data_shelxl _audit_creation_method SHELXL-2013 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point 359(2) _chemical_formula_moiety 'C13 H21 N O6' _chemical_formula_sum 'C13 H21 N O6' _chemical_formula_weight 287.31 _chemical_absolute_configuration syn loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system 'Monoclinic' _space_group_IT_number 4 _space_group_name_H-M_alt 'P 21' _space_group_name_Hall 'P 2yb' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' _cell_length_a 6.4895(4) _cell_length_b 12.4868(12) _cell_length_c 10.0658(9) _cell_angle_alpha 90.00 _cell_angle_beta 106.939(5) _cell_angle_gamma 90.00 _cell_volume 780.28(11) _cell_formula_units_Z 2 _cell_measurement_temperature 173(2) _cell_measurement_reflns_used 426 _cell_measurement_theta_min ? _cell_measurement_theta_max ? _exptl_crystal_description prism _exptl_crystal_colour colourless _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_density_diffrn 1.223 _exptl_crystal_F_000 308 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.60 _exptl_crystal_size_mid 0.25 _exptl_crystal_size_min 0.20 _exptl_absorpt_coefficient_mu 0.097 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type none _exptl_absorpt_correction_T_min ? _exptl_absorpt_correction_T_max ? _exptl_absorpt_process_details ? _exptl_special_details ; ? ; _diffrn_ambient_temperature 173(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'normal-focus sealed tube' _diffrn_measurement_device_type 'Nonius Kappa CCD' _diffrn_measurement_method 'CCD' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 4898 _diffrn_reflns_av_unetI/netI 0.0874 _diffrn_reflns_av_R_equivalents 0.0418 _diffrn_reflns_limit_h_min -8 _diffrn_reflns_limit_h_max 8 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_l_min -13 _diffrn_reflns_limit_l_max 13 _diffrn_reflns_theta_min 3.723 _diffrn_reflns_theta_max 27.478 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.981 _diffrn_measured_fraction_theta_full 0.986 _diffrn_reflns_Laue_measured_fraction_max 0.981 _diffrn_reflns_Laue_measured_fraction_full 0.986 _diffrn_reflns_point_group_measured_fraction_max 0.852 _diffrn_reflns_point_group_measured_fraction_full 0.882 _reflns_number_total 3053 _reflns_number_gt 2427 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.658 _reflns_Friedel_fraction_max 0.709 _reflns_Friedel_fraction_full 0.767 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Nonius Kappa CCD' _computing_cell_refinement 'Denzo and Scalepak (1997)' _computing_data_reduction 'Denzo and Scalepak (1997)' _computing_structure_solution 'SIR 2004' _computing_structure_refinement 'SHELXL-2013 (Sheldrick, 2013)' _computing_molecular_graphics 'ORTEP III' _computing_publication_material 'SHELXL-2013 (Sheldrick, 2013)' _refine_special_details ; ? ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details ; w=1/[\s^2^(Fo^2^)+(0.0428P)^2^] where P=(Fo^2^+2Fc^2^)/3 ; _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 3053 _refine_ls_number_parameters 182 _refine_ls_number_restraints 1 _refine_ls_R_factor_all 0.0630 _refine_ls_R_factor_gt 0.0481 _refine_ls_wR_factor_ref 0.1196 _refine_ls_wR_factor_gt 0.1123 _refine_ls_goodness_of_fit_ref 0.993 _refine_ls_restrained_S_all 0.993 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.1289(3) 0.04358(19) -0.3489(2) 0.0379(5) Uani 1 1 d . . . . . O2 O 0.4377(3) 0.03133(17) 0.0459(2) 0.0353(5) Uani 1 1 d . . . . . O3 O 0.5029(4) 0.12036(16) -0.1316(2) 0.0408(6) Uani 1 1 d . . . . . O4 O 0.5827(3) -0.19692(18) -0.0055(2) 0.0379(5) Uani 1 1 d . . . . . H4 H 0.5592 -0.2602 0.0065 0.057 Uiso 1 1 calc R U . . . O5 O 0.1206(3) -0.0577(2) 0.0281(2) 0.0433(6) Uani 1 1 d . . . . . N1 N 0.4164(4) -0.0584(2) -0.1468(2) 0.0305(6) Uani 1 1 d . . . . . O6 O 0.2850(4) -0.0041(2) -0.5140(2) 0.0588(8) Uani 1 1 d . . . . . C2 C 0.3409(5) -0.0710(2) 0.0619(3) 0.0306(6) Uani 1 1 d . . . . . C3 C 0.2042(6) -0.2173(3) -0.1223(4) 0.0438(8) Uani 1 1 d . . . . . H3A H 0.0724 -0.1774 -0.1539 0.066 Uiso 1 1 calc R U . . . H3B H 0.1904 -0.2703 -0.0563 0.066 Uiso 1 1 calc R U . . . H3C H 0.2336 -0.2519 -0.2000 0.066 Uiso 1 1 calc R U . . . C4 C 0.3868(5) -0.1421(2) -0.0542(3) 0.0305(6) Uani 1 1 d . . . . . C5 C 0.4196(5) -0.0754(3) -0.2861(3) 0.0355(7) Uani 1 1 d . . . . . C6 C 0.4549(5) 0.0378(3) -0.0849(3) 0.0322(7) Uani 1 1 d . . . . . C7 C 0.4471(6) -0.1093(3) 0.2078(3) 0.0408(8) Uani 1 1 d . . . . . H7A H 0.5993 -0.1162 0.2221 0.061 Uiso 1 1 calc R U . . . H7B H 0.3882 -0.1775 0.2215 0.061 Uiso 1 1 calc R U . . . H7C H 0.4214 -0.0584 0.2728 0.061 Uiso 1 1 calc R U . . . C8 C 0.2697(5) -0.0076(3) -0.3967(3) 0.0368(7) Uani 1 1 d . . . . . C9 C 0.5355(6) -0.1507(3) -0.3206(4) 0.0508(9) Uani 1 1 d . . . . . H9A H 0.6203 -0.1956 -0.2527 0.061 Uiso 1 1 calc R U . . . H9B H 0.5329 -0.1591 -0.4128 0.061 Uiso 1 1 calc R U . . . C10 C -0.1854(6) 0.0707(4) -0.5485(4) 0.0552(10) Uani 1 1 d . . . . . H10A H -0.1177 0.0410 -0.6133 0.083 Uiso 1 1 calc R U . . . H10B H -0.2926 0.1218 -0.5953 0.083 Uiso 1 1 calc R U . . . H10C H -0.2525 0.0144 -0.5111 0.083 Uiso 1 1 calc R U . . . C11 C -0.0196(5) 0.1251(3) -0.4332(3) 0.0432(8) Uani 1 1 d . . . . . C12 C 0.1080(6) 0.2093(4) -0.4838(5) 0.0649(12) Uani 1 1 d . . . . . H12A H 0.2109 0.2416 -0.4056 0.097 Uiso 1 1 calc R U . . . H12B H 0.0117 0.2633 -0.5349 0.097 Uiso 1 1 calc R U . . . H12C H 0.1821 0.1765 -0.5430 0.097 Uiso 1 1 calc R U . . . C13 C 0.0435(7) 0.0088(4) 0.1185(5) 0.0726(15) Uani 1 1 d . . . . . H13A H -0.1108 0.0127 0.0855 0.109 Uiso 1 1 calc R U . . . H13B H 0.1030 0.0794 0.1203 0.109 Uiso 1 1 calc R U . . . H13C H 0.0864 -0.0208 0.2105 0.109 Uiso 1 1 calc R U . . . C14 C -0.1204(7) 0.1716(5) -0.3286(4) 0.0767(15) Uani 1 1 d . . . . . H14A H -0.0114 0.2062 -0.2558 0.115 Uiso 1 1 calc R U . . . H14B H -0.1858 0.1153 -0.2900 0.115 Uiso 1 1 calc R U . . . H14C H -0.2282 0.2230 -0.3736 0.115 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0440(13) 0.0457(14) 0.0253(10) 0.0043(10) 0.0121(9) 0.0084(11) O2 0.0522(13) 0.0299(11) 0.0233(10) -0.0041(9) 0.0100(9) -0.0041(10) O3 0.0626(16) 0.0265(13) 0.0334(12) -0.0001(10) 0.0141(10) -0.0091(11) O4 0.0442(13) 0.0304(12) 0.0392(13) 0.0044(10) 0.0124(10) 0.0070(10) O5 0.0344(12) 0.0533(15) 0.0419(13) -0.0043(11) 0.0109(9) 0.0056(11) N1 0.0414(14) 0.0262(14) 0.0237(11) -0.0013(10) 0.0092(9) -0.0037(11) O6 0.0676(17) 0.088(2) 0.0250(12) 0.0035(13) 0.0200(11) 0.0180(15) C2 0.0368(17) 0.0275(16) 0.0256(14) 0.0010(12) 0.0063(11) 0.0020(13) C3 0.050(2) 0.0386(19) 0.0391(19) -0.0090(15) 0.0079(15) -0.0112(16) C4 0.0382(17) 0.0251(15) 0.0269(14) 0.0016(12) 0.0073(11) -0.0008(13) C5 0.0459(17) 0.0372(18) 0.0254(14) -0.0040(13) 0.0136(12) -0.0001(15) C6 0.0419(17) 0.0292(16) 0.0249(14) 0.0003(13) 0.0090(12) -0.0006(14) C7 0.053(2) 0.0407(19) 0.0269(15) 0.0050(14) 0.0087(13) 0.0030(16) C8 0.0414(17) 0.044(2) 0.0259(15) -0.0070(13) 0.0120(13) -0.0039(15) C9 0.064(2) 0.052(2) 0.0410(19) -0.0035(17) 0.0224(16) 0.0112(19) C10 0.0473(19) 0.071(3) 0.042(2) 0.0073(18) 0.0055(15) -0.0044(19) C11 0.0449(19) 0.047(2) 0.0346(18) 0.0048(15) 0.0069(13) 0.0083(16) C12 0.073(3) 0.056(3) 0.052(3) 0.0122(19) -0.004(2) -0.010(2) C13 0.058(3) 0.097(4) 0.066(3) -0.012(3) 0.022(2) 0.030(3) C14 0.085(3) 0.103(4) 0.043(2) 0.003(2) 0.021(2) 0.049(3) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C8 1.315(4) . ? O1 C11 1.486(4) . ? O2 C6 1.356(3) . ? O2 C2 1.453(4) . ? O3 C6 1.211(4) . ? O4 C4 1.401(4) . ? O4 H4 0.8200 . ? O5 C2 1.380(3) . ? O5 C13 1.426(4) . ? N1 C6 1.343(4) . ? N1 C5 1.424(4) . ? N1 C4 1.450(4) . ? O6 C8 1.214(4) . ? C2 C7 1.507(4) . ? C2 C4 1.564(4) . ? C3 C4 1.511(4) . ? C3 H3A 0.9600 . ? C3 H3B 0.9600 . ? C3 H3C 0.9600 . ? C5 C9 1.312(5) . ? C5 C8 1.507(5) . ? C7 H7A 0.9600 . ? C7 H7B 0.9600 . ? C7 H7C 0.9600 . ? C9 H9A 0.9300 . ? C9 H9B 0.9300 . ? C10 C11 1.496(5) . ? C10 H10A 0.9600 . ? C10 H10B 0.9600 . ? C10 H10C 0.9600 . ? C11 C14 1.509(5) . ? C11 C12 1.516(5) . ? C12 H12A 0.9600 . ? C12 H12B 0.9600 . ? C12 H12C 0.9600 . ? C13 H13A 0.9600 . ? C13 H13B 0.9600 . ? C13 H13C 0.9600 . ? C14 H14A 0.9600 . ? C14 H14B 0.9600 . ? C14 H14C 0.9600 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C8 O1 C11 121.9(2) . . ? C6 O2 C2 108.7(2) . . ? C4 O4 H4 109.5 . . ? C2 O5 C13 116.3(3) . . ? C6 N1 C5 122.4(3) . . ? C6 N1 C4 112.8(2) . . ? C5 N1 C4 124.6(3) . . ? O5 C2 O2 108.5(2) . . ? O5 C2 C7 115.2(3) . . ? O2 C2 C7 107.3(2) . . ? O5 C2 C4 107.0(2) . . ? O2 C2 C4 103.5(2) . . ? C7 C2 C4 114.6(3) . . ? C4 C3 H3A 109.5 . . ? C4 C3 H3B 109.5 . . ? H3A C3 H3B 109.5 . . ? C4 C3 H3C 109.5 . . ? H3A C3 H3C 109.5 . . ? H3B C3 H3C 109.5 . . ? O4 C4 N1 107.5(2) . . ? O4 C4 C3 111.6(3) . . ? N1 C4 C3 112.9(3) . . ? O4 C4 C2 111.5(2) . . ? N1 C4 C2 99.3(2) . . ? C3 C4 C2 113.4(2) . . ? C9 C5 N1 122.8(3) . . ? C9 C5 C8 120.2(3) . . ? N1 C5 C8 116.8(3) . . ? O3 C6 N1 128.0(3) . . ? O3 C6 O2 122.0(3) . . ? N1 C6 O2 109.9(3) . . ? C2 C7 H7A 109.5 . . ? C2 C7 H7B 109.5 . . ? H7A C7 H7B 109.5 . . ? C2 C7 H7C 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? O6 C8 O1 126.9(3) . . ? O6 C8 C5 121.4(3) . . ? O1 C8 C5 111.8(2) . . ? C5 C9 H9A 120.0 . . ? C5 C9 H9B 120.0 . . ? H9A C9 H9B 120.0 . . ? C11 C10 H10A 109.5 . . ? C11 C10 H10B 109.5 . . ? H10A C10 H10B 109.5 . . ? C11 C10 H10C 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? O1 C11 C10 109.4(3) . . ? O1 C11 C14 101.9(3) . . ? C10 C11 C14 110.8(3) . . ? O1 C11 C12 109.9(3) . . ? C10 C11 C12 113.2(3) . . ? C14 C11 C12 110.9(4) . . ? C11 C12 H12A 109.5 . . ? C11 C12 H12B 109.5 . . ? H12A C12 H12B 109.5 . . ? C11 C12 H12C 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? O5 C13 H13A 109.5 . . ? O5 C13 H13B 109.5 . . ? H13A C13 H13B 109.5 . . ? O5 C13 H13C 109.5 . . ? H13A C13 H13C 109.5 . . ? H13B C13 H13C 109.5 . . ? C11 C14 H14A 109.5 . . ? C11 C14 H14B 109.5 . . ? H14A C14 H14B 109.5 . . ? C11 C14 H14C 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? _refine_diff_density_max 0.196 _refine_diff_density_min -0.238 _refine_diff_density_rms 0.046 _shelxl_version_number 2013-2 _shelx_res_file ; TITL c847-1 in P 21 CELL 0.71073 6.4900 12.4870 10.0660 90.000 106.939 90.000 ZERR 2.00 0.0000 0.0000 0.0000 0.000 0.000 0.000 LATT -1 SYMM - X, 1/2 + Y, - Z SFAC C H N O UNIT 26 42 2 12 MERG 2 BOND $H ACTA OMIT 0 -1 1 OMIT 0 1 1 OMIT 1 0 0 OMIT 0 2 0 OMIT 0 -2 0 FMAP 2 PLAN 25 L.S. 128 WGHT 0.042800 FVAR 3.97425 O1 4 0.128939 0.043577 -0.348929 11.00000 0.04399 0.04565 = 0.02529 0.00430 0.01214 0.00843 O2 4 0.437659 0.031332 0.045916 11.00000 0.05216 0.02992 = 0.02325 -0.00411 0.01002 -0.00409 O3 4 0.502946 0.120362 -0.131578 11.00000 0.06258 0.02649 = 0.03342 -0.00009 0.01413 -0.00905 O4 4 0.582722 -0.196921 -0.005499 11.00000 0.04421 0.03035 = 0.03925 0.00439 0.01243 0.00702 AFIX 147 H4 2 0.559217 -0.260171 0.006504 11.00000 -1.50000 AFIX 0 O5 4 0.120594 -0.057730 0.028146 11.00000 0.03444 0.05331 = 0.04187 -0.00427 0.01085 0.00562 N1 3 0.416408 -0.058396 -0.146825 11.00000 0.04144 0.02617 = 0.02371 -0.00133 0.00921 -0.00368 O6 4 0.284986 -0.004095 -0.513967 11.00000 0.06765 0.08803 = 0.02496 0.00349 0.02000 0.01799 C2 1 0.340896 -0.070980 0.061910 11.00000 0.03681 0.02750 = 0.02564 0.00102 0.00627 0.00196 C3 1 0.204172 -0.217271 -0.122314 11.00000 0.05038 0.03858 = 0.03907 -0.00902 0.00785 -0.01116 AFIX 33 H3A 2 0.072423 -0.177402 -0.153884 11.00000 -1.50000 H3B 2 0.190438 -0.270285 -0.056346 11.00000 -1.50000 H3C 2 0.233604 -0.251894 -0.199979 11.00000 -1.50000 AFIX 0 C4 1 0.386779 -0.142104 -0.054232 11.00000 0.03820 0.02511 = 0.02691 0.00164 0.00734 -0.00079 C5 1 0.419566 -0.075447 -0.286095 11.00000 0.04588 0.03720 = 0.02542 -0.00403 0.01362 -0.00007 C6 1 0.454915 0.037788 -0.084940 11.00000 0.04192 0.02925 = 0.02489 0.00031 0.00901 -0.00060 C7 1 0.447079 -0.109261 0.207788 11.00000 0.05290 0.04067 = 0.02691 0.00497 0.00874 0.00300 AFIX 33 H7A 2 0.599310 -0.116245 0.222073 11.00000 -1.50000 H7B 2 0.388182 -0.177486 0.221485 11.00000 -1.50000 H7C 2 0.421404 -0.058444 0.272756 11.00000 -1.50000 AFIX 0 C8 1 0.269719 -0.007580 -0.396666 11.00000 0.04135 0.04449 = 0.02594 -0.00698 0.01203 -0.00392 C9 1 0.535496 -0.150685 -0.320569 11.00000 0.06393 0.05198 = 0.04102 -0.00345 0.02238 0.01122 AFIX 93 H9A 2 0.620276 -0.195617 -0.252731 11.00000 -1.20000 H9B 2 0.532892 -0.159086 -0.412845 11.00000 -1.20000 AFIX 0 C10 1 -0.185440 0.070723 -0.548547 11.00000 0.04730 0.07150 = 0.04201 0.00727 0.00548 -0.00439 AFIX 33 H10A 2 -0.117726 0.041033 -0.613253 11.00000 -1.50000 H10B 2 -0.292552 0.121842 -0.595310 11.00000 -1.50000 H10C 2 -0.252474 0.014421 -0.511059 11.00000 -1.50000 AFIX 0 C11 1 -0.019562 0.125074 -0.433245 11.00000 0.04491 0.04701 = 0.03456 0.00484 0.00691 0.00831 C12 1 0.107989 0.209331 -0.483837 11.00000 0.07251 0.05640 = 0.05174 0.01221 -0.00412 -0.00956 AFIX 33 H12A 2 0.210908 0.241582 -0.405635 11.00000 -1.50000 H12B 2 0.011731 0.263303 -0.534906 11.00000 -1.50000 H12C 2 0.182117 0.176475 -0.543015 11.00000 -1.50000 AFIX 0 C13 1 0.043517 0.008827 0.118468 11.00000 0.05792 0.09674 = 0.06590 -0.01243 0.02221 0.02950 AFIX 33 H13A 2 -0.110777 0.012714 0.085482 11.00000 -1.50000 H13B 2 0.103001 0.079389 0.120286 11.00000 -1.50000 H13C 2 0.086429 -0.020805 0.210457 11.00000 -1.50000 AFIX 0 C14 1 -0.120402 0.171631 -0.328643 11.00000 0.08479 0.10330 = 0.04311 0.00302 0.02058 0.04924 AFIX 33 H14A 2 -0.011430 0.206151 -0.255786 11.00000 -1.50000 H14B 2 -0.185753 0.115333 -0.289993 11.00000 -1.50000 H14C 2 -0.228187 0.223032 -0.373596 11.00000 -1.50000 AFIX 0 HKLF 4 REM c847-1 in P 21 REM R1 = 0.0481 for 2427 Fo > 4sig(Fo) and 0.0630 for all 3053 data REM 182 parameters refined using 1 restraints END WGHT 0.0428 0.0000 REM Highest difference peak 0.196, deepest hole -0.238, 1-sigma level 0.046 Q1 1 0.1385 -0.0228 -0.3274 11.00000 0.05 0.20 Q2 1 0.4442 -0.0208 -0.1283 11.00000 0.05 0.19 Q3 1 0.5783 -0.1323 -0.0154 11.00000 0.05 0.18 Q4 1 0.1728 0.1120 -0.3199 11.00000 0.05 0.18 Q5 1 0.5119 0.1882 -0.1198 11.00000 0.05 0.18 Q6 1 0.1224 0.0217 0.0238 11.00000 0.05 0.16 Q7 1 0.4002 -0.1459 -0.3031 11.00000 0.05 0.16 Q8 1 0.4228 -0.0287 0.0666 11.00000 0.05 0.16 Q9 1 0.3640 -0.2154 -0.0908 11.00000 0.05 0.16 Q10 1 0.4322 -0.1935 0.1958 11.00000 0.05 0.16 Q11 1 0.2766 -0.1606 -0.0854 11.00000 0.05 0.16 Q12 1 0.3343 0.0036 0.2622 11.00000 0.05 0.16 Q13 1 0.1040 -0.1409 0.0187 11.00000 0.05 0.16 Q14 1 0.4083 -0.0929 -0.1043 11.00000 0.05 0.15 Q15 1 0.3822 0.0908 0.0741 11.00000 0.05 0.15 Q16 1 -0.1959 -0.0040 -0.5492 11.00000 0.05 0.14 Q17 1 -0.2293 -0.0201 -0.5762 11.00000 0.05 0.14 Q18 1 0.0951 0.1353 -0.4189 11.00000 0.05 0.14 Q19 1 -0.2497 0.1575 -0.5717 11.00000 0.05 0.14 Q20 1 -0.2793 0.0663 -0.3266 11.00000 0.05 0.13 Q21 1 0.4284 -0.0260 0.2249 11.00000 0.05 0.13 Q22 1 0.2991 -0.0996 -0.5095 11.00000 0.05 0.13 Q23 1 0.2701 -0.0872 -0.3584 11.00000 0.05 0.13 Q24 1 0.5465 -0.0776 -0.3007 11.00000 0.05 0.13 Q25 1 0.2039 -0.2932 -0.1543 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242.54 1 1 3 8 495.00 82.2622 1 1 3 9 449.10 91.334 1 1 3 10 29.60 69.0509 1 1 3 11 106.60 59.5438 1 1 4 -12 584.90 91.3568 1 1 4 -11 335.10 66.2953 1 1 4 -10 383.50 95.4557 1 1 4 -9 993.90 137.722 1 1 4 -8 1282.70 154.601 1 1 4 -7 675.10 82.5712 1 1 4 -6 1115.00 86.9418 1 1 4 -5 1493.05 99.1588 1 1 4 -414424.50 1019.30 1 1 4 -323329.80 1415.54 1 1 4 -211796.90 575.417 1 1 4 -110875.50 463.124 1 1 4 0 9213.81 364.48 1 1 4 1 6809.05 372.762 1 1 4 221906.30 2527.92 1 1 4 3 839.10 90.4588 1 1 4 4 3180.20 263.695 1 1 4 5 3850.30 388.102 1 1 4 6 557.50 102.913 1 1 4 7 1136.20 120.893 1 1 4 8 454.60 81.4883 1 1 4 9 26.30 45.2675 1 1 4 10 143.60 52.203 1 1 4 11 -36.40 60.669 1 1 5 -12 115.30 55.9963 1 1 5 -11 269.70 66.0273 1 1 5 -10 14.10 50.2208 1 1 5 -9 2733.80 343.627 1 1 5 -8 1892.40 210.412 1 1 5 -7 484.80 80.9743 1 1 5 -6 1061.60 125.634 1 1 5 -5 3347.45 244.919 1 1 5 -4 1143.05 77.9188 1 1 5 -3 3804.90 215.863 1 1 5 -2 2757.55 168.676 1 1 5 -1 4623.95 243.479 1 1 5 0 3095.85 143.963 1 1 5 112498.20 734.486 1 1 5 2 4610.40 350.609 1 1 5 3 6935.70 676.36 1 1 5 4 1913.40 169.889 1 1 5 5 720.10 94.7079 1 1 5 6 441.10 86.2156 1 1 5 7 1843.10 207.744 1 1 5 8 912.30 104.715 1 1 5 9 1493.80 146.876 1 1 5 10 101.00 67.4168 1 1 5 11 146.10 49.3587 1 1 6 -11 175.60 52.2375 1 1 6 -10 21.40 44.6285 1 1 6 -9 113.20 68.3936 1 1 6 -8 4376.80 501.784 1 1 6 -7 959.60 104.424 1 1 6 -6 3884.10 447.327 1 1 6 -5 3160.25 309.321 1 1 6 -4 5878.90 396.125 1 1 6 -3 5099.20 330.892 1 1 6 -2 6286.95 383.891 1 1 6 -1 1137.20 76.8669 1 1 6 0 115.598 19.8184 1 1 6 1 598.15 43.0565 1 1 6 2 5292.45 344.834 1 1 6 3 391.40 60.3041 1 1 6 4 221.10 54.2164 1 1 6 5 171.70 54.1316 1 1 6 6 4748.40 645.394 1 1 6 7 2091.80 227.566 1 1 6 8 1182.60 158.731 1 1 6 9 257.60 78.9672 1 1 6 10 65.70 48.397 1 1 6 11 -7.90 37.1156 1 1 7 -11 190.90 60.9412 1 1 7 -10 488.60 95.0442 1 1 7 -9 1228.70 145.528 1 1 7 -8 689.00 119.537 1 1 7 -7 274.70 87.0632 1 1 7 -6 665.00 79.8201 1 1 7 -5 2377.30 240.928 1 1 7 -4 311.65 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57.1697 1 1 9 -4 527.00 106.136 1 1 9 -3 1718.90 180.561 1 1 9 -2 947.70 113.455 1 1 9 -1 719.30 80.9023 1 1 9 0 170.00 40.599 1 1 9 1 2498.00 229.835 1 1 9 2 56.80 29.44 1 1 9 3 805.95 68.7947 1 1 9 4 682.50 99.3775 1 1 9 5 1297.80 148.434 1 1 9 6 781.90 103.889 1 1 9 7 587.20 86.1205 1 1 9 8 209.10 77.5561 1 1 9 9 121.00 44.8875 1 1 10 -10 336.40 71.4728 1 1 10 -9 264.70 73.7888 1 1 10 -8 877.00 115.49 1 1 10 -7 116.80 73.3069 1 1 10 -6 296.20 61.6822 1 1 10 -5 3344.80 355.68 1 1 10 -4 678.50 92.0595 1 1 10 -3 1051.50 158.856 1 1 10 -2 340.40 84.1502 1 1 10 -1 1469.30 167.317 1 1 10 0 1385.45 109.577 1 1 10 1 1270.40 98.6409 1 1 10 2 278.50 42.4675 1 1 10 3 871.40 70.5715 1 1 10 4 290.60 57.1886 1 1 10 5 699.60 92.813 1 1 10 6 84.10 50.8228 1 1 10 7 186.30 55.3816 1 1 10 8 85.50 61.475 1 1 10 9 271.90 46.3597 1 1 11 -9 145.30 56.9502 1 1 11 -8 88.90 65.5067 1 1 11 -7 56.60 65.6284 1 1 11 -6 417.70 70.0408 1 1 11 -5 517.50 78.1436 1 1 11 -4 431.90 91.5839 1 1 11 -3 587.80 80.4175 1 1 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95.10 52.9851 1 1 14 -5 164.40 64.7492 1 1 14 -4 70.40 42.934 1 1 14 -3 381.40 78.6261 1 1 14 -2 222.90 44.8139 1 1 14 -1 59.80 37.5943 1 1 14 0 62.30 48.6086 1 1 14 1 335.20 80.518 1 1 14 2 158.90 73.3758 1 1 14 3 180.80 75.3737 1 1 14 4 127.60 41.6504 1 1 14 5 234.00 54.7402 1 1 15 -4 161.30 59.8511 1 1 15 -3 59.65 38.6902 1 1 15 -2 74.55 27.47 1 1 15 -1 262.70 71.9019 1 1 15 0 217.80 50.9546 1 1 15 1 213.10 70.2844 1 1 15 2 162.20 49.6412 1 1 15 3 -12.50 54.6715 1 1 15 4 -15.90 30.6053 1 1 16 -1 269.40 63.1779 1 1 16 0 245.50 60.7416 1 2 -13 4 95.00 51.423 1 2 -13 5 345.40 67.1111 1 2 -12 3 222.90 67.8003 1 2 -12 4 88.30 63.8566 1 2 -12 5 139.90 60.3095 1 2 -12 6 61.00 40.9033 1 2 -11 2 381.90 74.7603 1 2 -11 3 264.90 59.9773 1 2 -11 4 21.20 64.6413 1 2 -11 5 365.80 63.1124 1 2 -11 6 236.60 70.1984 1 2 -11 7 38.70 39.5789 1 2 -10 2 736.20 93.3677 1 2 -10 3 77.10 54.2958 1 2 -10 4 51.70 46.602 1 2 -10 5 412.70 62.7736 1 2 -10 6 266.30 66.7715 1 2 -10 7 636.70 89.347 1 2 -10 8 36.70 60.1036 1 2 -9 2 21.70 46.9953 1 2 -9 3 270.00 61.8606 1 2 -9 4 98.70 53.4721 1 2 -9 5 1217.50 157.602 1 2 -9 6 261.50 76.9345 1 2 -9 7 321.00 60.013 1 2 -9 8 26.50 61.0844 1 2 -9 9 617.60 74.1991 1 2 -8 -5 86.20 28.3837 1 2 -8 -3 192.50 52.7038 1 2 -8 -2 539.20 64.6806 1 2 -8 -1 37.20 56.924 1 2 -8 0 456.30 52.1907 1 2 -8 1 1130.45 106.237 1 2 -8 2 1252.20 193.771 1 2 -8 3 2261.80 210.929 1 2 -8 4 1557.00 164.313 1 2 -8 5 471.10 79.387 1 2 -8 6 714.30 103.188 1 2 -8 7 -28.60 42.3773 1 2 -8 8 -16.50 38.8356 1 2 -8 9 185.40 45.8229 1 2 -7 -6 1257.70 120.496 1 2 -7 -5 1112.40 135.637 1 2 -7 -4 1861.60 212.087 1 2 -7 -3 2804.70 257.24 1 2 -7 -2 7438.00 801.875 1 2 -7 -1 7873.30 745.288 1 2 -7 0 1906.60 168.649 1 2 -7 1 611.70 55.3825 1 2 -7 2 2396.75 161.305 1 2 -7 3 486.45 52.2434 1 2 -7 4 2157.80 253.417 1 2 -7 5 148.50 68.689 1 2 -7 6 -22.80 42.7178 1 2 -7 7 191.80 51.4736 1 2 -7 8 173.10 49.5273 1 2 -7 9 154.40 66.5575 1 2 -6 -6 833.40 84.2482 1 2 -6 -5 40.20 30.0201 1 2 -6 -4 424.05 100.28 1 2 -6 -3 3633.50 320.728 1 2 -6 -2 1359.60 115.819 1 2 -6 -1 2168.60 192.115 1 2 -6 0 78.80 27.3711 1 2 -6 1 3620.55 223.862 1 2 -6 2 1466.10 91.5218 1 2 -6 3 564.75 60.3131 1 2 -6 4 221.00 45.4965 1 2 -6 5 724.60 83.2631 1 2 -6 6 207.80 66.0044 1 2 -6 7 200.20 76.0121 1 2 -6 8 88.70 46.2479 1 2 -6 9 461.40 83.8331 1 2 -6 10 257.40 67.613 1 2 -5 -8 557.20 64.5634 1 2 -5 -7 2488.30 246.795 1 2 -5 -6 2693.20 235.391 1 2 -5 -5 2164.60 339.725 1 2 -5 -4 2083.90 312.726 1 2 -5 -3 6669.60 881.446 1 2 -5 -215128.00 1393.94 1 2 -5 -1 7169.40 594.219 1 2 -5 0 4943.80 635.284 1 2 -5 1 5919.95 360.23 1 2 -5 2 3878.25 238.387 1 2 -5 3 2267.35 157.82 1 2 -5 4 3162.75 236.227 1 2 -5 5 380.30 62.5144 1 2 -5 6 922.60 114.163 1 2 -5 7 186.80 60.5416 1 2 -5 8 1767.80 202.783 1 2 -5 10 90.30 57.9819 1 2 -4 -8 1215.50 133.387 1 2 -4 -7 5116.30 912.226 1 2 -4 -6 556.95 135.556 1 2 -4 -5 2544.95 321.083 1 2 -4 -4 585.217 49.2981 1 2 -4 -3 2514.30 182.705 1 2 -4 -2 9043.85 509.149 1 2 -4 -1 4699.20 334.844 1 2 -4 0 8328.10 584.667 1 2 -4 121688.30 1253.38 1 2 -4 2 374.15 64.9702 1 2 -4 3 7754.60 563.789 1 2 -4 4 2793.10 280.359 1 2 -4 5 620.40 87.0339 1 2 -4 6 94.50 47.0669 1 2 -4 7 25.60 60.293 1 2 -4 8 117.40 52.7029 1 2 -4 9 372.80 67.7519 1 2 -4 10 663.00 102.38 1 2 -3 -7 558.05 138.38 1 2 -3 -6 305.45 119.952 1 2 -3 -5 385.40 57.8801 1 2 -3 -417063.90 1663.75 1 2 -3 -3 1593.18 74.6155 1 2 -3 -211455.80 555.798 1 2 -3 -1 5574.85 260.045 1 2 -3 0 5339.06 220.244 1 2 -3 1 3106.32 144.281 1 2 -3 2 8788.86 462.606 1 2 -3 3 5331.00 672.95 1 2 -3 4 374.85 99.9487 1 2 -3 5 210.30 44.0611 1 2 -3 6 158.90 50.2969 1 2 -3 7 411.20 85.4784 1 2 -3 8 438.50 91.392 1 2 -3 9 111.50 48.5731 1 2 -3 10 94.00 62.4532 1 2 -3 11 21.80 30.4035 1 2 -2 -7 492.30 61.4391 1 2 -2 -5 3689.60 258.672 1 2 -2 -416196.10 1517.14 1 2 -2 -3 7567.30 424.818 1 2 -2 -2 3320.25 160.102 1 2 -2 -128960.10 894.29 1 2 -2 0 77.3809 16.9556 1 2 -2 116516.30 651.664 1 2 -2 215442.90 1124.96 1 2 -2 3 76.75 28.3144 1 2 -2 4 1176.60 167.208 1 2 -2 5 202.55 34.0215 1 2 -2 6 437.25 94.0874 1 2 -2 7 975.30 109.439 1 2 -2 8 1377.30 150.173 1 2 -2 9 396.50 100.474 1 2 -2 10 245.60 61.0862 1 2 -2 11 132.10 46.1507 1 2 -1 -13 233.50 58.3199 1 2 -1 -7 5038.60 539.438 1 2 -1 -6 4726.30 438.10 1 2 -1 -5 4288.80 341.59 1 2 -1 -4 7708.50 591.656 1 2 -1 -312799.20 770.839 1 2 -1 -2 1324.60 89.1991 1 2 -1 -1 492.40 39.6747 1 2 -1 0 6658.40 353.899 1 2 -1 1 7629.50 387.919 1 2 -1 2 4534.15 240.216 1 2 -1 3 7782.80 619.329 1 2 -1 4 1104.45 112.73 1 2 -1 5 888.60 152.817 1 2 -1 6 8369.90 1113.24 1 2 -1 7 165.50 52.3913 1 2 -1 8 1641.60 189.163 1 2 -1 9 1149.80 133.456 1 2 -1 10 451.10 74.9552 1 2 -1 11 459.00 60.7302 1 2 0 -13 -13.30 44.6545 1 2 0 -12 113.40 63.0696 1 2 0 -11 52.10 52.0906 1 2 0 -7 718.90 94.305 1 2 0 -6 890.70 101.066 1 2 0 -5 437.70 51.3188 1 2 0 -4 -6.30 26.0969 1 2 0 -3 334.50 32.5354 1 2 0 -2 54.00 19.5827 1 2 0 019087.20 704.066 1 2 0 126154.00 929.552 1 2 0 2 6007.90 458.062 1 2 0 3 1124.60 112.989 1 2 0 4 803.95 60.8125 1 2 0 5 13.20 26.6175 1 2 0 6 343.00 75.4003 1 2 0 7 1219.00 118.157 1 2 0 8 2853.20 316.482 1 2 0 9 537.40 88.5268 1 2 0 10 137.60 51.7514 1 2 0 11 3.10 33.3047 1 2 1 -13 340.40 49.2287 1 2 1 -12 39.00 51.1019 1 2 1 -11 -10.60 56.4131 1 2 1 -10 87.20 70.0411 1 2 1 -9 3433.20 377.729 1 2 1 -8 994.30 109.827 1 2 1 -7 4641.75 362.202 1 2 1 -6 4299.10 371.41 1 2 1 -5 3819.10 330.682 1 2 1 -4 7119.35 405.691 1 2 1 -312895.20 594.005 1 2 1 -2 1329.75 189.191 1 2 1 -1 437.039 28.2703 1 2 1 0 6885.10 383.224 1 2 1 1 8217.30 504.574 1 2 1 2 4557.30 337.696 1 2 1 3 8414.70 781.675 1 2 1 4 1298.30 125.649 1 2 1 5 1029.50 95.8559 1 2 1 6 7974.20 999.063 1 2 1 7 238.50 71.2207 1 2 1 8 1697.30 189.229 1 2 1 9 1220.80 131.965 1 2 1 10 381.30 63.1738 1 2 1 11 388.50 68.3786 1 2 2 -12 132.90 63.3069 1 2 2 -11 589.30 100.577 1 2 2 -10 107.40 45.0722 1 2 2 -9 1386.90 167.011 1 2 2 -8 556.00 100.958 1 2 2 -7 437.20 46.5479 1 2 2 -6 8637.40 778.297 1 2 2 -5 3283.35 208.049 1 2 2 -417984.70 1066.72 1 2 2 -3 7815.45 404.271 1 2 2 -2 2937.90 145.634 1 2 2 -123656.70 912.305 1 2 2 0 71.20 12.6607 1 2 2 115845.30 2379.63 1 2 2 217237.80 1242.35 1 2 2 3 56.60 34.7571 1 2 2 4 1257.70 118.562 1 2 2 5 326.80 66.3035 1 2 2 6 442.90 70.5547 1 2 2 7 961.70 114.808 1 2 2 8 1282.00 167.214 1 2 2 9 406.00 78.5271 1 2 2 10 375.60 62.182 1 2 2 11 178.40 57.0686 1 2 3 -12 57.50 61.8635 1 2 3 -11 12.60 50.7389 1 2 3 -10 2014.40 267.041 1 2 3 -9 338.00 88.5486 1 2 3 -8 3064.30 370.904 1 2 3 -7 588.10 109.009 1 2 3 -6 272.80 40.2819 1 2 3 -5 428.25 43.1158 1 2 3 -418800.90 1725.52 1 2 3 -3 1430.90 76.1565 1 2 3 -210440.80 647.149 1 2 3 -1 5240.81 224.069 1 2 3 0 5393.45 457.525 1 2 3 1 3087.15 448.776 1 2 3 2 9609.10 811.073 1 2 3 3 6102.00 565.177 1 2 3 4 499.10 59.8584 1 2 3 5 252.20 53.5408 1 2 3 6 179.80 61.4289 1 2 3 7 367.80 82.8472 1 2 3 8 374.20 77.8731 1 2 3 9 145.50 49.5724 1 2 3 10 75.20 58.3739 1 2 3 11 57.20 35.7392 1 2 4 -12 31.60 59.7474 1 2 4 -11 497.90 85.0291 1 2 4 -10 588.90 87.1243 1 2 4 -9 2095.10 209.457 1 2 4 -8 1496.20 179.092 1 2 4 -7 4896.55 394.23 1 2 4 -6 588.80 55.5956 1 2 4 -5 2410.95 161.882 1 2 4 -4 533.90 43.2552 1 2 4 -3 2237.76 161.552 1 2 4 -2 8841.04 718.739 1 2 4 -1 4472.98 202.35 1 2 4 0 7819.75 375.775 1 2 4 122032.30 1627.65 1 2 4 2 279.15 58.9261 1 2 4 3 8183.10 835.843 1 2 4 4 2751.00 295.434 1 2 4 5 672.20 89.7832 1 2 4 6 88.20 43.5388 1 2 4 7 34.90 43.9631 1 2 4 8 113.60 47.9598 1 2 4 9 374.60 55.9142 1 2 4 10 565.10 96.8617 1 2 5 -12 214.90 61.0902 1 2 5 -11 321.60 76.8558 1 2 5 -10 181.10 66.7162 1 2 5 -9 47.20 41.6253 1 2 5 -8 674.90 102.514 1 2 5 -7 2330.70 279.216 1 2 5 -6 2420.20 178.212 1 2 5 -5 2006.55 174.245 1 2 5 -4 1952.75 119.564 1 2 5 -3 6386.25 428.08 1 2 5 -212564.10 723.011 1 2 5 -1 7043.19 359.387 1 2 5 0 4644.85 243.492 1 2 5 1 5944.50 415.655 1 2 5 2 3730.35 291.766 1 2 5 3 2408.50 232.153 1 2 5 4 3329.50 379.62 1 2 5 5 356.20 70.062 1 2 5 6 960.50 131.082 1 2 5 7 125.60 56.2136 1 2 5 8 1402.00 165.924 1 2 5 9 273.70 60.7847 1 2 5 10 78.00 42.0576 1 2 6 -12 12.90 53.619 1 2 6 -11 52.00 63.7974 1 2 6 -10 183.80 56.4228 1 2 6 -9 1104.60 140.105 1 2 6 -8 2285.50 224.413 1 2 6 -7 7335.70 854.437 1 2 6 -6 902.20 72.9431 1 2 6 -5 37.95 41.9357 1 2 6 -4 434.05 46.6185 1 2 6 -3 3477.70 227.512 1 2 6 -2 1296.74 79.8479 1 2 6 -1 2125.72 117.807 1 2 6 0 62.439 21.0044 1 2 6 1 3917.75 271.953 1 2 6 2 1391.85 183.265 1 2 6 3 575.40 83.0363 1 2 6 4 178.50 55.1369 1 2 6 5 702.60 96.4767 1 2 6 6 199.10 75.1982 1 2 6 7 219.80 59.1835 1 2 6 8 158.70 79.583 1 2 6 9 376.20 79.8313 1 2 6 10 287.60 62.6984 1 2 7 -11 44.20 36.7627 1 2 7 -10 1040.90 131.612 1 2 7 -9 229.30 76.3533 1 2 7 -8 1194.90 141.217 1 2 7 -7 1039.20 93.7669 1 2 7 -6 1429.30 145.473 1 2 7 -5 1266.60 92.7031 1 2 7 -4 1967.25 156.456 1 2 7 -3 2842.30 220.357 1 2 7 -2 6754.82 430.161 1 2 7 -1 7457.96 485.215 1 2 7 0 1887.18 115.304 1 2 7 1 544.75 105.781 1 2 7 2 2419.90 418.662 1 2 7 3 456.70 93.401 1 2 7 4 2251.60 250.605 1 2 7 5 163.80 50.894 1 2 7 6 -43.50 41.2056 1 2 7 7 212.90 77.6923 1 2 7 8 134.20 49.683 1 2 7 9 117.90 43.4889 1 2 8 -11 300.00 59.5132 1 2 8 -10 515.20 91.6003 1 2 8 -9 1045.00 126.996 1 2 8 -8 859.00 111.659 1 2 8 -7 721.00 105.465 1 2 8 -6 3046.40 335.483 1 2 8 -5 162.70 74.1912 1 2 8 -4 363.00 41.3171 1 2 8 -3 210.40 74.0381 1 2 8 -2 465.037 44.8903 1 2 8 -1 27.7136 27.8658 1 2 8 0 434.134 42.3088 1 2 8 1 1073.29 78.6822 1 2 8 2 1271.60 166.399 1 2 8 3 2121.85 366.617 1 2 8 4 1254.60 142.952 1 2 8 5 462.70 99.6262 1 2 8 6 685.30 106.926 1 2 8 7 -0.30 48.829 1 2 8 8 35.60 62.8849 1 2 8 9 234.50 51.3637 1 2 9 -10 160.20 66.2066 1 2 9 -9 109.70 44.9484 1 2 9 -8 353.40 82.9255 1 2 9 -7 729.70 108.088 1 2 9 -6 366.40 83.6401 1 2 9 -5 743.20 97.3714 1 2 9 -4 478.70 69.404 1 2 9 -3 1043.62 86.159 1 2 9 -2 326.383 37.0828 1 2 9 -1 171.227 26.4415 1 2 9 0 211.56 35.7034 1 2 9 1 1117.97 71.1205 1 2 9 2 85.55 40.9638 1 2 9 3 348.15 103.879 1 2 9 4 32.10 43.561 1 2 9 5 1083.80 122.046 1 2 9 6 337.60 53.9426 1 2 9 7 289.60 69.3343 1 2 9 8 3.70 56.9694 1 2 9 9 560.80 75.0066 1 2 10 -10 -9.80 52.5963 1 2 10 -9 31.00 52.6883 1 2 10 -8 244.70 68.0228 1 2 10 -7 127.30 58.1946 1 2 10 -6 1036.10 126.359 1 2 10 -5 521.10 74.0202 1 2 10 -4 1365.00 156.31 1 2 10 -3 553.60 81.084 1 2 10 -2 2231.25 265.329 1 2 10 -1 281.10 43.3219 1 2 10 0 2895.20 234.84 1 2 10 1 309.75 51.366 1 2 10 2 791.30 144.087 1 2 10 3 58.65 26.2618 1 2 10 4 43.30 50.0975 1 2 10 5 421.80 87.9326 1 2 10 6 217.10 58.8519 1 2 10 7 634.80 81.8298 1 2 10 8 54.80 61.1713 1 2 11 -9 38.20 55.8298 1 2 11 -8 68.50 60.1227 1 2 11 -7 553.70 73.5317 1 2 11 -6 111.60 70.4856 1 2 11 -5 315.10 64.5429 1 2 11 -4 78.10 67.6623 1 2 11 -3 447.70 79.9343 1 2 11 -2 164.55 46.9758 1 2 11 -1 269.95 51.2103 1 2 11 0 369.45 48.8178 1 2 11 1 4990.20 427.94 1 2 11 2 473.50 70.4028 1 2 11 3 320.75 47.3974 1 2 11 4 75.00 66.955 1 2 11 5 250.10 79.8724 1 2 11 6 393.70 76.3659 1 2 11 7 -32.30 38.0988 1 2 12 -8 8.70 52.107 1 2 12 -7 234.40 52.3226 1 2 12 -6 82.50 60.4688 1 2 12 -5 367.60 81.7594 1 2 12 -4 193.40 36.2397 1 2 12 -3 36.45 48.2988 1 2 12 -2 1327.15 224.218 1 2 12 -1 63.20 43.4421 1 2 12 0 1322.70 165.096 1 2 12 1 536.85 52.0904 1 2 12 2 136.45 58.9415 1 2 12 3 151.90 68.6987 1 2 12 4 -19.40 62.8563 1 2 12 5 58.30 42.2427 1 2 12 6 29.30 43.0678 1 2 13 -7 301.30 69.4836 1 2 13 -6 91.70 45.6807 1 2 13 -5 178.70 47.2546 1 2 13 -4 25.10 46.8121 1 2 13 -3 905.60 79.1588 1 2 13 -2 328.10 80.6358 1 2 13 -1 8.40 36.4042 1 2 13 0 394.80 52.2139 1 2 13 1 -28.90 55.1984 1 2 13 2 -46.40 55.4953 1 2 13 3 99.70 44.6466 1 2 13 4 97.70 49.3077 1 2 13 5 229.80 53.8183 1 2 14 -6 437.50 54.7258 1 2 14 -5 23.15 46.5998 1 2 14 -4 100.25 35.1052 1 2 14 -3 67.60 31.2565 1 2 14 -2 188.35 61.9435 1 2 14 -1 111.50 28.6841 1 2 14 0 353.80 60.2911 1 2 14 1 213.50 63.4856 1 2 14 2 97.30 59.3227 1 2 14 3 96.60 62.4331 1 2 14 4 11.70 39.9083 1 2 15 -4 150.20 109.062 1 2 15 -3 68.25 34.7354 1 2 15 -2 260.10 50.9366 1 2 15 -1 204.40 50.0261 1 2 15 0 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44.30 46.2066 1 3 -7 -6 297.75 75.3127 1 3 -7 -5 787.55 119.515 1 3 -7 -4 35.20 29.5235 1 3 -7 -3 769.65 129.62 1 3 -7 -2 2946.50 264.414 1 3 -7 -1 2090.30 187.235 1 3 -7 0 3406.50 315.377 1 3 -7 1 2000.85 146.442 1 3 -7 2 44.10 34.4179 1 3 -7 3 518.40 69.7796 1 3 -7 4 544.90 75.0032 1 3 -7 5 47.40 60.3411 1 3 -7 6 484.40 83.2788 1 3 -7 7 138.40 44.5795 1 3 -7 8 41.10 55.1511 1 3 -7 9 243.00 43.4229 1 3 -6 -6 124.40 56.855 1 3 -6 -5 675.15 54.1951 1 3 -6 -4 691.70 95.2409 1 3 -6 -3 3518.35 676.235 1 3 -6 -2 93.70 31.3555 1 3 -6 -1 2756.70 259.705 1 3 -6 0 1050.60 106.418 1 3 -6 1 2399.30 159.977 1 3 -6 2 1220.85 87.2103 1 3 -6 3 394.95 47.0178 1 3 -6 4 107.70 46.7016 1 3 -6 5 495.90 72.4434 1 3 -6 6 335.30 81.3545 1 3 -6 7 324.10 73.222 1 3 -6 8 123.20 52.5642 1 3 -6 9 104.20 40.3061 1 3 -5 -8 24.90 21.631 1 3 -5 -7 3533.65 257.814 1 3 -5 -6 932.75 73.0048 1 3 -5 -5 937.40 110.437 1 3 -5 -4 359.15 39.0377 1 3 -5 -3 881.75 120.803 1 3 -5 -2 5993.50 404.666 1 3 -5 -1 206.95 33.2814 1 3 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4406.29 360.696 1 3 -3 2 561.95 55.9352 1 3 -3 3 3516.50 346.482 1 3 -3 4 343.70 64.7152 1 3 -3 5 1877.70 205.534 1 3 -3 6 483.60 83.751 1 3 -3 7 1524.20 170.06 1 3 -3 8 227.00 68.837 1 3 -3 9 299.10 68.4959 1 3 -3 10 309.80 53.5259 1 3 -2 -11 9.20 42.8873 1 3 -2 -10 610.30 88.9923 1 3 -2 -9 286.00 62.7487 1 3 -2 -8 2705.20 306.168 1 3 -2 -7 422.50 120.111 1 3 -2 -6 4746.50 449.302 1 3 -2 -5 2630.05 523.711 1 3 -2 -4 1300.70 89.6569 1 3 -2 -3 743.30 51.7969 1 3 -2 -2 259.40 32.7493 1 3 -2 0 2377.90 331.931 1 3 -2 1 1227.20 75.6403 1 3 -2 2 592.30 47.1058 1 3 -2 3 2909.30 323.746 1 3 -2 4 333.30 56.3502 1 3 -2 5 3072.70 353.129 1 3 -2 6 1045.40 124.037 1 3 -2 7 142.80 61.7825 1 3 -2 8 304.60 70.7839 1 3 -2 9 48.90 49.9035 1 3 -2 10 262.00 48.7919 1 3 -1 -12 183.45 62.6461 1 3 -1 -11 3.30 47.396 1 3 -1 -10 517.20 82.0349 1 3 -1 -9 184.00 51.4664 1 3 -1 -8 1149.90 138.714 1 3 -1 -7 218.25 45.5104 1 3 -1 -6 1341.40 115.206 1 3 -1 -5 4477.60 383.811 1 3 -1 -4 3658.65 651.626 1 3 -1 -3 682.40 73.785 1 3 -1 -2 2128.50 206.688 1 3 -1 -1 5079.60 558.20 1 3 -1 119423.60 1864.61 1 3 -1 2 3672.90 266.558 1 3 -1 3 481.85 47.2056 1 3 -1 4 1278.45 183.48 1 3 -1 5 2994.90 290.663 1 3 -1 6 965.70 112.579 1 3 -1 7 262.70 51.3413 1 3 -1 8 1375.30 177.961 1 3 -1 9 237.90 52.2739 1 3 -1 10 601.20 70.168 1 3 0 -13 149.60 43.755 1 3 0 -12 187.75 36.3142 1 3 0 -11 226.20 39.8006 1 3 0 -10 2808.20 665.315 1 3 0 -8 175.50 58.0491 1 3 0 -7 -23.70 41.3755 1 3 0 -6 16.75 43.6293 1 3 0 -5 2922.50 259.483 1 3 0 -4 2242.10 176.707 1 3 0 -3 88.00 32.5862 1 3 0 -2 781.261 35.7791 1 3 0 -1 110.70 28.8241 1 3 0 0 8602.10 697.714 1 3 0 1 1900.20 144.452 1 3 0 2 179.70 36.0793 1 3 0 3 1994.80 187.958 1 3 0 4 673.40 72.1852 1 3 0 5 79.40 53.4838 1 3 0 6 3367.70 362.235 1 3 0 7 -5.20 61.9521 1 3 0 8 363.70 57.4259 1 3 0 9 302.00 57.5224 1 3 0 10 492.10 53.8115 1 3 1 -12 274.30 63.175 1 3 1 -11 81.50 48.9963 1 3 1 -10 761.40 111.743 1 3 1 -9 225.95 69.0354 1 3 1 -8 1080.59 87.3889 1 3 1 -7 182.724 38.4128 1 3 1 -6 1166.05 89.0727 1 3 1 -5 4392.15 316.546 1 3 1 -4 3909.55 296.085 1 3 1 -3 647.65 90.8763 1 3 1 -2 2016.10 113.192 1 3 1 -1 4593.40 389.624 1 3 1 014540.50 1215.68 1 3 1 121695.50 1962.78 1 3 1 2 3849.70 344.744 1 3 1 3 490.40 57.1244 1 3 1 4 1429.00 139.582 1 3 1 5 2834.40 297.414 1 3 1 6 947.60 109.671 1 3 1 7 223.40 55.002 1 3 1 8 1392.50 163.655 1 3 1 9 209.30 45.9626 1 3 1 10 647.70 76.241 1 3 2 -12 -1.10 43.4965 1 3 2 -11 202.50 67.3422 1 3 2 -10 977.50 129.158 1 3 2 -9 452.80 83.0798 1 3 2 -8 2644.25 194.37 1 3 2 -7 417.342 44.4239 1 3 2 -6 4299.55 323.124 1 3 2 -5 2780.10 182.883 1 3 2 -4 1209.00 103.463 1 3 2 -3 745.15 108.616 1 3 2 -2 260.40 37.3827 1 3 2 -1 2767.47 134.212 1 3 2 0 2289.20 186.018 1 3 2 1 1355.10 101.91 1 3 2 2 656.00 59.5214 1 3 2 3 3379.50 314.742 1 3 2 4 217.40 47.6418 1 3 2 5 3481.20 378.529 1 3 2 6 927.90 115.472 1 3 2 7 86.60 64.4185 1 3 2 8 288.50 69.8864 1 3 2 9 40.10 41.5812 1 3 2 10 258.90 49.5834 1 3 3 -12 15.70 46.4877 1 3 3 -11 287.70 60.1419 1 3 3 -10 561.10 99.5749 1 3 3 -9 1730.20 191.926 1 3 3 -8 434.40 50.1118 1 3 3 -7 2137.05 154.287 1 3 3 -6 942.60 78.1533 1 3 3 -5 1851.00 131.75 1 3 3 -4 3991.95 268.057 1 3 3 -3 4797.50 538.137 1 3 3 -2 1728.35 110.324 1 3 3 -114901.60 1464.27 1 3 3 0 9012.55 1146.55 1 3 3 1 4683.00 1045.32 1 3 3 2 716.50 76.8796 1 3 3 3 3742.10 348.24 1 3 3 4 296.20 64.1102 1 3 3 5 1963.30 206.58 1 3 3 6 514.40 67.2197 1 3 3 7 1285.80 159.426 1 3 3 8 286.90 71.5195 1 3 3 9 236.90 39.9734 1 3 3 10 281.10 64.3058 1 3 4 -12 262.70 68.7938 1 3 4 -11 161.00 54.6192 1 3 4 -10 584.80 97.523 1 3 4 -9 162.30 61.5458 1 3 4 -8 6046.60 537.94 1 3 4 -7 246.45 45.3479 1 3 4 -6 3574.15 269.405 1 3 4 -5 568.16 51.3516 1 3 4 -4 531.721 66.1579 1 3 4 -3 406.139 43.3628 1 3 4 -2 663.851 44.7644 1 3 4 -1 567.943 34.5653 1 3 4 0 2055.57 168.987 1 3 4 1 341.00 35.9848 1 3 4 2 3720.30 363.134 1 3 4 3 2426.20 256.216 1 3 4 4 2757.80 287.958 1 3 4 5 703.00 101.681 1 3 4 6 1695.20 171.208 1 3 4 7 231.40 72.4377 1 3 4 8 217.70 64.2833 1 3 4 9 158.30 43.809 1 3 5 -12 257.40 68.3313 1 3 5 -11 120.20 62.2655 1 3 5 -10 874.90 115.611 1 3 5 -9 86.00 43.8464 1 3 5 -8 58.30 45.9752 1 3 5 -7 3206.30 406.507 1 3 5 -6 851.504 106.029 1 3 5 -5 848.60 84.8223 1 3 5 -4 306.659 31.7179 1 3 5 -3 889.153 53.9934 1 3 5 -2 5868.72 343.368 1 3 5 -1 157.781 23.2819 1 3 5 0 3762.22 221.964 1 3 5 1 6.80 31.6935 1 3 5 2 273.05 61.7401 1 3 5 3 132.10 44.044 1 3 5 4 1018.00 117.23 1 3 5 5 384.70 58.9796 1 3 5 6 589.50 83.8683 1 3 5 7 957.20 130.856 1 3 5 8 505.20 83.7553 1 3 5 9 -24.50 45.7926 1 3 6 -12 372.60 85.4531 1 3 6 -11 30.10 62.8606 1 3 6 -10 99.50 42.9745 1 3 6 -9 92.80 60.2656 1 3 6 -8 3475.60 392.259 1 3 6 -7 1844.70 154.106 1 3 6 -6 134.417 40.8862 1 3 6 -5 707.83 55.5415 1 3 6 -4 646.312 77.7518 1 3 6 -3 3265.76 200.75 1 3 6 -2 82.7435 26.8772 1 3 6 -1 2854.35 222.721 1 3 6 0 1007.45 64.6762 1 3 6 1 2476.65 343.981 1 3 6 2 1227.20 120.787 1 3 6 3 432.00 79.4202 1 3 6 4 98.70 42.4385 1 3 6 5 531.40 73.4622 1 3 6 6 259.10 70.4907 1 3 6 7 357.40 64.5318 1 3 6 8 107.30 38.7813 1 3 6 9 23.00 40.0062 1 3 7 -11 261.90 55.9238 1 3 7 -10 455.50 76.9049 1 3 7 -9 19.10 42.9565 1 3 7 -8 109.70 62.0109 1 3 7 -7 556.90 72.0409 1 3 7 -6 307.374 51.8275 1 3 7 -5 866.853 64.799 1 3 7 -4 76.8471 30.377 1 3 7 -3 774.689 58.0521 1 3 7 -2 2583.44 154.009 1 3 7 -1 1968.08 110.696 1 3 7 0 3210.64 202.079 1 3 7 1 1971.56 116.222 1 3 7 2 34.25 42.7834 1 3 7 3 726.60 98.0542 1 3 7 4 420.80 56.6406 1 3 7 5 31.60 40.4641 1 3 7 6 383.50 76.3055 1 3 7 7 104.70 86.5988 1 3 7 8 156.00 54.6082 1 3 7 9 304.00 62.6518 1 3 8 -11 12.20 29.937 1 3 8 -10 138.30 68.7835 1 3 8 -9 213.20 68.1609 1 3 8 -8 85.30 46.0754 1 3 8 -7 1114.70 145.774 1 3 8 -6 465.00 63.7819 1 3 8 -5 814.096 86.337 1 3 8 -4 220.55 36.7762 1 3 8 -3 29.0381 21.6348 1 3 8 -2 1771.50 153.814 1 3 8 -1 284.861 40.433 1 3 8 0 802.532 59.0228 1 3 8 1 3164.29 194.741 1 3 8 2 1084.95 115.759 1 3 8 3 327.70 66.3428 1 3 8 4 707.10 108.603 1 3 8 5 866.40 118.603 1 3 8 6 99.80 46.4945 1 3 8 7 206.00 67.4114 1 3 8 8 46.00 34.557 1 3 9 -10 -9.30 37.4947 1 3 9 -9 183.10 64.7235 1 3 9 -8 546.20 80.4856 1 3 9 -7 141.00 72.3152 1 3 9 -6 417.70 60.4673 1 3 9 -5 339.10 52.4513 1 3 9 -4 1231.31 91.7497 1 3 9 -3 340.80 43.411 1 3 9 -2 3743.55 331.092 1 3 9 -1 451.486 41.3547 1 3 9 0 2243.98 136.185 1 3 9 1 430.474 42.7842 1 3 9 2 68.10 41.8746 1 3 9 3 501.80 74.863 1 3 9 4 34.30 41.2806 1 3 9 5 290.90 59.3573 1 3 9 6 219.70 52.65 1 3 9 7 348.60 74.7387 1 3 9 8 95.50 37.3856 1 3 10 -10 4.30 34.5055 1 3 10 -9 144.90 44.8026 1 3 10 -8 45.60 40.3811 1 3 10 -7 268.80 45.9824 1 3 10 -6 292.90 44.9208 1 3 10 -5 926.50 216.87 1 3 10 -4 270.45 123.323 1 3 10 -3 1011.90 102.235 1 3 10 -2 274.50 46.9249 1 3 10 -1 1142.70 108.709 1 3 10 0 259.30 42.2603 1 3 10 1 908.75 77.777 1 3 10 2 68.65 61.1744 1 3 10 3 179.50 57.7665 1 3 10 4 9.10 36.7831 1 3 10 5 210.60 46.9458 1 3 10 6 479.60 59.5585 1 3 10 7 41.90 49.7421 1 3 11 -9 275.10 45.4264 1 3 11 -8 409.70 54.0961 1 3 11 -7 52.25 66.9681 1 3 11 -6 304.60 76.0958 1 3 11 -5 664.25 75.5827 1 3 11 -4 86.35 47.3251 1 3 11 -3 255.80 46.3676 1 3 11 -2 1028.65 124.037 1 3 11 -1 172.60 41.9651 1 3 11 0 2737.45 309.712 1 3 11 1 1593.70 123.855 1 3 11 2 1184.35 89.4095 1 3 11 3 408.20 72.5089 1 3 11 4 83.60 55.3074 1 3 11 5 159.60 60.987 1 3 11 6 35.20 36.991 1 3 12 -8 255.20 34.3496 1 3 12 -7 200.40 42.3435 1 3 12 -6 98.50 37.7857 1 3 12 -5 435.75 76.889 1 3 12 -4 416.90 79.188 1 3 12 -3 -1.60 52.20 1 3 12 -2 44.75 34.9263 1 3 12 -1 629.15 66.81 1 3 12 0 715.15 91.8448 1 3 12 1 259.35 49.4557 1 3 12 2 207.10 46.8307 1 3 12 3 210.10 54.681 1 3 12 4 65.40 42.1894 1 3 12 5 -21.50 31.7909 1 3 13 -7 216.35 140.968 1 3 13 -6 5.80 36.1023 1 3 13 -5 35.45 32.3121 1 3 13 -4 56.30 37.8665 1 3 13 -3 129.75 42.203 1 3 13 -2 72.60 30.6064 1 3 13 -1 116.35 30.4562 1 3 13 0 128.60 34.1432 1 3 13 1 227.90 51.0203 1 3 13 2 -15.70 32.5849 1 3 13 3 26.70 36.8894 1 3 13 4 279.70 64.7078 1 3 14 -5 168.70 37.1662 1 3 14 -4 13.40 25.4745 1 3 14 -3 110.50 35.0831 1 3 14 -2 21.85 62.0142 1 3 14 -1 74.15 37.5406 1 3 14 0 216.10 69.7538 1 3 14 1 349.20 71.0048 1 3 14 2 182.00 45.6104 1 3 14 3 29.80 32.0669 1 3 15 -2 313.90 50.4493 1 3 15 -1 58.60 42.8783 1 3 15 0 92.70 36.1743 1 4 -12 4 -5.40 33.1944 1 4 -11 3 220.80 57.8908 1 4 -11 4 223.80 59.448 1 4 -11 5 58.60 42.9813 1 4 -10 2 180.80 39.0756 1 4 -10 3 161.50 60.0424 1 4 -10 4 194.50 64.2872 1 4 -10 5 62.80 38.5834 1 4 -10 6 44.70 47.6096 1 4 -9 2 273.00 71.6776 1 4 -9 3 122.70 35.728 1 4 -9 4 8.80 44.4353 1 4 -9 5 174.80 48.1048 1 4 -9 6 136.70 56.9989 1 4 -8 -4 558.10 83.6524 1 4 -8 -3 102.00 50.0236 1 4 -8 -2 569.80 70.1202 1 4 -8 -1 1108.30 119.82 1 4 -8 0 3642.40 424.14 1 4 -8 2 392.80 54.7222 1 4 -8 3 349.80 54.4138 1 4 -8 4 42.40 30.7401 1 4 -8 5 47.10 38.9608 1 4 -8 6 294.40 83.2487 1 4 -8 7 306.60 69.6663 1 4 -7 -5 3017.10 293.551 1 4 -7 -4 2986.10 286.307 1 4 -7 -3 1306.60 133.847 1 4 -7 -2 3469.00 353.656 1 4 -7 -1 2053.10 199.836 1 4 -7 0 1282.50 146.285 1 4 -7 1 477.40 85.8922 1 4 -7 2 572.60 52.814 1 4 -7 3 56.90 36.7625 1 4 -7 4 44.80 41.2631 1 4 -7 5 79.70 47.8766 1 4 -7 6 521.20 86.4846 1 4 -7 7 518.40 84.9515 1 4 -6 -6 1.00 36.9988 1 4 -6 -5 468.90 73.4798 1 4 -6 -4 1630.40 152.32 1 4 -6 -3 552.70 56.1542 1 4 -6 -2 609.30 82.5219 1 4 -6 -1 939.20 96.228 1 4 -6 0 1097.50 141.937 1 4 -6 1 2281.05 159.054 1 4 -6 2 160.60 35.2031 1 4 -6 3 372.60 57.9128 1 4 -6 4 232.20 72.8624 1 4 -6 5 126.10 56.429 1 4 -6 6 51.40 51.5986 1 4 -6 7 120.00 54.1188 1 4 -6 8 135.40 39.9796 1 4 -5 -8 1055.10 111.518 1 4 -5 -7 1070.35 86.0831 1 4 -5 -6 1426.10 104.902 1 4 -5 -5 1068.60 111.829 1 4 -5 -4 1004.70 97.8768 1 4 -5 -3 4326.50 432.735 1 4 -5 -2 1090.40 102.405 1 4 -5 -1 2606.70 244.451 1 4 -5 0 551.00 67.0359 1 4 -5 1 464.45 84.1133 1 4 -5 2 221.25 35.2286 1 4 -5 3 49.20 50.8716 1 4 -5 4 313.60 50.7112 1 4 -5 5 251.00 58.1577 1 4 -5 6 753.70 78.9606 1 4 -5 7 1117.20 125.428 1 4 -5 8 134.40 43.6609 1 4 -4 -9 1195.70 135.49 1 4 -4 -8 3382.00 409.578 1 4 -4 -7 762.40 67.4109 1 4 -4 -6 1783.60 139.526 1 4 -4 -5 1929.15 150.419 1 4 -4 -4 482.60 59.0168 1 4 -4 -3 78.70 31.8743 1 4 -4 -2 1185.00 106.707 1 4 -4 -1 723.70 76.953 1 4 -4 0 639.15 119.012 1 4 -4 1 1092.80 126.625 1 4 -4 2 337.50 61.1747 1 4 -4 3 317.80 61.2188 1 4 -4 4 842.00 96.1259 1 4 -4 5 467.20 71.8415 1 4 -4 6 93.70 51.917 1 4 -4 7 285.00 56.7834 1 4 -4 8 334.40 74.6427 1 4 -3 -10 71.40 40.0254 1 4 -3 -9 184.80 42.3927 1 4 -3 -8 964.25 87.0865 1 4 -3 -7 385.95 97.2774 1 4 -3 -6 1356.55 106.707 1 4 -3 -5 785.55 66.816 1 4 -3 -4 331.60 38.6822 1 4 -3 -3 2023.10 211.812 1 4 -3 0 107.70 28.3825 1 4 -3 1 1152.20 110.415 1 4 -3 2 1964.60 179.328 1 4 -3 3 1763.50 187.588 1 4 -3 4 1844.20 188.005 1 4 -3 5 618.70 96.1926 1 4 -3 6 2300.20 262.971 1 4 -3 7 576.30 94.9843 1 4 -3 8 29.80 54.3211 1 4 -2 -11 27.30 44.0253 1 4 -2 -10 56.60 38.6031 1 4 -2 -9 776.00 98.8108 1 4 -2 -8 903.70 74.0025 1 4 -2 -7 1164.20 114.485 1 4 -2 -6 2825.95 552.716 1 4 -2 -5 231.10 44.9792 1 4 -2 -4 369.30 66.7859 1 4 -2 -3 957.20 96.6552 1 4 -2 -2 1193.30 95.5942 1 4 -2 -1 5614.90 521.601 1 4 -2 0 2189.20 198.018 1 4 -2 1 4463.00 461.075 1 4 -2 2 3193.40 333.321 1 4 -2 3 792.40 86.7112 1 4 -2 4 871.80 108.533 1 4 -2 5 109.00 44.9656 1 4 -2 6 433.70 81.4979 1 4 -2 7 262.90 52.1478 1 4 -2 8 198.90 55.3669 1 4 -2 9 -6.30 42.9185 1 4 -1 -12 232.00 42.4861 1 4 -1 -11 28.60 45.4554 1 4 -1 -10 468.10 68.7796 1 4 -1 -9 63.10 37.1401 1 4 -1 -8 2742.55 499.054 1 4 -1 -7 660.30 234.426 1 4 -1 -6 1164.20 172.529 1 4 -1 -5 755.20 148.69 1 4 -1 -4 1265.20 126.592 1 4 -1 -3 1983.30 183.158 1 4 -1 -2 2925.50 291.50 1 4 -1 0 69.80 17.1052 1 4 -1 1 1373.30 127.23 1 4 -1 2 1733.90 180.892 1 4 -1 3 2930.40 346.163 1 4 -1 4 129.20 48.1659 1 4 -1 5 741.50 96.2059 1 4 -1 6 26.70 49.0086 1 4 -1 7 103.30 61.6203 1 4 -1 8 37.90 36.5677 1 4 -1 9 100.40 48.7983 1 4 0 -12 46.75 29.7057 1 4 0 -11 317.90 55.8054 1 4 0 -10 79.00 55.0271 1 4 0 -9 231.45 77.0908 1 4 0 -8 38.035 28.7874 1 4 0 -7 90.1351 22.9356 1 4 0 -611979.80 1189.57 1 4 0 -5 314.501 51.9899 1 4 0 -4 2048.75 307.112 1 4 0 -3 2054.20 183.53 1 4 0 -2 300.10 48.2867 1 4 0 -1 384.00 74.4896 1 4 0 0 1234.20 106.704 1 4 0 1 4272.00 409.289 1 4 0 2 1740.20 168.073 1 4 0 3 8462.50 1093.62 1 4 0 4 995.30 121.007 1 4 0 5 6.60 45.4191 1 4 0 6 153.80 57.1381 1 4 0 7 388.00 61.1127 1 4 0 8 51.80 35.8031 1 4 0 9 26.80 46.3991 1 4 1 -12 292.20 38.9075 1 4 1 -11 55.95 39.9656 1 4 1 -10 571.60 112.511 1 4 1 -9 24.40 39.4089 1 4 1 -8 3023.95 238.849 1 4 1 -7 662.166 82.2427 1 4 1 -6 1242.00 89.9149 1 4 1 -5 805.941 102.545 1 4 1 -4 1250.25 114.921 1 4 1 -3 1978.81 114.904 1 4 1 -2 2812.70 275.326 1 4 1 -1 2179.90 205.518 1 4 1 0 93.70 24.5198 1 4 1 1 1548.70 141.238 1 4 1 2 1915.00 167.334 1 4 1 3 3178.30 326.13 1 4 1 4 127.30 32.5757 1 4 1 5 690.50 95.5797 1 4 1 6 -21.20 32.2786 1 4 1 7 136.00 64.716 1 4 1 8 21.80 54.0067 1 4 1 9 241.10 50.9239 1 4 2 -12 38.70 35.2263 1 4 2 -11 26.45 35.9942 1 4 2 -10 101.45 41.1142 1 4 2 -9 824.45 256.092 1 4 2 -8 916.391 137.512 1 4 2 -7 1422.35 103.865 1 4 2 -6 2991.30 213.988 1 4 2 -5 209.843 26.8121 1 4 2 -4 368.70 38.5726 1 4 2 -3 805.80 58.6539 1 4 2 -2 1009.40 120.792 1 4 2 0 2075.30 187.496 1 4 2 1 5171.00 543.736 1 4 2 2 3539.40 339.60 1 4 2 3 824.60 93.85 1 4 2 4 900.00 95.4795 1 4 2 5 41.50 32.2088 1 4 2 6 475.50 70.8055 1 4 2 7 266.60 67.3803 1 4 2 8 221.70 57.5196 1 4 2 9 -33.80 37.6394 1 4 3 -12 295.65 81.0986 1 4 3 -11 127.35 36.3768 1 4 3 -10 54.00 35.5367 1 4 3 -9 227.90 52.3251 1 4 3 -8 1070.10 127.943 1 4 3 -7 315.184 46.7247 1 4 3 -6 1395.40 108.227 1 4 3 -5 796.467 111.281 1 4 3 -4 292.05 39.291 1 4 3 -3 1834.80 131.082 1 4 3 -2 24.4881 18.2428 1 4 3 -1 2883.75 191.314 1 4 3 0 150.40 36.0837 1 4 3 1 1392.30 114.388 1 4 3 2 2267.20 192.299 1 4 3 3 1635.90 152.553 1 4 3 4 1744.70 186.588 1 4 3 5 610.60 89.864 1 4 3 6 2401.10 295.543 1 4 3 7 604.10 74.4723 1 4 3 8 17.30 45.6787 1 4 4 -12 26.10 36.1743 1 4 4 -11 93.05 43.9657 1 4 4 -10 277.80 65.0609 1 4 4 -9 1369.10 170.196 1 4 4 -8 3237.50 365.863 1 4 4 -7 805.50 67.1522 1 4 4 -6 1636.05 121.567 1 4 4 -5 1833.73 183.855 1 4 4 -4 512.899 54.9417 1 4 4 -3 46.10 24.70 1 4 4 -2 1158.70 131.111 1 4 4 -1 744.10 97.0239 1 4 4 0 656.70 137.994 1 4 4 1 1012.95 245.112 1 4 4 2 472.40 64.9334 1 4 4 3 356.90 45.0566 1 4 4 4 957.70 98.9973 1 4 4 5 397.30 62.639 1 4 4 6 50.90 41.5564 1 4 4 7 201.80 45.7647 1 4 4 8 351.20 66.0606 1 4 5 -12 63.40 72.1319 1 4 5 -11 79.60 32.238 1 4 5 -10 235.15 83.1682 1 4 5 -9 241.95 62.5546 1 4 5 -8 926.65 114.713 1 4 5 -7 941.869 70.9864 1 4 5 -6 1233.76 85.0024 1 4 5 -5 1051.86 94.3165 1 4 5 -4 1041.17 95.0847 1 4 5 -3 4319.23 394.60 1 4 5 -2 1204.13 81.5711 1 4 5 -1 2452.72 165.703 1 4 5 0 566.224 43.4986 1 4 5 1 428.45 51.0152 1 4 5 2 255.40 55.789 1 4 5 3 79.20 33.7203 1 4 5 4 340.30 69.5651 1 4 5 5 200.20 42.6942 1 4 5 6 755.80 80.5773 1 4 5 7 1192.00 132.985 1 4 5 8 180.30 56.395 1 4 6 -11 69.75 109.254 1 4 6 -10 66.30 32.1855 1 4 6 -9 195.75 43.693 1 4 6 -8 645.55 143.411 1 4 6 -7 83.75 38.2306 1 4 6 -6 39.078 36.6705 1 4 6 -5 426.699 45.75 1 4 6 -4 1587.03 97.0442 1 4 6 -3 537.227 43.6876 1 4 6 -2 649.895 45.9871 1 4 6 -1 963.016 61.9663 1 4 6 0 1033.69 81.4992 1 4 6 1 1920.60 211.698 1 4 6 2 218.10 56.1129 1 4 6 3 312.70 55.2775 1 4 6 4 214.90 46.1103 1 4 6 5 185.30 53.6232 1 4 6 6 74.10 36.2889 1 4 6 7 104.50 42.6332 1 4 6 8 122.70 34.9282 1 4 7 -11 61.30 38.0623 1 4 7 -10 600.35 150.701 1 4 7 -9 60.60 50.5822 1 4 7 -8 419.40 61.4529 1 4 7 -7 49.75 29.6703 1 4 7 -6 43.25 40.1342 1 4 7 -5 3111.44 304.245 1 4 7 -4 2936.53 231.373 1 4 7 -3 1494.70 111.673 1 4 7 -2 3625.10 244.598 1 4 7 -1 2111.72 127.893 1 4 7 0 1246.54 82.1729 1 4 7 1 453.252 41.5258 1 4 7 2 643.20 102.189 1 4 7 3 70.80 40.3263 1 4 7 4 -0.50 34.6692 1 4 7 5 100.60 58.6161 1 4 7 6 429.90 65.8046 1 4 7 7 476.70 73.9488 1 4 8 -10 29.70 34.8357 1 4 8 -9 303.05 115.287 1 4 8 -8 178.75 61.23 1 4 8 -7 530.00 204.949 1 4 8 -6 1815.20 196.973 1 4 8 -5 258.40 91.0257 1 4 8 -4 537.794 55.6647 1 4 8 -3 151.405 31.2307 1 4 8 -2 545.335 43.3333 1 4 8 -1 1094.61 76.1099 1 4 8 0 3869.00 395.429 1 4 8 1 698.50 72.4065 1 4 8 2 408.75 97.0184 1 4 8 3 397.60 60.4198 1 4 8 4 81.70 54.9446 1 4 8 5 87.20 39.6373 1 4 8 6 70.90 49.7792 1 4 8 7 158.80 41.1427 1 4 9 -10 39.05 37.2212 1 4 9 -9 159.80 40.1787 1 4 9 -8 463.00 115.491 1 4 9 -7 46.05 87.1893 1 4 9 -6 70.10 39.4878 1 4 9 -5 2005.80 237.733 1 4 9 -4 172.95 42.3176 1 4 9 -3 604.05 64.3696 1 4 9 -2 649.20 62.0647 1 4 9 -1 393.00 47.2498 1 4 9 0 312.65 47.0162 1 4 9 1 232.60 43.264 1 4 9 2 275.35 54.4096 1 4 9 3 105.20 36.2324 1 4 9 4 72.70 41.7933 1 4 9 5 149.50 59.0003 1 4 9 6 224.40 42.2055 1 4 10 -9 17.60 35.9541 1 4 10 -8 4.45 41.9981 1 4 10 -7 -5.15 55.3642 1 4 10 -6 70.30 41.4708 1 4 10 -5 -2.00 36.9419 1 4 10 -4 75.35 35.6255 1 4 10 -3 82.15 39.4962 1 4 10 -2 22.35 42.9228 1 4 10 -1 102.00 36.4285 1 4 10 0 567.70 63.4874 1 4 10 1 240.70 34.4308 1 4 10 2 265.55 46.1781 1 4 10 3 82.50 55.5015 1 4 10 4 221.80 57.3918 1 4 10 5 72.50 44.4578 1 4 10 6 34.60 31.7968 1 4 11 -8 29.95 37.108 1 4 11 -7 76.60 38.9324 1 4 11 -6 122.35 38.3094 1 4 11 -5 22.35 68.3781 1 4 11 -4 80.20 43.2935 1 4 11 -3 78.10 40.2441 1 4 11 -2 100.00 31.1527 1 4 11 -1 304.85 68.2648 1 4 11 0 623.60 61.1883 1 4 11 1 345.45 104.018 1 4 11 2 715.75 119.261 1 4 11 3 232.70 42.5435 1 4 11 4 173.20 41.005 1 4 11 5 30.70 46.3512 1 4 12 -7 26.65 25.6101 1 4 12 -6 275.05 42.5786 1 4 12 -5 384.65 74.5654 1 4 12 -4 143.25 43.761 1 4 12 -3 -22.15 53.30 1 4 12 -2 24.90 30.931 1 4 12 -1 100.55 30.0971 1 4 12 0 102.10 97.5941 1 4 12 1 317.90 42.5147 1 4 12 2 321.20 59.8423 1 4 12 3 152.40 50.7438 1 4 12 4 -45.10 42.4142 1 4 13 -6 64.40 49.7907 1 4 13 -5 111.80 37.2358 1 4 13 -4 47.30 29.971 1 4 13 -3 57.10 53.3235 1 4 13 -2 51.70 52.8979 1 4 13 -1 4.50 38.4667 1 4 13 0 238.70 39.2175 1 4 13 1 -12.00 47.9652 1 4 13 2 281.00 48.445 1 4 14 -3 73.85 45.7647 1 4 14 -2 34.90 21.6892 1 4 14 -1 140.55 65.7278 1 4 14 0 393.70 65.0212 1 5 -10 3 198.60 48.2034 1 5 -10 4 175.60 44.6499 1 5 -9 3 39.80 33.1353 1 5 -9 4 72.10 43.037 1 5 -9 5 58.10 27.1753 1 5 -8 2 234.80 47.6502 1 5 -8 3 59.60 44.4893 1 5 -8 4 69.10 37.3458 1 5 -8 5 112.00 38.5747 1 5 -7 2 992.80 111.663 1 5 -7 3 105.50 47.0586 1 5 -7 4 96.50 35.4131 1 5 -7 5 125.40 50.2608 1 5 -7 6 12.30 34.3667 1 5 -6 1 467.80 65.3779 1 5 -6 2 22.00 38.5455 1 5 -6 3 4.30 41.9883 1 5 -6 4 86.40 31.6745 1 5 -6 5 19.30 34.4902 1 5 -6 6 377.20 57.6804 1 5 -5 -8 404.50 65.6638 1 5 -5 -7 608.30 78.109 1 5 -5 -4 1140.70 125.80 1 5 -5 -3 192.50 40.096 1 5 -5 -2 3048.70 313.044 1 5 -5 -1 124.30 39.9316 1 5 -5 1 1936.50 192.272 1 5 -5 2 445.90 64.9234 1 5 -5 3 39.30 42.6451 1 5 -5 4 102.70 47.7588 1 5 -5 5 108.90 36.8778 1 5 -5 6 415.00 65.8074 1 5 -5 7 -26.30 27.5334 1 5 -4 -9 1511.20 149.566 1 5 -4 -8 429.60 56.6846 1 5 -4 -7 1225.30 140.621 1 5 -4 -6 171.10 57.3657 1 5 -4 -5 489.75 46.734 1 5 -4 1 1218.10 120.514 1 5 -4 2 2015.00 196.173 1 5 -4 3 50.10 43.7169 1 5 -4 4 581.50 65.8057 1 5 -4 5 -30.30 40.1872 1 5 -4 6 102.50 47.2985 1 5 -4 7 216.40 45.2048 1 5 -3 -10 46.30 38.631 1 5 -3 -9 595.50 85.0632 1 5 -3 -8 1104.10 128.919 1 5 -3 -7 1180.70 149.768 1 5 -3 -6 1322.50 142.238 1 5 -3 -5 909.30 100.60 1 5 -3 -4 328.00 67.035 1 5 -3 -3 420.60 44.8702 1 5 -3 -2 1784.50 158.69 1 5 -3 2 1348.70 153.136 1 5 -3 3 410.60 47.088 1 5 -3 4 231.70 49.5399 1 5 -3 5 38.30 30.4306 1 5 -3 6 43.90 32.5197 1 5 -3 7 8.40 44.1633 1 5 -2 -12 87.70 46.6123 1 5 -2 -11 -13.60 37.7247 1 5 -2 -10 -11.50 43.1371 1 5 -2 -9 601.70 92.0786 1 5 -2 -8 1321.90 146.827 1 5 -2 -7 446.00 72.4741 1 5 -2 -6 487.35 45.4012 1 5 -2 -5 1360.90 146.505 1 5 -2 -4 441.05 44.5059 1 5 -2 -3 1235.30 160.46 1 5 -2 1 625.10 64.4554 1 5 -2 2 352.60 63.9949 1 5 -2 3 289.10 53.7186 1 5 -2 4 117.80 46.6869 1 5 -2 5 32.20 51.7421 1 5 -2 6 25.50 44.1682 1 5 -2 7 28.60 29.065 1 5 -1 -12 186.90 53.0667 1 5 -1 -11 64.15 34.7338 1 5 -1 -10 125.90 37.7372 1 5 -1 -9 366.50 46.6016 1 5 -1 -8 838.40 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