data_global _audit_update_record ; 2014-02-13 # Formatted by publCIF ; _audit_creation_date "13-04-19" _audit_creation_method CRYSTALS_ver_14.40 _oxford_structure_analysis_title 'abs_TCl_Sal_2 in P2(1)/c' _chemical_name_systematic ? _chemical_melting_point ? #looking for refcif # Check this file using the IUCr facility at: # http://checkcif.iucr.org/ # The content below is held in the file 'script/refcif.dat'. This is a text # file which you may edit to reflect local conditions. # Items which need looking at are represented by a '?'. # Items for which there are choices are prefixed with 'choose from'. _publ_contact_letter ; Please consider this CIF submission for publication as a Short Format Paper in Acta Crystallographica E. ; _publ_contact_author_name 'Anthony Other' _publ_contact_author_address ; Chemical Crystallography Laboratory, Department of Chemistry, University of Nowhere, Nowhere, NO1 4T, UK. ; _publ_contact_author_phone '+44 1865 000000' _publ_contact_author_fax '+44 1865 000000' _publ_contact_author_email 'a.n.other@chem.no.ac.uk' _publ_requested_journal 'Section E' _publ_requested_category EO # choose from: FI FM FO CI CM CO AD _publ_requested_coeditor_name 'Prof William Clegg' _publ_section_title # Title of paper - generally just the systematic or trivial name ; Title (type here to add) ; # The loop structure below should contain the names and addresses of all # authors, in the required order of publication. Repeat as necessary. loop_ _publ_author_name _publ_author_address _publ_author_footnote 'Other, Anthony N.' # Author 1 ; ? # Address for author 1 ; ; ? # Footnote for author 1 ; 'Else, S. O.' # Author 2 ; ? # Address 2 ; ; ? # Footnote 2 ; _publ_section_abstract # Text of the abstract # (a) The Abstract must be self-contained and comprehensible # without the rest of the paper. This means no references # to atom names or to compound numbers; compounds must be # identified as the title compound, or by name or by some other # means such as derivatives of each other (e.g. "the # corresponding ketone"). # (b) The chemical formula of "the title compound" must be given. # (c) Any crystallographic molecular symmetry should be # mentioned, and also the presence of more than one molecule # in the asymmetric unit (i.e. anything other than Z'=1). ; (type here to add abstract) ; _publ_section_related_literature # Not in version 2.3.1 ############################################################### # Essential references (e.g. to the origin of the material studied, related # structural studies, and to information supporting the reported structure) # should be cited in this section, with appropriate very brief explanatory # text, for example `The synthesis of the complex is described by Jones # (2001). The anhydrous complex has essentially the same coordination # geometry (Smith, 2003).' In addition, all references included in the # supplementary materials, but not elsewhere in the published article, # should be given here. The simple text `For related literature, see:...' # may be used, but further details should be provided in the Comment # section, which forms part of the supplementary material. ############################################################### ? _publ_section_comment # Text of the paper # Note that atoms are referenced as N2, not N(2) or N~2~ # If text containing () occur within (), the outer ones should be [] # Figures should be referenced as Fig. ; (type here to add) ; _publ_section_acknowledgements # Acknowledgments ; ? ; _publ_section_figure_captions # Captions to figures - Start each caption on a new line after a blank line ; Fig. 1. The title compound with displacement ellipsoids drawn at the 50% probability level. H atoms are shown as spheres of arbitary radius. ; _publ_section_exptl_refinement # Some potentially useful phrases are donated by Bill Clegg: ; In the absence of significant anomalous scattering, Friedel pairs were merged. The absolute configuration was arbitrarily assigned. The relatively large ratio of minimum to maximum corrections applied in the multiscan process (1:nnn) reflect changes in the illuminated volume of the crystal. Changes in illuminated volume were kept to a minimum, and were taken into account (G\"orbitz, 1999) by the multi-scan inter-frame scaling (DENZO/SCALEPACK, Otwinowski & Minor, 1997). G\"orbitz, C. H. (1999). Acta Cryst. B55, 1090--1098. The H atoms were all located in a difference map, but those attached to carbon atoms were repositioned geometrically. The H atoms were initially refined with soft restraints on the bond lengths and angles to regularize their geometry (C---H in the range 0.93--0.98, N---H in the range 0.86--0.89 N---H to 0.86 O---H = 0.82 \%A) and U~iso~(H) (in the range 1.2--1.5 times U~eq~ of the parent atom), after which the positions were refined with riding constraints (Cooper et al., 2010). Cooper, R. I., Thompson, A. L. & Watkin, D. J. (2010). J. Appl. Cryst. 43, 1100--1107. ; _publ_section_exptl_prep # Brief details or a reference. Include solvent if known ; (type here to add preparation details) ; # Hand-made tables can be put in the cif. The number of columns # is set in the loop header. # The contants of each column can either be a piece of text # without any spaces (eg a number) or other text enclosed in " " # Remove the leading # in the following example #geom_extra_table_head_A #; #Table 2. #Molecular parameters deviating most from MOGUL averages #; # #loop_ #_geom_extra_tableA_col_1 #_geom_extra_tableA_col_2 #_geom_extra_tableA_col_3 #_geom_extra_tableA_col_4 # #Parameter "Observed Value" "MOGUL Value" "MOGUL e.s.d" #N5-C6-C4 129 124 "7 (\%)" #C3-O10-C2 105 109 "2 (\%)" #C6-O7 1.25 1.22 ".02 (\%A)" # data_VS_TCl_Sal _exptl_special_details ; The crystal was placed in the cold stream of an Oxford Cryosystems open-flow nitrogen cryostat (Cosier & Glazer, 1986) with a nominal stability of 0.1K. Cosier, J. & Glazer, A.M., 1986. J. Appl. Cryst. 105-107. ; _refine_special_details ? #--------------------------------------------------------------- # _oxford_ data items, April 2010: # There is some uncertainty about the correct way of forming local data # names, e.g. # _atom_site_special_shape_oxford # or # _oxford_atom_site_special_shape # see: # http://www.iucr.org/resources/cif/spec/version1.1/semantics#namespace # A reserved prefix, e.g. foo, must be used in the following way # " If the data file contains items defined in a DDL1 dictionary, the # local data names assigned under the reserved prefix must contain it as # their first component, e.g. _foo_atom_site_my_item. " # However, this seems to say the opposite: # http://www.iucr.org/__data/iucr/cif/standard/cifstd8.html # According to advice from the IUCr, CRYSTALS is correct #--------------------------------------------------------------- # End of 'script/refcif.dat' #end of refcif _cell_length_a 20.0561(5) _cell_length_b 19.5073(2) _cell_length_c 9.6398(2) _cell_angle_alpha 90 _cell_angle_beta 130.671(4) _cell_angle_gamma 90 _cell_volume 2860.5(2) _symmetry_cell_setting monoclinic _symmetry_space_group_name_H-M 'P 1 21/c 1 ' _symmetry_space_group_name_Hall '-P 2ybc' loop_ _symmetry_equiv_pos_as_xyz 'x,y,z' '-x,-y,-z' '-x,y+1/2,-z+1/2' 'x,-y+1/2,z+1/2' loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source C 0.0181 0.0091 2.3100 20.8439 1.0200 10.2075 1.5886 0.5687 0.8650 51.6512 0.2156 'International Tables Vol C 4.2.6.8 and 6.1.1.4' H 0.0000 0.0000 0.4930 10.5109 0.3229 26.1257 0.1402 3.1424 0.0408 57.7998 0.0030 'International Tables Vol C 4.2.6.8 and 6.1.1.4' N 0.0311 0.0180 12.2126 0.0057 3.1322 9.8933 2.0125 28.9975 1.1663 0.5826 -11.5290 'International Tables Vol C 4.2.6.8 and 6.1.1.4' O 0.0492 0.0322 3.0485 13.2771 2.2868 5.7011 1.5463 0.3239 0.8670 32.9089 0.2508 'International Tables Vol C 4.2.6.8 and 6.1.1.4' Cl 0.3639 0.7018 11.4604 0.0104 7.1964 1.1662 6.2556 18.5194 1.6455 47.7784 -9.5574 'International Tables Vol C 4.2.6.8 and 6.1.1.4' _cell_formula_units_Z 4 # Given Formula = C32 H35 Cl1 N1 O6 # Dc = 1.31 Fooo = 1200.00 Mu = 15.57 M = 565.09 # Found Formula = C32 H36 Cl1 N1 O6 # Dc = 1.31 FOOO = 1200.00 Mu = 15.57 M = 566.09 _chemical_formula_sum 'C32 H36 Cl1 N1 O6' _chemical_formula_moiety 'C25 H30 N O3, C7 H6 O3, Cl' _chemical_compound_source ? _chemical_formula_weight 566.09 _cell_measurement_reflns_used 11467 _cell_measurement_theta_min 5 _cell_measurement_theta_max 76 _cell_measurement_temperature 180 _exptl_crystal_description 'plate' _exptl_crystal_colour 'colourless' _exptl_crystal_size_min 0.065 _exptl_crystal_size_mid 0.370 _exptl_crystal_size_max 0.611 _exptl_crystal_density_diffrn 1.314 _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' # Non-dispersive F(000): _exptl_crystal_F_000 1200 _exptl_absorpt_coefficient_mu 1.557 # Sheldrick geometric approximatio 0.56 0.90 _exptl_absorpt_correction_type analytical _exptl_absorpt_process_details ; Analytical Absorption (De Meulenaer & Tompa, 1965) ; _exptl_absorpt_correction_T_min 0.55 _exptl_absorpt_correction_T_max 0.90 _diffrn_measurement_device_type 'Oxford Diffraction XCALIBUR' _diffrn_measurement_device 'Area' _diffrn_radiation_monochromator 'graphite' _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_measurement_method \w # If a reference occurs more than once, delete the author # and date from subsequent references. _computing_data_collection 'Xcalibur, (Oxford Diffraction, 2002)' _computing_cell_refinement 'CrysAlis, (Oxford Diffraction, 2002)' _computing_data_reduction 'CrysAlis, (Oxford Diffraction, 2002)' _computing_structure_solution 'SIR92 (Altomare et al., 1994)' _computing_structure_refinement 'CRYSTALS (Betteridge et al., 2003)' _computing_publication_material 'CRYSTALS (Betteridge et al., 2003)' _computing_molecular_graphics 'CAMERON (Watkin et al., 1996)' _diffrn_standards_interval_time . _diffrn_standards_interval_count . _diffrn_standards_number 0 _diffrn_standards_decay_% ? _diffrn_ambient_temperature 180 _diffrn_ambient_pressure 101 _diffrn_reflns_number 24852 _reflns_number_total 5881 _diffrn_reflns_av_R_equivalents 0.038 # Number of reflections without Friedels Law is 0 # Number of reflections with Friedels Law is 5881 # Theoretical number of reflections is about 12023 _diffrn_reflns_theta_min 4.533 _diffrn_reflns_theta_max 76.504 _diffrn_measured_fraction_theta_max 0.979 _diffrn_reflns_theta_full 71.149 _diffrn_measured_fraction_theta_full 0.997 _diffrn_reflns_limit_h_min -25 _diffrn_reflns_limit_h_max 21 _diffrn_reflns_limit_k_min -24 _diffrn_reflns_limit_k_max 24 _diffrn_reflns_limit_l_min -6 _diffrn_reflns_limit_l_max 11 _reflns_limit_h_min -25 _reflns_limit_h_max 19 _reflns_limit_k_min 0 _reflns_limit_k_max 24 _reflns_limit_l_min 0 _reflns_limit_l_max 11 _oxford_diffrn_Wilson_B_factor 3.47 _oxford_diffrn_Wilson_scale 0.08 _atom_sites_solution_primary direct #heavy,direct,difmap,geom # _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens difmap _refine_diff_density_min -0.27 _refine_diff_density_max 0.25 # The current dictionary definitions do not cover the # situation where the reflections used for refinement were # selected by a user-defined sigma threshold # The values actually used during refinement _oxford_reflns_threshold_expression_ref I>0.0\s(I) _refine_ls_number_reflns 5862 _refine_ls_number_restraints 0 _refine_ls_number_parameters 361 _oxford_refine_ls_R_factor_ref 0.0551 _refine_ls_wR_factor_ref 0.1292 _refine_ls_goodness_of_fit_ref 0.9703 _refine_ls_shift/su_max 0.0076071 _refine_ls_shift/su_mean 0.0008400 # The values computed with all filters except I/sigma _oxford_reflns_number_all 5863 _refine_ls_R_factor_all 0.0551 _refine_ls_wR_factor_all 0.1292 # The values computed with a 2 sigma cutoff - a la SHELX _reflns_threshold_expression I>2.0\s(I) _reflns_number_gt 4810 _refine_ls_R_factor_gt 0.0449 _refine_ls_wR_factor_gt 0.1108 # choose from: rm (reference molecule of known chirality), # ad (anomolous dispersion - Flack), rmad (rm and ad), # syn (from synthesis), unk (unknown) or . (not applicable). _chemical_absolute_configuration . _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_hydrogen_treatment constr #undef, noref, refall, # refxyz, refU, constr or mixed _refine_ls_weighting_scheme calc _refine_ls_weighting_details ; Method, part 1, Chebychev polynomial, (Watkin, 1994, Prince, 1982) [weight] = 1.0/[A~0~*T~0~(x)+A~1~*T~1~(x) ... +A~n-1~]*T~n-1~(x)] where A~i~ are the Chebychev coefficients listed below and x= Fcalc/Fmax Method = Robust Weighting (Prince, 1982) W = [weight] * [1-(deltaF/6*sigmaF)^2^]^2^ A~i~ are: 0.212E+04 0.354E+04 0.211E+04 829. 168. ; # Insert your own references if required - in alphabetical order _publ_section_references ; Altomare, A., Cascarano, G., Giacovazzo, C., Guagliardi, A., Burla, M. C., Polidori, G. & Camalli, M. (1994). J. Appl. Cryst. 27, 435--?. Betteridge, P. W., Carruthers, J. R., Cooper, R. I., Prout, K. & Watkin, D. J. (2003). J. Appl. Cryst. 36, 1487--?. De Meulenaer, J. & Tompa, H. (1965). Acta Cryst. 19, 1014--?. Oxford Diffraction, (2010). CrysAlis PRO. Oxford Diffraction, (2002). Xcalibur User Manual. Prince, E. Mathematical Techniques in Crystallography and Materials Science Springer-Verlag, New York, 1982. Watkin, D. J. (1994). Acta Cryst. A50, 411--437. Watkin, D. J., Prout, C. K. & Pearce, L. J. (1996). CAMERON, Chemical Crystallography Laboratory, Oxford, UK. ; # Uequiv = arithmetic mean of Ui i.e. Ueqiv = (U1+U2+U3)/3 # Replace last . with number of unfound hydrogen atoms attached to an atom. # ..._refinement_flags_... # . no refinement constraints S special position constraint on site # G rigid group refinement of site R riding atom # D distance or angle restraint on site T thermal displacement constraints # U Uiso or Uij restraint (rigid bond) P partial occupancy constraint loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_occupancy _atom_site_adp_type _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group _atom_site_attached_hydrogens C30 C 0.20800(13) 0.35654(10) -0.4471(3) 0.0439 1.0000 Uani . . . . . . C31 C 0.12571(14) 0.38374(11) -0.5932(3) 0.0498 1.0000 Uani . . . . . . C32 C 0.05620(15) 0.37740(12) -0.5932(3) 0.0567 1.0000 Uani . . . . . . C33 C 0.06821(15) 0.34384(13) -0.4537(4) 0.0600 1.0000 Uani . . . . . . C34 C 0.14908(16) 0.31554(14) -0.3096(3) 0.0600 1.0000 Uani . . . . . . C35 C 0.21835(14) 0.32237(12) -0.3072(3) 0.0501 1.0000 Uani . . . . . . C36 C 0.28257(14) 0.36726(10) -0.4423(3) 0.0452 1.0000 Uani . . . . . . O37 O 0.35878(9) 0.34367(8) -0.2931(2) 0.0498 1.0000 Uani . . . . . . O38 O 0.27498(11) 0.39678(10) -0.5636(2) 0.0618 1.0000 Uani . . . . . . O39 O 0.11007(12) 0.41724(10) -0.7345(2) 0.0688 1.0000 Uani . . . . . . C1 C 0.70313(11) 0.44872(9) 0.2337(2) 0.0356 1.0000 Uani . . . . . . C2 C 0.75925(11) 0.39426(9) 0.2335(2) 0.0345 1.0000 Uani . . . . . . C3 C 0.79761(12) 0.42313(9) 0.1503(2) 0.0372 1.0000 Uani . . . . . . C4 C 0.79194(13) 0.38510(11) 0.0219(3) 0.0441 1.0000 Uani . . . . . . C5 C 0.82841(14) 0.40985(13) -0.0514(3) 0.0522 1.0000 Uani . . . . . . C6 C 0.86890(15) 0.47301(13) 0.0007(3) 0.0531 1.0000 Uani . . . . . . C7 C 0.87550(15) 0.51099(11) 0.1301(3) 0.0528 1.0000 Uani . . . . . . C8 C 0.84019(14) 0.48619(10) 0.2053(3) 0.0465 1.0000 Uani . . . . . . C9 C 0.83209(11) 0.36773(9) 0.4275(2) 0.0369 1.0000 Uani . . . . . . C10 C 0.85384(14) 0.29864(11) 0.4542(3) 0.0522 1.0000 Uani . . . . . . C11 C 0.92004(17) 0.27400(13) 0.6292(4) 0.0704 1.0000 Uani . . . . . . C12 C 0.96418(16) 0.31748(15) 0.7785(3) 0.0651 1.0000 Uani . . . . . . C13 C 0.94373(14) 0.38564(14) 0.7527(3) 0.0552 1.0000 Uani . . . . . . C14 C 0.87804(13) 0.41126(11) 0.5771(3) 0.0465 1.0000 Uani . . . . . . C15 C 0.60840(12) 0.46000(9) 0.3016(2) 0.0369 1.0000 Uani . . . . . . C16 C 0.62440(12) 0.45002(9) 0.4778(2) 0.0391 1.0000 Uani . . . . . . C17 C 0.59298(13) 0.38138(9) 0.4910(2) 0.0385 1.0000 Uani . . . . . . C18 C 0.63160(15) 0.31950(10) 0.4664(3) 0.0472 1.0000 Uani . . . . . . C19 C 0.56903(15) 0.30805(9) 0.2569(3) 0.0467 1.0000 Uani . . . . . . C20 C 0.49714(13) 0.36296(9) 0.1743(2) 0.0391 1.0000 Uani . . . . . . C21 C 0.52092(12) 0.43043(9) 0.1353(2) 0.0371 1.0000 Uani . . . . . . C22 C 0.43846(13) 0.43206(10) 0.3040(3) 0.0400 1.0000 Uani . . . . . . C23 C 0.34612(14) 0.40367(12) 0.1750(3) 0.0510 1.0000 Uani . . . . . . C24 C 0.35664(16) 0.32749(13) 0.2219(4) 0.0590 1.0000 Uani . . . . . . C25 C 0.45475(15) 0.31249(10) 0.3469(3) 0.0446 1.0000 Uani . . . . . . O1 O 0.67904(9) 0.42429(6) 0.32485(19) 0.0410 1.0000 Uani . . . . . . O2 O 0.68004(10) 0.50284(7) 0.1566(2) 0.0483 1.0000 Uani . . . . . . O3 O 0.70178(8) 0.33842(6) 0.12956(18) 0.0397 1.0000 Uani . . . . . . Cl1 Cl 0.51939(3) 0.38222(2) -0.23745(6) 0.0406 1.0000 Uani . . . . . . N1 N 0.49521(10) 0.37410(7) 0.3285(2) 0.0356 1.0000 Uani . . . . . . H151 H 0.6117 0.5082 0.2812 0.0432 1.0000 Uiso R . . . . . H212 H 0.5228 0.4223 0.0387 0.0453 1.0000 Uiso R . . . . . H211 H 0.4752 0.4631 0.0924 0.0442 1.0000 Uiso R . . . . . H201 H 0.4383 0.3463 0.0618 0.0472 1.0000 Uiso R . . . . . H171 H 0.6024 0.3788 0.6010 0.0464 1.0000 Uiso R . . . . . H162 H 0.5934 0.4864 0.4847 0.0472 1.0000 Uiso R . . . . . H161 H 0.6862 0.4556 0.5806 0.0475 1.0000 Uiso R . . . . . H182 H 0.6326 0.2796 0.5270 0.0561 1.0000 Uiso R . . . . . H181 H 0.6926 0.3305 0.5160 0.0578 1.0000 Uiso R . . . . . H191 H 0.5432 0.2626 0.2253 0.0559 1.0000 Uiso R . . . . . H192 H 0.6011 0.3134 0.2130 0.0553 1.0000 Uiso R . . . . . H221 H 0.4586 0.4414 0.4262 0.0481 1.0000 Uiso R . . . . . H222 H 0.4462 0.4740 0.2589 0.0468 1.0000 Uiso R . . . . . H231 H 0.3194 0.4104 0.0461 0.0623 1.0000 Uiso R . . . . . H232 H 0.3101 0.4272 0.1917 0.0616 1.0000 Uiso R . . . . . H241 H 0.3255 0.2995 0.1108 0.0717 1.0000 Uiso R . . . . . H242 H 0.3348 0.3158 0.2831 0.0721 1.0000 Uiso R . . . . . H251 H 0.4675 0.2713 0.3133 0.0543 1.0000 Uiso R . . . . . H252 H 0.4823 0.3100 0.4763 0.0534 1.0000 Uiso R . . . . . H101 H 0.8223 0.2683 0.3526 0.0634 1.0000 Uiso R . . . . . H111 H 0.9349 0.2262 0.6480 0.0860 1.0000 Uiso R . . . . . H121 H 1.0091 0.2994 0.8972 0.0789 1.0000 Uiso R . . . . . H131 H 0.9739 0.4156 0.8538 0.0676 1.0000 Uiso R . . . . . H141 H 0.8643 0.4587 0.5577 0.0561 1.0000 Uiso R . . . . . H41 H 0.7639 0.3419 -0.0140 0.0538 1.0000 Uiso R . . . . . H51 H 0.8246 0.3841 -0.1370 0.0624 1.0000 Uiso R . . . . . H61 H 0.8925 0.4898 -0.0503 0.0644 1.0000 Uiso R . . . . . H71 H 0.9033 0.5531 0.1687 0.0630 1.0000 Uiso R . . . . . H81 H 0.8461 0.5132 0.2942 0.0553 1.0000 Uiso R . . . . . H321 H 0.0017 0.3962 -0.6905 0.0690 1.0000 Uiso R . . . . . H331 H 0.0197 0.3397 -0.4583 0.0715 1.0000 Uiso R . . . . . H341 H 0.1565 0.2917 -0.2152 0.0715 1.0000 Uiso R . . . . . H351 H 0.2754 0.3031 -0.2075 0.0593 1.0000 Uiso R . . . . . H31 H 0.6562 0.3530 0.0310 0.0610 1.0000 Uiso R . . . . . H371 H 0.3999 0.3545 -0.2916 0.0743 1.0000 Uiso R . . . . . H391 H 0.1571 0.4133 -0.7157 0.1047 1.0000 Uiso R . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C30 0.0432(10) 0.0377(9) 0.0444(10) -0.0042(8) 0.0258(9) -0.0032(8) C31 0.0457(11) 0.0426(10) 0.0459(11) -0.0028(8) 0.0230(9) -0.0035(8) C32 0.0403(10) 0.0572(13) 0.0554(13) -0.0060(10) 0.0237(10) -0.0009(9) C33 0.0446(11) 0.0655(14) 0.0657(14) -0.0142(11) 0.0340(11) -0.0096(10) C34 0.0537(12) 0.0723(15) 0.0563(13) 0.0004(11) 0.0369(11) -0.0055(11) C35 0.0434(10) 0.0542(12) 0.0463(11) 0.0002(9) 0.0264(9) -0.0014(9) C36 0.0472(10) 0.0387(10) 0.0444(10) -0.0024(8) 0.0276(9) -0.0020(8) O37 0.0421(7) 0.0509(8) 0.0508(8) 0.0072(6) 0.0279(7) 0.0024(6) O38 0.0560(9) 0.0764(11) 0.0498(9) 0.0104(8) 0.0330(8) -0.0018(8) O39 0.0549(9) 0.0744(12) 0.0560(10) 0.0187(8) 0.0269(8) 0.0063(8) C1 0.0339(8) 0.0336(8) 0.0381(8) 0.0008(7) 0.0229(7) -0.0003(7) C2 0.0335(8) 0.0320(8) 0.0362(9) 0.0008(6) 0.0219(7) 0.0006(6) C3 0.0351(8) 0.0367(9) 0.0371(9) 0.0059(7) 0.0224(8) 0.0061(7) C4 0.0423(10) 0.0482(10) 0.0398(10) -0.0011(8) 0.0259(9) 0.0007(8) C5 0.0476(11) 0.0708(14) 0.0404(10) 0.0026(10) 0.0296(9) 0.0047(10) C6 0.0503(11) 0.0661(14) 0.0535(12) 0.0166(10) 0.0386(10) 0.0096(10) C7 0.0532(12) 0.0451(11) 0.0715(14) 0.0085(10) 0.0456(12) 0.0011(9) C8 0.0497(11) 0.0405(10) 0.0597(12) -0.0014(9) 0.0402(10) -0.0020(8) C9 0.0330(8) 0.0382(9) 0.0386(9) 0.0035(7) 0.0229(8) 0.0008(7) C10 0.0479(11) 0.0398(10) 0.0509(11) 0.0060(9) 0.0242(10) 0.0018(8) C11 0.0563(14) 0.0505(13) 0.0663(15) 0.0224(11) 0.0231(12) 0.0045(11) C12 0.0471(12) 0.0782(17) 0.0474(12) 0.0206(11) 0.0207(10) 0.0006(11) C13 0.0420(10) 0.0795(16) 0.0404(11) -0.0054(10) 0.0252(9) -0.0082(10) C14 0.0401(10) 0.0506(11) 0.0437(10) -0.0019(8) 0.0250(9) -0.0001(8) C15 0.0392(9) 0.0320(8) 0.0432(9) 0.0026(7) 0.0286(8) 0.0055(7) C16 0.0410(9) 0.0373(9) 0.0372(9) -0.0038(7) 0.0246(8) 0.0015(7) C17 0.0451(10) 0.0397(9) 0.0308(9) 0.0029(7) 0.0248(8) 0.0056(7) C18 0.0611(12) 0.0362(9) 0.0527(11) 0.0122(8) 0.0407(10) 0.0143(9) C19 0.0713(14) 0.0312(9) 0.0576(12) -0.0009(8) 0.0509(12) 0.0009(9) C20 0.0518(10) 0.0366(9) 0.0338(9) -0.0044(7) 0.0301(9) -0.0060(8) C21 0.0431(9) 0.0381(9) 0.0342(8) 0.0043(7) 0.0270(8) 0.0009(7) C22 0.0454(10) 0.0374(9) 0.0437(10) 0.0038(7) 0.0320(9) 0.0037(7) C23 0.0459(11) 0.0572(12) 0.0507(11) 0.0052(10) 0.0317(10) -0.0011(9) C24 0.0588(13) 0.0586(13) 0.0607(13) 0.0052(11) 0.0395(12) -0.0101(11) C25 0.0631(12) 0.0349(9) 0.0464(10) 0.0001(7) 0.0403(10) -0.0050(8) O1 0.0458(7) 0.0375(7) 0.0492(7) 0.0091(5) 0.0351(6) 0.0095(5) O2 0.0535(8) 0.0367(7) 0.0663(9) 0.0141(6) 0.0442(8) 0.0102(6) O3 0.0363(6) 0.0344(6) 0.0403(7) -0.0020(5) 0.0213(6) -0.0026(5) Cl1 0.0422(2) 0.0452(2) 0.0351(2) 0.00002(16) 0.0255(2) 0.00325(17) N1 0.0449(8) 0.0321(7) 0.0333(7) 0.0006(5) 0.0270(7) 0.0001(6) _refine_ls_extinction_method 'None' _oxford_refine_ls_scale 3.40(3) loop_ _geom_bond_atom_site_label_1 _geom_bond_site_symmetry_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag C30 . C31 . 1.400(3) yes C30 . C35 . 1.393(3) yes C30 . C36 . 1.480(3) yes C31 . C32 . 1.400(3) yes C31 . O39 . 1.350(3) yes C32 . C33 . 1.368(4) yes C32 . H321 . 0.935 no C33 . C34 . 1.389(4) yes C33 . H331 . 0.949 no C34 . C35 . 1.381(3) yes C34 . H341 . 0.944 no C35 . H351 . 0.971 no C36 . O37 . 1.324(2) yes C36 . O38 . 1.220(3) yes O37 . H371 . 0.841 no O39 . H391 . 0.839 no C1 . C2 . 1.549(2) yes C1 . O1 . 1.337(2) yes C1 . O2 . 1.197(2) yes C2 . C3 . 1.535(2) yes C2 . C9 . 1.529(2) yes C2 . O3 . 1.419(2) yes C3 . C4 . 1.383(3) yes C3 . C8 . 1.391(3) yes C4 . C5 . 1.394(3) yes C4 . H41 . 0.945 no C5 . C6 . 1.378(3) yes C5 . H51 . 0.926 no C6 . C7 . 1.381(3) yes C6 . H61 . 0.936 no C7 . C8 . 1.389(3) yes C7 . H71 . 0.924 no C8 . H81 . 0.945 no C9 . C10 . 1.388(3) yes C9 . C14 . 1.385(3) yes C10 . C11 . 1.386(3) yes C10 . H101 . 0.949 no C11 . C12 . 1.384(4) yes C11 . H111 . 0.959 no C12 . C13 . 1.366(4) yes C12 . H121 . 0.950 no C13 . C14 . 1.395(3) yes C13 . H131 . 0.942 no C14 . H141 . 0.949 no C15 . C16 . 1.521(2) yes C15 . C21 . 1.522(3) yes C15 . O1 . 1.459(2) yes C15 . H151 . 0.972 no C16 . C17 . 1.520(3) yes C16 . H162 . 0.973 no C16 . H161 . 0.964 no C17 . C18 . 1.534(3) yes C17 . N1 . 1.522(2) yes C17 . H171 . 0.950 no C18 . C19 . 1.549(3) yes C18 . H182 . 0.966 no C18 . H181 . 1.005 no C19 . C20 . 1.537(3) yes C19 . H191 . 0.970 no C19 . H192 . 0.980 no C20 . C21 . 1.528(2) yes C20 . N1 . 1.527(2) yes C20 . H201 . 1.003 no C21 . H212 . 0.969 no C21 . H211 . 0.961 no C22 . C23 . 1.510(3) yes C22 . N1 . 1.510(2) yes C22 . H221 . 0.982 no C22 . H222 . 0.985 no C23 . C24 . 1.527(3) yes C23 . H231 . 0.990 no C23 . H232 . 0.955 no C24 . C25 . 1.523(3) yes C24 . H241 . 0.982 no C24 . H242 . 0.964 no C25 . N1 . 1.524(2) yes C25 . H251 . 0.961 no C25 . H252 . 0.982 no O3 . H31 . 0.829 no loop_ _geom_angle_atom_site_label_1 _geom_angle_site_symmetry_1 _geom_angle_atom_site_label_2 _geom_angle_site_symmetry_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C31 . C30 . C35 . 119.3(2) yes C31 . C30 . C36 . 118.88(19) yes C35 . C30 . C36 . 121.80(18) yes C30 . C31 . C32 . 119.2(2) yes C30 . C31 . O39 . 123.0(2) yes C32 . C31 . O39 . 117.8(2) yes C31 . C32 . C33 . 120.3(2) yes C31 . C32 . H321 . 118.6 no C33 . C32 . H321 . 121.0 no C32 . C33 . C34 . 121.1(2) yes C32 . C33 . H331 . 118.4 no C34 . C33 . H331 . 120.5 no C33 . C34 . C35 . 119.0(2) yes C33 . C34 . H341 . 120.5 no C35 . C34 . H341 . 120.5 no C30 . C35 . C34 . 121.1(2) yes C30 . C35 . H351 . 118.7 no C34 . C35 . H351 . 120.2 no C30 . C36 . O37 . 114.37(18) yes C30 . C36 . O38 . 122.93(19) yes O37 . C36 . O38 . 122.7(2) yes C36 . O37 . H371 . 110.8 no C31 . O39 . H391 . 104.3 no C2 . C1 . O1 . 109.31(14) yes C2 . C1 . O2 . 126.27(17) yes O1 . C1 . O2 . 124.29(17) yes C1 . C2 . C3 . 111.16(14) yes C1 . C2 . C9 . 110.26(14) yes C3 . C2 . C9 . 111.00(14) yes C1 . C2 . O3 . 105.72(13) yes C3 . C2 . O3 . 111.47(14) yes C9 . C2 . O3 . 107.02(14) yes C2 . C3 . C4 . 119.60(17) yes C2 . C3 . C8 . 121.22(17) yes C4 . C3 . C8 . 119.16(18) yes C3 . C4 . C5 . 120.3(2) yes C3 . C4 . H41 . 119.3 no C5 . C4 . H41 . 120.5 no C4 . C5 . C6 . 120.3(2) yes C4 . C5 . H51 . 119.9 no C6 . C5 . H51 . 119.8 no C5 . C6 . C7 . 119.7(2) yes C5 . C6 . H61 . 120.0 no C7 . C6 . H61 . 120.2 no C6 . C7 . C8 . 120.2(2) yes C6 . C7 . H71 . 121.2 no C8 . C7 . H71 . 118.7 no C3 . C8 . C7 . 120.3(2) yes C3 . C8 . H81 . 121.4 no C7 . C8 . H81 . 118.3 no C2 . C9 . C10 . 119.30(17) yes C2 . C9 . C14 . 121.54(17) yes C10 . C9 . C14 . 119.15(18) yes C9 . C10 . C11 . 119.9(2) yes C9 . C10 . H101 . 119.7 no C11 . C10 . H101 . 120.4 no C10 . C11 . C12 . 120.7(2) yes C10 . C11 . H111 . 120.0 no C12 . C11 . H111 . 119.3 no C11 . C12 . C13 . 119.7(2) yes C11 . C12 . H121 . 119.1 no C13 . C12 . H121 . 121.2 no C12 . C13 . C14 . 120.3(2) yes C12 . C13 . H131 . 120.0 no C14 . C13 . H131 . 119.7 no C13 . C14 . C9 . 120.4(2) yes C13 . C14 . H141 . 120.8 no C9 . C14 . H141 . 118.8 no C16 . C15 . C21 . 112.79(15) yes C16 . C15 . O1 . 106.88(14) yes C21 . C15 . O1 . 108.54(14) yes C16 . C15 . H151 . 110.9 no C21 . C15 . H151 . 109.7 no O1 . C15 . H151 . 107.9 no C15 . C16 . C17 . 114.12(15) yes C15 . C16 . H162 . 107.6 no C17 . C16 . H162 . 108.6 no C15 . C16 . H161 . 109.1 no C17 . C16 . H161 . 109.9 no H162 . C16 . H161 . 107.3 no C16 . C17 . C18 . 113.69(16) yes C16 . C17 . N1 . 108.81(14) yes C18 . C17 . N1 . 102.07(15) yes C16 . C17 . H171 . 110.4 no C18 . C17 . H171 . 112.2 no N1 . C17 . H171 . 109.3 no C17 . C18 . C19 . 104.67(15) yes C17 . C18 . H182 . 110.8 no C19 . C18 . H182 . 110.6 no C17 . C18 . H181 . 109.8 no C19 . C18 . H181 . 110.6 no H182 . C18 . H181 . 110.2 no C18 . C19 . C20 . 105.32(14) yes C18 . C19 . H191 . 110.8 no C20 . C19 . H191 . 110.2 no C18 . C19 . H192 . 110.2 no C20 . C19 . H192 . 111.1 no H191 . C19 . H192 . 109.2 no C19 . C20 . C21 . 112.94(16) yes C19 . C20 . N1 . 101.83(14) yes C21 . C20 . N1 . 109.08(14) yes C19 . C20 . H201 . 112.3 no C21 . C20 . H201 . 110.4 no N1 . C20 . H201 . 109.9 no C20 . C21 . C15 . 113.43(15) yes C20 . C21 . H212 . 108.1 no C15 . C21 . H212 . 109.5 no C20 . C21 . H211 . 108.2 no C15 . C21 . H211 . 108.9 no H212 . C21 . H211 . 108.6 no C23 . C22 . N1 . 104.43(16) yes C23 . C22 . H221 . 112.3 no N1 . C22 . H221 . 105.9 no C23 . C22 . H222 . 113.8 no N1 . C22 . H222 . 111.7 no H221 . C22 . H222 . 108.4 no C22 . C23 . C24 . 104.74(18) yes C22 . C23 . H231 . 110.7 no C24 . C23 . H231 . 111.0 no C22 . C23 . H232 . 110.0 no C24 . C23 . H232 . 113.1 no H231 . C23 . H232 . 107.4 no C23 . C24 . C25 . 106.21(18) yes C23 . C24 . H241 . 110.6 no C25 . C24 . H241 . 109.3 no C23 . C24 . H242 . 112.4 no C25 . C24 . H242 . 109.8 no H241 . C24 . H242 . 108.5 no C24 . C25 . N1 . 105.54(16) yes C24 . C25 . H251 . 112.6 no N1 . C25 . H251 . 110.0 no C24 . C25 . H252 . 112.5 no N1 . C25 . H252 . 106.6 no H251 . C25 . H252 . 109.4 no C15 . O1 . C1 . 117.37(13) yes C2 . O3 . H31 . 109.1 no C20 . N1 . C25 . 110.75(13) yes C20 . N1 . C17 . 100.49(13) yes C25 . N1 . C17 . 112.37(14) yes C20 . N1 . C22 . 116.67(14) yes C25 . N1 . C22 . 101.81(14) yes C17 . N1 . C22 . 115.18(14) yes loop_ _geom_hbond_atom_site_label_D _geom_hbond_site_symmetry_D _geom_hbond_atom_site_label_H _geom_hbond_site_symmetry_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_angle_DHA _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_publ_flag C21 . H211 . O2 2_665 147 0.961 2.481 3.328(4) yes C18 . H182 . O3 4_555 139 0.966 2.532 3.326(4) yes C23 . H231 . O2 2_665 140 0.990 2.590 3.411(4) yes O39 . H391 . C36 . 121 0.839 2.333 2.855(4) yes O39 . H391 . O38 . 151 0.839 1.824 2.590(4) yes _iucr_refine_instruction_details_constraints ; # # Punched on 19/04/13 at 15:33:39 # #LIST 12 BLOCK SCALE X'S, U'S RIDE C ( 32,X'S) H ( 321,X'S) RIDE C ( 33,X'S) H ( 331,X'S) RIDE C ( 34,X'S) H ( 341,X'S) RIDE C ( 35,X'S) H ( 351,X'S) RIDE O ( 37,X'S) H ( 371,X'S) RIDE O ( 39,X'S) H ( 391,X'S) RIDE C ( 4,X'S) H ( 41,X'S) RIDE C ( 5,X'S) H ( 51,X'S) RIDE C ( 6,X'S) H ( 61,X'S) RIDE C ( 7,X'S) H ( 71,X'S) RIDE C ( 8,X'S) H ( 81,X'S) RIDE C ( 10,X'S) H ( 101,X'S) RIDE C ( 11,X'S) H ( 111,X'S) RIDE C ( 12,X'S) H ( 121,X'S) RIDE C ( 13,X'S) H ( 131,X'S) RIDE C ( 14,X'S) H ( 141,X'S) RIDE C ( 15,X'S) H ( 151,X'S) RIDE C ( 16,X'S) H ( 162,X'S) H ( 161,X'S) RIDE C ( 17,X'S) H ( 171,X'S) RIDE C ( 18,X'S) H ( 182,X'S) H ( 181,X'S) RIDE C ( 19,X'S) H ( 191,X'S) H ( 192,X'S) RIDE C ( 20,X'S) H ( 201,X'S) RIDE C ( 21,X'S) H ( 212,X'S) H ( 211,X'S) RIDE C ( 22,X'S) H ( 221,X'S) H ( 222,X'S) RIDE C ( 23,X'S) H ( 231,X'S) H ( 232,X'S) RIDE C ( 24,X'S) H ( 241,X'S) H ( 242,X'S) RIDE C ( 25,X'S) H ( 251,X'S) H ( 252,X'S) RIDE O ( 3,X'S) H ( 31,X'S) END ; _iucr_refine_instruction_details_restraints ; # # Punched on 19/04/13 at 15:33:39 # #LIST 16 NO REM HREST START (DO NOT REMOVE THIS LINE) REM HREST END (DO NOT REMOVE THIS LINE) END ; data_VS_TCl_Stav _exptl_special_details ; The crystal was placed in the cold stream of an Oxford Cryosystems open-flow nitrogen cryostat (Cosier & Glazer, 1986) with a nominal stability of 0.1K. Cosier, J. & Glazer, A.M., 1986. J. Appl. Cryst. 105-107. ; _refine_special_details ? #--------------------------------------------------------------- # _oxford_ data items, April 2010: # There is some uncertainty about the correct way of forming local data # names, e.g. # _atom_site_special_shape_oxford # or # _oxford_atom_site_special_shape # see: # http://www.iucr.org/resources/cif/spec/version1.1/semantics#namespace # A reserved prefix, e.g. foo, must be used in the following way # " If the data file contains items defined in a DDL1 dictionary, the # local data names assigned under the reserved prefix must contain it as # their first component, e.g. _foo_atom_site_my_item. " # However, this seems to say the opposite: # http://www.iucr.org/__data/iucr/cif/standard/cifstd8.html # According to advice from the IUCr, CRYSTALS is correct #--------------------------------------------------------------- # End of 'script/refcif.dat' #end of refcif _cell_length_a 43.4462(7) _cell_length_b 6.61949(10) _cell_length_c 16.5083(2) _cell_angle_alpha 90 _cell_angle_beta 99.7909(14) _cell_angle_gamma 90 _cell_volume 4678.51(12) _symmetry_cell_setting monoclinic _symmetry_space_group_name_H-M 'C 2/c' _symmetry_space_group_name_Hall '-C 2yc' loop_ _symmetry_equiv_pos_as_xyz 'x,y,z' '-x,-y,-z' 'x+1/2,y+1/2,z' '-x+1/2,-y+1/2,-z' 'x,-y,z+1/2' '-x,y,-z+1/2' 'x+1/2,-y+1/2,z+1/2' '-x+1/2,y+1/2,-z+1/2' loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source C 0.0181 0.0091 2.3100 20.8439 1.0200 10.2075 1.5886 0.5687 0.8650 51.6512 0.2156 'International Tables Vol C 4.2.6.8 and 6.1.1.4' H 0.0000 0.0000 0.4930 10.5109 0.3229 26.1257 0.1402 3.1424 0.0408 57.7998 0.0030 'International Tables Vol C 4.2.6.8 and 6.1.1.4' N 0.0311 0.0180 12.2126 0.0057 3.1322 9.8933 2.0125 28.9975 1.1663 0.5826 -11.5290 'International Tables Vol C 4.2.6.8 and 6.1.1.4' O 0.0492 0.0322 3.0485 13.2771 2.2868 5.7011 1.5463 0.3239 0.8670 32.9089 0.2508 'International Tables Vol C 4.2.6.8 and 6.1.1.4' Cl 0.3639 0.7018 11.4604 0.0104 7.1964 1.1662 6.2556 18.5194 1.6455 47.7784 -9.5574 'International Tables Vol C 4.2.6.8 and 6.1.1.4' _cell_formula_units_Z 4 # Given Formula = C52 Cl2 N2 O10 # Dc = 1.25 Fooo = 2008.00 Mu = 17.56 M = 441.74 # Found Formula = C52 H62 Cl2 N2 O10 # Dc = 1.34 FOOO = 2008.00 Mu = 17.60 M = 472.99 _chemical_formula_sum 'C52 H62 Cl2 N2 O10' _chemical_formula_moiety '2(C25 H30 N O3), C2 H2 O4, 2Cl' _chemical_compound_source ? _chemical_formula_weight 945.98 _cell_measurement_reflns_used 16642 _cell_measurement_theta_min 5 _cell_measurement_theta_max 77 _cell_measurement_temperature 190 _exptl_crystal_description 'plane' _exptl_crystal_colour 'colourless' _exptl_crystal_size_min 0.090 _exptl_crystal_size_mid 0.407 _exptl_crystal_size_max 0.533 _exptl_crystal_density_diffrn 1.343 _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' # Non-dispersive F(000): _exptl_crystal_F_000 2008 _exptl_absorpt_coefficient_mu 1.760 # Sheldrick geometric approximatio 0.49 0.85 _exptl_absorpt_correction_type analytical _exptl_absorpt_process_details ; Analytical Absorption (De Meulenaer & Tompa, 1965) ; _exptl_absorpt_correction_T_min 0.59 _exptl_absorpt_correction_T_max 0.85 _diffrn_measurement_device_type 'Oxford Diffraction XCALIBUR' _diffrn_measurement_device 'Area' _diffrn_radiation_monochromator 'graphite' _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_measurement_method '\f & \w scans' # If a reference occurs more than once, delete the author # and date from subsequent references. _computing_data_collection 'Xcalibur, (Oxford Diffraction, 2002)' _computing_cell_refinement 'CrysAlis, (Oxford Diffraction, 2002)' _computing_data_reduction 'XRED (Stoe & Cie 1996)' _computing_structure_solution 'SIR92 (Altomare et al., 1994)' _computing_structure_refinement 'CRYSTALS (Betteridge et al., 2003)' _computing_publication_material 'CRYSTALS (Betteridge et al., 2003)' _computing_molecular_graphics 'CAMERON (Watkin et al., 1996)' _diffrn_standards_interval_time . _diffrn_standards_interval_count . _diffrn_standards_number 0 _diffrn_standards_decay_% ? _diffrn_ambient_temperature 190 _diffrn_ambient_pressure 101 _diffrn_reflns_number 30810 _reflns_number_total 4939 _diffrn_reflns_av_R_equivalents 0.028 # Number of reflections without Friedels Law is 0 # Number of reflections with Friedels Law is 4939 # Theoretical number of reflections is about 9921 _diffrn_reflns_theta_min 5.439 _diffrn_reflns_theta_max 77.249 _diffrn_measured_fraction_theta_max 0.992 _diffrn_reflns_theta_full 75.704 _diffrn_measured_fraction_theta_full 0.997 _diffrn_reflns_limit_h_min -54 _diffrn_reflns_limit_h_max 54 _diffrn_reflns_limit_k_min -8 _diffrn_reflns_limit_k_max 8 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_limit_l_max 20 _reflns_limit_h_min -54 _reflns_limit_h_max 53 _reflns_limit_k_min 0 _reflns_limit_k_max 8 _reflns_limit_l_min 0 _reflns_limit_l_max 20 _oxford_diffrn_Wilson_B_factor 3.36 _oxford_diffrn_Wilson_scale 0.07 _atom_sites_solution_primary direct #heavy,direct,difmap,geom # _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens difmap _refine_diff_density_min -0.29 _refine_diff_density_max 0.26 # The current dictionary definitions do not cover the # situation where the reflections used for refinement were # selected by a user-defined sigma threshold # The values actually used during refinement _oxford_reflns_threshold_expression_ref I>-10.0\s(I) _refine_ls_number_reflns 4939 _refine_ls_number_restraints 0 _refine_ls_number_parameters 298 _oxford_refine_ls_R_factor_ref 0.0428 _refine_ls_wR_factor_ref 0.1221 _refine_ls_goodness_of_fit_ref 0.9214 _refine_ls_shift/su_max 0.0014079 _refine_ls_shift/su_mean 0.0000612 # The values computed with all filters except I/sigma _oxford_reflns_number_all 4939 _refine_ls_R_factor_all 0.0428 _refine_ls_wR_factor_all 0.1221 # The values computed with a 2 sigma cutoff - a la SHELX _reflns_threshold_expression I>2.0\s(I) _reflns_number_gt 4512 _refine_ls_R_factor_gt 0.0403 _refine_ls_wR_factor_gt 0.1174 # choose from: rm (reference molecule of known chirality), # ad (anomolous dispersion - Flack), rmad (rm and ad), # syn (from synthesis), unk (unknown) or . (not applicable). _chemical_absolute_configuration . _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_hydrogen_treatment constr #undef, noref, refall, # refxyz, refU, constr or mixed _refine_ls_weighting_scheme calc _refine_ls_weighting_details ; Method= Modified Sheldrick w=1/[\s^2^(F^2^) + ( 0.10P)^2^ + 1.58P] ,where P=(max(Fo^2^,0) + 2Fc^2^)/3 ; # Insert your own references if required - in alphabetical order _publ_section_references ; Altomare, A., Cascarano, G., Giacovazzo, C., Guagliardi, A., Burla, M.C., Polidori, G. & Camalli, M. (1994). J. Appl. Cryst. 27, 435. Betteridge, P.W., Carruthers, J.R., Cooper, R.I., Prout, K. & Watkin, D.J. (2003). J. Appl. Cryst. 36, 1487. De Meulenaer, J. & Tompa, H. (1965). Acta Cryst. 19, 1014. Oxford Diffraction, (2010). CrysAlisPro. Oxford Diffraction, (2002). Xcalibur User Manual. Stoe & Cie (1996). IPDS Software. Watkin, D.J., Prout, C.K. & Pearce, L.J. (1996). CAMERON, Chemical Crystallography Laboratory, Oxford, UK. ; # Uequiv = arithmetic mean of Ui i.e. Ueqiv = (U1+U2+U3)/3 # Replace last . with number of unfound hydrogen atoms attached to an atom. # ..._refinement_flags_... # . no refinement constraints S special position constraint on site # G rigid group refinement of site R riding atom # D distance or angle restraint on site T thermal displacement constraints # U Uiso or Uij restraint (rigid bond) P partial occupancy constraint loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_occupancy _atom_site_adp_type _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group _atom_site_attached_hydrogens C1 C 0.36059(3) 0.56260(19) 0.30403(7) 0.0325 1.0000 Uani . . . . . . C2 C 0.33771(3) 0.74200(18) 0.30214(7) 0.0314 1.0000 Uani . . . . . . C3 C 0.32806(2) 0.77043(18) 0.38669(7) 0.0320 1.0000 Uani . . . . . . C4 C 0.31219(3) 0.6173(2) 0.42041(7) 0.0383 1.0000 Uani . . . . . . C5 C 0.30226(3) 0.6438(2) 0.49528(8) 0.0432 1.0000 Uani . . . . . . C6 C 0.30809(3) 0.8241(2) 0.53701(8) 0.0445 1.0000 Uani . . . . . . C7 C 0.32372(3) 0.9779(2) 0.50429(8) 0.0427 1.0000 Uani . . . . . . C8 C 0.33376(3) 0.9517(2) 0.42902(7) 0.0372 1.0000 Uani . . . . . . C9 C 0.30832(3) 0.6935(2) 0.23921(7) 0.0352 1.0000 Uani . . . . . . C10 C 0.29677(4) 0.4982(2) 0.22601(9) 0.0465 1.0000 Uani . . . . . . C11 C 0.26842(4) 0.4654(3) 0.17387(10) 0.0573 1.0000 Uani . . . . . . C12 C 0.25200(3) 0.6254(4) 0.13376(9) 0.0616 1.0000 Uani . . . . . . C13 C 0.26368(4) 0.8172(3) 0.14627(10) 0.0625 1.0000 Uani . . . . . . C14 C 0.29158(3) 0.8530(3) 0.19954(9) 0.0480 1.0000 Uani . . . . . . C15 C 0.40095(3) 0.4277(2) 0.23754(7) 0.0370 1.0000 Uani . . . . . . C16 C 0.43013(3) 0.5352(2) 0.22047(8) 0.0402 1.0000 Uani . . . . . . C17 C 0.42768(3) 0.60570(19) 0.13141(7) 0.0361 1.0000 Uani . . . . . . C18 C 0.39891(3) 0.73860(19) 0.10280(8) 0.0408 1.0000 Uani . . . . . . C19 C 0.37252(3) 0.5894(2) 0.06856(8) 0.0384 1.0000 Uani . . . . . . C20 C 0.38732(3) 0.38007(18) 0.08168(7) 0.0336 1.0000 Uani . . . . . . C21 C 0.38660(3) 0.29143(18) 0.16684(8) 0.0371 1.0000 Uani . . . . . . C22 C 0.44320(3) 0.2491(2) 0.08939(8) 0.0391 1.0000 Uani . . . . . . C23 C 0.47194(3) 0.3187(3) 0.05592(10) 0.0529 1.0000 Uani . . . . . . C24 C 0.45954(4) 0.4667(3) -0.01305(10) 0.0503 1.0000 Uani . . . . . . C25 C 0.42454(3) 0.4815(2) -0.01337(8) 0.0405 1.0000 Uani . . . . . . C30 C 0.49141(3) 0.9202(2) 0.28692(8) 0.0431 1.0000 Uani . . . . . . O31 O 0.46568(3) 1.02366(18) 0.27326(7) 0.0545 1.0000 Uani . . . . . . O32 O 0.50081(3) 0.8260(3) 0.34764(9) 0.0846 1.0000 Uani . . . . . . O1 O 0.37880(2) 0.58812(14) 0.24799(5) 0.0402 1.0000 Uani . . . . . . O2 O 0.36138(3) 0.41763(17) 0.34808(6) 0.0508 1.0000 Uani . . . . . . O3 O 0.35093(2) 0.91972(13) 0.27513(5) 0.0369 1.0000 Uani . . . . . . N1 N 0.42092(2) 0.42465(15) 0.07383(6) 0.0312 1.0000 Uani . . . . . . Cl1 Cl 0.419721(7) 0.99657(5) 0.382930(19) 0.0437 1.0000 Uani . . . . . . H41 H 0.3072 0.4944 0.3923 0.0476 1.0000 Uiso R . . . . . H51 H 0.2918 0.5385 0.5187 0.0535 1.0000 Uiso R . . . . . H61 H 0.3015 0.8466 0.5880 0.0536 1.0000 Uiso R . . . . . H71 H 0.3277 1.0958 0.5344 0.0525 1.0000 Uiso R . . . . . H81 H 0.3443 1.0530 0.4058 0.0444 1.0000 Uiso R . . . . . H101 H 0.3078 0.3871 0.2524 0.0559 1.0000 Uiso R . . . . . H111 H 0.2601 0.3369 0.1649 0.0694 1.0000 Uiso R . . . . . H121 H 0.2331 0.6015 0.0981 0.0740 1.0000 Uiso R . . . . . H131 H 0.2527 0.9272 0.1184 0.0761 1.0000 Uiso R . . . . . H141 H 0.2989 0.9873 0.2089 0.0570 1.0000 Uiso R . . . . . H151 H 0.4055 0.3503 0.2883 0.0442 1.0000 Uiso R . . . . . H161 H 0.4481 0.4471 0.2348 0.0486 1.0000 Uiso R . . . . . H162 H 0.4334 0.6511 0.2556 0.0480 1.0000 Uiso R . . . . . H171 H 0.4473 0.6736 0.1219 0.0444 1.0000 Uiso R . . . . . H201 H 0.3785 0.2862 0.0395 0.0402 1.0000 Uiso R . . . . . H212 H 0.3971 0.1573 0.1712 0.0462 1.0000 Uiso R . . . . . H211 H 0.3649 0.2660 0.1721 0.0456 1.0000 Uiso R . . . . . H192 H 0.3656 0.6155 0.0108 0.0445 1.0000 Uiso R . . . . . H191 H 0.3547 0.6010 0.0981 0.0467 1.0000 Uiso R . . . . . H182 H 0.4022 0.8337 0.0609 0.0499 1.0000 Uiso R . . . . . H181 H 0.3939 0.8106 0.1497 0.0494 1.0000 Uiso R . . . . . H221 H 0.4475 0.2043 0.1471 0.0452 1.0000 Uiso R . . . . . H222 H 0.4329 0.1387 0.0574 0.0465 1.0000 Uiso R . . . . . H231 H 0.4867 0.3849 0.0986 0.0622 1.0000 Uiso R . . . . . H232 H 0.4820 0.2024 0.0363 0.0642 1.0000 Uiso R . . . . . H241 H 0.4691 0.5975 -0.0028 0.0605 1.0000 Uiso R . . . . . H242 H 0.4638 0.4164 -0.0672 0.0623 1.0000 Uiso R . . . . . H252 H 0.4156 0.6143 -0.0285 0.0465 1.0000 Uiso R . . . . . H251 H 0.4135 0.3785 -0.0497 0.0497 1.0000 Uiso R . . . . . H31 H 0.3689 0.9429 0.3045 0.0581 1.0000 Uiso R . . . . . H311 H 0.4547 1.0102 0.3133 0.0834 1.0000 Uiso R . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.0316(5) 0.0380(6) 0.0278(5) -0.0016(4) 0.0050(4) -0.0007(4) C2 0.0304(5) 0.0351(6) 0.0291(5) 0.0010(4) 0.0061(4) 0.0001(4) C3 0.0278(5) 0.0396(6) 0.0280(5) -0.0009(4) 0.0030(4) 0.0025(4) C4 0.0382(6) 0.0447(6) 0.0329(6) -0.0033(5) 0.0088(4) -0.0042(5) C5 0.0414(6) 0.0540(8) 0.0366(6) -0.0003(5) 0.0131(5) -0.0031(6) C6 0.0412(6) 0.0614(8) 0.0321(5) -0.0061(5) 0.0096(5) 0.0055(6) C7 0.0409(6) 0.0473(7) 0.0395(6) -0.0122(5) 0.0054(5) 0.0030(5) C8 0.0342(6) 0.0403(6) 0.0364(6) -0.0028(5) 0.0039(4) 0.0022(5) C9 0.0304(5) 0.0501(7) 0.0258(5) -0.0021(4) 0.0069(4) -0.0002(5) C10 0.0421(7) 0.0538(8) 0.0425(7) -0.0119(6) 0.0039(6) -0.0035(5) C11 0.0432(8) 0.0792(11) 0.0492(8) -0.0244(7) 0.0073(6) -0.0133(7) C12 0.0322(6) 0.1118(15) 0.0390(7) -0.0111(8) 0.0013(5) -0.0045(8) C13 0.0383(7) 0.0928(13) 0.0521(8) 0.0149(8) -0.0049(6) 0.0052(8) C14 0.0374(6) 0.0613(9) 0.0437(7) 0.0101(6) 0.0022(5) 0.0015(6) C15 0.0387(6) 0.0392(6) 0.0346(5) 0.0025(5) 0.0102(5) 0.0083(5) C16 0.0333(6) 0.0502(7) 0.0364(6) -0.0099(5) 0.0042(5) -0.0004(5) C17 0.0350(5) 0.0342(6) 0.0407(6) -0.0076(5) 0.0107(4) -0.0075(4) C18 0.0491(7) 0.0296(6) 0.0469(6) 0.0004(5) 0.0173(5) 0.0002(5) C19 0.0359(6) 0.0419(6) 0.0377(6) 0.0043(5) 0.0068(5) 0.0054(5) C20 0.0297(5) 0.0349(6) 0.0364(5) -0.0044(4) 0.0061(4) -0.0053(4) C21 0.0380(6) 0.0313(5) 0.0446(6) 0.0018(5) 0.0145(5) -0.0024(4) C22 0.0386(6) 0.0394(6) 0.0407(6) -0.0003(5) 0.0108(5) 0.0061(5) C23 0.0390(7) 0.0639(9) 0.0591(8) -0.0010(7) 0.0174(6) 0.0060(6) C24 0.0481(8) 0.0571(8) 0.0517(8) -0.0011(6) 0.0251(6) -0.0034(6) C25 0.0462(7) 0.0427(7) 0.0351(6) 0.0014(5) 0.0142(5) -0.0001(5) C30 0.0317(6) 0.0474(7) 0.0494(7) 0.0055(6) 0.0043(5) 0.0016(5) O31 0.0467(6) 0.0663(7) 0.0533(6) 0.0186(5) 0.0162(5) 0.0186(5) O32 0.0547(7) 0.1263(13) 0.0765(8) 0.0491(9) 0.0217(6) 0.0397(8) O1 0.0454(5) 0.0410(5) 0.0384(4) 0.0037(3) 0.0188(4) 0.0094(4) O2 0.0566(6) 0.0493(6) 0.0521(5) 0.0176(4) 0.0252(5) 0.0149(5) O3 0.0350(4) 0.0379(4) 0.0383(4) 0.0052(3) 0.0074(3) -0.0015(3) N1 0.0308(5) 0.0316(5) 0.0324(4) -0.0022(4) 0.0083(3) -0.0025(4) Cl1 0.03976(19) 0.0454(2) 0.04609(19) 0.00483(12) 0.00739(13) 0.00472(11) _refine_ls_extinction_method 'None' _oxford_refine_ls_scale 2.22(2) loop_ _geom_bond_atom_site_label_1 _geom_bond_site_symmetry_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag C1 . C2 . 1.5454(16) yes C1 . O1 . 1.3264(14) yes C1 . O2 . 1.2010(16) yes C2 . C3 . 1.5357(14) yes C2 . C9 . 1.5371(15) yes C2 . O3 . 1.4141(14) yes C3 . C4 . 1.3941(17) yes C3 . C8 . 1.3896(17) yes C4 . C5 . 1.3880(17) yes C4 . H41 . 0.943 no C5 . C6 . 1.380(2) yes C5 . H51 . 0.950 no C6 . C7 . 1.383(2) yes C6 . H61 . 0.945 no C7 . C8 . 1.3960(18) yes C7 . H71 . 0.926 no C8 . H81 . 0.931 no C9 . C10 . 1.3905(19) yes C9 . C14 . 1.3818(19) yes C10 . C11 . 1.394(2) yes C10 . H101 . 0.943 no C11 . C12 . 1.381(3) yes C11 . H111 . 0.926 no C12 . C13 . 1.370(3) yes C12 . H121 . 0.939 no C13 . C14 . 1.391(2) yes C13 . H131 . 0.946 no C14 . H141 . 0.948 no C15 . C16 . 1.5212(18) yes C15 . C21 . 1.5223(18) yes C15 . O1 . 1.4627(14) yes C15 . H151 . 0.974 no C16 . C17 . 1.5288(18) yes C16 . H161 . 0.971 no C16 . H162 . 0.958 no C17 . C18 . 1.5356(18) yes C17 . N1 . 1.5268(14) yes C17 . H171 . 1.001 no C18 . C19 . 1.5455(18) yes C18 . H182 . 0.964 no C18 . H181 . 0.965 no C19 . C20 . 1.5277(17) yes C19 . H192 . 0.966 no C19 . H191 . 0.985 no C20 . C21 . 1.5286(16) yes C20 . N1 . 1.5162(14) yes C20 . H201 . 0.962 no C21 . H212 . 0.996 no C21 . H211 . 0.976 no C22 . C23 . 1.5204(19) yes C22 . N1 . 1.5065(15) yes C22 . H221 . 0.984 no C22 . H222 . 0.965 no C23 . C24 . 1.529(2) yes C23 . H231 . 0.974 no C23 . H232 . 0.967 no C24 . C25 . 1.523(2) yes C24 . H241 . 0.962 no C24 . H242 . 1.001 no C25 . N1 . 1.5219(15) yes C25 . H252 . 0.976 no C25 . H251 . 0.978 no C30 . C30 6_655 1.534(3) yes C30 . O31 . 1.2977(17) yes C30 . O32 . 1.1920(19) yes O31 . H311 . 0.883 no O3 . H31 . 0.858 no loop_ _geom_angle_atom_site_label_1 _geom_angle_site_symmetry_1 _geom_angle_atom_site_label_2 _geom_angle_site_symmetry_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C2 . C1 . O1 . 110.23(10) yes C2 . C1 . O2 . 125.33(10) yes O1 . C1 . O2 . 124.41(11) yes C1 . C2 . C3 . 110.48(9) yes C1 . C2 . C9 . 108.10(9) yes C3 . C2 . C9 . 108.42(9) yes C1 . C2 . O3 . 110.57(9) yes C3 . C2 . O3 . 111.90(9) yes C9 . C2 . O3 . 107.21(9) yes C2 . C3 . C4 . 120.25(10) yes C2 . C3 . C8 . 120.67(11) yes C4 . C3 . C8 . 119.02(11) yes C3 . C4 . C5 . 120.89(12) yes C3 . C4 . H41 . 121.2 no C5 . C4 . H41 . 117.9 no C4 . C5 . C6 . 119.70(13) yes C4 . C5 . H51 . 120.9 no C6 . C5 . H51 . 119.4 no C5 . C6 . C7 . 120.15(11) yes C5 . C6 . H61 . 121.5 no C7 . C6 . H61 . 118.3 no C6 . C7 . C8 . 120.31(12) yes C6 . C7 . H71 . 118.1 no C8 . C7 . H71 . 121.6 no C7 . C8 . C3 . 119.93(12) yes C7 . C8 . H81 . 121.9 no C3 . C8 . H81 . 118.2 no C2 . C9 . C10 . 122.43(12) yes C2 . C9 . C14 . 118.07(12) yes C10 . C9 . C14 . 119.29(12) yes C9 . C10 . C11 . 119.93(15) yes C9 . C10 . H101 . 120.8 no C11 . C10 . H101 . 119.3 no C10 . C11 . C12 . 120.42(17) yes C10 . C11 . H111 . 121.4 no C12 . C11 . H111 . 118.2 no C11 . C12 . C13 . 119.37(14) yes C11 . C12 . H121 . 119.8 no C13 . C12 . H121 . 120.8 no C12 . C13 . C14 . 120.90(17) yes C12 . C13 . H131 . 119.8 no C14 . C13 . H131 . 119.3 no C13 . C14 . C9 . 120.07(16) yes C13 . C14 . H141 . 119.7 no C9 . C14 . H141 . 120.2 no C16 . C15 . C21 . 112.38(10) yes C16 . C15 . O1 . 105.55(10) yes C21 . C15 . O1 . 109.20(10) yes C16 . C15 . H151 . 110.5 no C21 . C15 . H151 . 110.2 no O1 . C15 . H151 . 108.8 no C15 . C16 . C17 . 113.39(10) yes C15 . C16 . H161 . 109.6 no C17 . C16 . H161 . 109.8 no C15 . C16 . H162 . 107.8 no C17 . C16 . H162 . 108.5 no H161 . C16 . H162 . 107.6 no C16 . C17 . C18 . 112.99(10) yes C16 . C17 . N1 . 109.50(10) yes C18 . C17 . N1 . 101.41(9) yes C16 . C17 . H171 . 111.5 no C18 . C17 . H171 . 111.5 no N1 . C17 . H171 . 109.5 no C17 . C18 . C19 . 105.12(10) yes C17 . C18 . H182 . 112.5 no C19 . C18 . H182 . 110.3 no C17 . C18 . H181 . 108.5 no C19 . C18 . H181 . 110.8 no H182 . C18 . H181 . 109.5 no C18 . C19 . C20 . 105.04(10) yes C18 . C19 . H192 . 109.6 no C20 . C19 . H192 . 110.8 no C18 . C19 . H191 . 111.5 no C20 . C19 . H191 . 110.3 no H192 . C19 . H191 . 109.5 no C19 . C20 . C21 . 113.87(10) yes C19 . C20 . N1 . 101.50(9) yes C21 . C20 . N1 . 108.89(9) yes C19 . C20 . H201 . 112.2 no C21 . C20 . H201 . 110.5 no N1 . C20 . H201 . 109.5 no C20 . C21 . C15 . 114.07(10) yes C20 . C21 . H212 . 109.1 no C15 . C21 . H212 . 110.5 no C20 . C21 . H211 . 108.6 no C15 . C21 . H211 . 108.0 no H212 . C21 . H211 . 106.2 no C23 . C22 . N1 . 104.36(11) yes C23 . C22 . H221 . 114.2 no N1 . C22 . H221 . 114.1 no C23 . C22 . H222 . 111.3 no N1 . C22 . H222 . 105.4 no H221 . C22 . H222 . 107.2 no C22 . C23 . C24 . 104.93(11) yes C22 . C23 . H231 . 110.8 no C24 . C23 . H231 . 110.9 no C22 . C23 . H232 . 109.0 no C24 . C23 . H232 . 112.5 no H231 . C23 . H232 . 108.8 no C23 . C24 . C25 . 105.60(11) yes C23 . C24 . H241 . 111.1 no C25 . C24 . H241 . 110.0 no C23 . C24 . H242 . 110.9 no C25 . C24 . H242 . 110.8 no H241 . C24 . H242 . 108.4 no C24 . C25 . N1 . 104.17(11) yes C24 . C25 . H252 . 114.4 no N1 . C25 . H252 . 111.4 no C24 . C25 . H251 . 110.0 no N1 . C25 . H251 . 106.7 no H252 . C25 . H251 . 109.8 no C30 6_655 C30 . O31 . 112.53(13) yes C30 6_655 C30 . O32 . 121.65(13) yes O31 . C30 . O32 . 125.74(14) yes C30 . O31 . H311 . 112.1 no C15 . O1 . C1 . 118.18(10) yes C2 . O3 . H31 . 110.4 no C17 . N1 . C25 . 110.78(9) yes C17 . N1 . C20 . 100.70(8) yes C25 . N1 . C20 . 112.64(9) yes C17 . N1 . C22 . 116.71(9) yes C25 . N1 . C22 . 100.67(9) yes C20 . N1 . C22 . 115.81(9) yes loop_ _geom_hbond_atom_site_label_D _geom_hbond_site_symmetry_D _geom_hbond_atom_site_label_H _geom_hbond_site_symmetry_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_angle_DHA _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_publ_flag C10 . H101 . O2 . 124 0.943 2.590 3.2096(19) yes C17 . H171 . O32 6_655 159 1.001 2.441 3.3961(19) yes C22 . H221 . O31 1_545 165 0.984 2.415 3.3743(19) yes _iucr_refine_instruction_details_constraints ; # # Punched on 19/04/13 at 16:10:49 # #LIST 12 BLOCK SCALE X'S, U'S RIDE C ( 4,X'S) H ( 41,X'S) RIDE C ( 5,X'S) H ( 51,X'S) RIDE C ( 6,X'S) H ( 61,X'S) RIDE C ( 7,X'S) H ( 71,X'S) RIDE C ( 8,X'S) H ( 81,X'S) RIDE C ( 10,X'S) H ( 101,X'S) RIDE C ( 11,X'S) H ( 111,X'S) RIDE C ( 12,X'S) H ( 121,X'S) RIDE C ( 13,X'S) H ( 131,X'S) RIDE C ( 14,X'S) H ( 141,X'S) RIDE C ( 15,X'S) H ( 151,X'S) RIDE C ( 16,X'S) H ( 161,X'S) H ( 162,X'S) RIDE C ( 17,X'S) H ( 171,X'S) RIDE C ( 18,X'S) H ( 182,X'S) H ( 181,X'S) RIDE C ( 19,X'S) H ( 192,X'S) H ( 191,X'S) RIDE C ( 20,X'S) H ( 201,X'S) RIDE C ( 21,X'S) H ( 212,X'S) H ( 211,X'S) RIDE C ( 22,X'S) H ( 221,X'S) H ( 222,X'S) RIDE C ( 23,X'S) H ( 231,X'S) H ( 232,X'S) RIDE C ( 24,X'S) H ( 241,X'S) H ( 242,X'S) RIDE C ( 25,X'S) H ( 252,X'S) H ( 251,X'S) RIDE O ( 31,X'S) H ( 311,X'S) RIDE O ( 3,X'S) H ( 31,X'S) END ; _iucr_refine_instruction_details_restraints ; # # Punched on 19/04/13 at 16:10:49 # #LIST 16 NO REM HREST START (DO NOT REMOVE THIS LINE) REM HREST END (DO NOT REMOVE THIS LINE) END ; #======================================================================= data_TCl_GLU #======================================================================= # 5. CHEMICAL DATA _chemical_name_systematic ? _chemical_name_common ? _chemical_formula_moiety 'C25 H30 N O3, C5 H8 O4, Cl' _chemical_formula_structural ? _chemical_formula_analytical ? _chemical_formula_iupac ? _chemical_formula_sum 'C30 H38 Cl1 N1 O7' _chemical_formula_weight 560.1 _chemical_melting_point ? _chemical_compound_source ? _chemical_absolute_configuration . #======================================================================= # 6. POWDER SPECIMEN AND CRYSTAL DATA _symmetry_cell_setting monoclinic _symmetry_space_group_name_H-M 'P 1 21/c 1' _symmetry_space_group_name_Hall '-P 2ycb' _symmetry_Int_Tables_number 14 loop_ _symmetry_equiv_pos_site_id _symmetry_equiv_pos_as_xyz 1 x,y,z 2 -x,y+1/2,-z+1/2 3 -x,-y,-z 4 x,-y+1/2,z+1/2 _cell_length_a 25.4311(5) _cell_length_b 6.66631(12) _cell_length_c 16.7131(3) _cell_angle_alpha 90 _cell_angle_beta 95.0570(17) _cell_angle_gamma 90 _cell_volume 2822.38(9) _cell_formula_units_Z 4 _cell_measurement_temperature 293 _cell_special_details ? _exptl_crystal_density_diffrn 1.3177 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_F_000 280 _pd_spec_size_axial ? _pd_spec_size_equat ? _pd_spec_size_thick ? _pd_spec_mounting ? _pd_spec_mount_mode ? _pd_spec_shape ? _pd_char_particle_morphology ? _pd_char_colour white _pd_prep_cool_rate ? _pd_prep_pressure ? _pd_prep_temperature 298 _exptl_absorpt_coefficient_mu 1.596 _exptl_absorpt_correction_type ? _exptl_absorpt_process_details ? _exptl_absorpt_correction_T_min ? _exptl_absorpt_correction_T_max ? #======================================================================= # 7. EXPERIMENTAL DATA _exptl_special_details ? _pd_instr_location ? _pd_calibration_special_details ? _diffrn_ambient_temperature 293 _diffrn_source ? _diffrn_source_target ? _diffrn_source_type ? _diffrn_radiation_type 'CuK\a' _diffrn_radiation_wavelength 1.5418 _diffrn_radiation_monochromator ? _diffrn_measurement_device ? _diffrn_measurement_device_type 'PANalytical Empyrean' _diffrn_detector 'PIXCel3D' _diffrn_detector_type ? _pd_meas_scan_method ? _pd_meas_special_details ? _pd_meas_number_of_points 5788 _pd_meas_2theta_range_min 4.007 _pd_meas_2theta_range_max 79.992 _pd_meas_2theta_range_inc 0.013 _diffrn_radiation_probe x-ray #======================================================================= # 8. REFINEMENT DATA _pd_proc_ls_special_details ? _pd_proc_ls_profile_function 'Pseudo-Voigt' _pd_proc_ls_background_function '30 Legendre polynoms' _pd_proc_ls_pref_orient_corr none _pd_proc_ls_prof_R_factor 0.0153 _pd_proc_ls_prof_wR_factor 0.0203 _pd_proc_ls_prof_wR_expected 0.0130 _refine_special_details ? _refine_ls_R_factor_gt 0.0854 _refine_ls_wR_factor_gt 0.0741 _refine_ls_R_factor_all 0.1127 _refine_ls_wR_factor_all 0.0792 _refine_ls_goodness_of_fit_all 1.56 _refine_ls_restrained_S_gt ? _refine_ls_restrained_S_all ? _refine_ls_number_parameters 161 _refine_ls_number_restraints 99 _refine_ls_number_constraints 995 _refine_ls_weighting_scheme sigma _refine_ls_weighting_details ? _refine_ls_hydrogen_treatment constr _refine_ls_shift/su_max 0.0425 _refine_ls_shift/su_mean 0.0081 _refine_diff_density_max 0.32 _refine_diff_density_min -0.49 _refine_ls_extinction_method ? _refine_ls_extinction_coef ? _pd_proc_2theta_range_min 4.007 _pd_proc_2theta_range_max 79.992 _pd_proc_2theta_range_inc 0.013 _pd_proc_wavelength ? _pd_block_diffractogram_id ? _pd_proc_info_excluded_regions ? _pd_proc_info_data_reduction ? loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C 0.0181 0.0091 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' H 0.0000 0.0000 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Cl 0.3639 0.7018 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' N 0.0311 0.0180 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' O 0.0492 0.0322 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution ? _computing_structure_refinement ? _computing_molecular_graphics ? _computing_publication_material ? loop_ _restr_distance_atom_site_label_1 _restr_distance_site_symmetry_1 _restr_distance_atom_site_label_2 _restr_distance_site_symmetry_2 _restr_distance_target _restr_distance_target_weight_param C1 . O1 . 1.34 0.001 C15 . O1 . 1.461 0.001 O2 . C1 . 1.198 0.001 C2 . C1 . 1.532 0.001 C16 . C15 . 1.528 0.001 C19 . C15 . 1.52 0.001 O3 . C2 . 1.433 0.001 C9 . C2 . 1.536 0.001 C3 . C2 . 1.547 0.001 C17 . C16 . 1.519 0.001 C18 . C19 . 1.521 0.001 C10 . C9 . 1.378 0.001 C14 . C9 . 1.387 0.001 C4 . C3 . 1.377 0.001 C8 . C3 . 1.396 0.001 N1 . C17 . 1.533 0.001 C21 . C17 . 1.53 0.001 N1 . C18 . 1.525 0.001 C20 . C18 . 1.524 0.001 C11 . C10 . 1.396 0.001 C13 . C14 . 1.398 0.001 C5 . C4 . 1.391 0.001 C7 . C8 . 1.39 0.001 C22 . N1 . 1.507 0.001 C25 . N1 . 1.517 0.001 C20 . C21 . 1.548 0.001 C12 . C11 . 1.375 0.001 C12 . C13 . 1.365 0.001 C6 . C5 . 1.367 0.001 C6 . C7 . 1.376 0.001 C23 . C22 . 1.512 0.001 C24 . C25 . 1.514 0.001 C24 . C23 . 1.543 0.001 O5 . C26 . 1.308 0.001 O7 . C30 . 1.308 0.001 O4 . C26 . 1.224 0.001 O6 . C30 . 1.224 0.001 C26 . C27 . 1.491 0.001 C30 . C29 . 1.491 0.001 C27 . C28 . 1.519 0.001 C29 . C28 . 1.519 0.001 loop_ _restr_angle_atom_site_label_1 _restr_angle_site_symmetry_1 _restr_angle_atom_site_label_2 _restr_angle_site_symmetry_2 _restr_angle_atom_site_label_3 _restr_angle_site_symmetry_3 _restr_angle_target _restr_angle_target_weight_param ? ? ? ? ? ? ? ? loop_ _restr_torsion_atom_site_label_1 _restr_torsion_site_symmetry_1 _restr_torsion_atom_site_label_2 _restr_torsion_site_symmetry_2 _restr_torsion_atom_site_label_3 _restr_torsion_site_symmetry_3 _restr_torsion_atom_site_label_4 _restr_torsion_site_symmetry_4 _restr_torsion_angle_target _restr_torsion_weight_param ? ? ? ? ? ? ? ? ? ? loop_ _restr_equal_distance_atom_site_label_1 _restr_equal_distance_site_symmetry_1 _restr_equal_distance_atom_site_label_2 _restr_equal_distance_site_symmetry_2 _restr_equal_distance_class_class_id _restr_equal_distance_class_target_weight_param ? ? ? ? ? ? loop_ _restr_equal_angle_atom_site_label_1 _restr_equal_angle_site_symmetry_1 _restr_equal_angle_atom_site_label_2 _restr_equal_angle_site_symmetry_2 _restr_equal_angle_atom_site_label_3 _restr_equal_angle_site_symmetry_3 _restr_equal_angle_class_class_id _restr_equal_angle_class_target_weight_param ? ? ? ? ? ? ? ? loop_ _restr_equal_torsion_atom_site_label_1 _restr_equal_torsion_site_symmetry_1 _restr_equal_torsion_atom_site_label_2 _restr_equal_torsion_site_symmetry_2 _restr_equal_torsion_atom_site_label_3 _restr_equal_torsion_site_symmetry_3 _restr_equal_torsion_atom_site_label_4 _restr_equal_torsion_site_symmetry_4 _restr_equal_torsion_class_class_id _restr_equal_torsion_class_target_weight_param ? ? ? ? ? ? ? ? ? ? #======================================================================= # 9. ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_site_symmetry_multiplicity _atom_site_occupancy _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.2177(3) 0.1412(6) 0.3497(3) Uiso 0.034(3) 4 1 d . . . O2 O 0.1920(3) 0.3312(6) 0.2423(3) Uiso 0.034(3) 4 1 d . . . O3 O 0.17606(3) -0.17640(10) 0.29275(4) Uiso 0.034(3) 4 1 d . . . N1 N 0.30126(15) 0.2589(8) 0.5466(2) Uiso 0.034(3) 4 1 d . . . C1 C 0.18806(14) 0.1821(2) 0.28138(15) Uiso 0.034(3) 4 1 d . . . C2 C 0.15168(9) 0.00318(16) 0.26017(11) Uiso 0.034(3) 4 1 d . . . C3 C 0.10033(8) 0.0382(3) 0.30137(18) Uiso 0.034(3) 4 1 d . . . C4 C 0.0795(3) 0.2261(5) 0.3117(8) Uiso 0.034(3) 4 1 d . . . C5 C 0.0303(3) 0.2488(8) 0.3409(9) Uiso 0.034(3) 4 1 d . . . C6 C 0.0031(4) 0.0833(11) 0.3624(13) Uiso 0.034(3) 4 1 d . . . C7 C 0.0238(5) -0.1056(10) 0.3543(16) Uiso 0.034(3) 4 1 d . . . C8 C 0.0726(3) -0.1301(5) 0.3241(9) Uiso 0.034(3) 4 1 d . . . C9 C 0.13581(14) -0.0219(3) 0.16990(12) Uiso 0.034(3) 4 1 d . . . C10 C 0.1403(6) -0.2004(7) 0.1295(2) Uiso 0.034(3) 4 1 d . . . C11 C 0.1234(7) -0.2145(10) 0.0479(3) Uiso 0.034(3) 4 1 d . . . C12 C 0.1010(10) -0.0526(15) 0.0068(4) Uiso 0.034(3) 4 1 d . . . C13 C 0.0954(7) 0.1234(11) 0.0469(3) Uiso 0.034(3) 4 1 d . . . C14 C 0.1123(6) 0.1397(9) 0.1286(3) Uiso 0.034(3) 4 1 d . . . C15 C 0.2588(3) 0.2851(7) 0.3768(3) Uiso 0.034(3) 4 1 d . . . C19 C 0.2374(4) 0.4070(8) 0.4436(6) Uiso 0.034(3) 4 1 d . . . C18 C 0.24287(18) 0.3018(17) 0.5247(4) Uiso 0.034(3) 4 1 d . . . C20 C 0.2188(2) 0.092(2) 0.5240(3) Uiso 0.034(3) 4 1 d . . . C21 C 0.2624(4) -0.0514(10) 0.4998(5) Uiso 0.034(3) 4 1 d . . . C17 C 0.3095(2) 0.0859(6) 0.4886(3) Uiso 0.034(3) 4 1 d . . . C16 C 0.3094(2) 0.1720(14) 0.4044(2) Uiso 0.034(3) 4 1 d . . . C22 C 0.3369(3) 0.4391(7) 0.5442(4) Uiso 0.034(3) 4 1 d . . . C23 C 0.3884(3) 0.3704(13) 0.5877(3) Uiso 0.034(3) 4 1 d . . . C24 C 0.3719(2) 0.2196(12) 0.6509(3) Uiso 0.034(3) 4 1 d . . . C25 C 0.3129(2) 0.1927(17) 0.6333(2) Uiso 0.034(3) 4 1 d . . . Cl1 Cl 0.2832(4) 0.8001(12) 0.2089(6) Uiso 0.055(6) 4 1 d . . . H1c4 H 0.099131 0.342769 0.298675 Uiso 0.0404 4 1 d . . . H1c5 H 0.015457 0.380223 0.345969 Uiso 0.0404 4 1 d . . . H1c6 H -0.03067 0.098957 0.383311 Uiso 0.0404 4 1 d . . . H1c7 H 0.004433 -0.220966 0.369661 Uiso 0.0404 4 1 d . . . H1c10 H 0.155073 -0.315644 0.157617 Uiso 0.0404 4 1 d . . . H1c11 H 0.127483 -0.338824 0.020196 Uiso 0.0404 4 1 d . . . H1c12 H 0.08954 -0.063308 -0.049352 Uiso 0.0404 4 1 d . . . H1c13 H 0.079801 0.23718 0.018775 Uiso 0.0404 4 1 d . . . H1c14 H 0.107454 0.263662 0.156244 Uiso 0.0404 4 1 d . . . H1c15 H 0.267513 0.374119 0.334816 Uiso 0.0404 4 1 d . . . H1c19 H 0.200905 0.438312 0.429295 Uiso 0.0404 4 1 d . . . H2c19 H 0.255046 0.534272 0.448026 Uiso 0.0404 4 1 d . . . H1c18 H 0.225845 0.388861 0.560222 Uiso 0.0404 4 1 d . . . H1c20 H 0.189071 0.086672 0.484432 Uiso 0.0404 4 1 d . . . H2c20 H 0.209761 0.059181 0.577018 Uiso 0.0404 4 1 d . . . H1c21 H 0.251097 -0.114505 0.449564 Uiso 0.0404 4 1 d . . . H2c21 H 0.27162 -0.14367 0.542843 Uiso 0.0404 4 1 d . . . H1c17 H 0.342115 0.013804 0.497888 Uiso 0.0404 4 1 d . . . H1c16 H 0.31482 0.065855 0.367222 Uiso 0.0404 4 1 d . . . H2c16 H 0.339152 0.259546 0.401939 Uiso 0.0404 4 1 d . . . H1c22 H 0.322664 0.547578 0.573397 Uiso 0.0404 4 1 d . . . H2c22 H 0.342212 0.470162 0.489465 Uiso 0.0404 4 1 d . . . H1c23 H 0.409083 0.302735 0.550598 Uiso 0.0404 4 1 d . . . H2c23 H 0.405916 0.482701 0.614298 Uiso 0.0404 4 1 d . . . H1c24 H 0.389353 0.093743 0.644229 Uiso 0.0404 4 1 d . . . H2c24 H 0.379233 0.275595 0.703667 Uiso 0.0404 4 1 d . . . H1c25 H 0.3041 0.053478 0.638072 Uiso 0.0404 4 1 d . . . H2c25 H 0.29476 0.278956 0.667665 Uiso 0.0404 4 1 d . . . O4 O 0.45028(15) -0.1535(5) 0.61292(17) Uiso 0.065(4) 4 1 d . . . O5 O 0.498605(18) -0.26153(13) 0.51721(5) Uiso 0.065(4) 4 1 d . . . O6 O 0.57335(6) 0.3704(5) 0.5842(3) Uiso 0.065(4) 4 1 d . . . O7 O 0.65107(4) 0.39098(11) 0.65557(5) Uiso 0.065(4) 4 1 d . . . C26 C 0.49243(11) -0.1606(3) 0.58285(8) Uiso 0.065(4) 4 1 d . . . C27 C 0.54145(14) -0.0643(9) 0.6204(3) Uiso 0.065(4) 4 1 d . . . C28 C 0.5349(3) 0.0777(11) 0.6899(4) Uiso 0.065(4) 4 1 d . . . C29 C 0.5850(2) 0.1980(8) 0.7096(3) Uiso 0.065(4) 4 1 d . . . C30 C 0.60208(7) 0.3299(3) 0.6446(2) Uiso 0.065(4) 4 1 d . . . H1c27 H 0.55909 0.00411 0.579825 Uiso 0.0781 4 1 d . . . H2c27 H 0.566781 -0.166042 0.637136 Uiso 0.0781 4 1 d . . . H1c28 H 0.527003 0.001931 0.736165 Uiso 0.0781 4 1 d . . . H2c28 H 0.50603 0.167508 0.675686 Uiso 0.0781 4 1 d . . . H1c29 H 0.5817 0.276482 0.757072 Uiso 0.0781 4 1 d . . . H2c29 H 0.613341 0.108957 0.727488 Uiso 0.0781 4 1 d . . . H1c8 H 0.087065 -0.261892 0.318853 Uiso 0.0404 4 1 d . . . H1o3 H 0.203414 -0.197388 0.271556 Uiso 0.0404 4 1 d . . . H1o5 H 0.470645 -0.31542 0.501246 Uiso 0.0781 4 1 d . . . H1o7 H 0.66435 0.350317 0.69905 Uiso 0.0781 4 1 d . . . loop_ _atom_site_aniso_label _atom_site_aniso_type_symbol _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 ? ? ? ? ? ? ? ? loop_ _jana_atom_site_ADP_C_label _jana_atom_site_ADP_C_type_symbol _jana_atom_site_ADP_C_111 _jana_atom_site_ADP_C_112 _jana_atom_site_ADP_C_113 _jana_atom_site_ADP_C_122 _jana_atom_site_ADP_C_123 _jana_atom_site_ADP_C_133 _jana_atom_site_ADP_C_222 _jana_atom_site_ADP_C_223 _jana_atom_site_ADP_C_233 _jana_atom_site_ADP_C_333 ? ? ? ? ? ? ? ? ? ? ? ? loop_ _jana_atom_site_ADP_D_label _jana_atom_site_ADP_D_type_symbol _jana_atom_site_ADP_D_1111 _jana_atom_site_ADP_D_1112 _jana_atom_site_ADP_D_1113 _jana_atom_site_ADP_D_1122 _jana_atom_site_ADP_D_1123 _jana_atom_site_ADP_D_1133 _jana_atom_site_ADP_D_1222 _jana_atom_site_ADP_D_1223 _jana_atom_site_ADP_D_1233 _jana_atom_site_ADP_D_1333 _jana_atom_site_ADP_D_2222 _jana_atom_site_ADP_D_2223 _jana_atom_site_ADP_D_2233 _jana_atom_site_ADP_D_2333 _jana_atom_site_ADP_D_3333 ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? loop_ _jana_atom_site_ADP_E_label _jana_atom_site_ADP_E_type_symbol _jana_atom_site_ADP_E_11111 _jana_atom_site_ADP_E_11112 _jana_atom_site_ADP_E_11113 _jana_atom_site_ADP_E_11122 _jana_atom_site_ADP_E_11123 _jana_atom_site_ADP_E_11133 _jana_atom_site_ADP_E_11222 _jana_atom_site_ADP_E_11223 _jana_atom_site_ADP_E_11233 _jana_atom_site_ADP_E_11333 _jana_atom_site_ADP_E_12222 _jana_atom_site_ADP_E_12223 _jana_atom_site_ADP_E_12233 _jana_atom_site_ADP_E_12333 _jana_atom_site_ADP_E_13333 _jana_atom_site_ADP_E_22222 _jana_atom_site_ADP_E_22223 _jana_atom_site_ADP_E_22233 _jana_atom_site_ADP_E_22333 _jana_atom_site_ADP_E_23333 _jana_atom_site_ADP_E_33333 ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? loop_ _jana_atom_site_ADP_F_label _jana_atom_site_ADP_F_type_symbol _jana_atom_site_ADP_F_111111 _jana_atom_site_ADP_F_111112 _jana_atom_site_ADP_F_111113 _jana_atom_site_ADP_F_111122 _jana_atom_site_ADP_F_111123 _jana_atom_site_ADP_F_111133 _jana_atom_site_ADP_F_111222 _jana_atom_site_ADP_F_111223 _jana_atom_site_ADP_F_111233 _jana_atom_site_ADP_F_111333 _jana_atom_site_ADP_F_112222 _jana_atom_site_ADP_F_112223 _jana_atom_site_ADP_F_112233 _jana_atom_site_ADP_F_112333 _jana_atom_site_ADP_F_113333 _jana_atom_site_ADP_F_122222 _jana_atom_site_ADP_F_122223 _jana_atom_site_ADP_F_122233 _jana_atom_site_ADP_F_122333 _jana_atom_site_ADP_F_123333 _jana_atom_site_ADP_F_133333 _jana_atom_site_ADP_F_222222 _jana_atom_site_ADP_F_222223 _jana_atom_site_ADP_F_222233 _jana_atom_site_ADP_F_222333 _jana_atom_site_ADP_F_223333 _jana_atom_site_ADP_F_233333 _jana_atom_site_ADP_F_333333 ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? #======================================================================= # 10. MOLECULAR GEOMETRY loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag O1 C1 . . 1.339(6) ? O1 C15 . . 1.461(8) ? O2 C1 . . 1.198(5) ? O3 C2 . . 1.4334(16) ? O3 H1o3 . . 0.82 ? N1 C18 . . 1.525(6) ? N1 C17 . . 1.533(7) ? N1 C22 . . 1.507(8) ? N1 C25 . . 1.517(6) ? C1 C2 . . 1.532(3) ? C2 C3 . . 1.547(3) ? C2 C9 . . 1.536(3) ? C3 C4 . . 1.377(5) ? C3 C8 . . 1.396(7) ? C4 C5 . . 1.391(14) ? C4 H1c4 . . 0.96 ? C5 C6 . . 1.367(13) ? C5 H1c5 . . 0.96 ? C6 C7 . . 1.376(12) ? C6 H1c6 . . 0.96 ? C7 C8 . . 1.390(19) ? C7 H1c7 . . 0.96 ? C8 H1c8 . . 0.96 ? C9 C10 . . 1.378(5) ? C9 C14 . . 1.387(8) ? C10 C11 . . 1.396(7) ? C10 H1c10 . . 0.96 ? C11 C12 . . 1.376(15) ? C11 H1c11 . . 0.96 ? C12 C13 . . 1.366(12) ? C12 H1c12 . . 0.96 ? C13 C14 . . 1.398(8) ? C13 H1c13 . . 0.96 ? C14 H1c14 . . 0.96 ? C15 C19 . . 1.520(10) ? C15 C16 . . 1.528(9) ? C15 H1c15 . . 0.96 ? C19 C18 . . 1.521(12) ? C19 H1c19 . . 0.96 ? C19 H2c19 . . 0.96 ? C18 C20 . . 1.524(17) ? C18 H1c18 . . 0.96 ? C20 C21 . . 1.548(14) ? C20 H1c20 . . 0.96 ? C20 H2c20 . . 0.96 ? C21 C17 . . 1.530(10) ? C21 H1c21 . . 0.96 ? C21 H2c21 . . 0.96 ? C17 C16 . . 1.519(7) ? C17 H1c17 . . 0.96 ? C16 H1c16 . . 0.96 ? C16 H2c16 . . 0.96 ? C22 C23 . . 1.512(10) ? C22 H1c22 . . 0.96 ? C22 H2c22 . . 0.96 ? C23 C24 . . 1.543(10) ? C23 H1c23 . . 0.96 ? C23 H2c23 . . 0.96 ? C24 C25 . . 1.514(8) ? C24 H1c24 . . 0.96 ? C24 H2c24 . . 0.96 ? C25 H1c25 . . 0.96 ? C25 H2c25 . . 0.96 ? O4 C26 . . 1.224(5) ? O5 C26 . . 1.3082(17) ? O5 H1o5 . . 0.82 ? O6 C30 . . 1.224(5) ? O7 C30 . . 1.308(2) ? O7 H1o7 . . 0.82 ? C26 C27 . . 1.491(5) ? C27 C28 . . 1.519(9) ? C27 H1c27 . . 0.96 ? C27 H2c27 . . 0.96 ? C28 C29 . . 1.519(9) ? C28 H1c28 . . 0.96 ? C28 H2c28 . . 0.96 ? C29 C30 . . 1.491(6) ? C29 H1c29 . . 0.96 ? C29 H2c29 . . 0.96 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_2 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C1 O1 C15 . . . 117.6(4) ? C2 O3 H1o3 . . . 109.47 ? C18 N1 C17 . . . 100.0(5) ? C18 N1 C22 . . . 114.7(6) ? C18 N1 C25 . . . 112.9(4) ? C17 N1 C22 . . . 117.9(4) ? C17 N1 C25 . . . 111.0(5) ? C22 N1 C25 . . . 100.9(5) ? O1 C1 O2 . . . 124.4(4) ? O1 C1 C2 . . . 108.7(2) ? O2 C1 C2 . . . 126.7(3) ? O3 C2 C1 . . . 109.29(17) ? O3 C2 C3 . . . 108.11(15) ? O3 C2 C9 . . . 110.47(12) ? C1 C2 C3 . . . 107.20(17) ? C1 C2 C9 . . . 114.40(17) ? C3 C2 C9 . . . 107.1(2) ? C2 C3 C4 . . . 122.9(4) ? C2 C3 C8 . . . 117.8(4) ? C4 C3 C8 . . . 119.2(5) ? C3 C4 C5 . . . 120.8(5) ? C3 C4 H1c4 . . . 119.62 ? C5 C4 H1c4 . . . 119.62 ? C4 C5 C6 . . . 119.7(7) ? C4 C5 H1c5 . . . 120.13 ? C6 C5 H1c5 . . . 120.13 ? C5 C6 C7 . . . 120.4(13) ? C5 C6 H1c6 . . . 119.8 ? C7 C6 H1c6 . . . 119.8 ? C6 C7 C8 . . . 120.3(10) ? C6 C7 H1c7 . . . 119.84 ? C8 C7 H1c7 . . . 119.84 ? C3 C8 C7 . . . 119.6(5) ? C3 C8 H1c8 . . . 120.21 ? C7 C8 H1c8 . . . 120.21 ? C2 C9 C10 . . . 123.3(3) ? C2 C9 C14 . . . 118.0(3) ? C10 C9 C14 . . . 118.5(4) ? C9 C10 C11 . . . 120.3(6) ? C9 C10 H1c10 . . . 119.83 ? C11 C10 H1c10 . . . 119.83 ? C10 C11 C12 . . . 120.9(6) ? C10 C11 H1c11 . . . 119.54 ? C12 C11 H1c11 . . . 119.54 ? C11 C12 C13 . . . 119.0(7) ? C11 C12 H1c12 . . . 120.51 ? C13 C12 H1c12 . . . 120.51 ? C12 C13 C14 . . . 120.7(9) ? C12 C13 H1c13 . . . 119.66 ? C14 C13 H1c13 . . . 119.65 ? C9 C14 C13 . . . 120.5(6) ? C9 C14 H1c14 . . . 119.75 ? C13 C14 H1c14 . . . 119.76 ? O1 C15 C19 . . . 106.6(6) ? O1 C15 C16 . . . 109.3(5) ? O1 C15 H1c15 . . . 112.67 ? C19 C15 C16 . . . 112.8(5) ? C19 C15 H1c15 . . . 109.11 ? C16 C15 H1c15 . . . 106.42 ? C15 C19 C18 . . . 113.4(6) ? C15 C19 H1c19 . . . 109.47 ? C15 C19 H2c19 . . . 109.47 ? C18 C19 H1c19 . . . 109.47 ? C18 C19 H2c19 . . . 109.47 ? H1c19 C19 H2c19 . . . 105.22 ? N1 C18 C19 . . . 108.2(5) ? N1 C18 C20 . . . 102.3(7) ? N1 C18 H1c18 . . . 116.58 ? C19 C18 C20 . . . 114.2(6) ? C19 C18 H1c18 . . . 105.15 ? C20 C18 H1c18 . . . 110.79 ? C18 C20 C21 . . . 105.8(6) ? C18 C20 H1c20 . . . 109.47 ? C18 C20 H2c20 . . . 109.47 ? C21 C20 H1c20 . . . 109.47 ? C21 C20 H2c20 . . . 109.47 ? H1c20 C20 H2c20 . . . 112.93 ? C20 C21 C17 . . . 104.4(6) ? C20 C21 H1c21 . . . 109.47 ? C20 C21 H2c21 . . . 109.47 ? C17 C21 H1c21 . . . 109.47 ? C17 C21 H2c21 . . . 109.47 ? H1c21 C21 H2c21 . . . 114.15 ? N1 C17 C21 . . . 102.8(5) ? N1 C17 C16 . . . 108.2(4) ? N1 C17 H1c17 . . . 116.01 ? C21 C17 C16 . . . 113.7(5) ? C21 C17 H1c17 . . . 110.8 ? C16 C17 H1c17 . . . 105.61 ? C15 C16 C17 . . . 113.5(4) ? C15 C16 H1c16 . . . 109.47 ? C15 C16 H2c16 . . . 109.47 ? C17 C16 H1c16 . . . 109.47 ? C17 C16 H2c16 . . . 109.47 ? H1c16 C16 H2c16 . . . 105.1 ? N1 C22 C23 . . . 104.1(5) ? N1 C22 H1c22 . . . 109.47 ? N1 C22 H2c22 . . . 109.47 ? C23 C22 H1c22 . . . 109.47 ? C23 C22 H2c22 . . . 109.47 ? H1c22 C22 H2c22 . . . 114.38 ? C22 C23 C24 . . . 104.5(5) ? C22 C23 H1c23 . . . 109.47 ? C22 C23 H2c23 . . . 109.47 ? C24 C23 H1c23 . . . 109.47 ? C24 C23 H2c23 . . . 109.47 ? H1c23 C23 H2c23 . . . 114.05 ? C23 C24 C25 . . . 105.5(5) ? C23 C24 H1c24 . . . 109.47 ? C23 C24 H2c24 . . . 109.47 ? C25 C24 H1c24 . . . 109.47 ? C25 C24 H2c24 . . . 109.47 ? H1c24 C24 H2c24 . . . 113.15 ? N1 C25 C24 . . . 105.0(4) ? N1 C25 H1c25 . . . 109.47 ? N1 C25 H2c25 . . . 109.47 ? C24 C25 H1c25 . . . 109.47 ? C24 C25 H2c25 . . . 109.47 ? H1c25 C25 H2c25 . . . 113.6 ? C26 O5 H1o5 . . . 109.47 ? C30 O7 H1o7 . . . 109.47 ? O4 C26 O5 . . . 122.6(2) ? O4 C26 C27 . . . 122.7(3) ? O5 C26 C27 . . . 114.6(3) ? C26 C27 C28 . . . 116.5(4) ? C26 C27 H1c27 . . . 109.47 ? C26 C27 H2c27 . . . 109.47 ? C28 C27 H1c27 . . . 109.47 ? C28 C27 H2c27 . . . 109.47 ? H1c27 C27 H2c27 . . . 101.46 ? C27 C28 C29 . . . 110.4(5) ? C27 C28 H1c28 . . . 109.47 ? C27 C28 H2c28 . . . 109.47 ? C29 C28 H1c28 . . . 109.47 ? C29 C28 H2c28 . . . 109.47 ? H1c28 C28 H2c28 . . . 108.55 ? C28 C29 C30 . . . 116.4(4) ? C28 C29 H1c29 . . . 109.47 ? C28 C29 H2c29 . . . 109.47 ? C30 C29 H1c29 . . . 109.47 ? C30 C29 H2c29 . . . 109.47 ? H1c29 C29 H2c29 . . . 101.46 ? O6 C30 O7 . . . 122.6(3) ? O6 C30 C29 . . . 122.7(3) ? O7 C30 C29 . . . 114.6(3) ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag ? ? ? ? ? ? ? ? ? ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_D _geom_hbond_site_symmetry_H _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag C10 H1c10 O3 . . . 0.96 2.46 2.803(5) 101.03 ? C15 H1c15 O2 . . . 0.96 2.37 2.711(8) 100.07 ? C20 H1c20 O1 . . . 0.96 2.45 2.929(7) 110.37 ? C21 H1c21 O1 . . . 0.96 2.48 2.955(9) 110.20 ? C24 H1c24 O4 . . . 0.96 2.35 3.284(8) 163.37 ? C27 H1c27 O6 . . . 0.96 2.47 3.083(7) 121.71 ? C29 H1c29 O4 . . 2_656 0.96 2.43 3.325(6) 154.66 ? C8 H1c8 O3 . . . 0.96 2.41 2.746(9) 100.05 ? O3 H1o3 Cl1 . . 1_545 0.82 2.36 3.176(10) 170.57 ? O5 H1o5 O6 . . 3_656 0.82 1.77 2.490(4) 145.10 ? O7 H1o7 Cl1 . . 3_666 0.82 2.19 2.980(9) 162.24 ? #======================================================================= # 11. POWDER PROFILE loop_ _pd_proc_point_id _pd_proc_2theta_corrected _pd_proc_intensity_net _pd_calc_intensity_net _pd_proc_ls_weight 1 3.9902 16575.00 16388.50 129.00 2 4.0033 16318.00 16265.10 128.00 3 4.0164 16323.00 16144.90 128.00 4 4.0296 16329.00 16027.80 128.00 5 4.0427 16375.00 15913.70 128.00 6 4.0558 16175.00 15802.60 127.00 7 4.0690 16040.00 15694.50 127.00 8 4.0821 15739.00 15589.20 125.00 9 4.0952 15571.00 15486.70 125.00 10 4.1083 15401.00 15386.90 124.00 11 4.1215 15336.00 15289.80 124.00 12 4.1346 15054.00 15195.40 123.00 13 4.1477 15164.00 15103.50 123.00 14 4.1609 14851.00 15014.10 122.00 15 4.1740 14757.00 14927.20 121.00 16 4.1871 14533.00 14842.60 121.00 17 4.2003 14746.00 14760.40 121.00 18 4.2134 14578.00 14680.50 121.00 19 4.2265 14278.00 14602.80 119.00 20 4.2396 14199.00 14527.30 119.00 21 4.2528 14201.00 14454.00 119.00 22 4.2659 14011.00 14382.70 118.00 23 4.2790 13930.00 14313.40 118.00 24 4.2922 14059.00 14246.10 119.00 25 4.3053 14114.00 14180.70 119.00 26 4.3184 14039.00 14117.30 118.00 27 4.3316 13979.00 14055.60 118.00 28 4.3447 13823.00 13995.80 118.00 29 4.3578 13611.00 13937.60 117.00 30 4.3709 13659.00 13881.20 117.00 31 4.3841 13588.00 13826.40 117.00 32 4.3972 13612.00 13773.30 117.00 33 4.4103 13562.00 13721.70 116.00 34 4.4235 13734.00 13671.60 117.00 35 4.4366 13634.00 13623.00 117.00 36 4.4497 13571.00 13575.80 116.00 37 4.4629 13589.00 13530.00 117.00 38 4.4760 13508.00 13485.60 116.00 39 4.4891 13181.00 13442.50 115.00 40 4.5023 13484.00 13400.70 116.00 41 4.5154 13597.00 13360.20 117.00 42 4.5285 13234.00 13320.80 115.00 43 4.5416 13081.00 13282.70 114.00 44 4.5548 13251.00 13245.70 115.00 45 4.5679 13245.00 13209.70 115.00 46 4.5810 13108.00 13174.90 114.00 47 4.5942 13299.00 13141.10 115.00 48 4.6073 13365.00 13108.30 116.00 49 4.6204 13059.00 13076.40 114.00 50 4.6336 13120.00 13045.60 115.00 51 4.6467 12824.00 13015.60 113.00 52 4.6598 12865.00 12986.50 113.00 53 4.6729 13042.00 12958.30 114.00 54 4.6861 13091.00 12930.90 114.00 55 4.6992 12850.00 12904.30 113.00 56 4.7123 13072.00 12878.40 114.00 57 4.7255 12905.00 12853.30 114.00 58 4.7386 12786.00 12829.00 113.00 59 4.7517 13004.00 12805.30 114.00 60 4.7649 12829.00 12782.30 113.00 61 4.7780 12978.00 12759.90 114.00 62 4.7911 12857.00 12738.10 113.00 63 4.8042 12828.00 12717.00 113.00 64 4.8174 12681.00 12696.40 113.00 65 4.8305 12963.00 12676.40 114.00 66 4.8436 12994.00 12656.90 114.00 67 4.8568 12695.00 12637.90 113.00 68 4.8699 12901.00 12619.50 114.00 69 4.8830 12688.00 12601.50 113.00 70 4.8962 12942.00 12583.90 114.00 71 4.9093 12798.00 12566.80 113.00 72 4.9224 12811.00 12550.00 113.00 73 4.9356 12472.00 12533.70 112.00 74 4.9487 12459.00 12517.80 112.00 75 4.9618 12724.00 12502.20 113.00 76 4.9749 12607.00 12487.00 112.00 77 4.9881 12535.00 12472.10 112.00 78 5.0012 12433.00 12457.60 112.00 79 5.0143 12519.00 12443.30 112.00 80 5.0275 12350.00 12429.30 111.00 81 5.0406 12707.00 12415.60 113.00 82 5.0537 12489.00 12402.10 112.00 83 5.0669 12435.00 12388.90 112.00 84 5.0800 12290.00 12376.00 111.00 85 5.0931 12394.00 12363.20 111.00 86 5.1062 12294.00 12350.70 111.00 87 5.1194 12488.00 12338.30 112.00 88 5.1325 12282.00 12326.20 111.00 89 5.1456 12281.00 12314.20 111.00 90 5.1588 12430.00 12302.40 111.00 91 5.1719 12325.00 12290.70 111.00 92 5.1850 12464.00 12279.20 112.00 93 5.1982 12604.00 12267.80 112.00 94 5.2113 12301.00 12256.60 111.00 95 5.2244 12312.00 12245.50 111.00 96 5.2375 12332.00 12234.40 111.00 97 5.2507 12358.00 12223.50 111.00 98 5.2638 12168.00 12212.70 110.00 99 5.2769 12073.00 12201.90 110.00 100 5.2901 12398.00 12191.30 111.00 101 5.3032 12211.00 12180.70 111.00 102 5.3163 12101.00 12170.20 110.00 103 5.3295 12116.00 12159.70 110.00 104 5.3426 12102.00 12149.30 110.00 105 5.3557 11986.00 12139.00 109.00 106 5.3688 12128.00 12128.60 110.00 107 5.3820 12064.00 12118.40 110.00 108 5.3951 12064.00 12108.10 110.00 109 5.4082 12256.00 12097.90 111.00 110 5.4214 11956.00 12087.70 109.00 111 5.4345 12071.00 12077.50 110.00 112 5.4476 11889.00 12067.40 109.00 113 5.4608 12080.00 12057.20 110.00 114 5.4739 11910.00 12047.10 109.00 115 5.4870 11946.00 12037.00 109.00 116 5.5002 11873.00 12026.80 109.00 117 5.5133 12021.00 12016.70 110.00 118 5.5264 12008.00 12006.50 110.00 119 5.5395 11986.00 11996.40 109.00 120 5.5527 11984.00 11986.20 109.00 121 5.5658 11941.00 11976.10 109.00 122 5.5789 12057.00 11965.90 110.00 123 5.5921 11901.00 11955.70 109.00 124 5.6052 11884.00 11945.50 109.00 125 5.6183 11908.00 11935.20 109.00 126 5.6315 11997.00 11925.00 110.00 127 5.6446 11874.00 11914.70 109.00 128 5.6577 11851.00 11904.40 109.00 129 5.6708 11736.00 11894.00 108.00 130 5.6840 12037.00 11883.70 110.00 131 5.6971 11714.00 11873.30 108.00 132 5.7102 11879.00 11862.90 109.00 133 5.7234 11832.00 11852.40 109.00 134 5.7365 11773.00 11842.00 109.00 135 5.7496 11865.00 11831.50 109.00 136 5.7628 11739.00 11820.90 108.00 137 5.7759 11725.00 11810.40 108.00 138 5.7890 11558.00 11799.80 108.00 139 5.8021 11617.00 11789.20 108.00 140 5.8153 11934.00 11778.50 109.00 141 5.8284 11875.00 11767.90 109.00 142 5.8415 11639.00 11757.10 108.00 143 5.8547 11483.00 11746.40 107.00 144 5.8678 11737.00 11735.70 108.00 145 5.8809 11635.00 11724.90 108.00 146 5.8941 11547.00 11714.00 107.00 147 5.9072 11793.00 11703.20 109.00 148 5.9203 11598.00 11692.30 108.00 149 5.9335 11674.00 11681.50 108.00 150 5.9466 11745.00 11670.50 108.00 151 5.9597 11439.00 11659.60 107.00 152 5.9728 11587.00 11648.60 108.00 153 5.9860 11503.00 11637.70 107.00 154 5.9991 11549.00 11626.70 107.00 155 6.0122 11535.00 11615.60 107.00 156 6.0254 11749.00 11604.60 108.00 157 6.0385 11477.00 11593.50 107.00 158 6.0516 11408.00 11582.50 107.00 159 6.0648 11588.00 11571.40 108.00 160 6.0779 11375.00 11560.30 107.00 161 6.0910 11333.00 11549.20 106.00 162 6.1041 11328.00 11538.10 106.00 163 6.1173 11610.00 11526.90 108.00 164 6.1304 11492.00 11515.80 107.00 165 6.1435 11536.00 11504.70 107.00 166 6.1567 11335.00 11493.50 106.00 167 6.1698 11362.00 11482.40 107.00 168 6.1829 11486.00 11471.20 107.00 169 6.1961 11428.00 11460.00 107.00 170 6.2092 11507.00 11448.90 107.00 171 6.2223 11375.00 11437.70 107.00 172 6.2354 11324.00 11426.60 106.00 173 6.2486 11418.00 11415.40 107.00 174 6.2617 11396.00 11404.30 107.00 175 6.2748 11373.00 11393.20 107.00 176 6.2880 11443.00 11382.00 107.00 177 6.3011 11347.00 11370.90 107.00 178 6.3142 11326.00 11359.80 106.00 179 6.3274 11340.00 11348.70 106.00 180 6.3405 11290.00 11337.70 106.00 181 6.3536 11240.00 11326.60 106.00 182 6.3667 11187.00 11315.60 106.00 183 6.3799 11215.00 11304.50 106.00 184 6.3930 11257.00 11293.50 106.00 185 6.4061 11309.00 11282.50 106.00 186 6.4193 11314.00 11271.60 106.00 187 6.4324 11241.00 11260.70 106.00 188 6.4455 11146.00 11249.70 106.00 189 6.4587 11228.00 11238.90 106.00 190 6.4718 11084.00 11228.00 105.00 191 6.4849 11160.00 11217.20 106.00 192 6.4981 11153.00 11206.40 106.00 193 6.5112 11167.00 11195.60 106.00 194 6.5243 11317.00 11184.90 106.00 195 6.5374 11086.00 11174.20 105.00 196 6.5506 11225.00 11163.50 106.00 197 6.5637 11182.00 11152.90 106.00 198 6.5768 11054.00 11142.30 105.00 199 6.5900 11120.00 11131.80 105.00 200 6.6031 10915.00 11121.30 104.00 201 6.6162 11284.00 11110.80 106.00 202 6.6294 11057.00 11100.40 105.00 203 6.6425 11129.00 11090.00 105.00 204 6.6556 10844.00 11085.80 104.00 205 6.6687 11163.00 11076.20 106.00 206 6.6819 11166.00 11070.10 106.00 207 6.6950 11066.00 11061.40 105.00 208 6.7081 11157.00 11053.10 106.00 209 6.7213 11158.00 11046.10 106.00 210 6.7344 11180.00 11043.90 106.00 211 6.7475 11266.00 11058.70 106.00 212 6.7607 11275.00 11112.30 106.00 213 6.7738 11269.00 11223.60 106.00 214 6.7869 11296.00 11394.40 106.00 215 6.8000 11652.00 11613.50 108.00 216 6.8132 11769.00 11871.60 108.00 217 6.8263 11874.00 12168.30 109.00 218 6.8394 12209.00 12510.10 110.00 219 6.8526 12955.00 12908.50 114.00 220 6.8657 13422.00 13380.70 116.00 221 6.8788 13864.00 13952.90 118.00 222 6.8920 14313.00 14667.20 120.00 223 6.9051 15233.00 15598.60 123.00 224 6.9182 16471.00 16892.30 128.00 225 6.9314 19360.00 18807.00 139.00 226 6.9445 23117.00 21503.50 152.00 227 6.9576 25333.00 24080.00 159.00 228 6.9707 24099.00 24148.10 155.00 229 6.9839 19266.00 20637.90 139.00 230 6.9970 14947.00 15911.00 122.00 231 7.0101 12653.00 12651.50 112.00 232 7.0233 11571.00 11301.60 108.00 233 7.0364 11273.00 10943.90 106.00 234 7.0495 11142.00 10866.30 106.00 235 7.0627 10926.00 10837.50 105.00 236 7.0758 11062.00 10817.60 105.00 237 7.0889 11074.00 10801.10 105.00 238 7.1020 10911.00 10786.80 104.00 239 7.1152 10836.00 10774.00 104.00 240 7.1283 10731.00 10762.30 104.00 241 7.1414 10844.00 10751.30 104.00 242 7.1546 10733.00 10740.90 104.00 243 7.1677 10810.00 10730.90 104.00 244 7.1808 10989.00 10721.40 105.00 245 7.1940 10909.00 10712.10 104.00 246 7.2071 10767.00 10703.00 104.00 247 7.2202 10756.00 10694.20 104.00 248 7.2333 10700.00 10685.60 103.00 249 7.2465 10827.00 10677.10 104.00 250 7.2596 10779.00 10668.80 104.00 251 7.2727 10763.00 10660.60 104.00 252 7.2859 10683.00 10652.50 103.00 253 7.2990 10831.00 10641.20 104.00 254 7.3121 10711.00 10631.90 103.00 255 7.3253 10444.00 10624.50 102.00 256 7.3384 10615.00 10617.10 103.00 257 7.3515 10666.00 10609.70 103.00 258 7.3646 10568.00 10602.40 103.00 259 7.3778 10720.00 10595.20 104.00 260 7.3909 10663.00 10588.00 103.00 261 7.4040 10548.00 10580.90 103.00 262 7.4172 10448.00 10573.80 102.00 263 7.4303 10388.00 10566.80 102.00 264 7.4434 10764.00 10559.90 104.00 265 7.4566 10618.00 10553.00 103.00 266 7.4697 10713.00 10546.10 104.00 267 7.4828 10676.00 10539.30 103.00 268 7.4960 10432.00 10532.60 102.00 269 7.5091 10546.00 10525.90 103.00 270 7.5222 10636.00 10519.20 103.00 271 7.5353 10453.00 10512.70 102.00 272 7.5485 10528.00 10506.10 103.00 273 7.5616 10469.00 10499.60 102.00 274 7.5747 10597.00 10493.20 103.00 275 7.5879 10619.00 10486.80 103.00 276 7.6010 10634.00 10480.40 103.00 277 7.6141 10724.00 10474.10 104.00 278 7.6273 10592.00 10467.90 103.00 279 7.6404 10461.00 10461.60 102.00 280 7.6535 10593.00 10455.50 103.00 281 7.6666 10445.00 10449.40 102.00 282 7.6798 10601.00 10443.30 103.00 283 7.6929 10438.00 10437.20 102.00 284 7.7060 10423.00 10431.20 102.00 285 7.7192 10363.00 10425.30 102.00 286 7.7323 10347.00 10419.40 102.00 287 7.7454 10396.00 10413.50 102.00 288 7.7586 10415.00 10407.70 102.00 289 7.7717 10521.00 10401.90 103.00 290 7.7848 10406.00 10396.10 102.00 291 7.7979 10440.00 10390.40 102.00 292 7.8111 10290.00 10384.70 101.00 293 7.8242 10397.00 10379.00 102.00 294 7.8373 10344.00 10373.40 102.00 295 7.8505 10577.00 10367.80 103.00 296 7.8636 10294.00 10362.30 101.00 297 7.8767 10367.00 10356.80 102.00 298 7.8899 10523.00 10351.30 103.00 299 7.9030 10460.00 10345.90 102.00 300 7.9161 10488.00 10340.70 102.00 301 7.9292 10344.00 10335.90 102.00 302 7.9424 10329.00 10332.00 102.00 303 7.9555 10432.00 10329.60 102.00 304 7.9686 10421.00 10329.70 102.00 305 7.9818 10234.00 10333.50 101.00 306 7.9949 10363.00 10341.70 102.00 307 8.0080 10493.00 10355.10 102.00 308 8.0212 10457.00 10374.30 102.00 309 8.0343 10394.00 10399.90 102.00 310 8.0474 10357.00 10433.20 102.00 311 8.0605 10476.00 10476.70 102.00 312 8.0737 10488.00 10534.00 102.00 313 8.0868 10554.00 10609.60 103.00 314 8.0999 10634.00 10705.60 103.00 315 8.1131 10774.00 10816.70 104.00 316 8.1262 11096.00 10924.80 105.00 317 8.1393 11375.00 10999.60 107.00 318 8.1525 11337.00 11009.50 106.00 319 8.1656 11208.00 10939.70 106.00 320 8.1787 10968.00 10803.30 105.00 321 8.1919 10545.00 10636.50 103.00 322 8.2050 10484.00 10479.90 102.00 323 8.2181 10317.00 10359.80 102.00 324 8.2312 10371.00 10282.40 102.00 325 8.2444 10245.00 10239.00 101.00 326 8.2575 10313.00 10217.00 102.00 327 8.2706 10319.00 10205.60 102.00 328 8.2838 10238.00 10198.60 101.00 329 8.2969 10188.00 10193.20 101.00 330 8.3100 10264.00 10188.20 101.00 331 8.3232 10116.00 10183.30 101.00 332 8.3363 10182.00 10178.50 101.00 333 8.3494 10209.00 10173.70 101.00 334 8.3625 10087.00 10168.80 100.00 335 8.3757 10074.00 10164.00 100.00 336 8.3888 10104.00 10159.20 101.00 337 8.4019 10096.00 10154.40 100.00 338 8.4151 10129.00 10149.60 101.00 339 8.4282 10023.00 10144.80 100.00 340 8.4413 9996.00 10140.00 100.00 341 8.4545 10175.00 10135.30 101.00 342 8.4676 10038.00 10130.50 100.00 343 8.4807 10039.00 10125.70 100.00 344 8.4938 10105.00 10120.90 101.00 345 8.5070 9985.00 10116.10 100.00 346 8.5201 10088.00 10111.40 100.00 347 8.5332 10101.00 10106.60 101.00 348 8.5464 9974.00 10101.80 100.00 349 8.5595 10032.00 10097.00 100.00 350 8.5726 10199.00 10092.20 101.00 351 8.5858 10055.00 10087.50 100.00 352 8.5989 10279.00 10082.70 101.00 353 8.6120 9940.00 10077.90 100.00 354 8.6251 10031.00 10073.10 100.00 355 8.6383 10036.00 10068.30 100.00 356 8.6514 10059.00 10063.50 100.00 357 8.6645 10224.00 10058.70 101.00 358 8.6777 10177.00 10053.90 101.00 359 8.6908 9922.00 10049.10 100.00 360 8.7039 10019.00 10044.30 100.00 361 8.7171 9957.00 10039.50 100.00 362 8.7302 10143.00 10034.60 101.00 363 8.7433 10119.00 10029.80 101.00 364 8.7565 10043.00 10025.00 100.00 365 8.7696 10037.00 10020.10 100.00 366 8.7827 10035.00 10015.30 100.00 367 8.7958 9915.00 10010.40 100.00 368 8.8090 9888.00 10005.60 99.00 369 8.8221 10015.00 10000.70 100.00 370 8.8352 9905.00 9995.83 100.00 371 8.8484 9946.00 9990.94 100.00 372 8.8615 10020.00 9986.05 100.00 373 8.8746 9956.00 9981.14 100.00 374 8.8878 9881.00 9976.23 99.00 375 8.9009 10051.00 9971.32 100.00 376 8.9140 10092.00 9966.39 100.00 377 8.9271 9933.00 9961.45 100.00 378 8.9403 9892.00 9956.51 99.00 379 8.9534 9848.00 9951.55 99.00 380 8.9665 9812.00 9946.59 99.00 381 8.9797 9982.00 9941.62 100.00 382 8.9928 9707.00 9936.63 99.00 383 9.0059 9754.00 9931.64 99.00 384 9.0191 9782.00 9926.64 99.00 385 9.0322 9820.00 9921.63 99.00 386 9.0453 9887.00 9916.61 99.00 387 9.0584 9959.00 9911.58 100.00 388 9.0716 9934.00 9906.54 100.00 389 9.0847 9853.00 9901.49 99.00 390 9.0978 9921.00 9896.43 100.00 391 9.1110 9744.00 9891.36 99.00 392 9.1241 9724.00 9886.28 99.00 393 9.1372 9783.00 9881.19 99.00 394 9.1504 9830.00 9876.09 99.00 395 9.1635 9830.00 9870.98 99.00 396 9.1766 9570.00 9865.86 98.00 397 9.1898 9738.00 9860.74 99.00 398 9.2029 9764.00 9855.60 99.00 399 9.2160 9807.00 9850.45 99.00 400 9.2291 9808.00 9845.29 99.00 401 9.2423 9685.00 9840.13 98.00 402 9.2554 9785.00 9834.96 99.00 403 9.2685 9743.00 9829.77 99.00 404 9.2817 9915.00 9824.58 100.00 405 9.2948 9816.00 9819.38 99.00 406 9.3079 9642.00 9814.17 98.00 407 9.3211 9706.00 9808.95 99.00 408 9.3342 9894.00 9803.72 99.00 409 9.3473 9901.00 9798.48 100.00 410 9.3604 9737.00 9793.24 99.00 411 9.3736 9599.00 9787.99 98.00 412 9.3867 9747.00 9782.73 99.00 413 9.3998 9628.00 9777.46 98.00 414 9.4130 9723.00 9772.19 99.00 415 9.4261 9725.00 9766.90 99.00 416 9.4392 9773.00 9761.61 99.00 417 9.4524 9596.00 9756.32 98.00 418 9.4655 9584.00 9751.02 98.00 419 9.4786 9697.00 9745.71 98.00 420 9.4917 9561.00 9740.39 98.00 421 9.5049 9595.00 9735.07 98.00 422 9.5180 9904.00 9729.74 100.00 423 9.5311 9672.00 9724.41 98.00 424 9.5443 9634.00 9719.08 98.00 425 9.5574 9425.00 9713.73 97.00 426 9.5705 9675.00 9708.38 98.00 427 9.5837 9687.00 9703.03 98.00 428 9.5968 9590.00 9697.67 98.00 429 9.6099 9667.00 9692.32 98.00 430 9.6231 9572.00 9686.97 98.00 431 9.6362 9571.00 9681.63 98.00 432 9.6493 9660.00 9676.33 98.00 433 9.6624 9676.00 9671.12 98.00 434 9.6756 9643.00 9666.03 98.00 435 9.6887 9517.00 9661.14 98.00 436 9.7018 9635.00 9656.52 98.00 437 9.7150 9478.00 9652.22 97.00 438 9.7281 9598.00 9648.32 98.00 439 9.7412 9544.00 9644.93 98.00 440 9.7544 9681.00 9642.21 98.00 441 9.7675 9728.00 9640.30 99.00 442 9.7806 9448.00 9639.22 97.00 443 9.7937 9615.00 9638.58 98.00 444 9.8069 9571.00 9637.52 98.00 445 9.8200 9840.00 9634.79 99.00 446 9.8331 9743.00 9629.33 99.00 447 9.8463 9655.00 9620.88 98.00 448 9.8594 9548.00 9610.22 98.00 449 9.8725 9383.00 9598.80 97.00 450 9.8857 9486.00 9588.02 97.00 451 9.8988 9473.00 9578.67 97.00 452 9.9119 9482.00 9570.84 97.00 453 9.9250 9364.00 9564.20 97.00 454 9.9382 9373.00 9558.27 97.00 455 9.9513 9410.00 9552.70 97.00 456 9.9644 9386.00 9547.29 97.00 457 9.9776 9496.00 9541.93 97.00 458 9.9907 9407.00 9536.59 97.00 459 10.0038 9404.00 9531.26 97.00 460 10.0170 9587.00 9525.93 98.00 461 10.0301 9442.00 9520.62 97.00 462 10.0432 9615.00 9515.31 98.00 463 10.0564 9532.00 9510.01 98.00 464 10.0695 9317.00 9504.72 97.00 465 10.0826 9561.00 9499.43 98.00 466 10.0957 9385.00 9494.16 97.00 467 10.1089 9473.00 9488.89 97.00 468 10.1220 9289.00 9483.63 96.00 469 10.1351 9454.00 9478.90 97.00 470 10.1483 9331.00 9473.71 97.00 471 10.1614 9608.00 9468.79 98.00 472 10.1745 9523.00 9463.66 98.00 473 10.1877 9420.00 9458.56 97.00 474 10.2008 9516.00 9453.49 98.00 475 10.2139 9348.00 9448.45 97.00 476 10.2270 9295.00 9443.46 96.00 477 10.2402 9353.00 9438.51 97.00 478 10.2533 9634.00 9433.63 98.00 479 10.2664 9355.00 9428.84 97.00 480 10.2796 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9300.96 97.00 914 15.9781 9449.00 9314.38 97.00 915 15.9912 9708.00 9332.28 99.00 916 16.0044 9468.00 9359.11 97.00 917 16.0175 9603.00 9408.95 98.00 918 16.0306 9527.00 9514.83 98.00 919 16.0438 9894.00 9731.09 99.00 920 16.0569 10145.00 10122.10 101.00 921 16.0700 10774.00 10766.60 104.00 922 16.0832 11375.00 11792.70 107.00 923 16.0963 13081.00 13335.30 114.00 924 16.1094 15218.00 15205.10 123.00 925 16.1225 16795.00 16628.50 130.00 926 16.1357 16779.00 16943.30 130.00 927 16.1488 17045.00 16848.70 131.00 928 16.1619 17387.00 17137.00 132.00 929 16.1751 17896.00 17490.40 134.00 930 16.1882 17811.00 17650.60 133.00 931 16.2013 17731.00 17661.50 133.00 932 16.2145 17177.00 17345.80 131.00 933 16.2276 16275.00 16527.80 128.00 934 16.2407 15020.00 15280.30 123.00 935 16.2539 13817.00 13849.60 118.00 936 16.2670 12399.00 12491.30 111.00 937 16.2801 11508.00 11389.40 107.00 938 16.2932 10804.00 10633.40 104.00 939 16.3064 10565.00 10220.40 103.00 940 16.3195 10614.00 10075.00 103.00 941 16.3326 10418.00 10087.20 102.00 942 16.3458 10476.00 10150.40 102.00 943 16.3589 10653.00 10188.70 103.00 944 16.3720 10561.00 10166.90 103.00 945 16.3852 10364.00 10086.30 102.00 946 16.3983 10413.00 9969.20 102.00 947 16.4114 10230.00 9842.65 101.00 948 16.4245 10013.00 9728.53 100.00 949 16.4377 9896.00 9640.31 99.00 950 16.4508 9608.00 9582.36 98.00 951 16.4639 9673.00 9554.53 98.00 952 16.4771 9714.00 9542.99 99.00 953 16.4902 9735.00 9537.58 99.00 954 16.5033 9825.00 9544.58 99.00 955 16.5165 9608.00 9552.36 98.00 956 16.5296 9804.00 9558.43 99.00 957 16.5427 9595.00 9567.56 98.00 958 16.5558 9614.00 9576.90 98.00 959 16.5690 9408.00 9586.46 97.00 960 16.5821 9666.00 9603.32 98.00 961 16.5952 9804.00 9614.00 99.00 962 16.6084 9724.00 9625.11 99.00 963 16.6215 9563.00 9640.20 98.00 964 16.6346 9788.00 9652.82 99.00 965 16.6478 9812.00 9666.38 99.00 966 16.6609 9547.00 9681.22 98.00 967 16.6740 9803.00 9698.13 99.00 968 16.6871 9803.00 9718.46 99.00 969 16.7003 9839.00 9747.46 99.00 970 16.7134 9775.00 9798.14 99.00 971 16.7265 9892.00 9893.18 99.00 972 16.7397 10038.00 10060.40 100.00 973 16.7528 10819.00 10332.10 104.00 974 16.7659 11055.00 10760.20 105.00 975 16.7791 11567.00 11383.80 108.00 976 16.7922 12739.00 12074.50 113.00 977 16.8053 12932.00 12439.50 114.00 978 16.8185 12566.00 12213.00 112.00 979 16.8316 12279.00 11814.80 111.00 980 16.8447 12094.00 11609.40 110.00 981 16.8578 11856.00 11531.70 109.00 982 16.8710 11438.00 11641.20 107.00 983 16.8841 11873.00 12233.80 109.00 984 16.8972 13217.00 13416.30 115.00 985 16.9104 14760.00 14847.40 121.00 986 16.9235 15332.00 15611.50 124.00 987 16.9366 14734.00 15053.90 121.00 988 16.9498 14285.00 13978.20 120.00 989 16.9629 13716.00 13156.50 117.00 990 16.9760 12609.00 12296.40 112.00 991 16.9891 11473.00 11336.10 107.00 992 17.0023 10766.00 10673.40 104.00 993 17.0154 10505.00 10381.80 102.00 994 17.0285 10473.00 10278.30 102.00 995 17.0417 10216.00 10233.90 101.00 996 17.0548 10502.00 10220.50 102.00 997 17.0679 10352.00 10227.30 102.00 998 17.0811 10307.00 10261.70 102.00 999 17.0942 10560.00 10374.50 103.00 1000 17.1073 10848.00 10649.70 104.00 1001 17.1204 11573.00 11189.00 108.00 1002 17.1336 12398.00 12107.10 111.00 1003 17.1467 13878.00 13581.60 118.00 1004 17.1598 15674.00 15738.40 125.00 1005 17.1730 17691.00 18085.20 133.00 1006 17.1861 18021.00 19211.60 134.00 1007 17.1992 17283.00 18204.10 131.00 1008 17.2124 16276.00 16487.10 128.00 1009 17.2255 15249.00 15207.60 123.00 1010 17.2386 13567.00 13823.70 116.00 1011 17.2518 11990.00 12240.00 109.00 1012 17.2649 11377.00 11115.50 107.00 1013 17.2780 11074.00 10596.20 105.00 1014 17.2911 10591.00 10415.30 103.00 1015 17.3043 10416.00 10359.60 102.00 1016 17.3174 10346.00 10338.80 102.00 1017 17.3305 10352.00 10332.90 102.00 1018 17.3437 10513.00 10334.90 103.00 1019 17.3568 10138.00 10350.60 101.00 1020 17.3699 10289.00 10383.30 101.00 1021 17.3831 10346.00 10449.10 102.00 1022 17.3962 10621.00 10577.40 103.00 1023 17.4093 10743.00 10809.60 104.00 1024 17.4224 10993.00 11200.00 105.00 1025 17.4356 11661.00 11813.00 108.00 1026 17.4487 12910.00 12650.30 114.00 1027 17.4618 13478.00 13488.30 116.00 1028 17.4750 13725.00 13892.20 117.00 1029 17.4881 13283.00 13670.80 115.00 1030 17.5012 13074.00 13120.50 114.00 1031 17.5144 12493.00 12625.50 112.00 1032 17.5275 12086.00 12196.80 110.00 1033 17.5406 11556.00 11789.30 107.00 1034 17.5537 11236.00 11496.90 106.00 1035 17.5669 11199.00 11329.70 106.00 1036 17.5800 11122.00 11154.20 105.00 1037 17.5931 10968.00 10996.10 105.00 1038 17.6063 10882.00 10892.40 104.00 1039 17.6194 10882.00 10792.40 104.00 1040 17.6325 10674.00 10675.60 103.00 1041 17.6457 10464.00 10592.60 102.00 1042 17.6588 10647.00 10557.70 103.00 1043 17.6719 10302.00 10552.60 101.00 1044 17.6850 10636.00 10557.10 103.00 1045 17.6982 10553.00 10570.80 103.00 1046 17.7113 10614.00 10581.30 103.00 1047 17.7244 10548.00 10592.20 103.00 1048 17.7376 10525.00 10606.70 103.00 1049 17.7507 10601.00 10619.30 103.00 1050 17.7638 10572.00 10632.40 103.00 1051 17.7770 10634.00 10646.10 103.00 1052 17.7901 10470.00 10660.20 102.00 1053 17.8032 10494.00 10674.90 102.00 1054 17.8164 10805.00 10690.20 104.00 1055 17.8295 10664.00 10706.30 103.00 1056 17.8426 10684.00 10721.70 103.00 1057 17.8557 10695.00 10737.80 103.00 1058 17.8689 10614.00 10757.60 103.00 1059 17.8820 10553.00 10778.20 103.00 1060 17.8951 10766.00 10801.70 104.00 1061 17.9083 10630.00 10827.10 103.00 1062 17.9214 10902.00 10858.80 104.00 1063 17.9345 10907.00 10903.30 104.00 1064 17.9477 10718.00 10978.10 104.00 1065 17.9608 11005.00 11121.60 105.00 1066 17.9739 11276.00 11392.90 106.00 1067 17.9870 11625.00 11871.90 108.00 1068 18.0002 12552.00 12641.90 112.00 1069 18.0133 14101.00 13735.80 119.00 1070 18.0264 15502.00 14995.30 125.00 1071 18.0396 16040.00 15937.60 127.00 1072 18.0527 15753.00 15971.50 126.00 1073 18.0658 14885.00 15127.10 122.00 1074 18.0790 14336.00 14250.20 120.00 1075 18.0921 13583.00 13581.70 117.00 1076 18.1052 12927.00 12798.50 114.00 1077 18.1183 11728.00 11993.00 108.00 1078 18.1315 11503.00 11475.90 107.00 1079 18.1446 11304.00 11256.40 106.00 1080 18.1577 11092.00 11189.60 105.00 1081 18.1709 10986.00 11172.90 105.00 1082 18.1840 11225.00 11170.80 106.00 1083 18.1971 11209.00 11176.50 106.00 1084 18.2103 11172.00 11190.10 106.00 1085 18.2234 11074.00 11212.80 105.00 1086 18.2365 11149.00 11244.90 106.00 1087 18.2496 11049.00 11284.80 105.00 1088 18.2628 11172.00 11330.20 106.00 1089 18.2759 11378.00 11380.30 107.00 1090 18.2890 11309.00 11434.70 106.00 1091 18.3022 11354.00 11480.10 107.00 1092 18.3153 11300.00 11488.00 106.00 1093 18.3284 11453.00 11451.50 107.00 1094 18.3416 11402.00 11411.30 107.00 1095 18.3547 11156.00 11386.90 106.00 1096 18.3678 11299.00 11362.60 106.00 1097 18.3810 11358.00 11335.80 107.00 1098 18.3941 11262.00 11321.20 106.00 1099 18.4072 11394.00 11323.00 107.00 1100 18.4203 11193.00 11327.60 106.00 1101 18.4335 11136.00 11340.30 106.00 1102 18.4466 11299.00 11353.70 106.00 1103 18.4597 11129.00 11369.10 105.00 1104 18.4729 11304.00 11381.40 106.00 1105 18.4860 11300.00 11396.30 106.00 1106 18.4991 11276.00 11411.40 106.00 1107 18.5123 11286.00 11426.60 106.00 1108 18.5254 11194.00 11441.90 106.00 1109 18.5385 11490.00 11457.40 107.00 1110 18.5516 11183.00 11473.10 106.00 1111 18.5648 11386.00 11489.00 107.00 1112 18.5779 11341.00 11505.20 106.00 1113 18.5910 11311.00 11521.70 106.00 1114 18.6042 11360.00 11538.70 107.00 1115 18.6173 11448.00 11556.40 107.00 1116 18.6304 11317.00 11575.10 106.00 1117 18.6436 11502.00 11595.20 107.00 1118 18.6567 11480.00 11618.20 107.00 1119 18.6698 11556.00 11648.30 107.00 1120 18.6829 11733.00 11696.50 108.00 1121 18.6961 11723.00 11783.30 108.00 1122 18.7092 11796.00 11938.40 109.00 1123 18.7223 12186.00 12197.10 110.00 1124 18.7355 12498.00 12596.60 112.00 1125 18.7486 13204.00 13108.30 115.00 1126 18.7617 13133.00 13519.70 115.00 1127 18.7749 13180.00 13523.70 115.00 1128 18.7880 13096.00 13193.80 114.00 1129 18.8011 12609.00 12922.10 112.00 1130 18.8143 12446.00 12746.70 112.00 1131 18.8274 12367.00 12484.50 111.00 1132 18.8405 12271.00 12182.40 111.00 1133 18.8536 11878.00 11984.40 109.00 1134 18.8668 11793.00 11902.90 109.00 1135 18.8799 11498.00 11882.80 107.00 1136 18.8930 11744.00 11883.80 108.00 1137 18.9062 11765.00 11891.80 108.00 1138 18.9193 11763.00 11903.70 108.00 1139 18.9324 11835.00 11918.80 109.00 1140 18.9456 11641.00 11939.40 108.00 1141 18.9587 11760.00 11959.50 108.00 1142 18.9718 12134.00 11979.80 110.00 1143 18.9849 12030.00 11998.20 110.00 1144 18.9981 12020.00 12014.60 110.00 1145 19.0112 11954.00 12026.30 109.00 1146 19.0243 12189.00 12035.30 110.00 1147 19.0375 11963.00 12043.20 109.00 1148 19.0506 11916.00 12051.00 109.00 1149 19.0637 11952.00 12059.90 109.00 1150 19.0769 12036.00 12071.70 110.00 1151 19.0900 11983.00 12090.50 109.00 1152 19.1031 12097.00 12125.10 110.00 1153 19.1162 12222.00 12194.60 111.00 1154 19.1294 12167.00 12334.00 110.00 1155 19.1425 12836.00 12597.00 113.00 1156 19.1556 12906.00 13054.80 114.00 1157 19.1688 13687.00 13742.80 117.00 1158 19.1819 14375.00 14649.50 120.00 1159 19.1950 15333.00 15649.50 124.00 1160 19.2082 16005.00 16530.30 127.00 1161 19.2213 16682.00 17064.40 129.00 1162 19.2344 16821.00 17161.50 130.00 1163 19.2475 16455.00 16901.80 128.00 1164 19.2607 16190.00 16476.00 127.00 1165 19.2738 15945.00 16082.00 126.00 1166 19.2869 15686.00 15823.90 125.00 1167 19.3001 15371.00 15597.00 124.00 1168 19.3132 14936.00 15138.50 122.00 1169 19.3263 14100.00 14423.70 119.00 1170 19.3395 13617.00 13885.50 117.00 1171 19.3526 13548.00 13604.70 116.00 1172 19.3657 13272.00 13341.60 115.00 1173 19.3789 12836.00 13010.50 113.00 1174 19.3920 12609.00 12775.10 112.00 1175 19.4051 12755.00 12682.30 113.00 1176 19.4182 12588.00 12696.10 112.00 1177 19.4314 12598.00 12796.80 112.00 1178 19.4445 13048.00 13029.80 114.00 1179 19.4576 13320.00 13493.00 115.00 1180 19.4708 13911.00 14313.20 118.00 1181 19.4839 15123.00 15610.20 123.00 1182 19.4970 17010.00 17277.70 130.00 1183 19.5102 17704.00 18617.30 133.00 1184 19.5233 17425.00 18625.70 132.00 1185 19.5364 16843.00 17555.60 130.00 1186 19.5495 16458.00 16752.40 128.00 1187 19.5627 15963.00 16417.30 126.00 1188 19.5758 15338.00 15924.50 124.00 1189 19.5889 14750.00 15361.10 121.00 1190 19.6021 14808.00 15336.80 122.00 1191 19.6152 15309.00 16093.50 124.00 1192 19.6283 16493.00 17661.20 128.00 1193 19.6415 19100.00 20098.50 138.00 1194 19.6546 22467.00 23097.80 150.00 1195 19.6677 24669.00 25438.80 157.00 1196 19.6808 24810.00 25826.40 158.00 1197 19.6940 24279.00 24983.10 156.00 1198 19.7071 23381.00 23852.10 153.00 1199 19.7202 21834.00 22031.90 148.00 1200 19.7334 19611.00 19683.30 140.00 1201 19.7465 17410.00 17615.80 132.00 1202 19.7596 15862.00 16005.70 126.00 1203 19.7728 14297.00 14690.40 120.00 1204 19.7859 13683.00 13833.70 117.00 1205 19.7990 13428.00 13440.20 116.00 1206 19.8122 13280.00 13341.80 115.00 1207 19.8253 13462.00 13384.10 116.00 1208 19.8384 13146.00 13484.10 115.00 1209 19.8515 13473.00 13590.80 116.00 1210 19.8647 13377.00 13662.30 116.00 1211 19.8778 13321.00 13673.30 115.00 1212 19.8909 13385.00 13623.80 116.00 1213 19.9041 13316.00 13526.00 115.00 1214 19.9172 13280.00 13416.20 115.00 1215 19.9303 13291.00 13303.30 115.00 1216 19.9435 13251.00 13198.50 115.00 1217 19.9566 12963.00 13108.10 114.00 1218 19.9697 13305.00 13045.90 115.00 1219 19.9828 13174.00 13009.20 115.00 1220 19.9960 12915.00 12993.10 114.00 1221 20.0091 12977.00 12996.50 114.00 1222 20.0222 13140.00 13000.60 115.00 1223 20.0354 13062.00 13007.70 114.00 1224 20.0485 13155.00 13019.10 115.00 1225 20.0616 12995.00 13017.70 114.00 1226 20.0748 12960.00 13027.80 114.00 1227 20.0879 12917.00 13032.20 114.00 1228 20.1010 12948.00 13037.70 114.00 1229 20.1141 12935.00 13049.10 114.00 1230 20.1273 13004.00 13060.80 114.00 1231 20.1404 13129.00 13069.90 115.00 1232 20.1535 12989.00 13082.50 114.00 1233 20.1667 13065.00 13095.50 114.00 1234 20.1798 13147.00 13109.20 115.00 1235 20.1929 12975.00 13123.80 114.00 1236 20.2061 12967.00 13139.60 114.00 1237 20.2192 12852.00 13157.10 113.00 1238 20.2323 13044.00 13177.10 114.00 1239 20.2454 13245.00 13201.10 115.00 1240 20.2586 13151.00 13232.50 115.00 1241 20.2717 13179.00 13281.50 115.00 1242 20.2848 13333.00 13375.50 115.00 1243 20.2980 13480.00 13571.30 116.00 1244 20.3111 13814.00 13956.20 118.00 1245 20.3242 14246.00 14633.90 119.00 1246 20.3374 15204.00 15665.90 123.00 1247 20.3505 16421.00 16865.60 128.00 1248 20.3636 16935.00 17601.10 130.00 1249 20.3768 16240.00 17265.60 127.00 1250 20.3899 16173.00 16403.70 127.00 1251 20.4030 15595.00 15879.80 125.00 1252 20.4161 15676.00 15579.60 125.00 1253 20.4293 14873.00 15001.20 122.00 1254 20.4424 14448.00 14266.60 120.00 1255 20.4555 13803.00 13749.20 117.00 1256 20.4687 13485.00 13509.20 116.00 1257 20.4818 13455.00 13426.30 116.00 1258 20.4949 13553.00 13401.60 116.00 1259 20.5081 13299.00 13391.50 115.00 1260 20.5212 13447.00 13383.50 116.00 1261 20.5343 13188.00 13376.30 115.00 1262 20.5474 13401.00 13373.10 116.00 1263 20.5606 13503.00 13373.10 116.00 1264 20.5737 13375.00 13373.40 116.00 1265 20.5868 13470.00 13373.80 116.00 1266 20.6000 13482.00 13375.90 116.00 1267 20.6131 13404.00 13380.30 116.00 1268 20.6262 13644.00 13386.60 117.00 1269 20.6394 13312.00 13394.40 115.00 1270 20.6525 13328.00 13403.70 115.00 1271 20.6656 13620.00 13414.30 117.00 1272 20.6787 13347.00 13426.20 116.00 1273 20.6919 13400.00 13439.80 116.00 1274 20.7050 13662.00 13457.60 117.00 1275 20.7181 13539.00 13487.20 116.00 1276 20.7313 13688.00 13547.00 117.00 1277 20.7444 13746.00 13668.10 117.00 1278 20.7575 13712.00 13885.80 117.00 1279 20.7707 14017.00 14243.20 118.00 1280 20.7838 14631.00 14697.60 121.00 1281 20.7969 14694.00 15052.10 121.00 1282 20.8101 14531.00 15032.10 121.00 1283 20.8232 14565.00 14719.70 121.00 1284 20.8363 14393.00 14485.40 120.00 1285 20.8494 14239.00 14389.90 119.00 1286 20.8626 14152.00 14230.60 119.00 1287 20.8757 14108.00 13954.30 119.00 1288 20.8888 13860.00 13718.10 118.00 1289 20.9020 13522.00 13592.40 116.00 1290 20.9151 13920.00 13543.60 118.00 1291 20.9282 13584.00 13525.00 117.00 1292 20.9414 13714.00 13519.00 117.00 1293 20.9545 13537.00 13515.90 116.00 1294 20.9676 13455.00 13518.10 116.00 1295 20.9807 13513.00 13522.10 116.00 1296 20.9939 13679.00 13529.70 117.00 1297 21.0070 13328.00 13536.50 115.00 1298 21.0201 13673.00 13541.10 117.00 1299 21.0333 13542.00 13541.00 116.00 1300 21.0464 13611.00 13541.00 117.00 1301 21.0595 13486.00 13543.00 116.00 1302 21.0727 13655.00 13545.50 117.00 1303 21.0858 13944.00 13546.70 118.00 1304 21.0989 13456.00 13562.50 116.00 1305 21.1120 13580.00 13566.50 117.00 1306 21.1252 13730.00 13572.40 117.00 1307 21.1383 13615.00 13583.00 117.00 1308 21.1514 13625.00 13600.40 117.00 1309 21.1646 13800.00 13615.50 117.00 1310 21.1777 13631.00 13637.80 117.00 1311 21.1908 13716.00 13670.60 117.00 1312 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11353.80 107.00 1682 26.0622 11140.00 11515.40 106.00 1683 26.0753 11356.00 11484.40 107.00 1684 26.0884 11127.00 11301.40 105.00 1685 26.1016 11009.00 11059.20 105.00 1686 26.1147 10788.00 10821.00 104.00 1687 26.1278 10745.00 10581.20 104.00 1688 26.1409 10414.00 10312.60 102.00 1689 26.1541 10022.00 10012.10 100.00 1690 26.1672 9721.00 9716.05 99.00 1691 26.1803 9650.00 9466.30 98.00 1692 26.1935 9545.00 9281.84 98.00 1693 26.2066 9457.00 9157.59 97.00 1694 26.2197 9102.00 9077.61 95.00 1695 26.2329 9075.00 9026.79 95.00 1696 26.2460 9066.00 8994.14 95.00 1697 26.2591 9103.00 8971.93 95.00 1698 26.2722 8954.00 8955.47 95.00 1699 26.2854 9058.00 8942.71 95.00 1700 26.2985 8971.00 8934.71 95.00 1701 26.3116 8890.00 8934.14 94.00 1702 26.3248 9003.00 8948.23 95.00 1703 26.3379 8890.00 8969.98 94.00 1704 26.3510 9015.00 8990.52 95.00 1705 26.3642 9003.00 8997.26 95.00 1706 26.3773 8920.00 8988.64 94.00 1707 26.3904 8989.00 8989.60 95.00 1708 26.4036 9026.00 9007.08 95.00 1709 26.4167 9123.00 9031.91 96.00 1710 26.4298 9140.00 9056.47 96.00 1711 26.4430 9207.00 9083.55 96.00 1712 26.4561 9151.00 9096.81 96.00 1713 26.4692 8896.00 9054.91 94.00 1714 26.4823 8989.00 8968.26 95.00 1715 26.4955 8974.00 8894.69 95.00 1716 26.5086 8874.00 8860.11 94.00 1717 26.5217 8777.00 8846.16 94.00 1718 26.5349 8691.00 8817.76 93.00 1719 26.5480 8648.00 8773.50 93.00 1720 26.5611 8861.00 8745.60 94.00 1721 26.5742 8646.00 8749.09 93.00 1722 26.5874 8618.00 8775.22 93.00 1723 26.6005 8927.00 8797.72 94.00 1724 26.6136 8910.00 8794.32 94.00 1725 26.6268 8681.00 8778.19 93.00 1726 26.6399 8738.00 8792.44 93.00 1727 26.6530 9031.00 8884.98 95.00 1728 26.6662 9156.00 9092.86 96.00 1729 26.6793 9437.00 9436.10 97.00 1730 26.6924 9939.00 9875.90 100.00 1731 26.7055 10559.00 10260.90 103.00 1732 26.7187 10540.00 10324.40 103.00 1733 26.7318 10086.00 9966.57 100.00 1734 26.7449 9665.00 9558.99 98.00 1735 26.7581 9525.00 9383.60 98.00 1736 26.7712 9752.00 9388.30 99.00 1737 26.7843 9160.00 9351.75 96.00 1738 26.7975 9192.00 9118.51 96.00 1739 26.8106 8774.00 8810.60 94.00 1740 26.8237 8652.00 8583.10 93.00 1741 26.8369 8570.00 8458.54 93.00 1742 26.8500 8216.00 8397.64 91.00 1743 26.8631 8200.00 8364.23 91.00 1744 26.8763 8391.00 8342.18 92.00 1745 26.8894 8414.00 8330.07 92.00 1746 26.9025 8209.00 8331.68 91.00 1747 26.9156 8568.00 8352.82 93.00 1748 26.9288 8386.00 8390.68 92.00 1749 26.9419 8302.00 8423.20 91.00 1750 26.9550 8369.00 8414.44 91.00 1751 26.9682 8129.00 8358.14 90.00 1752 26.9813 8252.00 8301.22 91.00 1753 26.9944 8261.00 8273.46 91.00 1754 27.0076 8211.00 8266.54 91.00 1755 27.0207 8255.00 8252.88 91.00 1756 27.0338 8342.00 8216.37 91.00 1757 27.0469 8194.00 8172.38 91.00 1758 27.0601 8182.00 8137.41 90.00 1759 27.0732 8075.00 8112.96 90.00 1760 27.0863 8088.00 8094.28 90.00 1761 27.0995 8032.00 8077.62 90.00 1762 27.1126 8185.00 8062.18 90.00 1763 27.1257 8190.00 8047.68 90.00 1764 27.1388 8404.00 8032.19 92.00 1765 27.1520 8351.00 8025.52 91.00 1766 27.1651 8225.00 8032.41 91.00 1767 27.1782 8441.00 8076.64 92.00 1768 27.1914 8429.00 8199.97 92.00 1769 27.2045 8860.00 8453.33 94.00 1770 27.2176 9197.00 8871.39 96.00 1771 27.2308 9495.00 9409.84 97.00 1772 27.2439 9993.00 9927.63 100.00 1773 27.2570 10137.00 10237.60 101.00 1774 27.2702 9871.00 10234.90 99.00 1775 27.2833 9730.00 9982.97 99.00 1776 27.2964 9414.00 9659.63 97.00 1777 27.3096 9539.00 9404.20 98.00 1778 27.3227 9271.00 9220.79 96.00 1779 27.3358 9192.00 9025.57 96.00 1780 27.3489 8958.00 8761.88 95.00 1781 27.3621 8744.00 8457.44 94.00 1782 27.3752 8496.00 8186.38 92.00 1783 27.3883 8225.00 8003.25 91.00 1784 27.4015 8097.00 7911.51 90.00 1785 27.4146 7877.00 7877.55 89.00 1786 27.4277 7864.00 7857.91 89.00 1787 27.4409 7924.00 7828.77 89.00 1788 27.4540 7873.00 7801.67 89.00 1789 27.4671 7899.00 7791.29 89.00 1790 27.4802 7956.00 7801.74 89.00 1791 27.4934 7874.00 7835.42 89.00 1792 27.5065 8066.00 7904.43 90.00 1793 27.5196 8108.00 8022.97 90.00 1794 27.5328 8282.00 8168.49 91.00 1795 27.5459 8408.00 8250.73 92.00 1796 27.5590 8118.00 8180.21 90.00 1797 27.5721 7998.00 8032.28 89.00 1798 27.5853 8121.00 7942.35 90.00 1799 27.5984 8051.00 7952.95 90.00 1800 27.6115 8119.00 8013.34 90.00 1801 27.6247 8090.00 8036.69 90.00 1802 27.6378 8006.00 7985.03 89.00 1803 27.6509 7794.00 7880.72 88.00 1804 27.6641 7641.00 7767.32 87.00 1805 27.6772 7720.00 7695.52 88.00 1806 27.6903 7805.00 7671.03 88.00 1807 27.7035 7678.00 7671.47 88.00 1808 27.7166 7732.00 7662.19 88.00 1809 27.7297 7503.00 7626.59 87.00 1810 27.7429 7605.00 7582.52 87.00 1811 27.7560 7544.00 7547.95 87.00 1812 27.7691 7527.00 7524.43 87.00 1813 27.7822 7386.00 7509.46 86.00 1814 27.7954 7529.00 7499.32 87.00 1815 27.8085 7482.00 7491.71 86.00 1816 27.8216 7437.00 7487.02 86.00 1817 27.8348 7482.00 7487.74 86.00 1818 27.8479 7459.00 7503.01 86.00 1819 27.8610 7572.00 7548.01 87.00 1820 27.8742 7681.00 7637.17 88.00 1821 27.8873 7736.00 7768.00 88.00 1822 27.9004 7837.00 7901.31 89.00 1823 27.9135 8080.00 7999.83 90.00 1824 27.9267 8208.00 8124.99 91.00 1825 27.9398 8760.00 8410.24 94.00 1826 27.9529 9003.00 8827.89 95.00 1827 27.9661 9098.00 9112.51 95.00 1828 27.9792 8757.00 8967.99 94.00 1829 27.9923 8614.00 8535.90 93.00 1830 28.0055 8247.00 8227.72 91.00 1831 28.0186 8479.00 8194.73 92.00 1832 28.0317 8368.00 8327.81 91.00 1833 28.0448 8307.00 8429.97 91.00 1834 28.0580 8120.00 8441.78 90.00 1835 28.0711 8250.00 8459.37 91.00 1836 28.0842 8148.00 8440.57 90.00 1837 28.0974 8085.00 8270.95 90.00 1838 28.1105 7909.00 8046.39 89.00 1839 28.1236 7853.00 7911.35 89.00 1840 28.1367 7792.00 7881.18 88.00 1841 28.1499 7636.00 7881.02 87.00 1842 28.1630 7767.00 7815.92 88.00 1843 28.1761 7653.00 7694.31 87.00 1844 28.1893 7639.00 7607.73 87.00 1845 28.2024 7466.00 7581.26 86.00 1846 28.2155 7406.00 7572.18 86.00 1847 28.2287 7440.00 7538.99 86.00 1848 28.2418 7564.00 7526.52 87.00 1849 28.2549 7624.00 7615.49 87.00 1850 28.2681 7971.00 7803.92 89.00 1851 28.2812 8038.00 7974.83 90.00 1852 28.2943 8059.00 7957.89 90.00 1853 28.3075 7739.00 7755.52 88.00 1854 28.3206 7622.00 7575.74 87.00 1855 28.3337 7641.00 7527.63 87.00 1856 28.3468 7805.00 7578.54 88.00 1857 28.3600 7822.00 7621.50 88.00 1858 28.3731 7707.00 7578.00 88.00 1859 28.3862 7473.00 7485.55 86.00 1860 28.3994 7607.00 7400.20 87.00 1861 28.4125 7388.00 7343.94 86.00 1862 28.4256 7466.00 7312.49 86.00 1863 28.4388 7317.00 7304.00 86.00 1864 28.4519 7323.00 7306.90 86.00 1865 28.4650 7280.00 7298.17 85.00 1866 28.4781 7192.00 7263.21 85.00 1867 28.4913 7285.00 7204.58 85.00 1868 28.5044 7268.00 7142.08 85.00 1869 28.5175 7119.00 7099.88 84.00 1870 28.5307 7353.00 7082.70 86.00 1871 28.5438 7132.00 7079.80 84.00 1872 28.5569 7320.00 7074.93 86.00 1873 28.5701 7071.00 7057.98 84.00 1874 28.5832 7234.00 7027.31 85.00 1875 28.5963 6994.00 6991.44 84.00 1876 28.6094 7154.00 6958.50 85.00 1877 28.6226 6926.00 6934.15 83.00 1878 28.6357 7071.00 6918.36 84.00 1879 28.6488 6905.00 6907.50 83.00 1880 28.6620 6905.00 6901.47 83.00 1881 28.6751 6968.00 6905.46 83.00 1882 28.6882 7062.00 6930.69 84.00 1883 28.7014 6889.00 6984.05 83.00 1884 28.7145 6914.00 7051.19 83.00 1885 28.7276 6928.00 7093.33 83.00 1886 28.7408 7065.00 7064.88 84.00 1887 28.7539 6998.00 7000.34 84.00 1888 28.7670 6926.00 6975.51 83.00 1889 28.7801 7024.00 7025.64 84.00 1890 28.7933 7152.00 7138.96 85.00 1891 28.8064 7433.00 7254.99 86.00 1892 28.8195 7337.00 7285.15 86.00 1893 28.8327 7204.00 7189.42 85.00 1894 28.8458 7036.00 7049.68 84.00 1895 28.8589 6937.00 6976.88 83.00 1896 28.8721 7077.00 7004.23 84.00 1897 28.8852 7115.00 7088.85 84.00 1898 28.8983 7035.00 7141.65 84.00 1899 28.9114 7070.00 7093.79 84.00 1900 28.9246 7040.00 6976.50 84.00 1901 28.9377 6859.00 6877.97 83.00 1902 28.9508 6825.00 6833.07 83.00 1903 28.9640 6742.00 6819.92 82.00 1904 28.9771 6760.00 6804.33 82.00 1905 28.9902 6686.00 6766.52 82.00 1906 29.0034 6678.00 6716.60 82.00 1907 29.0165 6674.00 6676.59 82.00 1908 29.0296 6483.00 6649.24 81.00 1909 29.0427 6498.00 6626.90 81.00 1910 29.0559 6621.00 6608.79 81.00 1911 29.0690 6612.00 6595.91 81.00 1912 29.0821 6594.00 6589.76 81.00 1913 29.0953 6625.00 6592.07 81.00 1914 29.1084 6591.00 6608.24 81.00 1915 29.1215 6666.00 6646.15 82.00 1916 29.1347 6862.00 6704.90 83.00 1917 29.1478 6823.00 6763.04 83.00 1918 29.1609 6787.00 6780.94 82.00 1919 29.1741 6650.00 6753.56 82.00 1920 29.1872 6747.00 6747.90 82.00 1921 29.2003 6805.00 6835.19 82.00 1922 29.2134 7090.00 7044.11 84.00 1923 29.2266 7244.00 7324.82 85.00 1924 29.2397 7361.00 7524.49 86.00 1925 29.2528 7213.00 7471.94 85.00 1926 29.2660 7056.00 7214.58 84.00 1927 29.2791 6898.00 6993.15 83.00 1928 29.2922 6783.00 6924.75 82.00 1929 29.3054 6865.00 6965.59 83.00 1930 29.3185 7003.00 6991.02 84.00 1931 29.3316 6715.00 6899.41 82.00 1932 29.3447 6837.00 6737.22 83.00 1933 29.3579 6683.00 6601.42 82.00 1934 29.3710 6728.00 6521.29 82.00 1935 29.3841 6631.00 6484.00 81.00 1936 29.3973 6640.00 6475.64 81.00 1937 29.4104 6693.00 6495.94 82.00 1938 29.4235 6807.00 6551.81 83.00 1939 29.4367 6821.00 6635.03 83.00 1940 29.4498 6893.00 6705.43 83.00 1941 29.4629 6875.00 6707.95 83.00 1942 29.4760 6769.00 6643.72 82.00 1943 29.4892 6740.00 6589.07 82.00 1944 29.5023 6645.00 6589.90 82.00 1945 29.5154 6660.00 6624.42 82.00 1946 29.5286 6739.00 6645.69 82.00 1947 29.5417 6648.00 6613.58 82.00 1948 29.5548 6506.00 6541.00 81.00 1949 29.5680 6472.00 6472.42 80.00 1950 29.5811 6532.00 6431.95 81.00 1951 29.5942 6491.00 6415.07 81.00 1952 29.6074 6454.00 6411.24 80.00 1953 29.6205 6516.00 6407.70 81.00 1954 29.6336 6388.00 6397.29 80.00 1955 29.6467 6515.00 6378.82 81.00 1956 29.6599 6375.00 6357.39 80.00 1957 29.6730 6358.00 6339.57 80.00 1958 29.6861 6443.00 6334.06 80.00 1959 29.6993 6331.00 6338.44 80.00 1960 29.7124 6217.00 6346.65 79.00 1961 29.7255 6381.00 6352.44 80.00 1962 29.7387 6383.00 6354.78 80.00 1963 29.7518 6312.00 6357.65 79.00 1964 29.7649 6252.00 6368.29 79.00 1965 29.7780 6400.00 6385.81 80.00 1966 29.7912 6308.00 6402.95 79.00 1967 29.8043 6415.00 6411.25 80.00 1968 29.8174 6301.00 6409.23 79.00 1969 29.8306 6367.00 6404.87 80.00 1970 29.8437 6289.00 6410.62 79.00 1971 29.8568 6239.00 6445.84 79.00 1972 29.8700 6580.00 6547.75 81.00 1973 29.8831 6824.00 6763.18 83.00 1974 29.8962 6958.00 7079.40 83.00 1975 29.9093 7130.00 7363.43 84.00 1976 29.9225 6990.00 7395.65 84.00 1977 29.9356 6722.00 7152.28 82.00 1978 29.9487 6685.00 6907.40 82.00 1979 29.9619 6660.00 6821.28 82.00 1980 29.9750 6771.00 6847.48 82.00 1981 29.9881 6590.00 6866.77 81.00 1982 30.0013 6605.00 6775.95 81.00 1983 30.0144 6362.00 6596.32 80.00 1984 30.0275 6308.00 6443.24 79.00 1985 30.0407 6205.00 6346.63 79.00 1986 30.0538 6116.00 6273.57 78.00 1987 30.0669 6081.00 6208.64 78.00 1988 30.0800 6123.00 6159.40 78.00 1989 30.0932 6254.00 6131.66 79.00 1990 30.1063 6142.00 6122.87 78.00 1991 30.1194 6224.00 6124.74 79.00 1992 30.1326 6154.00 6126.16 78.00 1993 30.1457 6087.00 6120.28 78.00 1994 30.1588 6090.00 6106.05 78.00 1995 30.1720 6110.00 6088.74 78.00 1996 30.1851 6167.00 6077.54 79.00 1997 30.1982 6056.00 6082.65 78.00 1998 30.2113 6019.00 6111.66 78.00 1999 30.2245 6140.00 6165.39 78.00 2000 30.2376 6061.00 6229.47 78.00 2001 30.2507 6292.00 6272.23 79.00 2002 30.2639 6199.00 6269.44 79.00 2003 30.2770 6129.00 6219.77 78.00 2004 30.2901 6073.00 6150.60 78.00 2005 30.3033 6072.00 6107.60 78.00 2006 30.3164 6062.00 6098.96 78.00 2007 30.3295 6156.00 6102.50 78.00 2008 30.3426 6162.00 6099.57 78.00 2009 30.3558 6243.00 6087.31 79.00 2010 30.3689 6012.00 6091.92 78.00 2011 30.3820 6329.00 6133.73 80.00 2012 30.3952 6413.00 6196.34 80.00 2013 30.4083 6313.00 6231.83 79.00 2014 30.4214 6387.00 6226.00 80.00 2015 30.4346 6332.00 6245.86 80.00 2016 30.4477 6311.00 6349.10 79.00 2017 30.4608 6464.00 6517.48 80.00 2018 30.4740 6653.00 6682.77 82.00 2019 30.4871 6477.00 6772.49 80.00 2020 30.5002 6628.00 6760.85 81.00 2021 30.5133 6699.00 6687.24 82.00 2022 30.5265 6730.00 6591.59 82.00 2023 30.5396 6328.00 6483.02 80.00 2024 30.5527 6418.00 6378.80 80.00 2025 30.5659 6344.00 6296.77 80.00 2026 30.5790 6220.00 6227.40 79.00 2027 30.5921 6146.00 6155.29 78.00 2028 30.6053 6152.00 6071.18 78.00 2029 30.6184 6009.00 5976.67 78.00 2030 30.6315 5945.00 5891.55 77.00 2031 30.6446 5848.00 5833.60 76.00 2032 30.6578 5865.00 5801.57 77.00 2033 30.6709 5882.00 5785.05 77.00 2034 30.6840 5828.00 5775.82 76.00 2035 30.6972 5700.00 5770.83 75.00 2036 30.7103 5728.00 5769.23 76.00 2037 30.7234 5767.00 5773.01 76.00 2038 30.7366 5740.00 5781.59 76.00 2039 30.7497 5715.00 5790.19 76.00 2040 30.7628 5751.00 5791.93 76.00 2041 30.7759 5702.00 5788.38 76.00 2042 30.7891 5802.00 5795.17 76.00 2043 30.8022 5860.00 5824.16 77.00 2044 30.8153 5862.00 5869.71 77.00 2045 30.8285 5937.00 5897.87 77.00 2046 30.8416 5851.00 5877.87 76.00 2047 30.8547 5913.00 5830.82 77.00 2048 30.8679 5885.00 5789.93 77.00 2049 30.8810 5800.00 5777.32 76.00 2050 30.8941 5825.00 5790.70 76.00 2051 30.9073 5720.00 5801.56 76.00 2052 30.9204 5787.00 5798.59 76.00 2053 30.9335 5806.00 5797.77 76.00 2054 30.9466 5685.00 5813.72 75.00 2055 30.9598 5747.00 5856.75 76.00 2056 30.9729 5756.00 5915.75 76.00 2057 30.9860 5833.00 5965.32 76.00 2058 30.9992 5890.00 5995.80 77.00 2059 31.0123 5885.00 6001.48 77.00 2060 31.0254 5817.00 6006.83 76.00 2061 31.0386 5957.00 6064.56 77.00 2062 31.0517 6024.00 6165.53 78.00 2063 31.0648 6084.00 6237.31 78.00 2064 31.0779 5992.00 6211.62 77.00 2065 31.0911 5905.00 6096.90 77.00 2066 31.1042 6027.00 5981.09 78.00 2067 31.1173 5928.00 5932.30 77.00 2068 31.1305 5822.00 5948.51 76.00 2069 31.1436 5924.00 5987.17 77.00 2070 31.1567 6003.00 6011.49 77.00 2071 31.1699 5785.00 6032.68 76.00 2072 31.1830 6070.00 6109.45 78.00 2073 31.1961 6268.00 6306.33 79.00 2074 31.2092 6567.00 6682.17 81.00 2075 31.2224 7351.00 7264.44 86.00 2076 31.2355 8166.00 7999.13 90.00 2077 31.2486 9043.00 8738.25 95.00 2078 31.2618 9441.00 9366.75 97.00 2079 31.2749 9700.00 9693.55 98.00 2080 31.2880 9848.00 9630.00 99.00 2081 31.3012 9742.00 9519.63 99.00 2082 31.3143 9499.00 9431.52 97.00 2083 31.3274 9191.00 9222.93 96.00 2084 31.3405 9096.00 9029.31 95.00 2085 31.3537 8838.00 8788.67 94.00 2086 31.3668 8536.00 8303.00 92.00 2087 31.3799 8045.00 7754.53 90.00 2088 31.3931 7428.00 7297.07 86.00 2089 31.4062 6978.00 6906.30 84.00 2090 31.4193 6567.00 6645.40 81.00 2091 31.4325 6166.00 6502.14 79.00 2092 31.4456 6285.00 6350.98 79.00 2093 31.4587 6042.00 6139.41 78.00 2094 31.4719 5628.00 5920.12 75.00 2095 31.4850 5713.00 5764.83 76.00 2096 31.4981 5634.00 5689.86 75.00 2097 31.5112 5551.00 5671.38 75.00 2098 31.5244 5549.00 5670.11 74.00 2099 31.5375 5481.00 5647.14 74.00 2100 31.5506 5618.00 5596.00 75.00 2101 31.5638 5492.00 5544.68 74.00 2102 31.5769 5424.00 5509.09 74.00 2103 31.5900 5482.00 5488.62 74.00 2104 31.6032 5516.00 5477.84 74.00 2105 31.6163 5442.00 5472.34 74.00 2106 31.6294 5215.00 5470.22 72.00 2107 31.6425 5289.00 5470.63 73.00 2108 31.6557 5538.00 5474.24 74.00 2109 31.6688 5255.00 5484.42 72.00 2110 31.6819 5388.00 5508.06 73.00 2111 31.6951 5582.00 5565.11 75.00 2112 31.7082 5735.00 5691.14 76.00 2113 31.7213 6307.00 5952.73 79.00 2114 31.7345 6478.00 6372.65 80.00 2115 31.7476 7087.00 6852.31 84.00 2116 31.7607 7345.00 7121.51 86.00 2117 31.7738 7131.00 6960.11 84.00 2118 31.7870 6645.00 6526.74 82.00 2119 31.8001 6472.00 6190.38 80.00 2120 31.8132 6421.00 6118.88 80.00 2121 31.8264 6719.00 6237.72 82.00 2122 31.8395 6361.00 6348.01 80.00 2123 31.8526 6327.00 6266.65 80.00 2124 31.8658 5960.00 6008.15 77.00 2125 31.8789 5795.00 5743.31 76.00 2126 31.8920 5525.00 5572.10 74.00 2127 31.9052 5434.00 5492.88 74.00 2128 31.9183 5658.00 5464.49 75.00 2129 31.9314 5471.00 5444.45 74.00 2130 31.9445 5400.00 5412.08 73.00 2131 31.9577 5394.00 5375.62 73.00 2132 31.9708 5337.00 5347.34 73.00 2133 31.9839 5199.00 5332.84 72.00 2134 31.9971 5270.00 5329.15 73.00 2135 32.0102 5391.00 5329.07 73.00 2136 32.0233 5386.00 5328.48 73.00 2137 32.0364 5215.00 5335.84 72.00 2138 32.0496 5280.00 5368.88 73.00 2139 32.0627 5320.00 5451.62 73.00 2140 32.0758 5591.00 5605.63 75.00 2141 32.0890 5830.00 5820.52 76.00 2142 32.1021 5854.00 6025.93 77.00 2143 32.1152 5927.00 6124.86 77.00 2144 32.1284 6085.00 6133.23 78.00 2145 32.1415 6012.00 6129.40 78.00 2146 32.1546 6104.00 6092.76 78.00 2147 32.1678 5948.00 6029.16 77.00 2148 32.1809 6000.00 6027.77 77.00 2149 32.1940 6199.00 6120.13 79.00 2150 32.2071 6268.00 6290.08 79.00 2151 32.2203 6639.00 6492.97 81.00 2152 32.2334 6584.00 6566.19 81.00 2153 32.2465 6404.00 6404.79 80.00 2154 32.2597 6181.00 6154.83 79.00 2155 32.2728 5960.00 6004.95 77.00 2156 32.2859 6095.00 5989.81 78.00 2157 32.2991 5879.00 6031.42 77.00 2158 32.3122 5906.00 6014.90 77.00 2159 32.3253 6095.00 5883.74 78.00 2160 32.3385 5740.00 5703.96 76.00 2161 32.3516 5688.00 5573.74 75.00 2162 32.3647 5634.00 5517.44 75.00 2163 32.3778 5626.00 5492.89 75.00 2164 32.3910 5514.00 5443.49 74.00 2165 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52.6116 2668.00 2638.98 52.00 3705 52.6247 2593.00 2622.42 51.00 3706 52.6379 2517.00 2608.49 50.00 3707 52.6510 2582.00 2596.32 51.00 3708 52.6641 2598.00 2586.89 51.00 3709 52.6772 2599.00 2582.85 51.00 3710 52.6904 2552.00 2586.81 51.00 3711 52.7035 2524.00 2597.15 50.00 3712 52.7166 2601.00 2605.85 51.00 3713 52.7298 2622.00 2603.87 51.00 3714 52.7429 2518.00 2593.01 50.00 3715 52.7560 2627.00 2580.94 51.00 3716 52.7692 2521.00 2571.42 50.00 3717 52.7823 2487.00 2565.36 50.00 3718 52.7954 2530.00 2562.15 50.00 3719 52.8086 2663.00 2561.11 52.00 3720 52.8217 2501.00 2560.92 50.00 3721 52.8348 2502.00 2559.28 50.00 3722 52.8479 2617.00 2555.24 51.00 3723 52.8611 2629.00 2550.93 51.00 3724 52.8742 2552.00 2547.71 51.00 3725 52.8873 2630.00 2546.31 51.00 3726 52.9005 2441.00 2547.63 49.00 3727 52.9136 2496.00 2551.68 50.00 3728 52.9267 2648.00 2559.60 51.00 3729 52.9399 2542.00 2573.25 50.00 3730 52.9530 2574.00 2594.49 51.00 3731 52.9661 2614.00 2621.97 51.00 3732 52.9793 2514.00 2651.62 50.00 3733 52.9924 2591.00 2677.28 51.00 3734 53.0055 2636.00 2690.25 51.00 3735 53.0187 2531.00 2686.11 50.00 3736 53.0318 2617.00 2670.09 51.00 3737 53.0449 2538.00 2650.50 50.00 3738 53.0580 2609.00 2633.26 51.00 3739 53.0712 2594.00 2619.37 51.00 3740 53.0843 2545.00 2607.99 50.00 3741 53.0974 2609.00 2600.07 51.00 3742 53.1105 2597.00 2598.19 51.00 3743 53.1237 2573.00 2603.98 51.00 3744 53.1368 2508.00 2615.76 50.00 3745 53.1499 2573.00 2627.16 51.00 3746 53.1631 2526.00 2633.54 50.00 3747 53.1762 2665.00 2633.82 52.00 3748 53.1893 2647.00 2627.73 51.00 3749 53.2025 2529.00 2613.96 50.00 3750 53.2156 2678.00 2593.73 52.00 3751 53.2287 2612.00 2570.74 51.00 3752 53.2419 2695.00 2550.74 52.00 3753 53.2550 2579.00 2538.18 51.00 3754 53.2681 2617.00 2534.14 51.00 3755 53.2812 2619.00 2536.66 51.00 3756 53.2944 2588.00 2542.46 51.00 3757 53.3075 2636.00 2549.43 51.00 3758 53.3206 2533.00 2555.70 50.00 3759 53.3338 2720.00 2558.83 52.00 3760 53.3469 2554.00 2557.35 51.00 3761 53.3600 2559.00 2552.50 51.00 3762 53.3732 2679.00 2548.00 52.00 3763 53.3863 2631.00 2546.03 51.00 3764 53.3994 2587.00 2545.72 51.00 3765 53.4126 2583.00 2544.56 51.00 3766 53.4257 2622.00 2541.16 51.00 3767 53.4388 2543.00 2537.17 50.00 3768 53.4520 2572.00 2535.31 51.00 3769 53.4651 2533.00 2536.50 50.00 3770 53.4782 2511.00 2540.24 50.00 3771 53.4913 2510.00 2546.28 50.00 3772 53.5045 2530.00 2555.95 50.00 3773 53.5176 2495.00 2571.44 50.00 3774 53.5307 2583.00 2593.61 51.00 3775 53.5438 2555.00 2618.55 51.00 3776 53.5570 2562.00 2638.31 51.00 3777 53.5701 2587.00 2653.67 51.00 3778 53.5832 2654.00 2677.02 52.00 3779 53.5964 2614.00 2711.33 51.00 3780 53.6095 2627.00 2737.32 51.00 3781 53.6226 2626.00 2731.12 51.00 3782 53.6358 2682.00 2696.92 52.00 3783 53.6489 2634.00 2653.77 51.00 3784 53.6620 2592.00 2616.91 51.00 3785 53.6752 2625.00 2594.15 51.00 3786 53.6883 2616.00 2583.94 51.00 3787 53.7014 2575.00 2580.05 51.00 3788 53.7146 2540.00 2580.50 50.00 3789 53.7277 2675.00 2588.81 52.00 3790 53.7408 2556.00 2604.06 51.00 3791 53.7539 2529.00 2615.51 50.00 3792 53.7671 2621.00 2611.71 51.00 3793 53.7802 2566.00 2595.21 51.00 3794 53.7933 2549.00 2574.08 50.00 3795 53.8065 2491.00 2555.47 50.00 3796 53.8196 2517.00 2545.04 50.00 3797 53.8327 2498.00 2545.06 50.00 3798 53.8459 2559.00 2554.36 51.00 3799 53.8590 2537.00 2567.94 50.00 3800 53.8721 2561.00 2579.12 51.00 3801 53.8853 2475.00 2586.04 50.00 3802 53.8984 2600.00 2589.03 51.00 3803 53.9115 2534.00 2588.47 50.00 3804 53.9246 2496.00 2583.83 50.00 3805 53.9378 2455.00 2574.17 50.00 3806 53.9509 2461.00 2562.16 50.00 3807 53.9640 2452.00 2554.91 50.00 3808 53.9771 2547.00 2555.91 50.00 3809 53.9903 2652.00 2560.62 51.00 3810 54.0034 2524.00 2562.81 50.00 3811 54.0165 2540.00 2562.05 50.00 3812 54.0297 2507.00 2561.51 50.00 3813 54.0428 2613.00 2562.69 51.00 3814 54.0559 2505.00 2564.56 50.00 3815 54.0691 2500.00 2563.26 50.00 3816 54.0822 2535.00 2554.91 50.00 3817 54.0953 2554.00 2542.46 51.00 3818 54.1085 2496.00 2532.28 50.00 3819 54.1216 2528.00 2525.59 50.00 3820 54.1347 2507.00 2518.63 50.00 3821 54.1479 2540.00 2510.37 50.00 3822 54.1610 2529.00 2503.08 50.00 3823 54.1741 2573.00 2499.02 51.00 3824 54.1872 2493.00 2498.04 50.00 3825 54.2004 2434.00 2499.95 49.00 3826 54.2135 2596.00 2501.59 51.00 3827 54.2266 2525.00 2501.34 50.00 3828 54.2398 2532.00 2500.78 50.00 3829 54.2529 2501.00 2502.02 50.00 3830 54.2660 2464.00 2503.87 50.00 3831 54.2792 2503.00 2503.89 50.00 3832 54.2923 2431.00 2504.06 49.00 3833 54.3054 2577.00 2507.56 51.00 3834 54.3186 2579.00 2515.49 51.00 3835 54.3317 2482.00 2525.95 50.00 3836 54.3448 2484.00 2535.09 50.00 3837 54.3579 2524.00 2539.22 50.00 3838 54.3711 2572.00 2540.62 51.00 3839 54.3842 2581.00 2542.76 51.00 3840 54.3973 2457.00 2547.02 50.00 3841 54.4104 2583.00 2552.73 51.00 3842 54.4236 2602.00 2554.41 51.00 3843 54.4367 2603.00 2546.65 51.00 3844 54.4498 2580.00 2535.08 51.00 3845 54.4630 2492.00 2528.12 50.00 3846 54.4761 2622.00 2527.94 51.00 3847 54.4892 2601.00 2530.90 51.00 3848 54.5024 2601.00 2532.77 51.00 3849 54.5155 2552.00 2534.05 51.00 3850 54.5286 2538.00 2537.04 50.00 3851 54.5418 2484.00 2539.76 50.00 3852 54.5549 2549.00 2538.29 50.00 3853 54.5680 2439.00 2531.23 49.00 3854 54.5812 2517.00 2519.68 50.00 3855 54.5943 2483.00 2507.14 50.00 3856 54.6074 2553.00 2496.72 51.00 3857 54.6205 2481.00 2488.70 50.00 3858 54.6337 2500.00 2482.97 50.00 3859 54.6468 2508.00 2479.40 50.00 3860 54.6599 2549.00 2478.13 50.00 3861 54.6731 2480.00 2479.72 50.00 3862 54.6862 2428.00 2482.49 49.00 3863 54.6993 2443.00 2484.11 49.00 3864 54.7125 2530.00 2484.62 50.00 3865 54.7256 2507.00 2486.36 50.00 3866 54.7387 2522.00 2490.25 50.00 3867 54.7519 2445.00 2494.70 49.00 3868 54.7650 2485.00 2497.01 50.00 3869 54.7781 2395.00 2496.00 49.00 3870 54.7912 2410.00 2492.43 49.00 3871 54.8044 2365.00 2488.27 49.00 3872 54.8175 2520.00 2485.75 50.00 3873 54.8306 2445.00 2485.78 49.00 3874 54.8438 2362.00 2486.52 49.00 3875 54.8569 2474.00 2487.08 50.00 3876 54.8700 2530.00 2486.97 50.00 3877 54.8831 2574.00 2486.15 51.00 3878 54.8963 2559.00 2485.81 51.00 3879 54.9094 2446.00 2485.09 49.00 3880 54.9225 2464.00 2482.39 50.00 3881 54.9357 2524.00 2477.78 50.00 3882 54.9488 2467.00 2472.58 50.00 3883 54.9619 2312.00 2468.53 48.00 3884 54.9751 2505.00 2466.70 50.00 3885 54.9882 2505.00 2466.34 50.00 3886 55.0013 2497.00 2466.11 50.00 3887 55.0145 2500.00 2465.43 50.00 3888 55.0276 2449.00 2463.99 49.00 3889 55.0407 2492.00 2462.38 50.00 3890 55.0538 2470.00 2460.42 50.00 3891 55.0670 2512.00 2457.56 50.00 3892 55.0801 2448.00 2454.63 49.00 3893 55.0932 2407.00 2452.79 49.00 3894 55.1064 2412.00 2451.93 49.00 3895 55.1195 2466.00 2452.11 50.00 3896 55.1326 2415.00 2453.83 49.00 3897 55.1458 2482.00 2457.35 50.00 3898 55.1589 2480.00 2462.01 50.00 3899 55.1720 2488.00 2467.27 50.00 3900 55.1852 2398.00 2474.42 49.00 3901 55.1983 2471.00 2485.53 50.00 3902 55.2114 2488.00 2501.35 50.00 3903 55.2245 2515.00 2519.38 50.00 3904 55.2377 2544.00 2532.33 50.00 3905 55.2508 2509.00 2531.65 50.00 3906 55.2639 2635.00 2518.72 51.00 3907 55.2771 2506.00 2503.80 50.00 3908 55.2902 2535.00 2494.48 50.00 3909 55.3033 2518.00 2492.17 50.00 3910 55.3164 2481.00 2495.94 50.00 3911 55.3296 2426.00 2504.86 49.00 3912 55.3427 2466.00 2516.45 50.00 3913 55.3558 2443.00 2525.02 49.00 3914 55.3690 2462.00 2528.57 50.00 3915 55.3821 2526.00 2529.68 50.00 3916 55.3952 2495.00 2527.52 50.00 3917 55.4084 2402.00 2519.36 49.00 3918 55.4215 2500.00 2504.89 50.00 3919 55.4346 2449.00 2488.43 49.00 3920 55.4478 2429.00 2475.29 49.00 3921 55.4609 2425.00 2467.93 49.00 3922 55.4740 2471.00 2466.23 50.00 3923 55.4871 2467.00 2468.58 50.00 3924 55.5003 2530.00 2471.56 50.00 3925 55.5134 2441.00 2472.65 49.00 3926 55.5265 2485.00 2474.15 50.00 3927 55.5396 2489.00 2479.65 50.00 3928 55.5528 2504.00 2489.94 50.00 3929 55.5659 2502.00 2501.48 50.00 3930 55.5791 2561.00 2508.85 51.00 3931 55.5922 2491.00 2505.49 50.00 3932 55.6053 2425.00 2489.97 49.00 3933 55.6184 2432.00 2470.95 49.00 3934 55.6316 2413.00 2456.26 49.00 3935 55.6447 2440.00 2448.31 49.00 3936 55.6578 2431.00 2446.52 49.00 3937 55.6710 2525.00 2449.09 50.00 3938 55.6841 2479.00 2454.30 50.00 3939 55.6972 2420.00 2460.86 49.00 3940 55.7104 2558.00 2467.63 51.00 3941 55.7235 2519.00 2474.28 50.00 3942 55.7366 2453.00 2479.53 50.00 3943 55.7497 2493.00 2481.67 50.00 3944 55.7629 2471.00 2482.32 50.00 3945 55.7760 2445.00 2483.72 49.00 3946 55.7891 2548.00 2485.81 50.00 3947 55.8023 2461.00 2485.34 50.00 3948 55.8154 2464.00 2481.77 50.00 3949 55.8285 2459.00 2476.36 50.00 3950 55.8417 2425.00 2469.03 49.00 3951 55.8548 2530.00 2460.76 50.00 3952 55.8679 2419.00 2453.39 49.00 3953 55.8811 2556.00 2450.45 51.00 3954 55.8942 2422.00 2454.29 49.00 3955 55.9073 2422.00 2464.70 49.00 3956 55.9204 2446.00 2477.81 49.00 3957 55.9336 2460.00 2486.35 50.00 3958 55.9467 2456.00 2485.14 50.00 3959 55.9598 2404.00 2477.47 49.00 3960 55.9729 2443.00 2468.97 49.00 3961 55.9861 2507.00 2461.04 50.00 3962 55.9992 2478.00 2452.61 50.00 3963 56.0123 2462.00 2443.77 50.00 3964 56.0255 2427.00 2437.35 49.00 3965 56.0386 2478.00 2435.29 50.00 3966 56.0517 2504.00 2438.50 50.00 3967 56.0649 2439.00 2446.94 49.00 3968 56.0780 2425.00 2459.57 49.00 3969 56.0911 2410.00 2474.54 49.00 3970 56.1043 2527.00 2492.60 50.00 3971 56.1174 2440.00 2513.42 49.00 3972 56.1305 2474.00 2528.85 50.00 3973 56.1437 2552.00 2529.79 51.00 3974 56.1568 2480.00 2518.77 50.00 3975 56.1699 2561.00 2505.93 51.00 3976 56.1830 2495.00 2499.95 50.00 3977 56.1962 2389.00 2505.51 49.00 3978 56.2093 2495.00 2521.97 50.00 3979 56.2224 2418.00 2546.25 49.00 3980 56.2356 2390.00 2571.92 49.00 3981 56.2487 2526.00 2591.25 50.00 3982 56.2618 2561.00 2599.23 51.00 3983 56.2750 2550.00 2594.05 50.00 3984 56.2881 2657.00 2574.26 52.00 3985 56.3012 2668.00 2544.02 52.00 3986 56.3144 2527.00 2515.34 50.00 3987 56.3275 2458.00 2496.98 50.00 3988 56.3406 2428.00 2490.29 49.00 3989 56.3537 2416.00 2491.94 49.00 3990 56.3669 2559.00 2499.98 51.00 3991 56.3800 2600.00 2513.61 51.00 3992 56.3931 2507.00 2528.84 50.00 3993 56.4062 2572.00 2539.48 51.00 3994 56.4194 2525.00 2539.63 50.00 3995 56.4325 2443.00 2527.86 49.00 3996 56.4456 2502.00 2506.01 50.00 3997 56.4588 2497.00 2481.49 50.00 3998 56.4719 2492.00 2463.14 50.00 3999 56.4850 2505.00 2454.21 50.00 4000 56.4982 2493.00 2453.16 50.00 4001 56.5113 2449.00 2457.64 49.00 4002 56.5244 2458.00 2466.13 50.00 4003 56.5376 2441.00 2478.03 49.00 4004 56.5507 2560.00 2494.09 51.00 4005 56.5638 2503.00 2512.84 50.00 4006 56.5770 2583.00 2527.28 51.00 4007 56.5901 2608.00 2528.54 51.00 4008 56.6032 2562.00 2517.33 51.00 4009 56.6163 2519.00 2504.79 50.00 4010 56.6295 2645.00 2499.02 51.00 4011 56.6426 2591.00 2500.25 51.00 4012 56.6557 2444.00 2502.88 49.00 4013 56.6689 2549.00 2502.52 50.00 4014 56.6820 2563.00 2501.85 51.00 4015 56.6951 2551.00 2505.85 51.00 4016 56.7083 2544.00 2518.01 50.00 4017 56.7214 2613.00 2539.39 51.00 4018 56.7345 2485.00 2562.83 50.00 4019 56.7477 2575.00 2572.47 51.00 4020 56.7608 2505.00 2560.16 50.00 4021 56.7739 2546.00 2537.70 50.00 4022 56.7870 2463.00 2517.38 50.00 4023 56.8002 2624.00 2500.99 51.00 4024 56.8133 2416.00 2485.71 49.00 4025 56.8264 2447.00 2471.50 49.00 4026 56.8396 2421.00 2461.78 49.00 4027 56.8527 2602.00 2459.23 51.00 4028 56.8658 2489.00 2465.14 50.00 4029 56.8789 2539.00 2478.88 50.00 4030 56.8921 2537.00 2496.74 50.00 4031 56.9052 2550.00 2511.25 50.00 4032 56.9183 2491.00 2519.35 50.00 4033 56.9315 2442.00 2524.43 49.00 4034 56.9446 2391.00 2525.32 49.00 4035 56.9577 2636.00 2518.26 51.00 4036 56.9709 2513.00 2506.96 50.00 4037 56.9840 2500.00 2497.51 50.00 4038 56.9971 2553.00 2489.56 51.00 4039 57.0103 2548.00 2480.62 50.00 4040 57.0234 2479.00 2472.78 50.00 4041 57.0365 2483.00 2469.09 50.00 4042 57.0496 2524.00 2470.06 50.00 4043 57.0628 2527.00 2473.02 50.00 4044 57.0759 2579.00 2475.10 51.00 4045 57.0890 2609.00 2474.27 51.00 4046 57.1022 2514.00 2469.27 50.00 4047 57.1153 2479.00 2460.52 50.00 4048 57.1284 2456.00 2451.86 50.00 4049 57.1416 2412.00 2446.11 49.00 4050 57.1547 2465.00 2442.17 50.00 4051 57.1678 2463.00 2438.75 50.00 4052 57.1809 2499.00 2436.57 50.00 4053 57.1941 2413.00 2437.66 49.00 4054 57.2072 2417.00 2443.27 49.00 4055 57.2203 2487.00 2452.23 50.00 4056 57.2335 2508.00 2462.03 50.00 4057 57.2466 2340.00 2468.99 48.00 4058 57.2597 2510.00 2471.81 50.00 4059 57.2729 2485.00 2473.13 50.00 4060 57.2860 2427.00 2470.73 49.00 4061 57.2991 2461.00 2462.45 50.00 4062 57.3122 2438.00 2450.10 49.00 4063 57.3254 2482.00 2438.24 50.00 4064 57.3385 2417.00 2431.56 49.00 4065 57.3516 2363.00 2432.93 49.00 4066 57.3648 2395.00 2442.47 49.00 4067 57.3779 2480.00 2455.75 50.00 4068 57.3910 2535.00 2466.26 50.00 4069 57.4042 2428.00 2470.09 49.00 4070 57.4173 2517.00 2469.92 50.00 4071 57.4304 2402.00 2469.86 49.00 4072 57.4436 2531.00 2471.58 50.00 4073 57.4567 2421.00 2474.98 49.00 4074 57.4698 2539.00 2478.74 50.00 4075 57.4829 2442.00 2480.73 49.00 4076 57.4961 2621.00 2478.64 51.00 4077 57.5092 2469.00 2471.17 50.00 4078 57.5223 2456.00 2461.88 50.00 4079 57.5355 2452.00 2455.13 50.00 4080 57.5486 2463.00 2452.77 50.00 4081 57.5617 2415.00 2455.71 49.00 4082 57.5749 2525.00 2464.62 50.00 4083 57.5880 2426.00 2478.81 49.00 4084 57.6011 2459.00 2497.21 50.00 4085 57.6142 2431.00 2520.76 49.00 4086 57.6274 2583.00 2547.90 51.00 4087 57.6405 2418.00 2569.68 49.00 4088 57.6536 2517.00 2574.79 50.00 4089 57.6668 2397.00 2562.96 49.00 4090 57.6799 2573.00 2543.43 51.00 4091 57.6930 2572.00 2523.90 51.00 4092 57.7062 2548.00 2507.06 50.00 4093 57.7193 2501.00 2492.04 50.00 4094 57.7324 2506.00 2478.75 50.00 4095 57.7455 2431.00 2468.76 49.00 4096 57.7587 2452.00 2463.44 50.00 4097 57.7718 2404.00 2463.33 49.00 4098 57.7849 2482.00 2466.86 50.00 4099 57.7981 2553.00 2469.57 51.00 4100 57.8112 2493.00 2467.12 50.00 4101 57.8243 2451.00 2459.93 50.00 4102 57.8375 2477.00 2451.12 50.00 4103 57.8506 2526.00 2442.52 50.00 4104 57.8637 2417.00 2434.50 49.00 4105 57.8769 2395.00 2426.27 49.00 4106 57.8900 2470.00 2418.44 50.00 4107 57.9031 2428.00 2412.61 49.00 4108 57.9162 2402.00 2409.68 49.00 4109 57.9294 2351.00 2408.85 48.00 4110 57.9425 2475.00 2407.96 50.00 4111 57.9556 2474.00 2406.90 50.00 4112 57.9688 2408.00 2406.99 49.00 4113 57.9819 2430.00 2406.87 49.00 4114 57.9950 2401.00 2404.67 49.00 4115 58.0082 2396.00 2399.99 49.00 4116 58.0213 2365.00 2394.54 49.00 4117 58.0344 2416.00 2390.18 49.00 4118 58.0475 2388.00 2387.85 49.00 4119 58.0607 2482.00 2387.76 50.00 4120 58.0738 2432.00 2389.76 49.00 4121 58.0869 2412.00 2393.71 49.00 4122 58.1001 2387.00 2399.39 49.00 4123 58.1132 2447.00 2407.49 49.00 4124 58.1263 2402.00 2417.00 49.00 4125 58.1395 2525.00 2426.07 50.00 4126 58.1526 2430.00 2431.32 49.00 4127 58.1657 2361.00 2431.13 49.00 4128 58.1788 2439.00 2428.87 49.00 4129 58.1920 2469.00 2429.57 50.00 4130 58.2051 2408.00 2435.00 49.00 4131 58.2182 2449.00 2441.11 49.00 4132 58.2314 2369.00 2440.91 49.00 4133 58.2445 2417.00 2434.54 49.00 4134 58.2576 2501.00 2428.03 50.00 4135 58.2708 2333.00 2425.82 48.00 4136 58.2839 2375.00 2427.49 49.00 4137 58.2970 2429.00 2430.44 49.00 4138 58.3102 2499.00 2431.07 50.00 4139 58.3233 2432.00 2429.15 49.00 4140 58.3364 2492.00 2428.08 50.00 4141 58.3495 2589.00 2432.19 51.00 4142 58.3627 2442.00 2443.07 49.00 4143 58.3758 2559.00 2458.81 51.00 4144 58.3889 2511.00 2474.46 50.00 4145 58.4021 2567.00 2485.25 51.00 4146 58.4152 2471.00 2486.92 50.00 4147 58.4283 2442.00 2479.73 49.00 4148 58.4415 2429.00 2469.85 49.00 4149 58.4546 2408.00 2462.49 49.00 4150 58.4677 2415.00 2457.31 49.00 4151 58.4808 2491.00 2451.84 50.00 4152 58.4940 2454.00 2446.38 50.00 4153 58.5071 2476.00 2443.51 50.00 4154 58.5202 2543.00 2445.03 50.00 4155 58.5334 2491.00 2451.64 50.00 4156 58.5465 2555.00 2463.93 51.00 4157 58.5596 2520.00 2480.19 50.00 4158 58.5728 2582.00 2494.22 51.00 4159 58.5859 2562.00 2499.30 51.00 4160 58.5990 2452.00 2492.21 50.00 4161 58.6121 2538.00 2476.25 50.00 4162 58.6253 2512.00 2459.97 50.00 4163 58.6384 2505.00 2448.11 50.00 4164 58.6515 2389.00 2441.09 49.00 4165 58.6647 2485.00 2437.94 50.00 4166 58.6778 2473.00 2436.81 50.00 4167 58.6909 2447.00 2436.84 49.00 4168 58.7041 2397.00 2439.65 49.00 4169 58.7172 2571.00 2445.97 51.00 4170 58.7303 2473.00 2453.01 50.00 4171 58.7435 2340.00 2456.51 48.00 4172 58.7566 2479.00 2452.52 50.00 4173 58.7697 2522.00 2440.89 50.00 4174 58.7828 2486.00 2427.29 50.00 4175 58.7960 2406.00 2417.23 49.00 4176 58.8091 2362.00 2412.65 49.00 4177 58.8222 2487.00 2412.78 50.00 4178 58.8354 2311.00 2415.29 48.00 4179 58.8485 2424.00 2418.04 49.00 4180 58.8616 2355.00 2419.75 49.00 4181 58.8748 2455.00 2421.25 50.00 4182 58.8879 2497.00 2423.46 50.00 4183 58.9010 2399.00 2425.73 49.00 4184 58.9141 2469.00 2425.99 50.00 4185 58.9273 2442.00 2422.87 49.00 4186 58.9404 2360.00 2416.99 49.00 4187 58.9535 2417.00 2410.27 49.00 4188 58.9667 2377.00 2404.99 49.00 4189 58.9798 2352.00 2402.73 48.00 4190 58.9929 2412.00 2403.90 49.00 4191 59.0061 2422.00 2407.92 49.00 4192 59.0192 2402.00 2412.75 49.00 4193 59.0323 2425.00 2416.70 49.00 4194 59.0454 2501.00 2420.42 50.00 4195 59.0586 2280.00 2425.67 48.00 4196 59.0717 2387.00 2432.20 49.00 4197 59.0848 2370.00 2436.71 49.00 4198 59.0980 2413.00 2436.62 49.00 4199 59.1111 2387.00 2432.68 49.00 4200 59.1242 2384.00 2427.05 49.00 4201 59.1374 2343.00 2421.70 48.00 4202 59.1505 2425.00 2419.57 49.00 4203 59.1636 2410.00 2422.55 49.00 4204 59.1767 2385.00 2429.16 49.00 4205 59.1899 2375.00 2435.08 49.00 4206 59.2030 2379.00 2436.35 49.00 4207 59.2161 2425.00 2432.02 49.00 4208 59.2293 2339.00 2424.89 48.00 4209 59.2424 2379.00 2417.62 49.00 4210 59.2555 2350.00 2411.51 48.00 4211 59.2687 2444.00 2407.04 49.00 4212 59.2818 2351.00 2404.19 48.00 4213 59.2949 2397.00 2402.49 49.00 4214 59.3081 2379.00 2402.43 49.00 4215 59.3212 2417.00 2404.81 49.00 4216 59.3343 2442.00 2409.15 49.00 4217 59.3474 2347.00 2413.42 48.00 4218 59.3606 2335.00 2414.96 48.00 4219 59.3737 2385.00 2412.17 49.00 4220 59.3868 2438.00 2406.03 49.00 4221 59.4000 2353.00 2399.31 49.00 4222 59.4131 2405.00 2393.77 49.00 4223 59.4262 2434.00 2390.59 49.00 4224 59.4394 2479.00 2389.25 50.00 4225 59.4525 2449.00 2389.10 49.00 4226 59.4656 2424.00 2389.90 49.00 4227 59.4787 2319.00 2391.90 48.00 4228 59.4919 2342.00 2394.84 48.00 4229 59.5050 2412.00 2398.00 49.00 4230 59.5181 2384.00 2400.81 49.00 4231 59.5313 2460.00 2403.21 50.00 4232 59.5444 2379.00 2405.56 49.00 4233 59.5575 2384.00 2407.49 49.00 4234 59.5707 2427.00 2408.08 49.00 4235 59.5838 2356.00 2407.00 49.00 4236 59.5969 2469.00 2405.00 50.00 4237 59.6100 2502.00 2403.28 50.00 4238 59.6232 2456.00 2403.04 50.00 4239 59.6363 2398.00 2405.30 49.00 4240 59.6494 2450.00 2410.71 49.00 4241 59.6626 2404.00 2419.92 49.00 4242 59.6757 2475.00 2432.65 50.00 4243 59.6888 2348.00 2447.62 48.00 4244 59.7020 2461.00 2461.04 50.00 4245 59.7151 2463.00 2466.61 50.00 4246 59.7282 2371.00 2461.73 49.00 4247 59.7413 2393.00 2451.81 49.00 4248 59.7545 2471.00 2443.50 50.00 4249 59.7676 2452.00 2439.45 50.00 4250 59.7807 2504.00 2439.17 50.00 4251 59.7939 2456.00 2440.90 50.00 4252 59.8070 2458.00 2442.97 50.00 4253 59.8201 2552.00 2444.47 51.00 4254 59.8333 2444.00 2445.69 49.00 4255 59.8464 2441.00 2447.58 49.00 4256 59.8595 2516.00 2450.91 50.00 4257 59.8727 2416.00 2455.11 49.00 4258 59.8858 2536.00 2459.35 50.00 4259 59.8989 2543.00 2465.39 50.00 4260 59.9120 2483.00 2475.81 50.00 4261 59.9252 2483.00 2489.66 50.00 4262 59.9383 2513.00 2499.31 50.00 4263 59.9514 2466.00 2495.81 50.00 4264 59.9646 2501.00 2481.59 50.00 4265 59.9777 2551.00 2465.57 51.00 4266 59.9908 2500.00 2452.93 50.00 4267 60.0040 2497.00 2444.96 50.00 4268 60.0171 2390.00 2442.31 49.00 4269 60.0302 2425.00 2445.97 49.00 4270 60.0433 2519.00 2457.25 50.00 4271 60.0565 2372.00 2475.94 49.00 4272 60.0696 2453.00 2498.60 50.00 4273 60.0827 2457.00 2518.46 50.00 4274 60.0959 2565.00 2527.90 51.00 4275 60.1090 2433.00 2522.13 49.00 4276 60.1221 2533.00 2503.82 50.00 4277 60.1353 2492.00 2481.58 50.00 4278 60.1484 2402.00 2461.45 49.00 4279 60.1615 2448.00 2445.73 49.00 4280 60.1746 2409.00 2435.48 49.00 4281 60.1878 2404.00 2431.37 49.00 4282 60.2009 2493.00 2433.76 50.00 4283 60.2140 2400.00 2441.86 49.00 4284 60.2272 2418.00 2453.30 49.00 4285 60.2403 2463.00 2463.78 50.00 4286 60.2534 2429.00 2468.73 49.00 4287 60.2666 2402.00 2466.51 49.00 4288 60.2797 2462.00 2460.09 50.00 4289 60.2928 2372.00 2453.76 49.00 4290 60.3060 2449.00 2449.79 49.00 4291 60.3191 2402.00 2447.42 49.00 4292 60.3322 2345.00 2444.49 48.00 4293 60.3453 2452.00 2440.67 50.00 4294 60.3585 2478.00 2437.97 50.00 4295 60.3716 2445.00 2439.15 49.00 4296 60.3847 2432.00 2446.74 49.00 4297 60.3979 2459.00 2460.88 50.00 4298 60.4110 2510.00 2478.23 50.00 4299 60.4241 2429.00 2492.94 49.00 4300 60.4373 2469.00 2499.60 50.00 4301 60.4504 2578.00 2496.10 51.00 4302 60.4635 2420.00 2484.45 49.00 4303 60.4766 2497.00 2471.40 50.00 4304 60.4898 2551.00 2460.85 51.00 4305 60.5029 2488.00 2453.48 50.00 4306 60.5160 2349.00 2448.88 48.00 4307 60.5292 2470.00 2446.03 50.00 4308 60.5423 2518.00 2443.99 50.00 4309 60.5554 2477.00 2443.59 50.00 4310 60.5686 2422.00 2446.18 49.00 4311 60.5817 2502.00 2453.41 50.00 4312 60.5948 2404.00 2464.28 49.00 4313 60.6079 2357.00 2476.06 49.00 4314 60.6211 2550.00 2484.73 50.00 4315 60.6342 2477.00 2487.16 50.00 4316 60.6473 2569.00 2481.85 51.00 4317 60.6605 2504.00 2469.78 50.00 4318 60.6736 2471.00 2455.33 50.00 4319 60.6867 2385.00 2443.56 49.00 4320 60.6999 2428.00 2436.74 49.00 4321 60.7130 2436.00 2434.38 49.00 4322 60.7261 2396.00 2436.09 49.00 4323 60.7393 2479.00 2442.38 50.00 4324 60.7524 2506.00 2453.02 50.00 4325 60.7655 2481.00 2466.45 50.00 4326 60.7786 2442.00 2479.03 49.00 4327 60.7918 2509.00 2487.76 50.00 4328 60.8049 2508.00 2491.01 50.00 4329 60.8180 2503.00 2489.63 50.00 4330 60.8312 2545.00 2488.33 50.00 4331 60.8443 2541.00 2492.90 50.00 4332 60.8574 2529.00 2506.14 50.00 4333 60.8706 2550.00 2527.05 50.00 4334 60.8837 2484.00 2549.96 50.00 4335 60.8968 2508.00 2563.18 50.00 4336 60.9099 2509.00 2557.00 50.00 4337 60.9231 2527.00 2535.54 50.00 4338 60.9362 2443.00 2510.72 49.00 4339 60.9493 2444.00 2488.98 49.00 4340 60.9625 2497.00 2472.11 50.00 4341 60.9756 2345.00 2460.10 48.00 4342 60.9887 2456.00 2453.04 50.00 4343 61.0019 2456.00 2451.69 50.00 4344 61.0150 2545.00 2456.32 50.00 4345 61.0281 2467.00 2466.33 50.00 4346 61.0412 2338.00 2480.28 48.00 4347 61.0544 2398.00 2494.91 49.00 4348 61.0675 2461.00 2504.38 50.00 4349 61.0806 2491.00 2505.32 50.00 4350 61.0938 2466.00 2501.56 50.00 4351 61.1069 2416.00 2498.66 49.00 4352 61.1200 2434.00 2499.00 49.00 4353 61.1332 2485.00 2501.57 50.00 4354 61.1463 2519.00 2500.79 50.00 4355 61.1594 2503.00 2494.24 50.00 4356 61.1726 2482.00 2485.69 50.00 4357 61.1857 2579.00 2479.86 51.00 4358 61.1988 2466.00 2480.08 50.00 4359 61.2119 2567.00 2486.93 51.00 4360 61.2251 2526.00 2497.63 50.00 4361 61.2382 2516.00 2507.18 50.00 4362 61.2513 2525.00 2510.99 50.00 4363 61.2645 2507.00 2507.81 50.00 4364 61.2776 2459.00 2500.30 50.00 4365 61.2907 2500.00 2491.98 50.00 4366 61.3039 2501.00 2484.52 50.00 4367 61.3170 2492.00 2476.21 50.00 4368 61.3301 2484.00 2466.33 50.00 4369 61.3432 2424.00 2456.91 49.00 4370 61.3564 2520.00 2450.20 50.00 4371 61.3695 2447.00 2447.71 49.00 4372 61.3826 2409.00 2449.24 49.00 4373 61.3958 2443.00 2452.87 49.00 4374 61.4089 2430.00 2455.89 49.00 4375 61.4220 2399.00 2456.36 49.00 4376 61.4352 2403.00 2453.87 49.00 4377 61.4483 2550.00 2449.69 50.00 4378 61.4614 2474.00 2445.22 50.00 4379 61.4745 2328.00 2442.26 48.00 4380 61.4877 2342.00 2441.48 48.00 4381 61.5008 2425.00 2441.33 49.00 4382 61.5139 2437.00 2440.08 49.00 4383 61.5271 2375.00 2437.00 49.00 4384 61.5402 2562.00 2432.19 51.00 4385 61.5533 2410.00 2426.96 49.00 4386 61.5665 2385.00 2422.74 49.00 4387 61.5796 2420.00 2420.60 49.00 4388 61.5927 2468.00 2421.09 50.00 4389 61.6059 2403.00 2424.05 49.00 4390 61.6190 2473.00 2429.29 50.00 4391 61.6321 2544.00 2436.48 50.00 4392 61.6452 2556.00 2445.13 51.00 4393 61.6584 2415.00 2453.83 49.00 4394 61.6715 2437.00 2459.02 49.00 4395 61.6846 2440.00 2457.85 49.00 4396 61.6978 2451.00 2451.72 50.00 4397 61.7109 2396.00 2444.07 49.00 4398 61.7240 2469.00 2437.36 50.00 4399 61.7372 2431.00 2432.27 49.00 4400 61.7503 2445.00 2428.95 49.00 4401 61.7634 2449.00 2426.86 49.00 4402 61.7765 2374.00 2425.69 49.00 4403 61.7897 2446.00 2425.62 49.00 4404 61.8028 2425.00 2426.49 49.00 4405 61.8159 2456.00 2428.33 50.00 4406 61.8291 2411.00 2430.77 49.00 4407 61.8422 2386.00 2433.11 49.00 4408 61.8553 2352.00 2433.91 48.00 4409 61.8685 2419.00 2433.95 49.00 4410 61.8816 2428.00 2433.86 49.00 4411 61.8947 2425.00 2434.04 49.00 4412 61.9078 2456.00 2434.48 50.00 4413 61.9210 2439.00 2435.61 49.00 4414 61.9341 2355.00 2437.25 49.00 4415 61.9472 2391.00 2438.48 49.00 4416 61.9604 2381.00 2439.02 49.00 4417 61.9735 2404.00 2439.17 49.00 4418 61.9866 2388.00 2438.83 49.00 4419 61.9998 2389.00 2437.77 49.00 4420 62.0129 2423.00 2436.03 49.00 4421 62.0260 2427.00 2433.44 49.00 4422 62.0392 2446.00 2430.46 49.00 4423 62.0523 2396.00 2428.13 49.00 4424 62.0654 2418.00 2427.17 49.00 4425 62.0785 2415.00 2427.35 49.00 4426 62.0917 2408.00 2428.68 49.00 4427 62.1048 2462.00 2430.79 50.00 4428 62.1179 2458.00 2434.04 50.00 4429 62.1311 2428.00 2438.97 49.00 4430 62.1442 2448.00 2445.73 49.00 4431 62.1573 2328.00 2452.76 48.00 4432 62.1705 2498.00 2456.69 50.00 4433 62.1836 2408.00 2454.72 49.00 4434 62.1967 2454.00 2448.28 50.00 4435 62.2098 2456.00 2441.63 50.00 4436 62.2230 2474.00 2437.93 50.00 4437 62.2361 2463.00 2437.84 50.00 4438 62.2492 2376.00 2439.88 49.00 4439 62.2624 2471.00 2441.01 50.00 4440 62.2755 2398.00 2439.58 49.00 4441 62.2886 2470.00 2437.17 50.00 4442 62.3018 2357.00 2436.35 49.00 4443 62.3149 2465.00 2438.21 50.00 4444 62.3280 2402.00 2442.42 49.00 4445 62.3411 2425.00 2447.46 49.00 4446 62.3543 2342.00 2452.59 48.00 4447 62.3674 2470.00 2459.03 50.00 4448 62.3805 2445.00 2468.11 49.00 4449 62.3937 2433.00 2477.58 49.00 4450 62.4068 2438.00 2481.45 49.00 4451 62.4199 2418.00 2476.77 49.00 4452 62.4331 2482.00 2467.42 50.00 4453 62.4462 2335.00 2456.93 48.00 4454 62.4593 2408.00 2447.12 49.00 4455 62.4725 2390.00 2439.62 49.00 4456 62.4856 2459.00 2435.74 50.00 4457 62.4987 2450.00 2436.17 49.00 4458 62.5118 2470.00 2440.51 50.00 4459 62.5250 2446.00 2448.00 49.00 4460 62.5381 2453.00 2456.78 50.00 4461 62.5512 2509.00 2464.11 50.00 4462 62.5644 2477.00 2467.22 50.00 4463 62.5775 2466.00 2464.17 50.00 4464 62.5906 2461.00 2455.70 50.00 4465 62.6038 2523.00 2446.00 50.00 4466 62.6169 2505.00 2438.87 50.00 4467 62.6300 2512.00 2435.63 50.00 4468 62.6431 2518.00 2436.71 50.00 4469 62.6563 2454.00 2442.32 50.00 4470 62.6694 2499.00 2451.60 50.00 4471 62.6825 2414.00 2461.71 49.00 4472 62.6957 2408.00 2468.58 49.00 4473 62.7088 2517.00 2471.00 50.00 4474 62.7219 2524.00 2468.66 50.00 4475 62.7351 2390.00 2460.64 49.00 4476 62.7482 2438.00 2448.54 49.00 4477 62.7613 2433.00 2436.35 49.00 4478 62.7744 2373.00 2426.99 49.00 4479 62.7876 2474.00 2421.61 50.00 4480 62.8007 2389.00 2420.28 49.00 4481 62.8138 2362.00 2422.60 49.00 4482 62.8270 2398.00 2427.94 49.00 4483 62.8401 2438.00 2434.96 49.00 4484 62.8532 2444.00 2441.65 49.00 4485 62.8664 2502.00 2446.09 50.00 4486 62.8795 2417.00 2448.11 49.00 4487 62.8926 2459.00 2448.52 50.00 4488 62.9057 2365.00 2446.55 49.00 4489 62.9189 2483.00 2441.44 50.00 4490 62.9320 2376.00 2435.17 49.00 4491 62.9451 2381.00 2430.98 49.00 4492 62.9583 2394.00 2430.20 49.00 4493 62.9714 2409.00 2431.76 49.00 4494 62.9845 2415.00 2433.58 49.00 4495 62.9977 2389.00 2434.19 49.00 4496 63.0108 2507.00 2433.04 50.00 4497 63.0239 2470.00 2430.40 50.00 4498 63.0371 2412.00 2426.80 49.00 4499 63.0502 2446.00 2422.93 49.00 4500 63.0633 2354.00 2420.17 49.00 4501 63.0764 2524.00 2418.35 50.00 4502 63.0896 2416.00 2416.70 49.00 4503 63.1027 2403.00 2414.75 49.00 4504 63.1158 2418.00 2413.12 49.00 4505 63.1290 2339.00 2412.41 48.00 4506 63.1421 2419.00 2412.40 49.00 4507 63.1552 2493.00 2412.47 50.00 4508 63.1684 2404.00 2412.09 49.00 4509 63.1815 2519.00 2411.13 50.00 4510 63.1946 2459.00 2409.91 50.00 4511 63.2077 2438.00 2408.94 49.00 4512 63.2209 2445.00 2408.57 49.00 4513 63.2340 2484.00 2409.58 50.00 4514 63.2471 2403.00 2412.25 49.00 4515 63.2603 2531.00 2415.99 50.00 4516 63.2734 2541.00 2419.10 50.00 4517 63.2865 2442.00 2419.79 49.00 4518 63.2997 2405.00 2417.78 49.00 4519 63.3128 2367.00 2414.35 49.00 4520 63.3259 2329.00 2411.23 48.00 4521 63.3390 2361.00 2409.42 49.00 4522 63.3522 2417.00 2409.13 49.00 4523 63.3653 2435.00 2409.90 49.00 4524 63.3784 2391.00 2410.90 49.00 4525 63.3916 2409.00 2411.54 49.00 4526 63.4047 2476.00 2412.05 50.00 4527 63.4178 2402.00 2413.35 49.00 4528 63.4310 2408.00 2416.20 49.00 4529 63.4441 2435.00 2420.21 49.00 4530 63.4572 2386.00 2424.48 49.00 4531 63.4703 2435.00 2428.24 49.00 4532 63.4835 2431.00 2429.34 49.00 4533 63.4966 2411.00 2427.78 49.00 4534 63.5097 2496.00 2424.10 50.00 4535 63.5229 2459.00 2419.34 50.00 4536 63.5360 2471.00 2414.76 50.00 4537 63.5491 2473.00 2410.83 50.00 4538 63.5623 2430.00 2407.63 49.00 4539 63.5754 2405.00 2405.18 49.00 4540 63.5885 2432.00 2403.57 49.00 4541 63.6017 2455.00 2403.19 50.00 4542 63.6148 2386.00 2404.26 49.00 4543 63.6279 2428.00 2406.98 49.00 4544 63.6410 2486.00 2411.34 50.00 4545 63.6542 2409.00 2417.07 49.00 4546 63.6673 2455.00 2423.57 50.00 4547 63.6804 2401.00 2430.28 49.00 4548 63.6936 2455.00 2435.68 50.00 4549 63.7067 2466.00 2436.82 50.00 4550 63.7198 2577.00 2432.84 51.00 4551 63.7330 2430.00 2427.43 49.00 4552 63.7461 2370.00 2424.50 49.00 4553 63.7592 2493.00 2425.03 50.00 4554 63.7723 2408.00 2427.35 49.00 4555 63.7855 2441.00 2428.57 49.00 4556 63.7986 2391.00 2426.50 49.00 4557 63.8117 2483.00 2422.03 50.00 4558 63.8249 2351.00 2417.88 48.00 4559 63.8380 2417.00 2416.08 49.00 4560 63.8511 2455.00 2417.18 50.00 4561 63.8643 2454.00 2420.46 50.00 4562 63.8774 2333.00 2424.09 48.00 4563 63.8905 2504.00 2426.45 50.00 4564 63.9036 2420.00 2428.81 49.00 4565 63.9168 2455.00 2434.20 50.00 4566 63.9299 2445.00 2444.27 49.00 4567 63.9430 2449.00 2458.26 49.00 4568 63.9562 2546.00 2472.14 50.00 4569 63.9693 2454.00 2480.03 50.00 4570 63.9824 2505.00 2478.05 50.00 4571 63.9956 2517.00 2467.38 50.00 4572 64.0087 2385.00 2454.18 49.00 4573 64.0218 2438.00 2444.07 49.00 4574 64.0350 2392.00 2439.49 49.00 4575 64.0481 2337.00 2439.97 48.00 4576 64.0612 2486.00 2444.56 50.00 4577 64.0743 2421.00 2452.21 49.00 4578 64.0875 2459.00 2460.78 50.00 4579 64.1006 2349.00 2468.24 48.00 4580 64.1137 2451.00 2473.47 50.00 4581 64.1269 2444.00 2474.60 49.00 4582 64.1400 2551.00 2470.45 51.00 4583 64.1531 2453.00 2462.10 50.00 4584 64.1663 2495.00 2451.55 50.00 4585 64.1794 2444.00 2441.34 49.00 4586 64.1925 2425.00 2433.98 49.00 4587 64.2056 2559.00 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64.5864 2409.00 2416.36 49.00 4617 64.5996 2401.00 2416.79 49.00 4618 64.6127 2478.00 2414.78 50.00 4619 64.6258 2420.00 2412.34 49.00 4620 64.6389 2325.00 2410.01 48.00 4621 64.6521 2426.00 2407.64 49.00 4622 64.6652 2381.00 2404.37 49.00 4623 64.6783 2408.00 2400.15 49.00 4624 64.6915 2496.00 2396.05 50.00 4625 64.7046 2303.00 2393.17 48.00 4626 64.7177 2389.00 2391.91 49.00 4627 64.7309 2386.00 2392.29 49.00 4628 64.7440 2377.00 2394.05 49.00 4629 64.7571 2435.00 2396.51 49.00 4630 64.7702 2464.00 2397.98 50.00 4631 64.7834 2457.00 2397.36 50.00 4632 64.7965 2424.00 2395.41 49.00 4633 64.8096 2427.00 2393.36 49.00 4634 64.8228 2457.00 2391.78 50.00 4635 64.8359 2458.00 2390.68 50.00 4636 64.8490 2363.00 2389.72 49.00 4637 64.8622 2385.00 2389.17 49.00 4638 64.8753 2338.00 2389.59 48.00 4639 64.8884 2411.00 2391.90 49.00 4640 64.9016 2407.00 2397.13 49.00 4641 64.9147 2408.00 2406.65 49.00 4642 64.9278 2467.00 2421.50 50.00 4643 64.9409 2390.00 2441.45 49.00 4644 64.9541 2424.00 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65.3348 2325.00 2403.93 48.00 4674 65.3480 2384.00 2405.94 49.00 4675 65.3611 2455.00 2404.46 50.00 4676 65.3742 2330.00 2400.95 48.00 4677 65.3874 2394.00 2397.70 49.00 4678 65.4005 2398.00 2395.22 49.00 4679 65.4136 2404.00 2392.94 49.00 4680 65.4268 2303.00 2390.75 48.00 4681 65.4399 2387.00 2388.59 49.00 4682 65.4530 2446.00 2386.32 49.00 4683 65.4662 2382.00 2384.36 49.00 4684 65.4793 2229.00 2383.73 47.00 4685 65.4924 2366.00 2384.92 49.00 4686 65.5055 2401.00 2387.30 49.00 4687 65.5187 2363.00 2389.27 49.00 4688 65.5318 2457.00 2389.57 50.00 4689 65.5449 2401.00 2387.63 49.00 4690 65.5581 2336.00 2384.03 48.00 4691 65.5712 2457.00 2379.65 50.00 4692 65.5843 2414.00 2375.47 49.00 4693 65.5975 2355.00 2371.85 49.00 4694 65.6106 2416.00 2369.00 49.00 4695 65.6237 2358.00 2366.90 49.00 4696 65.6368 2334.00 2365.24 48.00 4697 65.6500 2332.00 2364.06 48.00 4698 65.6631 2291.00 2363.87 48.00 4699 65.6762 2399.00 2364.68 49.00 4700 65.6894 2365.00 2366.29 49.00 4701 65.7025 2344.00 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66.0833 2382.00 2377.40 49.00 4731 66.0964 2431.00 2377.10 49.00 4732 66.1095 2305.00 2378.04 48.00 4733 66.1227 2384.00 2381.03 49.00 4734 66.1358 2356.00 2386.10 49.00 4735 66.1489 2419.00 2391.63 49.00 4736 66.1621 2298.00 2395.08 48.00 4737 66.1752 2417.00 2394.67 49.00 4738 66.1883 2391.00 2391.01 49.00 4739 66.2014 2432.00 2385.67 49.00 4740 66.2146 2428.00 2380.58 49.00 4741 66.2277 2313.00 2376.93 48.00 4742 66.2408 2336.00 2374.47 48.00 4743 66.2540 2390.00 2372.09 49.00 4744 66.2671 2381.00 2369.53 49.00 4745 66.2802 2376.00 2367.31 49.00 4746 66.2934 2350.00 2366.04 48.00 4747 66.3065 2400.00 2365.94 49.00 4748 66.3196 2422.00 2366.92 49.00 4749 66.3327 2467.00 2368.78 50.00 4750 66.3459 2412.00 2370.60 49.00 4751 66.3590 2371.00 2371.20 49.00 4752 66.3721 2410.00 2370.90 49.00 4753 66.3853 2341.00 2371.17 48.00 4754 66.3984 2442.00 2372.99 49.00 4755 66.4115 2472.00 2376.92 50.00 4756 66.4247 2350.00 2382.09 48.00 4757 66.4378 2376.00 2385.82 49.00 4758 66.4509 2443.00 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66.8317 2362.00 2341.88 49.00 4788 66.8448 2314.00 2342.02 48.00 4789 66.8580 2289.00 2342.99 48.00 4790 66.8711 2365.00 2344.42 49.00 4791 66.8842 2305.00 2345.33 48.00 4792 66.8973 2359.00 2344.47 49.00 4793 66.9105 2427.00 2342.00 49.00 4794 66.9236 2357.00 2339.36 49.00 4795 66.9367 2303.00 2337.66 48.00 4796 66.9499 2284.00 2337.03 48.00 4797 66.9630 2456.00 2337.18 50.00 4798 66.9761 2211.00 2337.93 47.00 4799 66.9893 2348.00 2338.75 48.00 4800 67.0024 2383.00 2339.38 49.00 4801 67.0155 2342.00 2340.31 48.00 4802 67.0287 2250.00 2341.87 47.00 4803 67.0418 2355.00 2343.95 49.00 4804 67.0549 2242.00 2345.95 47.00 4805 67.0680 2362.00 2347.08 49.00 4806 67.0812 2341.00 2346.50 48.00 4807 67.0943 2341.00 2344.23 48.00 4808 67.1074 2377.00 2341.57 49.00 4809 67.1206 2424.00 2340.08 49.00 4810 67.1337 2329.00 2340.95 48.00 4811 67.1468 2424.00 2343.91 49.00 4812 67.1600 2408.00 2347.61 49.00 4813 67.1731 2379.00 2349.79 49.00 4814 67.1862 2426.00 2349.35 49.00 4815 67.1993 2381.00 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67.5801 2391.00 2344.49 49.00 4845 67.5933 2299.00 2339.73 48.00 4846 67.6064 2339.00 2335.15 48.00 4847 67.6195 2318.00 2330.85 48.00 4848 67.6327 2259.00 2326.44 48.00 4849 67.6458 2273.00 2322.03 48.00 4850 67.6589 2283.00 2318.36 48.00 4851 67.6720 2305.00 2316.39 48.00 4852 67.6852 2294.00 2316.67 48.00 4853 67.6983 2317.00 2319.41 48.00 4854 67.7114 2280.00 2324.28 48.00 4855 67.7246 2250.00 2330.55 47.00 4856 67.7377 2281.00 2336.20 48.00 4857 67.7508 2254.00 2339.16 47.00 4858 67.7639 2359.00 2339.57 49.00 4859 67.7771 2369.00 2338.76 49.00 4860 67.7902 2396.00 2337.74 49.00 4861 67.8033 2320.00 2335.88 48.00 4862 67.8165 2327.00 2332.12 48.00 4863 67.8296 2296.00 2327.06 48.00 4864 67.8427 2282.00 2322.42 48.00 4865 67.8559 2395.00 2319.50 49.00 4866 67.8690 2372.00 2319.19 49.00 4867 67.8821 2239.00 2321.83 47.00 4868 67.8953 2383.00 2327.94 49.00 4869 67.9084 2374.00 2337.73 49.00 4870 67.9215 2374.00 2350.21 49.00 4871 67.9346 2368.00 2362.11 49.00 4872 67.9478 2282.00 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70.5738 2208.00 2228.77 47.00 5073 70.5870 2185.00 2227.28 47.00 5074 70.6001 2220.00 2227.25 47.00 5075 70.6132 2202.00 2228.84 47.00 5076 70.6264 2214.00 2230.93 47.00 5077 70.6395 2180.00 2232.04 47.00 5078 70.6526 2183.00 2231.13 47.00 5079 70.6657 2226.00 2228.04 47.00 5080 70.6789 2255.00 2223.93 47.00 5081 70.6920 2313.00 2220.98 48.00 5082 70.7051 2127.00 2220.79 46.00 5083 70.7183 2298.00 2223.36 48.00 5084 70.7314 2274.00 2227.10 48.00 5085 70.7445 2241.00 2229.80 47.00 5086 70.7577 2228.00 2229.99 47.00 5087 70.7708 2213.00 2227.31 47.00 5088 70.7839 2257.00 2222.95 48.00 5089 70.7971 2204.00 2218.67 47.00 5090 70.8102 2267.00 2215.87 48.00 5091 70.8233 2218.00 2214.94 47.00 5092 70.8364 2244.00 2215.35 47.00 5093 70.8496 2213.00 2216.65 47.00 5094 70.8627 2204.00 2218.97 47.00 5095 70.8758 2222.00 2222.63 47.00 5096 70.8890 2223.00 2228.09 47.00 5097 70.9021 2211.00 2235.01 47.00 5098 70.9152 2289.00 2241.85 48.00 5099 70.9284 2275.00 2246.28 48.00 5100 70.9415 2124.00 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71.3223 2206.00 2223.30 47.00 5130 71.3354 2159.00 2220.65 46.00 5131 71.3485 2212.00 2218.66 47.00 5132 71.3616 2172.00 2216.00 47.00 5133 71.3748 2231.00 2211.81 47.00 5134 71.3879 2186.00 2206.95 47.00 5135 71.4010 2192.00 2202.59 47.00 5136 71.4142 2112.00 2199.13 46.00 5137 71.4273 2216.00 2196.52 47.00 5138 71.4404 2142.00 2194.65 46.00 5139 71.4536 2081.00 2193.50 46.00 5140 71.4667 2131.00 2192.88 46.00 5141 71.4798 2171.00 2192.41 47.00 5142 71.4930 2270.00 2191.68 48.00 5143 71.5061 2292.00 2190.58 48.00 5144 71.5192 2266.00 2189.52 48.00 5145 71.5323 2167.00 2189.24 47.00 5146 71.5455 2207.00 2190.48 47.00 5147 71.5586 2222.00 2192.47 47.00 5148 71.5717 2230.00 2194.74 47.00 5149 71.5849 2204.00 2196.69 47.00 5150 71.5980 2241.00 2198.13 47.00 5151 71.6111 2224.00 2199.10 47.00 5152 71.6243 2243.00 2199.77 47.00 5153 71.6374 2174.00 2200.73 47.00 5154 71.6505 2240.00 2202.84 47.00 5155 71.6636 2171.00 2205.72 47.00 5156 71.6768 2316.00 2207.50 48.00 5157 71.6899 2166.00 2206.27 47.00 5158 71.7030 2153.00 2202.24 46.00 5159 71.7162 2224.00 2197.55 47.00 5160 71.7293 2249.00 2193.57 47.00 5161 71.7424 2174.00 2190.91 47.00 5162 71.7556 2196.00 2189.87 47.00 5163 71.7687 2162.00 2191.30 46.00 5164 71.7818 2165.00 2195.49 47.00 5165 71.7950 2149.00 2201.53 46.00 5166 71.8081 2106.00 2207.31 46.00 5167 71.8212 2223.00 2211.05 47.00 5168 71.8343 2216.00 2211.29 47.00 5169 71.8475 2115.00 2208.50 46.00 5170 71.8606 2273.00 2204.74 48.00 5171 71.8737 2208.00 2201.59 47.00 5172 71.8869 2185.00 2198.92 47.00 5173 71.9000 2264.00 2195.59 48.00 5174 71.9131 2124.00 2191.28 46.00 5175 71.9262 2200.00 2186.71 47.00 5176 71.9394 2145.00 2182.32 46.00 5177 71.9525 2159.00 2178.52 46.00 5178 71.9656 2135.00 2175.75 46.00 5179 71.9788 2241.00 2174.63 47.00 5180 71.9919 2209.00 2175.32 47.00 5181 72.0050 2108.00 2177.39 46.00 5182 72.0182 2192.00 2179.89 47.00 5183 72.0313 2218.00 2181.86 47.00 5184 72.0444 2102.00 2182.51 46.00 5185 72.0576 2205.00 2181.95 47.00 5186 72.0707 2190.00 2180.76 47.00 5187 72.0838 2155.00 2179.97 46.00 5188 72.0969 2176.00 2180.20 47.00 5189 72.1101 2161.00 2181.32 46.00 5190 72.1232 2201.00 2183.18 47.00 5191 72.1363 2218.00 2186.14 47.00 5192 72.1495 2208.00 2190.77 47.00 5193 72.1626 2245.00 2197.18 47.00 5194 72.1757 2155.00 2204.17 46.00 5195 72.1889 2115.00 2208.98 46.00 5196 72.2020 2187.00 2208.88 47.00 5197 72.2151 2260.00 2203.95 48.00 5198 72.2282 2209.00 2197.23 47.00 5199 72.2414 2218.00 2191.33 47.00 5200 72.2545 2097.00 2187.06 46.00 5201 72.2676 2228.00 2184.14 47.00 5202 72.2808 2175.00 2182.45 47.00 5203 72.2939 2160.00 2180.88 46.00 5204 72.3070 2165.00 2179.35 47.00 5205 72.3202 2191.00 2177.66 47.00 5206 72.3333 2181.00 2176.10 47.00 5207 72.3464 2143.00 2175.73 46.00 5208 72.3596 2117.00 2177.64 46.00 5209 72.3727 2235.00 2181.82 47.00 5210 72.3858 2178.00 2186.98 47.00 5211 72.3989 2207.00 2190.73 47.00 5212 72.4121 2132.00 2191.02 46.00 5213 72.4252 2203.00 2188.05 47.00 5214 72.4383 2152.00 2183.39 46.00 5215 72.4515 2174.00 2178.60 47.00 5216 72.4646 2235.00 2174.73 47.00 5217 72.4777 2112.00 2172.37 46.00 5218 72.4909 2124.00 2171.41 46.00 5219 72.5040 2184.00 2171.17 47.00 5220 72.5171 2213.00 2170.89 47.00 5221 72.5302 2161.00 2170.47 46.00 5222 72.5434 2215.00 2170.26 47.00 5223 72.5565 2101.00 2170.70 46.00 5224 72.5696 2112.00 2171.60 46.00 5225 72.5828 2111.00 2171.79 46.00 5226 72.5959 2188.00 2170.49 47.00 5227 72.6090 2148.00 2167.73 46.00 5228 72.6221 2203.00 2164.07 47.00 5229 72.6353 2188.00 2160.12 47.00 5230 72.6484 2196.00 2156.64 47.00 5231 72.6615 2149.00 2153.94 46.00 5232 72.6747 2242.00 2152.51 47.00 5233 72.6878 2074.00 2152.64 46.00 5234 72.7009 2240.00 2154.18 47.00 5235 72.7141 2149.00 2156.69 46.00 5236 72.7272 2177.00 2159.52 47.00 5237 72.7403 2185.00 2162.07 47.00 5238 72.7535 2111.00 2163.93 46.00 5239 72.7666 2160.00 2165.31 46.00 5240 72.7797 2222.00 2166.42 47.00 5241 72.7928 2208.00 2166.75 47.00 5242 72.8060 2214.00 2165.98 47.00 5243 72.8191 2191.00 2164.83 47.00 5244 72.8322 2166.00 2164.67 47.00 5245 72.8454 2098.00 2166.71 46.00 5246 72.8585 2157.00 2171.52 46.00 5247 72.8716 2110.00 2179.04 46.00 5248 72.8848 2236.00 2187.71 47.00 5249 72.8979 2234.00 2194.56 47.00 5250 72.9110 2159.00 2196.65 46.00 5251 72.9242 2224.00 2193.97 47.00 5252 72.9373 2135.00 2188.79 46.00 5253 72.9504 2143.00 2183.26 46.00 5254 72.9635 2142.00 2178.51 46.00 5255 72.9767 2153.00 2174.84 46.00 5256 72.9898 2198.00 2172.58 47.00 5257 73.0029 2113.00 2171.47 46.00 5258 73.0161 2163.00 2170.63 47.00 5259 73.0292 2134.00 2169.42 46.00 5260 73.0423 2195.00 2168.52 47.00 5261 73.0555 2214.00 2168.87 47.00 5262 73.0686 2222.00 2170.94 47.00 5263 73.0817 2211.00 2174.60 47.00 5264 73.0948 2029.00 2179.56 45.00 5265 73.1080 2145.00 2184.98 46.00 5266 73.1211 2186.00 2189.24 47.00 5267 73.1342 2177.00 2190.77 47.00 5268 73.1474 2193.00 2188.72 47.00 5269 73.1605 2121.00 2182.34 46.00 5270 73.1736 2212.00 2173.17 47.00 5271 73.1868 2162.00 2163.77 46.00 5272 73.1999 2159.00 2156.53 46.00 5273 73.2130 2144.00 2152.33 46.00 5274 73.2262 2133.00 2150.69 46.00 5275 73.2393 2140.00 2150.55 46.00 5276 73.2524 2184.00 2150.96 47.00 5277 73.2655 2167.00 2151.23 47.00 5278 73.2787 2127.00 2151.36 46.00 5279 73.2918 2156.00 2151.78 46.00 5280 73.3049 2169.00 2153.10 47.00 5281 73.3181 2166.00 2156.16 47.00 5282 73.3312 2153.00 2160.74 46.00 5283 73.3443 2152.00 2165.36 46.00 5284 73.3575 2120.00 2167.81 46.00 5285 73.3706 2186.00 2166.81 47.00 5286 73.3837 2189.00 2162.94 47.00 5287 73.3968 2185.00 2158.90 47.00 5288 73.4100 2157.00 2156.88 46.00 5289 73.4231 2141.00 2157.00 46.00 5290 73.4362 2161.00 2157.42 46.00 5291 73.4494 2237.00 2156.26 47.00 5292 73.4625 2188.00 2153.05 47.00 5293 73.4756 2161.00 2148.58 46.00 5294 73.4887 2166.00 2144.20 47.00 5295 73.5019 2085.00 2141.19 46.00 5296 73.5150 2151.00 2140.34 46.00 5297 73.5281 2128.00 2141.50 46.00 5298 73.5413 2137.00 2143.89 46.00 5299 73.5544 2134.00 2146.44 46.00 5300 73.5675 2108.00 2148.38 46.00 5301 73.5807 2134.00 2149.41 46.00 5302 73.5938 2190.00 2150.19 47.00 5303 73.6069 2164.00 2151.63 47.00 5304 73.6201 2187.00 2154.56 47.00 5305 73.6332 2119.00 2158.97 46.00 5306 73.6463 2122.00 2163.72 46.00 5307 73.6594 2155.00 2166.75 46.00 5308 73.6726 2089.00 2166.28 46.00 5309 73.6857 2185.00 2161.40 47.00 5310 73.6988 2190.00 2153.24 47.00 5311 73.7120 2126.00 2144.21 46.00 5312 73.7251 2175.00 2136.69 47.00 5313 73.7382 2231.00 2131.94 47.00 5314 73.7514 2117.00 2129.78 46.00 5315 73.7645 2150.00 2129.84 46.00 5316 73.7776 2115.00 2131.72 46.00 5317 73.7907 2220.00 2135.31 47.00 5318 73.8039 2235.00 2140.66 47.00 5319 73.8170 2108.00 2147.28 46.00 5320 73.8301 2146.00 2153.86 46.00 5321 73.8433 2144.00 2158.85 46.00 5322 73.8564 2082.00 2161.72 46.00 5323 73.8695 2128.00 2162.78 46.00 5324 73.8827 2149.00 2162.30 46.00 5325 73.8958 2115.00 2160.30 46.00 5326 73.9089 2181.00 2157.07 47.00 5327 73.9221 2196.00 2153.02 47.00 5328 73.9352 2121.00 2148.24 46.00 5329 73.9483 2195.00 2143.07 47.00 5330 73.9614 2158.00 2138.84 46.00 5331 73.9746 2150.00 2136.96 46.00 5332 73.9877 2089.00 2137.56 46.00 5333 74.0008 2097.00 2139.80 46.00 5334 74.0140 2137.00 2143.27 46.00 5335 74.0271 2151.00 2148.13 46.00 5336 74.0402 2063.00 2153.58 45.00 5337 74.0534 2191.00 2157.67 47.00 5338 74.0665 2149.00 2158.92 46.00 5339 74.0796 2152.00 2157.38 46.00 5340 74.0928 2181.00 2154.10 47.00 5341 74.1059 2146.00 2150.19 46.00 5342 74.1190 2179.00 2146.49 47.00 5343 74.1321 2119.00 2143.80 46.00 5344 74.1453 2101.00 2142.42 46.00 5345 74.1584 2158.00 2142.09 46.00 5346 74.1715 2260.00 2142.53 48.00 5347 74.1847 2150.00 2143.75 46.00 5348 74.1978 2170.00 2145.22 47.00 5349 74.2109 2129.00 2146.48 46.00 5350 74.2241 2196.00 2147.16 47.00 5351 74.2372 2118.00 2146.75 46.00 5352 74.2503 2133.00 2145.18 46.00 5353 74.2634 2125.00 2143.40 46.00 5354 74.2766 2260.00 2141.98 48.00 5355 74.2897 2102.00 2141.42 46.00 5356 74.3028 2187.00 2141.36 47.00 5357 74.3160 2175.00 2141.10 47.00 5358 74.3291 2114.00 2139.95 46.00 5359 74.3422 2239.00 2137.72 47.00 5360 74.3553 2219.00 2134.66 47.00 5361 74.3685 2082.00 2131.65 46.00 5362 74.3816 2085.00 2129.54 46.00 5363 74.3947 2219.00 2128.81 47.00 5364 74.4079 2163.00 2129.09 47.00 5365 74.4210 2036.00 2129.77 45.00 5366 74.4341 2187.00 2129.94 47.00 5367 74.4473 2094.00 2129.44 46.00 5368 74.4604 2102.00 2128.54 46.00 5369 74.4735 2167.00 2128.38 47.00 5370 74.4867 2163.00 2129.95 47.00 5371 74.4998 2078.00 2132.85 46.00 5372 74.5129 2143.00 2134.93 46.00 5373 74.5260 2086.00 2134.31 46.00 5374 74.5392 2129.00 2131.30 46.00 5375 74.5523 2158.00 2127.53 46.00 5376 74.5654 2039.00 2124.11 45.00 5377 74.5786 2131.00 2121.68 46.00 5378 74.5917 2165.00 2120.59 47.00 5379 74.6048 2212.00 2120.99 47.00 5380 74.6180 2235.00 2122.78 47.00 5381 74.6311 2102.00 2125.39 46.00 5382 74.6442 2172.00 2127.69 47.00 5383 74.6573 2109.00 2128.64 46.00 5384 74.6705 2056.00 2128.08 45.00 5385 74.6836 2065.00 2126.79 45.00 5386 74.6967 2070.00 2125.91 45.00 5387 74.7099 2055.00 2126.23 45.00 5388 74.7230 2142.00 2128.21 46.00 5389 74.7361 2144.00 2131.93 46.00 5390 74.7493 2219.00 2137.61 47.00 5391 74.7624 2123.00 2145.07 46.00 5392 74.7755 2178.00 2152.34 47.00 5393 74.7887 2171.00 2156.61 47.00 5394 74.8018 2081.00 2156.21 46.00 5395 74.8149 2078.00 2151.47 46.00 5396 74.8280 2188.00 2144.76 47.00 5397 74.8412 2138.00 2138.89 46.00 5398 74.8543 2130.00 2135.58 46.00 5399 74.8674 2131.00 2135.42 46.00 5400 74.8806 2236.00 2138.43 47.00 5401 74.8937 2124.00 2144.44 46.00 5402 74.9068 2142.00 2152.48 46.00 5403 74.9200 2157.00 2160.51 46.00 5404 74.9331 2172.00 2166.73 47.00 5405 74.9462 2102.00 2170.70 46.00 5406 74.9594 2208.00 2173.03 47.00 5407 74.9725 2130.00 2174.82 46.00 5408 74.9856 2192.00 2175.95 47.00 5409 74.9987 2173.00 2174.75 47.00 5410 75.0119 2262.00 2169.68 48.00 5411 75.0250 2146.00 2161.60 46.00 5412 75.0381 2146.00 2153.04 46.00 5413 75.0513 2133.00 2146.25 46.00 5414 75.0644 2183.00 2142.29 47.00 5415 75.0775 2132.00 2140.64 46.00 5416 75.0907 2181.00 2140.28 47.00 5417 75.1038 2116.00 2141.47 46.00 5418 75.1169 2173.00 2145.29 47.00 5419 75.1300 2203.00 2151.99 47.00 5420 75.1432 2168.00 2160.35 47.00 5421 75.1563 2167.00 2168.16 47.00 5422 75.1694 2107.00 2173.09 46.00 5423 75.1826 2187.00 2174.12 47.00 5424 75.1957 2131.00 2171.66 46.00 5425 75.2088 2199.00 2166.04 47.00 5426 75.2219 2216.00 2157.76 47.00 5427 75.2351 2077.00 2148.78 46.00 5428 75.2482 2155.00 2141.73 46.00 5429 75.2613 2162.00 2137.83 46.00 5430 75.2745 2110.00 2136.62 46.00 5431 75.2876 2148.00 2136.58 46.00 5432 75.3007 2200.00 2135.97 47.00 5433 75.3139 2146.00 2133.82 46.00 5434 75.3270 2102.00 2130.58 46.00 5435 75.3401 2130.00 2127.59 46.00 5436 75.3533 2132.00 2126.13 46.00 5437 75.3664 2123.00 2126.55 46.00 5438 75.3795 2149.00 2127.99 46.00 5439 75.3926 2110.00 2129.10 46.00 5440 75.4058 2210.00 2129.19 47.00 5441 75.4189 2220.00 2128.34 47.00 5442 75.4320 2149.00 2126.78 46.00 5443 75.4452 2110.00 2125.08 46.00 5444 75.4583 2141.00 2124.17 46.00 5445 75.4714 2121.00 2124.75 46.00 5446 75.4846 2180.00 2126.56 47.00 5447 75.4977 2133.00 2128.67 46.00 5448 75.5108 2135.00 2129.97 46.00 5449 75.5239 2151.00 2130.16 46.00 5450 75.5371 2177.00 2129.53 47.00 5451 75.5502 2094.00 2128.25 46.00 5452 75.5633 2181.00 2126.61 47.00 5453 75.5765 2176.00 2125.18 47.00 5454 75.5896 2101.00 2124.21 46.00 5455 75.6027 2091.00 2123.49 46.00 5456 75.6159 2187.00 2122.94 47.00 5457 75.6290 2087.00 2122.76 46.00 5458 75.6421 2156.00 2123.44 46.00 5459 75.6553 2142.00 2124.90 46.00 5460 75.6684 2104.00 2126.61 46.00 5461 75.6815 2067.00 2127.82 45.00 5462 75.6946 2067.00 2128.03 45.00 5463 75.7078 2177.00 2127.33 47.00 5464 75.7209 2082.00 2126.43 46.00 5465 75.7340 2060.00 2126.22 45.00 5466 75.7472 2145.00 2127.14 46.00 5467 75.7603 2108.00 2128.93 46.00 5468 75.7734 2195.00 2130.29 47.00 5469 75.7866 2198.00 2130.25 47.00 5470 75.7997 2067.00 2128.78 45.00 5471 75.8128 2016.00 2126.30 45.00 5472 75.8259 2212.00 2123.46 47.00 5473 75.8391 2136.00 2120.92 46.00 5474 75.8522 2099.00 2119.35 46.00 5475 75.8653 2102.00 2118.92 46.00 5476 75.8785 2118.00 2119.53 46.00 5477 75.8916 2042.00 2120.75 45.00 5478 75.9047 2162.00 2122.19 46.00 5479 75.9178 2076.00 2123.72 46.00 5480 75.9310 2195.00 2125.58 47.00 5481 75.9441 2090.00 2127.95 46.00 5482 75.9573 2153.00 2130.90 46.00 5483 75.9704 2177.00 2134.16 47.00 5484 75.9835 2173.00 2137.23 47.00 5485 75.9966 2064.00 2139.20 45.00 5486 76.0098 2153.00 2139.98 46.00 5487 76.0229 2265.00 2140.46 48.00 5488 76.0360 2162.00 2141.48 46.00 5489 76.0492 2129.00 2142.92 46.00 5490 76.0623 2099.00 2143.85 46.00 5491 76.0754 2154.00 2143.32 46.00 5492 76.0885 2209.00 2140.76 47.00 5493 76.1017 2134.00 2136.21 46.00 5494 76.1148 2101.00 2130.37 46.00 5495 76.1279 2107.00 2124.47 46.00 5496 76.1411 2137.00 2119.83 46.00 5497 76.1542 2174.00 2117.28 47.00 5498 76.1673 2090.00 2116.75 46.00 5499 76.1805 2093.00 2117.84 46.00 5500 76.1936 2097.00 2120.06 46.00 5501 76.2067 2086.00 2122.72 46.00 5502 76.2199 2110.00 2125.14 46.00 5503 76.2330 2052.00 2126.86 45.00 5504 76.2461 2132.00 2127.98 46.00 5505 76.2592 2113.00 2128.69 46.00 5506 76.2724 2088.00 2129.39 46.00 5507 76.2855 2114.00 2130.12 46.00 5508 76.2986 2094.00 2130.69 46.00 5509 76.3118 2121.00 2130.84 46.00 5510 76.3249 2138.00 2129.95 46.00 5511 76.3380 2153.00 2128.24 46.00 5512 76.3512 2201.00 2126.36 47.00 5513 76.3643 2115.00 2125.56 46.00 5514 76.3774 2122.00 2126.91 46.00 5515 76.3905 2121.00 2130.54 46.00 5516 76.4037 2122.00 2135.58 46.00 5517 76.4168 2066.00 2140.74 45.00 5518 76.4299 2137.00 2144.60 46.00 5519 76.4431 2179.00 2145.87 47.00 5520 76.4562 2168.00 2143.82 47.00 5521 76.4693 2146.00 2139.42 46.00 5522 76.4825 2010.00 2134.51 45.00 5523 76.4956 2174.00 2130.18 47.00 5524 76.5087 2105.00 2126.74 46.00 5525 76.5219 2056.00 2124.22 45.00 5526 76.5350 2099.00 2122.95 46.00 5527 76.5481 2089.00 2122.89 46.00 5528 76.5612 2161.00 2124.50 46.00 5529 76.5744 2145.00 2128.02 46.00 5530 76.5875 2069.00 2132.97 45.00 5531 76.6006 2205.00 2137.96 47.00 5532 76.6138 2171.00 2141.23 47.00 5533 76.6269 2168.00 2142.23 47.00 5534 76.6400 2181.00 2141.50 47.00 5535 76.6532 2042.00 2139.45 45.00 5536 76.6663 2156.00 2136.65 46.00 5537 76.6794 2191.00 2133.66 47.00 5538 76.6925 2074.00 2131.55 46.00 5539 76.7057 2094.00 2131.12 46.00 5540 76.7188 2158.00 2132.11 46.00 5541 76.7319 2178.00 2133.05 47.00 5542 76.7451 1985.00 2132.38 45.00 5543 76.7582 2165.00 2129.78 47.00 5544 76.7713 2106.00 2126.58 46.00 5545 76.7844 2112.00 2124.49 46.00 5546 76.7976 2109.00 2124.49 46.00 5547 76.8107 2145.00 2126.55 46.00 5548 76.8238 2095.00 2129.40 46.00 5549 76.8370 2163.00 2131.21 47.00 5550 76.8501 2172.00 2131.50 47.00 5551 76.8632 2019.00 2131.32 45.00 5552 76.8764 2079.00 2131.62 46.00 5553 76.8895 2137.00 2132.39 46.00 5554 76.9026 2118.00 2133.20 46.00 5555 76.9158 2220.00 2134.04 47.00 5556 76.9289 2105.00 2135.60 46.00 5557 76.9420 2155.00 2138.40 46.00 5558 76.9551 2033.00 2141.71 45.00 5559 76.9683 2162.00 2143.62 46.00 5560 76.9814 2025.00 2142.44 45.00 5561 76.9945 2230.00 2138.43 47.00 5562 77.0077 1987.00 2133.53 45.00 5563 77.0208 2121.00 2129.79 46.00 5564 77.0339 2112.00 2128.31 46.00 5565 77.0471 2181.00 2129.21 47.00 5566 77.0602 2117.00 2131.92 46.00 5567 77.0733 2122.00 2135.80 46.00 5568 77.0865 2132.00 2140.56 46.00 5569 77.0996 2146.00 2145.78 46.00 5570 77.1127 2156.00 2150.29 46.00 5571 77.1258 2146.00 2152.34 46.00 5572 77.1390 2037.00 2151.03 45.00 5573 77.1521 2135.00 2147.08 46.00 5574 77.1652 2083.00 2142.35 46.00 5575 77.1784 2178.00 2138.67 47.00 5576 77.1915 2199.00 2136.71 47.00 5577 77.2046 2060.00 2135.66 45.00 5578 77.2178 2104.00 2133.69 46.00 5579 77.2309 2164.00 2129.39 47.00 5580 77.2440 2087.00 2123.12 46.00 5581 77.2571 2122.00 2116.60 46.00 5582 77.2703 2122.00 2111.43 46.00 5583 77.2834 2129.00 2108.25 46.00 5584 77.2965 2154.00 2107.10 46.00 5585 77.3097 2008.00 2107.64 45.00 5586 77.3228 2142.00 2109.21 46.00 5587 77.3359 2189.00 2110.86 47.00 5588 77.3491 2113.00 2111.55 46.00 5589 77.3622 2092.00 2110.65 46.00 5590 77.3753 2247.00 2108.54 47.00 5591 77.3885 2157.00 2106.39 46.00 5592 77.4016 2205.00 2104.92 47.00 5593 77.4147 2160.00 2104.07 46.00 5594 77.4278 2132.00 2103.07 46.00 5595 77.4410 2064.00 2101.10 45.00 5596 77.4541 2099.00 2097.75 46.00 5597 77.4672 2113.00 2093.26 46.00 5598 77.4804 2060.00 2088.85 45.00 5599 77.4935 2084.00 2085.89 46.00 5600 77.5066 2082.00 2085.27 46.00 5601 77.5198 2166.00 2087.40 47.00 5602 77.5329 2160.00 2092.22 46.00 5603 77.5460 2090.00 2098.79 46.00 5604 77.5591 2043.00 2105.53 45.00 5605 77.5723 2206.00 2110.48 47.00 5606 77.5854 2218.00 2112.28 47.00 5607 77.5985 2178.00 2111.16 47.00 5608 77.6117 2067.00 2108.77 45.00 5609 77.6248 2082.00 2106.89 46.00 5610 77.6379 2106.00 2105.80 46.00 5611 77.6510 2124.00 2104.38 46.00 5612 77.6642 2102.00 2101.42 46.00 5613 77.6773 2114.00 2097.20 46.00 5614 77.6904 2150.00 2092.91 46.00 5615 77.7036 2082.00 2088.97 46.00 5616 77.7167 2090.00 2085.42 46.00 5617 77.7298 2116.00 2082.52 46.00 5618 77.7430 2091.00 2081.09 46.00 5619 77.7561 2225.00 2081.65 47.00 5620 77.7692 2138.00 2084.08 46.00 5621 77.7824 2056.00 2087.47 45.00 5622 77.7955 2059.00 2090.78 45.00 5623 77.8086 2211.00 2093.42 47.00 5624 77.8217 2120.00 2095.44 46.00 5625 77.8349 2091.00 2097.00 46.00 5626 77.8480 2161.00 2097.75 46.00 5627 77.8611 2063.00 2097.14 45.00 5628 77.8743 2046.00 2095.01 45.00 5629 77.8874 2062.00 2092.06 45.00 5630 77.9005 2041.00 2090.02 45.00 5631 77.9137 2117.00 2090.30 46.00 5632 77.9268 2049.00 2092.86 45.00 5633 77.9399 2128.00 2096.21 46.00 5634 77.9530 2044.00 2099.05 45.00 5635 77.9662 2039.00 2101.56 45.00 5636 77.9793 2105.00 2104.93 46.00 5637 77.9924 2037.00 2109.80 45.00 5638 78.0056 2162.00 2114.70 46.00 5639 78.0187 2108.00 2116.97 46.00 5640 78.0318 2017.00 2114.60 45.00 5641 78.0450 2127.00 2107.72 46.00 5642 78.0581 2082.00 2098.58 46.00 5643 78.0712 2162.00 2090.32 46.00 5644 78.0844 2121.00 2085.05 46.00 5645 78.0975 2180.00 2083.03 47.00 5646 78.1106 2073.00 2083.37 46.00 5647 78.1237 2120.00 2084.98 46.00 5648 78.1369 2075.00 2087.36 46.00 5649 78.1500 2026.00 2090.18 45.00 5650 78.1631 2153.00 2092.72 46.00 5651 78.1763 2033.00 2093.73 45.00 5652 78.1894 2113.00 2092.37 46.00 5653 78.2025 2162.00 2089.40 46.00 5654 78.2157 2093.00 2086.69 46.00 5655 78.2288 2082.00 2084.89 46.00 5656 78.2419 2097.00 2083.74 46.00 5657 78.2551 2099.00 2082.04 46.00 5658 78.2682 2085.00 2079.01 46.00 5659 78.2813 2051.00 2075.05 45.00 5660 78.2944 2173.00 2071.69 47.00 5661 78.3076 2048.00 2070.69 45.00 5662 78.3207 2080.00 2072.73 46.00 5663 78.3338 2097.00 2077.18 46.00 5664 78.3470 2058.00 2082.40 45.00 5665 78.3601 2156.00 2086.54 46.00 5666 78.3732 2118.00 2088.14 46.00 5667 78.3864 1998.00 2086.57 45.00 5668 78.3995 2108.00 2082.38 46.00 5669 78.4126 2116.00 2076.90 46.00 5670 78.4257 2050.00 2071.51 45.00 5671 78.4389 2145.00 2066.93 46.00 5672 78.4520 2022.00 2063.97 45.00 5673 78.4651 2032.00 2062.55 45.00 5674 78.4783 2045.00 2062.19 45.00 5675 78.4914 2041.00 2062.27 45.00 5676 78.5045 2129.00 2062.62 46.00 5677 78.5176 2077.00 2063.72 46.00 5678 78.5308 2020.00 2065.95 45.00 5679 78.5439 2012.00 2069.23 45.00 5680 78.5570 2178.00 2073.05 47.00 5681 78.5702 2014.00 2077.68 45.00 5682 78.5833 2071.00 2083.51 46.00 5683 78.5964 2045.00 2089.95 45.00 5684 78.6096 2067.00 2094.91 45.00 5685 78.6227 2041.00 2095.79 45.00 5686 78.6358 2060.00 2091.71 45.00 5687 78.6490 2112.00 2084.14 46.00 5688 78.6621 2085.00 2075.87 46.00 5689 78.6752 2072.00 2069.57 46.00 5690 78.6883 2062.00 2066.74 45.00 5691 78.7015 2113.00 2067.27 46.00 5692 78.7146 2071.00 2070.41 46.00 5693 78.7277 2031.00 2074.88 45.00 5694 78.7409 2034.00 2079.09 45.00 5695 78.7540 2055.00 2081.55 45.00 5696 78.7671 2023.00 2081.08 45.00 5697 78.7803 2042.00 2077.90 45.00 5698 78.7934 2072.00 2073.75 46.00 5699 78.8065 2023.00 2070.77 45.00 5700 78.8196 2066.00 2070.08 45.00 5701 78.8328 2054.00 2071.88 45.00 5702 78.8459 2113.00 2075.05 46.00 5703 78.8590 2108.00 2077.84 46.00 5704 78.8722 2117.00 2078.66 46.00 5705 78.8853 2041.00 2076.86 45.00 5706 78.8984 2082.00 2072.99 46.00 5707 78.9116 2085.00 2068.57 46.00 5708 78.9247 2117.00 2065.35 46.00 5709 78.9378 2060.00 2064.82 45.00 5710 78.9510 2032.00 2067.85 45.00 5711 78.9641 2109.00 2074.28 46.00 5712 78.9772 2034.00 2082.59 45.00 5713 78.9903 2001.00 2089.87 45.00 5714 79.0035 2104.00 2093.02 46.00 5715 79.0166 2100.00 2090.93 46.00 5716 79.0297 2031.00 2084.90 45.00 5717 79.0429 2029.00 2077.16 45.00 5718 79.0560 2020.00 2069.87 45.00 5719 79.0691 2071.00 2064.47 46.00 5720 79.0823 2047.00 2061.45 45.00 5721 79.0954 2109.00 2060.10 46.00 5722 79.1085 2011.00 2059.28 45.00 5723 79.1217 2081.00 2058.32 46.00 5724 79.1348 2085.00 2057.18 46.00 5725 79.1479 2021.00 2056.14 45.00 5726 79.1610 2130.00 2055.81 46.00 5727 79.1742 2067.00 2056.94 45.00 5728 79.1873 2062.00 2060.02 45.00 5729 79.2004 2013.00 2064.86 45.00 5730 79.2136 2114.00 2070.99 46.00 5731 79.2267 2031.00 2077.36 45.00 5732 79.2398 1993.00 2082.20 45.00 5733 79.2530 1998.00 2083.62 45.00 5734 79.2661 2138.00 2080.36 46.00 5735 79.2792 2024.00 2072.65 45.00 5736 79.2923 2076.00 2062.70 46.00 5737 79.3055 2121.00 2053.59 46.00 5738 79.3186 2108.00 2047.61 46.00 5739 79.3317 2017.00 2045.40 45.00 5740 79.3449 2013.00 2046.34 45.00 5741 79.3580 2155.00 2049.28 46.00 5742 79.3711 2108.00 2052.65 46.00 5743 79.3842 2046.00 2055.04 45.00 5744 79.3974 2072.00 2055.75 46.00 5745 79.4105 2057.00 2054.77 45.00 5746 79.4237 2143.00 2052.37 46.00 5747 79.4368 1994.00 2048.87 45.00 5748 79.4499 2049.00 2044.97 45.00 5749 79.4630 2101.00 2042.10 46.00 5750 79.4762 1993.00 2040.59 45.00 5751 79.4893 2102.00 2039.13 46.00 5752 79.5024 2088.00 2035.99 46.00 5753 79.5156 2027.00 2030.58 45.00 5754 79.5287 2055.00 2024.00 45.00 5755 79.5418 2040.00 2018.48 45.00 5756 79.5549 1962.00 2015.80 44.00 5757 79.5681 2067.00 2016.55 45.00 5758 79.5812 1991.00 2020.07 45.00 5759 79.5943 2055.00 2024.98 45.00 5760 79.6075 1967.00 2029.58 44.00 5761 79.6206 1999.00 2032.22 45.00 5762 79.6337 2037.00 2031.85 45.00 5763 79.6469 2048.00 2028.44 45.00 5764 79.6600 1979.00 2022.99 44.00 5765 79.6731 2004.00 2017.15 45.00 5766 79.6862 1995.00 2012.71 45.00 5767 79.6994 1974.00 2010.85 44.00 5768 79.7125 2105.00 2011.24 46.00 5769 79.7256 1987.00 2012.69 45.00 5770 79.7388 2061.00 2014.18 45.00 5771 79.7519 2085.00 2015.42 46.00 5772 79.7650 2041.00 2015.81 45.00 5773 79.7782 2030.00 2014.86 45.00 5774 79.7913 2009.00 2012.27 45.00 5775 79.8044 1980.00 2008.92 44.00 5776 79.8176 2015.00 2006.11 45.00 5777 79.8307 2049.00 2005.04 45.00 5778 79.8438 1948.00 2005.63 44.00 5779 79.8569 2046.00 2007.05 45.00 5780 79.8701 1987.00 2008.60 45.00 5781 79.8832 1939.00 2010.06 44.00 5782 79.8963 2069.00 2011.66 45.00 5783 79.9095 1978.00 2014.03 44.00 5784 79.9226 1968.00 2017.96 44.00 5785 79.9357 2073.00 2024.22 46.00 5786 79.9489 2008.00 2033.31 45.00 5787 79.9620 2040.00 2045.37 45.00 5788 79.9751 2063.00 2059.98 45.00 # 12. STRUCTURE-FACTOR LIST loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_observed_status _refln_d_spacing 2 0 0 9705.23 9660.10 o 12.666059 3 0 0 1145.15 1729.43 o 8.444040 0 0 2 98.59 115.01 < 8.324042 -1 0 2 10159.15 10249.62 o 8.123255 1 0 2 6471.41 6454.37 o 7.709083 -2 0 2 19.10 221.68 < 7.256032 2 0 2 386.90 108.47 < 6.690866 1 1 0 7696.56 7198.27 o 6.446821 4 0 0 466.88 557.72 o 6.333030 -3 0 2 590.34 605.10 o 6.207839 0 1 1 70.60 28.80 < 6.188606 -1 1 1 9245.59 8394.41 o 6.057742 1 1 1 4283.80 3370.15 o 5.966902 2 1 0 780.25 969.93 o 5.899146 3 0 2 2236.93 1762.48 o 5.682810 -2 1 1 7094.19 6279.09 o 5.633674 2 1 1 11123.63 11129.39 o 5.489885 -4 0 2 11306.36 13616.50 o 5.268918 3 1 0 12725.05 12469.52 o 5.232283 0 1 2 274.35 305.99 o 5.203355 -1 1 2 20539.39 19272.92 o 5.153212 -3 1 1 3891.10 3726.98 o 5.071423 5 0 0 9729.39 9290.27 o 5.066424 1 1 2 1581.17 1466.83 o 5.042476 3 1 1 2362.97 2370.92 o 4.915360 -2 1 2 11340.38 11418.66 o 4.909057 4 0 2 1097.06 622.40 < 4.838802 2 1 2 5281.69 4438.43 o 4.722451 4 1 0 6209.71 5753.10 o 4.591431 -3 1 2 18974.54 16355.81 o 4.543046 -5 0 2 61073.48 56114.85 o 4.507892 -4 1 1 16446.27 15480.37 o 4.500511 4 1 1 15215.65 12915.82 o 4.355421 3 1 2 84.20 88.80 o 4.324687 0 1 3 6091.47 4896.73 o 4.264992 -1 1 3 78.35 63.18 o 4.253239 6 0 0 134.57 131.27 < 4.222020 5 0 2 438.89 470.63 o 4.167737 -1 0 4 14448.21 15485.15 o 4.166129 0 0 4 1406.18 1507.55 o 4.162021 1 1 3 4134.41 4426.76 o 4.159914 -4 1 2 37735.23 36565.56 o 4.133660 -2 1 3 7326.97 7080.20 o 4.127444 -2 0 4 4062.87 7173.55 o 4.061627 1 0 4 2441.22 3082.21 o 4.050241 5 1 0 15.83 20.26 o 4.033687 -5 1 1 237.97 263.68 o 3.984780 2 1 3 10589.61 9864.44 o 3.961640 4 1 2 5339.47 4994.36 o 3.915945 -3 1 3 675.21 631.57 o 3.915178 -6 0 2 30702.38 28287.67 o 3.906863 -3 0 4 598.46 657.05 o 3.870934 5 1 1 355.19 399.70 o 3.858773 2 0 4 45826.72 52601.20 o 3.854542 -5 1 2 1180.92 616.87 < 3.734246 3 1 3 1507.90 1422.40 o 3.707217 -4 1 3 5662.44 5627.32 o 3.654124 6 0 2 5966.23 4847.08 o 3.638216 -4 0 4 685.17 360.32 o 3.628016 7 0 0 1633.79 1318.21 o 3.618874 3 0 4 51121.71 41934.66 o 3.609148 6 1 0 13898.75 12138.52 o 3.566837 -6 1 1 12409.90 11097.49 o 3.542140 5 1 2 6759.32 5904.72 o 3.533926 -1 1 4 6391.10 5583.05 o 3.532945 0 1 4 148.86 124.92 o 3.530439 -2 1 4 8531.65 7799.85 o 3.468541 1 1 4 448.15 431.40 o 3.461441 6 1 1 111.19 134.48 o 3.435673 4 1 3 702.88 864.40 o 3.431502 -7 0 2 12139.42 14929.12 o 3.431232 -5 1 3 619.55 554.44 < 3.377483 -6 1 2 485.99 483.01 o 3.370657 -5 0 4 3384.44 3529.70 o 3.364769 -3 1 4 634.44 519.81 o 3.347503 4 0 4 928.76 929.72 o 3.345433 2 1 4 1082.65 1183.94 o 3.336885 0 2 0 23463.12 26172.08 o 3.333155 1 2 0 1350.24 845.72 < 3.304671 0 2 1 8.29 7.86 o 3.268294 -1 2 1 637.63 974.56 o 3.248569 1 2 1 4297.34 4849.72 o 3.234332 2 2 0 1495.32 1592.90 o 3.223410 7 0 2 30.76 26.62 o 3.216744 6 1 2 3021.50 3395.33 o 3.193562 -4 1 4 11754.13 12210.31 o 3.186656 7 1 0 24.50 22.88 o 3.180456 -2 2 1 285.63 256.18 o 3.177969 3 1 4 6478.35 5447.90 o 3.173848 -7 1 1 58.97 47.56 o 3.169544 8 0 0 95.21 80.40 o 3.166515 5 1 3 1932.90 1820.89 o 3.159070 2 2 1 5741.83 6138.52 o 3.151471 -6 1 3 120.86 88.46 o 3.107600 -6 0 4 4706.52 3578.42 o 3.103919 3 2 0 68.29 64.47 o 3.100353 0 2 2 3591.14 3821.51 o 3.094303 5 0 4 4070.94 3834.66 o 3.085375 -1 2 2 69.03 64.38 o 3.083658 7 1 1 466.68 402.28 o 3.080288 -3 2 1 12.39 15.30 o 3.065862 1 2 2 1878.52 1884.99 o 3.059432 -7 1 2 1257.38 1048.40 o 3.050823 -8 0 2 13865.80 11546.22 o 3.050307 3 2 1 350.01 520.34 o 3.030350 -2 2 2 2653.45 3740.50 o 3.028871 -5 1 4 0.93 0.75 o 3.003821 4 1 4 429.68 360.34 o 2.990040 -1 1 5 2.93 2.19 o 2.985785 2 2 2 10729.21 8180.03 o 2.983451 0 1 5 1827.96 1313.95 o 2.978732 -2 1 5 1244.31 909.34 o 2.951966 4 2 0 1817.67 1321.97 o 2.949573 -3 2 2 2649.16 2821.15 o 2.936626 1 1 5 399.11 360.13 o 2.931658 -4 2 1 1732.72 1563.82 o 2.925043 6 1 3 436.45 354.31 < 2.903755 7 1 2 1572.49 1687.32 o 2.897095 4 2 1 1061.60 637.91 o 2.884074 -3 1 5 2145.57 1455.30 o 2.881259 8 0 2 2833.24 2055.63 o 2.876545 3 2 2 3010.70 2174.17 o 2.875097 8 1 0 10548.05 10907.43 o 2.860239 -7 0 4 544.26 563.40 o 2.858523 0 2 3 21827.21 22490.21 o 2.857353 -8 1 1 3789.49 3904.60 o 2.857157 -7 1 3 1554.01 1602.70 o 2.856513 -1 2 3 17985.19 18538.53 o 2.853810 2 1 5 8430.57 8751.50 o 2.849975 6 0 4 5624.43 5203.63 o 2.841405 1 2 3 68.73 46.06 < 2.825102 -4 2 2 8.32 9.35 o 2.816837 -2 2 3 6504.57 7482.38 o 2.814868 9 0 0 1746.63 2009.19 o 2.814680 -6 1 4 11687.48 13648.08 o 2.813855 5 1 4 576.31 554.83 o 2.800016 -1 0 6 12790.27 11342.75 o 2.784882 5 2 0 462.33 410.00 o 2.784579 8 1 1 1130.69 1043.99 o 2.782212 -4 1 5 5466.69 5088.24 o 2.781255 0 0 6 9735.32 9901.96 o 2.774681 -8 1 2 4495.02 4536.61 o 2.773728 -5 2 1 1253.21 1256.87 o 2.768335 -2 0 6 2009.34 2388.33 o 2.761773 2 2 3 413.14 478.61 o 2.760541 4 2 2 162.41 159.21 o 2.744942 -3 2 3 1728.15 1693.56 o 2.744678 3 1 5 42.17 42.69 o 2.742056 -9 0 2 12999.83 13276.82 o 2.740685 1 0 6 695.53 643.00 o 2.732241 5 2 1 3275.83 2996.97 o 2.725030 -3 0 6 1364.11 271.20 < 2.707752 -5 2 2 3184.57 746.55 < 2.680093 7 1 3 1585.43 1208.58 o 2.671554 3 2 3 4014.59 3224.74 o 2.670047 2 0 6 5768.60 4947.34 o 2.661806 -5 1 5 11992.39 10231.89 o 2.661129 -4 2 3 795.17 672.22 o 2.650005 8 1 2 781.48 527.23 o 2.641149 -8 0 4 17684.95 16093.85 o 2.634459 -8 1 3 3170.72 3087.07 o 2.629079 -4 0 6 9526.53 9152.03 o 2.628032 -7 1 4 18.07 17.49 o 2.627178 7 0 4 5209.15 5835.52 o 2.618994 4 1 5 592.70 697.68 o 2.617146 6 2 0 6.26 7.41 o 2.616142 6 1 4 1130.98 1215.87 o 2.613871 -6 2 1 472.99 479.40 o 2.606350 5 2 2 1634.70 1931.02 o 2.603072 -1 2 4 64.72 76.46 o 2.602680 0 2 4 510.16 589.27 o 2.601677 9 0 2 5274.00 5895.20 o 2.597792 -9 1 1 440.39 489.73 o 2.594365 9 1 0 2813.48 3122.85 o 2.593020 -2 2 4 5230.74 3890.88 o 2.576606 1 2 4 846.37 946.57 o 2.573692 3 0 6 23276.41 31216.07 o 2.569694 -1 1 6 27.02 36.23 o 2.569666 6 2 1 14.41 20.27 o 2.563046 0 1 6 365.91 535.43 o 2.561646 4 2 3 89.67 130.42 o 2.561314 -2 1 6 58.72 59.75 < 2.551478 -5 2 3 747.00 401.45 o 2.538613 -6 2 2 760.39 394.56 o 2.535711 -9 1 2 217.06 113.81 o 2.534822 10 0 0 10428.52 5315.85 o 2.533212 9 1 1 4.04 1.96 o 2.531064 -6 1 5 211.73 100.41 o 2.529722 -5 0 6 56.08 26.88 o 2.529362 1 1 6 141.70 66.42 o 2.528137 -3 2 4 32.66 16.21 o 2.525809 2 2 4 962.49 811.61 o 2.521238 -3 1 6 2110.63 2398.97 o 2.508699 -10 0 2 461.26 498.93 < 2.485258 5 1 5 689.17 759.56 o 2.483661 2 1 6 63.39 84.88 o 2.472028 8 1 3 49.26 37.40 o 2.463773 4 0 6 4656.02 3519.33 o 2.462911 6 2 2 10465.55 7721.21 o 2.457680 -4 2 4 104.20 82.91 o 2.454529 7 2 0 283.08 269.18 o 2.451692 -8 1 4 4.20 4.10 o 2.450076 3 2 4 3440.61 3388.95 o 2.448661 -7 2 1 28.04 28.08 o 2.446683 -4 1 6 559.66 597.71 o 2.444904 5 2 3 577.42 558.28 o 2.441856 7 1 4 6636.38 5778.50 o 2.437622 -9 0 4 8546.17 8129.46 o 2.433214 -9 1 3 1645.42 1529.60 o 2.425983 9 1 2 1012.75 968.58 o 2.420499 8 0 4 3142.58 3016.76 o 2.419401 -6 0 6 283.47 277.60 o 2.418677 -6 2 3 514.38 514.32 o 2.417850 7 2 1 4196.17 4663.41 o 2.404919 3 1 6 989.03 1723.86 o 2.397722 -7 1 5 359.90 466.84 o 2.394357 -7 2 2 91.05 105.77 o 2.390818 -10 1 1 383.10 337.59 o 2.371811 10 1 0 1571.92 1696.39 o 2.368003 -5 2 4 881.17 950.94 o 2.367994 10 0 2 134.21 111.37 o 2.366079 -5 1 6 377.88 191.92 o 2.364858 4 2 4 5772.60 2990.19 o 2.361225 -1 2 5 465.90 232.74 o 2.359128 0 2 5 591.09 400.98 o 2.355644 6 1 5 2374.34 2383.67 o 2.348274 5 0 6 9437.35 9557.42 o 2.347986 -2 2 5 2726.05 2328.71 o 2.342340 1 2 5 306.36 264.70 o 2.332155 -10 1 2 2039.02 2302.59 o 2.328693 6 2 3 56.73 68.00 < 2.318034 10 1 1 0.25 0.30 < 2.317930 7 2 2 1.08 0.51 < 2.314642 4 1 6 249.71 47.47 < 2.310279 -3 2 5 379.47 208.85 o 2.306541 11 0 0 524.97 334.46 o 2.302920 -7 0 6 5440.37 3460.67 o 2.302106 8 2 0 498.80 334.39 o 2.295715 -8 2 1 262.56 168.34 o 2.294121 -7 2 3 3658.65 2345.81 o 2.293788 2 2 5 935.63 611.73 o 2.290398 -9 1 4 94.72 50.55 < 2.285714 9 1 3 2939.47 658.44 < 2.279298 8 1 4 2639.55 1070.30 o 2.274253 -6 1 6 15.63 6.50 o 2.273652 -11 0 2 1619.16 799.98 o 2.271598 -6 2 4 1317.68 651.03 o 2.271523 5 2 4 15.69 5.53 o 2.264225 -8 1 5 655.69 392.37 o 2.260413 8 2 1 349.50 479.49 o 2.254779 -4 2 5 39.66 56.38 o 2.254270 -10 0 4 2492.73 3543.37 o 2.253946 -8 2 2 2212.12 2046.83 o 2.250256 -1 1 7 1070.45 848.58 o 2.247738 -10 1 3 2137.14 1563.90 o 2.245824 9 0 4 2825.96 2070.69 o 2.241671 0 1 7 979.72 716.53 o 2.240011 -2 1 7 1808.99 1367.14 o 2.237874 3 2 5 2531.20 1668.12 o 2.233245 6 0 6 52.06 34.29 o 2.230289 10 1 2 444.62 296.39 o 2.229794 7 1 5 74.38 75.53 o 2.215711 1 1 7 45.00 46.02 o 2.215227 5 1 6 10156.54 10559.90 o 2.214631 1 3 0 261.79 275.50 o 2.213603 -3 1 7 1095.48 1245.10 o 2.211097 0 3 1 78.90 51.79 < 2.202570 -1 3 1 607.43 478.99 o 2.196503 7 2 3 57.95 51.73 o 2.194660 1 3 1 725.55 886.93 o 2.192086 -5 2 5 3209.91 3895.53 o 2.188870 2 3 0 496.32 602.33 o 2.188676 -8 0 6 8645.86 8420.84 o 2.184485 -11 1 1 385.65 319.80 o 2.181820 8 2 2 5155.89 4795.30 o 2.177710 11 1 0 2576.79 2385.87 o 2.176696 -7 1 6 119.88 108.38 o 2.176009 2 1 7 30.11 27.67 o 2.175034 -2 3 1 278.27 251.40 o 2.174288 -8 2 3 975.14 897.11 o 2.170929 11 0 2 24566.34 22600.62 o 2.170912 -7 2 4 43.23 39.82 o 2.169859 -4 1 7 3258.49 3015.93 o 2.169178 2 3 1 1014.81 932.63 o 2.165745 4 2 5 1529.24 1369.27 o 2.164197 6 2 4 1.33 1.17 o 2.162343 -9 2 1 362.05 275.69 o 2.151262 9 2 0 8834.02 6834.06 o 2.150495 -11 1 2 132.86 102.54 o 2.150190 3 3 0 1313.08 1044.98 o 2.148940 0 3 2 1365.19 1191.12 o 2.146922 -1 3 2 84.34 92.76 o 2.143358 -3 3 1 1263.24 1305.26 o 2.137355 -1 2 6 1045.07 1097.18 o 2.137117 11 1 1 1603.17 1647.65 o 2.135575 -10 1 4 117.69 123.86 o 2.135201 1 3 2 179.10 188.50 o 2.135172 0 2 6 4.01 5.16 o 2.132496 -9 1 5 227.09 289.19 o 2.131444 -2 2 6 305.38 577.05 o 2.126620 3 3 1 1766.21 2038.43 o 2.125214 9 1 4 67.40 77.62 o 2.124757 -2 3 2 15.93 18.34 o 2.124704 3 1 7 6612.82 6707.23 o 2.121905 -9 2 2 998.44 974.46 o 2.116947 10 1 3 91.76 91.58 o 2.115969 6 1 6 29.70 29.70 o 2.115057 9 2 1 16594.96 16595.10 o 2.114756 -5 1 7 35.92 36.15 o 2.114663 -6 2 5 9.71 9.93 o 2.113973 7 0 6 802.81 819.22 o 2.113810 1 2 6 1440.10 1481.73 o 2.113048 12 0 0 11.86 13.54 o 2.111010 2 3 2 402.44 569.18 o 2.108845 -3 2 6 2994.90 3349.89 o 2.101659 4 3 0 1631.22 1474.56 o 2.096778 -11 0 4 1472.22 1264.79 o 2.094764 -3 3 2 264.89 198.65 < 2.092111 -12 0 2 34.03 28.55 o 2.090615 -1 0 8 463.82 376.96 o 2.089105 8 1 5 0.09 0.07 o 2.088976 -4 3 1 148.72 122.13 o 2.087911 5 2 5 2539.34 2000.44 o 2.086872 -11 1 3 4248.49 3377.16 o 2.086338 10 0 4 2621.33 2213.91 o 2.083869 -2 0 8 1528.95 1350.09 o 2.083064 0 0 8 890.79 840.32 o 2.081011 2 2 6 1731.88 1824.60 o 2.079957 -8 1 6 1152.10 1466.65 o 2.075872 8 2 3 2817.03 3890.01 o 2.075032 4 3 1 1613.02 1651.33 o 2.072856 3 3 2 1265.16 1098.27 o 2.069516 -9 0 6 1746.12 1553.36 o 2.069279 -8 2 4 78.08 68.79 o 2.066830 11 1 2 64.84 52.89 o 2.064214 -4 2 6 2749.33 2176.63 o 2.063722 -3 0 8 289.98 237.08 o 2.063251 0 3 3 1519.11 1189.38 o 2.062869 -1 3 3 70.25 51.21 o 2.061534 7 2 4 42.98 30.22 o 2.059337 1 0 8 1720.02 1209.55 o 2.059266 4 1 7 5765.55 4279.16 o 2.058754 -9 2 3 190.18 161.03 o 2.052305 1 3 3 214.33 185.92 o 2.050634 -6 1 7 15.24 13.22 o 2.050494 9 2 2 30.35 27.17 o 2.048981 -4 3 2 207.21 166.16 o 2.047467 -2 3 3 3643.98 2970.92 o 2.046710 3 2 6 2464.64 2977.51 o 2.035110 5 3 0 660.09 797.45 o 2.034978 -7 2 5 30.92 38.20 o 2.033051 -4 0 8 65.08 65.49 o 2.030814 -5 3 1 392.32 279.78 o 2.028612 2 3 3 3460.00 2667.26 o 2.025539 2 0 8 1971.78 1520.01 o 2.025120 4 3 2 686.52 591.50 o 2.019352 -3 3 3 1255.73 1081.93 o 2.019247 -10 2 1 1508.25 1299.49 o 2.019195 -12 1 1 189.67 167.53 o 2.018278 10 2 0 4483.31 3778.53 o 2.016843 7 1 6 163.44 134.01 o 2.014940 -5 2 6 2883.63 2399.32 o 2.014899 12 1 0 1381.70 1151.68 o 2.012514 5 3 1 509.86 419.21 o 2.011385 -10 1 5 1562.52 1303.45 o 2.009530 6 2 5 2.20 1.18 < 2.004612 12 0 2 5263.56 2829.54 < 2.004564 8 0 6 1658.31 815.65 o 2.001253 -11 1 4 3131.43 1875.04 o 1.998422 -12 1 2 3764.11 3183.45 o 1.994819 -1 1 8 4040.13 3468.21 o 1.993507 -5 3 2 29.99 26.36 o 1.993109 -10 2 2 1291.02 1154.77 o 1.992390 10 1 4 1102.31 1038.28 o 1.988956 3 3 3 1575.21 1483.71 o 1.988967 5 1 7 1435.45 1375.65 o 1.988558 -2 1 8 2122.03 2000.54 o 1.988256 -5 0 8 386.32 361.02 o 1.987511 0 1 8 1589.75 1523.86 o 1.986471 10 2 1 1385.38 1292.88 o 1.985636 4 2 6 1195.53 1159.66 o 1.980820 -4 3 3 955.44 926.77 o 1.980641 3 0 8 1736.79 1671.29 o 1.980404 -7 1 7 125.80 119.52 o 1.979631 12 1 1 2573.10 2375.08 o 1.978260 -9 1 6 761.46 814.41 o 1.976259 11 1 3 15.61 12.10 o 1.971323 -3 1 8 9889.18 7667.67 o 1.971005 9 1 5 472.40 365.21 o 1.969747 1 1 8 339.86 306.10 o 1.967530 6 3 0 303.80 298.39 o 1.966382 -9 2 4 875.84 906.45 o 1.965272 -6 3 1 1660.06 1424.28 o 1.962214 9 2 3 27.19 22.92 o 1.961189 5 3 2 1783.59 1503.20 o 1.960814 -1 3 4 916.23 782.77 o 1.960646 0 3 4 118.91 103.12 o 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< 1.567256 3 2 9 443.19 371.63 < 1.566382 -7 0 10 268.22 227.36 < 1.565752 14 1 4 738.57 349.16 < 1.563509 8 3 5 13.18 5.84 < 1.563309 -5 4 2 185.30 82.86 < 1.563171 9 1 8 499.31 250.28 < 1.562235 -11 3 3 57.27 27.00 < 1.562202 3 1 10 1139.84 537.35 < 1.561981 3 4 3 823.68 319.39 < 1.561170 -14 2 3 168.35 65.28 < 1.561060 -8 3 6 68.47 21.29 < 1.557794 -4 4 3 2.50 1.04 < 1.557134 -12 2 6 144.80 77.16 < 1.553800 -6 1 10 34.93 15.80 < 1.553566 11 3 2 0.47 0.26 < 1.552849 -12 0 8 566.56 335.22 < 1.551960 -6 2 9 355.60 254.15 < 1.550831 4 3 7 471.19 316.80 < 1.550521 6 4 0 271.57 226.26 < 1.550177 -13 2 5 93.85 69.76 < 1.549698 -9 2 8 18.47 12.05 < 1.548480 -6 4 1 88.80 60.36 < 1.548132 7 1 9 180.26 130.18 < 1.547745 5 4 2 93.33 70.09 < 1.547444 -1 4 4 860.55 646.32 < 1.547362 0 4 4 2149.02 1675.87 < 1.547151 -6 3 7 816.45 636.69 < 1.546983 -16 1 1 15.31 12.58 < 1.546069 9 2 7 2.79 2.86 o 1.544205 11 1 7 111.10 117.31 o 1.542958 10 0 8 634.28 676.18 o 1.542687 -2 4 4 613.10 612.78 o 1.541829 5 0 10 7354.33 7350.47 o 1.541817 7 2 8 664.99 664.64 o 1.541765 1 4 4 7.49 6.93 o 1.541204 16 1 0 9.47 7.99 o 1.540409 14 2 2 207.07 155.00 o 1.540144 4 2 9 608.20 435.18 o 1.538930 6 4 1 241.94 173.12 o 1.538909 4 4 3 1467.40 1010.30 o 1.538534 -16 1 2 1214.14 835.94 o 1.538483 -14 1 6 1930.32 1285.72 o 1.538081 -11 2 7 49.68 32.57 o 1.537238 15 1 3 0.02 0.01 < 1.534999 -13 1 7 371.72 210.08 < 1.534630 4 1 10 50.75 29.71 < 1.534001 -5 4 3 31.94 19.33 < 1.533572 -12 3 1 106.95 74.93 < 1.533007 -6 4 2 1071.76 750.92 < 1.532931 13 0 6 1485.92 959.93 < 1.532396 7 3 6 5.95 4.36 o 1.531543 16 0 2 1614.46 1261.22 o 1.530801 -3 4 4 39.49 32.08 o 1.530735 12 3 0 662.06 547.61 o 1.530477 -8 0 10 4200.99 3600.09 o 1.530164 2 4 4 401.57 340.75 o 1.529716 -10 3 5 235.61 200.38 o 1.529163 12 2 5 39.70 34.35 < 1.525535 -14 2 4 523.21 466.58 < 1.525411 -16 0 4 28.15 24.55 < 1.525154 -7 1 10 8.64 8.27 o 1.524272 -11 3 4 135.49 129.60 o 1.524252 -12 3 2 1084.50 1190.17 o 1.522651 -1 3 8 824.45 742.75 o 1.522068 16 1 1 694.11 625.33 o 1.521929 -15 1 5 178.69 155.64 o 1.521497 -7 2 9 375.11 306.91 o 1.520953 10 3 4 912.80 748.97 o 1.520039 13 2 4 1220.55 985.34 o 1.519989 5 3 7 240.07 193.80 o 1.519861 -10 1 9 3428.06 2779.93 o 1.519757 -2 3 8 1674.59 1357.98 o 1.519727 15 0 4 498.35 387.44 o 1.518936 0 3 8 25.44 19.78 o 1.518929 -16 1 3 74.23 50.10 o 1.518222 -7 3 7 5.29 3.49 o 1.515865 12 3 1 3.50 2.39 o 1.515248 6 4 2 291.85 199.21 o 1.515175 -4 4 4 89.70 66.69 o 1.514436 11 2 6 1805.32 1377.57 o 1.514377 -9 3 6 1852.05 1413.23 o 1.514349 7 4 0 1079.23 947.90 o 1.513769 3 4 4 0.52 0.46 o 1.513054 -7 4 1 550.38 572.91 o 1.512587 11 3 3 1319.75 1378.00 o 1.512125 -3 3 8 1208.17 1249.01 o 1.511981 -12 1 8 1122.55 1163.50 o 1.511538 5 4 3 284.79 297.00 o 1.511445 9 3 5 50.68 52.85 o 1.511413 -15 2 1 130.85 130.11 o 1.511047 1 3 8 3.56 3.39 o 1.510411 5 2 9 554.22 323.45 < 1.507505 15 2 0 683.11 338.06 < 1.506475 -6 4 3 326.40 205.87 < 1.505700 6 0 10 219.27 150.90 < 1.504168 -15 2 2 510.42 340.80 < 1.503252 10 1 8 18.21 12.74 < 1.502968 -15 0 6 2356.88 1714.88 < 1.502631 7 4 1 969.47 695.38 < 1.502561 5 1 10 197.30 143.28 < 1.502163 -10 2 8 88.27 64.18 < 1.501910 -12 3 3 133.92 97.72 < 1.500170 8 1 9 24.93 17.19 < 1.499765 -7 4 2 44.44 35.24 < 1.499104 -4 3 8 0.37 0.30 < 1.499076 14 2 3 130.42 76.84 < 1.498272 2 3 8 968.13 471.81 < 1.496781 14 1 5 225.46 107.29 < 1.495044 8 2 8 566.29 269.49 < 1.495020 -1 2 10 179.24 128.64 < 1.493716 13 1 6 248.12 164.89 < 1.493446 -5 4 4 0.50 0.33 < 1.493428 -2 2 10 21.59 17.05 < 1.492892 16 1 2 229.50 195.92 < 1.491970 4 4 4 4.36 3.76 < 1.491726 -9 0 10 3917.99 3112.72 < 1.491697 -8 1 10 20.52 17.12 < 1.491380 -1 4 5 49.22 42.50 < 1.491196 0 4 5 2.20 1.68 < 1.490315 17 0 0 196.72 138.20 < 1.490125 15 2 1 930.63 618.63 < 1.489867 -17 0 2 908.13 629.95 < 1.489762 -13 2 6 51.36 38.55 < 1.489637 -13 0 8 381.15 262.28 < 1.489395 0 2 10 0.63 0.43 < 1.489366 12 3 2 323.69 171.31 < 1.488424 10 2 7 3.57 1.86 < 1.487579 -8 2 9 1.41 0.74 < 1.487582 8 3 6 2.56 1.38 < 1.487067 -2 4 5 619.77 334.93 < 1.486929 -3 2 10 9.25 5.00 < 1.486920 -16 1 4 3540.10 1933.79 < 1.486740 6 3 7 671.42 411.37 < 1.485813 1 4 5 2.78 2.41 < 1.484313 -15 2 3 532.98 566.09 < 1.483651 -8 3 7 22.81 20.52 < 1.481459 -5 3 8 23.87 20.53 < 1.481403 15 1 4 9.86 8.08 < 1.480978 -1 1 11 922.76 732.65 < 1.480815 -12 2 7 1067.90 855.58 < 1.480729 -2 1 11 3.01 2.41 < 1.480690 6 4 3 207.92 166.58 < 1.480653 11 0 8 523.65 397.00 < 1.480454 -14 2 5 128.54 93.72 < 1.480256 1 2 10 937.75 656.22 < 1.479976 7 4 2 997.30 675.10 < 1.479768 3 3 8 20.82 15.04 < 1.478453 -3 4 5 40.77 25.53 < 1.477645 -11 3 5 38.71 24.86 < 1.477170 12 1 7 55.51 31.11 < 1.476333 -4 2 10 1296.14 775.61 < 1.475983 0 1 11 18.84 11.28 < 1.475904 -3 1 11 33.12 21.84 < 1.475534 8 4 0 594.71 357.71 < 1.474787 -8 4 1 470.31 278.24 < 1.474364 -7 4 3 13.16 7.79 < 1.474275 2 4 5 397.27 199.00 < 1.473374 6 2 9 86.80 54.05 < 1.472925 -11 1 9 105.60 98.68 < 1.471342 -10 3 6 35.72 34.51 < 1.469378 -14 1 7 751.27 768.16 < 1.468429 -6 4 4 266.47 238.43 < 1.468313 -13 3 1 705.39 620.53 < 1.467969 6 1 10 81.97 64.46 < 1.467280 -12 3 4 5.50 4.33 < 1.467128 5 4 4 325.52 247.86 < 1.466336 1 1 11 162.82 128.24 < 1.466106 -15 1 6 118.52 86.05 < 1.465853 2 2 10 216.37 157.10 < 1.465829 -4 1 11 19.79 15.43 < 1.465502 13 3 0 292.25 252.59 < 1.465089 7 0 10 1173.41 1036.43 < 1.464232 8 4 1 183.10 172.70 < 1.463761 -4 4 5 349.49 329.64 < 1.463622 11 3 4 232.81 219.18 < 1.463014 -8 4 2 8.90 8.24 < 1.462522 15 2 2 97.51 109.08 < 1.462381 -5 2 10 16.29 16.44 < 1.460406 -17 1 1 7.76 6.67 < 1.459646 -13 3 2 1723.90 1481.66 < 1.459517 10 3 5 224.44 192.90 < 1.459495 -6 3 8 679.25 583.80 < 1.459472 14 0 6 862.50 741.17 < 1.457976 3 4 5 987.55 959.47 < 1.457821 13 2 5 553.86 506.59 < 1.457505 4 3 8 247.13 248.78 o 1.455948 -9 1 10 0.69 0.72 o 1.455698 -11 2 8 875.00 768.26 o 1.454486 17 1 0 1189.58 1065.28 o 1.454236 -17 1 2 3150.54 2695.00 o 1.453899 -15 2 4 163.01 142.61 o 1.453588 -13 1 8 439.58 351.11 o 1.453558 16 1 3 618.42 492.54 o 1.452528 12 2 6 64.79 52.01 o 1.451877 12 3 3 1073.06 861.37 o 1.451807 2 1 11 683.71 550.12 o 1.451709 -9 2 9 309.77 237.96 o 1.451525 9 1 9 931.48 689.96 o 1.451201 -10 0 10 1024.80 759.08 o 1.451206 13 3 1 49.39 39.09 o 1.451074 -5 1 11 1662.61 1287.17 o 1.450888 7 3 7 927.69 884.99 o 1.449189 14 2 4 326.60 359.94 o 1.448548 9 2 8 778.19 801.33 < 1.447534 3 2 10 85.14 82.59 < 1.447332 7 4 3 51.09 46.77 < 1.446926 -16 1 5 126.51 125.88 < 1.446102 -5 4 5 1317.29 1221.78 < 1.445263 11 1 8 1468.95 1362.44 < 1.445244 17 0 2 44.66 40.03 < 1.444882 -9 3 7 1113.92 898.91 < 1.444574 -17 0 4 0.09 0.07 < 1.443890 8 4 2 74.49 62.54 < 1.442037 9 3 6 709.71 630.11 < 1.441562 -6 2 10 249.98 205.68 < 1.440629 -13 3 3 605.95 567.88 < 1.440307 -8 4 3 536.79 496.80 < 1.440063 -7 4 4 92.90 83.85 < 1.439750 16 0 4 319.53 294.80 < 1.438272 4 4 5 195.33 180.21 < 1.438093 17 1 1 692.05 615.83 < 1.438035 6 4 4 302.49 322.65 < 1.437548 -17 1 3 14.85 15.46 < 1.437383 7 2 9 88.33 55.30 < 1.435984 -16 2 1 267.70 148.17 < 1.434646 -9 4 1 696.99 384.83 < 1.434278 9 4 0 1920.73 1069.10 < 1.434051 -7 3 8 4146.76 2337.78 < 1.433871 3 1 11 145.58 83.65 < 1.433119 11 2 7 0.16 0.09 < 1.432159 -6 1 11 30.77 16.63 < 1.432104 -16 0 6 373.50 229.48 < 1.430486 7 1 10 1491.94 933.95 < 1.430140 16 2 0 1357.67 849.89 < 1.430119 -1 4 6 37.19 23.61 < 1.430063 5 3 8 15.73 9.89 < 1.429863 -14 0 8 261.18 155.59 < 1.429261 0 4 6 255.40 159.29 < 1.428676 -16 2 2 62.51 38.99 < 1.428578 -14 2 6 97.58 55.64 < 1.428257 -2 4 6 89.64 66.31 < 1.426905 13 3 2 1434.75 1061.38 < 1.426856 15 2 3 399.47 263.16 < 1.425788 -12 3 5 273.29 183.68 < 1.425608 -13 2 7 98.72 63.64 < 1.425491 4 2 10 6.17 4.81 < 1.424988 -1 3 9 563.24 471.50 < 1.424841 14 1 6 14.82 11.96 < 1.424310 -9 4 2 34.77 30.42 < 1.423972 -11 3 6 460.32 403.66 < 1.423672 -2 3 9 94.46 80.31 < 1.423523 9 4 1 200.97 158.81 < 1.423305 -6 4 5 380.23 310.11 < 1.423066 8 0 10 23.40 18.38 < 1.422807 1 4 6 629.19 494.28 < 1.422784 -12 1 9 80.72 63.41 < 1.422768 15 1 5 11.78 8.98 < 1.421801 0 3 9 27.73 20.37 < 1.421664 12 0 8 2.49 1.47 < 1.420702 -3 4 6 590.96 402.17 < 1.419292 -10 1 10 28.21 20.57 < 1.417996 -3 3 9 512.40 461.49 < 1.417746 -7 2 10 302.67 275.00 < 1.417179 16 2 1 27.66 24.93 < 1.415295 -15 2 5 69.92 64.77 < 1.414948 5 4 5 1145.43 1043.04 < 1.414711 1 3 9 1462.31 1329.36 < 1.414081 -10 2 9 330.09 282.69 < 1.413548 13 1 7 899.71 809.50 < 1.413235 2 4 6 865.51 831.34 < 1.412551 -16 2 3 42.94 42.44 < 1.412312 17 1 2 28.78 28.11 < 1.412094 -13 3 4 222.82 191.10 < 1.411577 -17 1 4 1134.04 1012.40 < 1.411168 8 4 3 120.38 104.78 < 1.411006 4 1 11 93.63 82.71 < 1.410829 8 3 7 1.69 1.52 < 1.410751 -7 1 11 279.03 259.13 < 1.409646 -11 0 10 1401.98 1429.99 < 1.409460 -8 4 4 538.09 563.83 < 1.408418 11 3 5 5.50 4.71 < 1.408212 -18 0 2 2.41 2.06 < 1.408200 -4 3 9 77.12 70.79 < 1.407673 12 3 4 496.33 455.59 < 1.407594 -4 4 6 5.09 5.13 < 1.407434 18 0 0 119.29 117.89 < 1.407340 -12 2 8 53.83 54.03 < 1.406927 -14 3 1 23.92 21.73 < 1.406209 7 4 4 0.76 0.68 < 1.406041 -10 3 7 777.45 687.13 < 1.405962 16 1 4 747.44 660.61 < 1.405922 -15 1 7 70.22 60.24 < 1.405767 -8 3 8 86.99 67.63 < 1.405227 -9 4 3 18.05 12.33 < 1.403796 14 3 0 78.77 38.75 < 1.403099 10 1 9 100.54 45.31 < 1.402747 9 4 2 3.10 1.40 < 1.402731 2 3 9 962.05 463.22 < 1.402302 6 3 8 93.96 63.51 < 1.400828 10 2 8 248.65 158.52 < 1.400008 5 2 10 2.38 1.91 < 1.399357 -14 3 2 2.13 1.71 < 1.399347 -16 1 6 308.02 244.53 < 1.398647 3 4 6 13.71 10.22 < 1.398256 -7 4 5 2.71 1.82 < 1.397588 -14 1 8 1095.90 875.48 < 1.397502 8 2 9 11.25 9.60 < 1.397418 10 3 6 787.17 781.47 < 1.395738 13 3 3 257.03 317.60 < 1.393935 14 2 5 228.91 283.11 < 1.393597 -5 3 9 27.41 33.90 < 1.393574 -10 4 1 68.39 78.23 < 1.393062 -2 0 12 1090.04 1154.33 < 1.392441 13 2 6 731.52 774.66 < 1.392302 10 4 0 172.62 182.80 < 1.392290 -1 0 12 7.96 8.05 < 1.391980 -5 4 6 21.17 23.42 < 1.391649 8 1 10 196.55 219.61 < 1.391467 16 2 2 1250.99 1211.10 < 1.391106 -8 2 10 19.46 17.48 < 1.390628 14 3 1 69.39 58.66 < 1.390213 12 1 8 1.47 1.30 < 1.389498 15 0 6 2212.36 1885.06 < 1.389246 -3 0 12 594.79 537.22 < 1.388710 6 4 5 183.86 157.03 < 1.388247 0 0 12 989.19 736.53 < 1.387340 -16 2 4 121.32 89.52 < 1.386864 3 3 9 0.83 0.61 < 1.386638 5 1 11 1770.42 1048.96 < 1.385386 -10 4 2 508.26 281.40 < 1.384168 -8 1 11 39.10 18.69 < 1.384062 -14 3 3 68.21 44.76 < 1.382942 15 2 4 451.51 261.31 < 1.382184 -18 1 1 78.17 45.24 < 1.382131 -1 2 11 77.70 44.97 < 1.382051 -2 2 11 518.74 315.25 < 1.381949 10 4 1 230.33 139.98 < 1.381897 -4 0 12 2340.51 1817.91 < 1.380886 9 0 10 716.65 611.18 < 1.380591 4 4 6 87.29 64.13 < 1.380271 -11 1 10 6.32 3.32 < 1.378975 1 0 12 175.07 89.58 < 1.378645 12 2 7 4072.54 2210.21 < 1.378405 0 2 11 76.40 42.57 < 1.378056 17 1 3 5.10 2.88 < 1.377969 -12 3 6 21.42 12.12 < 1.377887 -18 1 2 1173.47 663.85 < 1.377795 -3 2 11 39.58 21.70 < 1.377755 18 1 0 1254.27 650.61 < 1.376989 -17 1 5 334.95 162.15 < 1.376823 -6 3 9 486.18 237.58 < 1.375815 -13 3 5 421.47 211.06 < 1.375024 -9 4 4 42.54 21.30 < 1.374978 -13 1 9 1.74 0.92 < 1.374642 -11 2 9 1041.93 525.52 < 1.374340 -9 3 8 871.64 447.02 < 1.374173 9 4 3 1598.48 836.68 < 1.373578 8 4 4 0.23 0.15 < 1.372471 -6 4 6 1552.93 966.02 < 1.372339 -14 2 7 232.97 143.30 < 1.371965 -15 0 8 514.66 300.60 < 1.371829 9 3 7 6.33 3.80 < 1.371182 6 2 10 1488.90 876.75 < 1.371028 -18 0 4 233.02 128.50 < 1.370343 1 2 11 295.97 158.40 < 1.370070 -15 2 6 172.36 98.51 < 1.369864 -4 2 11 365.88 181.19 < 1.369577 7 3 8 13.10 6.49 < 1.369473 -8 4 5 654.98 332.75 < 1.369412 -5 0 12 2880.45 1613.26 < 1.369177 14 3 2 30.84 13.62 < 1.368337 18 0 2 499.87 230.76 < 1.367969 4 3 9 251.48 113.32 < 1.367485 -12 0 10 446.78 213.84 < 1.367121 -1 4 7 42.65 20.87 < 1.366578 -11 3 7 167.12 80.72 < 1.366298 -10 4 3 802.78 399.69 < 1.366148 2 0 12 575.97 295.26 < 1.366121 17 0 4 903.27 478.04 < 1.365248 0 4 7 58.03 28.74 < 1.364836 -17 2 1 3.93 1.86 < 1.364794 -2 4 7 95.85 50.22 < 1.364352 -18 1 3 120.47 56.44 < 1.364246 -17 0 6 1380.00 726.45 < 1.363854 13 0 8 409.23 251.15 < 1.363678 -2 1 12 317.53 256.38 < 1.363024 18 1 1 0.03 0.02 < 1.362682 -1 1 12 51.26 40.88 < 1.362592 10 4 2 110.32 87.46 < 1.362515 -9 2 10 163.84 125.38 < 1.361565 17 2 0 48.23 46.39 < 1.360369 -17 2 2 31.75 34.85 < 1.360093 15 1 6 241.69 263.70 < 1.360027 -13 2 8 35.77 34.00 < 1.359813 -3 1 12 75.53 73.04 < 1.359524 7 4 5 70.46 70.98 < 1.359283 1 4 7 1069.05 1076.94 < 1.359171 5 4 6 150.46 153.05 < 1.359033 16 2 3 8.98 9.13 < 1.358970 2 2 11 122.80 141.20 < 1.358299 0 1 12 302.64 351.29 < 1.358239 -3 4 7 18.48 21.45 < 1.358216 12 3 5 345.74 407.42 < 1.358061 -14 3 4 3.24 3.65 < 1.357974 9 2 9 1197.89 1321.95 < 1.357883 -5 2 11 6.72 7.60 < 1.357627 6 1 11 624.42 695.72 < 1.357358 -9 1 11 274.12 273.70 < 1.355921 11 1 9 139.25 145.42 < 1.354950 -7 3 9 259.17 252.80 < 1.354825 16 1 5 1.91 1.59 < 1.354477 13 3 4 404.46 296.90 < 1.354144 -6 0 12 2498.45 1724.99 < 1.353876 14 1 7 40.48 24.74 < 1.353710 -16 2 5 248.93 152.16 < 1.353703 11 2 8 50.02 38.49 < 1.352999 -4 1 12 1166.28 784.95 < 1.352181 9 1 10 1159.96 792.48 < 1.351904 -11 4 1 1005.69 705.46 < 1.351345 11 3 6 583.76 453.88 < 1.350171 11 4 0 78.39 60.95 < 1.350125 3 0 12 225.52 175.35 < 1.350080 1 1 12 1303.41 1013.42 < 1.350076 -7 4 6 43.74 36.62 < 1.349961 2 4 7 99.97 92.60 < 1.349728 -4 4 7 0.38 0.41 < 1.348325 -15 3 1 468.83 436.28 < 1.347810 17 2 1 129.03 113.83 < 1.347079 -16 1 7 2.19 1.86 < 1.346677 -17 2 3 279.35 243.83 < 1.346543 5 3 9 1358.80 1360.14 < 1.345294 15 3 0 86.38 72.37 < 1.344562 -11 4 2 2.08 1.96 < 1.343728 -15 1 8 96.68 90.74 < 1.343673 3 2 11 86.27 71.80 < 1.343036 -18 1 4 329.69 224.59 < 1.342276 -15 3 2 214.99 146.46 < 1.342269 -6 2 11 262.57 182.45 < 1.342200 -10 3 8 271.31 174.08 < 1.341314 -5 1 12 1193.73 761.13 < 1.341181 7 2 10 5.11 3.39 < 1.340582 11 4 1 870.66 600.20 < 1.340139 18 1 2 378.83 265.73 < 1.340045 -10 4 4 830.83 582.79 < 1.340046 -12 1 10 1051.11 805.69 < 1.339249 -9 4 5 685.37 507.21 < 1.339116 14 3 3 103.21 84.00 < 1.338720 2 1 12 155.31 128.36 < 1.338308 10 0 10 1.08 0.89 < 1.338173 17 1 4 23.70 20.41 < 1.337487 9 4 4 388.90 334.87 < 1.337453 3 4 7 1562.26 1405.50 < 1.336741 8 3 8 4.35 3.83 < 1.336399 -17 1 6 12.13 10.81 < 1.336177 13 1 8 152.46 136.78 < 1.336011 14 2 6 112.99 100.06 < 1.335777 -1 3 10 9.16 7.88 < 1.335467 -7 0 12 2342.84 2015.16 < 1.335351 10 4 3 595.21 529.63 < 1.335253 6 4 6 329.45 294.54 < 1.335024 -19 0 2 871.17 778.84 < 1.334994 -5 4 7 27.61 24.68 < 1.334925 -2 3 10 11.54 10.01 < 1.334878 -12 2 9 12.75 10.49 < 1.334505 15 2 5 170.96 128.81 < 1.333707 19 0 0 888.82 590.28 < 1.333269 15 3 1 143.57 97.00 < 1.332715 -13 3 6 354.73 251.21 < 1.332550 0 3 10 35.81 24.96 < 1.332356 1 5 0 1.03 0.72 < 1.331419 10 3 7 75.08 57.76 < 1.331076 -8 3 9 14.93 11.48 < 1.331078 4 0 12 776.61 612.60 < 1.330903 -3 3 10 219.66 186.29 < 1.330604 -10 2 10 17.26 14.64 < 1.330564 0 5 1 212.03 165.26 < 1.329007 8 4 5 86.71 60.54 < 1.328391 -15 3 3 201.53 140.70 < 1.328260 -11 4 3 822.22 590.90 < 1.327712 -1 5 1 1907.36 1370.75 < 1.327671 -14 1 9 359.69 266.65 < 1.327431 7 1 11 246.96 194.80 o 1.327305 -6 1 12 279.68 202.05 o 1.326790 1 5 1 350.65 271.70 o 1.326693 13 2 7 781.57 605.59 o 1.326629 -12 3 7 1982.94 1426.67 o 1.326162 2 5 0 871.16 601.87 o 1.325936 -14 3 5 298.58 207.02 o 1.325822 -10 1 11 85.48 59.27 o 1.325783 16 0 6 985.13 683.05 o 1.325754 17 2 2 2.38 1.65 o 1.325685 1 3 10 33.69 22.23 o 1.325621 -8 4 6 690.07 497.20 o 1.325003 -17 2 4 5406.37 3797.72 o 1.324919 -13 0 10 828.06 598.04 o 1.324745 4 2 11 432.16 312.11 o 1.324638 -7 2 11 40.22 26.50 < 1.323659 3 1 12 636.41 390.67 < 1.323217 -4 3 10 226.75 130.11 < 1.322749 -2 5 1 13.99 8.03 < 1.322717 11 4 2 43.10 26.82 < 1.321956 2 5 1 383.39 207.77 < 1.320787 16 2 4 169.30 99.55 < 1.320574 6 3 9 26.95 16.45 < 1.320547 4 4 7 1351.05 824.50 < 1.320519 -15 2 7 18.65 11.38 < 1.320446 -6 4 7 150.50 131.48 < 1.318331 10 2 9 13.49 12.81 < 1.317942 -16 0 8 19.91 18.03 < 1.317230 3 5 0 445.87 302.05 < 1.316947 0 5 2 406.63 316.68 < 1.316482 -1 5 2 745.93 492.14 < 1.315659 2 3 10 2290.27 1339.19 < 1.315426 -16 2 6 725.14 406.53 < 1.314539 -3 5 1 230.28 142.01 < 1.314267 -8 0 12 106.14 65.29 < 1.314016 1 5 2 470.14 320.85 < 1.313759 -14 2 8 5.21 3.33 < 1.313589 -18 1 5 0.02 0.02 < 1.313090 15 3 2 20.62 14.40 < 1.312932 -19 1 1 223.91 152.87 < 1.312248 10 1 10 588.61 432.25 < 1.312001 -5 3 10 1.15 1.06 < 1.311502 3 5 1 10.60 9.80 < 1.311429 -2 5 2 6.35 5.71 < 1.311309 18 1 3 1.23 0.95 < 1.310307 -12 4 1 52.11 50.69 < 1.309649 14 0 8 576.11 430.74 < 1.309497 13 3 5 0.40 0.31 < 1.309400 -7 1 12 184.89 143.89 < 1.309340 -19 1 2 146.59 100.07 < 1.309004 5 0 12 45.39 30.99 < 1.309011 7 4 6 2.81 2.10 < 1.308736 8 2 10 422.31 329.77 < 1.308573 12 1 9 87.24 68.81 < 1.308226 12 4 0 3.29 2.68 < 1.308071 2 5 2 1490.78 1144.44 < 1.307555 19 1 0 1226.99 914.55 < 1.307378 -10 4 5 2685.67 2047.65 < 1.307250 -11 3 8 247.96 189.05 < 1.307209 12 2 8 145.54 115.65 < 1.306935 -15 3 4 115.36 86.19 < 1.306558 12 3 6 512.03 424.59 < 1.305315 4 1 12 15.17 11.88 < 1.305147 -9 3 9 70.55 55.28 < 1.305059 4 5 0 181.81 128.70 < 1.304664 -11 4 4 171.48 122.90 < 1.304178 -19 0 4 202.97 152.15 < 1.303533 -3 5 2 446.23 334.49 < 1.303537 5 2 11 36.33 26.36 < 1.303512 -12 4 2 126.61 83.02 < 1.303175 14 3 4 2.27 1.70 < 1.302894 -1 4 8 106.86 79.80 < 1.302809 -4 5 1 534.59 379.24 < 1.302519 -8 2 11 152.46 106.27 < 1.302409 -18 0 6 56.20 36.61 < 1.302288 9 3 8 0.90 0.60 < 1.302156 3 3 10 515.51 393.04 < 1.302009 10 4 4 168.12 133.13 < 1.301536 5 4 7 1154.25 895.65 < 1.301424 -2 4 8 11.41 8.98 < 1.301340 0 4 8 29.23 25.68 < 1.300839 -18 2 1 87.58 76.94 < 1.300799 16 1 6 152.92 119.83 < 1.300290 -13 1 10 13.73 15.63 < 1.299337 -7 4 7 66.79 68.58 < 1.298913 18 0 4 198.06 203.36 < 1.298896 4 5 1 672.77 673.79 < 1.298840 19 0 2 76.26 64.43 < 1.298733 12 4 1 9.94 9.22 < 1.298525 -11 2 10 86.57 88.15 < 1.298167 3 5 2 571.13 488.82 < 1.298017 -9 4 6 65.60 56.15 < 1.297958 -19 1 3 0.43 0.40 < 1.297825 15 1 7 0.48 0.38 < 1.297705 17 2 3 42.89 31.74 < 1.297328 -18 2 2 3.93 2.71 < 1.297183 -6 3 10 0.53 0.36 < 1.297123 11 4 3 1335.64 893.19 < 1.296557 18 2 0 216.04 146.71 < 1.296510 -3 4 8 10.80 7.33 < 1.296467 -17 2 5 3229.35 2154.87 < 1.296371 0 5 3 18.55 12.38 < 1.296372 9 4 5 155.70 101.59 < 1.296108 -1 5 3 900.81 587.76 < 1.296041 11 0 10 1346.15 878.34 < 1.296033 8 1 11 34.84 22.61 < 1.295761 1 4 8 1157.87 800.14 < 1.295476 19 1 1 661.36 456.48 < 1.294661 -13 2 9 291.44 190.26 < 1.294550 -11 1 11 19.95 12.38 < 1.294178 7 3 9 908.23 666.88 < 1.293729 1 5 3 15.44 12.06 < 1.293319 -16 3 1 458.47 366.75 < 1.292750 17 1 5 317.72 262.98 < 1.292514 -4 5 2 1447.04 1197.74 < 1.292523 -2 5 3 78.85 63.70 < 1.292333 -16 1 8 15.52 12.68 < 1.292244 -17 1 7 489.59 390.26 < 1.291095 11 3 7 213.91 175.76 < 1.290930 -9 0 12 659.52 577.70 < 1.290311 16 3 0 61.47 58.88 < 1.289435 5 5 0 138.07 134.03 < 1.289364 -8 1 12 735.69 713.47 < 1.289209 -12 4 3 168.86 158.45 < 1.288998 -16 3 2 1548.08 1428.03 < 1.288305 -4 4 8 14.24 13.13 < 1.288303 -14 3 6 898.09 772.39 < 1.288069 -5 5 1 250.41 220.87 < 1.287740 2 5 3 257.32 200.77 < 1.286953 2 4 8 34.65 27.03 < 1.286846 15 3 3 21.27 15.53 < 1.286258 -13 3 7 361.32 258.54 < 1.286040 -18 2 3 370.87 262.20 < 1.285856 4 3 10 619.42 434.80 < 1.285670 4 5 2 2.00 1.40 < 1.285362 -3 5 3 44.01 30.81 < 1.285335 14 1 8 321.03 222.53 < 1.284941 6 0 12 772.46 530.87 < 1.284847 -2 2 12 1031.86 709.14 < 1.284833 18 2 1 1288.82 919.10 < 1.284547 5 1 12 256.30 182.78 < 1.284482 -1 2 12 373.40 266.28 < 1.284471 5 5 1 92.84 58.66 < 1.283300 -14 0 10 4.60 3.36 < 1.282777 15 2 6 573.19 383.74 < 1.282322 -3 2 12 0.20 0.14 < 1.281900 12 4 2 282.42 179.48 < 1.281523 -15 1 9 14.31 9.28 < 1.281480 0 2 12 1605.89 1068.65 < 1.280823 8 4 6 22.91 16.16 < 1.280657 6 2 11 239.38 189.95 < 1.280084 -7 3 10 611.38 521.79 < 1.279926 6 4 7 1187.07 1013.12 < 1.279856 -19 1 4 481.53 406.58 < 1.279305 -9 2 11 71.15 62.46 < 1.278879 16 3 1 115.20 98.12 < 1.278538 -5 5 2 23.99 20.44 < 1.278515 -15 3 5 1453.47 1256.91 < 1.278282 -18 1 6 2.22 1.91 < 1.278127 11 2 9 51.07 43.92 < 1.278064 16 2 5 56.52 49.29 o 1.277667 3 5 3 27.66 25.37 o 1.277420 -10 3 9 443.33 387.54 o 1.277250 -8 4 7 284.93 246.43 < 1.277070 -5 4 8 123.07 106.67 < 1.277034 14 2 7 446.41 396.23 < 1.277023 -16 3 3 1703.77 1446.59 < 1.276338 -4 2 12 17.23 14.66 < 1.275739 9 2 10 663.57 560.09 < 1.275506 -4 5 3 826.86 666.38 < 1.275206 3 4 8 259.18 208.88 < 1.275142 18 1 4 505.16 373.93 < 1.274921 19 1 2 263.59 187.92 < 1.274767 -11 4 5 8.29 5.80 < 1.274320 1 2 12 66.06 49.27 < 1.273971 -12 3 8 2017.78 1545.41 < 1.272359 11 1 10 1119.35 867.06 < 1.272213 6 5 0 0.24 0.16 < 1.271376 -16 2 7 184.50 124.15 < 1.271114 -6 5 1 590.23 509.79 < 1.270247 5 5 2 25.29 18.91 < 1.269867 -1 5 4 298.32 223.16 < 1.269822 0 5 4 327.54 220.26 < 1.269705 -10 4 6 10.10 7.21 < 1.269307 -20 0 2 0.06 0.04 < 1.268938 -15 2 8 556.95 409.08 < 1.268587 -13 4 1 110.46 83.64 < 1.268398 -12 4 4 19.57 16.34 < 1.267856 -18 2 4 628.47 476.75 o 1.267411 10 3 8 248.80 194.70 o 1.267234 17 0 6 386.49 305.11 o 1.267059 -9 1 12 78.89 65.44 o 1.266800 -2 5 4 0.78 0.65 o 1.266759 5 3 10 271.36 225.08 o 1.266752 20 0 0 90.70 73.35 o 1.266606 13 4 0 54.34 43.95 o 1.266539 -5 2 12 1556.57 1239.23 o 1.266488 1 5 4 143.83 114.51 o 1.266412 18 2 2 87.20 74.88 o 1.265532 -17 0 8 17.47 15.00 o 1.265500 8 3 9 3081.32 2682.87 o 1.265313 11 4 4 5.45 4.84 o 1.265197 6 5 1 668.44 587.34 o 1.265138 4 5 3 40.10 36.17 o 1.264929 -12 2 10 91.85 82.85 o 1.264861 -10 0 12 402.58 366.94 o 1.264681 2 2 12 2132.86 1865.89 o 1.264069 17 2 4 5.42 4.81 o 1.263377 9 1 11 221.53 192.04 o 1.263211 -13 4 2 1621.43 1402.90 o 1.262934 10 4 5 735.55 636.42 o 1.262919 -6 4 8 7.89 6.81 o 1.262904 13 1 9 24.56 21.21 o 1.262873 14 3 5 33.18 28.96 o 1.262474 -17 2 6 452.14 386.95 o 1.262273 -2 1 13 329.06 281.61 o 1.262262 -5 5 3 60.44 51.98 o 1.262167 13 2 8 481.14 406.02 o 1.262132 -6 5 2 106.88 93.07 o 1.261810 6 1 12 82.84 71.30 o 1.261628 -12 1 11 141.65 121.92 o 1.261590 13 3 6 37.37 31.20 o 1.261511 -1 1 13 243.75 203.48 o 1.261499 16 3 2 69.05 68.63 < 1.260621 4 4 8 23.50 23.36 < 1.260619 -3 5 4 636.77 632.95 < 1.260585 -8 3 10 92.45 81.17 < 1.260265 2 5 4 5.16 5.18 < 1.260015 -3 1 13 18.43 18.18 < 1.259898 -14 1 10 256.16 246.75 < 1.259667 7 0 12 675.06 650.42 < 1.258853 15 0 8 2046.61 1976.54 < 1.258186 12 4 3 645.06 574.01 < 1.257928 0 1 13 48.78 47.25 < 1.257627 -16 3 4 292.63 257.59 < 1.257462 13 4 1 764.96 673.36 < 1.257452 7 4 7 6.95 4.60 < 1.256225 -14 2 9 255.36 151.43 < 1.254891 7 2 11 19.11 12.32 < 1.254785 12 0 10 66.34 40.59 < 1.254551 -4 1 13 7.19 4.69 < 1.254460 -19 1 5 792.03 510.97 < 1.254373 -6 2 12 141.40 91.22 < 1.254349 15 3 4 304.93 170.78 < 1.253970 -1 3 11 290.47 174.62 < 1.253871 -2 3 11 28.03 17.73 < 1.253795 -10 2 11 443.12 288.65 < 1.253499 -9 4 7 90.11 66.57 < 1.253214 6 5 2 282.93 228.19 < 1.251851 -4 5 4 201.13 175.80 < 1.251434 3 2 12 92.62 83.50 < 1.251329 9 4 6 323.18 273.77 < 1.251247 12 3 7 553.17 480.68 < 1.251146 7 5 0 741.61 624.37 < 1.251058 0 3 11 103.08 87.68 < 1.250885 1 1 13 87.88 75.22 < 1.250729 -3 3 11 15.14 13.05 < 1.250660 3 5 4 1.91 1.65 < 1.250655 -13 4 3 79.79 68.02 < 1.250426 -7 5 1 278.49 237.41 < 1.250391 5 5 3 11.15 8.55 < 1.249745 -20 1 1 130.27 81.58 < 1.248948 19 1 3 21.53 11.49 < 1.248678 -11 3 9 149.87 88.90 < 1.248104 -20 1 2 0.83 0.58 < 1.246555 -6 5 3 342.70 252.80 < 1.246492 -14 3 7 586.19 457.69 < 1.246325 -7 4 8 259.67 206.46 < 1.246207 -5 1 13 58.86 46.18 < 1.246066 6 3 10 27.41 21.70 < 1.245622 -19 0 6 231.87 181.62 < 1.245350 16 1 7 63.84 51.99 < 1.245102 1 3 11 2396.06 2014.43 < 1.244903 17 1 6 24.53 20.76 < 1.244774 -15 3 6 562.03 475.73 < 1.244749 7 5 1 322.71 260.39 < 1.244709 -4 3 11 33.10 27.20 < 1.244533 20 1 0 279.09 237.75 < 1.244344 5 4 8 184.43 180.19 < 1.243573 -17 1 8 15.52 17.06 < 1.243296 -18 2 5 893.50 774.73 < 1.242754 -7 5 2 1423.82 1234.54 < 1.242742 -20 0 4 256.44 232.61 < 1.242629 -10 1 12 38.41 34.86 < 1.242519 -19 2 1 141.64 131.50 < 1.242040 10 2 10 308.45 281.63 < 1.241831 13 4 2 32.72 31.81 < 1.241594 -15 0 10 142.76 138.78 < 1.241568 2 1 13 744.41 697.84 < 1.240955 -17 3 1 1.70 1.60 < 1.240941 -12 4 5 1276.75 1115.86 < 1.240771 18 2 3 210.28 155.00 < 1.240394 -1 4 9 84.96 65.01 < 1.240265 -7 2 12 1601.92 1165.21 < 1.239574 -5 5 4 14.50 11.83 < 1.239502 -11 4 6 19.75 16.11 < 1.239494 -2 4 9 219.63 179.14 < 1.239395 -19 2 2 42.23 31.73 < 1.239289 -18 1 7 32.12 24.27 < 1.238898 12 2 9 96.25 72.89 < 1.238628 4 5 4 98.24 73.62 < 1.238529 -9 3 10 23.81 17.84 < 1.238512 19 0 4 40.33 31.58 < 1.238394 -1 5 5 16.33 12.85 < 1.238226 0 4 9 70.37 55.37 < 1.238168 19 2 0 1332.94 1068.26 < 1.237909 0 5 5 336.66 272.83 < 1.237721 17 3 0 1841.32 1492.17 < 1.237612 -11 0 12 906.02 717.50 < 1.237556 -17 3 2 615.35 511.33 < 1.237404 -20 1 3 16.92 14.22 o 1.237285 -13 3 8 44.12 38.42 o 1.237193 -16 1 9 144.97 116.88 < 1.237032 7 1 12 170.48 137.87 o 1.236991 16 3 3 488.79 377.25 < 1.236558 15 1 8 406.99 333.06 o 1.236357 20 0 2 2807.33 2132.18 < 1.236094 2 3 11 153.58 116.65 < 1.236053 4 2 12 242.07 183.86 < 1.236014 -2 5 5 329.52 255.91 < 1.235779 9 3 9 1392.24 1047.90 < 1.235739 -3 4 9 802.49 597.94 < 1.235578 -5 3 11 376.95 280.87 < 1.235546 18 1 5 248.60 189.29 o 1.235395 -6 1 13 306.23 234.59 < 1.234893 1 5 5 2057.48 1624.25 < 1.234277 1 4 9 65.92 63.41 < 1.233149 20 1 1 12.72 10.99 < 1.232972 12 1 10 172.97 141.32 < 1.232908 -16 3 5 369.90 375.46 < 1.232587 6 5 3 3.29 3.60 < 1.232170 11 3 8 15.77 17.35 < 1.232055 16 2 6 39.91 43.33 < 1.231886 7 5 2 375.42 390.84 < 1.231659 -13 4 4 118.36 107.82 < 1.231488 8 0 12 3.58 3.27 < 1.231456 -13 2 10 220.34 221.11 < 1.231076 8 4 7 6.46 6.64 < 1.230939 -3 5 5 54.48 45.95 < 1.230434 10 1 11 605.37 514.82 < 1.230086 -19 2 3 37.34 31.88 < 1.229789 15 2 7 3.45 2.93 < 1.229687 11 4 5 44.32 39.89 < 1.229251 -4 4 9 277.34 261.36 < 1.228892 12 4 4 41.99 39.57 < 1.228840 8 5 0 78.31 73.79 < 1.228782 -8 5 1 1562.74 1406.33 < 1.228538 3 1 13 39.43 35.48 < 1.228508 -7 5 3 872.03 784.75 < 1.228486 -13 1 11 610.76 549.64 < 1.228447 8 2 11 0.81 0.75 < 1.228033 2 5 5 245.45 232.69 < 1.227965 -14 4 1 617.98 585.87 < 1.227918 -10 4 7 16.42 14.93 < 1.227754 17 3 1 281.46 255.41 < 1.227580 -8 4 8 7.06 5.78 < 1.227264 -17 3 3 5.02 4.10 < 1.227174 19 2 1 333.58 269.93 < 1.227096 -11 2 11 14.31 10.50 < 1.226686 14 4 0 94.73 51.55 < 1.225846 2 4 9 82.36 47.69 < 1.225314 17 2 5 7.23 4.18 < 1.225268 -16 2 8 1.49 0.87 < 1.225038 -6 5 4 225.55 132.56 < 1.225030 3 3 11 281.32 172.76 < 1.224517 6 4 8 165.21 100.81 < 1.224331 -19 1 6 0.12 0.07 < 1.224172 -17 2 7 518.01 307.82 < 1.224059 5 5 4 1449.14 918.77 < 1.223882 -6 3 11 5.01 3.18 < 1.223884 -14 4 2 5.98 4.05 < 1.223342 7 3 10 314.13 245.11 < 1.222657 -8 2 12 40.27 33.52 < 1.222452 8 5 1 95.32 79.34 < 1.222383 -4 5 5 244.00 206.73 < 1.222302 -8 5 2 89.33 87.36 < 1.221661 -20 1 4 1005.09 916.06 < 1.221587 -7 1 13 105.74 99.86 < 1.221167 10 4 6 202.38 182.12 < 1.220928 -15 1 10 29.47 26.39 < 1.220579 13 4 3 518.49 528.91 < 1.219721 -5 4 9 7.97 7.43 < 1.219479 14 1 9 34.98 29.98 < 1.219099 14 3 6 491.62 407.59 < 1.219008 3 5 5 1004.24 832.58 < 1.218917 14 2 8 390.88 314.10 < 1.218811 5 2 12 86.23 67.74 < 1.218419 -12 3 9 35.88 28.31 < 1.218042 19 1 4 1076.37 651.09 < 1.217563 15 3 5 64.73 30.66 < 1.217435 14 4 1 15.91 6.49 < 1.217224 -11 1 12 1035.23 476.88 < 1.216766 -18 0 8 407.60 196.82 < 1.216607 -15 2 9 324.29 154.62 < 1.215856 20 1 2 48.35 20.32 < 1.215376 -10 3 10 73.65 32.51 < 1.215043 3 4 9 346.75 155.72 < 1.214823 13 0 10 66.91 40.52 < 1.214015 -19 2 4 2191.14 1327.05 < 1.213998 4 1 13 552.00 358.77 < 1.213632 -18 2 6 39.50 24.26 < 1.212992 18 0 6 137.17 68.10 < 1.212739 7 5 3 499.07 309.94 < 1.212528 -14 4 3 314.44 219.79 < 1.212335 13 3 7 400.10 245.11 < 1.212044 -5 5 5 36.18 22.88 < 1.211548 17 3 2 43.75 28.21 < 1.211324 8 1 12 1967.94 1170.95 < 1.210967 -17 3 4 468.07 263.46 < 1.210739 4 3 11 494.79 299.78 < 1.210525 18 2 4 142.02 86.13 < 1.210249 19 2 2 23.10 13.71 < 1.210118 -7 3 11 17.15 10.59 < 1.209778 16 0 8 2340.65 1323.83 < 1.209700 8 5 2 223.84 120.78 < 1.209646 -12 0 12 77.78 37.27 < 1.209339 -21 0 2 276.92 131.52 < 1.209043 -12 4 6 11.08 4.60 < 1.208925 -8 5 3 1151.84 696.93 < 1.208480 -7 5 4 10.02 5.66 < 1.208295 11 2 10 1.11 0.61 < 1.207933 -6 4 9 1732.60 1101.67 < 1.207525 16 3 4 4.46 2.77 < 1.207421 -15 3 7 360.44 235.24 < 1.207323 4 5 5 572.57 383.86 < 1.207315 -13 4 5 4.62 2.99 < 1.206990 6 5 4 123.15 79.73 < 1.206993 -9 4 8 23.64 14.79 < 1.206414 21 0 0 16.09 11.28 < 1.206291 10 3 9 2713.22 2573.06 < 1.205408 -8 1 13 2.03 1.75 < 1.205152 -9 5 1 63.06 56.02 < 1.205055 9 5 0 7.87 6.87 < 1.204920 9 4 7 8.02 6.88 < 1.204389 -9 2 12 488.40 310.54 < 1.203296 7 4 8 43.84 28.94 < 1.203231 9 0 12 1648.65 1215.46 < 1.203049 -16 3 6 1.91 1.34 < 1.202803 -1 5 6 130.77 94.96 < 1.202552 14 4 2 23.28 16.41 < 1.202460 -14 3 8 258.46 179.51 < 1.202075 4 4 9 47.80 32.25 < 1.201882 0 5 6 22.98 16.43 < 1.201727 -16 0 10 85.44 60.74 < 1.201379 -11 4 7 138.24 99.94 < 1.201075 -2 5 6 2.15 1.66 < 1.200673 9 2 11 361.65 315.33 < 1.200219 -20 1 5 33.82 28.79 < 1.200186 13 2 9 0.32 0.29 < 1.199930 -2 2 13 516.47 407.73 < 1.199405 -9 5 2 111.15 88.41 < 1.198924 6 2 12 15.70 11.91 < 1.198861 -12 2 11 153.75 116.66 < 1.198829 -1 2 13 9.01 6.84 < 1.198751 _publcif_info_exptl_table_max_cols 4 _publcif_info_exptl_table_use_headnotes n loop_ _publcif_info_tables.block_id _publcif_info_tables.reference_item "{5b332a7d-e417-4717-b1fe-e5605d0d98fc}" "_publcif_info_datablock.publ_exptl" loop_ _publcif_info_datablock.id _publcif_info_datablock.publ_exptl _publcif_info_datablock.publ_geom _publcif_info_datablock.structure '{5b332a7d-e417-4717-b1fe-e5605d0d98fc}' ? ? ? '{d3d78d5c-a0fa-4c26-a555-2d559a7c88ce}' y y y loop_ _publcif_info_exptl_table_extra_item ? loop_ _publcif_info_exptl_table_header_item ? #======================================================================= data_TCl_AD #======================================================================= # 5. CHEMICAL DATA _chemical_name_systematic ? _chemical_name_common ? _chemical_formula_moiety 'C25 H30 N O3, 0.5(C6 H10 O4), Cl' _chemical_formula_structural ? _chemical_formula_analytical ? _chemical_formula_iupac ? _chemical_formula_sum 'C28 H35 Cl1 N1 O5' _chemical_formula_weight 501 _chemical_melting_point ? _chemical_compound_source ? _chemical_absolute_configuration . #======================================================================= # 6. POWDER SPECIMEN AND CRYSTAL DATA _symmetry_cell_setting monoclinic _symmetry_space_group_name_H-M 'P 1 21/c 1' _symmetry_space_group_name_Hall '-P 2ycb' _symmetry_Int_Tables_number 14 loop_ _symmetry_equiv_pos_site_id _symmetry_equiv_pos_as_xyz 1 x,y,z 2 -x,y+1/2,-z+1/2 3 -x,-y,-z 4 x,-y+1/2,z+1/2 _cell_length_a 24.2324(6) _cell_length_b 6.76298(12) _cell_length_c 16.5907(3) _cell_angle_alpha 90 _cell_angle_beta 107.6063(9) _cell_angle_gamma 90 _cell_volume 2591.58(9) _cell_formula_units_Z 4 _cell_measurement_temperature 293 _cell_special_details ? _exptl_crystal_density_diffrn 1.2837 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_F_000 454 _pd_spec_size_axial ? _pd_spec_size_equat ? _pd_spec_size_thick ? _pd_spec_mounting ? _pd_spec_mount_mode ? _pd_spec_shape ? _pd_char_particle_morphology ? _pd_char_colour white _pd_prep_cool_rate ? _pd_prep_pressure ? _pd_prep_temperature 298 _exptl_absorpt_coefficient_mu 1.616 _exptl_absorpt_correction_type ? _exptl_absorpt_process_details ? _exptl_absorpt_correction_T_min ? _exptl_absorpt_correction_T_max ? #======================================================================= # 7. EXPERIMENTAL DATA _exptl_special_details ? _pd_instr_location ? _pd_calibration_special_details ? _diffrn_ambient_temperature 293 _diffrn_source ? _diffrn_source_target ? _diffrn_source_type ? _diffrn_radiation_type 'CuK\a' _diffrn_radiation_wavelength 1.5418 _diffrn_radiation_monochromator ? _diffrn_measurement_device ? _diffrn_measurement_device_type 'PANalytical Empyrean' _diffrn_detector 'PIXCel3D' _diffrn_detector_type ? _pd_meas_scan_method ? _pd_meas_special_details ? _pd_meas_number_of_points 5788 _pd_meas_2theta_range_min 4.003 _pd_meas_2theta_range_max 79.988 _pd_meas_2theta_range_inc 0.013 _diffrn_radiation_probe x-ray #======================================================================= # 8. REFINEMENT DATA _pd_proc_ls_special_details ? _pd_proc_ls_profile_function 'Pseudo-Voigt' _pd_proc_ls_background_function '25 Legendre polynoms' _pd_proc_ls_pref_orient_corr 'March & Dollase' _pd_proc_ls_prof_R_factor 0.0210 _pd_proc_ls_prof_wR_factor 0.0282 _pd_proc_ls_prof_wR_expected 0.0101 _refine_special_details ? _refine_ls_R_factor_gt 0.0482 _refine_ls_wR_factor_gt 0.0513 _refine_ls_R_factor_all 0.0690 _refine_ls_wR_factor_all 0.0565 _refine_ls_goodness_of_fit_all 2.81 _refine_ls_restrained_S_gt ? _refine_ls_restrained_S_all ? _refine_ls_number_parameters 144 _refine_ls_number_restraints 92 _refine_ls_number_constraints 945 _refine_ls_weighting_scheme sigma _refine_ls_weighting_details ? _refine_ls_hydrogen_treatment constr _refine_ls_shift/su_max 0.0437 _refine_ls_shift/su_mean 0.0075 _refine_diff_density_max 0.11 _refine_diff_density_min -0.12 _refine_ls_extinction_method ? _refine_ls_extinction_coef ? _pd_proc_2theta_range_min 4.003 _pd_proc_2theta_range_max 79.988 _pd_proc_2theta_range_inc 0.013 _pd_proc_wavelength ? _pd_block_diffractogram_id ? _pd_proc_info_excluded_regions ? _pd_proc_info_data_reduction ? loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C 0.0181 0.0091 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' H 0.0000 0.0000 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Cl 0.3639 0.7018 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' N 0.0311 0.0180 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' O 0.0492 0.0322 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution ? _computing_structure_refinement ? _computing_molecular_graphics ? _computing_publication_material ? loop_ _restr_distance_atom_site_label_1 _restr_distance_site_symmetry_1 _restr_distance_atom_site_label_2 _restr_distance_site_symmetry_2 _restr_distance_target _restr_distance_target_weight_param C1 . O1 . 1.34 0.001 C15 . O1 . 1.461 0.001 O2 . C1 . 1.198 0.001 C2 . C1 . 1.532 0.001 C16 . C15 . 1.528 0.001 C19 . C15 . 1.52 0.001 O3 . C2 . 1.433 0.001 C9 . C2 . 1.536 0.001 C3 . C2 . 1.547 0.001 C17 . C16 . 1.519 0.001 C18 . C19 . 1.521 0.001 C10 . C9 . 1.378 0.001 C14 . C9 . 1.387 0.001 C4 . C3 . 1.377 0.001 C8 . C3 . 1.396 0.001 N1 . C17 . 1.533 0.001 C21 . C17 . 1.53 0.001 N1 . C18 . 1.525 0.001 C20 . C18 . 1.524 0.001 C11 . C10 . 1.396 0.001 C13 . C14 . 1.398 0.001 C5 . C4 . 1.391 0.001 C7 . C8 . 1.39 0.001 C22 . N1 . 1.507 0.001 C25 . N1 . 1.517 0.001 C20 . C21 . 1.548 0.001 C12 . C11 . 1.375 0.001 C12 . C13 . 1.365 0.001 C6 . C5 . 1.367 0.001 C6 . C7 . 1.376 0.001 C23 . C22 . 1.512 0.001 C24 . C25 . 1.514 0.001 C24 . C23 . 1.543 0.001 O5 . C26 . 1.326 0.001 O4 . C26 . 1.232 0.001 C26 . C27 . 1.511 0.001 C27 . C28 . 1.527 0.001 C28 . C28 3_675 1.542 0.001 loop_ _restr_angle_atom_site_label_1 _restr_angle_site_symmetry_1 _restr_angle_atom_site_label_2 _restr_angle_site_symmetry_2 _restr_angle_atom_site_label_3 _restr_angle_site_symmetry_3 _restr_angle_target _restr_angle_target_weight_param ? ? ? ? ? ? ? ? loop_ _restr_torsion_atom_site_label_1 _restr_torsion_site_symmetry_1 _restr_torsion_atom_site_label_2 _restr_torsion_site_symmetry_2 _restr_torsion_atom_site_label_3 _restr_torsion_site_symmetry_3 _restr_torsion_atom_site_label_4 _restr_torsion_site_symmetry_4 _restr_torsion_angle_target _restr_torsion_weight_param ? ? ? ? ? ? ? ? ? ? loop_ _restr_equal_distance_atom_site_label_1 _restr_equal_distance_site_symmetry_1 _restr_equal_distance_atom_site_label_2 _restr_equal_distance_site_symmetry_2 _restr_equal_distance_class_class_id _restr_equal_distance_class_target_weight_param ? ? ? ? ? ? loop_ _restr_equal_angle_atom_site_label_1 _restr_equal_angle_site_symmetry_1 _restr_equal_angle_atom_site_label_2 _restr_equal_angle_site_symmetry_2 _restr_equal_angle_atom_site_label_3 _restr_equal_angle_site_symmetry_3 _restr_equal_angle_class_class_id _restr_equal_angle_class_target_weight_param ? ? ? ? ? ? ? ? loop_ _restr_equal_torsion_atom_site_label_1 _restr_equal_torsion_site_symmetry_1 _restr_equal_torsion_atom_site_label_2 _restr_equal_torsion_site_symmetry_2 _restr_equal_torsion_atom_site_label_3 _restr_equal_torsion_site_symmetry_3 _restr_equal_torsion_atom_site_label_4 _restr_equal_torsion_site_symmetry_4 _restr_equal_torsion_class_class_id _restr_equal_torsion_class_target_weight_param ? ? ? ? ? ? ? ? ? ? #======================================================================= # 9. ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_site_symmetry_multiplicity _atom_site_occupancy _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.77152(15) 0.1626(5) 0.07947(17) Uiso 0.0639(16) 4 1 d . . . C1 C 0.79562(11) 0.1782(3) 0.16327(17) Uiso 0.0639(16) 4 1 d . . . O2 O 0.78376(20) 0.3038(5) 0.2062(2) Uiso 0.0639(16) 4 1 d . . . C2 C 0.83681(9) 0.0029(3) 0.19420(15) Uiso 0.0639(16) 4 1 d . . . O3 O 0.80950(9) -0.1746(3) 0.15443(17) Uiso 0.0639(16) 4 1 d . . . C3 C 0.89089(10) 0.0403(3) 0.16518(20) Uiso 0.0639(16) 4 1 d . . . C4 C 0.9223(2) -0.1100(4) 0.1442(6) Uiso 0.0639(16) 4 1 d . . . C5 C 0.9744(2) -0.0712(6) 0.1283(6) Uiso 0.0639(16) 4 1 d . . . C6 C 0.99388(19) 0.1191(6) 0.1311(5) Uiso 0.0639(16) 4 1 d . . . C7 C 0.9630(2) 0.2716(5) 0.1516(6) Uiso 0.0639(16) 4 1 d . . . C8 C 0.9107(2) 0.2346(3) 0.1669(5) Uiso 0.0639(16) 4 1 d . . . C9 C 0.85803(15) -0.0223(3) 0.29067(17) Uiso 0.0639(16) 4 1 d . . . C10 C 0.8508(3) -0.1938(6) 0.3311(2) Uiso 0.0639(16) 4 1 d . . . C11 C 0.8697(4) -0.2047(8) 0.4192(2) Uiso 0.0639(16) 4 1 d . . . C12 C 0.8956(3) -0.0451(8) 0.46732(18) Uiso 0.0639(16) 4 1 d . . . C13 C 0.9009(4) 0.1276(8) 0.42766(18) Uiso 0.0639(16) 4 1 d . . . C14 C 0.8820(4) 0.1408(5) 0.33949(18) Uiso 0.0639(16) 4 1 d . . . C15 C 0.72219(17) 0.2907(6) 0.03952(19) Uiso 0.0639(16) 4 1 d . . . C16 C 0.66937(14) 0.1632(9) -0.0029(2) Uiso 0.0639(16) 4 1 d . . . C17 C 0.66928(16) 0.0820(4) -0.0883(2) Uiso 0.0639(16) 4 1 d . . . N1 N 0.67200(13) 0.2570(4) -0.14575(18) Uiso 0.0639(16) 4 1 d . . . C18 C 0.73498(15) 0.3190(6) -0.1066(2) Uiso 0.0639(16) 4 1 d . . . C19 C 0.7404(2) 0.4208(4) -0.0228(3) Uiso 0.0639(16) 4 1 d . . . C20 C 0.76681(16) 0.1221(9) -0.0981(2) Uiso 0.0639(16) 4 1 d . . . C21 C 0.7238(2) -0.0356(5) -0.0854(2) Uiso 0.0639(16) 4 1 d . . . C22 C 0.6285(2) 0.4212(6) -0.1544(2) Uiso 0.0639(16) 4 1 d . . . C23 C 0.57307(16) 0.3373(9) -0.2137(3) Uiso 0.0639(16) 4 1 d . . . C24 C 0.59343(19) 0.1960(7) -0.2721(2) Uiso 0.0639(16) 4 1 d . . . C25 C 0.65874(18) 0.1913(7) -0.23703(19) Uiso 0.0639(16) 4 1 d . . . Cl1 Cl 0.30743(17) 0.3170(5) 0.3092(3) Uiso 0.070(2) 4 1 d . . . H1c4 H 0.908094 -0.243263 0.140564 Uiso 0.0767 4 1 d . . . H1c5 H 0.996575 -0.177597 0.115502 Uiso 0.0767 4 1 d . . . H1c6 H 1.029297 0.146544 0.118575 Uiso 0.0767 4 1 d . . . H1c7 H 0.977739 0.404181 0.155339 Uiso 0.0767 4 1 d . . . H1c8 H 0.888354 0.341934 0.178536 Uiso 0.0767 4 1 d . . . H1c10 H 0.83263 -0.306327 0.298496 Uiso 0.0767 4 1 d . . . H1c11 H 0.864509 -0.325191 0.446641 Uiso 0.0767 4 1 d . . . H1c12 H 0.909799 -0.055061 0.527824 Uiso 0.0767 4 1 d . . . H1c13 H 0.917739 0.241153 0.4607 Uiso 0.0767 4 1 d . . . H1c14 H 0.885608 0.263553 0.312497 Uiso 0.0767 4 1 d . . . H1c15 H 0.711508 0.37319 0.079493 Uiso 0.0767 4 1 d . . . H1c16 H 0.66723 0.055788 0.033844 Uiso 0.0767 4 1 d . . . H2c16 H 0.634752 0.238775 -0.009389 Uiso 0.0767 4 1 d . . . H1c17 H 0.635445 0.000037 -0.106885 Uiso 0.0767 4 1 d . . . H1c18 H 0.750195 0.411959 -0.138131 Uiso 0.0767 4 1 d . . . H1c19 H 0.71759 0.539555 -0.032856 Uiso 0.0767 4 1 d . . . H2c19 H 0.779562 0.463911 0.002302 Uiso 0.0767 4 1 d . . . H1c20 H 0.800379 0.125407 -0.049189 Uiso 0.0767 4 1 d . . . H2c20 H 0.775982 0.09471 -0.149388 Uiso 0.0767 4 1 d . . . H1c21 H 0.715126 -0.127864 -0.1315 Uiso 0.0767 4 1 d . . . H2c21 H 0.739236 -0.095329 -0.030662 Uiso 0.0767 4 1 d . . . H1c22 H 0.640313 0.533923 -0.180294 Uiso 0.0767 4 1 d . . . H2c22 H 0.62325 0.447413 -0.100351 Uiso 0.0767 4 1 d . . . H1c23 H 0.553121 0.263091 -0.181702 Uiso 0.0767 4 1 d . . . H2c23 H 0.550529 0.442221 -0.246721 Uiso 0.0767 4 1 d . . . H1c24 H 0.582398 0.24883 -0.328431 Uiso 0.0767 4 1 d . . . H2c24 H 0.578254 0.066065 -0.269066 Uiso 0.0767 4 1 d . . . H1c25 H 0.672177 0.058272 -0.238772 Uiso 0.0767 4 1 d . . . H2c25 H 0.675047 0.284144 -0.267236 Uiso 0.0767 4 1 d . . . O4 O 0.54172(10) 0.6497(10) -0.0778(3) Uiso 0.107(3) 4 1 d . . . O5 O 0.62421(15) 0.6380(18) 0.0308(2) Uiso 0.107(3) 4 1 d . . . C26 C 0.56867(8) 0.6827(7) -0.0033(2) Uiso 0.107(3) 4 1 d . . . C27 C 0.54205(19) 0.7726(6) 0.0597(2) Uiso 0.107(3) 4 1 d . . . C28 C 0.49062(9) 0.9084(3) 0.0203(3) Uiso 0.107(3) 4 1 d . . . H1c27 H 0.571134 0.844119 0.101852 Uiso 0.1284 4 1 d . . . H2c27 H 0.530374 0.669187 0.090692 Uiso 0.1284 4 1 d . . . H1c28 H 0.473817 0.950022 0.062973 Uiso 0.1284 4 1 d . . . H2c28 H 0.461577 0.837028 -0.022 Uiso 0.1284 4 1 d . . . H1o3 H 0.778559 -0.216662 0.163944 Uiso 0.0767 4 1 d . . . H1o5 H 0.641066 0.661091 0.083487 Uiso 0.1284 4 1 d . . . loop_ _atom_site_aniso_label _atom_site_aniso_type_symbol _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 ? ? ? ? ? ? ? ? loop_ _jana_atom_site_ADP_C_label _jana_atom_site_ADP_C_type_symbol _jana_atom_site_ADP_C_111 _jana_atom_site_ADP_C_112 _jana_atom_site_ADP_C_113 _jana_atom_site_ADP_C_122 _jana_atom_site_ADP_C_123 _jana_atom_site_ADP_C_133 _jana_atom_site_ADP_C_222 _jana_atom_site_ADP_C_223 _jana_atom_site_ADP_C_233 _jana_atom_site_ADP_C_333 ? ? ? ? ? ? ? ? ? ? ? ? loop_ _jana_atom_site_ADP_D_label _jana_atom_site_ADP_D_type_symbol _jana_atom_site_ADP_D_1111 _jana_atom_site_ADP_D_1112 _jana_atom_site_ADP_D_1113 _jana_atom_site_ADP_D_1122 _jana_atom_site_ADP_D_1123 _jana_atom_site_ADP_D_1133 _jana_atom_site_ADP_D_1222 _jana_atom_site_ADP_D_1223 _jana_atom_site_ADP_D_1233 _jana_atom_site_ADP_D_1333 _jana_atom_site_ADP_D_2222 _jana_atom_site_ADP_D_2223 _jana_atom_site_ADP_D_2233 _jana_atom_site_ADP_D_2333 _jana_atom_site_ADP_D_3333 ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? loop_ _jana_atom_site_ADP_E_label _jana_atom_site_ADP_E_type_symbol _jana_atom_site_ADP_E_11111 _jana_atom_site_ADP_E_11112 _jana_atom_site_ADP_E_11113 _jana_atom_site_ADP_E_11122 _jana_atom_site_ADP_E_11123 _jana_atom_site_ADP_E_11133 _jana_atom_site_ADP_E_11222 _jana_atom_site_ADP_E_11223 _jana_atom_site_ADP_E_11233 _jana_atom_site_ADP_E_11333 _jana_atom_site_ADP_E_12222 _jana_atom_site_ADP_E_12223 _jana_atom_site_ADP_E_12233 _jana_atom_site_ADP_E_12333 _jana_atom_site_ADP_E_13333 _jana_atom_site_ADP_E_22222 _jana_atom_site_ADP_E_22223 _jana_atom_site_ADP_E_22233 _jana_atom_site_ADP_E_22333 _jana_atom_site_ADP_E_23333 _jana_atom_site_ADP_E_33333 ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? loop_ _jana_atom_site_ADP_F_label _jana_atom_site_ADP_F_type_symbol _jana_atom_site_ADP_F_111111 _jana_atom_site_ADP_F_111112 _jana_atom_site_ADP_F_111113 _jana_atom_site_ADP_F_111122 _jana_atom_site_ADP_F_111123 _jana_atom_site_ADP_F_111133 _jana_atom_site_ADP_F_111222 _jana_atom_site_ADP_F_111223 _jana_atom_site_ADP_F_111233 _jana_atom_site_ADP_F_111333 _jana_atom_site_ADP_F_112222 _jana_atom_site_ADP_F_112223 _jana_atom_site_ADP_F_112233 _jana_atom_site_ADP_F_112333 _jana_atom_site_ADP_F_113333 _jana_atom_site_ADP_F_122222 _jana_atom_site_ADP_F_122223 _jana_atom_site_ADP_F_122233 _jana_atom_site_ADP_F_122333 _jana_atom_site_ADP_F_123333 _jana_atom_site_ADP_F_133333 _jana_atom_site_ADP_F_222222 _jana_atom_site_ADP_F_222223 _jana_atom_site_ADP_F_222233 _jana_atom_site_ADP_F_222333 _jana_atom_site_ADP_F_223333 _jana_atom_site_ADP_F_233333 _jana_atom_site_ADP_F_333333 ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? ? #======================================================================= # 10. MOLECULAR GEOMETRY loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag O1 C1 . . 1.340(4) ? O1 C15 . . 1.463(5) ? C1 O2 . . 1.198(5) ? C1 C2 . . 1.535(3) ? C2 O3 . . 1.432(3) ? C2 C3 . . 1.547(4) ? C2 C9 . . 1.535(4) ? O3 H1o3 . . 0.86 ? C3 C4 . . 1.376(6) ? C3 C8 . . 1.397(4) ? C4 C5 . . 1.390(10) ? C4 H1c4 . . 0.96 ? C5 C6 . . 1.367(6) ? C5 H1c5 . . 0.96 ? C6 C7 . . 1.375(8) ? C6 H1c6 . . 0.96 ? C7 C8 . . 1.389(9) ? C7 H1c7 . . 0.96 ? C8 H1c8 . . 0.96 ? C9 C10 . . 1.377(5) ? C9 C14 . . 1.388(5) ? C10 C11 . . 1.395(4) ? C10 H1c10 . . 0.96 ? C11 C12 . . 1.376(7) ? C11 H1c11 . . 0.96 ? C12 C13 . . 1.365(8) ? C12 H1c12 . . 0.96 ? C13 C14 . . 1.397(4) ? C13 H1c13 . . 0.96 ? C14 H1c14 . . 0.96 ? C15 C16 . . 1.527(6) ? C15 C19 . . 1.520(6) ? C15 H1c15 . . 0.96 ? C16 C17 . . 1.518(6) ? C16 H1c16 . . 0.96 ? C16 H2c16 . . 0.96 ? C17 N1 . . 1.534(4) ? C17 C21 . . 1.531(7) ? C17 H1c17 . . 0.96 ? N1 C18 . . 1.526(4) ? N1 C22 . . 1.508(5) ? N1 C25 . . 1.516(4) ? C18 C19 . . 1.521(6) ? C18 C20 . . 1.524(7) ? C18 H1c18 . . 0.96 ? C19 H1c19 . . 0.96 ? C19 H2c19 . . 0.96 ? C20 C21 . . 1.549(7) ? C20 H1c20 . . 0.96 ? C20 H2c20 . . 0.96 ? C21 H1c21 . . 0.96 ? C21 H2c21 . . 0.96 ? C22 C23 . . 1.515(5) ? C22 H1c22 . . 0.96 ? C22 H2c22 . . 0.96 ? C23 C24 . . 1.544(7) ? C23 H1c23 . . 0.96 ? C23 H2c23 . . 0.96 ? C24 C25 . . 1.512(6) ? C24 H1c24 . . 0.96 ? C24 H2c24 . . 0.96 ? C25 H1c25 . . 0.96 ? C25 H2c25 . . 0.96 ? O4 C26 . . 1.231(5) ? O5 C26 . . 1.327(5) ? O5 H1o5 . . 0.86 ? C26 C27 . . 1.512(6) ? C27 C28 . . 1.527(4) ? C27 H1c27 . . 0.96 ? C27 H2c27 . . 0.96 ? C28 C28 . 3_675 1.542(4) ? C28 H1c28 . . 0.96 ? C28 H2c28 . . 0.96 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_2 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C1 O1 C15 . . . 117.6(3) ? O1 C1 O2 . . . 124.4(3) ? O1 C1 C2 . . . 108.7(2) ? O2 C1 C2 . . . 126.7(3) ? C1 C2 O3 . . . 109.29(17) ? C1 C2 C3 . . . 107.21(19) ? C1 C2 C9 . . . 114.4(2) ? O3 C2 C3 . . . 108.1(2) ? O3 C2 C9 . . . 110.47(19) ? C3 C2 C9 . . . 107.1(2) ? C2 O3 H1o3 . . . 120 ? C2 C3 C4 . . . 122.9(3) ? C2 C3 C8 . . . 117.8(3) ? C4 C3 C8 . . . 119.1(4) ? C3 C4 C5 . . . 120.8(3) ? C3 C4 H1c4 . . . 119.62 ? C5 C4 H1c4 . . . 119.62 ? C4 C5 C6 . . . 119.7(5) ? C4 C5 H1c5 . . . 120.13 ? C6 C5 H1c5 . . . 120.13 ? C5 C6 C7 . . . 120.4(6) ? C5 C6 H1c6 . . . 119.81 ? C7 C6 H1c6 . . . 119.81 ? C6 C7 C8 . . . 120.3(4) ? C6 C7 H1c7 . . . 119.84 ? C8 C7 H1c7 . . . 119.84 ? C3 C8 C7 . . . 119.6(4) ? C3 C8 H1c8 . . . 120.22 ? C7 C8 H1c8 . . . 120.22 ? C2 C9 C10 . . . 123.3(2) ? C2 C9 C14 . . . 118.0(2) ? C10 C9 C14 . . . 118.5(3) ? C9 C10 C11 . . . 120.3(4) ? C9 C10 H1c10 . . . 119.84 ? C11 C10 H1c10 . . . 119.83 ? C10 C11 C12 . . . 120.9(5) ? C10 C11 H1c11 . . . 119.54 ? C12 C11 H1c11 . . . 119.54 ? C11 C12 C13 . . . 119.0(3) ? C11 C12 H1c12 . . . 120.52 ? C13 C12 H1c12 . . . 120.52 ? C12 C13 C14 . . . 120.7(4) ? C12 C13 H1c13 . . . 119.66 ? C14 C13 H1c13 . . . 119.66 ? C9 C14 C13 . . . 120.5(4) ? C9 C14 H1c14 . . . 119.76 ? C13 C14 H1c14 . . . 119.76 ? O1 C15 C16 . . . 109.3(3) ? O1 C15 C19 . . . 106.6(4) ? O1 C15 H1c15 . . . 112.67 ? C16 C15 C19 . . . 112.8(3) ? C16 C15 H1c15 . . . 106.43 ? C19 C15 H1c15 . . . 109.12 ? C15 C16 C17 . . . 113.5(3) ? C15 C16 H1c16 . . . 109.47 ? C15 C16 H2c16 . . . 109.47 ? C17 C16 H1c16 . . . 109.47 ? C17 C16 H2c16 . . . 109.47 ? H1c16 C16 H2c16 . . . 105.12 ? C16 C17 N1 . . . 108.2(3) ? C16 C17 C21 . . . 113.6(3) ? C16 C17 H1c17 . . . 105.62 ? N1 C17 C21 . . . 102.8(3) ? N1 C17 H1c17 . . . 116.01 ? C21 C17 H1c17 . . . 110.81 ? C17 N1 C18 . . . 100.0(2) ? C17 N1 C22 . . . 117.9(3) ? C17 N1 C25 . . . 111.0(3) ? C18 N1 C22 . . . 114.7(3) ? C18 N1 C25 . . . 112.9(3) ? C22 N1 C25 . . . 100.9(3) ? N1 C18 C19 . . . 108.2(3) ? N1 C18 C20 . . . 102.2(3) ? N1 C18 H1c18 . . . 116.58 ? C19 C18 C20 . . . 114.2(3) ? C19 C18 H1c18 . . . 105.15 ? C20 C18 H1c18 . . . 110.8 ? C15 C19 C18 . . . 113.4(3) ? C15 C19 H1c19 . . . 109.47 ? C15 C19 H2c19 . . . 109.47 ? C18 C19 H1c19 . . . 109.47 ? C18 C19 H2c19 . . . 109.47 ? H1c19 C19 H2c19 . . . 105.22 ? C18 C20 C21 . . . 105.8(3) ? C18 C20 H1c20 . . . 109.47 ? C18 C20 H2c20 . . . 109.47 ? C21 C20 H1c20 . . . 109.47 ? C21 C20 H2c20 . . . 109.47 ? H1c20 C20 H2c20 . . . 112.94 ? C17 C21 C20 . . . 104.3(3) ? C17 C21 H1c21 . . . 109.47 ? C17 C21 H2c21 . . . 109.47 ? C20 C21 H1c21 . . . 109.47 ? C20 C21 H2c21 . . . 109.47 ? H1c21 C21 H2c21 . . . 114.15 ? N1 C22 C23 . . . 104.1(3) ? N1 C22 H1c22 . . . 109.47 ? N1 C22 H2c22 . . . 109.47 ? C23 C22 H1c22 . . . 109.47 ? C23 C22 H2c22 . . . 109.47 ? H1c22 C22 H2c22 . . . 114.38 ? C22 C23 C24 . . . 104.5(3) ? C22 C23 H1c23 . . . 109.47 ? C22 C23 H2c23 . . . 109.47 ? C24 C23 H1c23 . . . 109.47 ? C24 C23 H2c23 . . . 109.47 ? H1c23 C23 H2c23 . . . 114.04 ? C23 C24 C25 . . . 105.5(3) ? C23 C24 H1c24 . . . 109.47 ? C23 C24 H2c24 . . . 109.47 ? C25 C24 H1c24 . . . 109.47 ? C25 C24 H2c24 . . . 109.47 ? H1c24 C24 H2c24 . . . 113.15 ? N1 C25 C24 . . . 105.0(3) ? N1 C25 H1c25 . . . 109.47 ? N1 C25 H2c25 . . . 109.47 ? C24 C25 H1c25 . . . 109.47 ? C24 C25 H2c25 . . . 109.47 ? H1c25 C25 H2c25 . . . 113.6 ? C26 O5 H1o5 . . . 120 ? O4 C26 O5 . . . 123.2(4) ? O4 C26 C27 . . . 124.0(3) ? O5 C26 C27 . . . 112.8(3) ? C26 C27 C28 . . . 114.2(3) ? C26 C27 H1c27 . . . 109.47 ? C26 C27 H2c27 . . . 109.47 ? C28 C27 H1c27 . . . 109.47 ? C28 C27 H2c27 . . . 109.47 ? H1c27 C27 H2c27 . . . 104.31 ? C27 C28 C28 . . 3_675 111.1(2) ? C27 C28 H1c28 . . . 109.47 ? C27 C28 H2c28 . . . 109.47 ? C28 C28 H1c28 3_675 . . 109.47 ? C28 C28 H2c28 3_675 . . 109.47 ? H1c28 C28 H2c28 . . . 107.79 ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag ? ? ? ? ? ? ? ? ? ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_D _geom_hbond_site_symmetry_H _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag C8 H1c8 C1 . . . 0.96 2.45 2.798(7) 101.19 ? C10 H1c10 O3 . . . 0.96 2.45 2.799(4) 101.05 ? C15 H1c15 O2 . . . 0.96 2.34 2.717(4) 102.66 ? C20 H1c20 O1 . . . 0.96 2.45 2.927(5) 110.28 ? C21 H2c21 O1 . . . 0.96 2.48 2.949(5) 110.32 ? O3 H1o3 Cl1 . . 2_645 0.86 2.27 3.071(5) 154.92 ? O5 H1o5 Cl1 . . 2_655 0.86 2.12 2.932(7) 157.20 ? #======================================================================= # 11. POWDER PROFILE loop_ _pd_proc_point_id _pd_proc_2theta_corrected _pd_proc_intensity_net _pd_calc_intensity_net _pd_proc_ls_weight 1 4.0068 20561.00 19892.80 143.39 2 4.0199 20436.00 19786.80 142.96 3 4.0330 20338.00 19682.20 142.61 4 4.0462 20063.00 19579.30 141.64 5 4.0593 20058.00 19478.10 141.63 6 4.0724 20007.00 19378.70 141.45 7 4.0856 19743.00 19281.10 140.51 8 4.0987 19500.00 19185.30 139.64 9 4.1118 19519.00 19091.30 139.71 10 4.1249 19154.00 18998.90 138.40 11 4.1381 19218.00 18908.30 138.63 12 4.1512 19294.00 18819.40 138.90 13 4.1643 18807.00 18732.00 137.14 14 4.1775 18761.00 18646.30 136.97 15 4.1906 18443.00 18562.20 135.80 16 4.2037 18391.00 18479.60 135.61 17 4.2169 17986.00 18398.50 134.11 18 4.2300 18009.00 18318.90 134.20 19 4.2431 17734.00 18240.80 133.17 20 4.2562 17677.00 18164.10 132.96 21 4.2694 17630.00 18088.90 132.78 22 4.2825 17643.00 18015.10 132.83 23 4.2956 17548.00 17942.60 132.47 24 4.3088 17368.00 17871.50 131.79 25 4.3219 17271.00 17801.70 131.42 26 4.3350 17307.00 17733.20 131.56 27 4.3482 17401.00 17666.00 131.91 28 4.3613 17419.00 17600.10 131.98 29 4.3744 17082.00 17535.40 130.70 30 4.3875 17045.00 17472.00 130.56 31 4.4007 17160.00 17409.70 131.00 32 4.4138 17009.00 17348.60 130.42 33 4.4269 17143.00 17288.70 130.93 34 4.4401 16828.00 17229.90 129.72 35 4.4532 17067.00 17172.30 130.64 36 4.4663 16823.00 17115.10 129.70 37 4.4795 16809.00 17059.40 129.65 38 4.4926 16537.00 17005.00 128.60 39 4.5057 16826.00 16951.70 129.71 40 4.5189 16676.00 16899.40 129.14 41 4.5320 16610.00 16848.10 128.88 42 4.5451 16558.00 16797.80 128.68 43 4.5582 16469.00 16748.50 128.33 44 4.5714 16348.00 16700.10 127.86 45 4.5845 16480.00 16652.70 128.37 46 4.5976 16533.00 16606.20 128.58 47 4.6108 16494.00 16560.60 128.43 48 4.6239 16506.00 16515.90 128.48 49 4.6370 16393.00 16472.10 128.04 50 4.6502 16395.00 16429.10 128.04 51 4.6633 16108.00 16386.90 126.92 52 4.6764 16120.00 16345.60 126.96 53 4.6895 16119.00 16305.10 126.96 54 4.7027 16055.00 16265.40 126.71 55 4.7158 16547.00 16226.50 128.63 56 4.7289 15873.00 16188.40 125.99 57 4.7421 16215.00 16151.00 127.34 58 4.7552 16024.00 16114.30 126.59 59 4.7683 15945.00 16078.30 126.27 60 4.7815 16332.00 16043.10 127.80 61 4.7946 16035.00 16008.60 126.63 62 4.8077 15989.00 15974.70 126.45 63 4.8208 15856.00 15941.50 125.92 64 4.8340 15762.00 15909.00 125.55 65 4.8471 15857.00 15877.10 125.93 66 4.8602 16001.00 15845.90 126.50 67 4.8734 16023.00 15815.20 126.58 68 4.8865 15911.00 15785.20 126.14 69 4.8996 15884.00 15755.70 126.03 70 4.9128 16058.00 15726.90 126.72 71 4.9259 15698.00 15698.60 125.29 72 4.9390 15567.00 15670.80 124.77 73 4.9522 15772.00 15643.60 125.59 74 4.9653 15685.00 15617.00 125.24 75 4.9784 15693.00 15590.80 125.27 76 4.9915 15685.00 15565.20 125.24 77 5.0047 15696.00 15540.10 125.28 78 5.0178 15656.00 15515.40 125.12 79 5.0309 15766.00 15491.30 125.56 80 5.0441 15603.00 15467.60 124.91 81 5.0572 15341.00 15444.30 123.86 82 5.0703 15478.00 15421.50 124.41 83 5.0835 15550.00 15399.20 124.70 84 5.0966 15470.00 15377.30 124.38 85 5.1097 15593.00 15355.80 124.87 86 5.1228 15413.00 15334.70 124.15 87 5.1360 15759.00 15314.00 125.54 88 5.1491 15582.00 15293.70 124.83 89 5.1622 15600.00 15273.70 124.90 90 5.1754 15420.00 15254.20 124.18 91 5.1885 15483.00 15235.00 124.43 92 5.2016 15510.00 15216.10 124.54 93 5.2148 15481.00 15197.60 124.42 94 5.2279 15339.00 15179.50 123.85 95 5.2410 15416.00 15161.70 124.16 96 5.2541 15109.00 15144.20 122.92 97 5.2673 15370.00 15127.00 123.98 98 5.2804 15378.00 15110.10 124.01 99 5.2935 15139.00 15093.50 123.04 100 5.3067 15034.00 15077.20 122.61 101 5.3198 15347.00 15061.10 123.88 102 5.3329 15303.00 15045.40 123.71 103 5.3461 15225.00 15029.90 123.39 104 5.3592 15147.00 15014.70 123.07 105 5.3723 15206.00 14999.70 123.31 106 5.3854 15071.00 14985.00 122.76 107 5.3986 15168.00 14970.50 123.16 108 5.4117 15106.00 14956.30 122.91 109 5.4248 14972.00 14942.30 122.36 110 5.4380 15113.00 14928.50 122.93 111 5.4511 15222.00 14914.90 123.38 112 5.4642 15213.00 14901.50 123.34 113 5.4774 14878.00 14888.30 121.97 114 5.4905 15011.00 14875.30 122.52 115 5.5036 14856.00 14862.50 121.89 116 5.5168 14964.00 14849.90 122.33 117 5.5299 14955.00 14837.50 122.29 118 5.5430 14997.00 14825.20 122.46 119 5.5561 15056.00 14813.10 122.70 120 5.5693 14913.00 14801.20 122.12 121 5.5824 14904.00 14789.40 122.08 122 5.5955 14867.00 14777.80 121.93 123 5.6087 15108.00 14766.30 122.92 124 5.6218 14981.00 14755.00 122.40 125 5.6349 14843.00 14743.80 121.83 126 5.6481 14894.00 14732.80 122.04 127 5.6612 14874.00 14721.80 121.96 128 5.6743 14660.00 14711.00 121.08 129 5.6874 14873.00 14700.30 121.96 130 5.7006 14665.00 14689.70 121.10 131 5.7137 14711.00 14679.30 121.29 132 5.7268 14707.00 14668.90 121.27 133 5.7400 14913.00 14658.60 122.12 134 5.7531 14846.00 14648.50 121.84 135 5.7662 14767.00 14638.40 121.52 136 5.7794 14657.00 14628.40 121.07 137 5.7925 14578.00 14618.50 120.74 138 5.8056 14627.00 14608.70 120.94 139 5.8187 14832.00 14599.00 121.79 140 5.8319 14491.00 14589.30 120.38 141 5.8450 14602.00 14579.70 120.84 142 5.8581 14699.00 14570.20 121.24 143 5.8713 14366.00 14560.70 119.86 144 5.8844 14770.00 14551.40 121.53 145 5.8975 14375.00 14542.00 119.90 146 5.9107 14824.00 14532.70 121.75 147 5.9238 14396.00 14523.50 119.98 148 5.9369 14475.00 14514.40 120.31 149 5.9501 14469.00 14505.20 120.29 150 5.9632 14502.00 14496.10 120.42 151 5.9763 14524.00 14487.10 120.52 152 5.9894 14654.00 14478.10 121.05 153 6.0026 14488.00 14469.10 120.37 154 6.0157 14774.00 14460.20 121.55 155 6.0288 14229.00 14451.30 119.29 156 6.0420 14566.00 14442.50 120.69 157 6.0551 14552.00 14433.60 120.63 158 6.0682 14585.00 14424.80 120.77 159 6.0814 14155.00 14416.00 118.97 160 6.0945 14242.00 14407.20 119.34 161 6.1076 14332.00 14398.50 119.72 162 6.1207 14350.00 14389.80 119.79 163 6.1339 14281.00 14381.00 119.50 164 6.1470 14065.00 14372.30 118.60 165 6.1601 14088.00 14363.70 118.69 166 6.1733 14411.00 14355.00 120.05 167 6.1864 14441.00 14346.30 120.17 168 6.1995 14352.00 14337.60 119.80 169 6.2127 14206.00 14329.00 119.19 170 6.2258 14294.00 14320.30 119.56 171 6.2389 14427.00 14311.60 120.11 172 6.2520 14397.00 14303.00 119.99 173 6.2652 14243.00 14294.30 119.34 174 6.2783 14197.00 14285.70 119.15 175 6.2914 14159.00 14277.00 118.99 176 6.3046 13994.00 14268.30 118.30 177 6.3177 14157.00 14259.60 118.98 178 6.3308 14111.00 14251.00 118.79 179 6.3440 14114.00 14242.30 118.80 180 6.3571 14215.00 14233.60 119.23 181 6.3702 14349.00 14224.80 119.79 182 6.3834 14046.00 14216.10 118.52 183 6.3965 14097.00 14207.40 118.73 184 6.4096 13985.00 14198.60 118.26 185 6.4227 13998.00 14189.90 118.31 186 6.4359 14132.00 14181.10 118.88 187 6.4490 13780.00 14172.30 117.39 188 6.4621 14005.00 14163.50 118.34 189 6.4753 13932.00 14154.70 118.03 190 6.4884 14179.00 14145.80 119.08 191 6.5015 14066.00 14137.00 118.60 192 6.5147 14008.00 14128.10 118.36 193 6.5278 14008.00 14119.20 118.36 194 6.5409 14035.00 14110.30 118.47 195 6.5540 14193.00 14101.30 119.13 196 6.5672 13941.00 14092.40 118.07 197 6.5803 13957.00 14083.40 118.14 198 6.5934 13810.00 14074.40 117.52 199 6.6066 13957.00 14065.40 118.14 200 6.6197 13871.00 14056.30 117.78 201 6.6328 13870.00 14047.30 117.77 202 6.6460 13881.00 14038.20 117.82 203 6.6591 13885.00 14029.10 117.83 204 6.6722 13997.00 14019.90 118.31 205 6.6853 13875.00 14010.80 117.79 206 6.6985 13877.00 14001.60 117.80 207 6.7116 14055.00 13992.40 118.55 208 6.7247 13769.00 13983.20 117.34 209 6.7379 13797.00 13973.90 117.46 210 6.7510 13973.00 13964.60 118.21 211 6.7641 13886.00 13955.30 117.84 212 6.7773 13684.00 13946.00 116.98 213 6.7904 13876.00 13936.70 117.80 214 6.8035 13837.00 13927.30 117.63 215 6.8167 13776.00 13917.90 117.37 216 6.8298 13636.00 13908.50 116.77 217 6.8429 13984.00 13899.10 118.25 218 6.8560 13694.00 13889.60 117.02 219 6.8692 13802.00 13880.10 117.48 220 6.8823 13892.00 13870.60 117.86 221 6.8954 13823.00 13861.10 117.57 222 6.9086 13855.00 13851.60 117.71 223 6.9217 14097.00 13842.00 118.73 224 6.9348 13942.00 13832.40 118.08 225 6.9480 13708.00 13822.80 117.08 226 6.9611 13854.00 13813.20 117.70 227 6.9742 13786.00 13803.50 117.41 228 6.9873 13807.00 13793.80 117.50 229 7.0005 13811.00 13895.70 117.52 230 7.0136 13798.00 13944.80 117.46 231 7.0267 13501.00 13942.30 116.19 232 7.0399 13648.00 13940.10 116.82 233 7.0530 13719.00 13938.50 117.13 234 7.0661 13518.00 13937.40 116.27 235 7.0793 13899.00 13936.90 117.89 236 7.0924 13843.00 13937.00 117.66 237 7.1055 13687.00 13937.80 116.99 238 7.1186 13831.00 13939.40 117.61 239 7.1318 13626.00 13941.80 116.73 240 7.1449 13662.00 13945.20 116.89 241 7.1580 13551.00 13949.60 116.41 242 7.1712 13766.00 13955.20 117.33 243 7.1843 13720.00 13962.10 117.13 244 7.1974 13824.00 13970.40 117.58 245 7.2106 13740.00 13980.30 117.22 246 7.2237 13518.00 13992.00 116.27 247 7.2368 13816.00 14005.80 117.54 248 7.2500 13619.00 14021.90 116.70 249 7.2631 13816.00 14040.60 117.54 250 7.2762 13818.00 14062.30 117.55 251 7.2893 13988.00 14087.40 118.27 252 7.3025 13899.00 14116.40 117.89 253 7.3156 13957.00 14150.00 118.14 254 7.3287 14255.00 14188.90 119.39 255 7.3419 14276.00 14233.90 119.48 256 7.3550 14402.00 14286.60 120.01 257 7.3681 14393.00 14347.80 119.97 258 7.3813 14283.00 14419.60 119.51 259 7.3944 14211.00 14504.60 119.21 260 7.4075 14722.00 14606.90 121.33 261 7.4206 14528.00 14732.90 120.53 262 7.4338 14996.00 14892.60 122.46 263 7.4469 15523.00 15101.50 124.59 264 7.4600 15639.00 15383.20 125.06 265 7.4732 16362.00 15770.90 127.91 266 7.4863 17284.00 16307.20 131.47 267 7.4994 18081.00 17041.60 134.47 268 7.5126 19705.00 18031.40 140.37 269 7.5257 21321.00 19363.10 146.02 270 7.5388 23748.00 21223.60 154.10 271 7.5519 26998.00 24006.80 164.31 272 7.5651 31015.00 28297.10 176.11 273 7.5782 36323.00 34522.00 190.59 274 7.5913 44113.00 42578.40 210.03 275 7.6045 53884.00 52511.50 232.13 276 7.6176 68758.00 66331.40 262.22 277 7.6307 90822.00 87684.50 301.37 278 7.6439 119780.00 115643.00 346.09 279 7.6570 144137.00 138552.00 379.65 280 7.6701 143821.00 142001.00 379.24 281 7.6832 120710.00 122774.00 347.43 282 7.6964 89710.00 90796.80 299.52 283 7.7095 59609.00 59710.90 244.15 284 7.7226 37714.00 37487.20 194.20 285 7.7358 25565.00 24855.40 159.89 286 7.7489 20194.00 18856.50 142.11 287 7.7620 17606.00 16371.60 132.69 288 7.7752 16556.00 15452.70 128.67 289 7.7883 15815.00 15156.10 125.76 290 7.8014 15379.00 15070.70 124.01 291 7.8146 14808.00 15024.30 121.69 292 7.8277 14486.00 14954.10 120.36 293 7.8408 14286.00 14848.80 119.52 294 7.8539 14059.00 14718.10 118.57 295 7.8671 14010.00 14576.40 118.36 296 7.8802 13683.00 14435.50 116.97 297 7.8933 13720.00 14302.70 117.13 298 7.9065 13667.00 14181.70 116.91 299 7.9196 13515.00 14073.30 116.25 300 7.9327 13420.00 13977.00 115.85 301 7.9459 13601.00 13891.60 116.62 302 7.9590 13352.00 13815.90 115.55 303 7.9721 13158.00 13748.60 114.71 304 7.9852 13444.00 13688.70 115.95 305 7.9984 13261.00 13635.50 115.16 306 8.0115 13462.00 13588.30 116.03 307 8.0246 13229.00 13547.40 115.02 308 8.0378 13304.00 13513.00 115.34 309 8.0509 13386.00 13485.90 115.70 310 8.0640 13305.00 13466.20 115.35 311 8.0772 13451.00 13453.40 115.98 312 8.0903 13184.00 13447.00 114.82 313 8.1034 13245.00 13449.70 115.09 314 8.1165 13367.00 13467.10 115.62 315 8.1297 13425.00 13503.90 115.87 316 8.1428 13431.00 13553.10 115.89 317 8.1559 13495.00 13591.40 116.17 318 8.1691 13453.00 13591.20 115.99 319 8.1822 13566.00 13540.10 116.47 320 8.1953 13453.00 13448.50 115.99 321 8.2085 13405.00 13340.50 115.78 322 8.2216 13381.00 13239.70 115.68 323 8.2347 13367.00 13159.20 115.62 324 8.2479 13250.00 13101.00 115.11 325 8.2610 13025.00 13060.60 114.13 326 8.2741 13179.00 13031.80 114.80 327 8.2872 13138.00 13009.70 114.62 328 8.3004 13047.00 12991.10 114.22 329 8.3135 13075.00 12868.50 114.35 330 8.3266 13085.00 12803.60 114.39 331 8.3398 12948.00 12794.60 113.79 332 8.3529 12908.00 12785.60 113.61 333 8.3660 12922.00 12776.60 113.68 334 8.3792 13044.00 12767.60 114.21 335 8.3923 13091.00 12758.50 114.42 336 8.4054 12884.00 12749.50 113.51 337 8.4185 12857.00 12740.50 113.39 338 8.4317 12915.00 12731.60 113.64 339 8.4448 12824.00 12722.70 113.24 340 8.4579 12704.00 12713.90 112.71 341 8.4711 12948.00 12705.20 113.79 342 8.4842 12923.00 12696.50 113.68 343 8.4973 12873.00 12687.80 113.46 344 8.5105 12643.00 12679.30 112.44 345 8.5236 12684.00 12670.80 112.62 346 8.5367 12682.00 12662.30 112.61 347 8.5498 12767.00 12653.90 112.99 348 8.5630 12693.00 12645.60 112.66 349 8.5761 12822.00 12637.30 113.23 350 8.5892 12872.00 12629.00 113.46 351 8.6024 12748.00 12620.80 112.91 352 8.6155 12796.00 12612.70 113.12 353 8.6286 12738.00 12604.60 112.86 354 8.6418 12864.00 12596.60 113.42 355 8.6549 12806.00 12588.50 113.16 356 8.6680 12847.00 12580.60 113.35 357 8.6812 12701.00 12572.70 112.70 358 8.6943 12693.00 12564.80 112.66 359 8.7074 12762.00 12557.00 112.97 360 8.7205 12815.00 12549.20 113.20 361 8.7337 12574.00 12541.50 112.13 362 8.7468 12850.00 12533.80 113.36 363 8.7599 12711.00 12526.10 112.74 364 8.7731 12479.00 12518.50 111.71 365 8.7862 12746.00 12511.00 112.90 366 8.7993 12574.00 12503.50 112.13 367 8.8125 12793.00 12496.00 113.11 368 8.8256 12633.00 12488.60 112.40 369 8.8387 12677.00 12481.20 112.59 370 8.8518 12703.00 12473.90 112.71 371 8.8650 12612.00 12466.60 112.30 372 8.8781 12489.00 12459.30 111.75 373 8.8912 12612.00 12452.10 112.30 374 8.9044 12743.00 12445.00 112.89 375 8.9175 12534.00 12437.90 111.96 376 8.9306 12323.00 12430.80 111.01 377 8.9438 12453.00 12423.70 111.59 378 8.9569 12706.00 12416.40 112.72 379 8.9700 12608.00 12409.50 112.29 380 8.9831 12385.00 12402.40 111.29 381 8.9963 12338.00 12395.60 111.08 382 9.0094 12502.00 12388.80 111.81 383 9.0225 12456.00 12382.00 111.61 384 9.0357 12419.00 12375.40 111.44 385 9.0488 12537.00 12368.70 111.97 386 9.0619 12405.00 12362.10 111.38 387 9.0751 12398.00 12355.50 111.35 388 9.0882 12364.00 12348.90 111.19 389 9.1013 12588.00 12342.40 112.20 390 9.1145 12590.00 12336.00 112.21 391 9.1276 12325.00 12329.50 111.02 392 9.1407 12427.00 12323.20 111.48 393 9.1538 12616.00 12316.80 112.32 394 9.1670 12316.00 12310.50 110.98 395 9.1801 12387.00 12304.30 111.30 396 9.1932 12512.00 12298.10 111.86 397 9.2064 12380.00 12291.90 111.26 398 9.2195 12362.00 12285.80 111.18 399 9.2326 12370.00 12279.70 111.22 400 9.2458 12421.00 12273.60 111.45 401 9.2589 12290.00 12267.60 110.86 402 9.2720 12429.00 12261.70 111.49 403 9.2851 12116.00 12255.70 110.07 404 9.2983 12265.00 12249.80 110.75 405 9.3114 12211.00 12244.00 110.50 406 9.3245 12049.00 12238.20 109.77 407 9.3377 12252.00 12232.40 110.69 408 9.3508 12331.00 12226.70 111.04 409 9.3639 12237.00 12221.00 110.62 410 9.3771 12284.00 12215.40 110.83 411 9.3902 12315.00 12209.80 110.97 412 9.4033 12198.00 12204.20 110.44 413 9.4164 12266.00 12198.70 110.75 414 9.4296 12267.00 12193.20 110.76 415 9.4427 12219.00 12187.70 110.54 416 9.4558 12305.00 12182.30 110.93 417 9.4690 12200.00 12176.90 110.45 418 9.4821 12167.00 12171.60 110.30 419 9.4952 12237.00 12166.30 110.62 420 9.5084 12468.00 12161.00 111.66 421 9.5215 12048.00 12155.80 109.76 422 9.5346 12161.00 12150.60 110.28 423 9.5478 12179.00 12145.50 110.36 424 9.5609 12105.00 12140.40 110.02 425 9.5740 12205.00 12135.30 110.48 426 9.5871 12187.00 12130.30 110.39 427 9.6003 12173.00 12125.30 110.33 428 9.6134 12176.00 12120.40 110.35 429 9.6265 12146.00 12115.50 110.21 430 9.6397 12458.00 12110.60 111.61 431 9.6528 12228.00 12105.80 110.58 432 9.6659 12435.00 12101.10 111.51 433 9.6791 12391.00 12096.40 111.32 434 9.6922 12235.00 12091.90 110.61 435 9.7053 12089.00 12087.40 109.95 436 9.7184 12321.00 12083.00 111.00 437 9.7316 12244.00 12078.90 110.65 438 9.7447 12028.00 12075.10 109.67 439 9.7578 11995.00 12071.60 109.52 440 9.7710 11990.00 12068.40 109.50 441 9.7841 12088.00 12065.70 109.94 442 9.7972 12222.00 12063.60 110.55 443 9.8104 12051.00 12062.50 109.78 444 9.8235 12184.00 12062.30 110.38 445 9.8366 12073.00 12062.50 109.88 446 9.8497 11986.00 12061.50 109.48 447 9.8629 11943.00 12058.00 109.28 448 9.8760 12164.00 12051.50 110.29 449 9.8891 12108.00 12042.80 110.04 450 9.9023 11971.00 12033.30 109.41 451 9.9154 12027.00 12024.10 109.67 452 9.9285 12007.00 12016.10 109.58 453 9.9417 12018.00 12009.30 109.63 454 9.9548 11932.00 12003.60 109.23 455 9.9679 11846.00 11998.60 108.84 456 9.9810 11807.00 11994.00 108.66 457 9.9942 11907.00 11989.70 109.12 458 10.0073 11819.00 11985.50 108.71 459 10.0204 11992.00 11981.30 109.51 460 10.0336 11889.00 11977.30 109.04 461 10.0467 12025.00 11994.30 109.66 462 10.0598 11974.00 11991.20 109.43 463 10.0730 11980.00 11998.50 109.45 464 10.0861 11768.00 11996.10 108.48 465 10.0992 11918.00 11993.70 109.17 466 10.1124 11879.00 11991.50 108.99 467 10.1255 11972.00 11989.50 109.42 468 10.1386 11902.00 11987.60 109.10 469 10.1517 12210.00 11985.80 110.50 470 10.1649 11864.00 11984.30 108.92 471 10.1780 12163.00 11983.00 110.29 472 10.1911 11958.00 11981.90 109.35 473 10.2043 11937.00 11981.00 109.26 474 10.2174 12091.00 11980.40 109.96 475 10.2305 11882.00 11980.20 109.00 476 10.2437 11882.00 11980.20 109.00 477 10.2568 12026.00 11980.70 109.66 478 10.2699 11773.00 11981.50 108.50 479 10.2830 11853.00 11982.90 108.87 480 10.2962 12057.00 11984.70 109.80 481 10.3093 12005.00 11987.20 109.57 482 10.3224 11899.00 11990.40 109.08 483 10.3356 11850.00 11994.50 108.86 484 10.3487 11822.00 11999.40 108.73 485 10.3618 12113.00 12005.50 110.06 486 10.3750 11858.00 12012.80 108.89 487 10.3881 11781.00 12021.70 108.54 488 10.4012 11909.00 12032.50 109.13 489 10.4143 11860.00 12045.40 108.90 490 10.4275 11866.00 12061.30 108.93 491 10.4406 11758.00 12080.80 108.43 492 10.4537 11879.00 12105.20 108.99 493 10.4669 12014.00 12136.60 109.61 494 10.4800 12003.00 12177.70 109.56 495 10.4931 12050.00 12232.90 109.77 496 10.5063 12336.00 12307.40 111.07 497 10.5194 12223.00 12408.10 110.56 498 10.5325 12428.00 12543.80 111.48 499 10.5457 12752.00 12730.00 112.93 500 10.5588 13017.00 13004.10 114.09 501 10.5719 13541.00 13447.20 116.37 502 10.5850 14161.00 14191.30 119.00 503 10.5982 15208.00 15373.10 123.32 504 10.6113 16771.00 17093.30 129.50 505 10.6244 19404.00 19533.70 139.30 506 10.6376 23107.00 23127.40 152.01 507 10.6507 28825.00 28169.70 169.78 508 10.6638 34657.00 33635.80 186.16 509 10.6770 37877.00 37026.50 194.62 510 10.6901 36097.00 36609.20 189.99 511 10.7032 31972.00 32609.80 178.81 512 10.7163 26057.00 26751.90 161.42 513 10.7295 20129.00 21128.40 141.88 514 10.7426 16086.00 16981.50 126.83 515 10.7557 13997.00 14486.00 118.31 516 10.7689 12920.00 13211.70 113.67 517 10.7820 12408.00 12631.30 111.39 518 10.7951 12181.00 12377.60 110.37 519 10.8083 12357.00 12260.10 111.16 520 10.8214 11973.00 12197.10 109.42 521 10.8345 12019.00 12151.60 109.63 522 10.8476 11984.00 12113.40 109.47 523 10.8608 11849.00 12080.40 108.85 524 10.8739 11826.00 12046.40 108.75 525 10.8870 11794.00 12016.60 108.60 526 10.9002 11897.00 11988.20 109.07 527 10.9133 11887.00 11962.80 109.03 528 10.9264 11819.00 11940.30 108.71 529 10.9396 11748.00 11920.50 108.39 530 10.9527 11746.00 11902.90 108.38 531 10.9658 11672.00 11887.40 108.04 532 10.9790 11898.00 11873.50 109.08 533 10.9921 11806.00 11861.10 108.65 534 11.0052 11619.00 11850.00 107.79 535 11.0183 11811.00 11840.00 108.68 536 11.0315 11796.00 11831.10 108.61 537 11.0446 11659.00 11823.00 107.98 538 11.0577 11785.00 11815.90 108.56 539 11.0709 11699.00 11809.70 108.16 540 11.0840 11721.00 11804.60 108.26 541 11.0971 11814.00 11800.80 108.69 542 11.1103 11649.00 11799.00 107.93 543 11.1234 11683.00 11799.30 108.09 544 11.1365 11698.00 11802.50 108.16 545 11.1496 11904.00 11809.50 109.11 546 11.1628 11823.00 11821.90 108.73 547 11.1759 11604.00 11837.70 107.72 548 11.1890 11757.00 11849.70 108.43 549 11.2022 11694.00 11851.00 108.14 550 11.2153 11805.00 11840.90 108.65 551 11.2284 11516.00 11823.50 107.31 552 11.2416 11601.00 11805.90 107.71 553 11.2547 11738.00 11793.20 108.34 554 11.2678 11588.00 11787.50 107.65 555 11.2809 11677.00 11788.80 108.06 556 11.2941 11576.00 11795.90 107.59 557 11.3072 11617.00 11789.10 107.78 558 11.3203 11700.00 11808.50 108.17 559 11.3335 11841.00 11825.60 108.82 560 11.3466 11721.00 11862.50 108.26 561 11.3597 11655.00 11913.40 107.96 562 11.3729 11661.00 11987.50 107.99 563 11.3860 11920.00 12103.00 109.18 564 11.3991 12031.00 12288.80 109.69 565 11.4123 12309.00 12578.00 110.95 566 11.4254 12421.00 13001.10 111.45 567 11.4385 13039.00 13603.20 114.19 568 11.4516 13504.00 14479.10 116.21 569 11.4648 14386.00 15719.20 119.94 570 11.4779 15184.00 17177.80 123.22 571 11.4910 16251.00 18327.00 127.48 572 11.5042 16755.00 18655.50 129.44 573 11.5173 15975.00 18061.70 126.39 574 11.5304 15442.00 16793.40 124.27 575 11.5436 14342.00 15303.20 119.76 576 11.5567 13263.00 13987.20 115.17 577 11.5698 12385.00 13029.50 111.29 578 11.5829 12313.00 12426.60 110.96 579 11.5961 11703.00 12083.80 108.18 580 11.6092 11779.00 11899.30 108.53 581 11.6223 11806.00 11800.90 108.65 582 11.6355 11737.00 11746.40 108.34 583 11.6486 11728.00 11713.60 108.30 584 11.6617 11573.00 11691.30 107.58 585 11.6749 11855.00 11674.10 108.88 586 11.6880 11680.00 11659.50 108.07 587 11.7011 11681.00 11646.60 108.08 588 11.7142 11511.00 11634.70 107.29 589 11.7274 11502.00 11623.80 107.25 590 11.7405 11706.00 11613.80 108.19 591 11.7536 11620.00 11604.50 107.80 592 11.7668 11399.00 11596.00 106.77 593 11.7799 11384.00 11588.00 106.70 594 11.7930 11628.00 11580.60 107.83 595 11.8062 11631.00 11573.70 107.85 596 11.8193 11427.00 11567.10 106.90 597 11.8324 11475.00 11560.90 107.12 598 11.8455 11381.00 11555.00 106.68 599 11.8587 11367.00 11549.50 106.62 600 11.8718 11314.00 11544.10 106.37 601 11.8849 11508.00 11539.00 107.28 602 11.8981 11461.00 11534.00 107.06 603 11.9112 11426.00 11529.20 106.89 604 11.9243 11566.00 11524.60 107.54 605 11.9375 11594.00 11520.10 107.68 606 11.9506 11385.00 11515.70 106.70 607 11.9637 11413.00 11511.30 106.83 608 11.9769 11499.00 11507.10 107.23 609 11.9900 11533.00 11502.90 107.39 610 12.0031 11451.00 11498.90 107.01 611 12.0162 11446.00 11494.80 106.99 612 12.0294 11293.00 11490.90 106.27 613 12.0425 11378.00 11487.00 106.67 614 12.0556 11435.00 11483.10 106.93 615 12.0688 11585.00 11479.30 107.63 616 12.0819 11547.00 11475.50 107.46 617 12.0950 11644.00 11471.80 107.91 618 12.1082 11385.00 11468.00 106.70 619 12.1213 11571.00 11461.20 107.57 620 12.1344 11436.00 11457.70 106.94 621 12.1475 11321.00 11452.60 106.40 622 12.1607 11301.00 11447.60 106.31 623 12.1738 11535.00 11444.20 107.40 624 12.1869 11551.00 11440.10 107.48 625 12.2001 11509.00 11436.80 107.28 626 12.2132 11563.00 11433.50 107.53 627 12.2263 11299.00 11430.20 106.30 628 12.2395 11475.00 11426.90 107.12 629 12.2526 11400.00 11443.00 106.77 630 12.2657 11617.00 11440.60 107.78 631 12.2788 11627.00 11447.60 107.83 632 12.2920 11424.00 11445.70 106.88 633 12.3051 11524.00 11442.90 107.35 634 12.3182 11506.00 11441.30 107.27 635 12.3314 11594.00 11439.10 107.68 636 12.3445 11486.00 11437.80 107.17 637 12.3576 11640.00 11436.40 107.89 638 12.3708 11562.00 11435.40 107.53 639 12.3839 11519.00 11434.50 107.33 640 12.3970 11532.00 11433.80 107.39 641 12.4102 11567.00 11433.20 107.55 642 12.4233 11507.00 11433.00 107.27 643 12.4364 11382.00 11433.00 106.69 644 12.4495 11436.00 11433.20 106.94 645 12.4627 11484.00 11433.90 107.16 646 12.4758 11264.00 11434.80 106.13 647 12.4889 11400.00 11436.30 106.77 648 12.5021 11283.00 11438.10 106.22 649 12.5152 11455.00 11440.60 107.03 650 12.5283 11355.00 11443.60 106.56 651 12.5415 11501.00 11447.40 107.24 652 12.5546 11329.00 11452.00 106.44 653 12.5677 11296.00 11457.60 106.28 654 12.5808 11505.00 11464.40 107.26 655 12.5940 11469.00 11472.50 107.09 656 12.6071 11366.00 11482.30 106.61 657 12.6202 11669.00 11494.10 108.02 658 12.6334 11395.00 11508.30 106.75 659 12.6465 11568.00 11525.80 107.56 660 12.6596 11510.00 11547.50 107.29 661 12.6728 11389.00 11574.70 106.72 662 12.6859 11579.00 11609.60 107.61 663 12.6990 11685.00 11655.10 108.10 664 12.7121 11425.00 11714.80 106.89 665 12.7253 11812.00 11793.50 108.68 666 12.7384 12051.00 11896.70 109.78 667 12.7515 11815.00 12034.70 108.70 668 12.7647 12087.00 12232.90 109.94 669 12.7778 12541.00 12550.50 111.99 670 12.7909 13032.00 13092.60 114.16 671 12.8041 13810.00 13990.60 117.52 672 12.8172 14997.00 15377.20 122.46 673 12.8303 16811.00 17453.00 129.66 674 12.8435 19333.00 20585.60 139.04 675 12.8566 23511.00 25019.80 153.33 676 12.8697 29489.00 29971.80 171.72 677 12.8828 33111.00 33381.40 181.96 678 12.8960 33328.00 33775.00 182.56 679 12.9091 30614.00 31290.40 174.97 680 12.9222 27076.00 26906.20 164.55 681 12.9354 21561.00 22040.00 146.84 682 12.9485 17635.00 17894.30 132.80 683 12.9616 14682.00 15063.80 121.17 684 12.9748 13101.00 13364.30 114.46 685 12.9879 12615.00 12493.90 112.32 686 13.0010 12247.00 12113.90 110.67 687 13.0141 12103.00 11920.20 110.01 688 13.0273 12067.00 11819.30 109.85 689 13.0404 11818.00 11757.50 108.71 690 13.0535 11847.00 11713.00 108.84 691 13.0667 11684.00 11677.30 108.09 692 13.0798 11775.00 11647.20 108.51 693 13.0929 11576.00 11621.70 107.59 694 13.1061 11733.00 11600.30 108.32 695 13.1192 11675.00 11582.80 108.05 696 13.1323 11504.00 11568.80 107.26 697 13.1454 11856.00 11558.20 108.89 698 13.1586 11738.00 11550.50 108.34 699 13.1717 11719.00 11545.60 108.25 700 13.1848 11718.00 11543.20 108.25 701 13.1980 11474.00 11543.10 107.12 702 13.2111 11756.00 11545.40 108.43 703 13.2242 11681.00 11550.00 108.08 704 13.2374 11570.00 11557.00 107.56 705 13.2505 11754.00 11566.50 108.42 706 13.2636 11836.00 11578.50 108.79 707 13.2768 11677.00 11595.90 108.06 708 13.2899 11539.00 11614.30 107.42 709 13.3030 11637.00 11637.00 107.88 710 13.3161 11648.00 11666.20 107.93 711 13.3293 11659.00 11701.30 107.98 712 13.3424 11693.00 11745.00 108.13 713 13.3555 11618.00 11800.00 107.79 714 13.3687 11809.00 11870.30 108.67 715 13.3818 11739.00 11957.90 108.35 716 13.3949 11985.00 12056.30 109.48 717 13.4081 11962.00 12152.30 109.37 718 13.4212 11976.00 12242.50 109.43 719 13.4343 12163.00 12335.60 110.29 720 13.4474 11956.00 12446.50 109.34 721 13.4606 12248.00 12594.50 110.67 722 13.4737 12354.00 12798.40 111.15 723 13.4868 12456.00 13075.40 111.61 724 13.5000 12925.00 13448.10 113.69 725 13.5131 13174.00 13946.30 114.78 726 13.5262 14292.00 14717.70 119.55 727 13.5394 15392.00 15927.20 124.06 728 13.5525 17171.00 17866.70 131.04 729 13.5656 20178.00 20830.70 142.05 730 13.5787 24710.00 25220.60 157.19 731 13.5919 31439.00 31757.10 177.31 732 13.6050 41158.00 41380.40 202.87 733 13.6181 54239.00 53878.20 232.89 734 13.6313 68103.00 66142.00 260.97 735 13.6444 74877.00 73221.00 273.64 736 13.6575 74473.00 72812.50 272.90 737 13.6707 67665.00 65790.70 260.12 738 13.6838 56171.00 54440.40 237.00 739 13.6969 43078.00 41996.70 207.55 740 13.7100 31471.00 31197.80 177.40 741 13.7232 23777.00 23320.70 154.20 742 13.7363 18576.00 18348.90 136.29 743 13.7494 16094.00 15558.00 126.86 744 13.7626 14626.00 14103.40 120.94 745 13.7757 13597.00 13354.90 116.61 746 13.7888 13224.00 12946.80 115.00 747 13.8020 12850.00 12698.00 113.36 748 13.8151 12709.00 12525.70 112.73 749 13.8282 12509.00 12393.30 111.84 750 13.8414 12398.00 12285.30 111.35 751 13.8545 12247.00 12195.30 110.67 752 13.8676 12016.00 12120.80 109.62 753 13.8807 12416.00 12060.80 111.43 754 13.8939 12009.00 12015.00 109.59 755 13.9070 12085.00 11983.60 109.93 756 13.9201 12077.00 11966.90 109.89 757 13.9333 11913.00 11964.20 109.15 758 13.9464 12298.00 11973.00 110.90 759 13.9595 11878.00 11990.80 108.99 760 13.9727 12019.00 12018.20 109.63 761 13.9858 11844.00 12061.00 108.83 762 13.9989 11991.00 12128.00 109.50 763 14.0120 12169.00 12231.60 110.31 764 14.0252 12349.00 12388.90 111.13 765 14.0383 12531.00 12622.70 111.94 766 14.0514 12888.00 12956.00 113.53 767 14.0646 13164.00 13387.50 114.73 768 14.0777 13517.00 13859.50 116.26 769 14.0908 14036.00 14258.00 118.47 770 14.1040 13970.00 14480.80 118.19 771 14.1171 14114.00 14497.20 118.80 772 14.1302 13937.00 14340.00 118.06 773 14.1433 13708.00 14091.40 117.08 774 14.1565 13508.00 13862.80 116.22 775 14.1696 13334.00 13761.80 115.47 776 14.1827 13769.00 13887.90 117.34 777 14.1959 14537.00 14347.80 120.57 778 14.2090 15516.00 15249.90 124.56 779 14.2221 17122.00 16658.20 130.85 780 14.2353 19108.00 18587.60 138.23 781 14.2484 21425.00 21159.90 146.37 782 14.2615 25132.00 24701.30 158.53 783 14.2747 30121.00 29331.70 173.55 784 14.2878 35634.00 34184.50 188.77 785 14.3009 38400.00 37417.00 195.96 786 14.3140 38384.00 37773.40 195.92 787 14.3272 36188.00 35535.50 190.23 788 14.3403 31901.00 31353.30 178.61 789 14.3534 26702.00 26278.30 163.41 790 14.3666 21676.00 21520.60 147.23 791 14.3797 17833.00 17762.80 133.54 792 14.3928 15154.00 15195.90 123.10 793 14.4060 13990.00 13644.30 118.28 794 14.4191 13167.00 12787.80 114.75 795 14.4322 12589.00 12333.30 112.20 796 14.4453 12505.00 12127.60 111.83 797 14.4585 12313.00 11982.70 110.96 798 14.4716 11983.00 11887.80 109.47 799 14.4847 12198.00 11838.20 110.44 800 14.4979 12235.00 11783.10 110.61 801 14.5110 12172.00 11737.80 110.33 802 14.5241 11928.00 11699.30 109.21 803 14.5373 12126.00 11666.70 110.12 804 14.5504 12002.00 11639.10 109.55 805 14.5635 11908.00 11616.10 109.12 806 14.5766 12165.00 11597.10 110.29 807 14.5898 12123.00 11581.60 110.10 808 14.6029 12227.00 11569.30 110.58 809 14.6160 11957.00 11559.60 109.35 810 14.6292 11793.00 11552.30 108.60 811 14.6423 11954.00 11549.00 109.33 812 14.6554 11827.00 11546.00 108.75 813 14.6686 12006.00 11586.10 109.57 814 14.6817 12053.00 11589.10 109.79 815 14.6948 12372.00 11592.80 111.23 816 14.7080 12044.00 11618.70 109.75 817 14.7211 11935.00 11626.50 109.25 818 14.7342 12332.00 11652.70 111.05 819 14.7473 12031.00 11664.50 109.69 820 14.7605 12230.00 11678.10 110.59 821 14.7736 11858.00 11701.70 108.89 822 14.7867 11840.00 11719.50 108.81 823 14.7999 12054.00 11739.30 109.79 824 14.8130 11867.00 11761.50 108.94 825 14.8261 12025.00 11786.30 109.66 826 14.8393 12058.00 11813.80 109.81 827 14.8524 12090.00 11844.50 109.96 828 14.8655 12041.00 11878.80 109.73 829 14.8786 12096.00 11917.10 109.98 830 14.8918 12143.00 11960.20 110.19 831 14.9049 12219.00 12006.60 110.54 832 14.9180 12254.00 12061.90 110.70 833 14.9312 12224.00 12125.40 110.56 834 14.9443 12268.00 12195.60 110.76 835 14.9574 12375.00 12281.60 111.24 836 14.9706 12428.00 12383.40 111.48 837 14.9837 12638.00 12478.20 112.42 838 14.9968 12404.00 12625.20 111.37 839 15.0099 12676.00 12802.00 112.59 840 15.0231 12910.00 13003.50 113.62 841 15.0362 12916.00 13267.90 113.65 842 15.0493 13333.00 13608.40 115.47 843 15.0625 14073.00 14078.90 118.63 844 15.0756 14475.00 14772.60 120.31 845 15.0887 15866.00 15821.40 125.96 846 15.1019 17449.00 17386.70 132.10 847 15.1150 19711.00 19684.10 140.40 848 15.1281 23118.00 23058.90 152.05 849 15.1413 28399.00 27997.30 168.52 850 15.1544 34978.00 34781.40 187.02 851 15.1675 43150.00 42677.80 207.73 852 15.1806 50277.00 49459.80 224.23 853 15.1938 53809.00 52849.00 231.97 854 15.2069 53232.00 52308.90 230.72 855 15.2200 49137.00 48490.10 221.67 856 15.2332 43619.00 42529.30 208.85 857 15.2463 36520.00 36063.00 191.10 858 15.2594 31481.00 30672.90 177.43 859 15.2726 27943.00 27394.20 167.16 860 15.2857 27255.00 26744.30 165.09 861 15.2988 29253.00 29012.00 171.04 862 15.3119 34541.00 34557.20 185.85 863 15.3251 43260.00 43626.50 207.99 864 15.3382 55229.00 55249.50 235.01 865 15.3513 66752.00 66227.10 258.36 866 15.3645 74505.00 72645.60 272.96 867 15.3776 74607.00 72590.30 273.14 868 15.3907 68638.00 66634.70 261.99 869 15.4039 58303.00 56748.20 241.46 870 15.4170 47015.00 45401.00 216.83 871 15.4301 35348.00 34830.00 188.01 872 15.4432 26733.00 26449.90 163.50 873 15.4564 20974.00 20706.20 144.82 874 15.4695 17473.00 17244.20 132.18 875 15.4826 15762.00 15352.40 125.55 876 15.4958 14783.00 14359.60 121.58 877 15.5089 14008.00 13818.90 118.36 878 15.5220 13966.00 13493.10 118.18 879 15.5352 13517.00 13270.70 116.26 880 15.5483 13380.00 13103.10 115.67 881 15.5614 13124.00 12968.80 114.56 882 15.5745 13168.00 12857.10 114.75 883 15.5877 12769.00 12763.00 113.00 884 15.6008 12863.00 12683.30 113.42 885 15.6139 12668.00 12615.90 112.55 886 15.6271 12939.00 12558.90 113.75 887 15.6402 12823.00 12511.10 113.24 888 15.6533 12683.00 12471.20 112.62 889 15.6665 12813.00 12438.00 113.19 890 15.6796 12601.00 12410.90 112.25 891 15.6927 12539.00 12389.00 111.98 892 15.7059 12694.00 12371.90 112.67 893 15.7190 12715.00 12359.00 112.76 894 15.7321 12697.00 12350.10 112.68 895 15.7452 12490.00 12345.00 111.76 896 15.7584 12487.00 12343.60 111.75 897 15.7715 12585.00 12345.80 112.18 898 15.7846 12558.00 12351.70 112.06 899 15.7978 12596.00 12361.70 112.23 900 15.8109 12588.00 12376.20 112.20 901 15.8240 12737.00 12396.00 112.86 902 15.8372 12765.00 12422.00 112.98 903 15.8503 12826.00 12455.70 113.25 904 15.8634 12761.00 12499.00 112.96 905 15.8765 12914.00 12553.30 113.64 906 15.8897 12812.00 12623.80 113.19 907 15.9028 12911.00 12718.00 113.63 908 15.9159 13201.00 12815.30 114.90 909 15.9291 13466.00 13045.00 116.04 910 15.9422 13887.00 13441.80 117.84 911 15.9553 14770.00 14087.50 121.53 912 15.9685 15762.00 15155.40 125.55 913 15.9816 17685.00 16840.10 132.99 914 15.9947 20511.00 19434.10 143.22 915 16.0078 24721.00 22941.20 157.23 916 16.0210 29366.00 26510.00 171.37 917 16.0341 31889.00 28539.00 178.57 918 16.0472 31554.00 28495.50 177.63 919 16.0604 30272.00 26877.80 173.99 920 16.0735 27941.00 24254.70 167.16 921 16.0866 23599.00 21232.00 153.62 922 16.0998 19821.00 18412.70 140.79 923 16.1129 17010.00 16244.10 130.42 924 16.1260 15718.00 14881.60 125.37 925 16.1392 15015.00 14213.60 122.54 926 16.1523 14530.00 14014.90 120.54 927 16.1654 14223.00 14119.20 119.26 928 16.1785 14588.00 14380.70 120.78 929 16.1917 14848.00 14748.00 121.85 930 16.2048 14797.00 15133.30 121.64 931 16.2179 15398.00 15405.00 124.09 932 16.2311 15423.00 15467.80 124.19 933 16.2442 15068.00 15327.80 122.75 934 16.2573 15073.00 15025.30 122.77 935 16.2705 14520.00 14608.50 120.50 936 16.2836 14319.00 14164.60 119.66 937 16.2967 13782.00 13766.90 117.40 938 16.3098 13735.00 13459.50 117.20 939 16.3230 13301.00 13253.30 115.33 940 16.3361 13453.00 13131.50 115.99 941 16.3492 13216.00 13062.70 114.96 942 16.3624 13441.00 13018.20 115.93 943 16.3755 13382.00 12980.50 115.68 944 16.3886 13581.00 12941.50 116.54 945 16.4018 13072.00 12900.20 114.33 946 16.4149 13252.00 12860.80 115.12 947 16.4280 13056.00 12828.40 114.26 948 16.4411 12687.00 12805.80 112.64 949 16.4543 12969.00 12793.80 113.88 950 16.4674 12808.00 12791.30 113.17 951 16.4805 13413.00 12803.30 115.82 952 16.4937 13245.00 12814.10 115.09 953 16.5068 13180.00 12828.80 114.80 954 16.5199 13168.00 12849.80 114.75 955 16.5331 12956.00 12876.60 113.82 956 16.5462 13006.00 12898.70 114.04 957 16.5593 13144.00 12922.80 114.65 958 16.5725 13070.00 12948.90 114.32 959 16.5856 13088.00 12980.50 114.40 960 16.5987 12961.00 13011.10 113.85 961 16.6118 13342.00 13044.20 115.51 962 16.6250 12971.00 13080.20 113.89 963 16.6381 13124.00 13119.60 114.56 964 16.6512 13338.00 13162.90 115.49 965 16.6644 13086.00 13197.10 114.39 966 16.6775 13372.00 13251.50 115.64 967 16.6906 13378.00 13312.80 115.66 968 16.7038 13406.00 13375.80 115.78 969 16.7169 13418.00 13465.90 115.84 970 16.7300 13465.00 13579.30 116.04 971 16.7431 13488.00 13688.90 116.14 972 16.7563 13496.00 13818.00 116.17 973 16.7694 13942.00 13989.60 118.08 974 16.7825 13957.00 14191.60 118.14 975 16.7957 14329.00 14469.40 119.70 976 16.8088 14784.00 14872.80 121.59 977 16.8219 15610.00 15470.80 124.94 978 16.8351 16460.00 16357.00 128.30 979 16.8482 17870.00 17675.70 133.68 980 16.8613 19876.00 19648.20 140.98 981 16.8744 23211.00 22524.20 152.35 982 16.8876 27350.00 26342.10 165.38 983 16.9007 31609.00 30569.60 177.79 984 16.9138 36009.00 34161.00 189.76 985 16.9270 38621.00 36448.30 196.52 986 16.9401 39911.00 37569.90 199.78 987 16.9532 40457.00 37728.30 201.14 988 16.9664 40110.00 36789.50 200.27 989 16.9795 37929.00 34703.30 194.75 990 16.9926 35015.00 31833.70 187.12 991 17.0058 31242.00 28680.00 176.75 992 17.0189 28056.00 25555.10 167.50 993 17.0320 24798.00 22671.30 157.47 994 17.0451 21708.00 20223.80 147.34 995 17.0583 19463.00 18315.20 139.51 996 17.0714 17729.00 16948.90 133.15 997 17.0845 16659.00 16061.20 129.07 998 17.0977 15915.00 15547.10 126.15 999 17.1108 15696.00 15306.10 125.28 1000 17.1239 15213.00 15271.80 123.34 1001 17.1371 15402.00 15422.90 124.11 1002 17.1502 15598.00 15778.20 124.89 1003 17.1633 16260.00 16397.70 127.51 1004 17.1764 17263.00 17394.40 131.39 1005 17.1896 18479.00 18910.10 135.94 1006 17.2027 20796.00 20980.00 144.21 1007 17.2158 23126.00 23303.40 152.07 1008 17.2290 25445.00 25262.30 159.51 1009 17.2421 26708.00 26357.30 163.43 1010 17.2552 26906.00 26445.50 164.03 1011 17.2684 26163.00 25636.70 161.75 1012 17.2815 25093.00 24180.10 158.41 1013 17.2946 22996.00 22395.00 151.64 1014 17.3077 21180.00 20617.10 145.53 1015 17.3209 19305.00 19141.30 138.94 1016 17.3340 18652.00 18156.50 136.57 1017 17.3471 18187.00 17753.20 134.86 1018 17.3603 18342.00 17974.90 135.43 1019 17.3734 19107.00 18882.50 138.23 1020 17.3865 21144.00 20630.20 145.41 1021 17.3997 24132.00 23495.50 155.35 1022 17.4128 28200.00 27702.10 167.93 1023 17.4259 33624.00 32904.60 183.37 1024 17.4391 39204.00 37709.80 198.00 1025 17.4522 42062.00 40396.70 205.09 1026 17.4653 41684.00 40470.00 204.17 1027 17.4784 39981.00 38488.80 199.95 1028 17.4916 36450.00 35027.70 190.92 1029 17.5047 31432.00 30702.60 177.29 1030 17.5178 26582.00 26310.20 163.04 1031 17.5310 22944.00 22501.70 151.47 1032 17.5441 19721.00 19601.50 140.43 1033 17.5572 17675.00 17634.50 132.95 1034 17.5704 16334.00 16423.30 127.81 1035 17.5835 15857.00 15724.30 125.93 1036 17.5966 15204.00 15327.80 123.31 1037 17.6097 15074.00 15108.60 122.78 1038 17.6229 14862.00 14963.30 121.91 1039 17.6360 14777.00 14865.20 121.56 1040 17.6491 14659.00 14794.60 121.07 1041 17.6623 14509.00 14728.10 120.45 1042 17.6754 14283.00 14688.30 119.51 1043 17.6885 14704.00 14657.60 121.26 1044 17.7017 14486.00 14624.00 120.36 1045 17.7148 14456.00 14606.80 120.23 1046 17.7279 14454.00 14582.20 120.22 1047 17.7410 14371.00 14574.10 119.88 1048 17.7542 14501.00 14569.50 120.42 1049 17.7673 14542.00 14561.80 120.59 1050 17.7804 14656.00 14562.80 121.06 1051 17.7936 14662.00 14565.90 121.09 1052 17.8067 14419.00 14571.00 120.08 1053 17.8198 14541.00 14577.70 120.59 1054 17.8330 14277.00 14585.90 119.49 1055 17.8461 14533.00 14595.40 120.55 1056 17.8592 14462.00 14606.10 120.26 1057 17.8723 14658.00 14617.90 121.07 1058 17.8855 14514.00 14630.60 120.47 1059 17.8986 14744.00 14644.20 121.43 1060 17.9117 14588.00 14652.00 120.78 1061 17.9249 14734.00 14667.50 121.38 1062 17.9380 14510.00 14683.80 120.46 1063 17.9511 14779.00 14697.40 121.57 1064 17.9643 14837.00 14715.20 121.81 1065 17.9774 14869.00 14733.60 121.94 1066 17.9905 14876.00 14752.80 121.97 1067 18.0037 14942.00 14772.70 122.24 1068 18.0168 14822.00 14786.80 121.75 1069 18.0299 15029.00 14808.50 122.59 1070 18.0430 15056.00 14831.00 122.70 1071 18.0562 14768.00 14851.30 121.52 1072 18.0693 15102.00 14999.10 122.89 1073 18.0824 14900.00 15029.80 122.07 1074 18.0956 14969.00 15062.20 122.35 1075 18.1087 14983.00 15096.70 122.40 1076 18.1218 15182.00 15195.50 123.21 1077 18.1350 15140.00 15237.80 123.04 1078 18.1481 15049.00 15283.60 122.67 1079 18.1612 14878.00 15314.10 121.97 1080 18.1743 15114.00 15359.20 122.94 1081 18.1875 15251.00 15418.40 123.50 1082 18.2006 15200.00 15483.30 123.29 1083 18.2137 15430.00 15541.40 124.22 1084 18.2269 15443.00 15622.60 124.27 1085 18.2400 15256.00 15715.20 123.51 1086 18.2531 15525.00 15823.90 124.60 1087 18.2663 15777.00 15958.70 125.61 1088 18.2794 15909.00 16138.50 126.13 1089 18.2925 15961.00 16393.60 126.34 1090 18.3056 16312.00 16766.30 127.72 1091 18.3188 16682.00 17312.70 129.16 1092 18.3319 17791.00 18106.40 133.38 1093 18.3450 18892.00 19241.20 137.45 1094 18.3582 20116.00 20813.00 141.83 1095 18.3713 22144.00 22820.90 148.81 1096 18.3844 24274.00 24975.60 155.80 1097 18.3976 25588.00 26684.30 159.96 1098 18.4107 26338.00 27479.80 162.29 1099 18.4238 26171.00 27352.10 161.77 1100 18.4370 25673.00 26507.10 160.23 1101 18.4501 24323.00 25148.60 155.96 1102 18.4632 22593.00 23468.10 150.31 1103 18.4763 21043.00 21788.10 145.06 1104 18.4895 19623.00 20327.30 140.08 1105 18.5026 18425.00 19224.00 135.74 1106 18.5157 17766.00 18476.10 133.29 1107 18.5289 17296.00 18051.50 131.51 1108 18.5420 17098.00 17867.50 130.76 1109 18.5551 16876.00 17854.60 129.91 1110 18.5683 16962.00 17961.10 130.24 1111 18.5814 17080.00 18157.80 130.69 1112 18.5945 17328.00 18432.00 131.64 1113 18.6076 17280.00 18801.40 131.45 1114 18.6208 18092.00 19241.70 134.51 1115 18.6339 18654.00 19808.10 136.58 1116 18.6470 19137.00 20604.20 138.34 1117 18.6602 21082.00 21810.40 145.20 1118 18.6733 23008.00 23771.30 151.68 1119 18.6864 26049.00 26978.70 161.40 1120 18.6996 30895.00 32139.70 175.77 1121 18.7127 38762.00 40374.80 196.88 1122 18.7258 51281.00 53304.30 226.45 1123 18.7389 69646.00 72217.10 263.90 1124 18.7521 93369.00 95638.50 305.56 1125 18.7652 114678.00 116965.00 338.64 1126 18.7783 126163.00 128186.00 355.19 1127 18.7915 124842.00 127693.00 353.33 1128 18.8046 117853.00 119120.00 343.30 1129 18.8177 105821.00 105308.00 325.30 1130 18.8309 87148.00 87992.20 295.21 1131 18.8440 68578.00 69813.20 261.87 1132 18.8571 51796.00 53470.70 227.59 1133 18.8703 39892.00 40659.20 199.73 1134 18.8834 31166.00 31813.40 176.54 1135 18.8965 26014.00 26350.20 161.29 1136 18.9096 23033.00 23232.20 151.77 1137 18.9228 21515.00 21509.30 146.68 1138 18.9359 20052.00 20541.80 141.60 1139 18.9490 19687.00 19978.80 140.31 1140 18.9622 19157.00 19656.20 138.41 1141 18.9753 18985.00 19523.30 137.79 1142 18.9884 18874.00 19631.50 137.38 1143 19.0016 19452.00 20039.00 139.47 1144 19.0147 20332.00 20929.50 142.59 1145 19.0278 21270.00 22576.10 145.84 1146 19.0409 23528.00 25388.10 153.39 1147 19.0541 27342.00 29818.30 165.35 1148 19.0672 32683.00 35614.90 180.78 1149 19.0803 37940.00 40960.70 194.78 1150 19.0935 39991.00 43493.90 199.98 1151 19.1066 39950.00 42907.20 199.88 1152 19.1197 38117.00 40605.50 195.24 1153 19.1329 36403.00 37579.30 190.80 1154 19.1460 32996.00 34140.80 181.65 1155 19.1591 29196.00 30818.40 170.87 1156 19.1722 26822.00 28309.80 163.77 1157 19.1854 25829.00 26976.30 160.71 1158 19.1985 25704.00 26569.10 160.32 1159 19.2116 26187.00 26408.80 161.82 1160 19.2248 26066.00 26054.10 161.45 1161 19.2379 25219.00 25447.80 158.80 1162 19.2510 24747.00 24620.50 157.31 1163 19.2642 24111.00 23647.60 155.28 1164 19.2773 23166.00 22704.20 152.20 1165 19.2904 22439.00 22014.60 149.80 1166 19.3036 22242.00 21788.00 149.14 1167 19.3167 22552.00 22212.10 150.17 1168 19.3298 23459.00 23447.60 153.16 1169 19.3429 25329.00 25548.60 159.15 1170 19.3561 28210.00 28265.00 167.96 1171 19.3692 30820.00 30869.30 175.56 1172 19.3823 32629.00 32484.70 180.63 1173 19.3955 32672.00 32787.50 180.75 1174 19.4086 32295.00 32025.80 179.71 1175 19.4217 30805.00 30490.10 175.51 1176 19.4349 28619.00 28391.40 169.17 1177 19.4480 25859.00 26038.90 160.81 1178 19.4611 23928.00 23789.10 154.69 1179 19.4742 21870.00 21763.20 147.88 1180 19.4874 20527.00 20320.10 143.27 1181 19.5005 19565.00 19333.10 139.88 1182 19.5136 18856.00 18663.60 137.32 1183 19.5268 18420.00 18319.90 135.72 1184 19.5399 18142.00 18149.60 134.69 1185 19.5530 18067.00 18093.20 134.41 1186 19.5662 18166.00 18128.80 134.78 1187 19.5793 18551.00 18270.20 136.20 1188 19.5924 18767.00 18564.00 136.99 1189 19.6055 18901.00 19089.30 137.48 1190 19.6187 19606.00 19972.60 140.02 1191 19.6318 21004.00 21418.20 144.93 1192 19.6449 23236.00 23692.80 152.43 1193 19.6581 25787.00 26933.00 160.58 1194 19.6712 29185.00 30716.70 170.84 1195 19.6843 32532.00 33840.20 180.37 1196 19.6975 33876.00 35185.10 184.05 1197 19.7106 34101.00 34786.20 184.66 1198 19.7237 32888.00 33281.10 181.35 1199 19.7368 31080.00 31106.10 176.29 1200 19.7500 28284.00 28438.80 168.18 1201 19.7631 25668.00 25627.10 160.21 1202 19.7762 23270.00 23091.00 152.54 1203 19.7894 20894.00 21079.80 144.55 1204 19.8025 19752.00 19675.70 140.54 1205 19.8156 18857.00 18801.40 137.32 1206 19.8288 18735.00 18305.30 136.88 1207 19.8419 18234.00 18042.30 135.03 1208 19.8550 18062.00 17910.30 134.40 1209 19.8682 17985.00 17845.90 134.11 1210 19.8813 18210.00 17809.50 134.94 1211 19.8944 17843.00 17778.20 133.58 1212 19.9075 17703.00 17743.20 133.05 1213 19.9207 17886.00 17697.20 133.74 1214 19.9338 17655.00 17654.40 132.87 1215 19.9469 17691.00 17609.90 133.01 1216 19.9601 17761.00 17567.50 133.27 1217 19.9732 17719.00 17528.20 133.11 1218 19.9863 17661.00 17507.70 132.90 1219 19.9995 17409.00 17490.90 131.94 1220 20.0126 17715.00 17483.90 133.10 1221 20.0257 17550.00 17485.60 132.48 1222 20.0388 17744.00 17496.30 133.21 1223 20.0520 17607.00 17546.80 132.69 1224 20.0651 17525.00 17570.70 132.38 1225 20.0782 17697.00 17604.10 133.03 1226 20.0914 17886.00 17652.50 133.74 1227 20.1045 17759.00 17745.40 133.26 1228 20.1176 17874.00 17864.70 133.69 1229 20.1308 18151.00 18051.90 134.73 1230 20.1439 18228.00 18327.20 135.01 1231 20.1570 18630.00 18783.20 136.49 1232 20.1701 19641.00 19462.60 140.15 1233 20.1833 20250.00 20374.50 142.30 1234 20.1964 21556.00 21375.30 146.82 1235 20.2095 22100.00 22192.40 148.66 1236 20.2227 22576.00 22582.70 150.25 1237 20.2358 22492.00 22553.30 149.97 1238 20.2489 22097.00 22227.20 148.65 1239 20.2621 21550.00 21686.00 146.80 1240 20.2752 21205.00 20992.20 145.62 1241 20.2883 20781.00 20243.70 144.16 1242 20.3015 19510.00 19542.40 139.68 1243 20.3146 18933.00 18959.40 137.60 1244 20.3277 18436.00 18525.50 135.78 1245 20.3408 17958.00 18233.80 134.01 1246 20.3540 17993.00 18054.60 134.14 1247 20.3671 17952.00 17952.40 133.99 1248 20.3802 18106.00 17898.30 134.56 1249 20.3934 17595.00 17853.40 132.65 1250 20.4065 17987.00 17845.80 134.12 1251 20.4196 17829.00 17849.20 133.52 1252 20.4328 17799.00 17860.60 133.41 1253 20.4459 17908.00 17868.80 133.82 1254 20.4590 17653.00 17892.70 132.87 1255 20.4721 17860.00 17922.20 133.64 1256 20.4853 17930.00 17957.60 133.90 1257 20.4984 18029.00 17999.50 134.27 1258 20.5115 17778.00 18048.70 133.33 1259 20.5247 17750.00 18106.30 133.23 1260 20.5378 17907.00 18173.70 133.82 1261 20.5509 18233.00 18264.80 135.03 1262 20.5641 18183.00 18356.80 134.84 1263 20.5772 18611.00 18463.50 136.42 1264 20.5903 18353.00 18588.00 135.47 1265 20.6034 18734.00 18744.40 136.87 1266 20.6166 18905.00 18938.30 137.49 1267 20.6297 19006.00 19219.70 137.86 1268 20.6428 19990.00 19670.80 141.39 1269 20.6560 20771.00 20423.10 144.12 1270 20.6691 22011.00 21678.10 148.36 1271 20.6822 24151.00 23757.90 155.41 1272 20.6954 26799.00 27156.90 163.70 1273 20.7085 31981.00 32394.60 178.83 1274 20.7216 39087.00 39426.30 197.70 1275 20.7348 46350.00 46767.80 215.29 1276 20.7479 51287.00 51863.60 226.47 1277 20.7610 53111.00 53461.90 230.46 1278 20.7741 51895.00 52353.60 227.80 1279 20.7873 49380.00 49619.80 222.22 1280 20.8004 45947.00 45631.00 214.35 1281 20.8135 40515.00 40694.20 201.28 1282 20.8267 35440.00 35453.70 188.26 1283 20.8398 31066.00 30602.70 176.26 1284 20.8529 26954.00 26653.00 164.18 1285 20.8661 24315.00 23784.40 155.93 1286 20.8792 22697.00 21880.00 150.65 1287 20.8923 21445.00 20679.90 146.44 1288 20.9054 20999.00 19931.10 144.91 1289 20.9186 20233.00 19452.90 142.24 1290 20.9317 20148.00 19134.80 141.94 1291 20.9448 19503.00 18911.80 139.65 1292 20.9580 19489.00 18745.30 139.60 1293 20.9711 18880.00 18613.70 137.40 1294 20.9842 18915.00 18515.30 137.53 1295 20.9974 18808.00 18429.80 137.14 1296 21.0105 18536.00 18362.40 136.15 1297 21.0236 18484.00 18310.60 135.96 1298 21.0367 18428.00 18275.50 135.75 1299 21.0499 18353.00 18247.40 135.47 1300 21.0630 18458.00 18227.60 135.86 1301 21.0761 18144.00 18214.30 134.70 1302 21.0893 18367.00 18207.10 135.52 1303 21.1024 18241.00 18205.10 135.06 1304 21.1155 18381.00 18208.00 135.58 1305 21.1287 18436.00 18215.80 135.78 1306 21.1418 18261.00 18228.50 135.13 1307 21.1549 18337.00 18246.30 135.41 1308 21.1681 18233.00 18269.30 135.03 1309 21.1812 18526.00 18298.00 136.11 1310 21.1943 18574.00 18333.70 136.29 1311 21.2074 18821.00 18379.40 137.19 1312 21.2206 18566.00 18441.70 136.26 1313 21.2337 18923.00 18532.30 137.56 1314 21.2468 19013.00 18670.30 137.89 1315 21.2600 19363.00 18884.50 139.15 1316 21.2731 19896.00 19217.60 141.05 1317 21.2862 20430.00 19735.50 142.93 1318 21.2994 21447.00 20537.90 146.45 1319 21.3125 23149.00 21738.90 152.15 1320 21.3256 24958.00 23414.20 157.98 1321 21.3387 27214.00 25468.60 164.97 1322 21.3519 29767.00 27535.20 172.53 1323 21.3650 31351.00 29138.00 177.06 1324 21.3781 31516.00 30117.50 177.53 1325 21.3913 32222.00 30711.70 179.51 1326 21.4044 32808.00 31177.20 181.13 1327 21.4175 33226.00 31416.50 182.28 1328 21.4307 32312.00 30939.20 179.76 1329 21.4438 30308.00 29617.10 174.09 1330 21.4569 28640.00 27792.70 169.23 1331 21.4700 27000.00 25991.30 164.32 1332 21.4832 25598.00 24393.80 159.99 1333 21.4963 23831.00 22981.50 154.37 1334 21.5094 22818.00 21728.10 151.06 1335 21.5226 21673.00 20720.40 147.22 1336 21.5357 21047.00 20059.70 145.08 1337 21.5488 20937.00 19802.50 144.70 1338 21.5620 20973.00 19967.50 144.82 1339 21.5751 21515.00 20606.20 146.68 1340 21.5882 22367.00 21725.10 149.56 1341 21.6013 24018.00 23130.00 154.98 1342 21.6145 25448.00 24289.60 159.52 1343 21.6276 26280.00 24745.90 162.11 1344 21.6407 25779.00 24603.30 160.56 1345 21.6539 25483.00 24293.30 159.63 1346 21.6670 25668.00 24092.70 160.21 1347 21.6801 25323.00 24056.40 159.13 1348 21.6933 24927.00 24231.70 157.88 1349 21.7064 25142.00 24607.80 158.56 1350 21.7195 25056.00 24951.10 158.29 1351 21.7327 25084.00 24961.30 158.38 1352 21.7458 24179.00 24624.90 155.50 1353 21.7589 23988.00 24040.00 154.88 1354 21.7720 23310.00 23337.80 152.68 1355 21.7852 22482.00 22524.20 149.94 1356 21.7983 21464.00 21615.90 146.51 1357 21.8114 20807.00 20725.00 144.25 1358 21.8246 19979.00 19931.60 141.35 1359 21.8377 19447.00 19316.80 139.45 1360 21.8508 19197.00 18903.70 138.55 1361 21.8640 18760.00 18664.70 136.97 1362 21.8771 18780.00 18580.80 137.04 1363 21.8902 18688.00 18641.40 136.70 1364 21.9033 18712.00 18838.50 136.79 1365 21.9165 18911.00 19143.40 137.52 1366 21.9296 18994.00 19438.80 137.82 1367 21.9427 19072.00 19572.40 138.10 1368 21.9559 19153.00 19516.30 138.39 1369 21.9690 18996.00 19366.30 137.83 1370 21.9821 18957.00 19204.80 137.68 1371 21.9953 18893.00 19033.70 137.45 1372 22.0084 18600.00 18835.30 136.38 1373 22.0215 18511.00 18627.40 136.05 1374 22.0346 18327.00 18446.50 135.38 1375 22.0478 18486.00 18320.30 135.96 1376 22.0609 18224.00 18249.70 135.00 1377 22.0740 18216.00 18237.60 134.97 1378 22.0872 18358.00 18269.80 135.49 1379 22.1003 18450.00 18347.50 135.83 1380 22.1134 18570.00 18484.10 136.27 1381 22.1266 18967.00 18705.20 137.72 1382 22.1397 19116.00 19063.20 138.26 1383 22.1528 19625.00 19621.70 140.09 1384 22.1660 20456.00 20432.10 143.02 1385 22.1791 21306.00 21518.20 145.97 1386 22.1922 22193.00 22718.90 148.97 1387 22.2053 23448.00 23724.60 153.13 1388 22.2185 23896.00 24271.30 154.58 1389 22.2316 23724.00 24363.90 154.03 1390 22.2447 23696.00 24142.60 153.93 1391 22.2579 23449.00 23709.50 153.13 1392 22.2710 22557.00 23104.00 150.19 1393 22.2841 22210.00 22417.00 149.03 1394 22.2973 22085.00 21783.00 148.61 1395 22.3104 21663.00 21366.60 147.18 1396 22.3235 21753.00 21348.00 147.49 1397 22.3366 22024.00 21957.30 148.40 1398 22.3498 23353.00 23527.70 152.82 1399 22.3629 25822.00 26557.30 160.69 1400 22.3760 29790.00 31496.10 172.60 1401 22.3892 35628.00 38006.60 188.75 1402 22.4023 41573.00 44133.20 203.90 1403 22.4154 45571.00 47309.40 213.47 1404 22.4286 44734.00 47155.20 211.50 1405 22.4417 43717.00 45438.90 209.09 1406 22.4548 42443.00 43630.50 206.02 1407 22.4679 40401.00 41566.40 201.00 1408 22.4811 37382.00 38536.30 193.34 1409 22.4942 33359.00 34711.60 182.64 1410 22.5073 30016.00 31038.30 173.25 1411 22.5205 28080.00 28406.30 167.57 1412 22.5336 26461.00 27124.30 162.67 1413 22.5467 26767.00 27001.70 163.61 1414 22.5599 27614.00 27765.10 166.18 1415 22.5730 28742.00 29178.60 169.54 1416 22.5861 30143.00 30898.30 173.62 1417 22.5993 31738.00 32308.10 178.15 1418 22.6124 32032.00 32853.00 178.98 1419 22.6255 31645.00 32458.90 177.89 1420 22.6386 30752.00 31406.40 175.36 1421 22.6518 29346.00 29932.00 171.31 1422 22.6649 27761.00 28136.60 166.62 1423 22.6780 25862.00 26153.70 160.82 1424 22.6912 23790.00 24187.90 154.24 1425 22.7043 22230.00 22423.10 149.10 1426 22.7174 20810.00 20970.30 144.26 1427 22.7306 19805.00 19867.50 140.73 1428 22.7437 19320.00 19088.60 139.00 1429 22.7568 18823.00 18568.20 137.20 1430 22.7699 18823.00 18230.80 137.20 1431 22.7831 18330.00 18012.30 135.39 1432 22.7962 18050.00 17867.80 134.35 1433 22.8093 18031.00 17768.10 134.28 1434 22.8225 17834.00 17693.50 133.54 1435 22.8356 18035.00 17630.80 134.29 1436 22.8487 17708.00 17572.40 133.07 1437 22.8619 17597.00 17516.60 132.65 1438 22.8750 17436.00 17463.20 132.04 1439 22.8881 17632.00 17412.00 132.79 1440 22.9012 17472.00 17362.50 132.18 1441 22.9144 17296.00 17315.50 131.51 1442 22.9275 17557.00 17271.80 132.50 1443 22.9406 17349.00 17232.30 131.72 1444 22.9538 17260.00 17197.50 131.38 1445 22.9669 17215.00 17167.50 131.21 1446 22.9800 17159.00 17141.90 130.99 1447 22.9932 17372.00 17120.60 131.80 1448 23.0063 17146.00 17096.40 130.94 1449 23.0194 17173.00 17083.90 131.05 1450 23.0326 17282.00 17077.00 131.46 1451 23.0457 17272.00 17077.50 131.42 1452 23.0588 17236.00 17083.90 131.29 1453 23.0719 16912.00 17074.10 130.05 1454 23.0851 17396.00 17101.20 131.89 1455 23.0982 17246.00 17131.60 131.32 1456 23.1113 17200.00 17165.90 131.15 1457 23.1245 17062.00 17211.20 130.62 1458 23.1376 17282.00 17309.00 131.46 1459 23.1507 17769.00 17463.20 133.30 1460 23.1639 17692.00 17698.60 133.01 1461 23.1770 18072.00 18031.90 134.43 1462 23.1901 19024.00 18438.00 137.93 1463 23.2032 19199.00 18801.00 138.56 1464 23.2164 19251.00 18997.50 138.75 1465 23.2295 19607.00 19040.60 140.02 1466 23.2426 19589.00 19060.50 139.96 1467 23.2558 19647.00 19177.70 140.17 1468 23.2689 19810.00 19427.80 140.75 1469 23.2820 19992.00 19769.40 141.39 1470 23.2952 20534.00 20097.60 143.30 1471 23.3083 20567.00 20305.30 143.41 1472 23.3214 20502.00 20222.80 143.18 1473 23.3345 20099.00 19968.30 141.77 1474 23.3477 19894.00 19638.90 141.05 1475 23.3608 19786.00 19293.90 140.66 1476 23.3739 19106.00 18874.00 138.22 1477 23.3871 18481.00 18416.70 135.95 1478 23.4002 18306.00 17959.50 135.30 1479 23.4133 17552.00 17547.20 132.48 1480 23.4265 17135.00 17222.40 130.90 1481 23.4396 16932.00 16981.10 130.12 1482 23.4527 16700.00 16815.00 129.23 1483 23.4658 16594.00 16702.30 128.82 1484 23.4790 16373.00 16625.70 127.96 1485 23.4921 16583.00 16576.30 128.77 1486 23.5052 16520.00 16540.50 128.53 1487 23.5184 16383.00 16513.00 128.00 1488 23.5315 16160.00 16491.20 127.12 1489 23.5446 16412.00 16473.60 128.11 1490 23.5578 16243.00 16459.30 127.45 1491 23.5709 16435.00 16448.00 128.20 1492 23.5840 16341.00 16439.20 127.83 1493 23.5972 16282.00 16437.20 127.60 1494 23.6103 16341.00 16433.80 127.83 1495 23.6234 16082.00 16433.30 126.82 1496 23.6365 16411.00 16435.70 128.10 1497 23.6497 16156.00 16443.60 127.11 1498 23.6628 16266.00 16453.30 127.54 1499 23.6759 16037.00 16467.60 126.64 1500 23.6891 16211.00 16487.30 127.32 1501 23.7022 16276.00 16513.10 127.58 1502 23.7153 16209.00 16546.30 127.32 1503 23.7285 16224.00 16588.20 127.37 1504 23.7416 16458.00 16640.10 128.29 1505 23.7547 16376.00 16703.30 127.97 1506 23.7678 16343.00 16778.60 127.84 1507 23.7810 16458.00 16866.80 128.29 1508 23.7941 16679.00 16969.10 129.15 1509 23.8072 16813.00 17091.80 129.66 1510 23.8204 16998.00 17257.60 130.38 1511 23.8335 17556.00 17527.30 132.50 1512 23.8466 18289.00 18026.70 135.24 1513 23.8598 19387.00 18980.40 139.24 1514 23.8729 21027.00 20778.50 145.01 1515 23.8860 24250.00 24121.80 155.72 1516 23.8991 29821.00 30076.20 172.69 1517 23.9123 39239.00 39534.40 198.09 1518 23.9254 52119.00 51604.50 228.30 1519 23.9385 63805.00 62128.30 252.60 1520 23.9517 67566.00 66246.30 259.93 1521 23.9648 64089.00 63786.90 253.16 1522 23.9779 59752.00 58548.50 244.44 1523 23.9911 56528.00 53689.40 237.76 1524 24.0042 51783.00 49170.00 227.56 1525 24.0173 44986.00 43568.70 212.10 1526 24.0305 37020.00 36843.80 192.41 1527 24.0436 29830.00 30161.70 172.71 1528 24.0567 24120.00 24733.00 155.31 1529 24.0698 20795.00 21066.00 144.21 1530 24.0830 18812.00 18921.50 137.16 1531 24.0961 17532.00 17770.20 132.41 1532 24.1092 16702.00 17146.40 129.24 1533 24.1224 16577.00 16778.40 128.75 1534 24.1355 16429.00 16535.50 128.18 1535 24.1486 16168.00 16366.90 127.15 1536 24.1618 16014.00 16248.40 126.55 1537 24.1749 15765.00 16169.40 125.56 1538 24.1880 16023.00 16129.20 126.58 1539 24.2011 16140.00 16131.20 127.04 1540 24.2143 15770.00 16178.90 125.58 1541 24.2274 16232.00 16268.20 127.40 1542 24.2405 16216.00 16376.70 127.34 1543 24.2537 16396.00 16465.80 128.05 1544 24.2668 16366.00 16503.10 127.93 1545 24.2799 16096.00 16487.20 126.87 1546 24.2931 16000.00 16440.70 126.49 1547 24.3062 15815.00 16388.20 125.76 1548 24.3193 16074.00 16348.30 126.78 1549 24.3324 15806.00 16344.90 125.72 1550 24.3456 15899.00 16417.10 126.09 1551 24.3587 16355.00 16612.00 127.89 1552 24.3718 16310.00 16961.20 127.71 1553 24.3850 16692.00 17448.10 129.20 1554 24.3981 17266.00 17951.80 131.40 1555 24.4112 17350.00 18308.30 131.72 1556 24.4244 17567.00 18419.20 132.54 1557 24.4375 17542.00 18319.50 132.45 1558 24.4506 16971.00 18099.50 130.27 1559 24.4638 16798.00 17806.30 129.61 1560 24.4769 16569.00 17443.20 128.72 1561 24.4900 16350.00 17024.50 127.87 1562 24.5031 15802.00 16588.70 125.71 1563 24.5163 15702.00 16179.20 125.31 1564 24.5294 15408.00 15834.00 124.13 1565 24.5425 15213.00 15555.20 123.34 1566 24.5557 14710.00 15349.80 121.29 1567 24.5688 14904.00 15205.80 122.08 1568 24.5819 14821.00 15058.40 121.74 1569 24.5951 14543.00 14993.80 120.59 1570 24.6082 14687.00 14943.90 121.19 1571 24.6213 14608.00 14903.80 120.86 1572 24.6344 14560.00 14868.80 120.67 1573 24.6476 14693.00 14813.70 121.21 1574 24.6607 14383.00 14785.80 119.93 1575 24.6738 14361.00 14760.70 119.84 1576 24.6870 14438.00 14738.30 120.16 1577 24.7001 14173.00 14719.00 119.05 1578 24.7132 14368.00 14704.20 119.87 1579 24.7264 14290.00 14697.70 119.54 1580 24.7395 14284.00 14707.30 119.52 1581 24.7526 14272.00 14747.30 119.46 1582 24.7657 14432.00 14836.50 120.13 1583 24.7789 14511.00 14984.30 120.46 1584 24.7920 14479.00 15161.70 120.33 1585 24.8051 14592.00 15288.30 120.80 1586 24.8183 14566.00 15299.30 120.69 1587 24.8314 14720.00 15216.90 121.33 1588 24.8445 14456.00 15112.70 120.23 1589 24.8577 14455.00 15023.90 120.23 1590 24.8708 14222.00 14941.70 119.26 1591 24.8839 14259.00 14839.80 119.41 1592 24.8971 14495.00 14719.30 120.39 1593 24.9102 14238.00 14602.10 119.32 1594 24.9233 13949.00 14505.20 118.11 1595 24.9364 14053.00 14437.80 118.54 1596 24.9496 13971.00 14411.90 118.20 1597 24.9627 13587.00 14387.30 116.56 1598 24.9758 14152.00 14372.50 118.96 1599 24.9890 13889.00 14363.80 117.85 1600 25.0021 14097.00 14359.60 118.73 1601 25.0152 13928.00 14368.80 118.02 1602 25.0284 14050.00 14378.40 118.53 1603 25.0415 14011.00 14401.10 118.37 1604 25.0546 14189.00 14443.90 119.12 1605 25.0677 14562.00 14514.20 120.67 1606 25.0809 14304.00 14624.10 119.60 1607 25.0940 15081.00 14801.80 122.81 1608 25.1071 15132.00 15103.90 123.01 1609 25.1203 15443.00 15593.00 124.27 1610 25.1334 16193.00 16293.40 127.25 1611 25.1465 17046.00 17135.50 130.56 1612 25.1597 17714.00 17977.50 133.09 1613 25.1728 18128.00 18690.40 134.64 1614 25.1859 18771.00 19159.20 137.01 1615 25.1990 18847.00 19307.60 137.28 1616 25.2122 18701.00 19170.30 136.75 1617 25.2253 18272.00 18825.40 135.17 1618 25.2384 17872.00 18385.70 133.69 1619 25.2516 17536.00 17907.00 132.42 1620 25.2647 16974.00 17442.50 130.28 1621 25.2778 16778.00 17088.70 129.53 1622 25.2910 16442.00 16946.50 128.23 1623 25.3041 16602.00 17116.40 128.85 1624 25.3172 17109.00 17612.40 130.80 1625 25.3303 17933.00 18319.70 133.91 1626 25.3435 18391.00 18968.20 135.61 1627 25.3566 18710.00 19303.10 136.79 1628 25.3697 18560.00 19269.70 136.24 1629 25.3829 18288.00 18987.10 135.23 1630 25.3960 17985.00 18583.80 134.11 1631 25.4091 17509.00 18094.30 132.32 1632 25.4223 17071.00 17511.00 130.66 1633 25.4354 16611.00 16858.10 128.88 1634 25.4485 15722.00 16197.80 125.39 1635 25.4617 15315.00 15594.80 123.75 1636 25.4748 14602.00 15093.90 120.84 1637 25.4879 14458.00 14716.10 120.24 1638 25.5010 14392.00 14458.90 119.97 1639 25.5142 14233.00 14304.70 119.30 1640 25.5273 13926.00 14234.60 118.01 1641 25.5404 14045.00 14237.40 118.51 1642 25.5536 14435.00 14318.60 120.15 1643 25.5667 14415.00 14501.30 120.06 1644 25.5798 15071.00 14818.10 122.76 1645 25.5930 15778.00 15288.10 125.61 1646 25.6061 16216.00 15893.70 127.34 1647 25.6192 17168.00 16516.20 131.03 1648 25.6323 17650.00 17111.50 132.85 1649 25.6455 17862.00 17790.90 133.65 1650 25.6586 18911.00 18819.50 137.52 1651 25.6717 20082.00 20458.70 141.71 1652 25.6849 21924.00 22712.80 148.07 1653 25.6980 24563.00 25151.70 156.73 1654 25.7111 26272.00 26936.70 162.09 1655 25.7243 26612.00 27453.50 163.13 1656 25.7374 26122.00 26861.90 161.62 1657 25.7505 25098.00 25760.40 158.42 1658 25.7636 24287.00 24582.70 155.84 1659 25.7768 23547.00 23353.10 153.45 1660 25.7899 21940.00 21933.40 148.12 1661 25.8030 20091.00 20357.60 141.74 1662 25.8162 18837.00 18825.70 137.25 1663 25.8293 17243.00 17546.30 131.31 1664 25.8424 16764.00 16732.10 129.48 1665 25.8556 16443.00 16558.10 128.23 1666 25.8687 17109.00 17150.50 130.80 1667 25.8818 18260.00 18521.10 135.13 1668 25.8950 20198.00 20373.60 142.12 1669 25.9081 21948.00 21966.80 148.15 1670 25.9212 23118.00 22601.30 152.05 1671 25.9343 22655.00 22234.20 150.52 1672 25.9475 21578.00 21415.90 146.90 1673 25.9606 20945.00 20696.80 144.72 1674 25.9737 20888.00 20224.20 144.53 1675 25.9869 20273.00 19849.60 142.38 1676 26.0000 19708.00 19510.60 140.38 1677 26.0131 19202.00 19255.00 138.57 1678 26.0263 18761.00 19044.60 136.97 1679 26.0394 18099.00 18717.70 134.53 1680 26.0525 17797.00 18218.50 133.40 1681 26.0656 17400.00 17671.30 131.91 1682 26.0788 17119.00 17201.20 130.84 1683 26.0919 16564.00 16807.00 128.70 1684 26.1050 16469.00 16377.30 128.33 1685 26.1182 15329.00 15847.50 123.81 1686 26.1313 14935.00 15257.40 122.21 1687 26.1444 14293.00 14686.40 119.55 1688 26.1576 14020.00 14198.70 118.41 1689 26.1707 13488.00 13815.60 116.14 1690 26.1838 13103.00 13548.90 114.47 1691 26.1969 12945.00 13365.20 113.78 1692 26.2101 13038.00 13250.00 114.18 1693 26.2232 12944.00 13197.90 113.77 1694 26.2363 13097.00 13216.30 114.44 1695 26.2495 13325.00 13343.90 115.43 1696 26.2626 13724.00 13640.60 117.15 1697 26.2757 14086.00 14229.50 118.68 1698 26.2889 15269.00 15287.90 123.57 1699 26.3020 16717.00 16976.30 129.29 1700 26.3151 18868.00 19251.80 137.36 1701 26.3283 20986.00 21625.40 144.87 1702 26.3414 22614.00 23246.20 150.38 1703 26.3545 22845.00 23616.90 151.15 1704 26.3676 22224.00 23032.90 149.08 1705 26.3808 21637.00 22111.50 147.10 1706 26.3939 20718.00 21225.90 143.94 1707 26.4070 19990.00 20312.80 141.39 1708 26.4202 19023.00 19182.80 137.92 1709 26.4333 17620.00 17845.30 132.74 1710 26.4464 16443.00 16470.60 128.23 1711 26.4596 14939.00 15246.90 122.22 1712 26.4727 14143.00 14280.30 118.92 1713 26.4858 13531.00 13632.50 116.32 1714 26.4989 13334.00 13241.60 115.47 1715 26.5121 13091.00 13043.40 114.42 1716 26.5252 13219.00 12994.60 114.97 1717 26.5383 13374.00 13084.90 115.65 1718 26.5515 13678.00 13378.40 116.95 1719 26.5646 14341.00 13958.40 119.75 1720 26.5777 15136.00 14959.00 123.03 1721 26.5909 16581.00 16459.00 128.77 1722 26.6040 18493.00 18351.40 135.99 1723 26.6171 21008.00 20236.60 144.94 1724 26.6302 22580.00 21508.40 150.27 1725 26.6434 24093.00 21876.80 155.22 1726 26.6565 23260.00 21545.30 152.51 1727 26.6696 22747.00 20895.40 150.82 1728 26.6828 21678.00 20157.60 147.24 1729 26.6959 20935.00 19305.10 144.69 1730 26.7090 19580.00 18263.80 139.93 1731 26.7222 18234.00 17076.40 135.03 1732 26.7353 16713.00 15868.40 129.28 1733 26.7484 15231.00 14774.80 123.41 1734 26.7616 14128.00 13878.40 118.86 1735 26.7747 13537.00 13209.90 116.35 1736 26.7878 12843.00 12746.10 113.33 1737 26.8009 12508.00 12438.10 111.84 1738 26.8141 12267.00 12241.10 110.76 1739 26.8272 12421.00 12116.80 111.45 1740 26.8403 12254.00 12045.10 110.70 1741 26.8535 12305.00 12021.50 110.93 1742 26.8666 12229.00 12056.90 110.58 1743 26.8797 12349.00 12179.50 111.13 1744 26.8929 12615.00 12436.00 112.32 1745 26.9060 13034.00 12872.00 114.17 1746 26.9191 13809.00 13498.60 117.51 1747 26.9322 14512.00 14246.40 120.47 1748 26.9454 15083.00 14959.40 122.81 1749 26.9585 15765.00 15507.60 125.56 1750 26.9716 16043.00 15848.30 126.66 1751 26.9848 15795.00 15942.90 125.68 1752 26.9979 16013.00 15768.00 126.54 1753 27.0110 15513.00 15380.90 124.55 1754 27.0242 14899.00 14884.20 122.06 1755 27.0373 14628.00 14374.70 120.95 1756 27.0504 14188.00 13879.10 119.11 1757 27.0635 13491.00 13356.70 116.15 1758 27.0767 13118.00 12843.30 114.53 1759 27.0898 12252.00 12371.90 110.69 1760 27.1029 11891.00 11988.10 109.05 1761 27.1161 11670.00 11709.20 108.03 1762 27.1292 11340.00 11515.70 106.49 1763 27.1423 11278.00 11394.90 106.20 1764 27.1555 11170.00 11314.60 105.69 1765 27.1686 10997.00 11257.70 104.87 1766 27.1817 11005.00 11214.70 104.90 1767 27.1949 10947.00 11180.30 104.63 1768 27.2080 11092.00 11151.60 105.32 1769 27.2211 10991.00 11127.30 104.84 1770 27.2342 10978.00 11107.00 104.78 1771 27.2474 10714.00 11090.90 103.51 1772 27.2605 10942.00 11080.30 104.60 1773 27.2736 10856.00 11078.20 104.19 1774 27.2868 10930.00 11089.40 104.55 1775 27.2999 10855.00 11123.10 104.19 1776 27.3130 11241.00 11193.00 106.02 1777 27.3262 11209.00 11314.80 105.87 1778 27.3393 11197.00 11498.60 105.82 1779 27.3524 11201.00 11733.80 105.83 1780 27.3655 11222.00 11974.00 105.93 1781 27.3787 11567.00 12160.30 107.55 1782 27.3918 11722.00 12261.40 108.27 1783 27.4049 11921.00 12311.30 109.18 1784 27.4181 11892.00 12376.00 109.05 1785 27.4312 12147.00 12498.40 110.21 1786 27.4443 12771.00 12672.80 113.01 1787 27.4575 12880.00 12817.30 113.49 1788 27.4706 12783.00 12835.70 113.06 1789 27.4837 12420.00 12700.80 111.44 1790 27.4968 12470.00 12470.90 111.67 1791 27.5100 12355.00 12232.90 111.15 1792 27.5231 12246.00 12032.60 110.66 1793 27.5362 12017.00 11860.70 109.62 1794 27.5494 11918.00 11690.10 109.17 1795 27.5625 11763.00 11497.60 108.46 1796 27.5756 11285.00 11298.20 106.23 1797 27.5888 11222.00 11111.80 105.93 1798 27.6019 10803.00 10956.10 103.94 1799 27.6150 10878.00 10838.10 104.30 1800 27.6281 10590.00 10753.90 102.91 1801 27.6413 10725.00 10691.00 103.56 1802 27.6544 10492.00 10641.30 102.43 1803 27.6675 10291.00 10603.10 101.44 1804 27.6807 10559.00 10568.00 102.76 1805 27.6938 10275.00 10541.90 101.37 1806 27.7069 10362.00 10516.90 101.79 1807 27.7201 10345.00 10492.00 101.71 1808 27.7332 10486.00 10473.40 102.40 1809 27.7463 10264.00 10458.50 101.31 1810 27.7595 10494.00 10443.70 102.44 1811 27.7726 10445.00 10432.20 102.20 1812 27.7857 10133.00 10417.40 100.66 1813 27.7988 10228.00 10405.50 101.13 1814 27.8120 10280.00 10394.50 101.39 1815 27.8251 10303.00 10384.90 101.50 1816 27.8382 10137.00 10377.60 100.68 1817 27.8514 10387.00 10369.00 101.92 1818 27.8645 10348.00 10361.50 101.72 1819 27.8776 10323.00 10354.90 101.60 1820 27.8908 10315.00 10349.40 101.56 1821 27.9039 10274.00 10345.40 101.36 1822 27.9170 10298.00 10343.40 101.48 1823 27.9301 10242.00 10341.90 101.20 1824 27.9433 10280.00 10341.20 101.39 1825 27.9564 10419.00 10342.60 102.07 1826 27.9695 10442.00 10343.80 102.19 1827 27.9827 10459.00 10345.70 102.27 1828 27.9958 10420.00 10348.80 102.08 1829 28.0089 10556.00 10355.60 102.74 1830 28.0221 10429.00 10375.00 102.12 1831 28.0352 10450.00 10407.80 102.22 1832 28.0483 10672.00 10474.70 103.31 1833 28.0614 10948.00 10608.00 104.63 1834 28.0746 11285.00 10868.10 106.23 1835 28.0877 11833.00 11348.80 108.78 1836 28.1008 12591.00 12151.80 112.21 1837 28.1140 13825.00 13289.50 117.58 1838 28.1271 14766.00 14563.50 121.51 1839 28.1402 15634.00 15529.00 125.04 1840 28.1534 15631.00 15831.50 125.02 1841 28.1665 15464.00 15548.10 124.35 1842 28.1796 14953.00 15027.80 122.28 1843 28.1928 14696.00 14566.70 121.23 1844 28.2059 14344.00 14214.10 119.77 1845 28.2190 14056.00 13819.10 118.56 1846 28.2321 13478.00 13276.80 116.10 1847 28.2453 12675.00 12627.90 112.58 1848 28.2584 12151.00 11986.00 110.23 1849 28.2715 11580.00 11456.90 107.61 1850 28.2847 11257.00 11104.00 106.10 1851 28.2978 11212.00 10935.30 105.89 1852 28.3109 11303.00 10946.40 106.32 1853 28.3241 11624.00 11134.70 107.82 1854 28.3372 11878.00 11519.00 108.99 1855 28.3503 12545.00 12104.50 112.00 1856 28.3634 13343.00 12831.50 115.51 1857 28.3766 14271.00 13542.50 119.46 1858 28.3897 14749.00 14043.20 121.44 1859 28.4028 15166.00 14246.40 123.15 1860 28.4160 15140.00 14250.00 123.04 1861 28.4291 15168.00 14226.40 123.16 1862 28.4422 15400.00 14313.10 124.10 1863 28.4554 15506.00 14556.80 124.52 1864 28.4685 16113.00 14929.50 126.94 1865 28.4816 16257.00 15357.80 127.50 1866 28.4947 16613.00 15752.70 128.89 1867 28.5079 16765.00 16034.40 129.48 1868 28.5210 16731.00 16132.30 129.35 1869 28.5341 16659.00 16001.90 129.07 1870 28.5473 15928.00 15667.90 126.21 1871 28.5604 15663.00 15215.40 125.15 1872 28.5735 15348.00 14719.00 123.89 1873 28.5867 14551.00 14223.10 120.63 1874 28.5998 14013.00 13739.80 118.38 1875 28.6129 13500.00 13291.50 116.19 1876 28.6261 13094.00 12941.70 114.43 1877 28.6392 12729.00 12771.90 112.82 1878 28.6523 12639.00 12822.30 112.42 1879 28.6654 13005.00 13044.30 114.04 1880 28.6786 13183.00 13293.00 114.82 1881 28.6917 13303.00 13411.30 115.34 1882 28.7048 13304.00 13345.20 115.34 1883 28.7180 12945.00 13160.10 113.78 1884 28.7311 12801.00 12965.40 113.14 1885 28.7442 12729.00 12837.70 112.82 1886 28.7574 12919.00 12802.80 113.66 1887 28.7705 12866.00 12873.50 113.43 1888 28.7836 13033.00 13067.90 114.16 1889 28.7967 13384.00 13361.10 115.69 1890 28.8099 13663.00 13631.00 116.89 1891 28.8230 13813.00 13699.90 117.53 1892 28.8361 13609.00 13514.80 116.66 1893 28.8493 13248.00 13171.20 115.10 1894 28.8624 13098.00 12797.90 114.45 1895 28.8755 12525.00 12482.10 111.92 1896 28.8887 12295.00 12196.60 110.88 1897 28.9018 12123.00 11874.40 110.10 1898 28.9149 11525.00 11499.40 107.36 1899 28.9280 11163.00 11096.80 105.65 1900 28.9412 10658.00 10716.50 103.24 1901 28.9543 10398.00 10392.70 101.97 1902 28.9674 10144.00 10147.10 100.72 1903 28.9806 10115.00 9981.45 100.57 1904 28.9937 10056.00 9888.85 100.28 1905 29.0068 9909.00 9862.76 99.54 1906 29.0200 10068.00 9903.25 100.34 1907 29.0331 10167.00 10015.50 100.83 1908 29.0462 10322.00 10203.50 101.60 1909 29.0594 10623.00 10464.60 103.07 1910 29.0725 11131.00 10800.20 105.50 1911 29.0856 11204.00 11236.40 105.85 1912 29.0987 11937.00 11800.00 109.26 1913 29.1119 12426.00 12436.10 111.47 1914 29.1250 12958.00 12963.60 113.83 1915 29.1381 13175.00 13192.40 114.78 1916 29.1513 13036.00 13094.40 114.18 1917 29.1644 13051.00 12800.10 114.24 1918 29.1775 12524.00 12469.60 111.91 1919 29.1907 12453.00 12179.90 111.59 1920 29.2038 11995.00 11897.70 109.52 1921 29.2169 11645.00 11566.30 107.91 1922 29.2300 11372.00 11196.40 106.64 1923 29.2432 10887.00 10827.00 104.34 1924 29.2563 10490.00 10509.10 102.42 1925 29.2694 10405.00 10273.90 102.00 1926 29.2826 10070.00 10124.60 100.35 1927 29.2957 9876.00 10022.20 99.38 1928 29.3088 9931.00 9949.85 99.65 1929 29.3220 10064.00 9905.81 100.32 1930 29.3351 9780.00 9898.50 98.89 1931 29.3482 9722.00 9946.62 98.60 1932 29.3613 10143.00 10065.80 100.71 1933 29.3745 10316.00 10267.70 101.57 1934 29.3876 10520.00 10543.10 102.57 1935 29.4007 10930.00 10859.30 104.55 1936 29.4139 11201.00 11141.90 105.83 1937 29.4270 11245.00 11317.00 106.04 1938 29.4401 11322.00 11374.40 106.40 1939 29.4533 11306.00 11367.80 106.33 1940 29.4664 11369.00 11390.20 106.63 1941 29.4795 11383.00 11538.80 106.69 1942 29.4926 11529.00 11893.20 107.37 1943 29.5058 12120.00 12454.50 110.09 1944 29.5189 12658.00 13103.70 112.51 1945 29.5320 13176.00 13545.60 114.79 1946 29.5452 12938.00 13530.50 113.75 1947 29.5583 12582.00 13116.00 112.17 1948 29.5714 12360.00 12564.10 111.18 1949 29.5846 11840.00 12112.80 108.81 1950 29.5977 11538.00 11831.50 107.42 1951 29.6108 11443.00 11594.50 106.97 1952 29.6240 11295.00 11271.50 106.28 1953 29.6371 10731.00 10845.30 103.59 1954 29.6502 10214.00 10385.10 101.06 1955 29.6633 9937.00 9972.32 99.68 1956 29.6765 9678.00 9656.24 98.38 1957 29.6896 9413.00 9440.51 97.02 1958 29.7027 9104.00 9306.30 95.41 1959 29.7159 9204.00 9222.67 95.94 1960 29.7290 9098.00 9167.71 95.38 1961 29.7421 9053.00 9129.07 95.15 1962 29.7553 8911.00 9100.79 94.40 1963 29.7684 8988.00 9080.94 94.81 1964 29.7815 8905.00 9068.50 94.37 1965 29.7946 8883.00 9062.49 94.25 1966 29.8078 8965.00 9060.05 94.68 1967 29.8209 8866.00 9058.17 94.16 1968 29.8340 8881.00 9054.21 94.24 1969 29.8472 8874.00 9047.78 94.20 1970 29.8603 8979.00 9036.99 94.76 1971 29.8734 8829.00 9030.60 93.96 1972 29.8866 9001.00 9025.70 94.87 1973 29.8997 8765.00 9022.12 93.62 1974 29.9128 8907.00 9019.37 94.38 1975 29.9259 9094.00 9017.41 95.36 1976 29.9391 8883.00 9017.61 94.25 1977 29.9522 9105.00 9023.60 95.42 1978 29.9653 9189.00 9043.51 95.86 1979 29.9785 9125.00 9085.49 95.52 1980 29.9916 9100.00 9164.32 95.39 1981 30.0047 9270.00 9299.49 96.28 1982 30.0179 9571.00 9513.18 97.83 1983 30.0310 10112.00 9826.26 100.56 1984 30.0441 10594.00 10257.00 102.93 1985 30.0573 11076.00 10815.40 105.24 1986 30.0704 11514.00 11513.30 107.30 1987 30.0835 12477.00 12341.10 111.70 1988 30.0966 13264.00 13204.10 115.17 1989 30.1098 14364.00 13902.60 119.85 1990 30.1229 14688.00 14244.00 121.19 1991 30.1360 14578.00 14198.30 120.74 1992 30.1492 14366.00 13898.00 119.86 1993 30.1623 13993.00 13515.40 118.29 1994 30.1754 13244.00 13165.90 115.08 1995 30.1886 13225.00 12845.30 115.00 1996 30.2017 12888.00 12555.90 113.53 1997 30.2148 12458.00 12351.80 111.61 1998 30.2279 12335.00 12292.00 111.06 1999 30.2411 12199.00 12416.30 110.45 2000 30.2542 11906.00 12628.30 109.11 2001 30.2673 11855.00 12742.80 108.88 2002 30.2805 11882.00 12632.90 109.00 2003 30.2936 11535.00 12361.90 107.40 2004 30.3067 11282.00 12069.60 106.22 2005 30.3199 11224.00 11881.50 105.94 2006 30.3330 11209.00 11788.30 105.87 2007 30.3461 11109.00 11676.20 105.40 2008 30.3592 10910.00 11441.40 104.45 2009 30.3724 10618.00 11082.50 103.04 2010 30.3855 10145.00 10661.30 100.72 2011 30.3986 9973.00 10262.10 99.86 2012 30.4118 9777.00 9932.68 98.88 2013 30.4249 9436.00 9681.09 97.14 2014 30.4380 9353.00 9491.67 96.71 2015 30.4512 8994.00 9348.06 94.84 2016 30.4643 9119.00 9239.44 95.49 2017 30.4774 9025.00 9162.58 95.00 2018 30.4906 8778.00 9110.05 93.69 2019 30.5037 8852.00 9071.37 94.09 2020 30.5168 8828.00 9035.00 93.96 2021 30.5299 8686.00 8997.39 93.20 2022 30.5431 8719.00 8963.33 93.38 2023 30.5562 8510.00 8939.87 92.25 2024 30.5693 8452.00 8930.97 91.93 2025 30.5825 8398.00 8935.84 91.64 2026 30.5956 8584.00 8947.76 92.65 2027 30.6087 8650.00 8956.73 93.01 2028 30.6219 8663.00 8952.69 93.08 2029 30.6350 8548.00 8932.24 92.46 2030 30.6481 8695.00 8900.94 93.25 2031 30.6612 8452.00 8868.15 91.93 2032 30.6744 8624.00 8840.71 92.87 2033 30.6875 8655.00 8819.97 93.03 2034 30.7006 8586.00 8802.54 92.66 2035 30.7138 8625.00 8785.23 92.87 2036 30.7269 8406.00 8767.83 91.68 2037 30.7400 8323.00 8752.17 91.23 2038 30.7532 8496.00 8740.42 92.17 2039 30.7663 8272.00 8734.03 90.95 2040 30.7794 8505.00 8732.51 92.22 2041 30.7925 8453.00 8735.35 91.94 2042 30.8057 8533.00 8741.17 92.37 2043 30.8188 8643.00 8749.66 92.97 2044 30.8319 8621.00 8768.65 92.85 2045 30.8451 8717.00 8784.38 93.36 2046 30.8582 8834.00 8805.41 93.99 2047 30.8713 8981.00 8835.10 94.77 2048 30.8845 9059.00 8880.21 95.18 2049 30.8976 9266.00 8959.09 96.26 2050 30.9107 9567.00 9092.82 97.81 2051 30.9239 9805.00 9330.01 99.02 2052 30.9370 10444.00 9738.88 102.20 2053 30.9501 11462.00 10393.20 107.06 2054 30.9632 12528.00 11387.20 111.93 2055 30.9764 13617.00 12763.00 116.69 2056 30.9895 15360.00 14453.50 123.93 2057 31.0026 16564.00 16206.00 128.70 2058 31.0158 17914.00 17620.80 133.84 2059 31.0289 18653.00 18428.40 136.58 2060 31.0420 19140.00 18818.40 138.35 2061 31.0552 19190.00 19209.10 138.53 2062 31.0683 19379.00 19863.40 139.21 2063 31.0814 20132.00 20631.30 141.89 2064 31.0945 20275.00 21034.20 142.39 2065 31.1077 19898.00 20707.20 141.06 2066 31.1208 18772.00 19729.20 137.01 2067 31.1339 17644.00 18465.20 132.83 2068 31.1471 16498.00 17273.50 128.45 2069 31.1602 15757.00 16325.40 125.53 2070 31.1733 15197.00 15560.50 123.28 2071 31.1865 14565.00 14852.30 120.69 2072 31.1996 13879.00 14101.50 117.81 2073 31.2127 13139.00 13285.20 114.62 2074 31.2258 12142.00 12463.20 110.19 2075 31.2390 11544.00 11735.70 107.44 2076 31.2521 11362.00 11172.90 106.59 2077 31.2652 10921.00 10795.40 104.50 2078 31.2784 10617.00 10557.80 103.04 2079 31.2915 10336.00 10378.60 101.67 2080 31.3046 10191.00 10191.30 100.95 2081 31.3178 9814.00 9977.05 99.07 2082 31.3309 9592.00 9758.84 97.94 2083 31.3440 9360.00 9572.99 96.75 2084 31.3571 9118.00 9445.75 95.49 2085 31.3703 9265.00 9376.26 96.25 2086 31.3834 9070.00 9343.78 95.24 2087 31.3965 8870.00 9319.86 94.18 2088 31.4097 8835.00 9282.17 93.99 2089 31.4228 8827.00 9221.07 93.95 2090 31.4359 8778.00 9142.41 93.69 2091 31.4491 8525.00 9069.75 92.33 2092 31.4622 8568.00 8994.21 92.56 2093 31.4753 8577.00 8929.15 92.61 2094 31.4885 8667.00 8870.73 93.10 2095 31.5016 8713.00 8813.64 93.34 2096 31.5147 8621.00 8756.79 92.85 2097 31.5278 8554.00 8704.55 92.49 2098 31.5410 8677.00 8664.14 93.15 2099 31.5541 8690.00 8647.42 93.22 2100 31.5672 8887.00 8674.40 94.27 2101 31.5804 9056.00 8779.47 95.16 2102 31.5935 9335.00 9016.33 96.62 2103 31.6066 9889.00 9453.02 99.44 2104 31.6198 10598.00 10146.90 102.95 2105 31.6329 11795.00 11093.60 108.61 2106 31.6460 12793.00 12167.50 113.11 2107 31.6591 13747.00 13104.60 117.25 2108 31.6723 14243.00 13635.50 119.34 2109 31.6854 14407.00 13694.90 120.03 2110 31.6985 14038.00 13432.50 118.48 2111 31.7117 13437.00 13058.50 115.92 2112 31.7248 13229.00 12719.60 115.02 2113 31.7379 12850.00 12419.60 113.36 2114 31.7511 12563.00 12073.80 112.08 2115 31.7642 12014.00 11635.70 109.61 2116 31.7773 11529.00 11101.10 107.37 2117 31.7904 10917.00 10541.10 104.48 2118 31.8036 10112.00 10026.20 100.56 2119 31.8167 9971.00 9627.56 99.85 2120 31.8298 9890.00 9393.48 99.45 2121 31.8430 9985.00 9392.41 99.93 2122 31.8561 10293.00 9697.00 101.45 2123 31.8692 11010.00 10352.30 104.93 2124 31.8824 11772.00 11319.50 108.50 2125 31.8955 12791.00 12370.20 113.10 2126 31.9086 13316.00 13107.50 115.39 2127 31.9218 13424.00 13295.10 115.86 2128 31.9349 13110.00 13026.00 114.50 2129 31.9480 12607.00 12599.40 112.28 2130 31.9611 12513.00 12280.40 111.86 2131 31.9743 12068.00 12185.50 109.85 2132 31.9874 12244.00 12179.10 110.65 2133 32.0005 11826.00 12060.50 108.75 2134 32.0137 11482.00 11730.60 107.15 2135 32.0268 10874.00 11232.50 104.28 2136 32.0399 10393.00 10670.00 101.95 2137 32.0531 9918.00 10163.90 99.59 2138 32.0662 9428.00 9769.86 97.10 2139 32.0793 9328.00 9492.79 96.58 2140 32.0924 9187.00 9301.30 95.85 2141 32.1056 9221.00 9162.59 96.03 2142 32.1187 9148.00 9061.45 95.65 2143 32.1318 8914.00 9005.82 94.41 2144 32.1450 8936.00 9008.91 94.53 2145 32.1581 8975.00 9077.25 94.74 2146 32.1712 9251.00 9212.08 96.18 2147 32.1844 9461.00 9396.99 97.27 2148 32.1975 9506.00 9607.39 97.50 2149 32.2106 9768.00 9840.83 98.83 2150 32.2237 10328.00 10136.20 101.63 2151 32.2369 10650.00 10548.90 103.20 2152 32.2500 11122.00 11112.40 105.46 2153 32.2631 11583.00 11793.70 107.62 2154 32.2763 12070.00 12476.00 109.86 2155 32.2894 12427.00 13003.00 111.48 2156 32.3025 12913.00 13291.90 113.64 2157 32.3157 13069.00 13414.00 114.32 2158 32.3288 13284.00 13579.20 115.26 2159 32.3419 14011.00 14054.90 118.37 2160 32.3551 14898.00 15047.70 122.06 2161 32.3682 16317.00 16566.80 127.74 2162 32.3813 18117.00 18382.00 134.60 2163 32.3944 19025.00 20248.40 137.93 2164 32.4076 20735.00 22006.20 144.00 2165 32.4207 21434.00 23297.10 146.40 2166 32.4338 22329.00 23772.80 149.43 2167 32.4470 22071.00 23501.30 148.56 2168 32.4601 21440.00 22707.30 146.42 2169 32.4732 20695.00 21695.50 143.86 2170 32.4864 19702.00 20829.90 140.36 2171 32.4995 19010.00 20164.40 137.88 2172 32.5126 18224.00 19402.40 135.00 2173 32.5257 17459.00 18379.40 132.13 2174 32.5389 16198.00 17119.80 127.27 2175 32.5520 14805.00 15772.80 121.68 2176 32.5651 13917.00 14551.00 117.97 2177 32.5783 13012.00 13557.20 114.07 2178 32.5914 12480.00 12755.20 111.71 2179 32.6045 11569.00 12066.10 107.56 2180 32.6177 11297.00 11445.10 106.29 2181 32.6308 10624.00 10892.80 103.07 2182 32.6439 10150.00 10429.00 100.75 2183 32.6570 9943.00 10059.40 99.71 2184 32.6702 9533.00 9784.26 97.64 2185 32.6833 9524.00 9585.24 97.59 2186 32.6964 9424.00 9453.39 97.08 2187 32.7096 9272.00 9379.82 96.29 2188 32.7227 9253.00 9359.88 96.19 2189 32.7358 9470.00 9409.28 97.31 2190 32.7490 9567.00 9589.12 97.81 2191 32.7621 9829.00 9909.84 99.14 2192 32.7752 10063.00 10283.70 100.32 2193 32.7883 10228.00 10495.70 101.13 2194 32.8015 10126.00 10403.90 100.63 2195 32.8146 9844.00 10072.60 99.22 2196 32.8277 9423.00 9681.14 97.07 2197 32.8409 9311.00 9397.31 96.49 2198 32.8540 9397.00 9266.57 96.94 2199 32.8671 9055.00 9201.64 95.16 2200 32.8803 8819.00 9072.75 93.91 2201 32.8934 8702.00 8841.99 93.28 2202 32.9065 8480.00 8557.09 92.09 2203 32.9197 8195.00 8289.75 90.53 2204 32.9328 7794.00 8084.36 88.28 2205 32.9459 7587.00 7954.75 87.10 2206 32.9590 7694.00 7874.30 87.72 2207 32.9722 7666.00 7828.18 87.56 2208 32.9853 7509.00 7799.84 86.65 2209 32.9984 7307.00 7780.43 85.48 2210 33.0116 7335.00 7766.60 85.64 2211 33.0247 7395.00 7751.88 85.99 2212 33.0378 7615.00 7742.78 87.26 2213 33.0510 7660.00 7737.38 87.52 2214 33.0641 7472.00 7734.40 86.44 2215 33.0772 7475.00 7725.59 86.46 2216 33.0903 7361.00 7723.95 85.80 2217 33.1035 7411.00 7717.93 86.09 2218 33.1166 7528.00 7713.17 86.76 2219 33.1297 7546.00 7711.23 86.87 2220 33.1429 7610.00 7712.51 87.24 2221 33.1560 7567.00 7718.67 86.99 2222 33.1691 7653.00 7748.86 87.48 2223 33.1823 8007.00 7818.48 89.48 2224 33.1954 8013.00 7990.06 89.52 2225 33.2085 8358.00 8342.90 91.42 2226 33.2216 9069.00 8974.24 95.23 2227 33.2348 10050.00 9921.50 100.25 2228 33.2479 10985.00 11064.10 104.81 2229 33.2610 11869.00 12043.50 108.94 2230 33.2742 12576.00 12478.70 112.14 2231 33.2873 12378.00 12301.20 111.26 2232 33.3004 11997.00 11765.30 109.53 2233 33.3136 11409.00 11211.60 106.81 2234 33.3267 11266.00 10869.20 106.14 2235 33.3398 11262.00 10743.50 106.12 2236 33.3530 11010.00 10651.50 104.93 2237 33.3661 10779.00 10408.90 103.82 2238 33.3792 10296.00 10018.40 101.47 2239 33.3923 9974.00 9619.28 99.87 2240 33.4055 9633.00 9405.66 98.15 2241 33.4186 9710.00 9554.27 98.54 2242 33.4317 10144.00 10130.80 100.72 2243 33.4449 10305.00 10986.00 101.51 2244 33.4580 10728.00 11731.30 103.58 2245 33.4711 10784.00 11983.80 103.85 2246 33.4843 10697.00 11703.90 103.43 2247 33.4974 10101.00 11155.60 100.50 2248 33.5105 9969.00 10647.60 99.84 2249 33.5236 9709.00 10379.90 98.53 2250 33.5368 9708.00 10320.90 98.53 2251 33.5499 9471.00 10258.40 97.32 2252 33.5630 9342.00 10020.10 96.65 2253 33.5762 9001.00 9605.48 94.87 2254 33.5893 8595.00 9114.79 92.71 2255 33.6024 8303.00 8660.90 91.12 2256 33.6156 8146.00 8318.06 90.26 2257 33.6287 8006.00 8104.41 89.48 2258 33.6418 7849.00 8005.92 88.59 2259 33.6549 7949.00 8004.56 89.16 2260 33.6681 8118.00 8100.13 90.10 2261 33.6812 8261.00 8306.79 90.89 2262 33.6943 8549.00 8633.51 92.46 2263 33.7075 8976.00 9052.57 94.74 2264 33.7206 9452.00 9480.74 97.22 2265 33.7337 9990.00 9802.33 99.95 2266 33.7469 10038.00 9951.04 100.19 2267 33.7600 9870.00 9952.43 99.35 2268 33.7731 9943.00 9879.42 99.71 2269 33.7863 9640.00 9788.83 98.18 2270 33.7994 9500.00 9695.35 97.47 2271 33.8125 9486.00 9576.76 97.40 2272 33.8256 9246.00 9404.31 96.16 2273 33.8388 8954.00 9175.10 94.63 2274 33.8519 8624.00 8913.37 92.87 2275 33.8650 8526.00 8648.77 92.34 2276 33.8782 8187.00 8400.30 90.48 2277 33.8913 7964.00 8179.56 89.24 2278 33.9044 7744.00 7998.64 88.00 2279 33.9176 7771.00 7879.38 88.15 2280 33.9307 7836.00 7868.19 88.52 2281 33.9438 8098.00 8045.78 89.99 2282 33.9569 8363.00 8494.49 91.45 2283 33.9701 8830.00 9197.84 93.97 2284 33.9832 9157.00 9939.69 95.69 2285 33.9963 9624.00 10342.70 98.10 2286 34.0095 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3588.00 3576.96 59.90 5421 75.1729 3588.00 3570.58 59.90 5422 75.1860 3489.00 3566.31 59.07 5423 75.1992 3453.00 3564.55 58.76 5424 75.2123 3565.00 3564.60 59.71 5425 75.2254 3522.00 3565.65 59.35 5426 75.2385 3537.00 3566.45 59.47 5427 75.2517 3442.00 3566.50 58.67 5428 75.2648 3542.00 3565.16 59.51 5429 75.2779 3548.00 3562.40 59.57 5430 75.2911 3520.00 3559.57 59.33 5431 75.3042 3556.00 3559.27 59.63 5432 75.3173 3561.00 3564.61 59.67 5433 75.3305 3667.00 3576.22 60.56 5434 75.3436 3630.00 3590.54 60.25 5435 75.3567 3684.00 3600.94 60.70 5436 75.3699 3585.00 3602.62 59.87 5437 75.3830 3584.00 3596.86 59.87 5438 75.3961 3563.00 3587.53 59.69 5439 75.4092 3512.00 3579.07 59.26 5440 75.4224 3601.00 3574.54 60.01 5441 75.4355 3552.00 3573.67 59.60 5442 75.4486 3593.00 3575.15 59.94 5443 75.4618 3534.00 3577.21 59.45 5444 75.4749 3562.00 3578.61 59.68 5445 75.4880 3650.00 3579.20 60.42 5446 75.5012 3546.00 3578.69 59.55 5447 75.5143 3597.00 3578.43 59.97 5448 75.5274 3567.00 3580.48 59.72 5449 75.5406 3537.00 3587.14 59.47 5450 75.5537 3688.00 3599.15 60.73 5451 75.5668 3669.00 3614.50 60.57 5452 75.5799 3665.00 3629.26 60.54 5453 75.5931 3602.00 3640.28 60.02 5454 75.6062 3577.00 3646.74 59.81 5455 75.6193 3676.00 3648.57 60.63 5456 75.6325 3683.00 3647.11 60.69 5457 75.6456 3556.00 3643.42 59.63 5458 75.6587 3634.00 3638.86 60.28 5459 75.6719 3641.00 3631.90 60.34 5460 75.6850 3616.00 3623.21 60.13 5461 75.6981 3588.00 3612.92 59.90 5462 75.7112 3686.00 3601.35 60.71 5463 75.7244 3634.00 3589.10 60.28 5464 75.7375 3596.00 3577.08 59.97 5465 75.7506 3571.00 3566.39 59.76 5466 75.7638 3585.00 3558.54 59.87 5467 75.7769 3502.00 3554.68 59.18 5468 75.7900 3629.00 3556.03 60.24 5469 75.8032 3702.00 3563.36 60.84 5470 75.8163 3535.00 3576.39 59.46 5471 75.8294 3703.00 3593.03 60.85 5472 75.8425 3495.00 3608.99 59.12 5473 75.8557 3587.00 3619.37 59.89 5474 75.8688 3689.00 3621.86 60.74 5475 75.8819 3698.00 3617.41 60.81 5476 75.8951 3621.00 3609.08 60.17 5477 75.9082 3722.00 3599.18 61.01 5478 75.9213 3558.00 3590.03 59.65 5479 75.9345 3550.00 3582.44 59.58 5480 75.9476 3570.00 3576.36 59.75 5481 75.9607 3554.00 3571.46 59.62 5482 75.9738 3549.00 3567.54 59.57 5483 75.9870 3500.00 3564.31 59.16 5484 76.0001 3653.00 3561.79 60.44 5485 76.0132 3653.00 3560.42 60.44 5486 76.0264 3607.00 3561.28 60.06 5487 76.0395 3627.00 3564.81 60.22 5488 76.0526 3583.00 3571.57 59.86 5489 76.0658 3494.00 3580.79 59.11 5490 76.0789 3661.00 3591.19 60.51 5491 76.0920 3591.00 3602.13 59.92 5492 76.1051 3599.00 3613.28 59.99 5493 76.1183 3652.00 3623.60 60.43 5494 76.1314 3618.00 3631.50 60.15 5495 76.1445 3586.00 3635.79 59.88 5496 76.1577 3578.00 3636.56 59.82 5497 76.1708 3645.00 3633.27 60.37 5498 76.1839 3646.00 3626.85 60.38 5499 76.1971 3533.00 3618.09 59.44 5500 76.2102 3550.00 3607.91 59.58 5501 76.2233 3699.00 3597.26 60.82 5502 76.2365 3623.00 3586.92 60.19 5503 76.2496 3645.00 3577.53 60.37 5504 76.2627 3626.00 3569.68 60.22 5505 76.2758 3643.00 3564.30 60.36 5506 76.2890 3567.00 3562.41 59.72 5507 76.3021 3645.00 3565.10 60.37 5508 76.3152 3648.00 3572.86 60.40 5509 76.3284 3607.00 3584.81 60.06 5510 76.3415 3698.00 3598.32 60.81 5511 76.3546 3617.00 3610.30 60.14 5512 76.3678 3697.00 3617.86 60.80 5513 76.3809 3635.00 3621.00 60.29 5514 76.3940 3674.00 3621.18 60.61 5515 76.4071 3704.00 3620.80 60.86 5516 76.4203 3587.00 3622.00 59.89 5517 76.4334 3729.00 3625.20 61.07 5518 76.4465 3605.00 3630.39 60.04 5519 76.4597 3527.00 3636.99 59.39 5520 76.4728 3671.00 3643.76 60.59 5521 76.4859 3687.00 3648.89 60.72 5522 76.4991 3690.00 3650.88 60.75 5523 76.5122 3648.00 3649.43 60.40 5524 76.5253 3671.00 3645.11 60.59 5525 76.5385 3667.00 3638.80 60.56 5526 76.5516 3636.00 3631.50 60.30 5527 76.5647 3625.00 3623.75 60.21 5528 76.5778 3612.00 3615.54 60.10 5529 76.5910 3649.00 3607.16 60.41 5530 76.6041 3594.00 3599.05 59.95 5531 76.6172 3637.00 3591.94 60.31 5532 76.6304 3626.00 3586.80 60.22 5533 76.6435 3583.00 3584.22 59.86 5534 76.6566 3576.00 3584.15 59.80 5535 76.6698 3654.00 3586.11 60.45 5536 76.6829 3559.00 3589.57 59.66 5537 76.6960 3608.00 3593.62 60.07 5538 76.7091 3627.00 3596.98 60.22 5539 76.7223 3628.00 3598.74 60.23 5540 76.7354 3759.00 3598.34 61.31 5541 76.7485 3648.00 3595.91 60.40 5542 76.7617 3663.00 3591.89 60.52 5543 76.7748 3632.00 3586.93 60.27 5544 76.7879 3675.00 3581.50 60.62 5545 76.8011 3657.00 3576.18 60.47 5546 76.8142 3489.00 3570.63 59.07 5547 76.8273 3689.00 3565.80 60.74 5548 76.8404 3603.00 3561.17 60.03 5549 76.8536 3646.00 3557.75 60.38 5550 76.8667 3461.00 3555.83 58.83 5551 76.8798 3509.00 3555.43 59.24 5552 76.8930 3533.00 3556.43 59.44 5553 76.9061 3609.00 3559.01 60.08 5554 76.9192 3543.00 3563.64 59.52 5555 76.9324 3585.00 3571.37 59.87 5556 76.9455 3558.00 3581.98 59.65 5557 76.9586 3657.00 3593.27 60.47 5558 76.9717 3653.00 3600.67 60.44 5559 76.9849 3523.00 3599.37 59.35 5560 76.9980 3585.00 3588.70 59.87 5561 77.0111 3572.00 3572.40 59.77 5562 77.0243 3655.00 3556.45 60.46 5563 77.0374 3558.00 3546.44 59.65 5564 77.0505 3528.00 3545.43 59.40 5565 77.0637 3589.00 3552.60 59.91 5566 77.0768 3506.00 3563.38 59.21 5567 77.0899 3538.00 3572.46 59.48 5568 77.1031 3554.00 3577.35 59.62 5569 77.1162 3540.00 3578.34 59.50 5570 77.1293 3626.00 3577.67 60.22 5571 77.1424 3606.00 3577.51 60.05 5572 77.1556 3445.00 3579.67 58.69 5573 77.1687 3532.00 3584.81 59.43 5574 77.1818 3591.00 3591.06 59.92 5575 77.1950 3701.00 3595.49 60.84 5576 77.2081 3481.00 3594.63 59.00 5577 77.2212 3596.00 3587.04 59.97 5578 77.2344 3450.00 3574.27 58.74 5579 77.2475 3522.00 3559.65 59.35 5580 77.2606 3503.00 3546.75 59.19 5581 77.2737 3539.00 3537.92 59.49 5582 77.2869 3540.00 3533.56 59.50 5583 77.3000 3525.00 3531.87 59.37 5584 77.3131 3509.00 3530.26 59.24 5585 77.3263 3481.00 3527.46 59.00 5586 77.3394 3534.00 3523.31 59.45 5587 77.3525 3521.00 3519.17 59.34 5588 77.3657 3418.00 3516.36 58.46 5589 77.3788 3476.00 3514.79 58.96 5590 77.3919 3474.00 3514.43 58.94 5591 77.4050 3482.00 3514.40 59.01 5592 77.4182 3600.00 3513.83 60.00 5593 77.4313 3458.00 3512.41 58.80 5594 77.4444 3456.00 3510.42 58.79 5595 77.4576 3501.00 3508.22 59.17 5596 77.4707 3542.00 3506.01 59.51 5597 77.4838 3553.00 3503.77 59.61 5598 77.4970 3585.00 3501.80 59.87 5599 77.5101 3503.00 3500.28 59.19 5600 77.5232 3646.00 3498.51 60.38 5601 77.5363 3526.00 3494.91 59.38 5602 77.5495 3652.00 3489.46 60.43 5603 77.5626 3589.00 3483.60 59.91 5604 77.5757 3527.00 3480.10 59.39 5605 77.5889 3593.00 3481.21 59.94 5606 77.6020 3525.00 3488.43 59.37 5607 77.6151 3518.00 3501.21 59.31 5608 77.6283 3489.00 3517.61 59.07 5609 77.6414 3640.00 3535.21 60.33 5610 77.6545 3492.00 3552.39 59.09 5611 77.6677 3609.00 3568.21 60.08 5612 77.6808 3638.00 3581.80 60.32 5613 77.6939 3629.00 3592.14 60.24 5614 77.7070 3589.00 3598.22 59.91 5615 77.7202 3649.00 3599.45 60.41 5616 77.7333 3582.00 3595.39 59.85 5617 77.7464 3461.00 3586.23 58.83 5618 77.7596 3547.00 3572.95 59.56 5619 77.7727 3491.00 3558.85 59.08 5620 77.7858 3565.00 3549.55 59.71 5621 77.7990 3569.00 3550.09 59.74 5622 77.8121 3599.00 3561.24 59.99 5623 77.8252 3665.00 3577.16 60.54 5624 77.8383 3508.00 3588.37 59.23 5625 77.8515 3615.00 3589.45 60.12 5626 77.8646 3488.00 3581.72 59.06 5627 77.8777 3509.00 3569.43 59.24 5628 77.8909 3501.00 3557.69 59.17 5629 77.9040 3554.00 3550.05 59.62 5630 77.9171 3581.00 3545.51 59.84 5631 77.9303 3508.00 3543.08 59.23 5632 77.9434 3552.00 3540.97 59.60 5633 77.9565 3557.00 3537.85 59.64 5634 77.9697 3574.00 3533.18 59.78 5635 77.9828 3555.00 3527.19 59.62 5636 77.9959 3460.00 3521.27 58.82 5637 78.0090 3463.00 3517.55 58.85 5638 78.0222 3505.00 3518.55 59.20 5639 78.0353 3544.00 3525.21 59.53 5640 78.0484 3490.00 3535.68 59.08 5641 78.0616 3473.00 3545.18 58.93 5642 78.0747 3455.00 3549.56 58.78 5643 78.0878 3537.00 3548.07 59.47 5644 78.1010 3442.00 3542.41 58.67 5645 78.1141 3655.00 3535.21 60.46 5646 78.1272 3429.00 3528.55 58.56 5647 78.1403 3380.00 3523.30 58.14 5648 78.1535 3537.00 3519.27 59.47 5649 78.1666 3571.00 3515.88 59.76 5650 78.1797 3463.00 3512.72 58.85 5651 78.1929 3497.00 3509.74 59.14 5652 78.2060 3540.00 3507.18 59.50 5653 78.2191 3537.00 3505.44 59.47 5654 78.2323 3560.00 3504.83 59.67 5655 78.2454 3628.00 3505.89 60.23 5656 78.2585 3490.00 3508.40 59.08 5657 78.2716 3475.00 3512.38 58.95 5658 78.2848 3478.00 3517.49 58.97 5659 78.2979 3496.00 3523.25 59.13 5660 78.3110 3578.00 3528.61 59.82 5661 78.3242 3481.00 3532.83 59.00 5662 78.3373 3486.00 3535.02 59.04 5663 78.3504 3461.00 3534.43 58.83 5664 78.3636 3504.00 3530.89 59.19 5665 78.3767 3433.00 3524.64 58.59 5666 78.3898 3398.00 3516.47 58.29 5667 78.4029 3562.00 3507.94 59.68 5668 78.4161 3553.00 3501.62 59.61 5669 78.4292 3441.00 3500.30 58.66 5670 78.4423 3555.00 3505.68 59.62 5671 78.4555 3474.00 3516.11 58.94 5672 78.4686 3449.00 3526.79 58.73 5673 78.4817 3452.00 3532.28 58.75 5674 78.4949 3525.00 3530.73 59.37 5675 78.5080 3667.00 3523.96 60.56 5676 78.5211 3596.00 3514.77 59.97 5677 78.5342 3439.00 3506.50 58.64 5678 78.5474 3481.00 3500.81 59.00 5679 78.5605 3639.00 3497.74 60.32 5680 78.5736 3458.00 3496.53 58.80 5681 78.5868 3501.00 3496.11 59.17 5682 78.5999 3431.00 3496.31 58.57 5683 78.6130 3627.00 3497.35 60.22 5684 78.6262 3524.00 3499.80 59.36 5685 78.6393 3438.00 3504.65 58.63 5686 78.6524 3583.00 3513.52 59.86 5687 78.6656 3622.00 3526.27 60.18 5688 78.6787 3600.00 3542.84 60.00 5689 78.6918 3485.00 3560.82 59.03 5690 78.7049 3482.00 3575.95 59.01 5691 78.7181 3440.00 3584.76 58.65 5692 78.7312 3542.00 3586.22 59.51 5693 78.7443 3449.00 3581.46 58.73 5694 78.7575 3595.00 3572.09 59.96 5695 78.7706 3588.00 3560.34 59.90 5696 78.7837 3533.00 3547.61 59.44 5697 78.7969 3514.00 3534.71 59.28 5698 78.8100 3487.00 3522.10 59.05 5699 78.8231 3512.00 3510.30 59.26 5700 78.8363 3541.00 3499.58 59.51 5701 78.8494 3501.00 3490.53 59.17 5702 78.8625 3549.00 3483.68 59.57 5703 78.8756 3428.00 3479.51 58.55 5704 78.8888 3493.00 3478.69 59.10 5705 78.9019 3483.00 3480.34 59.02 5706 78.9150 3504.00 3484.38 59.19 5707 78.9282 3515.00 3489.69 59.29 5708 78.9413 3513.00 3495.10 59.27 5709 78.9544 3513.00 3500.21 59.27 5710 78.9676 3493.00 3505.38 59.10 5711 78.9807 3478.00 3511.43 58.97 5712 78.9938 3422.00 3518.83 58.50 5713 79.0069 3420.00 3526.79 58.48 5714 79.0201 3491.00 3533.45 59.08 5715 79.0332 3599.00 3536.71 59.99 5716 79.0463 3510.00 3534.59 59.25 5717 79.0595 3413.00 3526.35 58.42 5718 79.0726 3501.00 3512.93 59.17 5719 79.0857 3532.00 3496.63 59.43 5720 79.0989 3541.00 3479.13 59.51 5721 79.1120 3587.00 3461.69 59.89 5722 79.1251 3541.00 3444.77 59.51 5723 79.1382 3477.00 3430.06 58.97 5724 79.1514 3375.00 3422.32 58.09 5725 79.1645 3515.00 3428.47 59.29 5726 79.1776 3655.00 3453.22 60.46 5727 79.1908 3435.00 3494.37 58.61 5728 79.2039 3508.00 3538.75 59.23 5729 79.2170 3446.00 3568.56 58.70 5730 79.2302 3450.00 3575.08 58.74 5731 79.2433 3531.00 3561.10 59.42 5732 79.2564 3469.00 3535.00 58.90 5733 79.2695 3564.00 3505.95 59.70 5734 79.2827 3375.00 3480.41 58.09 5735 79.2958 3543.00 3461.47 59.52 5736 79.3089 3457.00 3450.07 58.80 5737 79.3221 3443.00 3445.82 58.68 5738 79.3352 3476.00 3446.04 58.96 5739 79.3483 3529.00 3446.28 59.41 5740 79.3615 3571.00 3443.03 59.76 5741 79.3746 3511.00 3435.75 59.25 5742 79.3877 3415.00 3428.74 58.44 5743 79.4008 3467.00 3427.70 58.88 5744 79.4140 3435.00 3436.86 58.61 5745 79.4271 3453.00 3455.25 58.76 5746 79.4402 3529.00 3475.51 59.41 5747 79.4534 3508.00 3487.89 59.23 5748 79.4665 3551.00 3487.97 59.59 5749 79.4796 3520.00 3477.45 59.33 5750 79.4928 3459.00 3461.16 58.81 5751 79.5059 3510.00 3444.61 59.25 5752 79.5190 3429.00 3430.81 58.56 5753 79.5322 3524.00 3421.74 59.36 5754 79.5453 3428.00 3417.48 58.55 5755 79.5584 3442.00 3417.09 58.67 5756 79.5715 3464.00 3419.38 58.86 5757 79.5847 3458.00 3420.46 58.80 5758 79.5978 3503.00 3419.06 59.19 5759 79.6109 3276.00 3414.96 57.24 5760 79.6241 3374.00 3409.13 58.09 5761 79.6372 3510.00 3403.11 59.25 5762 79.6503 3546.00 3398.09 59.55 5763 79.6635 3406.00 3394.88 58.36 5764 79.6766 3416.00 3393.49 58.45 5765 79.6897 3446.00 3393.80 58.70 5766 79.7029 3315.00 3395.62 57.58 5767 79.7160 3370.00 3398.53 58.05 5768 79.7291 3348.00 3402.32 57.86 5769 79.7422 3386.00 3406.57 58.19 5770 79.7554 3514.00 3410.86 59.28 5771 79.7685 3295.00 3414.78 57.40 5772 79.7816 3493.00 3418.19 59.10 5773 79.7948 3419.00 3421.32 58.47 5774 79.8079 3451.00 3424.80 58.75 5775 79.8210 3500.00 3429.07 59.16 5776 79.8342 3417.00 3434.25 58.46 5777 79.8473 3358.00 3439.84 57.95 5778 79.8604 3487.00 3445.24 59.05 5779 79.8735 3491.00 3450.12 59.08 5780 79.8867 3493.00 3455.03 59.10 5781 79.8998 3433.00 3459.47 58.59 5782 79.9129 3407.00 3463.87 58.37 5783 79.9261 3487.00 3468.05 59.05 5784 79.9392 3466.00 3471.97 58.87 5785 79.9523 3363.00 3475.72 57.99 5786 79.9655 3517.00 3479.43 59.30 5787 79.9786 3342.00 3483.44 57.81 5788 79.9917 3499.00 3487.84 59.15 # 12. STRUCTURE-FACTOR LIST loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_observed_status _refln_d_spacing 2 0 0 14969.51 15305.07 o 11.548666 -1 0 2 5135.38 5115.31 o 8.288095 0 0 2 23.47 9.70 < 7.906760 -2 0 2 1058.53 735.51 o 7.699489 3 0 0 469.39 326.05 o 7.699111 1 0 2 7564.89 7270.56 o 6.870837 -3 0 2 61.96 46.94 o 6.604111 1 1 0 12380.67 12634.26 o 6.490474 0 1 1 446.23 462.40 o 6.218186 -1 1 1 5592.07 5788.60 o 6.192119 2 1 0 226.83 231.65 o 5.835936 1 1 1 10419.73 10646.48 o 5.832778 4 0 0 1005.77 1029.05 o 5.774333 -2 1 1 10605.74 10846.78 o 5.768895 2 0 2 9534.85 9745.47 o 5.762127 -4 0 2 9240.78 11186.92 o 5.526889 -1 1 2 6347.08 7041.49 o 5.239889 2 1 1 4088.70 4583.55 o 5.221879 -3 1 1 2295.10 2352.44 o 5.145896 0 1 2 2167.72 2226.67 o 5.139409 -2 1 2 6372.06 6710.15 o 5.081173 3 1 0 3318.22 3494.28 o 5.081064 3 0 2 144.62 130.47 o 4.833490 1 1 2 5138.79 4647.49 o 4.819830 -3 1 2 47021.26 45922.26 o 4.724979 -5 0 2 21993.34 19417.33 o 4.647665 5 0 0 5800.42 5421.03 o 4.619466 3 1 1 7900.60 7968.28 o 4.578611 -4 1 1 8924.59 8452.26 o 4.507022 4 1 0 2778.79 2783.40 o 4.391414 2 1 2 166.35 166.07 o 4.386038 -4 1 2 16599.18 16442.77 o 4.279578 -1 1 3 3243.35 3222.82 o 4.273361 -2 1 3 112.26 114.73 o 4.248045 0 1 3 6263.24 7113.09 o 4.157510 -2 0 4 6131.19 6870.53 o 4.144047 -1 0 4 846.18 1006.90 o 4.108859 4 0 2 6412.87 7630.89 o 4.108686 -3 1 3 3806.08 4045.75 o 4.088696 -3 0 4 1616.00 1350.47 o 4.049620 4 1 1 4306.05 4090.55 o 4.000671 -6 0 2 36988.75 34337.20 o 3.965222 0 0 4 5094.08 4790.40 o 3.953380 -5 1 1 1296.02 1230.05 o 3.939242 3 1 2 3830.95 3656.82 o 3.932406 1 1 3 6153.77 5889.93 o 3.931489 -4 0 4 46.17 48.62 o 3.849745 6 0 0 8.69 9.83 o 3.849555 -4 1 3 58.42 67.87 o 3.835664 -5 1 2 1286.31 1469.12 o 3.830369 5 1 0 2590.51 2863.85 o 3.814538 1 0 4 68197.44 70301.42 o 3.714362 2 1 3 2831.58 1972.38 o 3.644459 -5 0 4 1232.95 230.00 < 3.587040 5 0 2 160.16 147.08 o 3.548425 -5 1 3 1377.57 1258.75 o 3.538374 -2 1 4 3566.58 3237.85 o 3.533454 5 1 1 311.53 275.72 o 3.513524 -1 1 4 1155.11 1020.29 o 3.511564 4 1 2 3705.69 3273.18 o 3.511456 -3 1 4 2216.98 2134.62 o 3.474370 -6 1 1 12974.06 12500.84 o 3.462600 -7 0 2 11143.89 11404.97 o 3.436921 2 0 4 5420.53 5549.83 o 3.435419 -6 1 2 3273.82 3241.68 o 3.420631 0 1 4 376.56 351.94 o 3.413020 0 2 0 21092.66 19944.35 o 3.381490 1 2 0 2052.49 2362.42 o 3.345824 -4 1 4 354.52 408.06 o 3.345667 6 1 0 8378.12 9654.20 o 3.345543 3 1 3 217.42 250.70 o 3.340197 0 2 1 3093.91 3231.00 o 3.306734 -1 2 1 277.35 289.78 o 3.302796 -6 0 4 2569.13 2676.16 o 3.302055 7 0 0 417.49 433.19 o 3.299619 1 1 4 1511.62 1205.52 o 3.255655 2 2 0 1497.87 1387.13 o 3.245237 1 2 1 0.04 0.04 o 3.244694 -6 1 3 42.92 43.67 o 3.235553 -2 2 1 66.81 71.60 o 3.233571 -5 1 4 6126.25 6280.58 o 3.168895 3 0 4 37.62 43.37 o 3.150829 5 1 2 5154.39 6133.13 o 3.142177 -1 2 2 2890.96 3259.68 o 3.130930 2 2 1 4225.41 4692.93 o 3.127076 6 1 1 790.99 790.80 o 3.111646 6 0 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270.37 307.46 o 1.424195 -17 0 4 11.61 12.85 o 1.424108 -9 1 11 13.62 14.69 o 1.423360 0 4 6 106.23 119.88 o 1.423092 5 4 4 176.95 199.68 o 1.423080 14 1 3 264.45 298.09 o 1.421609 -13 3 1 606.71 693.65 < 1.419869 8 2 7 62.07 71.98 < 1.419736 4 0 10 206.56 233.36 < 1.419713 5 3 7 52.34 35.96 < 1.417690 -2 3 9 428.66 316.59 o 1.416523 -6 3 9 67.74 49.85 o 1.416015 -15 1 8 1445.06 1037.61 o 1.413088 12 2 4 315.10 241.39 o 1.412998 4 2 9 310.15 235.82 o 1.412824 -13 0 10 1382.67 1007.88 o 1.412291 -17 0 2 482.79 363.34 o 1.412235 -6 4 6 17.20 13.05 o 1.411906 9 4 0 269.88 204.80 o 1.411885 16 1 0 0.72 0.55 o 1.411779 11 1 6 137.09 112.99 o 1.411467 7 3 6 21.35 16.89 o 1.411188 -12 2 9 355.97 294.35 o 1.410812 6 1 9 519.01 437.08 o 1.410418 -8 4 5 17.16 14.94 o 1.409279 8 1 8 257.35 211.14 o 1.408925 -15 2 6 7.14 6.09 < 1.408442 -14 1 9 71.47 59.95 < 1.407918 13 2 3 53.01 49.75 < 1.407442 11 2 5 14.16 14.76 < 1.406733 1 4 6 106.99 93.95 < 1.406370 0 1 11 330.41 389.42 < 1.406175 1 2 10 144.74 145.04 < 1.406104 -13 3 5 16.29 17.92 < 1.405980 -9 4 4 91.77 94.14 < 1.405793 -10 3 8 0.31 0.21 < 1.403518 -1 3 9 1399.85 944.46 < 1.403512 -7 3 9 23.27 14.77 < 1.402771 -10 2 10 407.21 227.31 < 1.401425 15 2 0 144.29 83.85 < 1.401368 15 1 2 123.03 71.49 < 1.401241 3 3 8 53.98 32.96 < 1.401208 -10 1 11 0.89 0.54 < 1.398922 -16 1 7 45.51 27.81 < 1.397308 8 4 2 173.78 124.93 < 1.397160 7 4 3 1105.27 820.78 < 1.396943 4 4 5 130.92 99.04 < 1.396304 13 3 0 0.17 0.14 < 1.395422 11 3 3 260.20 207.45 < 1.394509 10 3 4 0.10 0.07 < 1.394207 -17 1 4 569.17 485.60 < 1.393547 -17 1 3 4.48 3.91 < 1.393325 -7 4 6 447.25 291.66 < 1.392026 -17 0 6 134.04 83.28 < 1.391116 14 2 2 204.07 129.58 < 1.390472 4 1 10 1098.94 630.79 < 1.389428 10 2 6 475.95 311.49 < 1.389106 -10 4 2 72.19 64.54 < 1.386569 9 4 1 317.03 235.83 < 1.386010 0 3 9 18.88 14.20 < 1.385837 6 4 4 258.90 197.27 < 1.385375 2 4 6 3.81 2.91 < 1.385215 10 1 7 324.73 293.66 o 1.385160 -8 3 9 623.10 463.22 o 1.384887 12 3 2 123.65 96.88 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3 3 6.46 5.61 < 1.372835 -15 2 7 360.98 315.62 o 1.371991 -11 2 10 91.35 68.93 < 1.371062 -11 1 11 23.12 19.52 < 1.370847 16 1 1 41.95 24.57 < 1.370732 5 2 9 85.20 47.08 < 1.370042 -3 0 12 270.62 164.78 < 1.369619 12 0 6 1191.93 686.65 < 1.369562 -3 2 11 121.88 69.68 < 1.369044 -11 3 8 510.29 287.40 < 1.368755 -14 3 2 280.37 161.14 < 1.368723 -8 4 6 18.42 10.62 < 1.368137 -13 2 9 1199.59 641.51 o 1.367979 -5 4 7 138.98 78.17 < 1.367608 -16 2 5 318.85 178.07 < 1.367442 -10 4 4 41.16 22.10 < 1.367175 -14 3 4 4.87 2.69 < 1.366661 -14 0 10 297.92 177.37 < 1.366648 -7 2 11 129.25 75.92 < 1.366354 4 3 8 37.76 22.04 < 1.366283 -1 4 7 247.07 151.34 < 1.365836 -8 0 12 7.42 4.85 < 1.364866 10 4 0 117.91 78.52 < 1.364286 1 3 9 99.70 69.48 < 1.364031 15 2 1 31.35 21.25 < 1.363290 5 4 5 65.48 46.80 < 1.363278 -9 3 9 20.80 14.95 < 1.362898 -17 1 6 245.11 176.94 < 1.362588 13 3 1 152.52 121.27 < 1.361979 -17 1 1 146.76 117.26 < 1.361552 9 2 7 1159.90 914.30 o 1.361360 8 3 6 550.81 425.86 < 1.360575 3 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10 275.77 231.80 < 1.343638 2 5 0 354.90 270.78 < 1.343413 1 5 1 191.39 151.52 < 1.343375 15 1 3 57.21 47.94 < 1.343354 13 2 4 154.81 136.87 < 1.343103 -10 4 5 54.29 45.13 < 1.343008 -2 5 1 285.15 241.78 < 1.342582 -3 1 12 114.21 107.28 < 1.342369 -1 2 11 9.78 9.22 < 1.342336 12 1 6 119.76 111.59 < 1.342314 -9 4 6 676.45 685.80 o 1.340895 -11 4 2 19.73 18.60 < 1.340879 -7 4 7 58.33 53.64 < 1.340552 12 2 5 392.95 362.72 o 1.340230 -12 1 11 0.49 0.54 o 1.339865 -14 1 10 229.08 238.32 o 1.339571 10 4 1 312.08 288.62 o 1.338907 -1 0 12 30.98 28.55 o 1.338886 -11 4 3 299.36 270.33 o 1.338744 2 3 9 1103.47 1016.17 o 1.338703 -12 2 10 22.98 20.15 o 1.338078 -8 1 12 674.45 585.52 o 1.337892 -13 3 7 275.79 239.36 o 1.337759 -10 3 9 69.58 61.07 o 1.337419 -9 2 11 155.37 133.36 o 1.337279 1 4 7 228.04 200.07 < 1.337220 14 2 3 24.91 20.93 < 1.335826 -4 3 10 3.12 2.63 < 1.335822 11 3 4 358.72 302.09 < 1.335780 -5 3 10 3.65 3.06 < 1.335455 -1 5 2 11.19 9.70 < 1.334936 2 5 1 6.74 5.64 < 1.334637 12 3 3 147.41 116.81 < 1.333557 -11 4 1 24.40 18.76 < 1.333441 -17 1 7 2.21 1.69 < 1.333410 -3 5 1 180.08 136.77 < 1.333342 0 5 2 135.60 102.15 < 1.333229 -2 5 2 186.42 138.85 < 1.332196 3 5 0 67.56 50.32 < 1.332194 4 4 6 0.27 0.19 < 1.332124 17 1 0 1964.69 1375.15 < 1.332052 -12 3 8 179.31 135.70 < 1.332001 -18 0 2 263.48 183.75 < 1.331918 -3 3 10 2.54 1.87 < 1.331739 14 3 0 24.71 17.94 < 1.331361 -10 0 12 313.80 226.13 < 1.330923 -6 3 10 38.88 25.94 < 1.330651 -2 1 12 57.10 42.65 < 1.329844 7 3 7 252.78 175.72 < 1.329526 5 3 8 25.85 18.14 < 1.329420 -15 2 8 329.50 239.24 < 1.328749 6 0 10 48.86 29.53 < 1.328327 6 4 5 0.31 0.22 < 1.328078 10 3 5 186.31 131.06 < 1.328025 16 2 0 0.93 0.62 < 1.327661 11 2 6 116.28 82.12 < 1.327401 -11 4 4 131.92 99.39 < 1.327170 1 5 2 574.94 433.99 < 1.327125 6 2 9 363.94 258.54 < 1.326528 -14 3 6 226.04 180.20 < 1.325692 8 2 8 58.97 50.22 < 1.325286 -3 5 2 1.44 1.24 < 1.325089 -14 2 9 25.26 20.72 < 1.324448 -9 1 12 88.81 72.26 < 1.323762 16 1 2 677.85 525.78 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1.90 o 1.310974 -1 3 10 525.19 542.61 o 1.310832 9 3 6 12.42 12.88 o 1.310802 3 3 9 31.26 32.04 o 1.310496 9 4 3 1189.49 1221.71 o 1.310401 0 5 3 34.35 34.02 o 1.310150 -4 4 8 88.12 88.10 o 1.309972 -3 4 8 23.59 23.80 o 1.309827 -15 3 4 0.15 0.14 o 1.309531 -11 3 9 82.12 78.76 o 1.309091 4 2 10 93.80 88.59 o 1.309021 -11 0 12 78.76 84.30 o 1.308528 -8 3 10 0.02 0.02 o 1.308414 -3 5 3 24.24 22.91 < 1.307948 -15 3 2 414.39 393.86 < 1.307625 8 1 9 28.28 25.21 < 1.307449 15 0 4 53.54 50.36 < 1.307316 -11 4 5 1341.41 1236.66 < 1.306874 -18 1 2 70.48 65.02 < 1.306816 -13 1 11 52.61 44.08 < 1.306691 -5 4 8 28.19 25.37 < 1.305922 10 4 2 43.30 38.97 < 1.305894 -10 1 12 0.17 0.18 < 1.305876 -2 4 8 224.76 198.37 < 1.305492 8 4 4 2.23 2.02 < 1.305470 10 2 7 419.48 398.22 o 1.305449 -16 1 9 258.19 249.65 < 1.305060 4 5 1 70.97 70.16 o 1.304981 -17 2 5 420.61 393.04 o 1.303697 6 1 10 184.28 167.11 o 1.303423 -13 2 10 208.06 187.13 o 1.303196 -17 2 2 0.47 0.41 < 1.303152 -5 5 1 197.16 172.17 < 1.302804 3 5 2 116.61 100.41 < 1.302556 1 5 3 354.82 308.27 < 1.302523 13 0 6 217.20 201.44 < 1.301963 5 4 6 25.16 22.13 < 1.301525 14 3 1 17.53 14.18 < 1.300398 1 2 11 294.60 223.65 < 1.300328 -4 5 3 329.97 281.04 < 1.298921 -5 5 2 297.14 248.08 < 1.298715 -9 4 7 63.00 57.54 < 1.298314 5 5 0 125.82 111.98 < 1.298095 -6 4 8 28.03 24.81 < 1.297793 -17 1 8 2.00 1.44 < 1.297212 -18 1 6 156.75 131.81 < 1.297199 -15 3 5 367.43 316.01 < 1.297192 -1 4 8 43.34 34.35 < 1.297089 -15 1 10 33.85 31.08 < 1.296331 17 1 1 468.63 366.50 < 1.295604 -12 4 2 275.10 211.23 < 1.295334 -12 4 3 2.08 1.61 < 1.295204 0 3 10 5.21 3.90 < 1.294597 -13 3 8 44.03 29.90 < 1.293977 3 4 7 308.30 228.61 < 1.293781 1 0 12 13.15 8.52 < 1.293590 -15 3 1 173.37 123.54 < 1.293495 0 1 12 135.23 86.59 < 1.293467 -11 2 11 17.80 11.98 < 1.293447 10 1 8 103.98 66.57 < 1.293431 -14 3 7 0.86 0.55 < 1.293366 16 2 1 84.42 60.84 < 1.293351 11 4 1 324.91 212.51 < 1.292237 -9 3 10 29.43 19.43 < 1.291604 7 4 5 1.00 0.67 < 1.291414 6 3 8 8.81 6.53 < 1.291333 2 5 3 63.71 50.52 < 1.290975 -18 1 1 170.32 123.92 < 1.287379 -12 4 1 114.12 86.74 < 1.286856 -17 2 6 390.01 258.08 < 1.286503 -12 4 4 8.71 6.30 < 1.286474 -5 5 3 167.70 129.85 < 1.286073 -2 5 4 2.21 1.70 < 1.285837 -7 4 8 1.50 1.13 < 1.285810 -17 2 1 81.46 61.11 < 1.285631 14 1 5 142.46 112.27 < 1.285469 8 3 7 163.82 134.28 < 1.285185 5 5 1 185.82 140.83 < 1.284869 0 4 8 107.35 91.19 < 1.284852 -1 5 4 2.34 1.83 < 1.284773 4 5 2 19.47 15.24 < 1.284768 -11 1 12 652.85 473.24 < 1.284702 15 1 4 348.43 304.45 < 1.283555 -12 0 12 222.19 181.46 < 1.283248 18 0 0 9.60 8.50 < 1.283185 7 2 9 20.57 18.77 < 1.282937 -3 5 4 68.18 63.56 < 1.282926 7 0 10 224.44 178.41 < 1.282812 -6 5 1 557.48 529.67 o 1.282331 4 1 11 11.38 10.92 < 1.281841 -15 2 9 49.52 52.80 o 1.280867 12 3 4 112.65 93.27 < 1.280181 -6 5 2 80.09 81.01 o 1.280165 4 3 9 1439.40 1149.32 < 1.280051 0 5 4 277.70 227.74 < 1.279765 -5 2 12 126.25 101.23 < 1.279545 -16 2 8 3.99 3.78 o 1.279063 -11 4 6 9.76 7.58 < 1.279031 -6 2 12 593.08 449.70 < 1.278767 14 2 4 9.37 6.93 < 1.278711 -12 3 9 4.47 3.34 < 1.278555 13 1 6 36.55 28.05 < 1.278487 13 2 5 12.10 8.97 < 1.278412 -15 3 6 322.96 217.15 < 1.276790 -4 2 12 1289.82 892.02 < 1.276409 17 0 2 40.56 27.53 < 1.276163 -4 5 4 55.03 36.60 < 1.276122 6 5 0 0.10 0.07 < 1.276115 13 3 3 253.31 168.41 < 1.276044 3 5 3 13.78 8.77 < 1.275818 9 2 8 17.71 11.70 < 1.275705 11 3 5 1.89 1.24 < 1.275516 -16 0 10 204.48 142.68 < 1.275410 -19 0 4 177.70 121.74 < 1.275374 1 3 10 10.24 6.85 < 1.275047 2 2 11 13.41 9.51 < 1.274884 -7 2 12 13.14 9.45 < 1.274095 -18 1 7 46.00 34.61 < 1.273656 5 2 10 142.52 89.49 < 1.273063 16 1 3 0.78 0.50 < 1.272862 -10 4 7 102.19 65.52 < 1.272802 -14 1 11 6.60 3.80 < 1.271989 -10 3 10 115.51 58.75 < 1.271555 15 3 0 402.23 213.76 < 1.271513 1 5 4 12.85 6.86 < 1.270950 1 1 12 0.00 0.00 < 1.270557 -8 4 8 286.00 157.35 < 1.270293 15 2 3 87.10 47.92 < 1.270277 12 4 0 5.73 3.15 < 1.270266 -6 5 3 488.51 218.71 < 1.269744 -12 4 5 222.84 96.39 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65.56 57.80 < 1.257439 -16 3 3 1623.45 1470.27 < 1.256768 -17 1 9 8.90 7.97 < 1.255814 -13 0 12 0.57 0.58 o 1.255651 -14 3 8 220.91 214.60 < 1.255310 -16 3 4 10.73 10.39 < 1.255290 17 1 2 82.07 74.40 < 1.254032 -6 1 13 31.83 28.79 < 1.253950 8 4 5 8.63 7.74 < 1.253917 -9 2 12 238.30 221.99 < 1.253674 16 2 2 3.43 3.14 < 1.253616 -5 3 11 10.60 9.65 < 1.253521 -16 1 10 201.50 180.70 < 1.253318 -19 1 4 247.66 221.39 < 1.253283 -5 1 13 13.36 12.64 < 1.253052 2 3 10 49.07 43.32 < 1.252656 7 3 8 55.20 48.74 < 1.252642 -2 5 5 213.31 193.24 < 1.252448 11 2 7 6.57 6.13 < 1.252209 -4 3 11 216.83 201.41 < 1.252195 -13 4 3 133.45 122.19 < 1.251958 -6 5 4 0.72 0.62 < 1.251658 -9 4 8 26.70 23.54 < 1.251633 7 5 0 367.11 314.43 < 1.251525 -3 5 5 35.92 32.20 < 1.251377 -6 3 11 58.39 53.67 < 1.251163 -7 1 13 16.43 14.62 < 1.251163 -18 2 4 19.71 18.45 < 1.250477 -13 4 2 189.67 180.19 < 1.250453 -16 3 2 329.35 316.76 < 1.250361 -7 5 3 26.79 24.85 < 1.250342 2 4 8 46.15 47.13 < 1.250246 -19 1 3 0.01 0.01 < 1.249875 -1 5 5 318.40 319.66 < 1.249845 -15 3 7 677.35 629.26 < 1.249447 -19 1 5 209.68 208.29 < 1.248857 -11 3 10 79.21 81.89 < 1.248745 -18 2 3 0.40 0.40 < 1.248701 -4 1 13 68.89 69.67 < 1.248492 5 3 9 641.92 675.40 o 1.247974 3 2 11 35.74 39.24 o 1.247225 -3 3 11 344.22 376.75 o 1.247220 -4 5 5 9.63 10.36 o 1.246662 12 4 1 289.69 312.75 o 1.246484 -13 3 9 16.68 17.98 o 1.246414 5 1 11 56.42 58.11 < 1.246413 -4 4 9 243.34 260.76 o 1.246017 -16 3 5 599.78 631.01 o 1.246008 -12 4 6 3.11 3.27 o 1.245675 -13 4 4 59.86 62.78 o 1.245667 2 1 12 80.31 81.10 o 1.245188 -7 3 11 140.29 148.11 o 1.245185 -11 4 7 6.15 6.42 o 1.245103 -1 2 12 54.59 56.39 o 1.244857 -8 1 13 44.53 46.00 o 1.244764 -18 2 5 1121.07 1132.67 o 1.244480 -3 4 9 10.67 11.36 o 1.244294 -5 4 9 511.59 545.30 o 1.244122 0 5 5 231.59 261.79 o 1.243637 -18 1 8 6.98 7.51 o 1.243586 3 5 4 368.64 397.71 o 1.242912 15 3 1 299.45 323.07 o 1.242864 9 3 7 404.38 420.09 < 1.241402 -13 4 1 350.94 363.18 < 1.241235 16 0 4 9.03 9.27 < 1.240495 6 5 2 385.59 391.48 < 1.240401 -3 1 13 12.55 12.68 < 1.240388 11 1 8 49.58 47.42 < 1.240008 14 0 6 36.56 34.27 < 1.239888 8 2 9 140.67 138.14 < 1.239791 5 4 7 79.80 75.09 < 1.239778 -18 2 2 138.97 125.31 < 1.239251 -13 2 11 22.65 21.39 < 1.239144 -2 4 9 0.28 0.23 < 1.238998 -19 1 2 53.18 46.88 < 1.238822 -2 3 11 208.04 174.41 < 1.238726 -6 4 9 1.66 1.39 < 1.238658 -10 2 12 436.19 406.94 o 1.238449 -5 5 5 405.39 354.18 < 1.238424 3 0 12 81.05 80.05 o 1.238120 8 0 10 50.89 50.26 o 1.238103 -16 2 9 339.95 315.58 o 1.237753 -19 1 6 5.78 4.75 < 1.236840 7 5 1 51.07 40.72 < 1.236516 -16 3 1 17.29 13.85 < 1.236422 6 2 10 418.33 324.24 < 1.236356 -15 1 11 218.40 182.86 < 1.236356 5 5 3 124.32 95.87 < 1.236276 -8 3 11 698.81 519.68 < 1.235739 7 4 6 8.31 6.19 < 1.235423 -9 1 13 76.48 53.22 < 1.234916 -7 5 4 319.78 214.74 < 1.234616 -8 5 2 82.83 56.28 < 1.234612 -13 1 12 12.67 9.50 < 1.234553 1 5 5 140.61 105.93 < 1.233984 -8 5 1 182.46 144.34 < 1.233434 -13 4 5 379.48 307.08 < 1.231924 -17 2 8 59.72 68.75 < 1.231051 -18 2 6 20.10 18.32 < 1.231041 -17 0 10 110.68 158.70 < 1.230871 -15 2 10 163.79 219.15 < 1.230298 -10 4 8 12.80 11.95 < 1.230267 -1 4 9 5.87 5.14 < 1.230263 -7 4 9 445.04 387.40 < 1.229764 17 2 1 119.74 106.38 < 1.229677 -16 3 6 69.34 62.61 < 1.229430 -2 1 13 249.27 221.10 < 1.228946 3 4 8 1.56 1.33 < 1.228710 -8 5 3 959.86 799.43 < 1.228314 18 1 1 0.36 0.31 < 1.228126 3 3 10 3.51 2.98 < 1.227920 0 2 12 114.45 98.29 < 1.227850 10 2 8 765.32 657.25 < 1.227819 13 3 4 27.92 23.20 < 1.227511 -1 3 11 43.31 32.21 < 1.226926 -6 5 5 96.48 73.25 < 1.226871 -14 0 12 1106.91 888.96 < 1.226290 12 3 5 83.76 56.92 < 1.225317 8 5 0 2.41 1.69 < 1.224845 13 4 0 59.78 42.28 < 1.224803 4 5 4 9.86 7.12 < 1.224377 11 4 3 372.19 262.79 < 1.224186 10 4 4 15.03 9.83 < 1.223981 15 1 5 43.36 26.62 < 1.223696 -12 3 10 2.47 1.52 < 1.223672 -9 3 11 119.18 70.63 < 1.223060 -18 2 1 521.97 281.32 < 1.222638 14 3 3 283.05 152.96 < 1.221949 -10 1 13 11.45 9.46 < 1.221864 2 5 5 131.82 83.57 < 1.221124 14 2 5 102.87 60.64 < 1.221002 -19 1 1 53.14 32.97 < 1.220716 -11 2 12 80.75 39.82 < 1.220345 16 1 4 306.67 169.05 < 1.220139 14 1 6 317.72 171.14 < 1.219562 15 2 4 0.02 0.01 < 1.219361 0 4 9 61.46 37.44 < 1.218306 4 2 11 212.48 128.98 < 1.217891 3 1 12 297.54 178.19 < 1.217880 -19 1 7 2.88 1.63 < 1.217875 8 1 10 1.90 1.14 < 1.217863 -8 4 9 185.19 111.04 < 1.217660 12 4 2 1.24 0.85 < 1.216722 -15 3 8 98.50 53.04 < 1.216524 9 4 5 173.63 123.75 < 1.216121 -12 4 7 47.74 32.17 < 1.215755 16 3 0 171.66 120.67 < 1.215690 19 0 0 195.60 134.39 < 1.215649 11 3 6 72.75 52.71 < 1.215490 13 2 6 0.52 0.38 < 1.215014 -8 5 4 483.11 345.24 < 1.214877 6 3 9 997.27 694.74 < 1.214820 -3 5 6 96.27 63.95 < 1.214814 7 5 2 103.03 69.36 < 1.214802 -1 1 13 14.16 8.99 < 1.214443 -2 5 6 17.21 11.54 < 1.214307 8 3 8 37.85 27.36 < 1.213865 -14 3 9 4.92 3.62 < 1.213221 6 5 3 2.10 1.63 < 1.212789 -7 5 5 49.97 38.62 < 1.212281 0 3 11 18.52 12.56 < 1.212105 -4 5 6 23.33 15.36 < 1.211970 -19 0 8 71.86 54.16 < 1.211912 -20 0 4 733.80 548.48 < 1.211551 -13 4 6 3.72 2.74 < 1.211453 -17 1 10 64.12 43.99 < 1.210978 -18 2 7 237.13 163.90 < 1.210865 10 1 9 33.45 24.93 < 1.210645 -1 5 6 394.23 275.32 < 1.210463 6 1 11 140.12 119.28 < 1.210431 16 2 3 41.04 29.06 < 1.210182 6 4 7 34.80 26.25 < 1.210180 18 0 2 760.16 549.47 < 1.210059 -14 4 3 91.74 68.80 < 1.209445 -14 2 11 38.45 25.65 < 1.209432 8 5 1 0.00 0.00 < 1.209298 17 1 3 25.57 19.15 < 1.209090 15 3 2 12.54 10.58 < 1.208941 -9 5 2 5.69 4.20 < 1.208591 -18 1 9 25.80 16.68 < 1.208432 12 0 8 2085.02 1348.06 < 1.208373 1 2 12 431.60 346.32 < 1.208201 13 1 7 2.54 1.89 < 1.207967 4 0 12 0.67 0.45 < 1.207947 -10 3 11 113.76 106.80 < 1.207451 -11 4 8 232.12 287.48 o 1.206652 -14 4 2 2.30 2.77 o 1.206630 -14 1 12 232.04 282.60 o 1.206615 -16 3 7 27.88 33.68 o 1.206413 -9 5 1 74.96 89.11 < 1.206031 -11 1 13 0.49 0.58 o 1.205917 -5 5 6 17.16 19.97 < 1.205846 3 5 5 1022.05 1095.10 < 1.205362 -14 4 4 131.96 154.20 o 1.205217 4 4 8 6.94 7.26 < 1.204957 -9 5 3 2.19 2.16 < 1.204124 -17 3 4 7.13 7.04 < 1.203990 -17 3 3 370.65 366.53 < 1.203847 1 4 9 24.34 22.22 < 1.203411 0 5 6 207.84 188.48 < 1.203376 5 5 4 47.26 42.86 < 1.203368 -9 4 9 0.62 0.50 < 1.202634 13 4 1 7.12 6.00 < 1.202002 12 2 7 0.14 0.12 < 1.201727 4 3 10 1134.65 898.51 < 1.201330 8 4 6 17.17 14.15 < 1.201036 -16 1 11 74.93 63.30 < 1.200303 -12 2 12 133.82 106.41 < 1.199762 18 2 0 117.26 93.56 < 1.199710 -20 0 6 139.05 117.22 < 1.199525 7 2 10 198.41 167.25 < 1.199405 10 3 7 515.41 431.33 < 1.198568 loop_ _publcif_info_datablock.id _publcif_info_datablock.publ_exptl _publcif_info_datablock.publ_geom _publcif_info_datablock.structure '{26b85eb2-729f-4157-be97-e1502d3a842c}' ? ? ? '{a267325d-6c55-4234-af2a-2258b906115c}' y y y loop_ _publcif_info_exptl_table_extra_item ? loop_ _publcif_info_exptl_table_header_item ? _publcif_info_exptl_table_max_cols 4 _publcif_info_exptl_table_use_headnotes n loop_ _publcif_info_tables.block_id _publcif_info_tables.reference_item "{26b85eb2-729f-4157-be97-e1502d3a842c}" "_publcif_info_datablock.publ_exptl"