4) C7A 0.071(6) 0.031(4) 0.041(5) -0.006(4) 0.003(4) -0.003(4) C8A 0.049(5) 0.065(6) 0.030(4) -0.016(4) -0.003(4) -0.008(5) C9A 0.055(5) 0.053(5) 0.025(4) -0.001(4) -0.004(4) -0.006(4) C10A 0.045(5) 0.035(4) 0.034(4) 0.005(3) -0.003(3) 0.004(4) C11A 0.028(3) 0.035(4) 0.031(4) 0.001(3) -0.004(3) -0.008(3) C12A 0.040(4) 0.028(4) 0.036(4) 0.003(3) -0.002(3) 0.000(3) C13A 0.055(5) 0.044(5) 0.026(4) -0.001(3) -0.001(3) -0.008(4) C14A 0.035(4) 0.032(4) 0.034(4) -0.003(3) 0.010(3) -0.007(3) C15A 0.035(4) 0.031(4) 0.041(4) -0.001(3) 0.000(3) -0.002(3) C16A 0.028(3) 0.044(4) 0.030(4) 0.004(3) 0.001(3) -0.001(3) C17A 0.051(5) 0.044(5) 0.051(5) -0.017(4) 0.009(4) -0.004(4) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Br1 C2 1.964(7) . ? S1 O3 1.433(5) . ? S1 O4 1.441(6) . ? S1 N1 1.675(6) . ? S1 C11 1.747(8) . ? F1 C10 1.351(8) . ? F2 C8 1.357(9) . ? F3 C6 1.354(8) . ? O1 C3 1.453(9) . ? O1 C4 1.338(9) . ? O2 C4 1.213(9) . ? N1 C1 1.474(9) . ? N1 C4 1.397(9) . ? C1 H1 0.9800 . ? C1 C2 1.512(10) . ? C1 C5 1.519(10) . ? C2 H2 0.9800 . ? C2 C3 1.502(10) . ? C3 H3A 0.9700 . ? C3 H3B 0.9700 . ? C5 C6 1.381(10) . ? C5 C10 1.398(10) . ? C6 C7 1.365(11) . ? C7 H7 0.9300 . ? C7 C8 1.370(11) . ? C8 C9 1.372(12) . ? C9 H9 0.9300 . ? C9 C10 1.385(11) . ? C11 C12 1.390(11) . ? C11 C16 1.376(10) . ? C12 H12 0.9300 . ? C12 C13 1.389(11) . ? C13 H13 0.9300 . ? C13 C14 1.399(11) . ? C14 C15 1.387(11) . ? C14 C17 1.503(11) . ? C15 H15 0.9300 . ? C15 C16 1.378(10) . ? C16 H16 0.9300 . ? C17 H17A 0.9600 . ? C17 H17B 0.9600 . ? C17 H17C 0.9600 . ? Br1A C2A 1.964(7) . ? S1A O3A 1.429(6) . ? S1A O4A 1.431(6) . ? S1A N1A 1.686(6) . ? S1A C11A 1.757(8) . ? F1A C10A 1.347(9) . ? F2A C8A 1.360(9) . ? F3A C6A 1.355(9) . ? O1A C3A 1.436(9) . ? O1A C4A 1.343(8) . ? O2A C4A 1.205(9) . ? N1A C1A 1.481(9) . ? N1A C4A 1.396(9) . ? C1A H1A 0.9800 . ? C1A C2A 1.512(11) . ? C1A C5A 1.531(10) . ? C2A H2A 0.9800 . ? C2A C3A 1.495(10) . ? C3A H3AA 0.9700 . ? C3A H3AB 0.9700 . ? C5A C6A 1.381(11) . ? C5A C10A 1.403(10) . ? C6A C7A 1.379(11) . ? C7A H7A 0.9300 . ? C7A C8A 1.384(12) . ? C8A C9A 1.360(13) . ? C9A H9A 0.9300 . ? C9A C10A 1.356(11) . ? C11A C12A 1.389(10) . ? C11A C16A 1.388(10) . ? C12A H12A 0.9300 . ? C12A C13A 1.388(11) . ? C13A H13A 0.9300 . ? C13A C14A 1.389(11) . ? C14A C15A 1.391(11) . ? C14A C17A 1.507(11) . ? C15A H15A 0.9300 . ? C15A C16A 1.365(10) . ? C16A H16A 0.9300 . ? C17A H17D 0.9600 . ? C17A H17E 0.9600 . ? C17A H17F 0.9600 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O3 S1 O4 118.6(3) . . ? O3 S1 N1 108.9(3) . . ? O3 S1 C11 110.5(4) . . ? O4 S1 N1 103.5(3) . . ? O4 S1 C11 109.3(3) . . ? N1 S1 C11 105.1(3) . . ? C4 O1 C3 123.0(6) . . ? C1 N1 S1 118.5(5) . . ? C4 N1 S1 118.3(5) . . ? C4 N1 C1 123.1(6) . . ? N1 C1 H1 107.5 . . ? N1 C1 C2 108.7(6) . . ? N1 C1 C5 112.0(6) . . ? C2 C1 H1 107.5 . . ? C2 C1 C5 113.4(6) . . ? C5 C1 H1 107.5 . . ? Br1 C2 H2 109.1 . . ? C1 C2 Br1 108.5(5) . . ? C1 C2 H2 109.1 . . ? C3 C2 Br1 109.7(5) . . ? C3 C2 C1 111.3(6) . . ? C3 C2 H2 109.1 . . ? O1 C3 C2 111.4(6) . . ? O1 C3 H3A 109.3 . . ? O1 C3 H3B 109.3 . . ? C2 C3 H3A 109.3 . . ? C2 C3 H3B 109.3 . . ? H3A C3 H3B 108.0 . . ? O1 C4 N1 118.6(6) . . ? O2 C4 O1 119.4(7) . . ? O2 C4 N1 121.9(7) . . ? C6 C5 C1 126.8(7) . . ? C6 C5 C10 113.9(7) . . ? C10 C5 C1 119.2(7) . . ? F3 C6 C5 118.2(6) . . ? F3 C6 C7 117.0(7) . . ? C7 C6 C5 124.7(7) . . ? C6 C7 H7 121.2 . . ? C6 C7 C8 117.5(8) . . ? C8 C7 H7 121.2 . . ? F2 C8 C7 118.4(8) . . ? F2 C8 C9 118.5(7) . . ? C7 C8 C9 123.0(8) . . ? C8 C9 H9 121.9 . . ? C8 C9 C10 116.1(7) . . ? C10 C9 H9 121.9 . . ? F1 C10 C5 117.9(7) . . ? F1 C10 C9 117.4(7) . . ? C9 C10 C5 124.7(7) . . ? C12 C11 S1 119.2(6) . . ? C16 C11 S1 119.7(6) . . ? C16 C11 C12 120.9(7) . . ? C11 C12 H12 120.4 . . ? C13 C12 C11 119.1(8) . . ? C13 C12 H12 120.4 . . ? C12 C13 H13 119.7 . . ? C12 C13 C14 120.6(8) . . ? C14 C13 H13 119.7 . . ? C13 C14 C17 120.3(8) . . ? C15 C14 C13 118.5(8) . . ? C15 C14 C17 121.1(7) . . ? C14 C15 H15 119.3 . . ? C16 C15 C14 121.4(7) . . ? C16 C15 H15 119.3 . . ? C11 C16 C15 119.4(8) . . ? C11 C16 H16 120.3 . . ? C15 C16 H16 120.3 . . ? C14 C17 H17A 109.5 . . ? C14 C17 H17B 109.5 . . ? C14 C17 H17C 109.5 . . ? H17A C17 H17B 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? O3A S1A O4A 119.9(4) . . ? O3A S1A N1A 108.7(3) . . ? O3A S1A C11A 110.4(3) . . ? O4A S1A N1A 103.1(3) . . ? O4A S1A C11A 108.6(4) . . ? N1A S1A C11A 104.9(3) . . ? C4A O1A C3A 122.1(6) . . ? C1A N1A S1A 118.3(5) . . ? C4A N1A S1A 117.4(5) . . ? C4A N1A C1A 123.2(6) . . ? N1A C1A H1A 107.9 . . ? N1A C1A C2A 108.7(6) . . ? N1A C1A C5A 114.5(6) . . ? C2A C1A H1A 107.9 . . ? C2A C1A C5A 109.9(6) . . ? C5A C1A H1A 107.9 . . ? Br1A C2A H2A 109.3 . . ? C1A C2A Br1A 108.8(5) . . ? C1A C2A H2A 109.3 . . ? C3A C2A Br1A 109.7(5) . . ? C3A C2A C1A 110.5(6) . . ? C3A C2A H2A 109.3 . . ? O1A C3A C2A 110.6(6) . . ? O1A C3A H3AA 109.5 . . ? O1A C3A H3AB 109.5 . . ? C2A C3A H3AA 109.5 . . ? C2A C3A H3AB 109.5 . . ? H3AA C3A H3AB 108.1 . . ? O1A C4A N1A 118.6(6) . . ? O2A C4A O1A 120.1(7) . . ? O2A C4A N1A 121.4(7) . . ? C6A C5A C1A 127.7(7) . . ? C6A C5A C10A 114.1(7) . . ? C10A C5A C1A 118.2(7) . . ? F3A C6A C5A 118.5(7) . . ? F3A C6A C7A 116.7(7) . . ? C7A C6A C5A 124.8(8) . . ? C6A C7A H7A 122.1 . . ? C6A C7A C8A 115.9(8) . . ? C8A C7A H7A 122.1 . . ? F2A C8A C7A 117.1(9) . . ? F2A C8A C9A 119.5(8) . . ? C9A C8A C7A 123.4(8) . . ? C8A C9A H9A 121.3 . . ? C10A C9A C8A 117.3(8) . . ? C10A C9A H9A 121.3 . . ? F1A C10A C5A 116.3(7) . . ? F1A C10A C9A 119.2(7) . . ? C9A C10A C5A 124.4(8) . . ? C12A C11A S1A 120.2(6) . . ? C16A C11A S1A 118.4(6) . . ? C16A C11A C12A 121.3(7) . . ? C11A C12A H12A 120.8 . . ? C13A C12A C11A 118.4(7) . . ? C13A C12A H12A 120.8 . . ? C12A C13A H13A 119.3 . . ? C12A C13A C14A 121.3(7) . . ? C14A C13A H13A 119.3 . . ? C13A C14A C15A 118.1(7) . . ? C13A C14A C17A 121.9(7) . . ? C15A C14A C17A 120.0(7) . . ? C14A C15A H15A 119.0 . . ? C16A C15A C14A 122.1(7) . . ? C16A C15A H15A 119.0 . . ? C11A C16A H16A 120.6 . . ? C15A C16A C11A 118.7(7) . . ? C15A C16A H16A 120.6 . . ? C14A C17A H17D 109.5 . . ? C14A C17A H17E 109.5 . . ? C14A C17A H17F 109.5 . . ? H17D C17A H17E 109.5 . . ? H17D C17A H17F 109.5 . . ? H17E C17A H17F 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Br1 C2 C3 O1 68.3(7) . . . . ? S1 N1 C1 C2 151.7(5) . . . . ? S1 N1 C1 C5 -82.2(7) . . . . ? S1 N1 C4 O1 -173.3(5) . . . . ? S1 N1 C4 O2 4.4(9) . . . . ? S1 C11 C12 C13 -177.8(7) . . . . ? S1 C11 C16 C15 177.9(6) . . . . ? F2 C8 C9 C10 178.7(7) . . . . ? F3 C6 C7 C8 179.5(8) . . . . ? O3 S1 N1 C1 114.5(5) . . . . ? O3 S1 N1 C4 -62.8(6) . . . . ? O3 S1 C11 C12 10.0(7) . . . . ? O3 S1 C11 C16 -165.7(6) . . . . ? O4 S1 N1 C1 -12.5(6) . . . . ? O4 S1 N1 C4 170.2(5) . . . . ? O4 S1 C11 C12 142.2(6) . . . . ? O4 S1 C11 C16 -33.5(7) . . . . ? N1 S1 C11 C12 -107.3(7) . . . . ? N1 S1 C11 C16 77.1(7) . . . . ? N1 C1 C2 Br1 -69.8(6) . . . . ? N1 C1 C2 C3 51.1(8) . . . . ? N1 C1 C5 C6 -38.5(10) . . . . ? N1 C1 C5 C10 138.5(7) . . . . ? C1 N1 C4 O1 9.5(10) . . . . ? C1 N1 C4 O2 -172.8(7) . . . . ? C1 C2 C3 O1 -51.9(8) . . . . ? C1 C5 C6 F3 -2.5(12) . . . . ? C1 C5 C6 C7 177.1(8) . . . . ? C1 C5 C10 F1 2.0(11) . . . . ? C1 C5 C10 C9 -177.1(8) . . . . ? C2 C1 C5 C6 85.0(9) . . . . ? C2 C1 C5 C10 -98.0(8) . . . . ? C3 O1 C4 O2 173.3(7) . . . . ? C3 O1 C4 N1 -8.9(10) . . . . ? C4 O1 C3 C2 30.8(10) . . . . ? C4 N1 C1 C2 -31.1(9) . . . . ? C4 N1 C1 C5 95.0(8) . . . . ? C5 C1 C2 Br1 165.0(5) . . . . ? C5 C1 C2 C3 -74.1(8) . . . . ? C5 C6 C7 C8 -0.1(14) . . . . ? C6 C5 C10 F1 179.4(7) . . . . ? C6 C5 C10 C9 0.3(12) . . . . ? C6 C7 C8 F2 -178.6(8) . . . . ? C6 C7 C8 C9 0.2(14) . . . . ? C7 C8 C9 C10 0.0(14) . . . . ? C8 C9 C10 F1 -179.3(7) . . . . ? C8 C9 C10 C5 -0.2(13) . . . . ? C10 C5 C6 F3 -179.7(7) . . . . ? C10 C5 C6 C7 -0.1(13) . . . . ? C11 S1 N1 C1 -127.1(5) . . . . ? C11 S1 N1 C4 55.5(6) . . . . ? C11 C12 C13 C14 0.2(14) . . . . ? C12 C11 C16 C15 2.3(12) . . . . ? C12 C13 C14 C15 1.6(13) . . . . ? C12 C13 C14 C17 -176.5(8) . . . . ? C13 C14 C15 C16 -1.5(12) . . . . ? C14 C15 C16 C11 -0.4(12) . . . . ? C16 C11 C12 C13 -2.2(13) . . . . ? C17 C14 C15 C16 176.5(7) . . . . ? Br1A C2A C3A O1A 62.4(7) . . . . ? S1A N1A C1A C2A 150.5(5) . . . . ? S1A N1A C1A C5A -86.3(7) . . . . ? S1A N1A C4A O1A -178.3(5) . . . . ? S1A N1A C4A O2A 2.0(10) . . . . ? S1A C11A C12A C13A -175.8(6) . . . . ? S1A C11A C16A C15A 177.6(6) . . . . ? F2A C8A C9A C10A 178.9(8) . . . . ? F3A C6A C7A C8A 179.5(8) . . . . ? O3A S1A N1A C1A 139.1(5) . . . . ? O3A S1A N1A C4A -52.6(6) . . . . ? O3A S1A C11A C12A 13.0(7) . . . . ? O3A S1A C11A C16A -164.2(6) . . . . ? O4A S1A N1A C1A 10.9(6) . . . . ? O4A S1A N1A C4A 179.2(5) . . . . ? O4A S1A C11A C12A 146.3(6) . . . . ? O4A S1A C11A C16A -30.9(7) . . . . ? N1A S1A C11A C12A -104.0(6) . . . . ? N1A S1A C11A C16A 78.8(6) . . . . ? N1A C1A C2A Br1A -70.7(6) . . . . ? N1A C1A C2A C3A 49.9(8) . . . . ? N1A C1A C5A C6A -26.9(11) . . . . ? N1A C1A C5A C10A 155.8(7) . . . . ? C1A N1A C4A O1A -10.7(10) . . . . ? C1A N1A C4A O2A 169.7(7) . . . . ? C1A C2A C3A O1A -57.5(8) . . . . ? C1A C5A C6A F3A 3.2(13) . . . . ? C1A C5A C6A C7A -177.7(8) . . . . ? C1A C5A C10A F1A -1.2(11) . . . . ? C1A C5A C10A C9A 177.7(8) . . . . ? C2A C1A C5A C6A 95.7(10) . . . . ? C2A C1A C5A C10A -81.6(9) . . . . ? C3A O1A C4A O2A -176.6(7) . . . . ? C3A O1A C4A N1A 3.7(10) . . . . ? C4A O1A C3A C2A 30.5(9) . . . . ? C4A N1A C1A C2A -17.1(9) . . . . ? C4A N1A C1A C5A 106.1(8) . . . . ? C5A C1A C2A Br1A 163.4(5) . . . . ? C5A C1A C2A C3A -76.0(8) . . . . ? C5A C6A C7A C8A 0.4(14) . . . . ? C6A C5A C10A F1A -178.9(7) . . . . ? C6A C5A C10A C9A 0.1(13) . . . . ? C6A C7A C8A F2A -179.3(8) . . . . ? C6A C7A C8A C9A -0.2(15) . . . . ? C7A C8A C9A C10A -0.1(15) . . . . ? C8A C9A C10A F1A 179.1(8) . . . . ? C8A C9A C10A C5A 0.2(14) . . . . ? C10A C5A C6A F3A -179.5(7) . . . . ? C10A C5A C6A C7A -0.4(13) . . . . ? C11A S1A N1A C1A -102.7(6) . . . . ? C11A S1A N1A C4A 65.5(6) . . . . ? C11A C12A C13A C14A -1.0(12) . . . . ? C12A C11A C16A C15A 0.4(11) . . . . ? C12A C13A C14A C15A -1.0(12) . . . . ? C12A C13A C14A C17A 179.1(8) . . . . ? C13A C14A C15A C16A 2.9(12) . . . . ? C14A C15A C16A C11A -2.5(11) . . . . ? C16A C11A C12A C13A 1.4(11) . . . . ? C17A C14A C15A C16A -177.2(7) . . . . ? _shelx_res_file ; sa4178.res created by SHELXL-2014/7 TITL sa4178_a.res in P2(1)2(1)2(1) CELL 0.71073 14.5998 14.9413 16.3178 90 90 90 ZERR 8 0.0036 0.0037 0.0042 0 0 0 LATT -1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H Br F N O S UNIT 136 104 8 24 8 32 8 L.S. 4 0 0 PLAN 20 BOND $H LIST 6 fmap 2 53 MORE -1 ACTA 52 CONF OMIT 2 0 0 OMIT 1 1 1 OMIT 0 1 1 OMIT 1 1 0 OMIT 0 0 2 REM REM REM WGHT 0.031800 6.653000 FVAR 0.22573 BR1 3 0.699800 0.183391 0.448384 11.00000 0.03899 0.02933 = 0.05800 -0.00249 0.00345 0.00163 S1 7 0.454060 0.348367 0.468548 11.00000 0.03112 0.02857 = 0.03809 -0.00348 0.00060 0.00115 F1 4 0.619380 0.307041 0.699055 11.00000 0.06896 0.04060 = 0.03777 0.01625 -0.00019 -0.00186 F2 4 0.637434 0.611213 0.766457 11.00000 0.07300 0.05713 = 0.03713 -0.01719 -0.00793 -0.00351 F3 4 0.645015 0.524328 0.492220 11.00000 0.08798 0.02968 = 0.02547 0.00420 -0.00192 -0.00637 O1 6 0.694863 0.386544 0.374963 11.00000 0.02791 0.03835 = 0.03543 0.00644 0.00332 -0.00178 O2 6 0.555255 0.414997 0.330707 11.00000 0.04036 0.03965 = 0.03141 0.00378 -0.00648 -0.00171 O3 6 0.414878 0.435972 0.461862 11.00000 0.03308 0.03172 = 0.05682 -0.00869 0.00210 0.00991 O4 6 0.442024 0.299581 0.543968 11.00000 0.04062 0.03956 = 0.03470 0.00151 0.00440 -0.00149 N1 5 0.568028 0.356530 0.459496 11.00000 0.02682 0.03147 = 0.02814 -0.00083 -0.00081 -0.00289 C1 1 0.625344 0.333579 0.530829 11.00000 0.02724 0.03239 = 0.03500 0.00590 -0.00624 -0.00223 AFIX 13 H1 2 0.595599 0.283731 0.559382 11.00000 -1.20000 AFIX 0 C2 1 0.717221 0.300587 0.500551 11.00000 0.03517 0.02621 = 0.03893 0.00415 -0.00667 0.00376 AFIX 13 H2 2 0.758700 0.293880 0.547368 11.00000 -1.20000 AFIX 0 C3 1 0.758717 0.364762 0.440251 11.00000 0.03086 0.04417 = 0.04301 0.00468 -0.00270 -0.00632 AFIX 23 H3A 2 0.776379 0.419209 0.468508 11.00000 -1.20000 H3B 2 0.813498 0.338387 0.416839 11.00000 -1.20000 AFIX 0 C4 1 0.604006 0.388420 0.385739 11.00000 0.03767 0.02600 = 0.03264 -0.00343 0.00095 -0.00195 C5 1 0.632645 0.410795 0.591053 11.00000 0.03555 0.02972 = 0.03013 0.00190 -0.00290 0.00040 C6 1 0.640191 0.500621 0.572183 11.00000 0.04994 0.02878 = 0.02407 0.00333 -0.00191 -0.00980 C7 1 0.642674 0.568117 0.628515 11.00000 0.06063 0.03709 = 0.02991 -0.00521 -0.00764 -0.00299 AFIX 43 H7 2 0.647927 0.627615 0.612449 11.00000 -1.20000 AFIX 0 C8 1 0.637140 0.544956 0.709591 11.00000 0.04869 0.04622 = 0.03042 -0.00983 -0.00674 -0.00333 C9 1 0.629585 0.457990 0.735804 11.00000 0.04612 0.05650 = 0.02301 0.00472 -0.00421 0.00321 AFIX 43 H9 2 0.625926 0.443390 0.791110 11.00000 -1.20000 AFIX 0 C10 1 0.627727 0.393220 0.675074 11.00000 0.03378 0.03170 = 0.03562 0.00725 -0.00746 -0.00347 C11 1 0.419515 0.281423 0.386417 11.00000 0.03108 0.02669 = 0.03891 0.00472 0.00385 -0.00130 C12 1 0.373859 0.320609 0.320834 11.00000 0.04630 0.02654 = 0.05526 0.00127 -0.01328 -0.00113 AFIX 43 H12 2 0.363696 0.382044 0.319758 11.00000 -1.20000 AFIX 0 C13 1 0.343620 0.266762 0.256921 11.00000 0.05263 0.03343 = 0.05070 -0.00291 -0.02104 0.00091 AFIX 43 H13 2 0.313173 0.292416 0.212714 11.00000 -1.20000 AFIX 0 C14 1 0.358560 0.174283 0.258463 11.00000 0.03412 0.03322 = 0.04004 -0.00375 0.00201 0.00041 C15 1 0.402053 0.137487 0.326093 11.00000 0.03018 0.03202 = 0.04373 -0.00387 0.00327 0.00053 AFIX 43 H15 2 0.411048 0.075920 0.328429 11.00000 -1.20000 AFIX 0 C16 1 0.432233 0.190230 0.389923 11.00000 0.02786 0.03384 = 0.04042 -0.00249 -0.00250 -0.00231 AFIX 43 H16 2 0.460944 0.164415 0.434973 11.00000 -1.20000 AFIX 0 C17 1 0.330553 0.117087 0.186974 11.00000 0.04632 0.04675 = 0.04133 -0.00811 -0.00549 -0.00930 AFIX 137 H17A 2 0.270777 0.134785 0.168586 11.00000 -1.50000 H17B 2 0.329200 0.055434 0.203491 11.00000 -1.50000 H17C 2 0.373793 0.124505 0.143175 11.00000 -1.50000 AFIX 0 BR1A 3 0.698768 0.765094 0.482704 11.00000 0.04043 0.03381 = 0.04145 -0.00264 -0.00035 0.00545 S1A 7 0.430931 0.893046 0.508002 11.00000 0.03189 0.04014 = 0.03376 -0.00932 -0.00039 0.00297 F1A 4 0.626383 0.818482 0.736667 11.00000 0.07288 0.04661 = 0.03621 0.00847 -0.00280 0.01420 F2A 4 0.602514 1.093671 0.872014 11.00000 0.08891 0.07907 = 0.03949 -0.02782 -0.01092 -0.00607 F3A 4 0.564986 1.080026 0.588244 11.00000 0.09383 0.03045 = 0.03497 0.00605 0.00244 -0.00111 O1A 6 0.674040 0.971015 0.442925 11.00000 0.03520 0.03417 = 0.03777 0.00751 -0.00116 -0.00771 O2A 6 0.539504 0.968119 0.381117 11.00000 0.04860 0.04175 = 0.04045 0.01105 -0.00947 -0.00520 O3A 6 0.382452 0.970253 0.479867 11.00000 0.04418 0.04176 = 0.06284 -0.02001 -0.01441 0.02065 O4A 6 0.412468 0.857539 0.587747 11.00000 0.04004 0.06768 = 0.03189 -0.01073 0.00873 -0.01077 N1A 5 0.543567 0.917499 0.512214 11.00000 0.03088 0.03008 = 0.02639 0.00455 -0.00048 0.00258 C1A 1 0.597083 0.884238 0.583044 11.00000 0.03828 0.03109 = 0.02981 0.00647 -0.00288 -0.00646 AFIX 13 H1A 2 0.571595 0.826195 0.599238 11.00000 -1.20000 AFIX 0 C2A 1 0.694930 0.869319 0.555995 11.00000 0.02943 0.03739 = 0.03426 0.00113 -0.00056 -0.00303 AFIX 13 H2A 2 0.733117 0.857525 0.604191 11.00000 -1.20000 AFIX 0 C3A 1 0.730697 0.949923 0.512203 11.00000 0.03098 0.03797 = 0.03964 0.00158 -0.00434 -0.00517 AFIX 23 H3AA 2 0.731990 1.000466 0.549492 11.00000 -1.20000 H3AB 2 0.792837 0.938646 0.493876 11.00000 -1.20000 AFIX 0 C4A 1 0.583885 0.953102 0.441814 11.00000 0.03394 0.02814 = 0.03707 0.00581 -0.00495 -0.00080 C5A 1 0.595132 0.945589 0.658140 11.00000 0.03680 0.02906 = 0.02785 -0.00122 0.00085 -0.00076 C6A 1 0.582189 1.037145 0.659746 11.00000 0.05244 0.03544 = 0.02957 -0.00231 -0.00121 -0.00672 C7A 1 0.584205 1.089132 0.729561 11.00000 0.07131 0.03117 = 0.04104 -0.00593 0.00307 -0.00308 AFIX 43 H7A 2 0.574724 1.150658 0.727984 11.00000 -1.20000 AFIX 0 C8A 1 0.601204 1.044122 0.802112 11.00000 0.04936 0.06527 = 0.02999 -0.01576 -0.00323 -0.00812 C9A 1 0.615127 0.954243 0.806423 11.00000 0.05475 0.05267 = 0.02483 -0.00110 -0.00429 -0.00628 AFIX 43 H9A 2 0.626536 0.925997 0.856173 11.00000 -1.20000 AFIX 0 C10A 1 0.611708 0.907454 0.735272 11.00000 0.04516 0.03466 = 0.03411 0.00516 -0.00287 0.00427 C11A 1 0.422479 0.805883 0.436126 11.00000 0.02812 0.03461 = 0.03070 0.00062 -0.00394 -0.00757 C12A 1 0.390017 0.823022 0.357650 11.00000 0.04011 0.02826 = 0.03602 0.00278 -0.00200 -0.00019 AFIX 43 H12A 2 0.376241 0.881067 0.341172 11.00000 -1.20000 AFIX 0 C13A 1 0.378641 0.751380 0.304418 11.00000 0.05468 0.04385 = 0.02598 -0.00086 -0.00119 -0.00819 AFIX 43 H13A 2 0.356035 0.761719 0.251982 11.00000 -1.20000 AFIX 0 C14A 1 0.400343 0.664586 0.327907 11.00000 0.03498 0.03182 = 0.03404 -0.00308 0.01034 -0.00707 C15A 1 0.435424 0.651279 0.406252 11.00000 0.03456 0.03111 = 0.04137 -0.00107 -0.00012 -0.00172 AFIX 43 H15A 2 0.452819 0.593886 0.421882 11.00000 -1.20000 AFIX 0 C16A 1 0.445108 0.719787 0.460873 11.00000 0.02809 0.04377 = 0.02997 0.00436 0.00068 -0.00091 AFIX 43 H16A 2 0.466454 0.709005 0.513655 11.00000 -1.20000 AFIX 0 C17A 1 0.387007 0.586049 0.271157 11.00000 0.05052 0.04396 = 0.05148 -0.01737 0.00897 -0.00402 AFIX 137 H17D 2 0.327793 0.560057 0.280531 11.00000 -1.50000 H17E 2 0.433582 0.542110 0.281454 11.00000 -1.50000 H17F 2 0.391153 0.605964 0.215347 11.00000 -1.50000 AFIX 0 HKLF 4 REM sa4178_a.res in P2(1)2(1)2(1) REM R1 = 0.0588 for 7342 Fo > 4sig(Fo) and 0.0669 for all 8164 data REM 489 parameters refined using 0 restraints END WGHT 0.0317 6.6448 REM Highest difference peak 0.470, deepest hole -0.592, 1-sigma level 0.092 Q1 1 0.6986 0.8622 0.4830 11.00000 0.05 0.47 Q2 1 0.6926 0.6029 0.4855 11.00000 0.05 0.39 Q3 1 0.4352 0.5053 0.5073 11.00000 0.05 0.39 Q4 1 0.3401 0.2865 0.1595 11.00000 0.05 0.39 Q5 1 0.7591 0.8363 0.4787 11.00000 0.05 0.37 Q6 1 0.6003 0.1977 0.4288 11.00000 0.05 0.36 Q7 1 0.5990 0.7826 0.4766 11.00000 0.05 0.36 Q8 1 0.6152 0.7666 0.4394 11.00000 0.05 0.36 Q9 1 0.6493 0.7832 0.5569 11.00000 0.05 0.35 Q10 1 0.6146 0.1457 0.4527 11.00000 0.05 0.35 Q11 1 0.7853 0.1420 0.4568 11.00000 0.05 0.35 Q12 1 0.6812 0.6764 0.4979 11.00000 0.05 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9.32 3.93 8 3 13 1.58 1.80 -8 3 -14 6.03 2.28 -8 3 14 6.93 3.09 8 3 14 4.62 1.57 8 3 -14 5.55 2.64 8 -3 14 6.67 4.19 -8 3 -15 2.79 1.62 -8 3 15 6.84 2.19 8 3 15 8.26 3.59 8 3 -15 13.40 5.10 8 -3 15 12.14 4.15 -8 3 -16 8.19 2.50 -8 3 16 5.16 1.22 8 3 16 13.09 4.11 8 3 -16 20.38 5.32 8 -3 -16 8.74 2.94 8 -3 16 18.21 5.35 8 3 17 28.73 4.64 8 3 -17 24.55 7.44 8 -3 -17 25.87 7.93 8 -3 17 22.25 6.25 8 3 18 7.57 2.60 8 3 -18 7.78 3.25 8 -3 -18 10.73 3.63 8 -3 18 3.51 2.50 -8 -4 0 5.31 2.09 -8 4 0 2.87 1.29 8 4 0 3.91 1.13 -8 -4 0 2.48 1.01 8 -4 0 7.10 3.83 -8 -4 -1 73.20 10.24 -8 -4 1 97.91 10.02 -8 4 -1 102.00 11.09 -8 4 1 75.67 11.91 8 4 1 77.21 9.04 8 4 -1 70.72 10.46 -8 -4 1 76.15 8.83 8 -4 -1 89.83 8.86 -8 -4 -1 67.11 8.61 8 -4 1 68.08 9.12 -8 -4 -2 5.50 1.71 -8 -4 2 1.84 0.82 -8 4 -2 9.66 2.29 -8 4 2 6.90 2.72 8 4 2 1.40 0.47 8 4 -2 5.69 1.31 -8 -4 2 2.50 0.74 8 -4 -2 3.81 2.31 8 -4 2 4.32 3.33 -8 -4 -2 5.29 0.94 -8 -4 -3 337.75 18.08 -8 -4 3 374.09 16.06 -8 4 -3 361.53 16.91 -8 4 3 308.92 13.50 8 4 -3 324.32 13.52 8 -4 -3 365.79 16.88 8 -4 3 327.37 13.98 -8 -4 -4 68.62 9.23 -8 -4 4 38.52 6.14 -8 4 -4 44.43 5.95 -8 4 4 73.10 10.60 8 4 -4 56.21 8.05 8 -4 -4 39.61 7.10 8 -4 4 67.19 7.20 -8 -4 -5 128.28 15.75 -8 -4 5 98.27 11.21 -8 4 -5 102.69 13.74 -8 4 5 111.96 10.67 8 4 -5 107.76 12.03 8 -4 -5 90.44 8.80 8 -4 5 124.46 12.05 -8 -4 6 24.64 5.19 -8 4 -6 20.37 5.64 -8 4 6 35.14 5.60 8 4 -6 36.51 6.68 8 -4 -6 14.02 4.63 8 -4 6 39.62 7.16 -8 -4 -7 92.96 13.20 -8 -4 7 73.44 9.96 -8 4 -7 96.14 14.18 -8 4 7 107.84 15.53 8 4 -7 99.65 15.86 8 -4 -7 71.98 8.51 8 -4 7 96.24 10.79 -8 -4 -8 12.96 3.13 -8 -4 8 38.67 5.81 -8 4 -8 38.19 6.18 -8 4 8 13.00 3.23 8 4 -8 22.14 5.13 8 -4 -8 40.60 6.17 8 -4 8 20.32 4.85 -8 -4 -9 34.26 7.59 -8 -4 9 20.32 5.25 -8 4 -9 28.11 7.31 -8 4 9 38.37 7.45 8 4 -9 20.33 5.37 8 4 -9 33.51 9.72 8 -4 -9 11.91 3.42 8 4 9 20.06 4.68 8 4 9 18.52 4.42 8 -4 9 40.61 6.77 -8 -4 -10 16.36 4.04 -8 -4 10 32.68 7.06 -8 4 -10 35.46 7.84 -8 4 10 24.30 5.63 8 4 -10 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3.61 -8 5 16 5.89 2.32 8 5 16 11.22 3.85 8 5 -16 2.43 2.46 8 -5 -16 10.47 3.45 8 -5 16 8.88 3.32 8 5 17 8.98 2.69 8 5 -17 3.36 2.07 8 -5 -17 2.61 1.74 8 -5 17 9.10 3.67 8 5 18 7.75 2.95 8 5 -18 7.93 2.76 8 -5 -18 12.86 4.21 8 -5 18 27.20 7.43 -8 -6 0 20.27 3.38 -8 -6 0 20.88 3.05 8 -6 0 28.33 5.86 -8 -6 -1 14.04 2.85 -8 -6 1 13.14 2.23 -8 6 -1 17.38 3.11 -8 6 1 12.48 3.43 8 6 -1 7.24 1.56 -8 -6 1 17.46 2.69 -8 -6 -1 16.76 2.38 8 -6 -1 23.49 4.61 8 -6 1 16.56 3.53 -8 -6 -1 7.73 1.22 -8 -6 -2 206.73 13.00 -8 -6 2 194.36 33.76 -8 6 -2 188.20 15.05 -8 6 2 185.28 14.72 8 6 -2 192.16 32.82 -8 -6 2 142.27 10.94 8 -6 -2 192.51 32.50 -8 -6 -2 177.55 13.41 8 -6 2 189.43 15.02 -8 -6 -2 180.64 13.61 -8 -6 -3 48.46 7.12 -8 -6 3 47.30 6.83 -8 6 -3 46.80 6.49 -8 6 3 37.71 7.63 8 6 -3 43.06 6.63 8 -6 -3 54.34 8.12 8 -6 3 37.05 5.92 -8 -6 -4 169.99 14.90 -8 -6 4 158.19 16.34 -8 6 -4 147.31 15.48 -8 6 4 166.21 19.67 8 6 -4 166.88 17.19 8 -6 -4 166.15 19.03 8 -6 4 145.09 13.91 -8 -6 -5 9.89 2.68 -8 -6 5 2.45 1.37 -8 6 -5 0.77 1.35 -8 6 5 5.31 1.77 8 6 -5 2.53 1.45 8 -6 -5 5.16 3.88 8 -6 5 0.72 3.06 -8 -6 -6 321.04 18.96 -8 -6 6 297.35 14.59 -8 6 -6 323.49 15.82 -8 6 6 316.79 16.07 8 6 -6 322.63 18.34 8 -6 -6 312.57 15.61 8 -6 6 313.15 21.04 -8 -6 7 13.53 3.78 -8 6 -7 23.07 6.29 -8 6 7 11.36 4.21 8 6 -7 12.78 3.55 8 -6 -7 15.08 4.70 8 -6 7 11.99 5.56 -8 -6 8 180.17 10.97 -8 6 -8 191.96 10.67 -8 6 8 207.72 12.01 8 6 8 181.95 10.97 8 6 -8 217.32 18.74 8 -6 -8 212.55 18.74 8 -6 8 198.78 11.59 -8 -6 9 25.02 5.19 -8 6 -9 36.11 7.62 -8 6 9 24.62 5.80 8 6 9 24.11 5.98 8 6 -9 33.20 7.61 8 -6 -9 28.74 6.92 8 -6 9 17.35 4.70 -8 -6 10 81.86 21.78 -8 6 -10 109.95 9.72 -8 6 10 130.41 8.66 8 6 10 97.35 12.83 8 6 -10 153.85 20.15 8 -6 -10 101.24 7.79 8 -6 10 121.76 9.04 -8 6 -11 45.04 6.64 -8 6 11 33.34 7.13 8 6 11 34.37 7.63 8 6 -11 41.66 8.73 8 -6 11 31.79 6.37 -8 6 -12 100.13 10.03 -8 6 12 115.89 13.23 8 6 12 76.52 12.14 8 6 -12 133.12 15.94 8 -6 -12 95.64 7.95 8 -6 12 135.00 9.82 -8 6 -13 58.31 10.48 -8 6 13 77.90 7.72 8 6 13 86.04 13.50 8 6 -13 54.75 7.56 8 -6 -13 103.37 10.83 8 -6 13 74.61 7.43 -8 6 -14 24.37 6.54 -8 6 14 25.55 7.29 8 6 14 27.03 7.06 8 6 -14 38.43 6.82 8 -6 -14 9.69 4.04 8 -6 14 23.60 6.82 -8 6 15 25.20 6.09 8 6 15 18.37 4.58 8 6 -15 21.95 6.62 8 -6 -15 13.28 4.33 8 -6 15 26.06 6.75 -8 6 16 5.98 1.80 8 6 16 11.08 4.33 8 6 -16 24.69 7.13 8 -6 -16 8.03 2.41 8 -6 16 14.45 5.20 -8 6 17 24.38 5.74 8 6 17 23.50 5.72 8 6 -17 34.56 8.09 8 -6 -17 31.14 7.65 8 6 18 3.07 3.14 8 6 -18 9.85 3.69 8 -6 -18 6.20 2.71 8 -6 18 8.08 4.26 -8 -7 0 387.70 25.82 -8 7 0 350.45 22.93 -8 -7 0 252.90 12.85 8 -7 0 329.87 17.72 -8 -7 0 322.58 16.37 -8 -7 -1 840.54 141.05 -8 -7 1 768.50 38.86 -8 7 -1 780.53 130.38 -8 7 1 821.58 137.33 -8 -7 1 642.61 32.24 -8 -7 -1 696.25 34.74 8 -7 -1 797.15 133.09 8 -7 1 834.61 139.33 -8 -7 -1 748.50 37.32 -8 -7 1 761.31 38.18 -8 -7 -2 219.20 15.86 -8 -7 2 208.34 13.86 -8 7 -2 200.14 11.34 -8 7 2 206.06 11.56 -8 -7 -2 165.18 12.47 8 -7 -2 199.18 11.72 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67.26 10.04 -8 7 -10 65.86 10.81 -8 7 10 57.35 9.59 8 7 10 64.58 7.43 8 7 -10 52.33 6.24 8 7 -10 82.33 9.45 8 -7 10 60.28 7.16 -8 7 -11 21.15 5.54 -8 7 11 24.18 6.46 8 7 11 15.25 4.65 8 7 -11 31.22 5.42 8 -7 -11 23.61 6.95 8 -7 11 23.00 6.19 -8 7 -12 6.40 1.85 -8 7 12 6.57 2.61 8 7 12 1.76 2.72 8 7 -12 9.97 3.64 8 -7 -12 7.06 4.32 8 -7 12 0.32 3.15 -8 7 -13 5.74 1.34 -8 7 13 10.07 3.12 8 7 13 9.83 3.73 8 7 -13 5.78 2.46 8 -7 -13 10.95 4.37 8 -7 13 13.10 5.25 -8 7 14 -0.50 2.14 8 7 14 2.45 2.63 8 -7 -14 3.26 2.84 -8 7 15 4.28 2.10 8 7 15 1.36 2.13 8 7 -15 -2.05 2.39 8 -7 -15 3.94 2.08 8 -7 15 6.42 3.30 -8 7 16 8.28 3.16 8 7 16 3.89 3.23 8 7 -16 4.24 2.69 8 -7 -16 6.21 4.85 8 -7 16 -0.39 2.95 -8 7 17 6.78 3.18 8 7 17 3.69 3.39 8 7 -17 1.18 3.03 8 -7 -17 1.74 1.92 8 -7 17 4.14 3.05 -8 8 0 4.78 2.34 -8 -8 0 5.38 1.47 8 -8 0 8.62 3.49 -8 -8 0 7.05 1.89 -8 8 -1 9.17 2.56 8 8 1 18.81 4.46 -8 -8 1 15.86 3.15 -8 -8 -1 11.81 2.22 8 -8 -1 28.81 6.58 8 -8 1 21.36 5.24 -8 -8 -1 18.56 3.53 -8 -8 1 16.00 3.28 -8 8 -2 11.16 3.15 -8 8 2 7.57 3.07 8 8 2 11.48 4.84 -8 -8 -2 3.55 0.86 8 -8 -2 16.34 5.10 8 -8 2 12.68 5.16 -8 -8 -2 11.59 2.20 -8 -8 2 9.86 2.35 -8 8 -3 4.14 2.02 -8 8 3 5.36 2.37 8 8 3 4.11 2.66 8 -8 -3 3.84 3.07 8 -8 3 0.76 3.36 -8 -8 3 9.04 2.60 -8 8 -4 95.91 16.33 -8 8 4 139.78 17.19 8 8 4 96.43 16.22 8 -8 -4 97.11 17.55 8 -8 4 118.02 17.22 -8 8 -5 10.68 3.29 -8 8 5 3.09 2.50 8 8 5 7.91 2.78 8 8 -5 10.92 3.06 8 8 -5 5.18 2.23 8 -8 -5 12.35 4.82 8 -8 5 10.54 5.27 -8 8 -6 194.78 14.58 -8 8 6 222.15 19.70 8 8 6 192.56 14.38 8 8 -6 185.02 12.65 8 8 -6 215.37 16.17 8 -8 -6 187.32 20.13 8 -8 6 203.29 18.69 -8 8 -7 34.17 7.99 -8 8 7 7.61 2.79 8 8 7 41.98 9.74 8 8 -7 12.10 3.65 8 8 -7 16.14 3.58 8 -8 -7 36.35 8.43 8 -8 7 15.46 4.67 -8 8 -8 239.52 15.65 -8 8 8 258.81 14.89 8 8 8 235.26 13.89 8 8 -8 253.83 13.57 8 8 -8 261.32 16.29 8 -8 8 262.88 15.47 -8 8 -9 115.47 8.12 -8 8 9 78.25 13.52 8 8 9 104.27 8.62 8 8 -9 73.24 6.87 8 8 -9 86.31 12.57 8 -8 9 67.31 7.59 -8 8 -10 128.26 9.84 -8 8 10 134.84 13.00 8 8 10 139.99 16.09 8 8 -10 149.35 14.13 8 -8 -10 134.39 9.44 8 -8 10 102.78 17.50 -8 8 -11 2.58 1.56 -8 8 11 1.84 2.52 8 8 11 11.93 4.79 8 8 -11 2.50 2.25 8 -8 -11 3.64 3.20 8 -8 11 2.58 3.33 -8 8 -12 5.64 1.82 -8 8 12 7.25 3.28 8 8 12 17.85 4.21 8 8 -12 10.06 3.85 8 -8 -12 9.75 4.84 8 -8 12 7.95 4.73 -8 8 -13 2.72 1.28 -8 8 13 10.69 4.37 8 8 13 10.14 4.41 8 8 -13 13.35 4.35 8 -8 -13 7.29 3.31 8 -8 13 17.79 6.15 -8 8 14 1.39 1.69 8 8 14 1.13 2.29 8 8 -14 4.48 2.12 8 -8 -14 2.48 2.66 8 -8 14 3.84 3.18 -8 8 15 6.85 2.37 8 8 15 6.45 2.62 8 -8 -15 4.98 3.04 8 -8 15 20.66 6.59 -8 8 16 4.43 2.68 8 8 16 13.31 4.82 8 8 -16 17.69 5.30 8 -8 -16 1.00 2.88 8 -8 16 19.92 5.44 -8 8 17 8.43 3.53 8 8 17 -0.81 2.64 8 8 -17 3.56 2.14 8 -8 -17 1.34 2.07 8 -8 17 9.13 3.80 -8 9 0 31.31 9.45 8 9 0 29.19 7.38 -8 -9 0 26.30 6.26 8 -9 0 30.76 8.34 -8 -9 0 28.43 6.83 -8 9 -1 185.52 11.01 -8 9 1 215.62 16.88 8 9 -1 193.41 10.86 8 9 1 174.38 10.23 -8 -9 -1 146.44 8.50 8 -9 -1 190.13 11.30 8 -9 1 217.06 12.65 -8 -9 -1 192.08 9.90 -8 -9 1 180.96 10.73 -8 9 -2 48.61 9.47 -8 9 2 32.55 9.58 8 9 -2 30.25 7.48 8 9 2 39.70 7.18 -8 -9 -2 10.38 2.43 8 -9 -2 33.14 9.30 8 -9 2 44.83 8.47 -8 -9 -2 37.65 5.88 -8 -9 2 31.86 8.32 -8 9 -3 23.74 6.69 -8 9 3 29.93 7.93 8 9 -3 19.94 5.70 8 9 3 21.02 6.06 -8 -9 -3 9.62 2.20 8 -9 -3 15.78 5.49 -8 -9 -3 14.90 3.69 8 -9 3 32.04 9.69 -8 -9 3 16.86 4.54 -8 9 -4 23.02 5.00 -8 9 4 16.19 4.91 8 9 4 15.20 5.33 8 9 -4 21.09 4.87 8 -9 -4 22.20 5.80 8 -9 4 13.20 4.89 -8 -9 4 25.15 5.42 -8 9 -5 34.92 7.45 -8 9 5 60.42 7.81 8 9 -5 48.95 4.83 8 9 5 37.96 8.48 8 -9 -5 39.71 8.67 8 -9 5 50.33 7.24 -8 -9 5 42.78 8.83 -8 9 -6 9.57 3.37 -8 9 6 2.19 1.62 8 9 6 3.63 2.21 8 9 -6 2.56 1.35 8 -9 -6 -2.43 2.83 8 -9 6 6.34 2.90 -8 -9 6 6.88 3.87 -8 9 -7 41.47 7.76 -8 9 7 41.73 6.71 8 9 7 32.92 7.16 8 9 -7 39.08 6.65 8 -9 7 46.82 7.53 -8 -9 7 44.21 6.21 -8 9 -8 2.81 1.79 -8 9 8 7.54 2.67 8 9 8 11.52 4.48 8 9 -8 6.09 2.38 8 9 -8 3.65 2.12 8 -9 8 9.90 5.91 -8 9 -9 25.20 5.93 -8 9 9 29.14 7.06 8 9 -9 21.24 4.89 8 9 9 30.23 5.88 8 9 -9 26.90 6.62 8 -9 -9 26.89 6.64 8 -9 9 34.89 7.00 -8 9 -10 70.66 6.09 -8 9 10 51.45 11.68 8 9 10 66.07 7.16 8 9 -10 69.11 8.88 8 -9 -10 75.95 7.81 8 -9 10 76.85 8.30 -8 9 -11 82.76 12.83 -8 9 11 104.78 14.67 8 9 11 96.72 9.56 8 9 -11 94.01 13.90 8 -9 -11 109.65 11.74 8 -9 11 95.33 11.00 -8 9 -12 12.61 3.83 -8 9 12 9.38 3.94 8 9 12 10.65 4.17 8 9 -12 14.02 4.14 8 -9 -12 9.71 4.14 8 -9 12 8.69 3.88 -8 9 13 14.49 4.63 8 9 13 6.17 3.08 8 9 -13 22.18 5.27 8 -9 -13 17.05 5.26 8 -9 13 22.17 6.31 -8 9 14 25.14 10.71 8 9 14 51.39 7.86 8 9 -14 44.82 9.04 8 -9 -14 50.94 8.13 8 -9 14 53.92 8.23 -8 9 15 14.26 5.32 8 9 15 21.27 4.93 8 9 -15 33.04 6.72 8 -9 -15 18.51 4.92 8 -9 15 10.29 3.89 -8 9 16 17.40 5.69 8 9 16 19.77 5.73 8 9 -16 15.83 4.84 8 -9 -16 17.63 5.69 8 -9 16 20.85 6.56 -8 10 0 2.23 2.36 8 10 0 1.16 0.94 8 -10 0 12.03 5.88 -8 -10 0 2.11 1.12 -8 10 -1 11.21 4.58 -8 10 1 10.53 3.54 8 10 -1 10.26 3.29 8 10 1 4.17 2.28 8 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13.11 8 -10 8 61.76 8.99 -8 -10 8 68.79 6.10 -8 10 -9 10.55 2.87 -8 10 9 16.86 5.20 8 10 9 15.01 4.78 8 -10 -9 18.01 5.37 8 -10 9 15.18 6.39 -8 -10 9 24.79 5.48 -8 10 -10 12.63 4.02 -8 10 10 5.08 2.87 8 10 10 12.32 4.47 8 -10 -10 14.60 4.78 8 -10 10 1.46 3.32 -8 -10 10 23.93 4.67 -8 10 -11 2.80 1.34 -8 10 11 5.82 2.69 8 10 11 8.41 4.00 8 -10 -11 14.34 6.50 8 -10 11 4.41 3.19 -8 -10 11 10.79 4.23 -8 10 -12 4.71 1.31 -8 10 12 0.99 2.64 8 10 12 0.48 2.70 8 -10 -12 5.79 4.26 8 -10 12 -3.01 3.16 -8 -10 12 3.14 2.72 -8 10 13 8.98 3.33 8 10 13 2.44 1.49 8 -10 13 8.16 3.55 -8 -10 13 12.60 4.80 -8 10 14 7.98 2.92 8 10 14 4.32 3.14 8 -10 -14 9.01 3.22 8 -10 14 9.88 4.99 -8 -10 14 1.14 2.71 -8 10 15 3.30 1.83 8 10 15 4.44 2.73 8 -10 -15 7.94 4.69 8 -10 15 -0.51 3.26 -8 -10 15 11.83 4.73 -8 11 0 23.04 5.37 8 11 0 40.33 6.83 8 -11 0 14.64 4.47 -8 -11 0 35.17 6.73 -8 11 -1 12.07 3.79 -8 11 1 26.75 6.11 8 11 1 9.02 3.53 8 11 -1 17.22 4.12 8 -11 -1 14.32 5.22 8 -11 1 22.86 6.64 -8 -11 -1 17.17 3.79 -8 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-9 1.79 3.21 8 -11 9 8.43 4.66 -8 -11 9 4.86 2.40 -8 11 -10 6.86 2.37 -8 11 10 4.22 3.54 8 11 10 8.92 3.36 8 -11 -10 11.94 3.76 8 -11 10 2.59 3.32 -8 -11 10 12.08 5.69 -8 11 -11 8.88 2.84 -8 11 11 4.83 2.83 8 11 11 11.52 4.44 8 -11 -11 5.87 3.07 8 -11 11 4.90 3.53 -8 -11 11 9.96 4.21 -8 11 12 37.26 8.77 8 11 12 37.77 7.02 8 -11 12 30.00 7.62 -8 -11 12 51.07 9.04 -8 11 13 6.70 2.75 8 11 13 8.39 3.14 8 -11 -13 2.53 2.68 8 -11 13 14.03 4.11 -8 -11 13 8.05 3.24 -8 11 14 39.19 8.83 8 11 14 65.06 14.26 8 -11 -14 23.01 5.62 8 -11 14 37.41 8.05 -8 -11 14 55.49 11.30 8 11 15 12.62 4.81 8 -11 15 15.94 5.71 -8 12 0 8.39 2.50 8 12 0 7.07 3.42 8 -12 0 14.58 6.13 -8 -12 0 8.54 2.52 -8 12 -1 2.72 3.08 -8 12 1 7.88 4.82 8 12 1 2.25 2.21 8 12 -1 5.24 1.59 8 -12 -1 9.85 3.51 8 -12 1 3.72 3.62 -8 -12 -1 1.36 1.09 -8 -12 1 3.83 1.97 -8 12 -2 48.71 7.49 -8 12 2 61.43 10.25 8 12 -2 42.24 6.59 8 12 2 67.63 7.63 8 -12 -2 53.36 8.21 8 -12 2 53.45 10.43 -8 -12 2 50.97 6.68 -8 12 -3 134.35 15.00 -8 12 3 125.59 11.62 8 12 -3 106.42 12.15 8 12 3 119.67 13.86 8 -12 3 138.11 10.19 -8 -12 3 121.92 9.55 -8 12 -4 112.99 7.70 -8 12 4 114.53 14.09 8 12 -4 113.50 10.29 8 12 4 120.09 8.94 8 -12 4 138.11 10.53 -8 -12 4 105.21 6.90 -8 12 -5 129.72 15.20 -8 12 5 118.57 13.17 8 12 -5 125.17 10.15 8 12 5 116.89 11.60 8 -12 -5 107.51 12.47 8 -12 5 109.12 17.32 -8 -12 5 132.92 10.89 -8 12 -6 99.96 11.94 -8 12 6 111.22 14.85 8 12 -6 106.00 10.80 8 12 6 116.90 12.25 8 -12 -6 107.24 9.77 8 -12 6 117.38 11.19 -8 -12 6 115.07 12.91 -8 12 -7 163.87 13.70 -8 12 7 188.32 38.41 8 12 -7 153.62 15.09 8 12 7 166.52 21.50 8 -12 -7 164.54 14.44 8 -12 7 178.41 33.77 -8 -12 7 159.96 13.62 -8 12 -8 29.62 7.56 -8 12 8 22.70 6.29 8 12 8 28.80 7.78 8 -12 8 15.11 5.28 -8 -12 8 28.33 7.45 -8 12 -9 84.87 12.37 -8 12 9 92.75 16.57 8 12 9 94.88 14.71 8 -12 -9 96.17 13.53 8 -12 9 74.45 10.45 -8 -12 9 107.25 13.71 -8 12 -10 11.14 3.57 -8 12 10 6.15 2.61 8 12 10 9.34 4.42 8 -12 -10 13.32 4.71 8 -12 10 13.68 4.51 -8 -12 10 7.21 4.31 8 12 11 42.89 6.56 8 -12 -11 25.67 5.09 8 -12 11 31.78 5.69 -8 -12 11 42.42 6.59 -8 12 12 9.26 3.18 8 12 12 5.53 3.07 8 -12 -12 1.26 2.85 8 -12 12 18.19 6.52 -8 -12 12 3.88 2.70 -8 12 13 20.19 5.63 8 12 13 5.76 3.05 8 -12 -13 3.10 2.96 8 -12 13 6.29 4.29 -8 -12 13 18.29 5.37 -8 12 14 0.30 2.70 8 12 14 2.80 3.18 8 -12 -14 4.19 3.05 8 -12 14 7.40 3.70 -8 -12 14 13.82 5.17 -8 13 0 110.49 12.92 8 13 0 114.64 12.70 8 -13 0 125.27 11.85 -8 -13 0 95.69 8.41 -8 13 -1 4.31 1.91 -8 13 1 7.88 3.13 8 13 1 6.59 3.12 8 13 -1 6.17 2.87 8 -13 -1 17.98 6.51 8 -13 1 5.42 3.91 -8 -13 1 6.96 2.60 -8 13 -2 55.43 12.02 -8 13 2 47.00 8.73 8 13 -2 46.56 8.59 8 13 2 56.60 11.34 8 -13 2 51.45 10.15 -8 -13 2 52.78 8.94 -8 13 -3 15.63 4.42 -8 13 3 17.72 5.64 8 13 -3 7.97 3.11 8 13 3 7.96 3.52 8 -13 -3 11.91 3.90 8 -13 3 10.84 4.07 -8 -13 3 14.23 3.85 -8 13 -4 104.04 10.57 -8 13 4 117.89 14.69 8 13 -4 108.33 12.41 8 13 4 127.03 14.45 8 -13 -4 100.89 16.53 8 -13 4 98.91 9.68 -8 -13 4 111.95 9.53 -8 13 -5 33.93 5.91 -8 13 5 42.63 8.00 8 13 -5 39.34 7.77 8 13 5 22.96 4.94 8 -13 -5 37.35 7.22 8 -13 5 32.23 7.02 -8 -13 5 47.19 5.14 -8 13 -6 12.85 3.85 -8 13 6 1.94 1.53 8 13 -6 6.01 2.32 8 13 6 9.60 5.11 8 -13 -6 9.76 5.28 8 -13 6 3.41 4.84 -8 -13 6 6.90 3.13 -8 13 -7 36.40 7.81 -8 13 7 50.65 8.29 8 13 7 50.91 8.48 8 -13 -7 45.47 8.32 8 -13 7 72.80 11.30 -8 -13 7 54.40 7.52 -8 13 -8 5.04 2.19 -8 13 8 5.36 2.65 8 -13 -8 11.37 3.99 8 -13 8 12.12 4.34 -8 -13 8 10.08 4.60 -8 13 -9 27.04 7.11 -8 13 9 36.76 6.78 8 13 9 17.64 5.47 8 -13 9 26.30 7.54 -8 -13 9 28.54 7.27 -8 13 10 14.18 4.54 8 13 10 36.20 6.12 8 -13 -10 21.90 6.87 8 -13 10 14.47 4.88 -8 -13 10 21.65 6.67 -8 13 11 22.12 5.00 8 13 11 30.94 6.88 8 -13 -11 17.72 5.84 8 -13 11 8.53 3.83 -8 -13 11 21.70 5.22 -8 13 12 22.29 6.78 8 13 12 15.48 4.94 8 -13 -12 10.07 3.96 8 -13 12 20.59 5.36 -8 -13 12 17.22 4.78 -8 14 0 8.83 3.70 8 14 0 2.54 1.97 8 -14 0 12.98 4.79 -8 14 -1 15.94 5.85 -8 14 1 27.49 7.38 8 14 -1 23.40 6.57 8 14 1 26.98 7.31 8 -14 1 35.02 4.92 -8 -14 1 25.44 6.28 -8 14 -2 90.86 10.93 -8 14 2 88.43 13.15 8 14 2 71.31 9.97 8 14 -2 82.56 9.12 8 -14 -2 92.04 9.19 8 -14 2 92.62 11.01 -8 -14 2 89.59 8.34 -8 14 -3 10.93 4.56 -8 14 3 32.93 4.47 8 14 -3 15.91 5.36 8 14 3 17.30 5.49 8 -14 -3 12.58 4.89 8 -14 3 15.27 5.26 -8 -14 3 10.97 3.58 -8 14 -4 7.31 3.03 -8 14 4 18.91 6.44 8 14 -4 9.96 3.57 8 14 4 17.01 5.29 8 -14 -4 11.12 4.54 8 -14 4 -2.02 3.56 -8 -14 4 18.84 5.11 -8 14 -5 62.52 10.46 8 14 -5 63.37 10.48 8 14 5 70.97 11.25 8 -14 -5 83.81 11.88 8 -14 5 72.37 10.31 -8 -14 5 64.83 10.00 -8 14 -6 39.81 7.29 -8 14 6 40.86 6.75 8 14 6 49.43 8.59 8 -14 -6 26.92 6.45 8 -14 6 38.76 9.31 -8 -14 6 48.62 6.98 -8 14 -7 15.21 5.73 -8 14 7 26.98 7.32 8 14 7 21.89 6.16 8 -14 7 38.03 7.77 -8 -14 7 35.46 6.18 -8 14 -8 13.36 4.23 -8 14 8 19.49 6.83 8 14 8 5.02 2.88 8 -14 -8 12.42 5.17 8 -14 8 23.73 7.37 -8 -14 8 24.84 7.47 -8 14 -9 24.62 5.90 -8 14 9 25.49 5.89 8 14 9 17.61 5.63 8 -14 -9 11.02 3.18 8 -14 9 21.92 5.22 -8 -14 9 11.01 3.22 -8 14 10 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17.06 -10 1 -7 89.49 16.06 -10 -1 7 81.24 13.71 -10 1 7 94.28 14.19 10 1 7 53.32 8.06 10 1 -7 107.47 20.37 10 -1 -7 85.76 13.09 10 1 7 74.63 10.74 10 -1 7 104.36 14.85 -10 -1 -8 112.06 14.43 -10 1 -8 115.00 15.27 -10 -1 8 94.04 9.78 -10 1 8 103.98 11.80 10 1 8 71.18 6.49 10 1 -8 113.45 19.33 10 -1 -8 124.97 9.05 10 1 8 108.90 9.26 10 -1 8 106.21 10.34 -10 -1 -9 93.08 11.44 -10 1 -9 46.82 13.30 -10 -1 9 58.93 5.85 -10 1 9 85.47 8.82 10 1 -9 73.76 13.61 10 -1 -9 42.84 8.50 -10 -1 -10 13.22 3.18 -10 1 -10 7.23 3.18 -10 -1 10 9.59 3.18 -10 1 10 7.17 2.97 10 1 -10 11.11 3.86 10 -1 -10 2.81 2.61 10 1 10 4.02 1.81 10 -1 10 6.14 2.83 -10 -1 -11 37.09 8.20 -10 1 -11 20.14 4.18 -10 -1 11 20.33 4.30 -10 1 11 33.88 6.51 10 1 -11 46.08 8.28 10 -1 -11 21.60 5.84 10 1 11 15.32 4.11 10 -1 11 25.22 6.14 -10 -1 -12 42.45 7.24 -10 1 -12 26.39 6.85 -10 -1 12 33.40 5.45 -10 1 12 39.59 5.89 10 1 -12 31.77 4.99 10 -1 -12 32.17 8.13 10 -1 12 29.96 5.11 -10 -1 -13 17.44 4.11 -10 1 -13 17.03 3.48 -10 -1 13 14.18 3.99 -10 1 13 8.86 3.11 10 1 -13 29.43 6.91 10 -1 -13 17.33 4.63 10 -1 13 7.89 2.00 -10 -1 -14 10.74 3.24 -10 1 -14 4.78 1.96 -10 1 14 2.30 0.80 10 1 -14 9.67 3.68 10 -1 -14 0.56 1.85 10 -1 14 2.59 1.60 -10 1 -15 23.04 6.76 10 1 -15 24.10 6.23 10 -1 -15 31.27 9.49 -10 1 -16 2.13 0.85 10 1 16 1.64 2.05 10 1 -16 9.97 3.54 10 -1 -16 3.09 2.75 10 1 17 14.43 5.02 10 -1 17 27.84 6.16 10 1 -17 16.16 5.43 10 -1 -17 11.52 4.96 -10 -2 0 468.20 24.42 -10 2 0 456.22 23.68 10 2 0 398.36 20.35 10 -2 0 432.11 22.23 -10 -2 0 410.44 20.79 -10 -2 -1 67.14 11.65 -10 -2 1 59.50 9.18 -10 2 -1 64.29 9.89 -10 2 1 66.01 8.69 10 2 -1 69.83 8.79 10 2 1 52.60 6.64 10 -2 -1 68.11 8.90 10 -2 1 78.09 9.98 -10 -2 -1 72.76 8.85 -10 -2 -2 611.25 31.31 -10 -2 2 510.24 29.03 -10 2 -2 501.10 26.04 -10 2 2 609.72 31.29 10 2 -2 653.02 33.08 10 2 2 460.76 23.29 10 -2 -2 501.91 25.72 10 -2 2 603.19 30.55 -10 -2 -2 583.56 29.20 -10 -2 -3 40.14 6.73 -10 -2 3 38.99 6.47 -10 2 3 48.52 7.64 10 2 -3 48.66 8.61 10 2 3 39.83 5.04 10 -2 -3 45.45 6.23 10 -2 3 44.26 7.63 -10 -2 -3 38.59 4.81 -10 -2 -4 135.84 14.29 -10 -2 4 92.34 9.09 -10 2 -4 100.44 12.17 -10 2 4 134.83 11.30 10 2 -4 137.18 11.12 10 -2 -4 111.04 9.34 10 -2 4 111.31 9.37 -10 -2 -4 107.06 8.77 -10 -2 -5 160.45 10.48 -10 2 -5 170.87 12.99 -10 -2 5 162.64 14.98 -10 2 5 145.52 11.43 10 2 -5 144.36 14.44 10 -2 -5 155.96 8.83 10 2 5 139.88 6.72 10 -2 5 147.76 7.99 -10 -2 -5 132.84 6.33 -10 -2 -6 139.31 11.94 -10 2 -6 105.75 15.19 -10 -2 6 108.41 13.78 -10 2 6 159.42 12.03 10 2 6 80.17 8.89 10 2 -6 128.81 13.83 10 -2 -6 131.09 13.62 10 2 6 100.98 10.65 10 -2 6 133.89 7.55 -10 -2 -7 144.30 9.27 -10 2 -7 151.95 12.50 -10 -2 7 166.75 9.61 -10 2 7 150.52 8.99 10 2 7 114.79 16.18 10 2 -7 167.01 17.21 10 -2 -7 162.16 10.07 10 2 7 140.68 7.23 10 -2 7 156.18 9.36 -10 -2 -8 17.65 4.51 -10 2 -8 22.95 4.93 -10 -2 8 11.18 3.46 -10 2 8 17.31 4.27 10 2 8 5.73 1.72 10 2 -8 10.96 4.07 10 -2 -8 16.73 4.96 10 2 8 8.99 2.54 10 -2 8 11.19 3.72 -10 -2 -9 13.04 3.60 -10 2 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10 2 17 19.89 4.88 10 2 -17 9.51 3.34 10 -2 -17 12.63 4.72 -10 -3 0 154.75 16.93 -10 3 0 147.36 12.52 10 3 0 122.92 12.03 10 -3 0 144.43 15.95 -10 -3 0 130.39 10.00 -10 -3 -1 84.02 15.56 -10 -3 1 73.93 11.30 -10 3 -1 84.47 16.00 -10 3 1 78.46 13.46 10 3 -1 68.70 10.97 10 3 1 74.49 9.75 10 -3 -1 77.22 9.87 10 -3 1 78.00 11.29 -10 -3 1 59.36 9.06 -10 -3 -1 68.92 9.57 -10 -3 -2 134.95 15.50 -10 -3 2 130.99 14.03 -10 3 -2 142.82 15.98 -10 3 2 155.83 17.28 10 3 -2 104.96 9.71 10 3 2 102.86 7.98 10 -3 -2 129.35 10.55 10 -3 2 125.25 10.31 -10 -3 -2 126.22 10.03 -10 -3 -3 163.95 14.17 -10 -3 3 192.82 35.24 -10 3 -3 158.50 12.75 -10 3 3 168.69 18.70 10 3 -3 148.48 13.84 10 3 3 138.04 10.80 10 -3 -3 165.71 13.35 10 -3 3 151.76 16.83 -10 -3 -3 132.26 10.17 -10 -3 -4 226.32 14.36 -10 -3 4 209.17 15.40 -10 3 -4 218.37 11.47 -10 3 4 229.05 11.94 10 3 -4 227.24 14.91 10 -3 -4 225.50 11.66 10 -3 4 254.30 12.63 -10 -3 -4 209.25 9.76 -10 -3 -5 184.08 12.77 -10 -3 5 219.75 16.97 -10 3 5 186.10 13.19 10 3 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212.51 9.88 -10 -4 -3 152.36 13.96 -10 -4 3 158.91 12.40 -10 4 -3 158.45 12.92 -10 4 3 140.47 16.69 10 4 3 101.44 10.68 10 4 -3 120.41 16.86 10 -4 -3 152.64 8.61 10 -4 3 126.08 28.44 -10 -4 -3 122.00 12.84 -10 -4 -4 366.51 22.68 -10 -4 4 370.98 21.86 -10 4 -4 352.56 20.12 -10 4 4 340.90 22.55 10 4 -4 298.67 14.50 10 -4 -4 346.86 17.14 10 -4 4 328.19 15.96 -10 -4 -5 203.93 19.09 -10 -4 5 186.59 14.41 -10 4 -5 201.04 16.41 -10 4 5 211.60 16.46 10 4 -5 174.58 15.60 10 -4 -5 203.47 10.86 10 -4 5 186.59 9.76 -10 -4 -6 215.92 15.82 -10 -4 6 208.87 17.57 -10 4 -6 205.58 11.46 -10 4 6 217.94 21.96 10 4 -6 201.56 11.07 10 -4 -6 227.47 13.06 10 -4 6 208.94 11.54 -10 -4 -7 148.02 10.64 -10 -4 7 160.96 14.06 -10 4 -7 153.01 12.90 -10 4 7 148.03 11.01 10 4 -7 151.07 14.46 10 -4 -7 154.76 10.27 10 -4 7 155.80 11.51 -10 -4 -8 25.37 6.02 -10 -4 8 25.80 5.61 -10 4 -8 29.44 6.76 -10 4 8 36.31 8.91 10 4 -8 31.01 7.15 10 -4 -8 22.73 5.39 10 -4 8 23.34 6.12 -10 -4 -9 1.82 2.02 -10 -4 9 2.32 1.55 -10 4 -9 5.22 1.91 -10 4 9 1.96 2.17 10 4 -9 6.20 2.83 10 -4 -9 8.65 4.23 10 -4 9 1.72 2.21 -10 -4 -10 40.69 8.70 -10 4 -10 24.39 5.37 -10 -4 10 7.76 2.39 -10 4 10 26.33 5.52 10 4 -10 34.94 8.51 10 -4 -10 39.87 8.63 10 -4 10 35.44 7.09 -10 -4 -11 52.31 9.61 -10 4 -11 41.35 6.47 -10 -4 11 29.08 7.16 -10 4 11 52.61 7.27 10 4 -11 61.58 12.03 10 -4 -11 44.09 6.77 10 -4 11 47.96 8.84 -10 4 -12 13.33 3.86 -10 4 12 13.18 3.67 10 4 -12 3.40 1.99 10 -4 -12 12.01 4.50 10 -4 12 17.37 5.15 -10 4 -13 16.04 4.70 -10 4 13 20.63 5.55 10 4 13 12.62 4.60 10 4 -13 32.98 6.47 10 -4 -13 -1.24 2.62 10 -4 13 17.02 4.68 -10 4 -14 15.80 4.41 -10 4 14 4.97 2.85 10 4 14 4.54 3.47 10 4 -14 5.27 2.18 10 -4 -14 2.74 2.94 10 -4 14 7.90 3.78 -10 4 -15 5.67 1.72 -10 4 15 16.66 5.63 10 4 15 24.44 6.58 10 4 -15 18.57 5.76 10 -4 -15 17.43 5.12 10 -4 15 20.49 5.70 -10 4 16 9.67 3.10 10 4 16 9.50 3.94 10 4 -16 8.50 4.87 10 -4 -16 14.34 5.58 10 -4 16 9.26 4.28 10 4 17 3.39 2.18 10 4 -17 5.10 2.50 10 -4 -17 7.28 3.50 -10 -5 0 120.90 15.75 -10 5 0 110.49 15.01 10 5 0 102.37 12.25 -10 -5 0 87.33 9.26 10 -5 0 96.60 16.62 -10 -5 -1 98.61 12.56 -10 -5 1 53.42 7.50 -10 5 1 89.29 11.11 10 5 1 38.80 5.49 10 5 -1 80.93 10.38 -10 -5 1 39.57 6.01 10 -5 -1 54.21 7.34 10 -5 1 84.65 11.78 -10 -5 -1 72.82 7.74 -10 -5 -2 107.95 13.49 -10 -5 2 84.57 11.73 -10 5 -2 89.51 12.38 -10 5 2 103.31 11.78 10 5 2 59.40 6.56 10 5 -2 101.52 12.40 10 -5 -2 100.67 16.61 10 -5 2 107.64 14.70 -10 -5 -2 98.47 10.32 -10 -5 -3 29.42 5.88 -10 -5 3 41.66 5.71 -10 5 -3 45.45 7.50 -10 5 3 25.15 5.51 10 5 -3 22.91 4.71 10 -5 -3 43.01 7.81 10 -5 3 22.46 4.51 -10 -5 -4 261.54 19.90 -10 -5 4 188.46 15.10 -10 5 -4 182.57 10.81 -10 5 4 222.79 17.52 10 5 -4 216.67 14.68 10 -5 -4 211.79 12.24 10 -5 4 233.17 12.80 -10 -5 -5 36.94 6.14 -10 -5 5 37.79 6.76 -10 5 -5 37.99 6.82 -10 5 5 28.81 8.14 10 5 -5 26.55 6.75 10 -5 -5 31.80 9.46 10 -5 5 21.30 5.79 -10 -5 -6 139.71 13.91 -10 -5 6 145.55 13.63 -10 5 -6 148.91 9.42 -10 5 6 129.41 10.03 10 5 -6 124.27 13.54 10 -5 -6 160.73 10.84 10 -5 6 123.34 11.42 -10 -5 -7 13.23 4.38 -10 -5 7 20.76 4.36 -10 5 -7 14.44 4.04 -10 5 7 18.93 4.61 10 5 -7 14.90 4.62 10 -5 -7 31.17 7.93 10 -5 7 12.11 4.12 -10 -5 -8 30.86 6.76 -10 -5 8 29.84 6.35 -10 5 -8 28.56 6.19 -10 5 8 21.40 4.80 10 5 -8 22.74 5.91 10 -5 -8 40.78 7.67 10 -5 8 23.91 5.67 -10 -5 -9 2.67 1.67 -10 -5 9 3.32 1.57 -10 5 -9 4.58 1.95 -10 5 9 3.81 2.02 10 5 -9 3.87 2.30 10 -5 -9 10.73 5.04 10 -5 9 4.01 3.52 -10 -5 -10 26.02 6.86 -10 -5 10 25.92 6.21 -10 5 -10 49.64 7.82 -10 5 10 28.44 6.72 10 5 -10 27.50 7.35 10 -5 -10 32.89 8.38 10 -5 10 22.15 5.52 -10 -5 11 7.74 2.15 -10 5 -11 13.87 3.29 -10 5 11 19.33 5.45 10 5 11 19.76 5.88 10 5 -11 19.04 5.07 10 -5 -11 17.36 6.03 10 -5 11 18.57 5.17 -10 5 -12 1.00 1.12 -10 5 12 4.09 1.90 10 5 12 2.84 2.62 10 5 -12 9.84 3.64 10 -5 -12 3.18 2.65 10 -5 12 -2.51 2.44 -10 5 -13 5.78 2.22 -10 5 13 3.86 2.07 10 5 13 0.13 2.39 10 5 -13 -0.25 2.53 10 -5 -13 3.94 2.73 10 -5 13 11.64 4.01 -10 5 -14 5.40 2.10 -10 5 14 8.11 2.72 10 5 14 6.48 2.75 10 5 -14 21.51 6.24 10 -5 -14 3.74 2.85 10 -5 14 8.41 2.93 -10 5 -15 5.96 1.71 -10 5 15 5.58 1.78 10 5 15 1.22 2.16 10 5 -15 -0.01 2.67 10 -5 -15 2.70 1.70 10 -5 15 3.15 2.52 -10 5 16 2.09 1.08 10 5 16 4.00 3.39 10 5 -16 11.85 3.44 10 -5 -16 4.42 2.32 10 -5 16 -2.30 2.40 10 5 17 3.88 2.42 10 5 -17 12.60 5.10 10 -5 -17 5.52 2.26 10 -5 17 4.54 2.45 -10 -6 0 9.05 2.33 -10 6 0 16.44 3.68 10 6 0 6.54 1.48 -10 -6 0 11.61 2.21 10 -6 0 14.60 4.28 -10 -6 -1 -1.62 2.03 -10 -6 1 4.64 1.58 -10 6 -1 1.99 2.17 -10 6 1 7.93 5.02 10 6 -1 -0.70 0.81 -10 -6 1 0.70 0.68 10 -6 -1 3.25 2.86 -10 -6 -1 1.29 0.54 10 -6 1 1.17 2.80 -10 -6 -2 22.30 5.74 -10 -6 2 23.26 6.30 -10 6 -2 35.72 7.12 -10 6 2 32.87 9.29 10 6 -2 28.81 7.08 10 -6 -2 28.27 8.05 10 -6 2 14.43 5.15 -10 -6 -2 17.33 4.28 -10 -6 -2 9.19 2.32 -10 -6 -3 31.65 8.84 -10 -6 3 25.17 6.53 -10 6 -3 15.83 5.08 -10 6 3 26.32 7.20 10 6 -3 30.70 7.50 10 -6 -3 9.18 4.54 10 -6 3 20.22 5.62 -10 -6 -4 81.55 14.00 -10 -6 4 67.36 11.13 -10 6 -4 80.90 13.00 -10 6 4 54.57 8.56 10 6 -4 69.16 11.70 10 -6 -4 61.38 9.55 10 -6 4 60.12 11.96 -10 -6 -5 86.90 10.97 -10 -6 5 78.19 8.87 -10 6 -5 82.12 7.70 -10 6 5 85.71 10.92 10 6 -5 81.51 9.56 10 -6 -5 86.54 9.68 10 -6 5 100.65 10.03 -10 -6 -6 33.75 7.27 -10 -6 6 5.68 2.15 -10 6 -6 18.70 4.34 -10 6 6 38.37 8.15 10 6 -6 39.91 8.92 10 -6 -6 13.64 5.42 10 -6 6 13.99 5.34 -10 -6 -7 72.58 11.82 -10 -6 7 62.82 10.16 -10 6 -7 71.25 10.97 -10 6 7 70.53 9.70 10 6 -7 79.12 13.29 10 -6 -7 88.40 13.24 10 -6 7 66.30 9.54 -10 -6 8 136.89 13.43 -10 6 -8 153.34 10.22 -10 6 8 166.73 11.67 10 6 -8 154.88 15.10 10 -6 -8 151.83 10.82 10 -6 8 145.30 10.45 -10 -6 9 14.07 3.01 -10 6 -9 26.55 5.67 -10 6 9 20.55 4.89 10 6 -9 22.49 5.31 10 -6 -9 14.83 4.46 10 -6 9 19.47 5.26 -10 -6 10 32.33 5.67 -10 6 -10 44.22 7.22 -10 6 10 36.64 6.10 10 6 10 47.20 8.33 10 6 -10 42.02 7.17 10 -6 -10 50.08 8.34 10 -6 10 29.24 4.84 -10 6 -11 16.30 4.04 -10 6 11 20.11 5.48 10 6 11 12.48 4.62 10 6 -11 18.97 5.13 10 -6 -11 9.05 4.47 10 -6 11 7.36 3.12 -10 6 -12 3.41 1.25 -10 6 12 3.91 1.77 10 6 12 4.06 3.16 10 6 -12 7.09 2.41 10 -6 -12 2.65 2.78 10 -6 12 2.07 2.62 -10 6 -13 38.62 8.35 -10 6 13 48.24 8.95 10 6 13 40.81 7.18 10 6 -13 46.80 10.32 10 -6 -13 57.51 9.52 10 -6 13 58.00 9.33 -10 6 -14 1.07 1.06 -10 6 14 5.00 2.29 10 6 14 6.47 2.59 10 6 -14 4.12 3.34 10 -6 -14 1.52 3.64 10 -6 14 5.30 2.69 -10 6 15 9.57 3.89 10 6 15 10.43 3.27 10 6 -15 15.17 5.73 10 -6 15 8.49 3.86 -10 6 16 6.86 3.03 10 6 16 16.43 5.88 10 6 -16 12.20 4.53 10 -6 -16 6.56 3.23 10 -6 16 9.16 4.12 -10 -7 0 5.47 1.99 -10 -7 0 6.77 1.77 10 -7 0 10.99 4.03 -10 -7 0 6.10 1.86 -10 -7 -1 286.51 23.95 -10 -7 1 291.22 20.02 -10 7 -1 282.67 18.34 -10 7 1 271.68 17.63 10 7 -1 184.31 11.54 -10 -7 1 222.65 12.67 -10 -7 -1 218.84 11.65 10 -7 -1 287.78 15.89 10 -7 1 247.92 16.93 -10 -7 -1 235.50 12.15 -10 -7 -2 81.60 13.65 -10 -7 2 93.29 14.73 -10 7 -2 72.67 11.00 -10 7 2 73.48 12.55 10 7 -2 72.90 11.82 10 -7 -2 82.42 12.53 10 -7 2 78.25 12.31 -10 -7 -3 168.63 16.18 -10 -7 3 159.19 14.97 -10 7 -3 158.65 17.43 -10 7 3 146.44 9.86 10 7 -3 164.33 12.85 10 -7 -3 151.26 10.97 10 -7 3 139.98 9.40 -10 -7 -4 45.77 12.85 -10 -7 4 53.67 6.07 -10 7 -4 55.46 9.26 -10 7 4 30.19 7.24 10 7 -4 45.81 12.61 10 -7 -4 42.94 8.87 10 -7 4 39.78 9.10 -10 -7 -5 20.01 4.43 -10 -7 5 17.99 4.16 -10 7 -5 24.71 5.68 -10 7 5 26.29 6.20 10 7 -5 30.65 6.56 10 -7 -5 25.59 6.12 10 -7 5 43.33 9.36 -10 -7 -6 7.09 2.39 -10 -7 6 7.53 2.35 -10 7 -6 0.77 1.94 -10 7 6 3.98 2.30 10 7 -6 -0.85 1.54 10 -7 -6 15.05 4.17 10 -7 6 -2.45 3.33 -10 -7 -7 21.19 4.86 -10 -7 7 38.78 7.71 -10 7 -7 36.00 8.03 -10 7 7 36.66 7.67 10 7 -7 40.69 7.86 10 -7 -7 25.94 6.90 10 -7 7 35.58 7.59 -10 -7 8 18.69 3.82 -10 7 -8 23.29 4.76 -10 7 8 13.33 5.68 10 7 8 21.64 5.28 10 7 -8 27.06 6.33 10 -7 -8 24.26 6.27 10 -7 8 18.57 5.49 -10 -7 9 23.35 5.81 -10 7 -9 25.90 6.60 -10 7 9 19.87 5.52 10 7 9 15.53 4.95 10 7 -9 26.78 6.98 10 -7 -9 25.55 6.85 10 -7 9 14.50 4.07 -10 7 -10 5.08 1.86 -10 7 10 2.73 2.48 10 7 10 4.76 2.86 10 7 -10 6.40 2.39 10 -7 -10 6.37 3.24 10 -7 10 11.11 4.67 -10 7 -11 13.02 3.83 -10 7 11 1.87 2.16 10 7 11 8.18 3.13 10 7 -11 -0.44 1.95 10 -7 -11 3.53 2.96 10 -7 11 19.47 5.46 -10 7 -12 4.83 1.65 -10 7 12 9.39 4.29 10 7 12 2.82 2.55 10 7 -12 3.91 2.08 10 -7 -12 4.56 2.84 10 -7 12 11.48 4.68 -10 7 -13 2.84 1.37 -10 7 13 4.53 2.39 10 7 13 1.72 2.65 10 7 -13 3.20 2.09 10 -7 -13 2.37 2.96 10 -7 13 2.41 2.77 -10 7 -14 2.86 1.11 -10 7 14 5.72 2.61 10 7 14 7.05 3.59 10 7 -14 6.97 3.25 10 -7 14 8.52 4.28 -10 7 15 6.75 3.80 10 7 15 0.21 2.47 10 7 -15 7.49 2.35 10 -7 -15 6.22 2.99 10 -7 15 7.27 3.37 -10 7 16 13.84 5.01 10 7 16 6.26 3.48 10 7 -16 20.69 5.30 10 -7 -16 15.14 5.27 10 -7 16 10.32 4.11 -10 -8 0 6.99 2.45 -10 8 0 14.64 4.87 10 -8 0 7.63 3.51 -10 -8 0 6.91 2.12 -10 -8 -1 28.86 6.38 -10 -8 1 13.05 4.70 -10 8 -1 16.82 4.21 -10 8 1 12.24 3.90 10 -8 -1 14.94 4.98 10 -8 1 25.06 6.51 -10 -8 -1 18.03 3.78 -10 -8 1 5.97 1.81 -10 -8 -2 11.21 4.22 -10 -8 2 5.45 2.01 -10 8 -2 7.68 3.04 -10 8 2 3.00 1.95 10 -8 -2 1.26 2.79 10 -8 2 6.16 2.67 -10 -8 2 2.30 1.17 -10 -8 -3 172.52 15.86 -10 -8 3 175.38 16.31 -10 8 -3 179.91 11.45 -10 8 3 187.63 20.16 10 -8 -3 160.95 20.30 10 -8 3 188.75 12.14 -10 -8 -4 15.44 3.99 -10 -8 4 28.55 6.61 -10 8 -4 27.31 7.21 -10 8 4 11.77 4.19 10 8 -4 22.70 4.92 10 -8 -4 28.66 6.88 10 -8 4 20.05 5.97 -10 -8 5 47.78 7.60 -10 8 -5 42.89 6.94 -10 8 5 58.06 9.47 10 8 5 52.68 8.71 10 8 -5 52.76 8.04 10 -8 -5 54.79 8.95 10 -8 5 58.37 9.41 -10 -8 6 40.37 8.42 -10 8 -6 54.10 9.06 -10 8 6 31.84 7.26 10 8 6 61.55 9.58 10 8 -6 40.07 8.30 10 -8 -6 34.99 7.14 10 -8 6 35.58 7.00 -10 -8 7 115.01 13.56 -10 8 -7 141.82 16.19 -10 8 7 144.46 13.15 10 8 7 149.07 11.01 10 8 -7 127.60 14.19 10 -8 -7 141.80 18.65 10 -8 7 144.34 10.94 -10 -8 8 134.69 13.66 -10 8 -8 168.24 11.97 -10 8 8 154.59 10.63 10 8 8 176.10 14.76 10 8 -8 162.96 16.75 10 -8 -8 156.82 11.05 10 -8 8 172.34 11.71 -10 8 -9 76.25 8.86 -10 8 9 95.19 11.09 10 8 9 98.87 9.25 10 8 -9 89.52 9.96 10 -8 -9 61.11 11.03 10 -8 9 72.73 12.90 -10 8 -10 99.76 15.23 -10 8 10 124.94 14.27 10 8 10 107.54 14.68 10 8 -10 111.85 13.92 10 -8 -10 113.54 11.22 10 -8 10 89.06 15.74 -10 8 -11 117.12 14.81 -10 8 11 108.78 12.19 10 8 11 105.53 13.78 10 8 -11 96.96 13.90 10 -8 -11 124.93 11.04 10 -8 11 94.37 8.97 -10 8 -12 16.72 4.29 -10 8 12 17.70 4.89 10 8 12 8.10 3.35 10 8 -12 15.04 4.42 -10 8 -13 13.19 3.68 -10 8 13 14.02 4.66 10 8 13 32.62 8.37 10 8 -13 15.92 4.98 10 -8 -13 30.84 8.22 -10 8 14 3.81 2.19 10 8 14 -0.81 2.65 10 8 -14 1.57 1.76 10 -8 -14 4.71 3.09 10 -8 14 0.14 2.85 -10 8 15 3.98 1.79 10 8 15 6.32 3.81 10 8 -15 7.77 2.72 10 -8 15 10.62 4.64 -10 9 0 6.85 2.99 10 9 0 2.58 2.41 10 -9 0 1.60 3.94 -10 -9 0 5.71 1.89 -10 9 -1 313.51 17.48 -10 9 1 320.83 20.03 10 9 1 312.03 23.62 10 -9 -1 327.16 18.34 10 -9 1 319.31 18.30 -10 -9 -1 297.23 15.29 -10 -9 1 306.96 16.51 -10 9 -2 28.35 7.57 -10 9 2 29.62 6.63 10 9 2 29.77 6.90 10 -9 -2 17.31 4.45 10 -9 2 19.96 4.60 -10 -9 2 16.92 3.95 -10 9 -3 349.09 19.08 -10 9 3 375.88 20.92 10 9 3 330.30 18.49 10 -9 -3 356.57 19.89 10 -9 3 354.28 19.78 -10 -9 3 356.42 18.85 -10 9 -4 72.08 10.09 -10 9 4 68.36 8.11 10 9 4 67.38 7.79 10 -9 -4 83.83 9.13 10 -9 4 73.20 8.30 -10 -9 4 71.88 7.62 -10 9 -5 64.49 7.17 -10 9 5 57.14 9.11 10 9 5 53.23 8.63 10 9 -5 51.79 7.12 10 -9 -5 67.98 8.37 10 -9 5 53.68 7.72 -10 -9 5 51.65 5.46 -10 9 -6 4.30 2.71 -10 9 6 1.95 2.49 10 9 -6 1.78 1.92 10 9 -6 -0.57 1.46 10 -9 -6 4.69 2.91 10 -9 6 18.02 6.18 -10 9 -7 1.45 1.77 -10 9 7 -0.80 2.59 10 9 7 12.15 4.37 10 9 -7 3.81 1.90 10 9 -7 2.45 1.36 10 -9 -7 7.29 2.85 10 -9 7 -1.31 3.42 -10 9 -8 4.06 1.98 -10 9 8 7.81 4.32 10 9 8 26.52 5.88 10 9 -8 6.37 1.99 10 9 -8 5.91 1.98 10 -9 -8 14.18 4.59 10 -9 8 18.97 5.11 -10 9 -9 19.50 4.01 -10 9 9 20.81 5.07 10 9 9 18.72 4.90 10 9 -9 17.08 3.51 10 -9 -9 10.77 3.88 10 -9 9 7.93 2.90 -10 9 -10 18.85 5.05 -10 9 10 19.52 5.93 10 9 10 9.16 4.32 10 9 -10 22.57 6.35 10 -9 -10 17.22 5.73 10 -9 10 20.48 6.62 -10 9 -11 23.95 5.59 -10 9 11 29.06 7.68 10 9 11 24.81 6.50 10 9 -11 24.84 5.78 10 -9 11 15.51 5.01 -10 9 -12 19.34 5.01 10 9 12 12.82 4.30 10 9 -12 24.95 6.58 10 -9 -12 37.42 7.93 10 -9 12 12.15 4.11 -10 9 13 5.24 2.52 10 9 13 10.18 4.66 10 9 -13 3.79 2.45 10 -9 -13 3.87 3.04 10 -9 13 6.24 2.67 -10 9 14 49.22 11.47 10 9 14 45.92 10.42 10 9 -14 41.10 11.38 10 -9 -14 23.11 5.56 10 -9 14 26.14 6.00 -10 9 15 7.65 4.19 10 9 15 3.31 2.52 10 9 -15 6.92 2.35 10 -9 -15 7.54 3.20 10 -9 15 10.47 5.80 -10 10 0 4.29 3.95 10 10 0 2.29 2.39 10 -10 0 7.54 3.98 -10 -10 0 0.76 0.77 -10 10 -1 88.93 13.62 -10 10 1 84.96 12.73 10 10 1 74.00 8.12 10 10 -1 89.75 9.71 10 -10 -1 64.13 7.94 10 -10 1 93.06 8.15 -10 -10 1 77.32 12.19 -10 10 -2 6.40 2.76 10 10 2 4.17 2.63 10 10 -2 5.62 2.31 10 -10 -2 3.51 3.39 10 -10 2 7.89 4.04 -10 -10 2 1.38 1.66 -10 10 -3 113.48 11.27 -10 10 3 123.37 11.80 10 10 3 88.31 9.79 10 10 -3 111.50 7.48 10 -10 -3 99.44 9.43 10 -10 3 126.86 9.98 -10 -10 3 106.37 6.81 -10 10 -4 7.08 2.22 -10 10 4 22.00 6.19 10 10 4 14.33 5.53 10 10 -4 9.59 3.33 10 -10 -4 18.70 6.06 10 -10 4 15.57 5.80 -10 -10 4 3.14 1.48 -10 10 -5 47.92 6.78 -10 10 5 91.75 7.28 10 10 5 43.83 9.64 10 10 -5 71.24 9.00 10 -10 -5 56.89 8.26 10 -10 5 95.80 8.14 -10 -10 5 56.38 7.55 -10 10 -6 58.87 8.74 -10 10 6 87.21 11.25 10 10 -6 66.53 7.76 10 10 6 76.96 8.02 10 -10 -6 60.39 7.86 10 -10 6 79.52 8.01 -10 -10 6 62.41 5.85 -10 10 -7 148.89 15.20 -10 10 7 143.12 20.26 10 -10 -7 139.65 12.93 10 -10 7 143.60 18.08 -10 -10 7 158.27 13.30 -10 10 -8 9.43 3.70 -10 10 8 11.12 3.26 10 10 8 13.93 5.14 10 10 -8 12.80 3.65 10 -10 -8 9.36 2.85 10 -10 8 16.44 5.23 -10 -10 8 15.53 5.44 -10 10 -9 35.29 5.24 -10 10 9 38.24 5.66 10 10 9 33.15 6.96 10 -10 -9 30.30 8.01 10 -10 9 31.59 9.03 -10 -10 9 41.43 4.84 -10 10 -10 21.39 4.77 -10 10 10 13.62 5.03 10 10 10 20.75 5.08 10 -10 10 3.28 3.50 -10 10 -11 10.78 3.01 -10 10 11 37.29 6.97 10 10 11 18.25 5.24 10 -10 -11 22.28 6.15 10 -10 11 19.76 6.48 -10 10 -12 37.91 6.38 -10 10 12 39.30 6.23 10 10 12 43.91 6.50 10 -10 -12 55.60 8.37 10 -10 12 45.78 6.64 -10 10 13 6.54 2.98 10 10 13 6.34 2.73 10 -10 -13 3.62 2.85 10 -10 13 11.32 5.41 -10 10 14 7.86 4.04 10 10 14 8.57 3.12 10 -10 -14 0.47 2.66 10 -10 14 2.89 3.22 -10 11 0 3.31 2.52 10 11 0 4.46 2.19 10 -11 0 2.79 3.70 -10 11 -1 85.85 8.70 -10 11 1 120.03 11.59 10 11 -1 86.88 7.41 10 11 1 86.78 9.33 10 -11 -1 90.30 8.99 10 -11 1 106.39 8.34 -10 -11 1 96.09 7.42 -10 11 -2 8.24 3.13 -10 11 2 20.87 5.50 10 11 -2 29.15 5.32 10 11 2 14.87 4.59 10 -11 -2 11.49 5.02 10 -11 2 16.59 4.67 -10 -11 2 9.99 2.54 -10 11 -3 31.52 7.56 -10 11 3 56.86 11.60 10 11 -3 26.33 4.99 10 11 3 25.86 5.54 10 -11 -3 20.84 5.33 10 -11 3 39.16 8.83 -10 -11 3 19.74 4.50 -10 11 -4 16.09 4.08 -10 11 4 10.64 4.19 10 11 -4 14.23 4.00 10 11 4 17.19 4.96 10 -11 -4 18.05 5.37 10 -11 4 8.85 3.62 -10 -11 4 16.27 3.97 -10 11 -5 31.22 6.60 -10 11 5 28.64 6.11 10 11 -5 22.63 4.50 10 11 5 35.29 7.53 10 -11 5 30.70 6.31 -10 -11 5 19.80 3.81 -10 11 -6 4.46 2.36 -10 11 6 10.92 3.58 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12 -1 8.82 3.96 10 12 1 4.26 3.30 10 -12 -1 10.18 5.20 10 -12 1 6.82 5.88 -10 12 -2 12.24 3.90 -10 12 2 9.34 4.48 10 12 2 15.48 5.48 10 -12 -2 3.61 4.27 10 -12 2 20.80 6.47 -10 -12 2 14.54 4.00 -10 12 -3 18.71 4.32 -10 12 3 27.76 6.56 10 12 3 19.66 4.34 10 12 -3 21.26 4.20 10 -12 -3 22.22 5.26 10 -12 3 18.86 4.62 -10 -12 3 20.67 4.09 -10 12 -4 19.35 5.54 -10 12 4 52.44 6.38 10 12 4 19.45 5.47 10 12 -4 30.05 7.71 10 -12 -4 22.50 6.48 10 -12 4 21.26 6.34 -10 -12 4 25.31 6.35 -10 12 -5 98.45 11.13 -10 12 5 91.19 14.12 10 12 -5 86.53 6.99 10 12 5 88.85 8.31 10 -12 -5 78.66 12.03 10 -12 5 88.99 7.98 -10 -12 5 81.24 6.99 -10 12 -6 4.79 2.77 -10 12 6 7.82 4.06 10 12 -6 2.77 1.47 10 12 6 4.50 2.71 10 -12 -6 1.98 2.05 -10 -12 6 3.31 2.59 -10 12 -7 22.40 6.19 -10 12 7 20.73 5.49 10 12 7 17.25 5.95 10 -12 7 23.87 6.72 -10 -12 7 26.46 5.65 -10 12 -8 2.17 1.02 -10 12 8 4.26 1.63 10 -12 -8 9.84 3.01 10 -12 8 -0.18 3.49 -10 -12 8 3.20 2.19 -10 12 -9 8.61 3.01 -10 12 9 3.30 1.79 10 12 9 2.50 2.79 10 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12.38 3.97 -10 13 -6 -0.42 1.78 -10 13 6 3.25 2.95 10 13 -6 1.81 0.74 10 13 6 6.26 2.84 10 -13 6 0.83 3.52 -10 -13 6 5.01 3.25 -10 13 -7 22.09 6.88 -10 13 7 20.06 6.54 10 13 7 4.38 2.92 10 -13 -7 18.13 5.95 10 -13 7 19.32 6.46 -10 -13 7 21.90 5.95 -10 13 -8 14.98 4.81 -10 13 8 13.86 4.21 10 13 8 14.74 5.36 10 -13 -8 14.59 5.80 10 -13 8 23.80 7.41 -10 13 -9 16.49 5.80 -10 13 9 13.62 5.22 10 13 9 15.76 5.56 10 -13 -9 14.10 4.19 10 -13 9 18.11 5.42 -10 -13 9 17.11 4.94 -10 13 -10 29.92 7.37 -10 13 10 41.00 9.19 10 13 10 40.82 10.79 10 -13 -10 30.59 7.06 10 -13 10 68.89 13.91 -10 -13 10 47.81 9.58 -10 13 11 8.40 3.37 10 13 11 4.05 3.27 10 -13 -11 9.46 3.99 10 -13 11 4.33 3.36 -10 -13 11 0.83 2.13 -10 14 0 169.97 41.59 10 14 0 113.51 17.12 10 -14 0 115.73 18.87 -10 14 -1 2.47 1.88 10 14 -1 6.90 3.25 10 14 1 2.77 2.38 10 -14 -1 13.68 5.55 -10 14 -2 89.11 14.07 -10 14 2 103.37 17.45 10 14 -2 79.30 16.02 10 14 2 66.35 12.83 10 -14 -2 59.64 9.99 10 -14 2 118.63 19.03 -10 14 -3 17.59 5.02 -10 14 3 17.70 5.16 10 14 -3 12.35 4.26 10 14 3 20.53 5.48 10 -14 -3 12.78 3.94 10 -14 3 20.42 6.60 -10 14 -4 6.90 3.44 -10 14 4 8.67 3.20 10 14 -4 9.90 3.33 10 14 4 -0.36 2.50 10 -14 -4 -0.39 2.97 10 -14 4 9.42 4.47 -10 14 5 15.88 5.07 10 14 -5 7.43 2.62 10 14 5 21.27 6.59 10 -14 5 7.38 3.32 -10 14 -6 3.89 2.06 -10 14 6 3.13 2.94 10 14 6 4.77 2.96 10 -14 -6 8.05 4.85 10 -14 6 6.46 3.61 -10 -14 6 4.24 2.01 -10 14 -7 16.94 5.01 -10 14 7 9.28 3.64 10 14 7 14.08 4.93 10 -14 -7 18.52 6.13 10 -14 7 7.23 3.86 -10 -14 7 14.71 4.21 -10 14 -8 16.19 5.00 -10 14 8 16.41 6.06 10 14 8 14.76 5.43 10 -14 8 9.40 4.12 -10 -14 8 15.60 4.84 -10 14 -9 4.59 1.92 -10 14 9 -0.51 2.76 10 14 9 5.71 3.23 10 -14 -9 9.08 3.37 10 -14 9 1.72 3.31 -10 -14 9 6.73 2.59 -10 15 0 4.81 2.76 10 15 0 4.56 2.70 10 -15 0 12.23 6.66 -10 15 -1 31.38 8.21 -10 15 1 36.52 6.90 10 15 1 31.79 6.02 10 15 -1 30.33 5.67 10 -15 -1 24.72 6.21 10 -15 1 19.45 6.46 -10 15 -2 1.55 2.06 -10 15 2 5.97 3.08 10 15 -2 6.12 2.82 10 15 2 2.38 2.84 10 -15 -2 7.18 3.73 10 -15 2 5.25 3.62 -10 15 -3 10.41 3.16 -10 15 3 14.28 8.84 10 15 -3 11.80 3.95 10 15 3 15.49 4.84 10 -15 3 7.77 3.66 -10 15 -4 19.29 5.86 -10 15 4 18.85 5.46 10 15 -4 8.18 3.06 10 15 4 14.14 4.83 10 -15 4 5.98 3.56 -10 15 -5 3.00 2.01 10 15 5 -2.11 2.88 10 -15 -5 8.62 4.19 10 -15 5 5.74 3.13 -10 15 -6 9.72 3.60 -10 15 6 8.33 3.73 10 15 6 17.23 6.01 10 -15 6 8.37 3.75 -10 15 -7 13.52 4.49 -10 15 7 2.09 1.98 10 15 7 6.78 3.00 10 -15 -7 9.07 4.33 10 -15 7 15.36 5.78 -10 16 0 84.22 20.46 10 16 0 67.14 15.59 10 -16 0 74.02 15.23 -10 16 -1 7.37 3.55 -10 16 1 2.03 2.71 10 16 -1 8.05 3.80 10 16 1 2.10 1.86 10 -16 -1 9.79 4.25 10 -16 1 8.96 4.15 -10 16 -2 57.62 14.20 -10 16 2 49.73 12.32 10 16 -2 35.06 10.32 10 16 2 46.26 11.55 10 -16 2 29.93 8.58 -10 16 -3 5.41 2.15 -10 16 3 6.17 2.83 10 16 -3 3.15 1.90 10 16 3 1.44 2.52 10 -16 -3 12.37 6.49 10 -16 3 12.60 5.78 -10 16 -4 7.65 3.45 -10 16 4 3.85 1.64 10 16 4 -0.80 2.55 10 -16 -4 3.12 3.18 10 -16 4 11.81 4.52 -11 0 0 8.37 3.34 11 0 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13.36 -11 -7 7 95.27 11.28 -11 7 -7 116.64 7.83 -11 7 7 117.43 16.43 11 7 -7 134.53 15.76 11 -7 -7 127.10 9.94 11 -7 7 131.49 9.53 -11 -7 8 15.31 4.11 -11 7 -8 20.59 4.81 -11 7 8 33.88 7.27 11 7 -8 29.05 5.61 11 -7 -8 10.94 3.86 11 -7 8 33.54 7.37 -11 -7 9 25.54 5.40 -11 7 -9 44.18 8.88 -11 7 9 44.30 9.12 11 7 9 36.47 8.47 11 7 -9 36.61 7.53 11 -7 -9 32.85 7.08 11 -7 9 37.86 7.59 -11 7 -10 6.94 2.01 -11 7 10 10.61 3.46 11 7 10 5.19 2.84 11 7 -10 7.75 2.29 11 -7 -10 11.69 4.04 11 -7 10 8.42 3.52 -11 7 -11 6.42 2.15 -11 7 11 12.02 4.72 11 7 11 3.05 2.53 11 7 -11 5.09 2.55 11 -7 -11 12.62 5.15 11 -7 11 8.39 3.05 -11 7 -12 5.94 1.85 -11 7 12 7.66 3.40 11 7 12 8.76 4.35 11 7 -12 9.40 2.74 11 -7 -12 4.72 2.97 11 -7 12 4.77 1.88 -11 7 -13 0.00 1.46 -11 7 13 8.48 2.62 11 7 13 6.68 2.86 11 7 -13 7.23 2.78 11 -7 -13 3.88 3.07 11 -7 13 5.18 4.02 -11 7 -14 -1.28 1.40 -11 7 14 6.44 2.92 11 7 14 -0.37 2.38 11 7 -14 5.73 2.98 11 -7 -14 -2.19 2.89 11 -7 14 6.94 3.67 -11 7 15 4.66 2.20 11 7 15 6.04 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66.59 6.72 -11 -8 7 11.87 3.45 -11 8 -7 10.28 3.25 -11 8 7 10.61 3.53 11 8 7 7.55 3.96 11 8 -7 11.06 2.85 11 -8 -7 15.00 5.38 11 -8 7 8.51 3.62 -11 -8 8 3.91 1.92 -11 8 -8 17.89 4.10 -11 8 8 12.42 4.69 11 8 8 9.73 4.27 11 8 -8 7.42 2.38 11 -8 -8 10.67 4.44 11 -8 8 13.18 4.45 -11 8 -9 34.76 5.91 -11 8 9 44.40 10.20 11 8 9 18.70 6.30 11 8 -9 45.55 6.28 11 -8 -9 27.71 5.59 11 -8 9 41.80 7.74 -11 8 -10 20.80 5.23 -11 8 10 43.31 7.51 11 8 10 10.01 3.81 11 8 -10 20.80 5.82 11 -8 -10 13.51 5.59 11 -8 10 12.51 4.84 -11 8 -11 -0.66 1.50 -11 8 11 3.32 2.36 11 8 11 11.11 3.87 11 8 -11 4.09 2.59 11 -8 -11 2.63 3.17 11 -8 11 4.32 2.33 -11 8 -12 15.66 4.35 -11 8 12 28.79 5.83 11 8 12 34.48 6.90 11 8 -12 29.93 6.05 11 -8 -12 12.89 4.12 11 -8 12 27.15 4.72 -11 8 -13 10.75 3.33 -11 8 13 9.37 3.98 11 8 13 15.03 5.12 11 8 -13 15.02 4.96 11 -8 -13 13.12 5.20 11 -8 13 13.74 5.02 -11 8 14 51.74 11.48 11 8 14 51.67 11.50 11 8 -14 47.68 12.96 11 -8 14 48.09 9.64 -11 -9 0 3.44 2.48 -11 9 0 12.26 4.42 11 -9 0 15.70 4.93 -11 -9 1 5.93 2.05 -11 -9 -1 4.90 1.96 -11 9 -1 11.75 4.99 11 -9 -1 9.11 4.66 11 -9 1 4.17 3.31 -11 -9 1 1.00 0.89 -11 -9 2 51.15 8.83 -11 9 -2 60.73 10.11 -11 9 2 70.67 10.54 11 -9 -2 51.59 7.60 11 -9 2 60.81 9.04 -11 -9 2 58.30 7.38 -11 -9 3 48.57 8.38 -11 9 -3 44.18 8.17 -11 9 3 32.23 5.46 11 9 3 64.88 15.19 11 -9 -3 62.63 9.76 11 -9 3 53.70 9.15 -11 -9 3 52.58 6.90 -11 -9 4 114.38 12.04 -11 9 -4 111.28 15.69 -11 9 4 130.28 17.21 11 9 4 142.05 16.20 11 -9 -4 108.56 11.42 11 -9 4 141.75 9.96 -11 -9 4 139.49 10.12 -11 -9 5 67.09 8.46 -11 9 -5 94.32 11.42 -11 9 5 86.63 11.28 11 9 5 95.52 8.91 11 -9 -5 109.92 10.70 11 -9 5 79.12 11.03 -11 -9 6 80.47 10.45 -11 9 -6 97.22 8.56 -11 9 6 88.10 8.75 11 9 -6 99.39 10.84 11 -9 -6 72.27 17.05 11 -9 6 107.96 10.48 -11 9 -7 8.51 3.18 -11 9 7 6.60 2.44 11 9 7 8.58 4.51 11 9 -7 5.60 1.65 11 -9 -7 7.86 4.74 11 -9 7 4.87 2.82 -11 9 -8 86.84 9.44 -11 9 8 66.22 7.44 11 9 8 85.37 11.40 11 9 -8 65.28 7.48 11 9 -8 72.44 9.54 11 -9 -8 68.54 12.77 11 -9 8 68.68 11.98 -11 9 -9 26.50 6.82 -11 9 9 24.94 6.75 11 9 9 18.17 5.44 11 9 -9 24.07 6.57 11 -9 -9 13.00 4.63 11 -9 9 15.35 5.69 -11 9 -10 39.61 7.54 -11 9 10 27.04 7.58 11 9 10 34.25 7.47 11 9 -10 41.30 7.58 11 -9 -10 34.13 7.96 11 -9 10 17.69 5.21 -11 9 11 7.37 2.92 11 9 11 17.58 5.32 11 9 -11 12.30 3.54 11 -9 11 15.36 4.62 -11 9 -12 36.49 6.83 -11 9 12 16.57 4.92 11 9 12 26.85 6.09 11 9 -12 33.64 6.82 11 -9 -12 37.01 7.13 11 -9 12 24.15 5.04 -11 9 13 8.06 3.08 11 9 13 8.48 3.67 11 9 -13 13.14 4.68 11 -9 13 5.68 3.32 -11 9 14 23.56 6.44 11 9 14 15.97 5.42 11 9 -14 19.61 5.76 11 -9 -14 6.87 3.56 11 -9 14 10.26 4.96 -11 10 0 125.88 14.70 11 10 0 106.87 7.71 11 -10 0 88.29 7.69 -11 10 -1 197.95 19.66 -11 10 1 218.72 21.89 11 10 -1 219.87 13.32 11 10 1 187.76 17.02 11 -10 -1 201.86 12.67 11 -10 1 223.29 14.63 -11 10 -2 74.59 9.04 -11 10 2 74.09 7.73 11 10 -2 62.20 6.40 11 10 2 75.26 10.59 11 -10 -2 64.49 7.34 11 -10 2 66.47 7.21 -11 -10 2 55.68 10.45 -11 10 -3 43.79 10.74 -11 10 3 70.22 10.97 11 10 3 45.69 8.51 11 10 -3 52.60 8.92 11 -10 -3 42.71 8.53 11 -10 3 55.92 10.72 -11 -10 3 40.54 6.83 -11 10 -4 53.59 9.52 -11 10 4 49.54 9.24 11 10 4 22.65 6.24 11 10 -4 39.58 7.37 11 -10 4 31.85 7.27 -11 -10 4 40.59 7.96 -11 10 -5 7.82 2.48 -11 10 5 10.51 3.52 11 10 5 17.52 4.06 11 10 -5 16.89 3.93 11 -10 -5 12.46 4.03 11 -10 5 22.13 6.85 -11 -10 5 10.59 3.26 -11 10 -6 -1.64 1.83 -11 10 6 6.82 2.96 11 10 6 3.64 2.88 11 10 -6 3.23 1.15 11 -10 -6 14.28 5.34 11 -10 6 8.42 3.97 -11 -10 6 1.24 1.84 -11 10 -7 19.67 5.80 -11 10 7 17.72 5.16 11 10 7 3.92 2.66 11 10 -7 13.93 4.34 11 -10 -7 12.95 5.27 11 -10 7 12.25 5.44 -11 -10 7 18.83 5.13 -11 10 -8 0.46 1.98 -11 10 8 6.47 3.11 11 10 8 6.47 4.62 11 -10 -8 1.75 2.89 11 -10 8 -1.70 2.83 -11 -10 8 4.75 2.34 -11 10 -9 3.27 2.26 -11 10 9 2.92 2.14 11 10 9 11.28 4.77 11 -10 -9 2.12 3.10 11 -10 9 1.66 2.82 -11 10 10 8.41 4.09 11 10 10 3.07 2.93 11 -10 -10 9.76 4.67 11 -10 10 10.42 4.80 -11 10 -11 6.45 2.17 -11 10 11 3.79 2.69 11 10 11 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33.02 8.06 11 11 6 38.91 8.09 11 -11 -6 26.62 7.00 -11 -11 6 37.37 7.03 -11 11 -7 7.36 2.47 -11 11 7 4.67 1.95 11 11 7 7.34 3.27 11 11 -7 2.78 1.37 11 -11 -7 13.65 5.44 11 -11 7 12.86 5.85 -11 -11 7 6.20 3.52 -11 11 -8 24.33 5.93 -11 11 8 16.90 5.73 11 11 8 26.76 7.30 11 -11 -8 15.82 5.56 11 -11 8 9.92 3.99 -11 -11 8 26.29 6.33 -11 11 -9 3.12 1.54 -11 11 9 21.52 6.30 11 11 9 8.46 3.52 11 -11 -9 20.88 6.40 11 -11 9 15.18 4.79 -11 -11 9 18.59 5.40 -11 11 -10 52.47 8.20 -11 11 10 45.88 11.13 11 11 10 73.36 12.23 -11 -11 10 62.24 12.53 -11 11 -11 12.28 3.99 -11 11 11 17.70 5.23 11 11 11 10.44 3.95 11 -11 -11 14.45 5.59 11 -11 11 21.11 6.12 -11 -11 11 13.33 4.65 -11 11 12 7.10 2.43 11 11 12 9.97 4.80 11 -11 -12 6.84 4.62 11 -11 12 3.69 3.36 -11 -11 12 10.16 4.28 -11 12 0 14.64 4.76 11 12 0 10.09 4.41 11 -12 0 7.38 3.26 -11 12 -1 51.08 6.16 -11 12 1 75.70 8.38 11 12 1 46.80 5.93 11 12 -1 56.11 6.76 11 -12 -1 49.58 7.60 11 -12 1 53.65 5.74 -11 12 -2 12.46 4.73 -11 12 2 2.64 1.70 11 12 -2 2.50 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10.03 -12 -7 -5 51.99 8.27 -12 -7 5 46.35 6.61 -12 7 -5 51.97 9.00 -12 7 5 54.51 8.08 12 7 -5 47.54 8.07 12 -7 -5 43.07 9.78 12 -7 5 58.77 8.78 -12 -7 -6 90.93 10.81 -12 -7 6 55.68 11.14 -12 7 -6 80.47 9.08 -12 7 6 73.87 9.30 12 7 -6 72.04 10.39 12 -7 -6 79.25 9.42 12 -7 6 76.82 8.94 -12 -7 -7 32.12 7.28 -12 -7 7 27.81 6.04 -12 7 -7 45.55 8.06 -12 7 7 45.14 9.07 12 7 -7 46.81 8.80 12 -7 -7 22.51 6.19 12 -7 7 34.62 6.37 -12 -7 -8 27.59 5.95 -12 -7 8 16.04 4.98 -12 7 -8 20.92 4.11 -12 7 8 30.29 7.34 12 7 -8 21.27 4.21 12 -7 -8 15.75 5.27 12 -7 8 25.42 5.27 -12 -7 9 15.47 4.84 -12 7 -9 29.10 7.67 -12 7 9 38.31 6.97 12 7 9 27.27 7.75 12 7 -9 39.27 5.49 12 -7 -9 23.21 6.75 12 -7 9 31.33 8.09 -12 7 -10 30.99 6.86 -12 7 10 36.89 8.50 12 7 10 33.78 7.65 12 7 -10 35.50 8.84 12 -7 -10 31.04 8.03 12 -7 10 30.06 7.09 -12 7 -11 21.58 5.63 -12 7 11 19.79 5.19 12 7 11 29.68 7.80 12 7 -11 22.47 5.45 12 -7 -11 20.50 6.01 12 -7 11 22.69 6.25 -12 7 -12 7.24 2.19 -12 7 12 25.83 4.73 12 7 12 13.52 4.96 12 7 -12 16.42 5.08 12 -7 -12 14.80 5.46 12 -7 12 7.22 2.72 -12 7 -13 10.28 3.33 -12 7 13 13.61 4.50 12 7 13 5.42 2.11 12 7 -13 4.54 2.63 12 -7 -13 6.41 3.58 12 -7 13 7.31 3.83 -12 7 14 3.91 3.02 12 7 14 3.73 2.69 12 7 -14 2.26 1.99 12 -7 -14 3.77 3.16 12 -7 14 2.02 2.23 -12 -8 0 30.74 5.25 -12 8 0 39.27 7.97 12 -8 0 39.87 6.79 -12 -8 -1 11.73 3.71 -12 -8 1 7.55 2.33 -12 8 -1 14.82 4.73 -12 8 1 15.81 4.51 12 -8 -1 11.24 4.67 12 -8 1 4.90 3.00 -12 -8 1 7.08 1.81 -12 -8 -2 3.24 2.17 -12 -8 2 1.25 1.04 -12 8 -2 0.01 2.54 -12 8 2 3.75 2.85 12 -8 -2 11.66 4.93 12 -8 2 12.34 4.82 -12 -8 -3 7.83 3.08 -12 -8 3 5.76 1.87 -12 8 -3 5.62 1.54 -12 8 3 2.24 2.54 12 8 -3 6.65 1.97 12 -8 -3 8.17 3.04 12 -8 3 7.01 2.79 -12 -8 -4 3.65 2.41 -12 -8 4 1.51 1.01 -12 8 -4 7.21 2.44 -12 8 4 6.41 1.93 12 8 -4 4.72 1.87 12 -8 -4 1.34 3.25 12 -8 4 4.22 3.19 -12 -8 -5 39.59 8.10 -12 -8 5 21.02 5.18 -12 8 -5 24.03 5.76 -12 8 5 26.79 6.54 12 8 -5 30.78 5.77 12 -8 -5 29.76 6.68 12 -8 5 25.02 5.67 -12 -8 -6 6.10 1.77 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8 21.54 6.13 -12 9 -9 8.06 2.61 -12 9 9 7.48 2.95 12 9 9 4.81 3.13 12 9 -9 10.58 3.23 12 -9 -9 5.93 3.47 12 -9 9 3.26 2.66 -12 9 -10 10.83 3.70 -12 9 10 15.74 4.89 12 9 10 12.50 4.75 12 9 -10 7.35 2.83 12 -9 -10 9.32 3.86 12 -9 10 9.56 4.34 -12 9 -11 14.18 3.95 -12 9 11 9.01 4.07 12 9 11 18.31 6.22 12 9 -11 7.41 2.85 12 -9 -11 13.57 5.45 12 -9 11 7.15 4.75 -12 9 -12 31.77 8.88 -12 9 12 33.09 9.77 12 9 12 52.96 11.24 12 9 -12 38.31 10.67 12 -9 -12 31.43 7.46 12 -9 12 31.95 7.06 -12 9 13 6.76 3.21 12 9 13 3.04 3.69 12 9 -13 0.74 0.85 12 -9 -13 5.04 3.38 12 -9 13 8.94 4.69 -12 10 0 -1.71 2.45 12 10 0 5.54 2.48 12 -10 0 1.90 3.98 -12 10 -1 5.04 2.30 -12 10 1 14.81 5.09 12 10 1 13.83 5.07 12 10 -1 4.97 1.69 12 -10 -1 11.65 5.08 12 -10 1 8.56 4.44 -12 10 -2 40.76 7.20 -12 10 2 30.03 6.15 12 10 2 37.60 7.08 12 10 -2 45.82 6.51 12 -10 -2 27.49 6.08 12 -10 2 49.63 7.78 -12 10 -3 26.01 6.17 -12 10 3 28.24 6.47 12 10 3 23.00 5.51 12 10 -3 29.48 5.99 12 -10 -3 29.37 5.68 12 -10 3 23.92 5.29 -12 10 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3.37 3.28 -12 -11 7 7.70 2.66 -12 11 -8 4.63 2.15 -12 11 8 4.05 1.93 12 11 8 3.23 2.98 12 -11 -8 6.19 3.30 12 -11 8 11.03 5.93 -12 -11 8 8.53 3.91 -12 11 -9 4.12 2.61 -12 11 9 3.86 2.13 12 11 9 10.53 5.65 12 -11 -9 6.34 3.04 12 -11 9 7.75 4.26 -12 -11 9 11.00 3.67 -12 11 -10 6.55 3.13 -12 11 10 6.71 4.21 12 11 10 16.81 5.15 12 -11 -10 12.91 5.75 12 -11 10 11.26 4.07 -12 -11 10 5.82 2.70 -12 11 -11 8.11 2.97 -12 11 11 7.94 3.98 12 11 11 27.50 7.85 12 -11 -11 12.37 6.02 12 -11 11 5.91 3.07 -12 -11 11 8.29 3.08 -12 12 0 49.87 8.34 12 12 0 48.53 8.92 12 -12 0 48.42 11.08 -12 12 -1 8.18 3.20 -12 12 1 16.86 5.21 12 12 -1 5.19 2.37 12 12 1 10.39 3.70 12 -12 -1 16.25 5.95 12 -12 1 4.41 3.43 -12 12 -2 35.50 7.25 -12 12 2 21.88 6.16 12 12 2 31.06 8.54 12 12 -2 16.33 4.76 12 -12 -2 28.90 7.53 12 -12 2 25.77 7.19 -12 12 -3 27.42 6.56 -12 12 3 31.65 7.47 12 12 3 23.63 6.05 12 12 -3 31.17 7.40 12 -12 -3 23.53 6.57 12 -12 3 26.23 7.28 -12 12 -4 13.97 4.97 -12 12 4 14.52 4.27 12 12 -4 14.39 4.23 12 12 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10.14 3.29 -17 8 -3 17.54 5.11 -17 8 3 8.13 3.49 17 -8 -3 25.81 7.39 17 -8 3 2.39 2.40 -18 0 0 39.27 8.14 -18 0 -1 23.71 5.25 -18 0 1 31.64 6.44 -18 0 -2 36.78 7.02 -18 0 2 28.71 8.39 -18 0 -3 17.07 4.27 -18 0 3 18.35 4.92 -18 0 -4 5.33 2.62 -18 0 4 3.45 3.25 18 0 -4 1.31 1.00 -18 0 -5 3.79 2.53 -18 0 5 -1.73 2.16 18 0 -5 4.50 1.99 -18 0 -6 3.93 1.73 -18 0 6 6.57 2.78 18 0 -6 8.91 2.98 -18 -1 0 10.86 4.76 -18 1 0 19.97 4.31 -18 -1 1 10.60 3.50 -18 -1 -1 4.00 1.97 -18 1 -1 2.17 1.81 -18 1 1 7.17 3.15 -18 -1 -2 21.07 4.89 -18 1 -2 7.52 3.24 -18 1 2 12.95 4.39 -18 -1 -3 6.65 2.99 -18 -1 3 15.89 6.20 -18 1 -3 10.97 4.31 -18 1 3 12.36 4.34 18 -1 -3 7.06 2.86 -18 -1 -4 14.19 4.10 -18 1 -4 20.91 5.30 -18 -1 4 14.57 5.20 -18 1 4 24.05 6.54 18 -1 -4 4.08 2.02 -18 -1 -5 10.64 4.64 -18 1 -5 21.61 5.68 -18 -1 5 12.09 4.42 -18 1 5 6.26 2.38 18 -1 -5 14.97 4.79 -18 -1 -6 8.69 3.05 -18 1 -6 8.90 3.70 -18 -1 6 11.12 4.24 -18 1 6 15.62 5.36 18 1 -6 4.14 1.75 18 -1 -6 11.97 4.24 -18 -2 0 21.52 6.26 -18 2 0 15.76 5.15 -18 -2 -1 12.65 4.23 -18 -2 1 13.55 4.19 -18 2 -1 15.55 4.66 -18 2 1 3.94 2.35 18 -2 -1 6.64 2.68 -18 -2 -2 8.55 3.85 -18 -2 2 22.46 6.06 -18 2 -2 9.81 4.96 -18 2 2 17.68 4.18 18 -2 -2 5.98 2.36 -18 -2 -3 4.66 2.03 -18 -2 3 6.72 2.63 -18 2 -3 6.23 2.07 -18 2 3 7.80 3.56 18 -2 -3 10.65 3.78 -18 -2 -4 35.94 9.50 -18 -2 4 27.61 7.22 -18 2 -4 23.83 6.44 -18 2 4 28.71 7.40 18 -2 -4 12.87 4.14 -18 -2 -5 10.75 4.67 -18 2 -5 8.03 3.35 -18 -2 5 9.10 3.70 -18 2 5 3.23 1.60 18 -2 -5 1.67 1.91 -18 -2 -6 12.29 5.26 -18 2 -6 8.48 2.81 -18 -2 6 5.69 1.76 -18 2 6 5.33 2.57 18 -2 -6 1.84 1.99 -18 -3 0 12.03 3.74 -18 3 0 16.86 4.51 18 -3 0 3.17 2.43 -18 -3 -1 5.73 2.13 -18 -3 1 10.33 3.36 -18 3 -1 6.15 3.51 -18 3 1 11.68 4.34 18 -3 -1 2.29 1.81 -18 -3 -2 20.59 5.11 -18 -3 2 8.13 4.00 -18 3 -2 6.79 2.40 -18 3 2 13.47 4.49 18 -3 -2 2.68 1.81 -18 -3 -3 9.65 2.84 -18 -3 3 14.64 4.85 -18 3 -3 9.65 3.38 -18 3 3 7.43 3.46 18 -3 -3 6.58 3.02 -18 -3 -4 16.20 5.09 -18 -3 4 2.66 1.96 -18 3 4 7.15 2.69 18 -3 -4 1.25 2.07 -18 -3 -5 25.29 8.44 -18 -3 5 27.33 6.87 -18 3 -5 27.92 8.88 -18 3 5 13.19 5.67 18 -3 -5 14.19 4.71 -18 -4 0 8.99 3.94 -18 4 0 21.14 5.93 18 -4 0 3.71 2.22 -18 -4 1 13.09 4.48 -18 -4 -1 11.57 5.02 -18 4 -1 2.33 3.05 -18 4 1 2.55 2.73 18 -4 -1 6.83 3.10 18 -4 1 5.34 2.50 -18 -4 -2 3.79 1.82 -18 -4 2 -2.50 2.62 -18 4 -2 6.95 2.53 -18 4 2 6.05 2.33 18 -4 -2 1.92 2.02 -18 -4 -3 3.01 2.04 -18 -4 3 6.19 2.39 -18 4 -3 5.73 2.13 -18 4 3 5.17 3.70 18 -4 -3 6.30 3.72 -18 -4 -4 13.86 5.56 -18 -4 4 8.02 3.22 -18 4 -4 7.13 3.67 -18 4 4 10.50 4.35 18 -4 -4 7.26 2.93 -18 -4 -5 7.57 3.83 -18 -4 5 15.52 4.35 -18 4 -5 10.80 4.05 -18 4 5 20.74 6.82 18 -4 -5 3.04 1.80 -18 -5 0 -1.51 2.48 -18 5 0 8.69 3.67 18 -5 0 0.63 1.80 -18 -5 -1 6.12 2.13 -18 -5 1 12.32 4.75 -18 5 -1 6.69 3.14 -18 5 1 7.17 3.23 18 -5 -1 2.29 1.97 18 -5 1 4.31 2.10 -18 -5 -2 6.71 2.46 -18 -5 2 3.34 1.56 -18 5 -2 6.83 2.33 -18 5 2 5.48 3.35 18 -5 -2 3.43 2.21 18 -5 2 3.15 1.95 -18 -5 -3 10.96 4.14 -18 -5 3 18.87 6.23 -18 5 -3 19.25 6.35 -18 5 3 3.81 2.95 18 -5 -3 2.99 2.24 -18 -6 0 4.96 2.02 -18 6 0 6.71 4.05 18 -6 0 5.89 3.77 -18 -6 -1 8.72 3.95 -18 -6 1 5.15 3.81 -18 6 -1 6.53 2.79 -18 6 1 8.26 3.54 18 -6 -1 7.09 2.47 18 -6 1 5.13 3.15 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 97675 _shelx_SHELXL_version_number '2014/7' _olex2_submission_special_instructions 'No special instructions were received'