data_P21n_a _audit_creation_method SHELXL-2014 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C46 H70 N2 Si' _chemical_formula_sum 'C46 H70 N2 Si' _chemical_formula_weight 679.13 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0015 0.0009 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0030 0.0019 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Si' 'Si' 0.0522 0.0431 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/n' _space_group_name_Hall '-P 2yn' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 9.533(2) _cell_length_b 18.139(2) _cell_length_c 22.863(3) _cell_angle_alpha 90 _cell_angle_beta 93.00(2) _cell_angle_gamma 90 _cell_volume 3948.0(11) _cell_formula_units_Z 4 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 4898 _cell_measurement_theta_min 2.2635 _cell_measurement_theta_max 17.0455 _exptl_crystal_description block _exptl_crystal_colour ? _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.143 _exptl_crystal_F_000 1496 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.100 _exptl_crystal_size_mid 0.090 _exptl_crystal_size_min 0.070 _exptl_absorpt_coefficient_mu 0.057 _shelx_estimated_absorpt_T_min 0.994 _shelx_estimated_absorpt_T_max 0.996 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.4004 _exptl_absorpt_correction_T_max 0.4249 _exptl_absorpt_process_details 'SADABS-2014/4' _exptl_special_details ; ? ; _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.56086 _diffrn_radiation_type AgK\a _diffrn_source 'INCOATEC Microsource' _diffrn_measurement_device_type 'Bruker Smart APEX II Quazar' _diffrn_measurement_method 'omega scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 61908 _diffrn_reflns_av_unetI/netI 0.0569 _diffrn_reflns_av_R_equivalents 0.0870 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_k_min -21 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_l_min -27 _diffrn_reflns_limit_l_max 27 _diffrn_reflns_theta_min 1.663 _diffrn_reflns_theta_max 19.809 _diffrn_reflns_theta_full 19.665 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measured_fraction_theta_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_point_group_measured_fraction_full 0.999 _reflns_number_total 7289 _reflns_number_gt 5196 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'APEX2 v2012.2' _computing_cell_refinement 'SAINT V8.30C' _computing_data_reduction 'SAINT V8.30C' _computing_structure_solution 'SHELXS-2012 (Sheldrick, 2012)' _computing_structure_refinement 'SHELXL-2014 (Sheldrick, 2014)' _computing_molecular_graphics 'Mercury CSD 3.3 (Build RC5)' _computing_publication_material 'Mercury CSD 3.3 (Build RC5)' _refine_special_details ; ? ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0765P)^2^+2.0326P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 7289 _refine_ls_number_parameters 457 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0831 _refine_ls_R_factor_gt 0.0540 _refine_ls_wR_factor_ref 0.1562 _refine_ls_wR_factor_gt 0.1400 _refine_ls_goodness_of_fit_ref 1.040 _refine_ls_restrained_S_all 1.040 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Si1 Si 0.68889(7) 0.43734(3) 0.26762(3) 0.01865(17) Uani 1 1 d . . . . . N1 N 0.68194(19) 0.35965(10) 0.37512(8) 0.0164(4) Uani 1 1 d . . . . . C1 C 0.6667(3) 0.43444(12) 0.35196(9) 0.0183(5) Uani 1 1 d . . . . . H1 H 0.568(3) 0.4505(13) 0.3579(10) 0.022 Uiso 1 1 d . U . . . N2 N 0.5084(2) 0.48194(10) 0.16731(8) 0.0180(4) Uani 1 1 d . . . . . C2 C 0.7623(3) 0.48319(13) 0.39501(10) 0.0222(5) Uani 1 1 d . . . . . C3 C 0.8613(3) 0.42605(13) 0.42565(10) 0.0220(5) Uani 1 1 d . . . . . H3A H 0.9479 0.4206 0.4039 0.026 Uiso 1 1 calc R U . . . H3B H 0.8880 0.4423 0.4660 0.026 Uiso 1 1 calc R U . . . C4 C 0.7827(2) 0.35260(13) 0.42688(9) 0.0193(5) Uani 1 1 d . . . . . C5 C 0.7124(3) 0.34355(15) 0.48607(10) 0.0307(6) Uani 1 1 d . . . . . H5A H 0.6393 0.3811 0.4893 0.046 Uiso 1 1 calc R U . . . H5B H 0.7833 0.3494 0.5184 0.046 Uiso 1 1 calc R U . . . H5C H 0.6702 0.2944 0.4880 0.046 Uiso 1 1 calc R U . . . C6 C 0.8797(3) 0.28578(14) 0.42194(11) 0.0287(6) Uani 1 1 d . . . . . H6A H 0.8239 0.2404 0.4223 0.043 Uiso 1 1 calc R U . . . H6B H 0.9492 0.2855 0.4551 0.043 Uiso 1 1 calc R U . . . H6C H 0.9281 0.2887 0.3852 0.043 Uiso 1 1 calc R U . . . C7 C 0.8463(3) 0.54293(14) 0.36460(11) 0.0290(6) Uani 1 1 d . . . . . H7A H 0.7812 0.5734 0.3396 0.035 Uiso 1 1 calc R U . . . H7B H 0.9136 0.5191 0.3390 0.035 Uiso 1 1 calc R U . . . C8 C 0.9273(3) 0.59298(15) 0.40896(12) 0.0386(7) Uani 1 1 d . . . . . H8A H 0.9998 0.5634 0.4309 0.046 Uiso 1 1 calc R U . . . H8B H 0.9759 0.6320 0.3875 0.046 Uiso 1 1 calc R U . . . C9 C 0.8328(4) 0.62842(16) 0.45176(14) 0.0465(8) Uani 1 1 d . . . . . H9A H 0.7677 0.6628 0.4305 0.056 Uiso 1 1 calc R U . . . H9B H 0.8906 0.6574 0.4808 0.056 Uiso 1 1 calc R U . . . C10 C 0.7486(3) 0.57146(15) 0.48353(12) 0.0385(7) Uani 1 1 d . . . . . H10A H 0.6817 0.5966 0.5086 0.046 Uiso 1 1 calc R U . . . H10B H 0.8126 0.5410 0.5090 0.046 Uiso 1 1 calc R U . . . C11 C 0.6681(3) 0.52214(14) 0.43915(11) 0.0302(6) Uani 1 1 d . . . . . H11A H 0.5972 0.5524 0.4169 0.036 Uiso 1 1 calc R U . . . H11B H 0.6171 0.4841 0.4607 0.036 Uiso 1 1 calc R U . . . C12 C 0.4389(3) 0.21525(16) 0.45978(12) 0.0383(7) Uani 1 1 d . . . . . H12A H 0.3911 0.1704 0.4454 0.058 Uiso 1 1 calc R U . . . H12B H 0.3884 0.2359 0.4922 0.058 Uiso 1 1 calc R U . . . H12C H 0.5353 0.2032 0.4735 0.058 Uiso 1 1 calc R U . . . C13 C 0.2927(3) 0.28593(17) 0.38417(13) 0.0383(7) Uani 1 1 d . . . . . H13A H 0.2952 0.3238 0.3537 0.057 Uiso 1 1 calc R U . . . H13B H 0.2331 0.3027 0.4152 0.057 Uiso 1 1 calc R U . . . H13C H 0.2542 0.2402 0.3671 0.057 Uiso 1 1 calc R U . . . C14 C 0.4417(3) 0.27194(14) 0.40998(11) 0.0278(6) Uani 1 1 d . . . . . H14 H 0.4783 0.3194 0.4271 0.033 Uiso 1 1 calc R U . . . C15 C 0.5361(2) 0.24969(13) 0.36124(10) 0.0229(5) Uani 1 1 d . . . . . C16 C 0.5094(3) 0.18286(13) 0.33225(11) 0.0284(6) Uani 1 1 d . . . . . H16 H 0.4425 0.1496 0.3467 0.034 Uiso 1 1 calc R U . . . C17 C 0.5791(3) 0.16473(14) 0.28279(11) 0.0309(6) Uani 1 1 d . . . . . H17 H 0.5671 0.1174 0.2654 0.037 Uiso 1 1 calc R U . . . C18 C 0.6670(3) 0.21620(13) 0.25874(10) 0.0255(6) Uani 1 1 d . . . . . H18 H 0.7078 0.2050 0.2228 0.031 Uiso 1 1 calc R U . . . C19 C 0.9310(3) 0.35072(14) 0.27974(11) 0.0286(6) Uani 1 1 d . . . . . H19A H 0.9785 0.3028 0.2792 0.043 Uiso 1 1 calc R U . . . H19B H 0.9295 0.3685 0.3202 0.043 Uiso 1 1 calc R U . . . H19C H 0.9816 0.3861 0.2563 0.043 Uiso 1 1 calc R U . . . C20 C 0.7936(3) 0.32152(14) 0.18942(10) 0.0273(6) Uani 1 1 d . . . . . H20A H 0.7001 0.3109 0.1715 0.041 Uiso 1 1 calc R U . . . H20B H 0.8532 0.2777 0.1869 0.041 Uiso 1 1 calc R U . . . H20C H 0.8357 0.3626 0.1687 0.041 Uiso 1 1 calc R U . . . C21 C 0.6394(2) 0.29752(12) 0.34062(9) 0.0175(5) Uani 1 1 d . . . . . C22 C 0.6977(2) 0.28423(12) 0.28576(10) 0.0194(5) Uani 1 1 d . . . . . C23 C 0.7806(3) 0.34252(13) 0.25415(10) 0.0213(5) Uani 1 1 d . . . . . C24 C 0.5344(2) 0.47387(12) 0.22704(9) 0.0187(5) Uani 1 1 d . . . . . C25 C 0.4223(2) 0.52158(13) 0.25660(10) 0.0219(5) Uani 1 1 d . . . . . C26 C 0.3325(3) 0.55396(14) 0.20420(10) 0.0258(6) Uani 1 1 d . . . . . H26A H 0.2444 0.5256 0.1977 0.031 Uiso 1 1 calc R U . . . H26B H 0.3084 0.6061 0.2118 0.031 Uiso 1 1 calc R U . . . C27 C 0.4218(3) 0.54828(13) 0.15104(10) 0.0230(5) Uani 1 1 d . . . . . C28 C 0.5118(3) 0.61779(13) 0.14489(12) 0.0313(6) Uani 1 1 d . . . . . H28A H 0.5586 0.6160 0.1078 0.047 Uiso 1 1 calc R U . . . H28B H 0.5826 0.6202 0.1775 0.047 Uiso 1 1 calc R U . . . H28C H 0.4516 0.6615 0.1455 0.047 Uiso 1 1 calc R U . . . C29 C 0.3338(3) 0.53635(15) 0.09429(11) 0.0293(6) Uani 1 1 d . . . . . H29A H 0.3960 0.5283 0.0621 0.044 Uiso 1 1 calc R U . . . H29B H 0.2755 0.5800 0.0859 0.044 Uiso 1 1 calc R U . . . H29C H 0.2734 0.4932 0.0984 0.044 Uiso 1 1 calc R U . . . C30 C 0.3273(3) 0.47099(15) 0.29222(11) 0.0288(6) Uani 1 1 d . . . . . H30A H 0.2788 0.4353 0.2653 0.035 Uiso 1 1 calc R U . . . H30B H 0.3868 0.4426 0.3210 0.035 Uiso 1 1 calc R U . . . C31 C 0.2178(3) 0.5142(2) 0.32454(13) 0.0469(8) Uani 1 1 d . . . . . H31A H 0.1629 0.4800 0.3481 0.056 Uiso 1 1 calc R U . . . H31B H 0.1522 0.5389 0.2958 0.056 Uiso 1 1 calc R U . . . C32 C 0.2893(4) 0.5720(2) 0.36471(14) 0.0578(10) Uani 1 1 d . . . . . H32A H 0.2170 0.6002 0.3848 0.069 Uiso 1 1 calc R U . . . H32B H 0.3503 0.5471 0.3950 0.069 Uiso 1 1 calc R U . . . C33 C 0.3768(3) 0.62454(18) 0.33008(13) 0.0482(9) Uani 1 1 d . . . . . H33A H 0.4254 0.6598 0.3573 0.058 Uiso 1 1 calc R U . . . H33B H 0.3142 0.6531 0.3026 0.058 Uiso 1 1 calc R U . . . C34 C 0.4853(3) 0.58379(14) 0.29575(11) 0.0301(6) Uani 1 1 d . . . . . H34A H 0.5571 0.5624 0.3237 0.036 Uiso 1 1 calc R U . . . H34B H 0.5330 0.6196 0.2708 0.036 Uiso 1 1 calc R U . . . C35 C 0.3619(3) 0.29633(14) 0.19430(11) 0.0288(6) Uani 1 1 d . . . . . H35A H 0.3925 0.2499 0.1771 0.043 Uiso 1 1 calc R U . . . H35B H 0.2759 0.2879 0.2150 0.043 Uiso 1 1 calc R U . . . H35C H 0.4358 0.3148 0.2220 0.043 Uiso 1 1 calc R U . . . C36 C 0.2086(3) 0.32895(15) 0.10542(11) 0.0304(6) Uani 1 1 d . . . . . H36A H 0.1939 0.3647 0.0736 0.046 Uiso 1 1 calc R U . . . H36B H 0.1241 0.3262 0.1279 0.046 Uiso 1 1 calc R U . . . H36C H 0.2282 0.2803 0.0890 0.046 Uiso 1 1 calc R U . . . C37 C 0.3332(3) 0.35329(13) 0.14568(10) 0.0236(5) Uani 1 1 d . . . . . H37 H 0.3064 0.4005 0.1647 0.028 Uiso 1 1 calc R U . . . C38 C 0.4647(2) 0.36802(13) 0.11272(9) 0.0204(5) Uani 1 1 d . . . . . C39 C 0.5028(3) 0.31935(13) 0.06935(10) 0.0266(6) Uani 1 1 d . . . . . H39 H 0.4462 0.2772 0.0610 0.032 Uiso 1 1 calc R U . . . C40 C 0.6213(3) 0.33098(14) 0.03810(10) 0.0276(6) Uani 1 1 d . . . . . H40 H 0.6449 0.2972 0.0084 0.033 Uiso 1 1 calc R U . . . C41 C 0.7053(3) 0.39195(14) 0.05017(10) 0.0261(6) Uani 1 1 d . . . . . H41 H 0.7870 0.3992 0.0288 0.031 Uiso 1 1 calc R U . . . C42 C 0.9216(3) 0.48945(16) 0.11889(13) 0.0374(7) Uani 1 1 d . . . . . H42A H 0.9554 0.4551 0.0897 0.056 Uiso 1 1 calc R U . . . H42B H 0.9282 0.4662 0.1576 0.056 Uiso 1 1 calc R U . . . H42C H 0.9791 0.5342 0.1195 0.056 Uiso 1 1 calc R U . . . C43 C 0.7625(3) 0.55838(15) 0.04805(11) 0.0366(7) Uani 1 1 d . . . . . H43A H 0.8158 0.5350 0.0176 0.055 Uiso 1 1 calc R U . . . H43B H 0.8033 0.6067 0.0578 0.055 Uiso 1 1 calc R U . . . H43C H 0.6645 0.5646 0.0337 0.055 Uiso 1 1 calc R U . . . C44 C 0.5518(2) 0.43025(12) 0.12414(9) 0.0183(5) Uani 1 1 d . . . . . C45 C 0.6728(3) 0.44276(13) 0.09296(10) 0.0216(5) Uani 1 1 d . . . . . C46 C 0.7683(3) 0.50948(13) 0.10295(11) 0.0264(6) Uani 1 1 d . . . . . H46 H 0.7321 0.5389 0.1360 0.032 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Si1 0.0197(3) 0.0169(3) 0.0191(3) 0.0002(3) -0.0016(3) 0.0021(3) N1 0.0194(10) 0.0126(9) 0.0166(9) -0.0009(7) -0.0044(8) -0.0010(8) C1 0.0213(12) 0.0132(11) 0.0198(11) -0.0001(9) -0.0063(10) 0.0004(10) N2 0.0217(10) 0.0140(10) 0.0182(9) 0.0005(8) -0.0012(8) 0.0031(8) C2 0.0271(13) 0.0167(12) 0.0218(11) -0.0007(10) -0.0082(10) -0.0049(10) C3 0.0233(13) 0.0224(13) 0.0193(11) 0.0008(10) -0.0075(10) -0.0041(10) C4 0.0233(12) 0.0177(12) 0.0163(11) 0.0008(9) -0.0059(10) -0.0008(10) C5 0.0397(16) 0.0329(15) 0.0191(12) 0.0048(11) -0.0037(11) -0.0072(13) C6 0.0335(15) 0.0228(13) 0.0284(13) 0.0015(11) -0.0113(11) 0.0033(12) C7 0.0344(15) 0.0227(13) 0.0290(13) 0.0041(11) -0.0090(12) -0.0074(12) C8 0.0439(17) 0.0271(15) 0.0435(16) 0.0059(13) -0.0107(14) -0.0131(13) C9 0.058(2) 0.0285(16) 0.0510(18) -0.0127(14) -0.0172(16) -0.0088(15) C10 0.0484(18) 0.0326(16) 0.0328(14) -0.0137(12) -0.0123(13) 0.0030(14) C11 0.0360(15) 0.0253(14) 0.0279(13) -0.0065(11) -0.0103(12) 0.0021(12) C12 0.0436(17) 0.0385(17) 0.0340(14) 0.0011(13) 0.0122(13) -0.0123(14) C13 0.0257(14) 0.0441(17) 0.0455(16) -0.0065(14) 0.0052(13) -0.0071(13) C14 0.0259(14) 0.0289(14) 0.0291(13) -0.0035(11) 0.0062(11) -0.0078(11) C15 0.0218(13) 0.0209(13) 0.0254(12) -0.0030(10) -0.0039(10) -0.0032(10) C16 0.0314(14) 0.0200(13) 0.0332(13) 0.0005(11) -0.0024(12) -0.0067(11) C17 0.0436(17) 0.0162(13) 0.0316(14) -0.0057(11) -0.0092(13) 0.0007(12) C18 0.0367(15) 0.0178(13) 0.0213(12) -0.0050(10) -0.0054(11) 0.0094(11) C19 0.0284(14) 0.0280(14) 0.0299(13) 0.0080(11) 0.0067(11) 0.0072(12) C20 0.0329(15) 0.0265(14) 0.0229(12) 0.0009(11) 0.0054(11) 0.0097(12) C21 0.0178(12) 0.0147(11) 0.0193(11) -0.0034(9) -0.0057(9) 0.0027(9) C22 0.0217(12) 0.0151(12) 0.0208(11) 0.0007(9) -0.0053(10) 0.0074(10) C23 0.0256(13) 0.0197(12) 0.0189(11) -0.0004(9) 0.0040(10) 0.0062(10) C24 0.0189(12) 0.0182(12) 0.0188(11) 0.0000(9) 0.0001(9) -0.0006(10) C25 0.0215(12) 0.0229(13) 0.0211(11) -0.0039(10) -0.0017(10) 0.0073(10) C26 0.0238(13) 0.0246(13) 0.0283(13) -0.0012(11) -0.0041(11) 0.0074(11) C27 0.0249(13) 0.0172(12) 0.0265(12) 0.0008(10) -0.0026(10) 0.0055(10) C28 0.0340(15) 0.0176(13) 0.0421(15) 0.0045(11) 0.0005(13) 0.0061(11) C29 0.0321(15) 0.0290(14) 0.0262(12) 0.0048(11) -0.0039(11) 0.0071(12) C30 0.0209(13) 0.0420(16) 0.0236(12) 0.0005(11) 0.0013(10) 0.0040(12) C31 0.0320(16) 0.075(2) 0.0339(15) -0.0040(16) 0.0085(13) 0.0147(16) C32 0.0454(19) 0.087(3) 0.0408(17) -0.0277(18) 0.0031(15) 0.0259(19) C33 0.052(2) 0.0480(19) 0.0439(17) -0.0219(15) -0.0069(16) 0.0253(16) C34 0.0343(15) 0.0242(14) 0.0310(13) -0.0078(11) -0.0052(12) 0.0090(12) C35 0.0294(14) 0.0262(14) 0.0306(13) 0.0038(11) 0.0001(11) -0.0049(12) C36 0.0282(14) 0.0318(15) 0.0307(13) -0.0005(12) -0.0032(12) -0.0034(12) C37 0.0263(13) 0.0197(12) 0.0246(12) -0.0002(10) 0.0000(11) -0.0013(11) C38 0.0219(12) 0.0200(12) 0.0191(11) 0.0031(9) -0.0005(10) 0.0005(10) C39 0.0333(15) 0.0186(13) 0.0277(13) -0.0035(10) -0.0004(11) -0.0010(11) C40 0.0339(15) 0.0265(14) 0.0228(12) -0.0073(11) 0.0052(11) 0.0001(12) C41 0.0306(14) 0.0278(14) 0.0206(12) 0.0034(10) 0.0087(11) 0.0020(12) C42 0.0276(15) 0.0324(16) 0.0523(17) -0.0038(13) 0.0042(13) -0.0052(13) C43 0.0505(18) 0.0258(14) 0.0341(14) 0.0036(12) 0.0073(13) -0.0081(13) C44 0.0234(12) 0.0163(12) 0.0152(10) 0.0012(9) -0.0015(9) 0.0021(10) C45 0.0236(13) 0.0200(12) 0.0207(11) 0.0036(10) -0.0023(10) 0.0005(10) C46 0.0304(14) 0.0209(13) 0.0285(13) 0.0008(10) 0.0051(11) -0.0028(11) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Si1 C24 1.824(2) . ? Si1 C1 1.952(2) . ? Si1 C23 1.961(2) . ? N1 C21 1.422(3) . ? N1 C1 1.461(3) . ? N1 C4 1.490(3) . ? C1 C2 1.577(3) . ? C1 H1 1.00(3) . ? N2 C24 1.383(3) . ? N2 C44 1.438(3) . ? N2 C27 1.495(3) . ? C2 C7 1.535(3) . ? C2 C3 1.544(3) . ? C2 C11 1.556(3) . ? C3 C4 1.529(3) . ? C3 H3A 0.9900 . ? C3 H3B 0.9900 . ? C4 C6 1.532(3) . ? C4 C5 1.550(3) . ? C5 H5A 0.9800 . ? C5 H5B 0.9800 . ? C5 H5C 0.9800 . ? C6 H6A 0.9800 . ? C6 H6B 0.9800 . ? C6 H6C 0.9800 . ? C7 C8 1.539(4) . ? C7 H7A 0.9900 . ? C7 H7B 0.9900 . ? C8 C9 1.508(4) . ? C8 H8A 0.9900 . ? C8 H8B 0.9900 . ? C9 C10 1.517(4) . ? C9 H9A 0.9900 . ? C9 H9B 0.9900 . ? C10 C11 1.529(3) . ? C10 H10A 0.9900 . ? C10 H10B 0.9900 . ? C11 H11A 0.9900 . ? C11 H11B 0.9900 . ? C12 C14 1.536(4) . ? C12 H12A 0.9800 . ? C12 H12B 0.9800 . ? C12 H12C 0.9800 . ? C13 C14 1.531(4) . ? C13 H13A 0.9800 . ? C13 H13B 0.9800 . ? C13 H13C 0.9800 . ? C14 C15 1.523(3) . ? C14 H14 1.0000 . ? C15 C16 1.399(3) . ? C15 C21 1.411(3) . ? C16 C17 1.381(4) . ? C16 H16 0.9500 . ? C17 C18 1.387(4) . ? C17 H17 0.9500 . ? C18 C22 1.404(3) . ? C18 H18 0.9500 . ? C19 C23 1.527(3) . ? C19 H19A 0.9800 . ? C19 H19B 0.9800 . ? C19 H19C 0.9800 . ? C20 C23 1.539(3) . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? C21 C22 1.419(3) . ? C22 C23 1.525(3) . ? C24 C25 1.557(3) . ? C25 C34 1.542(3) . ? C25 C30 1.550(3) . ? C25 C26 1.551(3) . ? C26 C27 1.523(3) . ? C26 H26A 0.9900 . ? C26 H26B 0.9900 . ? C27 C29 1.523(3) . ? C27 C28 1.536(3) . ? C28 H28A 0.9800 . ? C28 H28B 0.9800 . ? C28 H28C 0.9800 . ? C29 H29A 0.9800 . ? C29 H29B 0.9800 . ? C29 H29C 0.9800 . ? C30 C31 1.527(4) . ? C30 H30A 0.9900 . ? C30 H30B 0.9900 . ? C31 C32 1.530(5) . ? C31 H31A 0.9900 . ? C31 H31B 0.9900 . ? C32 C33 1.516(5) . ? C32 H32A 0.9900 . ? C32 H32B 0.9900 . ? C33 C34 1.522(4) . ? C33 H33A 0.9900 . ? C33 H33B 0.9900 . ? C34 H34A 0.9900 . ? C34 H34B 0.9900 . ? C35 C37 1.532(3) . ? C35 H35A 0.9800 . ? C35 H35B 0.9800 . ? C35 H35C 0.9800 . ? C36 C37 1.529(3) . ? C36 H36A 0.9800 . ? C36 H36B 0.9800 . ? C36 H36C 0.9800 . ? C37 C38 1.520(3) . ? C37 H37 1.0000 . ? C38 C39 1.390(3) . ? C38 C44 1.417(3) . ? C39 C40 1.384(4) . ? C39 H39 0.9500 . ? C40 C41 1.385(4) . ? C40 H40 0.9500 . ? C41 C45 1.391(3) . ? C41 H41 0.9500 . ? C42 C46 1.531(4) . ? C42 H42A 0.9800 . ? C42 H42B 0.9800 . ? C42 H42C 0.9800 . ? C43 C46 1.536(3) . ? C43 H43A 0.9800 . ? C43 H43B 0.9800 . ? C43 H43C 0.9800 . ? C44 C45 1.406(3) . ? C45 C46 1.524(3) . ? C46 H46 1.0000 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C24 Si1 C1 112.70(10) . . ? C24 Si1 C23 126.42(10) . . ? C1 Si1 C23 101.77(10) . . ? C21 N1 C1 120.98(17) . . ? C21 N1 C4 121.72(17) . . ? C1 N1 C4 114.54(17) . . ? N1 C1 C2 104.55(17) . . ? N1 C1 Si1 111.66(15) . . ? C2 C1 Si1 120.81(16) . . ? N1 C1 H1 107.4(14) . . ? C2 C1 H1 105.6(14) . . ? Si1 C1 H1 106.1(13) . . ? C24 N2 C44 124.46(18) . . ? C24 N2 C27 113.51(18) . . ? C44 N2 C27 121.93(17) . . ? C7 C2 C3 111.0(2) . . ? C7 C2 C11 107.8(2) . . ? C3 C2 C11 111.74(19) . . ? C7 C2 C1 114.29(19) . . ? C3 C2 C1 103.07(18) . . ? C11 C2 C1 108.93(19) . . ? C4 C3 C2 107.76(18) . . ? C4 C3 H3A 110.2 . . ? C2 C3 H3A 110.2 . . ? C4 C3 H3B 110.2 . . ? C2 C3 H3B 110.2 . . ? H3A C3 H3B 108.5 . . ? N1 C4 C3 101.92(17) . . ? N1 C4 C6 112.07(18) . . ? C3 C4 C6 112.9(2) . . ? N1 C4 C5 114.3(2) . . ? C3 C4 C5 110.05(19) . . ? C6 C4 C5 105.71(19) . . ? C4 C5 H5A 109.5 . . ? C4 C5 H5B 109.5 . . ? H5A C5 H5B 109.5 . . ? C4 C5 H5C 109.5 . . ? H5A C5 H5C 109.5 . . ? H5B C5 H5C 109.5 . . ? C4 C6 H6A 109.5 . . ? C4 C6 H6B 109.5 . . ? H6A C6 H6B 109.5 . . ? C4 C6 H6C 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C2 C7 C8 111.9(2) . . ? C2 C7 H7A 109.2 . . ? C8 C7 H7A 109.2 . . ? C2 C7 H7B 109.2 . . ? C8 C7 H7B 109.2 . . ? H7A C7 H7B 107.9 . . ? C9 C8 C7 112.5(2) . . ? C9 C8 H8A 109.1 . . ? C7 C8 H8A 109.1 . . ? C9 C8 H8B 109.1 . . ? C7 C8 H8B 109.1 . . ? H8A C8 H8B 107.8 . . ? C8 C9 C10 111.7(2) . . ? C8 C9 H9A 109.3 . . ? C10 C9 H9A 109.3 . . ? C8 C9 H9B 109.3 . . ? C10 C9 H9B 109.3 . . ? H9A C9 H9B 107.9 . . ? C9 C10 C11 109.9(2) . . ? C9 C10 H10A 109.7 . . ? C11 C10 H10A 109.7 . . ? C9 C10 H10B 109.7 . . ? C11 C10 H10B 109.7 . . ? H10A C10 H10B 108.2 . . ? C10 C11 C2 114.2(2) . . ? C10 C11 H11A 108.7 . . ? C2 C11 H11A 108.7 . . ? C10 C11 H11B 108.7 . . ? C2 C11 H11B 108.7 . . ? H11A C11 H11B 107.6 . . ? C14 C12 H12A 109.5 . . ? C14 C12 H12B 109.5 . . ? H12A C12 H12B 109.5 . . ? C14 C12 H12C 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? C14 C13 H13A 109.5 . . ? C14 C13 H13B 109.5 . . ? H13A C13 H13B 109.5 . . ? C14 C13 H13C 109.5 . . ? H13A C13 H13C 109.5 . . ? H13B C13 H13C 109.5 . . ? C15 C14 C13 109.5(2) . . ? C15 C14 C12 113.5(2) . . ? C13 C14 C12 110.2(2) . . ? C15 C14 H14 107.8 . . ? C13 C14 H14 107.8 . . ? C12 C14 H14 107.8 . . ? C16 C15 C21 119.2(2) . . ? C16 C15 C14 118.4(2) . . ? C21 C15 C14 122.1(2) . . ? C17 C16 C15 120.7(2) . . ? C17 C16 H16 119.6 . . ? C15 C16 H16 119.6 . . ? C16 C17 C18 119.4(2) . . ? C16 C17 H17 120.3 . . ? C18 C17 H17 120.3 . . ? C17 C18 C22 122.2(2) . . ? C17 C18 H18 118.9 . . ? C22 C18 H18 118.9 . . ? C23 C19 H19A 109.5 . . ? C23 C19 H19B 109.5 . . ? H19A C19 H19B 109.5 . . ? C23 C19 H19C 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C23 C20 H20A 109.5 . . ? C23 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C23 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? C15 C21 C22 120.2(2) . . ? C15 C21 N1 119.03(19) . . ? C22 C21 N1 120.7(2) . . ? C18 C22 C21 117.1(2) . . ? C18 C22 C23 120.1(2) . . ? C21 C22 C23 122.5(2) . . ? C22 C23 C19 112.68(19) . . ? C22 C23 C20 110.7(2) . . ? C19 C23 C20 105.8(2) . . ? C22 C23 Si1 106.69(15) . . ? C19 C23 Si1 105.77(16) . . ? C20 C23 Si1 115.27(16) . . ? N2 C24 C25 106.16(18) . . ? N2 C24 Si1 129.72(17) . . ? C25 C24 Si1 122.39(15) . . ? C34 C25 C30 110.4(2) . . ? C34 C25 C26 110.7(2) . . ? C30 C25 C26 108.45(19) . . ? C34 C25 C24 113.8(2) . . ? C30 C25 C24 109.40(19) . . ? C26 C25 C24 103.81(17) . . ? C27 C26 C25 106.39(19) . . ? C27 C26 H26A 110.5 . . ? C25 C26 H26A 110.5 . . ? C27 C26 H26B 110.5 . . ? C25 C26 H26B 110.5 . . ? H26A C26 H26B 108.6 . . ? N2 C27 C29 111.71(19) . . ? N2 C27 C26 100.38(18) . . ? C29 C27 C26 112.6(2) . . ? N2 C27 C28 112.32(19) . . ? C29 C27 C28 108.9(2) . . ? C26 C27 C28 110.8(2) . . ? C27 C28 H28A 109.5 . . ? C27 C28 H28B 109.5 . . ? H28A C28 H28B 109.5 . . ? C27 C28 H28C 109.5 . . ? H28A C28 H28C 109.5 . . ? H28B C28 H28C 109.5 . . ? C27 C29 H29A 109.5 . . ? C27 C29 H29B 109.5 . . ? H29A C29 H29B 109.5 . . ? C27 C29 H29C 109.5 . . ? H29A C29 H29C 109.5 . . ? H29B C29 H29C 109.5 . . ? C31 C30 C25 112.5(2) . . ? C31 C30 H30A 109.1 . . ? C25 C30 H30A 109.1 . . ? C31 C30 H30B 109.1 . . ? C25 C30 H30B 109.1 . . ? H30A C30 H30B 107.8 . . ? C30 C31 C32 110.4(2) . . ? C30 C31 H31A 109.6 . . ? C32 C31 H31A 109.6 . . ? C30 C31 H31B 109.6 . . ? C32 C31 H31B 109.6 . . ? H31A C31 H31B 108.1 . . ? C33 C32 C31 110.9(3) . . ? C33 C32 H32A 109.5 . . ? C31 C32 H32A 109.5 . . ? C33 C32 H32B 109.5 . . ? C31 C32 H32B 109.5 . . ? H32A C32 H32B 108.0 . . ? C32 C33 C34 111.8(3) . . ? C32 C33 H33A 109.3 . . ? C34 C33 H33A 109.3 . . ? C32 C33 H33B 109.3 . . ? C34 C33 H33B 109.3 . . ? H33A C33 H33B 107.9 . . ? C33 C34 C25 113.6(2) . . ? C33 C34 H34A 108.8 . . ? C25 C34 H34A 108.8 . . ? C33 C34 H34B 108.8 . . ? C25 C34 H34B 108.8 . . ? H34A C34 H34B 107.7 . . ? C37 C35 H35A 109.5 . . ? C37 C35 H35B 109.5 . . ? H35A C35 H35B 109.5 . . ? C37 C35 H35C 109.5 . . ? H35A C35 H35C 109.5 . . ? H35B C35 H35C 109.5 . . ? C37 C36 H36A 109.5 . . ? C37 C36 H36B 109.5 . . ? H36A C36 H36B 109.5 . . ? C37 C36 H36C 109.5 . . ? H36A C36 H36C 109.5 . . ? H36B C36 H36C 109.5 . . ? C38 C37 C36 112.8(2) . . ? C38 C37 C35 111.0(2) . . ? C36 C37 C35 110.2(2) . . ? C38 C37 H37 107.5 . . ? C36 C37 H37 107.5 . . ? C35 C37 H37 107.5 . . ? C39 C38 C44 117.7(2) . . ? C39 C38 C37 119.7(2) . . ? C44 C38 C37 122.6(2) . . ? C40 C39 C38 121.5(2) . . ? C40 C39 H39 119.3 . . ? C38 C39 H39 119.3 . . ? C39 C40 C41 119.9(2) . . ? C39 C40 H40 120.1 . . ? C41 C40 H40 120.1 . . ? C40 C41 C45 121.4(2) . . ? C40 C41 H41 119.3 . . ? C45 C41 H41 119.3 . . ? C46 C42 H42A 109.5 . . ? C46 C42 H42B 109.5 . . ? H42A C42 H42B 109.5 . . ? C46 C42 H42C 109.5 . . ? H42A C42 H42C 109.5 . . ? H42B C42 H42C 109.5 . . ? C46 C43 H43A 109.5 . . ? C46 C43 H43B 109.5 . . ? H43A C43 H43B 109.5 . . ? C46 C43 H43C 109.5 . . ? H43A C43 H43C 109.5 . . ? H43B C43 H43C 109.5 . . ? C45 C44 C38 121.6(2) . . ? C45 C44 N2 121.1(2) . . ? C38 C44 N2 117.3(2) . . ? C41 C45 C44 117.9(2) . . ? C41 C45 C46 118.6(2) . . ? C44 C45 C46 123.5(2) . . ? C45 C46 C42 113.7(2) . . ? C45 C46 C43 109.9(2) . . ? C42 C46 C43 109.0(2) . . ? C45 C46 H46 108.0 . . ? C42 C46 H46 108.0 . . ? C43 C46 H46 108.0 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C21 N1 C1 C2 -164.49(19) . . . . ? C4 N1 C1 C2 -3.0(3) . . . . ? C21 N1 C1 Si1 -32.2(3) . . . . ? C4 N1 C1 Si1 129.24(16) . . . . ? N1 C1 C2 C7 139.6(2) . . . . ? Si1 C1 C2 C7 12.8(3) . . . . ? N1 C1 C2 C3 19.0(2) . . . . ? Si1 C1 C2 C3 -107.75(19) . . . . ? N1 C1 C2 C11 -99.8(2) . . . . ? Si1 C1 C2 C11 133.46(18) . . . . ? C7 C2 C3 C4 -151.51(19) . . . . ? C11 C2 C3 C4 88.1(2) . . . . ? C1 C2 C3 C4 -28.7(2) . . . . ? C21 N1 C4 C3 146.9(2) . . . . ? C1 N1 C4 C3 -14.4(2) . . . . ? C21 N1 C4 C6 25.9(3) . . . . ? C1 N1 C4 C6 -135.5(2) . . . . ? C21 N1 C4 C5 -94.4(2) . . . . ? C1 N1 C4 C5 104.3(2) . . . . ? C2 C3 C4 N1 26.5(2) . . . . ? C2 C3 C4 C6 146.94(19) . . . . ? C2 C3 C4 C5 -95.2(2) . . . . ? C3 C2 C7 C8 -69.0(3) . . . . ? C11 C2 C7 C8 53.7(3) . . . . ? C1 C2 C7 C8 175.0(2) . . . . ? C2 C7 C8 C9 -56.0(3) . . . . ? C7 C8 C9 C10 55.4(3) . . . . ? C8 C9 C10 C11 -54.3(3) . . . . ? C9 C10 C11 C2 56.1(3) . . . . ? C7 C2 C11 C10 -55.4(3) . . . . ? C3 C2 C11 C10 66.8(3) . . . . ? C1 C2 C11 C10 -179.9(2) . . . . ? C13 C14 C15 C16 -65.7(3) . . . . ? C12 C14 C15 C16 57.9(3) . . . . ? C13 C14 C15 C21 107.6(3) . . . . ? C12 C14 C15 C21 -128.8(2) . . . . ? C21 C15 C16 C17 -2.3(4) . . . . ? C14 C15 C16 C17 171.2(2) . . . . ? C15 C16 C17 C18 -5.8(4) . . . . ? C16 C17 C18 C22 5.7(4) . . . . ? C16 C15 C21 C22 10.7(3) . . . . ? C14 C15 C21 C22 -162.5(2) . . . . ? C16 C15 C21 N1 -170.3(2) . . . . ? C14 C15 C21 N1 16.4(3) . . . . ? C1 N1 C21 C15 -120.8(2) . . . . ? C4 N1 C21 C15 79.0(3) . . . . ? C1 N1 C21 C22 58.1(3) . . . . ? C4 N1 C21 C22 -102.0(2) . . . . ? C17 C18 C22 C21 2.5(3) . . . . ? C17 C18 C22 C23 -172.8(2) . . . . ? C15 C21 C22 C18 -10.7(3) . . . . ? N1 C21 C22 C18 170.3(2) . . . . ? C15 C21 C22 C23 164.4(2) . . . . ? N1 C21 C22 C23 -14.5(3) . . . . ? C18 C22 C23 C19 -106.8(2) . . . . ? C21 C22 C23 C19 78.2(3) . . . . ? C18 C22 C23 C20 11.4(3) . . . . ? C21 C22 C23 C20 -163.6(2) . . . . ? C18 C22 C23 Si1 137.57(19) . . . . ? C21 C22 C23 Si1 -37.5(3) . . . . ? C44 N2 C24 C25 -157.5(2) . . . . ? C27 N2 C24 C25 19.0(2) . . . . ? C44 N2 C24 Si1 37.5(3) . . . . ? C27 N2 C24 Si1 -146.00(19) . . . . ? C1 Si1 C24 N2 -177.42(19) . . . . ? C23 Si1 C24 N2 -51.7(3) . . . . ? C1 Si1 C24 C25 19.8(2) . . . . ? C23 Si1 C24 C25 145.44(18) . . . . ? N2 C24 C25 C34 -119.1(2) . . . . ? Si1 C24 C25 C34 47.2(3) . . . . ? N2 C24 C25 C30 116.9(2) . . . . ? Si1 C24 C25 C30 -76.8(2) . . . . ? N2 C24 C25 C26 1.3(2) . . . . ? Si1 C24 C25 C26 167.62(17) . . . . ? C34 C25 C26 C27 102.6(2) . . . . ? C30 C25 C26 C27 -136.1(2) . . . . ? C24 C25 C26 C27 -19.9(2) . . . . ? C24 N2 C27 C29 -150.4(2) . . . . ? C44 N2 C27 C29 26.2(3) . . . . ? C24 N2 C27 C26 -30.9(2) . . . . ? C44 N2 C27 C26 145.7(2) . . . . ? C24 N2 C27 C28 86.9(2) . . . . ? C44 N2 C27 C28 -96.6(2) . . . . ? C25 C26 C27 N2 29.3(2) . . . . ? C25 C26 C27 C29 148.2(2) . . . . ? C25 C26 C27 C28 -89.6(2) . . . . ? C34 C25 C30 C31 51.8(3) . . . . ? C26 C25 C30 C31 -69.6(3) . . . . ? C24 C25 C30 C31 177.8(2) . . . . ? C25 C30 C31 C32 -56.5(3) . . . . ? C30 C31 C32 C33 58.1(3) . . . . ? C31 C32 C33 C34 -56.3(3) . . . . ? C32 C33 C34 C25 52.9(3) . . . . ? C30 C25 C34 C33 -49.8(3) . . . . ? C26 C25 C34 C33 70.3(3) . . . . ? C24 C25 C34 C33 -173.3(2) . . . . ? C36 C37 C38 C39 -43.5(3) . . . . ? C35 C37 C38 C39 80.7(3) . . . . ? C36 C37 C38 C44 136.3(2) . . . . ? C35 C37 C38 C44 -99.5(3) . . . . ? C44 C38 C39 C40 -0.2(3) . . . . ? C37 C38 C39 C40 179.6(2) . . . . ? C38 C39 C40 C41 0.5(4) . . . . ? C39 C40 C41 C45 -0.6(4) . . . . ? C39 C38 C44 C45 -0.1(3) . . . . ? C37 C38 C44 C45 -179.9(2) . . . . ? C39 C38 C44 N2 177.4(2) . . . . ? C37 C38 C44 N2 -2.4(3) . . . . ? C24 N2 C44 C45 -99.5(3) . . . . ? C27 N2 C44 C45 84.3(3) . . . . ? C24 N2 C44 C38 83.0(3) . . . . ? C27 N2 C44 C38 -93.2(2) . . . . ? C40 C41 C45 C44 0.4(3) . . . . ? C40 C41 C45 C46 -178.6(2) . . . . ? C38 C44 C45 C41 0.0(3) . . . . ? N2 C44 C45 C41 -177.4(2) . . . . ? C38 C44 C45 C46 178.9(2) . . . . ? N2 C44 C45 C46 1.5(3) . . . . ? C41 C45 C46 C42 -57.9(3) . . . . ? C44 C45 C46 C42 123.1(3) . . . . ? C41 C45 C46 C43 64.5(3) . . . . ? C44 C45 C46 C43 -114.4(3) . . . . ? _refine_diff_density_max 0.445 _refine_diff_density_min -0.436 _refine_diff_density_rms 0.057 _shelxl_version_number 2014-3 _shelx_res_file ; REM Solution 1 R1 0.160 Rweak 0.008, Alpha = 0.0508 in P2(1)/n REM Formula: C46 N2 Si TITL P21n in P2(1)/n CELL 0.56086 9.533 18.139 22.863 90.00 93.00 90.00 ZERR 4.00 0.002 0.002 0.003 0.00 0.02 0.00 LATT 1 SYMM 1/2-X, 1/2+Y, 1/2-Z SFAC C H N SI UNIT 184 280 8 4 TEMP -173.150 L.S. 10 SIZE 0.10 0.09 0.07 BOND $H CONF LIST 4 FMAP 2 PLAN 20 OMIT 0 1 1 ACTA WGHT 0.076500 2.032600 FVAR 0.34489 SI1 4 0.688889 0.437338 0.267619 11.00000 0.01969 0.01687 = 0.01910 0.00019 -0.00163 0.00208 N1 3 0.681940 0.359648 0.375117 11.00000 0.01938 0.01257 = 0.01665 -0.00094 -0.00442 -0.00102 C1 1 0.666667 0.434439 0.351965 11.00000 0.02133 0.01316 = 0.01975 -0.00011 -0.00629 0.00043 H1 2 0.568223 0.450484 0.357858 11.00000 -1.20000 N2 3 0.508422 0.481940 0.167313 11.00000 0.02166 0.01397 = 0.01822 0.00051 -0.00120 0.00314 C2 1 0.762341 0.483192 0.395010 11.00000 0.02708 0.01669 = 0.02180 -0.00065 -0.00820 -0.00491 C3 1 0.861278 0.426051 0.425649 11.00000 0.02333 0.02241 = 0.01925 0.00078 -0.00749 -0.00412 AFIX 23 H3A 2 0.947853 0.420631 0.403937 11.00000 -1.20000 H3B 2 0.888009 0.442302 0.466043 11.00000 -1.20000 AFIX 0 C4 1 0.782734 0.352602 0.426883 11.00000 0.02330 0.01766 = 0.01634 0.00082 -0.00587 -0.00084 C5 1 0.712448 0.343552 0.486075 11.00000 0.03970 0.03285 = 0.01909 0.00476 -0.00374 -0.00725 AFIX 137 H5A 2 0.639343 0.381104 0.489282 11.00000 -1.50000 H5B 2 0.783344 0.349415 0.518350 11.00000 -1.50000 H5C 2 0.670214 0.294413 0.488019 11.00000 -1.50000 AFIX 0 C6 1 0.879741 0.285781 0.421939 11.00000 0.03347 0.02279 = 0.02841 0.00152 -0.01134 0.00331 AFIX 137 H6A 2 0.823935 0.240427 0.422331 11.00000 -1.50000 H6B 2 0.949197 0.285477 0.455091 11.00000 -1.50000 H6C 2 0.928133 0.288704 0.385234 11.00000 -1.50000 AFIX 0 C7 1 0.846311 0.542930 0.364600 11.00000 0.03435 0.02271 = 0.02897 0.00409 -0.00897 -0.00742 AFIX 23 H7A 2 0.781191 0.573385 0.339600 11.00000 -1.20000 H7B 2 0.913552 0.519120 0.338970 11.00000 -1.20000 AFIX 0 C8 1 0.927337 0.592982 0.408956 11.00000 0.04388 0.02708 = 0.04349 0.00587 -0.01075 -0.01315 AFIX 23 H8A 2 0.999822 0.563418 0.430883 11.00000 -1.20000 H8B 2 0.975887 0.632025 0.387502 11.00000 -1.20000 AFIX 0 C9 1 0.832837 0.628424 0.451756 11.00000 0.05772 0.02854 = 0.05101 -0.01269 -0.01716 -0.00878 AFIX 23 H9A 2 0.767672 0.662803 0.430464 11.00000 -1.20000 H9B 2 0.890609 0.657359 0.480754 11.00000 -1.20000 AFIX 0 C10 1 0.748595 0.571464 0.483535 11.00000 0.04842 0.03259 = 0.03283 -0.01368 -0.01226 0.00299 AFIX 23 H10A 2 0.681705 0.596575 0.508577 11.00000 -1.20000 H10B 2 0.812592 0.541004 0.509033 11.00000 -1.20000 AFIX 0 C11 1 0.668059 0.522140 0.439151 11.00000 0.03603 0.02535 = 0.02789 -0.00647 -0.01027 0.00210 AFIX 23 H11A 2 0.597237 0.552443 0.416933 11.00000 -1.20000 H11B 2 0.617072 0.484071 0.460667 11.00000 -1.20000 AFIX 0 C12 1 0.438881 0.215246 0.459778 11.00000 0.04358 0.03851 = 0.03403 0.00114 0.01224 -0.01233 AFIX 137 H12A 2 0.391118 0.170422 0.445429 11.00000 -1.50000 H12B 2 0.388415 0.235936 0.492238 11.00000 -1.50000 H12C 2 0.535307 0.203195 0.473450 11.00000 -1.50000 AFIX 0 C13 1 0.292657 0.285927 0.384166 11.00000 0.02572 0.04407 = 0.04550 -0.00654 0.00524 -0.00705 AFIX 137 H13A 2 0.295195 0.323835 0.353698 11.00000 -1.50000 H13B 2 0.233123 0.302717 0.415199 11.00000 -1.50000 H13C 2 0.254243 0.240179 0.367076 11.00000 -1.50000 AFIX 0 C14 1 0.441706 0.271945 0.409981 11.00000 0.02591 0.02890 = 0.02910 -0.00345 0.00625 -0.00779 AFIX 13 H14 2 0.478324 0.319368 0.427058 11.00000 -1.20000 AFIX 0 C15 1 0.536128 0.249694 0.361245 11.00000 0.02181 0.02094 = 0.02538 -0.00299 -0.00389 -0.00324 C16 1 0.509371 0.182865 0.332255 11.00000 0.03140 0.01999 = 0.03324 0.00054 -0.00239 -0.00668 AFIX 43 H16 2 0.442497 0.149586 0.346735 11.00000 -1.20000 AFIX 0 C17 1 0.579145 0.164731 0.282792 11.00000 0.04363 0.01617 = 0.03161 -0.00566 -0.00924 0.00071 AFIX 43 H17 2 0.567057 0.117434 0.265407 11.00000 -1.20000 AFIX 0 C18 1 0.667007 0.216195 0.258738 11.00000 0.03666 0.01784 = 0.02132 -0.00496 -0.00540 0.00936 AFIX 43 H18 2 0.707808 0.205033 0.222757 11.00000 -1.20000 AFIX 0 C19 1 0.931014 0.350720 0.279738 11.00000 0.02836 0.02805 = 0.02993 0.00800 0.00674 0.00725 AFIX 137 H19A 2 0.978452 0.302812 0.279194 11.00000 -1.50000 H19B 2 0.929464 0.368487 0.320179 11.00000 -1.50000 H19C 2 0.981635 0.386123 0.256265 11.00000 -1.50000 AFIX 0 C20 1 0.793573 0.321523 0.189420 11.00000 0.03289 0.02655 = 0.02290 0.00091 0.00543 0.00967 AFIX 137 H20A 2 0.700106 0.310904 0.171517 11.00000 -1.50000 H20B 2 0.853183 0.277742 0.186881 11.00000 -1.50000 H20C 2 0.835669 0.362556 0.168653 11.00000 -1.50000 AFIX 0 C21 1 0.639362 0.297521 0.340615 11.00000 0.01779 0.01466 = 0.01931 -0.00338 -0.00567 0.00273 C22 1 0.697694 0.284226 0.285758 11.00000 0.02170 0.01514 = 0.02080 0.00069 -0.00532 0.00745 C23 1 0.780634 0.342518 0.254146 11.00000 0.02560 0.01975 = 0.01885 -0.00037 0.00405 0.00623 C24 1 0.534409 0.473869 0.227037 11.00000 0.01894 0.01821 = 0.01885 -0.00004 0.00012 -0.00057 C25 1 0.422259 0.521585 0.256604 11.00000 0.02149 0.02290 = 0.02105 -0.00386 -0.00167 0.00725 C26 1 0.332521 0.553964 0.204200 11.00000 0.02385 0.02458 = 0.02825 -0.00116 -0.00405 0.00738 AFIX 23 H26A 2 0.244384 0.525590 0.197652 11.00000 -1.20000 H26B 2 0.308405 0.606054 0.211813 11.00000 -1.20000 AFIX 0 C27 1 0.421804 0.548284 0.151040 11.00000 0.02493 0.01725 = 0.02647 0.00077 -0.00263 0.00548 C28 1 0.511778 0.617794 0.144893 11.00000 0.03402 0.01755 = 0.04213 0.00454 0.00055 0.00613 AFIX 137 H28A 2 0.558591 0.615965 0.107767 11.00000 -1.50000 H28B 2 0.582598 0.620231 0.177487 11.00000 -1.50000 H28C 2 0.451570 0.661550 0.145503 11.00000 -1.50000 AFIX 0 C29 1 0.333827 0.536351 0.094295 11.00000 0.03207 0.02897 = 0.02617 0.00483 -0.00389 0.00713 AFIX 137 H29A 2 0.396009 0.528256 0.062101 11.00000 -1.50000 H29B 2 0.275507 0.579960 0.085913 11.00000 -1.50000 H29C 2 0.273355 0.493158 0.098357 11.00000 -1.50000 AFIX 0 C30 1 0.327298 0.470987 0.292218 11.00000 0.02093 0.04204 = 0.02355 0.00050 0.00126 0.00404 AFIX 23 H30A 2 0.278788 0.435343 0.265327 11.00000 -1.20000 H30B 2 0.386755 0.442638 0.321015 11.00000 -1.20000 AFIX 0 C31 1 0.217797 0.514248 0.324539 11.00000 0.03203 0.07543 = 0.03386 -0.00404 0.00853 0.01468 AFIX 23 H31A 2 0.162881 0.479987 0.348105 11.00000 -1.20000 H31B 2 0.152171 0.538898 0.295797 11.00000 -1.20000 AFIX 0 C32 1 0.289300 0.572043 0.364705 11.00000 0.04536 0.08728 = 0.04085 -0.02766 0.00308 0.02591 AFIX 23 H32A 2 0.217016 0.600232 0.384782 11.00000 -1.20000 H32B 2 0.350306 0.547079 0.394975 11.00000 -1.20000 AFIX 0 C33 1 0.376825 0.624544 0.330076 11.00000 0.05158 0.04804 = 0.04392 -0.02193 -0.00689 0.02526 AFIX 23 H33A 2 0.425396 0.659804 0.357278 11.00000 -1.20000 H33B 2 0.314197 0.653072 0.302581 11.00000 -1.20000 AFIX 0 C34 1 0.485266 0.583788 0.295747 11.00000 0.03433 0.02416 = 0.03105 -0.00780 -0.00524 0.00901 AFIX 23 H34A 2 0.557077 0.562439 0.323659 11.00000 -1.20000 H34B 2 0.533010 0.619590 0.270848 11.00000 -1.20000 AFIX 0 C35 1 0.361909 0.296335 0.194304 11.00000 0.02943 0.02616 = 0.03057 0.00380 0.00006 -0.00487 AFIX 137 H35A 2 0.392472 0.249929 0.177086 11.00000 -1.50000 H35B 2 0.275865 0.287883 0.214981 11.00000 -1.50000 H35C 2 0.435762 0.314756 0.221955 11.00000 -1.50000 AFIX 0 C36 1 0.208644 0.328955 0.105421 11.00000 0.02823 0.03177 = 0.03071 -0.00047 -0.00320 -0.00336 AFIX 137 H36A 2 0.193867 0.364710 0.073559 11.00000 -1.50000 H36B 2 0.124054 0.326210 0.127905 11.00000 -1.50000 H36C 2 0.228169 0.280347 0.088994 11.00000 -1.50000 AFIX 0 C37 1 0.333196 0.353286 0.145677 11.00000 0.02631 0.01974 = 0.02459 -0.00015 0.00002 -0.00133 AFIX 13 H37 2 0.306407 0.400500 0.164728 11.00000 -1.20000 AFIX 0 C38 1 0.464702 0.368020 0.112715 11.00000 0.02195 0.01999 = 0.01913 0.00314 -0.00052 0.00049 C39 1 0.502782 0.319350 0.069354 11.00000 0.03325 0.01858 = 0.02769 -0.00346 -0.00036 -0.00100 AFIX 43 H39 2 0.446217 0.277151 0.060984 11.00000 -1.20000 AFIX 0 C40 1 0.621259 0.330985 0.038096 11.00000 0.03386 0.02650 = 0.02280 -0.00734 0.00525 0.00006 AFIX 43 H40 2 0.644875 0.297217 0.008410 11.00000 -1.20000 AFIX 0 C41 1 0.705333 0.391950 0.050174 11.00000 0.03057 0.02781 = 0.02060 0.00340 0.00870 0.00198 AFIX 43 H41 2 0.786971 0.399214 0.028765 11.00000 -1.20000 AFIX 0 C42 1 0.921551 0.489448 0.118890 11.00000 0.02764 0.03243 = 0.05232 -0.00383 0.00415 -0.00516 AFIX 137 H42A 2 0.955423 0.455079 0.089715 11.00000 -1.50000 H42B 2 0.928235 0.466206 0.157630 11.00000 -1.50000 H42C 2 0.979103 0.534237 0.119527 11.00000 -1.50000 AFIX 0 C43 1 0.762458 0.558381 0.048055 11.00000 0.05046 0.02584 = 0.03406 0.00363 0.00733 -0.00814 AFIX 137 H43A 2 0.815843 0.535037 0.017594 11.00000 -1.50000 H43B 2 0.803310 0.606693 0.057821 11.00000 -1.50000 H43C 2 0.664496 0.564620 0.033713 11.00000 -1.50000 AFIX 0 C44 1 0.551804 0.430254 0.124137 11.00000 0.02336 0.01625 = 0.01516 0.00122 -0.00147 0.00210 C45 1 0.672842 0.442756 0.092956 11.00000 0.02359 0.02003 = 0.02074 0.00356 -0.00234 0.00053 C46 1 0.768297 0.509480 0.102952 11.00000 0.03036 0.02087 = 0.02846 0.00083 0.00512 -0.00276 AFIX 13 H46 2 0.732102 0.538874 0.135958 11.00000 -1.20000 AFIX 0 HKLF 4 REM P21n in P2(1)/n REM R1 = 0.0540 for 5196 Fo > 4sig(Fo) and 0.0831 for all 7289 data REM 457 parameters refined using 0 restraints END WGHT 0.0765 2.0326 REM Highest difference peak 0.445, deepest hole -0.436, 1-sigma level 0.057 Q1 1 0.9833 0.3033 0.2543 11.00000 0.05 0.45 Q2 1 0.7397 0.3809 0.2577 11.00000 0.05 0.35 Q3 1 0.5109 0.2033 0.2950 11.00000 0.05 0.34 Q4 1 0.5715 0.1919 0.2495 11.00000 0.05 0.34 Q5 1 0.5334 0.2782 0.3303 11.00000 0.05 0.33 Q6 1 0.8563 0.3413 0.2651 11.00000 0.05 0.31 Q7 1 0.7322 0.3568 0.4027 11.00000 0.05 0.30 Q8 1 1.0184 0.5775 0.3849 11.00000 0.05 0.29 Q9 1 0.8217 0.3212 0.4240 11.00000 0.05 0.29 Q10 1 0.7435 0.5631 0.3694 11.00000 0.05 0.29 Q11 1 0.6969 0.4372 0.3166 11.00000 0.05 0.28 Q12 1 0.8239 0.5826 0.4597 11.00000 0.05 0.28 Q13 1 0.7457 0.3163 0.2719 11.00000 0.05 0.27 Q14 1 0.7165 0.2454 0.2810 11.00000 0.05 0.27 Q15 1 0.6859 0.3967 0.3607 11.00000 0.05 0.26 Q16 1 0.7962 0.3975 0.2132 11.00000 0.05 0.26 Q17 1 0.2977 0.2987 0.1055 11.00000 0.05 0.26 Q18 1 0.3663 0.2795 0.0949 11.00000 0.05 0.25 Q19 1 0.8324 0.6155 0.4084 11.00000 0.05 0.25 Q20 1 0.4372 0.2854 0.3723 11.00000 0.05 0.25 ; _shelx_res_checksum 59324 _shelx_hkl_file ; 1 0 0 6.60 1.20 -1 0 0 3.60 1.10 -1 0 0 7.90 1.40 -1 0 0 7.40 1.60 -1 0 0 4.80 0.90 1 0 0 6.10 1.50 1 0 0 0.30 0.90 2 0 0 2923.21 190.28 -2 0 0 2914.11 189.58 2 0 0 2888.51 190.68 2 0 0 2927.81 189.68 -2 0 0 2885.31 189.98 2 0 0 2961.60 190.08 -2 0 0 2885.11 189.68 -2 0 0 2877.31 190.58 -2 0 0 2957.60 190.38 3 0 0 0.60 3.10 -3 0 0 1.30 3.00 -3 0 0 -1.10 2.30 -3 0 0 2.00 2.40 -3 0 0 -1.90 1.80 -3 0 0 0.30 1.70 3 0 0 0.60 2.50 -4 0 0 410.66 28.10 4 0 0 396.66 30.20 -4 0 0 429.06 29.60 -4 0 0 386.36 27.80 4 0 0 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144.69 10.90 -3 4 0 160.38 12.00 3 4 0 144.59 12.60 3 4 0 143.99 12.20 -3 4 0 152.28 12.70 -4 -4 0 2.50 4.70 -4 -4 0 14.00 4.00 4 -4 0 9.80 5.40 4 4 0 3.10 3.30 -4 4 0 11.80 4.20 -4 4 0 7.20 2.70 -4 4 0 5.60 3.90 4 4 0 12.50 4.90 -5 -4 0 13.20 6.20 -5 -4 0 18.00 4.60 5 -4 0 17.60 6.70 -5 4 0 25.90 5.80 -5 4 0 21.50 5.70 -5 4 0 21.60 4.00 5 4 0 14.60 5.20 5 4 0 24.40 6.30 -6 -4 0 15.40 7.00 6 -4 0 22.00 7.90 -6 -4 0 27.70 5.90 -6 4 0 21.50 4.70 -6 4 0 18.70 6.30 6 4 0 18.40 7.20 6 4 0 26.10 7.00 -6 4 0 9.40 5.30 -7 -4 0 405.56 33.10 -7 -4 0 442.96 30.30 7 -4 0 390.36 33.70 7 4 0 379.36 33.00 -7 4 0 386.26 29.00 -7 4 0 391.06 31.20 -7 4 0 373.16 31.30 7 4 0 413.26 31.60 8 -4 0 3.40 7.90 -8 -4 0 10.00 6.10 -8 -4 0 -0.50 7.30 -8 4 0 2.30 4.30 8 4 0 -1.90 5.60 -8 4 0 3.50 7.40 -8 4 0 1.90 6.60 8 4 0 6.90 8.20 -9 -4 0 43.70 8.00 9 -4 0 39.30 12.80 -9 -4 0 37.10 11.60 -9 -4 0 48.50 11.20 -9 -4 0 41.50 8.60 9 4 0 27.20 11.70 -9 4 0 27.20 11.00 -9 4 0 39.90 7.40 -9 4 0 55.19 11.50 9 4 0 51.19 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9 -5 0 8.40 10.50 -9 5 0 16.00 9.50 9 5 0 29.30 12.60 9 5 0 20.00 9.80 -9 5 0 26.90 10.20 -9 5 0 13.00 5.90 -10 -5 0 8.60 6.90 -10 -5 0 25.50 7.30 -10 -5 0 24.10 12.30 -10 -5 0 33.90 11.20 10 -5 0 15.90 12.80 -10 5 0 14.60 6.90 10 5 0 34.40 13.10 -10 5 0 19.00 10.60 10 5 0 31.90 13.30 -10 5 0 21.50 12.30 11 -5 0 -6.30 11.70 -11 -5 0 9.10 11.10 -11 -5 0 4.80 7.20 -11 5 0 -2.80 6.70 -11 5 0 -0.70 12.00 11 5 0 7.10 12.30 0 -6 0 537.65 35.70 0 -6 0 518.95 34.80 0 -6 0 498.05 35.50 0 -6 0 524.15 34.70 0 -6 0 504.25 35.10 0 6 0 533.95 35.60 0 6 0 507.85 34.70 0 6 0 534.45 36.40 0 6 0 513.65 35.30 0 6 0 527.85 35.20 1 -6 0 58.19 6.60 -1 -6 0 76.29 6.50 1 -6 0 64.99 5.10 1 -6 0 62.79 5.00 -1 -6 0 61.09 5.90 1 -6 0 57.19 6.10 -1 -6 0 49.20 6.80 1 -6 0 57.89 6.20 1 6 0 56.79 7.20 1 6 0 62.39 6.10 1 6 0 46.20 5.90 -1 6 0 53.19 6.70 -1 6 0 62.89 5.00 -1 6 0 61.59 6.30 -1 6 0 50.59 5.80 -1 6 0 57.89 5.00 -1 6 0 65.19 7.70 2 -6 0 10.50 3.90 2 -6 0 9.80 3.10 -2 -6 0 24.70 5.30 2 -6 0 15.00 2.30 2 -6 0 12.00 2.90 -2 -6 0 12.10 3.20 2 -6 0 15.30 2.40 -2 6 0 8.70 2.90 2 6 0 21.40 4.70 -2 6 0 14.10 4.50 2 6 0 25.30 4.00 -2 6 0 10.50 2.10 3 -6 0 762.52 51.49 3 -6 0 758.92 48.90 -3 -6 0 718.33 51.49 3 -6 0 709.23 49.70 -3 -6 0 723.23 49.80 -3 6 0 780.72 51.29 -3 6 0 724.83 48.70 3 6 0 704.23 50.59 3 6 0 764.82 50.69 -3 6 0 717.73 49.60 -4 -6 0 48.90 9.20 4 -6 0 74.69 10.90 -4 -6 0 70.59 8.40 4 6 0 66.29 8.80 -4 6 0 65.49 9.30 -4 6 0 73.39 8.30 -4 6 0 77.59 6.50 4 6 0 67.59 9.20 5 -6 0 -4.60 4.60 -5 -6 0 -0.80 3.40 -5 -6 0 -0.70 4.50 5 6 0 1.30 4.20 -5 6 0 3.60 2.60 -5 6 0 2.20 4.40 -5 6 0 1.80 3.90 5 6 0 10.60 5.50 6 -6 0 66.19 12.70 -6 -6 0 85.39 12.40 -6 -6 0 65.99 8.70 -6 6 0 57.69 10.10 -6 6 0 52.89 7.10 6 6 0 73.89 11.50 6 6 0 70.39 9.90 -6 6 0 61.89 9.60 -7 -6 0 96.79 15.30 -7 -6 0 104.39 12.60 7 -6 0 92.69 15.80 -7 6 0 111.59 14.50 -7 6 0 129.59 11.70 7 6 0 125.79 15.40 -7 6 0 116.89 13.90 7 6 0 95.99 14.80 -8 -6 0 51.49 12.80 -8 -6 0 58.49 9.30 8 -6 0 53.49 13.40 -8 6 0 58.09 8.30 8 6 0 56.69 13.40 -8 6 0 61.49 11.90 8 6 0 64.69 12.10 -8 6 0 53.39 11.00 9 -6 0 16.70 11.50 -9 -6 0 7.30 6.30 -9 -6 0 -4.40 8.90 9 6 0 1.50 8.70 -9 6 0 4.50 5.10 9 6 0 6.20 9.10 -9 6 0 14.80 9.40 -9 6 0 -3.40 7.90 10 -6 0 31.90 15.70 -10 -6 0 13.30 11.80 -10 -6 0 14.40 7.40 10 6 0 16.80 11.80 -10 6 0 11.10 10.90 -10 6 0 28.80 7.40 -10 6 0 22.90 11.90 10 6 0 32.10 13.30 -11 -6 0 -11.90 5.80 -11 -6 0 -15.80 9.80 11 -6 0 -1.00 12.50 11 6 0 9.20 14.60 -11 6 0 -1.10 6.80 0 -7 0 0.20 1.80 0 -7 0 3.20 2.30 0 -7 0 -1.40 1.90 0 -7 0 0.30 1.80 0 7 0 2.60 2.20 0 7 0 0.50 1.80 0 7 0 1.50 2.50 0 7 0 2.10 2.40 1 -7 0 37.90 5.30 1 -7 0 29.20 3.60 -1 -7 0 47.10 6.40 1 -7 0 34.20 4.70 -1 -7 0 45.50 5.30 -1 -7 0 43.30 4.70 1 -7 0 29.80 3.70 1 -7 0 36.60 5.10 -1 7 0 40.10 5.90 -1 7 0 31.50 4.70 1 7 0 36.00 6.00 -1 7 0 31.40 4.80 -1 7 0 33.10 3.70 1 7 0 41.80 5.00 -1 7 0 31.80 6.00 1 7 0 35.70 4.60 -1 7 0 29.10 3.70 2 -7 0 311.77 20.90 -2 -7 0 299.47 23.30 2 -7 0 286.47 20.90 2 -7 0 314.87 21.80 2 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12.90 11.00 9 8 0 17.90 9.60 -9 8 0 25.30 6.40 -9 8 0 14.70 10.70 -9 8 0 1.70 9.30 10 -8 0 -4.50 11.70 -10 -8 0 0.80 9.10 -10 -8 0 -5.80 5.90 -10 8 0 -1.60 11.40 10 8 0 -2.00 11.70 10 8 0 12.10 13.90 0 -9 0 -0.20 2.10 0 -9 0 -1.60 3.00 0 -9 0 2.80 2.50 0 9 0 -2.80 2.30 0 9 0 -5.00 3.40 1 -9 0 22.00 3.40 1 -9 0 11.00 3.80 -1 -9 0 17.40 3.60 -1 -9 0 25.90 5.90 1 -9 0 23.20 4.60 -1 -9 0 18.00 4.10 1 9 0 15.80 3.70 -1 9 0 22.60 6.20 1 9 0 13.40 5.20 2 -9 0 1.80 1.90 -2 -9 0 2.50 2.70 -2 -9 0 -1.80 4.10 2 -9 0 0.50 3.60 2 -9 0 3.70 2.90 -2 9 0 2.10 3.10 -2 9 0 3.10 4.50 2 9 0 7.00 4.50 2 9 0 5.20 3.00 -2 9 0 1.00 2.00 -3 -9 0 223.78 17.80 3 -9 0 262.97 17.80 3 -9 0 227.08 16.30 -3 -9 0 231.58 20.00 3 -9 0 224.88 19.50 3 9 0 239.78 18.70 -3 9 0 215.28 16.40 -3 9 0 222.98 17.70 -3 9 0 248.48 20.20 3 9 0 254.87 20.00 4 -9 0 29.50 7.30 -4 -9 0 39.10 8.50 4 -9 0 30.00 5.50 -4 -9 0 36.80 5.90 -4 9 0 26.30 5.60 -4 9 0 31.20 4.20 4 9 0 26.40 6.80 4 9 0 15.50 6.10 -4 9 0 26.80 7.20 -5 -9 0 2.80 5.70 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0 139.59 12.10 1 10 0 111.89 10.70 -1 10 0 114.09 11.60 -1 10 0 107.79 12.90 1 10 0 88.29 12.20 2 -10 0 204.68 15.50 2 -10 0 226.18 17.90 -2 -10 0 233.38 18.80 2 -10 0 215.08 16.80 -2 -10 0 200.28 16.50 -2 10 0 215.88 15.60 2 10 0 221.18 17.00 -2 10 0 217.78 17.10 2 10 0 225.58 18.80 -2 10 0 224.58 20.80 3 -10 0 13.30 2.80 3 -10 0 11.70 3.90 -3 -10 0 10.40 4.00 3 -10 0 14.20 5.50 -3 -10 0 -2.10 4.40 -3 10 0 12.10 5.50 -3 10 0 13.60 2.90 3 10 0 6.60 5.00 3 10 0 6.50 4.20 -3 10 0 9.00 4.20 4 -10 0 15.50 3.20 4 -10 0 14.40 6.40 -4 -10 0 7.40 6.40 -4 -10 0 20.90 5.20 4 -10 0 15.40 4.70 -4 10 0 24.00 5.40 -4 10 0 21.90 3.50 -4 10 0 16.90 7.00 4 10 0 24.00 6.20 4 10 0 14.50 6.20 -5 -10 0 217.08 22.40 -5 -10 0 211.18 17.50 5 -10 0 241.18 22.60 5 10 0 216.08 20.40 5 10 0 206.68 21.00 -5 10 0 195.28 15.20 -5 10 0 177.38 17.60 -5 10 0 231.88 22.30 -6 -10 0 15.00 8.50 -6 -10 0 16.50 6.60 6 -10 0 17.60 8.50 6 10 0 8.10 7.40 -6 10 0 13.70 6.00 6 10 0 6.00 6.70 -6 10 0 26.90 4.60 -6 10 0 25.30 8.70 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3 28.20 14.60 11 4 -3 19.80 12.70 -11 4 3 14.80 7.70 10 -4 -3 34.40 13.90 -10 -4 3 33.00 12.70 -10 -4 3 22.30 7.50 -10 4 3 16.40 11.00 10 4 -3 16.10 11.60 -10 4 3 23.40 7.90 -9 -4 3 -4.90 4.90 -9 -4 3 5.40 6.80 -9 -4 3 4.10 8.70 -9 -4 3 6.60 4.70 9 -4 -3 4.40 9.70 9 4 -3 20.40 10.20 -9 4 3 -0.90 6.80 -9 4 3 1.50 4.60 9 4 -3 4.90 8.10 -9 4 3 2.40 9.00 -8 -4 3 76.09 10.10 -8 -4 3 67.79 13.50 8 -4 -3 44.60 13.70 -8 4 3 66.09 12.20 -8 4 3 59.39 10.60 -8 4 3 77.29 9.50 8 4 -3 56.49 10.70 8 4 -3 59.09 12.40 7 -4 -3 96.39 15.30 -7 -4 3 83.89 13.90 -7 -4 3 96.69 11.50 -7 4 3 89.99 13.30 7 4 -3 95.09 12.00 7 4 -3 111.29 15.10 -7 4 3 89.69 10.60 -7 4 3 95.09 11.90 6 -4 -3 193.28 21.30 -6 -4 3 193.78 16.80 -6 -4 3 170.28 20.30 -6 4 3 201.58 17.30 6 4 -3 198.08 17.10 6 4 -3 233.18 21.90 -6 4 3 215.98 20.40 -6 4 3 220.48 16.30 5 -4 -3 17.50 6.40 -5 -4 3 15.20 4.60 -5 -4 3 11.30 5.70 5 4 -3 26.30 5.30 -5 4 3 22.70 4.20 -5 4 3 29.20 5.60 5 4 -3 9.50 5.30 -5 4 3 34.70 7.00 4 -4 -3 7.60 4.70 -4 -4 3 2.90 3.30 -4 -4 3 2.30 4.60 -4 4 3 10.60 3.80 4 4 -3 7.40 4.40 -4 4 3 15.00 5.10 4 4 -3 5.20 3.10 -4 4 3 5.90 2.80 -3 -4 3 407.96 25.40 3 -4 -3 311.77 23.30 -3 -4 3 362.56 23.20 -3 -4 3 363.46 23.30 3 -4 -3 280.47 23.90 -3 4 3 285.17 23.50 -3 4 3 293.57 23.00 3 4 -3 354.56 24.30 -3 4 3 282.67 22.40 3 4 -3 338.47 23.00 -2 -4 3 500.85 35.30 2 -4 -3 518.85 35.70 -2 -4 3 499.95 35.10 2 -4 -3 558.54 35.20 -2 -4 3 487.15 36.20 2 -4 -3 520.95 35.50 -2 4 3 507.55 35.80 -2 4 3 503.85 35.50 2 4 -3 525.95 35.40 -2 4 3 515.05 35.40 2 4 -3 532.65 35.90 -2 4 3 532.35 34.90 1 -4 -3 8.50 2.20 1 -4 -3 5.90 2.60 -1 -4 3 13.60 3.10 -1 -4 3 10.50 3.30 -1 -4 3 11.60 3.00 1 -4 -3 8.90 2.30 1 -4 -3 12.80 3.30 -1 -4 3 5.10 2.10 1 -4 -3 5.80 2.10 1 -4 -3 6.80 2.60 -1 -4 3 8.70 2.80 -1 4 3 9.50 3.20 1 4 -3 12.40 3.10 -1 4 3 15.70 3.20 1 4 -3 9.90 2.80 -1 4 3 5.00 2.00 1 4 -3 5.50 2.50 1 4 -3 11.60 3.30 -1 4 3 7.20 1.90 1 4 -3 11.20 2.40 0 -4 -3 1878.11 126.39 0 -4 -3 1876.11 126.29 0 -4 -3 1887.71 126.29 0 -4 3 1976.40 124.99 0 -4 -3 1850.91 125.49 0 -4 3 1982.30 125.49 0 -4 3 1995.20 126.49 0 -4 -3 1895.61 125.49 0 -4 3 1953.60 126.39 0 -4 3 1924.71 126.29 0 4 3 1855.11 126.39 0 4 3 1830.92 125.49 0 4 -3 1965.80 126.29 0 4 -3 1955.30 126.29 0 4 -3 2005.50 124.99 0 4 -3 2032.20 125.49 0 4 -3 1875.41 126.39 0 4 3 1869.91 126.19 0 4 3 1894.91 126.29 0 4 3 1883.51 125.49 1 -4 3 39.50 5.40 -1 -4 -3 43.00 3.80 -1 -4 -3 30.70 4.10 -1 -4 -3 32.20 5.40 -1 4 -3 41.30 5.90 1 4 3 28.60 4.90 -1 4 -3 50.69 6.50 1 4 3 39.20 3.90 -2 -4 -3 120.69 11.70 -2 -4 -3 123.29 9.90 2 -4 3 130.59 8.60 2 -4 3 116.99 8.20 -2 -4 -3 132.89 9.80 2 -4 3 106.79 11.80 2 4 3 112.69 9.90 -2 4 -3 126.99 12.30 2 4 3 128.59 10.80 -2 4 -3 121.29 8.50 -2 4 -3 115.79 8.20 3 -4 3 59.09 5.60 3 -4 3 47.10 4.40 3 -4 3 47.60 7.80 -3 -4 -3 53.09 6.00 -3 -4 -3 51.09 7.40 3 4 3 54.49 7.40 3 4 3 45.90 7.10 -3 4 -3 50.99 7.60 -3 4 -3 49.70 5.40 -3 4 -3 50.29 4.40 -4 -4 -3 54.09 8.70 4 -4 3 35.90 8.20 4 -4 3 53.59 5.40 4 -4 3 37.80 7.90 4 -4 3 55.59 6.80 -4 -4 -3 65.09 7.10 4 4 3 42.70 7.70 -4 4 -3 65.39 9.00 -4 4 -3 49.40 5.30 4 4 3 66.39 8.60 -4 4 -3 51.49 6.50 -5 -4 -3 54.59 9.40 5 -4 3 67.79 10.60 5 -4 3 55.99 11.10 -5 -4 -3 53.79 7.30 -5 4 -3 67.09 10.00 5 4 3 50.99 9.00 -5 4 -3 53.99 7.70 5 4 3 61.49 9.50 -5 4 -3 60.59 6.40 6 -4 3 -5.80 5.60 -6 -4 -3 7.10 6.00 -6 -4 -3 -2.40 3.20 6 -4 3 5.70 6.90 -6 4 -3 1.70 2.80 -6 4 -3 11.70 6.00 -6 4 -3 9.50 4.80 6 4 3 -2.80 5.30 6 4 3 0.60 5.90 -7 -4 -3 3.90 4.60 7 -4 3 14.80 8.60 -7 -4 -3 11.20 7.70 7 -4 3 9.40 7.70 7 4 3 17.80 7.20 -7 4 -3 18.90 7.80 -7 4 -3 12.90 4.20 -7 4 -3 6.70 6.00 7 4 3 21.40 8.50 8 -4 3 -3.00 6.80 8 -4 3 8.50 8.80 -8 -4 -3 -0.40 7.00 -8 -4 -3 5.00 5.40 -8 4 -3 -3.70 6.40 -8 4 -3 2.10 4.00 8 4 3 -3.20 8.30 -8 4 -3 3.90 6.70 8 4 3 6.60 8.30 -9 -4 -3 37.80 10.90 9 -4 3 35.10 11.40 -9 -4 -3 37.80 11.80 9 -4 3 34.20 13.50 -9 -4 -3 49.30 9.60 -9 -4 -3 40.70 8.10 9 4 3 44.80 11.80 9 4 3 25.60 11.70 -9 4 -3 27.40 10.50 -9 4 -3 33.20 10.60 -9 4 -3 44.50 7.90 -10 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4.00 7 -5 -3 7.60 8.00 -7 -5 3 -2.80 5.80 -7 5 3 -0.50 5.70 -7 5 3 2.10 5.20 -7 5 3 1.10 3.90 7 5 -3 -5.50 6.90 7 5 -3 0.20 5.90 6 -5 -3 57.49 11.60 -6 -5 3 76.59 12.40 -6 -5 3 98.29 10.30 -6 5 3 56.39 10.50 6 5 -3 101.79 10.80 6 5 -3 87.09 12.50 -6 5 3 69.89 9.50 -6 5 3 62.79 8.20 5 -5 -3 315.57 27.90 -5 -5 3 358.86 25.80 -5 -5 3 336.37 27.80 5 5 -3 363.76 25.80 -5 5 3 357.66 26.00 -5 5 3 325.07 24.80 -5 5 3 342.97 26.60 5 5 -3 372.16 27.70 -4 -5 3 81.69 11.90 -4 -5 3 115.69 9.90 4 -5 -3 116.59 12.80 4 5 -3 102.39 10.40 -4 5 3 102.69 8.90 -4 5 3 78.29 10.50 -4 5 3 111.49 10.90 4 5 -3 84.69 11.30 3 -5 -3 2682.13 176.08 -3 -5 3 2571.04 176.38 -3 -5 3 2661.93 174.98 3 5 -3 2645.84 175.78 -3 5 3 2684.23 175.68 3 5 -3 2652.93 175.08 -3 5 3 2751.62 174.48 -3 5 3 2675.83 175.38 -2 -5 3 45.00 5.30 2 -5 -3 38.50 5.70 -2 -5 3 56.39 7.00 2 5 -3 56.09 6.20 -2 5 3 40.80 5.80 -2 5 3 37.00 5.60 -2 5 3 47.40 5.00 -2 5 3 42.30 6.10 2 5 -3 42.50 6.10 1 -5 -3 19.10 3.10 -1 -5 3 17.40 3.70 1 -5 -3 17.00 2.80 1 -5 -3 14.00 2.60 1 -5 -3 15.20 3.90 -1 -5 3 11.90 2.70 -1 -5 3 24.30 4.20 1 -5 -3 26.40 4.80 1 5 -3 13.90 3.60 -1 5 3 22.10 3.90 -1 5 3 21.70 3.20 1 5 -3 19.30 3.70 -1 5 3 16.60 2.90 -1 5 3 13.00 3.60 1 5 -3 11.70 3.50 1 5 -3 17.20 2.90 -1 5 3 20.10 4.40 -1 5 3 15.40 2.70 0 -5 3 72.39 7.50 0 -5 3 79.39 6.40 0 -5 -3 64.19 6.50 0 -5 -3 65.79 7.50 0 -5 -3 66.99 5.10 0 -5 3 80.29 5.60 0 5 -3 76.79 5.50 0 5 3 63.39 5.00 0 5 -3 75.69 6.20 0 5 -3 80.99 7.70 0 5 -3 93.29 8.70 0 5 3 80.79 8.40 0 5 3 62.59 5.20 0 5 3 67.89 7.60 0 5 3 65.99 6.10 -1 -5 -3 701.53 49.40 1 -5 3 723.83 47.10 -1 -5 -3 714.43 47.70 1 -5 3 755.82 47.20 1 -5 3 720.13 49.30 -1 -5 -3 738.93 48.40 1 -5 3 718.83 47.40 1 -5 3 707.23 47.40 1 5 3 769.82 49.60 -1 5 -3 722.33 47.10 1 5 3 690.33 47.80 -1 5 -3 721.33 47.40 -1 5 -3 727.53 49.70 2 -5 3 251.57 19.20 -2 -5 -3 255.37 17.60 2 -5 3 236.88 16.00 -2 -5 -3 237.38 18.90 2 -5 3 231.38 16.20 -2 -5 -3 260.27 17.50 2 -5 3 233.48 16.20 2 5 3 244.38 17.80 -2 5 -3 243.48 16.20 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8.60 8 6 -3 36.60 9.60 8 6 -3 34.20 11.30 -8 6 3 61.79 10.40 -8 6 3 39.40 7.20 -8 6 3 34.70 10.00 -7 -6 3 -8.10 5.10 7 -6 -3 3.60 8.00 -7 -6 3 2.90 4.60 -7 6 3 5.90 5.60 -7 6 3 -1.00 3.70 -7 6 3 5.40 6.40 7 6 -3 14.50 7.40 7 6 -3 9.70 6.30 -6 -6 3 -1.30 5.50 6 -6 -3 3.20 6.40 -6 -6 3 1.40 4.00 -6 6 3 0.90 2.60 -6 6 3 7.10 5.30 6 6 -3 0.90 4.30 6 6 -3 3.30 5.30 -6 6 3 4.90 5.80 -5 -6 3 252.57 18.90 5 -6 -3 244.48 21.20 -5 -6 3 204.98 22.40 -5 6 3 220.68 19.70 -5 6 3 226.18 19.20 5 6 -3 256.87 19.30 -5 6 3 239.88 17.80 5 6 -3 225.08 20.30 -4 -6 3 2.50 4.50 4 -6 -3 1.00 4.30 -4 -6 3 -2.20 2.80 -4 6 3 0.20 3.40 -4 6 3 1.50 4.10 -4 6 3 2.30 2.60 4 6 -3 2.70 3.00 4 6 -3 2.60 3.70 3 -6 -3 175.68 14.10 -3 -6 3 120.79 14.40 -3 -6 3 136.29 12.20 -3 6 3 159.48 11.70 3 6 -3 137.29 12.80 3 6 -3 167.28 14.70 -3 6 3 170.28 13.30 -3 6 3 150.88 13.20 2 -6 -3 331.57 24.10 -2 -6 3 405.56 26.30 2 -6 -3 347.77 25.20 2 -6 -3 339.57 25.30 -2 -6 3 379.06 24.70 -2 6 3 328.17 25.00 2 6 -3 429.16 25.80 -2 6 3 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11.70 -7 -15 -4 45.10 15.20 7 -15 4 92.29 17.60 7 15 4 61.69 14.80 -7 15 -4 55.39 14.50 8 -15 4 33.80 15.20 -8 -15 -4 1.10 7.70 -8 -15 -4 7.60 13.40 -8 15 -4 18.10 12.20 8 15 4 9.00 13.00 -7 -16 4 -6.30 6.70 7 -16 -4 0.10 12.00 -7 -16 4 8.10 11.40 -7 16 4 4.50 9.40 7 16 -4 6.40 11.20 7 16 -4 3.60 11.10 -6 -16 4 22.80 6.70 6 -16 -4 8.40 11.40 -6 -16 4 -6.80 9.00 6 16 -4 2.00 8.70 6 16 -4 14.00 10.80 -6 16 4 18.90 10.10 -5 -16 4 52.19 13.90 5 -16 -4 32.20 11.40 -5 -16 4 39.10 7.90 5 16 -4 49.20 11.60 5 16 -4 44.30 11.40 -5 16 4 43.60 12.20 -5 16 4 46.20 12.10 4 -16 -4 154.58 17.90 4 -16 -4 175.28 18.70 4 -16 -4 156.38 13.90 -4 -16 4 185.38 21.80 -4 -16 4 137.49 15.80 -4 16 4 139.19 18.10 4 16 -4 156.18 19.90 -4 16 4 134.39 19.40 4 16 -4 136.29 17.70 -4 16 4 171.58 14.40 3 -16 -4 59.29 10.50 -3 -16 4 30.00 7.60 3 -16 -4 42.00 7.00 -3 -16 4 28.30 10.70 3 -16 -4 37.10 9.80 3 16 -4 32.20 10.30 3 16 -4 62.19 10.80 -3 16 4 46.40 7.30 -3 16 4 50.79 11.60 -3 16 4 54.29 11.90 2 -16 -4 46.20 9.80 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0.70 7.90 -5 16 -4 -11.60 7.30 5 16 4 -1.80 8.10 6 -16 4 1.50 11.40 -6 -16 -4 5.90 5.80 -6 -16 -4 3.00 9.50 6 16 4 1.20 9.40 -6 16 -4 -1.40 9.50 -7 -16 -4 3.90 10.90 7 -16 4 11.70 14.00 -7 -16 -4 8.70 6.70 -7 16 -4 5.30 12.20 7 16 4 3.00 10.40 -7 -17 4 8.50 12.00 -7 -17 4 8.00 7.50 -7 17 4 9.90 11.20 7 17 -4 -3.60 11.00 7 17 -4 6.90 11.20 -6 -17 4 15.40 12.10 -6 -17 4 17.50 8.20 -6 17 4 25.20 12.20 6 17 -4 35.60 12.70 6 17 -4 29.50 11.10 -5 -17 4 43.60 8.90 -5 -17 4 57.59 14.20 5 17 -4 32.20 11.20 -5 17 4 38.90 12.30 5 17 -4 56.19 11.80 4 -17 -4 5.10 8.20 -4 -17 4 23.90 7.00 -4 -17 4 20.80 11.10 -4 17 4 15.10 10.30 4 17 -4 1.10 8.80 -4 17 4 13.20 10.20 4 17 -4 32.50 9.80 -4 17 4 21.40 6.10 3 -17 -4 172.98 19.30 3 -17 -4 154.88 13.90 -3 -17 4 153.88 20.20 -3 -17 4 160.48 16.20 3 17 -4 137.99 19.70 -3 17 4 178.48 21.00 3 17 -4 139.89 17.50 -2 -17 4 1.10 4.80 -2 -17 4 20.70 9.80 2 -17 -4 -0.40 4.00 2 -17 -4 -4.60 6.50 2 17 -4 8.00 6.90 2 17 -4 3.40 7.50 -2 17 4 6.30 7.90 1 -17 -4 32.10 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2 10 6.10 11.00 -9 2 -10 -3.60 6.30 -9 2 -10 1.00 4.40 -10 -2 -10 65.09 12.50 -10 -2 -10 52.19 16.40 -10 -2 -10 55.39 11.30 10 -2 10 72.09 17.90 -10 -2 -10 43.10 15.40 10 -2 10 57.29 17.50 10 2 10 84.49 19.20 -10 2 -10 51.49 16.50 10 2 10 53.59 17.00 -10 -3 10 60.49 16.90 -10 -3 10 56.69 11.00 10 -3 -10 57.69 16.80 10 3 -10 44.30 15.50 -10 3 10 43.10 14.00 -10 3 10 58.49 11.10 -9 -3 10 9.40 10.40 -9 -3 10 11.90 6.70 9 -3 -10 16.60 10.80 9 3 -10 7.50 10.00 -9 3 10 25.30 11.10 -9 3 10 24.10 7.60 -8 -3 10 1.30 4.50 -8 -3 10 4.80 8.90 8 -3 -10 6.50 9.80 8 3 -10 4.40 8.30 -8 3 10 7.60 8.30 -8 3 10 20.50 6.70 -7 -3 10 180.48 18.40 7 -3 -10 171.78 20.70 -7 -3 10 165.98 21.30 7 3 -10 141.09 19.80 -7 3 10 195.78 22.20 -7 3 10 209.78 17.40 -6 -3 10 7.70 6.90 -6 -3 10 0.60 4.40 6 -3 -10 2.20 5.80 -6 3 10 3.50 2.10 6 3 -10 3.20 5.70 6 3 -10 0.70 2.30 -6 3 10 -7.90 4.90 -6 3 10 4.10 3.90 -5 -3 10 22.90 7.90 5 -3 -10 33.50 8.30 5 -3 -10 32.80 4.30 -5 -3 10 38.00 4.30 -5 -3 10 36.40 6.70 -5 3 10 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55.29 8.00 6 4 -10 37.80 9.60 5 -4 -10 12.80 3.90 -5 -4 10 8.00 3.50 -5 -4 10 -3.40 3.20 5 -4 -10 9.80 6.20 -5 -4 10 -0.80 5.80 -5 4 10 6.10 5.80 5 4 -10 6.30 5.10 -5 4 10 14.40 4.60 -5 4 10 14.60 3.20 5 4 -10 8.10 3.20 -4 -4 10 41.90 6.00 4 -4 -10 45.80 7.80 -4 -4 10 44.70 9.40 4 -4 -10 51.59 6.10 -4 -4 10 49.70 7.00 4 4 -10 35.10 8.20 4 4 -10 47.90 5.60 -4 4 10 60.69 5.90 -4 4 10 68.69 10.50 -4 4 10 47.00 7.00 3 -4 -10 195.28 15.50 -3 -4 10 181.48 18.90 3 -4 -10 217.78 16.80 -3 -4 10 194.98 15.90 -3 -4 10 210.48 15.90 3 4 -10 203.98 15.40 3 4 -10 233.78 17.80 -3 4 10 196.58 15.40 -3 4 10 219.98 20.50 -3 4 10 203.88 16.30 -2 -4 10 180.08 16.70 2 -4 -10 163.78 13.50 -2 -4 10 184.98 15.30 -2 -4 10 166.68 13.30 -2 4 10 182.08 17.60 2 4 -10 181.78 13.90 -2 4 10 163.08 13.60 2 4 -10 155.18 15.70 -2 4 10 161.38 13.60 1 -4 -10 49.99 6.30 1 -4 -10 50.59 5.50 -1 -4 10 41.00 7.00 -1 -4 10 40.60 5.40 1 -4 -10 53.59 5.80 1 -4 -10 45.60 7.50 -1 -4 10 42.50 7.20 -1 4 10 44.70 6.00 -1 4 10 42.10 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283.77 20.00 -3 -4 -10 308.37 21.70 3 -4 10 323.17 25.60 -3 -4 -10 337.37 24.20 3 -4 10 294.07 21.10 3 4 10 268.97 24.10 -3 4 -10 291.67 20.10 -3 4 -10 289.77 21.10 -3 4 -10 307.87 25.10 3 4 10 333.37 23.30 -3 4 -10 279.57 21.20 -3 4 -10 267.27 20.00 4 -4 10 179.28 18.60 4 -4 10 165.08 18.70 -4 -4 -10 131.49 15.70 -4 -4 -10 134.79 12.40 -4 4 -10 138.29 12.30 4 4 10 131.59 15.20 -4 4 -10 151.18 11.10 -4 4 -10 165.38 18.40 4 4 10 161.68 17.80 5 -4 10 4.40 6.30 5 -4 10 -3.20 5.80 -5 -4 -10 4.70 3.30 -5 -4 -10 1.40 5.20 -5 4 -10 10.30 7.20 5 4 10 1.30 6.30 -5 4 -10 0.40 2.20 -5 4 -10 0.50 4.40 5 4 10 -5.30 5.60 -6 -4 -10 0.70 4.00 -6 -4 -10 7.20 6.70 6 -4 10 2.50 7.20 6 -4 10 4.60 7.60 -6 4 -10 -1.70 2.90 -6 4 -10 -1.50 5.00 6 4 10 1.10 8.00 6 4 10 -3.20 6.40 -6 4 -10 -2.60 6.50 -7 -4 -10 31.20 10.70 7 -4 10 67.39 13.30 7 -4 10 34.10 11.90 -7 -4 -10 41.70 7.90 7 4 10 48.70 12.60 -7 4 -10 56.19 7.00 -7 4 -10 33.50 9.10 -7 4 -10 36.40 11.30 7 4 10 19.40 10.00 -8 -4 -10 -0.40 5.00 8 -4 10 5.80 10.70 8 -4 10 -2.40 8.30 -8 -4 -10 5.80 5.70 -8 -4 -10 8.30 8.60 -8 -4 -10 -6.80 7.30 -8 4 -10 17.10 9.00 8 4 10 12.70 10.10 -8 4 -10 9.30 10.00 8 4 10 18.00 10.80 -8 4 -10 7.50 4.50 -9 -4 -10 267.17 30.10 9 -4 10 256.27 31.60 9 -4 10 286.27 32.90 -9 -4 -10 288.27 25.60 -9 -4 -10 290.27 31.80 -9 -4 -10 290.37 24.50 9 4 10 301.17 33.30 -9 4 -10 261.27 31.40 9 4 10 266.27 31.40 10 -4 10 -0.10 12.70 10 -4 10 -14.10 10.90 -10 -4 -10 -7.50 7.00 -10 -4 -10 -17.10 10.90 -10 -4 -10 -13.40 6.70 -10 -4 -10 4.80 10.80 10 4 10 -14.20 11.80 -10 4 -10 -0.70 12.10 10 4 10 4.70 11.80 -10 -5 10 24.20 9.70 10 -5 -10 18.80 14.40 -10 -5 10 33.90 14.40 -10 5 10 34.90 9.30 -10 5 10 28.90 13.20 10 5 -10 47.50 14.70 -9 -5 10 23.40 7.80 -9 -5 10 41.90 13.80 9 -5 -10 23.20 12.50 9 5 -10 30.60 11.00 -9 5 10 27.10 7.60 -9 5 10 26.10 11.90 8 -5 -10 2.20 9.40 -8 -5 10 -0.50 5.40 -8 -5 10 7.80 8.40 -8 5 10 5.40 9.80 -8 5 10 10.10 5.60 8 5 -10 -1.70 7.40 -7 -5 10 3.70 5.10 -7 -5 10 11.10 8.40 7 -5 -10 -4.70 7.00 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