data_shelx _audit_update_record ; 2014-10-27 # Formatted by publCIF ; _audit_creation_method SHELXL-97 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'Al8 Ce Co2' _chemical_formula_sum 'Al8 Ce Co2' _chemical_formula_weight 473.82 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'Ce' 'Ce' -0.2486 2.6331 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Co' 'Co' 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Al' 'Al' 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting Orthorhombic _symmetry_space_group_name_H-M 'Pbam' _symmetry_space_group_name_Hall '-P 2 2ab' loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'x+1/2, -y+1/2, -z' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x, y, -z' '-x-1/2, y-1/2, z' 'x-1/2, -y-1/2, z' _cell_length_a 12.4720(10) _cell_length_b 14.3870(15) _cell_length_c 4.022(3) _cell_angle_alpha 90.00 _cell_angle_beta 90.00 _cell_angle_gamma 90.00 _cell_volume 721.7(5) _cell_formula_units_Z 4 _cell_measurement_temperature 293(2) _cell_measurement_reflns_used ? _cell_measurement_theta_min ? _cell_measurement_theta_max ? _exptl_crystal_description Fragment _exptl_crystal_colour 'silver' _exptl_crystal_size_max 0.04 _exptl_crystal_size_mid 0.03 _exptl_crystal_size_min 0.03 _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 4.361 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 864 _exptl_absorpt_coefficient_mu 11.613 _exptl_absorpt_correction_type 'Multi-scan' _exptl_absorpt_correction_T_min 0.665 _exptl_absorpt_correction_T_max 0.706 _exptl_absorpt_process_details 'HKL scalepack (Otwinski & Minor, 1997)' _exptl_special_details ; ? ; _diffrn_ambient_temperature 293(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'Nonius Kappa CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean ? _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? _diffrn_reflns_number 2190 _diffrn_reflns_av_R_equivalents 0.0243 _diffrn_reflns_av_sigmaI/netI 0.0289 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_h_max 17 _diffrn_reflns_limit_k_min -20 _diffrn_reflns_limit_k_max 20 _diffrn_reflns_limit_l_min -5 _diffrn_reflns_limit_l_max 5 _diffrn_reflns_theta_min 3.27 _diffrn_reflns_theta_max 31.01 _reflns_number_total 1296 _reflns_number_gt 1141 _reflns_threshold_expression >2sigma(I) _computing_data_collection 'Collect (Nonius 1999)' _computing_cell_refinement 'Denzo and Scalepack (Otwinski & Minor 1997)' _computing_data_reduction 'Denzo and Scalepack (Otwinski & Minor 1997)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics 'Crystal Maker' _computing_publication_material 'Publcif' _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0243P)^2^+3.6274P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens ? _refine_ls_hydrogen_treatment ? _refine_ls_extinction_method SHELXL _refine_ls_extinction_coef 0.0048(2) _refine_ls_extinction_expression 'Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^' _refine_ls_number_reflns 1296 _refine_ls_number_parameters 70 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0314 _refine_ls_R_factor_gt 0.0255 _refine_ls_wR_factor_ref 0.0592 _refine_ls_wR_factor_gt 0.0560 _refine_ls_goodness_of_fit_ref 0.988 _refine_ls_restrained_S_all 0.988 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Ce1 Ce 0.340381(19) 0.318394(17) 0.0000 0.00852(9) Uani 1 2 d S . . Co2 Co 0.15166(4) 0.09648(4) 0.0000 0.00580(13) Uani 1 2 d S . . Co1 Co 0.03488(5) 0.40562(4) 0.0000 0.00709(13) Uani 1 2 d S . . Al8 Al 0.0000 0.5000 0.5000 0.0078(4) Uani 1 4 d S . . Al9 Al 0.0000 0.0000 0.0000 0.0084(4) Uani 1 4 d S . . Al2 Al 0.15953(10) 0.37925(9) 0.5000 0.0077(3) Uani 1 2 d S . . Al5 Al 0.45285(11) 0.17947(9) 0.5000 0.0071(3) Uani 1 2 d S . . Al3 Al 0.23624(11) 0.17249(9) 0.5000 0.0079(3) Uani 1 2 d S . . Al4 Al 0.33140(11) 0.49140(9) 0.5000 0.0082(3) Uani 1 2 d S . . Al1 Al 0.02558(11) 0.13180(9) 0.5000 0.0076(3) Uani 1 2 d S . . Al7 Al 0.33993(10) 0.04452(9) 0.0000 0.0098(3) Uani 1 2 d S . . Al6 Al 0.09585(10) 0.25276(8) 0.0000 0.0080(3) Uani 1 2 d S . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ce1 0.00831(14) 0.01134(13) 0.00592(14) 0.000 0.000 -0.00099(8) Co2 0.0065(3) 0.0057(2) 0.0051(3) 0.000 0.000 -0.00008(19) Co1 0.0083(3) 0.0070(2) 0.0060(3) 0.000 0.000 0.0006(2) Al8 0.0110(8) 0.0060(7) 0.0064(9) 0.000 0.000 0.0008(6) Al9 0.0080(8) 0.0082(8) 0.0090(9) 0.000 0.000 -0.0007(6) Al2 0.0068(6) 0.0087(6) 0.0075(7) 0.000 0.000 0.0005(4) Al5 0.0059(6) 0.0079(5) 0.0077(7) 0.000 0.000 0.0006(4) Al3 0.0067(6) 0.0097(6) 0.0071(7) 0.000 0.000 -0.0017(4) Al4 0.0096(6) 0.0073(5) 0.0075(6) 0.000 0.000 -0.0018(4) Al1 0.0081(6) 0.0085(5) 0.0062(6) 0.000 0.000 0.0005(5) Al7 0.0073(6) 0.0129(6) 0.0092(7) 0.000 0.000 0.0023(5) Al6 0.0095(6) 0.0064(5) 0.0080(6) 0.000 0.000 0.0006(4) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ce1 Al1 3.1452(13) 3_556 ? Ce1 Al1 3.1452(13) 3 ? Ce1 Al2 3.1461(13) 1_554 ? Ce1 Al2 3.1461(13) . ? Ce1 Al5 3.1633(13) . ? Ce1 Al5 3.1634(13) 1_554 ? Ce1 Al3 3.1840(13) . ? Ce1 Al3 3.1840(13) 1_554 ? Ce1 Al6 3.1927(13) . ? Ce1 Al4 3.2018(13) 1_554 ? Ce1 Al4 3.2018(13) . ? Ce1 Al9 3.285(2) 3 ? Co2 Al9 2.3461(6) . ? Co2 Al6 2.3537(14) . ? Co2 Al7 2.4643(14) . ? Co2 Al3 2.5204(13) 1_554 ? Co2 Al3 2.5205(13) . ? Co2 Al4 2.5248(13) 7_654 ? Co2 Al4 2.5248(13) 7_655 ? Co2 Al1 2.6029(13) . ? Co2 Al1 2.6029(13) 1_554 ? Co1 Al6 2.3269(14) . ? Co1 Al8 2.4652(11) . ? Co1 Al8 2.4652(11) 1_554 ? Co1 Al7 2.5360(15) 7_665 ? Co1 Al7 2.5350(14) 3_455 ? Co1 Al5 2.5669(13) 3_455 ? Co1 Al5 2.5669(13) 3_456 ? Co1 Al2 2.5700(13) . ? Co1 Al2 2.5700(13) 1_554 ? Co1 Co1 2.8517(11) 5_565 ? Al8 Co1 2.4652(11) 5_566 ? Al8 Co1 2.4652(11) 5_565 ? Al8 Co1 2.4652(11) 1_556 ? Al8 Al2 2.6414(13) 5_566 ? Al8 Al2 2.6414(13) . ? Al8 Al5 2.6481(13) 7_665 ? Al8 Al5 2.6481(13) 3_456 ? Al8 Al7 2.9051(13) 7_666 ? Al8 Al7 2.9051(13) 3_455 ? Al8 Al7 2.9051(13) 3_456 ? Al8 Al7 2.9051(13) 7_665 ? Al9 Co2 2.3462(6) 5 ? Al9 Al1 2.7823(13) . ? Al9 Al1 2.7823(13) 5 ? Al9 Al1 2.7823(13) 5_556 ? Al9 Al1 2.7823(13) 1_554 ? Al9 Al4 2.9123(13) 3_455 ? Al9 Al4 2.9123(13) 7_655 ? Al9 Al4 2.9123(13) 3_456 ? Al9 Al4 2.9123(13) 7_654 ? Al9 Ce1 3.285(2) 3_455 ? Al9 Ce1 3.285(2) 7_655 ? Al2 Co1 2.5700(13) 1_556 ? Al2 Al4 2.6829(19) . ? Al2 Al5 2.7125(18) 3_456 ? Al2 Al6 2.8261(16) . ? Al2 Al6 2.8261(16) 1_556 ? Al2 Ce1 3.1462(13) 1_556 ? Al5 Co1 2.5670(13) 3 ? Al5 Co1 2.5670(13) 3_556 ? Al5 Al8 2.6482(13) 3_556 ? Al5 Al3 2.703(2) . ? Al5 Al2 2.7126(18) 3_556 ? Al5 Al6 2.8592(16) 3_556 ? Al5 Al6 2.8592(16) 3 ? Al5 Al1 2.8627(18) 3_556 ? Al5 Ce1 3.1633(13) 1_556 ? Al3 Co2 2.5205(13) 1_556 ? Al3 Al1 2.6918(19) . ? Al3 Al4 2.7385(19) 7_655 ? Al3 Al6 2.9058(16) . ? Al3 Al6 2.9058(16) 1_556 ? Al3 Ce1 3.1840(13) 1_556 ? Al4 Co2 2.5248(13) 7_666 ? Al4 Co2 2.5248(13) 7_665 ? Al4 Al1 2.6949(19) 7_665 ? Al4 Al3 2.7385(19) 7_665 ? Al4 Al9 2.9123(13) 3_556 ? Al4 Al9 2.9122(13) 3 ? Al4 Ce1 3.2019(13) 1_556 ? Al1 Co2 2.6029(13) 1_556 ? Al1 Al4 2.6948(18) 7_655 ? Al1 Al9 2.7823(13) 1_556 ? Al1 Al6 2.8001(15) 1_556 ? Al1 Al6 2.8001(15) . ? Al1 Al5 2.8628(18) 3_456 ? Al1 Ce1 3.1453(13) 3_455 ? Al1 Ce1 3.1453(13) 3_456 ? Al7 Co1 2.5360(15) 7_655 ? Al7 Co1 2.5350(14) 3 ? Al7 Al8 2.9051(13) 3_556 ? Al7 Al8 2.9051(13) 3 ? Al6 Al1 2.8001(15) 1_554 ? Al6 Al2 2.8261(16) 1_554 ? Al6 Al5 2.8592(16) 3_455 ? Al6 Al5 2.8592(16) 3_456 ? Al6 Al3 2.9058(16) 1_554 ? Al6 Ce1 3.3465(13) 3_455 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Al1 Ce1 Al1 79.49(5) 3_556 3 ? Al1 Ce1 Al2 150.67(4) 3_556 1_554 ? Al1 Ce1 Al2 93.12(4) 3 1_554 ? Al1 Ce1 Al2 93.12(4) 3_556 . ? Al1 Ce1 Al2 150.67(4) 3 . ? Al2 Ce1 Al2 79.46(5) 1_554 . ? Al1 Ce1 Al5 53.97(4) 3_556 . ? Al1 Ce1 Al5 102.99(4) 3 . ? Al2 Ce1 Al5 154.17(4) 1_554 . ? Al2 Ce1 Al5 95.01(4) . . ? Al1 Ce1 Al5 102.99(4) 3_556 1_554 ? Al1 Ce1 Al5 53.97(3) 3 1_554 ? Al2 Ce1 Al5 95.01(4) 1_554 1_554 ? Al2 Ce1 Al5 154.17(4) . 1_554 ? Al5 Ce1 Al5 78.95(5) . 1_554 ? Al1 Ce1 Al3 92.63(4) 3_556 . ? Al1 Ce1 Al3 148.61(4) 3 . ? Al2 Ce1 Al3 107.14(4) 1_554 . ? Al2 Ce1 Al3 59.16(4) . . ? Al5 Ce1 Al3 50.42(4) . . ? Al5 Ce1 Al3 99.55(4) 1_554 . ? Al1 Ce1 Al3 148.61(4) 3_556 1_554 ? Al1 Ce1 Al3 92.63(4) 3 1_554 ? Al2 Ce1 Al3 59.16(4) 1_554 1_554 ? Al2 Ce1 Al3 107.14(4) . 1_554 ? Al5 Ce1 Al3 99.55(4) . 1_554 ? Al5 Ce1 Al3 50.42(4) 1_554 1_554 ? Al3 Ce1 Al3 78.34(5) . 1_554 ? Al1 Ce1 Al6 140.25(2) 3_556 . ? Al1 Ce1 Al6 140.25(2) 3 . ? Al2 Ce1 Al6 52.95(3) 1_554 . ? Al2 Ce1 Al6 52.95(3) . . ? Al5 Ce1 Al6 103.69(3) . . ? Al5 Ce1 Al6 103.69(3) 1_554 . ? Al3 Ce1 Al6 54.22(3) . . ? Al3 Ce1 Al6 54.22(3) 1_554 . ? Al1 Ce1 Al4 104.49(4) 3_556 1_554 ? Al1 Ce1 Al4 56.43(4) 3 1_554 ? Al2 Ce1 Al4 49.99(4) 1_554 1_554 ? Al2 Ce1 Al4 99.21(4) . 1_554 ? Al5 Ce1 Al4 154.95(4) . 1_554 ? Al5 Ce1 Al4 96.17(4) 1_554 1_554 ? Al3 Ce1 Al4 153.50(3) . 1_554 ? Al3 Ce1 Al4 95.83(4) 1_554 1_554 ? Al6 Ce1 Al4 101.33(3) . 1_554 ? Al1 Ce1 Al4 56.43(4) 3_556 . ? Al1 Ce1 Al4 104.49(4) 3 . ? Al2 Ce1 Al4 99.21(4) 1_554 . ? Al2 Ce1 Al4 49.99(4) . . ? Al5 Ce1 Al4 96.16(4) . . ? Al5 Ce1 Al4 154.95(3) 1_554 . ? Al3 Ce1 Al4 95.83(4) . . ? Al3 Ce1 Al4 153.50(3) 1_554 . ? Al6 Ce1 Al4 101.33(3) . . ? Al4 Ce1 Al4 77.82(5) 1_554 . ? Al1 Ce1 Al9 51.22(2) 3_556 3 ? Al1 Ce1 Al9 51.22(2) 3 3 ? Al2 Ce1 Al9 102.31(3) 1_554 3 ? Al2 Ce1 Al9 102.31(3) . 3 ? Al5 Ce1 Al9 103.52(2) . 3 ? Al5 Ce1 Al9 103.52(2) 1_554 3 ? Al3 Ce1 Al9 140.50(2) . 3 ? Al3 Ce1 Al9 140.50(2) 1_554 3 ? Al6 Ce1 Al9 144.51(2) . 3 ? Al4 Ce1 Al9 53.34(2) 1_554 3 ? Al4 Ce1 Al9 53.34(2) . 3 ? Al9 Co2 Al6 109.07(4) . . ? Al9 Co2 Al7 126.07(4) . . ? Al6 Co2 Al7 124.86(5) . . ? Al9 Co2 Al3 126.45(3) . 1_554 ? Al6 Co2 Al3 73.10(4) . 1_554 ? Al7 Co2 Al3 74.50(4) . 1_554 ? Al9 Co2 Al3 126.45(3) . . ? Al6 Co2 Al3 73.10(4) . . ? Al7 Co2 Al3 74.50(4) . . ? Al3 Co2 Al3 105.85(6) 1_554 . ? Al9 Co2 Al4 73.33(3) . 7_654 ? Al6 Co2 Al4 126.64(3) . 7_654 ? Al7 Co2 Al4 74.85(4) . 7_654 ? Al3 Co2 Al4 65.75(5) 1_554 7_654 ? Al3 Co2 Al4 149.35(5) . 7_654 ? Al9 Co2 Al4 73.33(3) . 7_655 ? Al6 Co2 Al4 126.64(3) . 7_655 ? Al7 Co2 Al4 74.85(4) . 7_655 ? Al3 Co2 Al4 149.35(5) 1_554 7_655 ? Al3 Co2 Al4 65.75(5) . 7_655 ? Al4 Co2 Al4 105.60(6) 7_654 7_655 ? Al9 Co2 Al1 68.19(3) . . ? Al6 Co2 Al1 68.58(4) . . ? Al7 Co2 Al1 129.41(3) . . ? Al3 Co2 Al1 141.68(5) 1_554 . ? Al3 Co2 Al1 63.37(5) . . ? Al4 Co2 Al1 141.52(5) 7_654 . ? Al4 Co2 Al1 63.39(5) 7_655 . ? Al9 Co2 Al1 68.19(3) . 1_554 ? Al6 Co2 Al1 68.58(4) . 1_554 ? Al7 Co2 Al1 129.41(3) . 1_554 ? Al3 Co2 Al1 63.37(5) 1_554 1_554 ? Al3 Co2 Al1 141.68(5) . 1_554 ? Al4 Co2 Al1 63.39(5) 7_654 1_554 ? Al4 Co2 Al1 141.52(5) 7_655 1_554 ? Al1 Co2 Al1 101.18(6) . 1_554 ? Al6 Co1 Al8 125.33(2) . . ? Al6 Co1 Al8 125.33(2) . 1_554 ? Al8 Co1 Al8 109.32(4) . 1_554 ? Al6 Co1 Al7 122.92(5) . 7_665 ? Al8 Co1 Al7 71.01(2) . 7_665 ? Al8 Co1 Al7 71.01(2) 1_554 7_665 ? Al6 Co1 Al7 125.51(5) . 3_455 ? Al8 Co1 Al7 71.03(2) . 3_455 ? Al8 Co1 Al7 71.03(2) 1_554 3_455 ? Al7 Co1 Al7 111.56(4) 7_665 3_455 ? Al6 Co1 Al5 71.31(4) . 3_455 ? Al8 Co1 Al5 146.25(4) . 3_455 ? Al8 Co1 Al5 63.47(4) 1_554 3_455 ? Al7 Co1 Al5 128.40(3) 7_665 3_455 ? Al7 Co1 Al5 75.68(4) 3_455 3_455 ? Al6 Co1 Al5 71.31(4) . 3_456 ? Al8 Co1 Al5 63.47(4) . 3_456 ? Al8 Co1 Al5 146.25(4) 1_554 3_456 ? Al7 Co1 Al5 128.40(3) 7_665 3_456 ? Al7 Co1 Al5 75.68(4) 3_455 3_456 ? Al5 Co1 Al5 103.15(6) 3_455 3_456 ? Al6 Co1 Al2 70.29(4) . . ? Al8 Co1 Al2 63.24(4) . . ? Al8 Co1 Al2 145.73(4) 1_554 . ? Al7 Co1 Al2 75.16(4) 7_665 . ? Al7 Co1 Al2 128.46(3) 3_455 . ? Al5 Co1 Al2 141.60(5) 3_455 . ? Al5 Co1 Al2 63.75(5) 3_456 . ? Al6 Co1 Al2 70.29(4) . 1_554 ? Al8 Co1 Al2 145.73(4) . 1_554 ? Al8 Co1 Al2 63.24(4) 1_554 1_554 ? Al7 Co1 Al2 75.16(4) 7_665 1_554 ? Al7 Co1 Al2 128.46(3) 3_455 1_554 ? Al5 Co1 Al2 63.75(5) 3_455 1_554 ? Al5 Co1 Al2 141.60(5) 3_456 1_554 ? Al2 Co1 Al2 102.98(6) . 1_554 ? Al6 Co1 Co1 178.69(5) . 5_565 ? Al8 Co1 Co1 54.66(2) . 5_565 ? Al8 Co1 Co1 54.66(2) 1_554 5_565 ? Al7 Co1 Co1 55.77(4) 7_665 5_565 ? Al7 Co1 Co1 55.80(4) 3_455 5_565 ? Al5 Co1 Co1 109.42(3) 3_455 5_565 ? Al5 Co1 Co1 109.42(3) 3_456 5_565 ? Al2 Co1 Co1 108.97(4) . 5_565 ? Al2 Co1 Co1 108.97(4) 1_554 5_565 ? Co1 Al8 Co1 109.33(4) 5_566 5_565 ? Co1 Al8 Co1 70.67(4) 5_566 1_556 ? Co1 Al8 Co1 180.00(2) 5_565 1_556 ? Co1 Al8 Co1 180.0 5_566 . ? Co1 Al8 Co1 70.68(4) 5_565 . ? Co1 Al8 Co1 109.32(4) 1_556 . ? Co1 Al8 Al2 60.32(2) 5_566 5_566 ? Co1 Al8 Al2 60.32(2) 5_565 5_566 ? Co1 Al8 Al2 119.68(2) 1_556 5_566 ? Co1 Al8 Al2 119.68(2) . 5_566 ? Co1 Al8 Al2 119.68(2) 5_566 . ? Co1 Al8 Al2 119.68(2) 5_565 . ? Co1 Al8 Al2 60.32(2) 1_556 . ? Co1 Al8 Al2 60.32(2) . . ? Al2 Al8 Al2 180.0 5_566 . ? Co1 Al8 Al5 60.14(2) 5_566 7_665 ? Co1 Al8 Al5 60.14(2) 5_565 7_665 ? Co1 Al8 Al5 119.86(2) 1_556 7_665 ? Co1 Al8 Al5 119.86(2) . 7_665 ? Al2 Al8 Al5 61.70(4) 5_566 7_665 ? Al2 Al8 Al5 118.30(4) . 7_665 ? Co1 Al8 Al5 119.86(2) 5_566 3_456 ? Co1 Al8 Al5 119.86(2) 5_565 3_456 ? Co1 Al8 Al5 60.14(2) 1_556 3_456 ? Co1 Al8 Al5 60.14(2) . 3_456 ? Al2 Al8 Al5 118.30(4) 5_566 3_456 ? Al2 Al8 Al5 61.70(4) . 3_456 ? Al5 Al8 Al5 180.0 7_665 3_456 ? Co1 Al8 Al7 55.61(3) 5_566 7_666 ? Co1 Al8 Al7 124.37(3) 5_565 7_666 ? Co1 Al8 Al7 55.63(3) 1_556 7_666 ? Co1 Al8 Al7 124.39(3) . 7_666 ? Al2 Al8 Al7 111.88(3) 5_566 7_666 ? Al2 Al8 Al7 68.12(3) . 7_666 ? Al5 Al8 Al7 68.44(3) 7_665 7_666 ? Al5 Al8 Al7 111.56(3) 3_456 7_666 ? Co1 Al8 Al7 124.39(3) 5_566 3_455 ? Co1 Al8 Al7 55.63(3) 5_565 3_455 ? Co1 Al8 Al7 124.37(3) 1_556 3_455 ? Co1 Al8 Al7 55.61(3) . 3_455 ? Al2 Al8 Al7 68.12(3) 5_566 3_455 ? Al2 Al8 Al7 111.88(3) . 3_455 ? Al5 Al8 Al7 111.56(3) 7_665 3_455 ? Al5 Al8 Al7 68.44(3) 3_456 3_455 ? Al7 Al8 Al7 180.0 7_666 3_455 ? Co1 Al8 Al7 55.63(3) 5_566 3_456 ? Co1 Al8 Al7 124.39(3) 5_565 3_456 ? Co1 Al8 Al7 55.61(3) 1_556 3_456 ? Co1 Al8 Al7 124.37(3) . 3_456 ? Al2 Al8 Al7 68.12(3) 5_566 3_456 ? Al2 Al8 Al7 111.88(3) . 3_456 ? Al5 Al8 Al7 111.56(3) 7_665 3_456 ? Al5 Al8 Al7 68.44(3) 3_456 3_456 ? Al7 Al8 Al7 92.39(5) 7_666 3_456 ? Al7 Al8 Al7 87.61(5) 3_455 3_456 ? Co1 Al8 Al7 124.37(3) 5_566 7_665 ? Co1 Al8 Al7 55.61(3) 5_565 7_665 ? Co1 Al8 Al7 124.39(3) 1_556 7_665 ? Co1 Al8 Al7 55.63(3) . 7_665 ? Al2 Al8 Al7 111.88(3) 5_566 7_665 ? Al2 Al8 Al7 68.12(3) . 7_665 ? Al5 Al8 Al7 68.44(3) 7_665 7_665 ? Al5 Al8 Al7 111.56(3) 3_456 7_665 ? Al7 Al8 Al7 87.61(5) 7_666 7_665 ? Al7 Al8 Al7 92.39(5) 3_455 7_665 ? Al7 Al8 Al7 180.0 3_456 7_665 ? Co2 Al9 Co2 180.0 . 5 ? Co2 Al9 Al1 60.29(3) . . ? Co2 Al9 Al1 119.71(3) 5 . ? Co2 Al9 Al1 119.71(3) . 5 ? Co2 Al9 Al1 60.29(3) 5 5 ? Al1 Al9 Al1 180.0 . 5 ? Co2 Al9 Al1 119.71(3) . 5_556 ? Co2 Al9 Al1 60.29(3) 5 5_556 ? Al1 Al9 Al1 87.43(5) . 5_556 ? Al1 Al9 Al1 92.57(5) 5 5_556 ? Co2 Al9 Al1 60.29(3) . 1_554 ? Co2 Al9 Al1 119.71(3) 5 1_554 ? Al1 Al9 Al1 92.57(5) . 1_554 ? Al1 Al9 Al1 87.43(5) 5 1_554 ? Al1 Al9 Al1 180.00(7) 5_556 1_554 ? Co2 Al9 Al4 123.85(3) . 3_455 ? Co2 Al9 Al4 56.15(3) 5 3_455 ? Al1 Al9 Al4 123.57(4) . 3_455 ? Al1 Al9 Al4 56.43(4) 5 3_455 ? Al1 Al9 Al4 116.44(4) 5_556 3_455 ? Al1 Al9 Al4 63.56(4) 1_554 3_455 ? Co2 Al9 Al4 56.15(3) . 7_655 ? Co2 Al9 Al4 123.85(3) 5 7_655 ? Al1 Al9 Al4 56.43(4) . 7_655 ? Al1 Al9 Al4 123.57(4) 5 7_655 ? Al1 Al9 Al4 63.56(4) 5_556 7_655 ? Al1 Al9 Al4 116.44(4) 1_554 7_655 ? Al4 Al9 Al4 180.00(5) 3_455 7_655 ? Co2 Al9 Al4 123.85(3) . 3_456 ? Co2 Al9 Al4 56.15(3) 5 3_456 ? Al1 Al9 Al4 63.56(4) . 3_456 ? Al1 Al9 Al4 116.44(4) 5 3_456 ? Al1 Al9 Al4 56.43(4) 5_556 3_456 ? Al1 Al9 Al4 123.57(4) 1_554 3_456 ? Al4 Al9 Al4 87.34(5) 3_455 3_456 ? Al4 Al9 Al4 92.66(5) 7_655 3_456 ? Co2 Al9 Al4 56.15(3) . 7_654 ? Co2 Al9 Al4 123.85(3) 5 7_654 ? Al1 Al9 Al4 116.44(4) . 7_654 ? Al1 Al9 Al4 63.56(4) 5 7_654 ? Al1 Al9 Al4 123.57(4) 5_556 7_654 ? Al1 Al9 Al4 56.43(4) 1_554 7_654 ? Al4 Al9 Al4 92.66(5) 3_455 7_654 ? Al4 Al9 Al4 87.34(5) 7_655 7_654 ? Al4 Al9 Al4 180.00(4) 3_456 7_654 ? Co2 Al9 Ce1 91.031(16) . 3_455 ? Co2 Al9 Ce1 88.969(16) 5 3_455 ? Al1 Al9 Ce1 61.80(3) . 3_455 ? Al1 Al9 Ce1 118.20(3) 5 3_455 ? Al1 Al9 Ce1 118.20(3) 5_556 3_455 ? Al1 Al9 Ce1 61.80(3) 1_554 3_455 ? Al4 Al9 Ce1 61.87(3) 3_455 3_455 ? Al4 Al9 Ce1 118.13(3) 7_655 3_455 ? Al4 Al9 Ce1 61.87(3) 3_456 3_455 ? Al4 Al9 Ce1 118.13(3) 7_654 3_455 ? Co2 Al9 Ce1 88.969(16) . 7_655 ? Co2 Al9 Ce1 91.031(16) 5 7_655 ? Al1 Al9 Ce1 118.20(3) . 7_655 ? Al1 Al9 Ce1 61.80(3) 5 7_655 ? Al1 Al9 Ce1 61.80(3) 5_556 7_655 ? Al1 Al9 Ce1 118.20(3) 1_554 7_655 ? Al4 Al9 Ce1 118.13(3) 3_455 7_655 ? Al4 Al9 Ce1 61.87(3) 7_655 7_655 ? Al4 Al9 Ce1 118.13(3) 3_456 7_655 ? Al4 Al9 Ce1 61.87(3) 7_654 7_655 ? Ce1 Al9 Ce1 180.000(7) 3_455 7_655 ? Co1 Al2 Co1 102.98(6) . 1_556 ? Co1 Al2 Al8 56.44(3) . . ? Co1 Al2 Al8 56.44(3) 1_556 . ? Co1 Al2 Al4 113.24(4) . . ? Co1 Al2 Al4 113.24(4) 1_556 . ? Al8 Al2 Al4 101.90(5) . . ? Co1 Al2 Al5 58.07(3) . 3_456 ? Co1 Al2 Al5 58.07(3) 1_556 3_456 ? Al8 Al2 Al5 59.27(4) . 3_456 ? Al4 Al2 Al5 161.18(7) . 3_456 ? Co1 Al2 Al6 50.82(3) . . ? Co1 Al2 Al6 118.81(6) 1_556 . ? Al8 Al2 Al6 102.23(4) . . ? Al4 Al2 Al6 127.72(4) . . ? Al5 Al2 Al6 62.12(4) 3_456 . ? Co1 Al2 Al6 118.81(6) . 1_556 ? Co1 Al2 Al6 50.82(3) 1_556 1_556 ? Al8 Al2 Al6 102.23(4) . 1_556 ? Al4 Al2 Al6 127.72(4) . 1_556 ? Al5 Al2 Al6 62.12(4) 3_456 1_556 ? Al6 Al2 Al6 90.73(6) . 1_556 ? Co1 Al2 Ce1 88.54(4) . . ? Co1 Al2 Ce1 167.14(4) 1_556 . ? Al8 Al2 Ce1 136.31(3) . . ? Al4 Al2 Ce1 66.08(3) . . ? Al5 Al2 Ce1 126.49(4) 3_456 . ? Al6 Al2 Ce1 64.37(4) . . ? Al6 Al2 Ce1 118.50(5) 1_556 . ? Co1 Al2 Ce1 167.14(4) . 1_556 ? Co1 Al2 Ce1 88.55(4) 1_556 1_556 ? Al8 Al2 Ce1 136.31(3) . 1_556 ? Al4 Al2 Ce1 66.08(3) . 1_556 ? Al5 Al2 Ce1 126.49(4) 3_456 1_556 ? Al6 Al2 Ce1 118.50(5) . 1_556 ? Al6 Al2 Ce1 64.37(4) 1_556 1_556 ? Ce1 Al2 Ce1 79.46(5) . 1_556 ? Co1 Al5 Co1 103.15(6) 3 3_556 ? Co1 Al5 Al8 56.39(3) 3 3_556 ? Co1 Al5 Al8 56.39(3) 3_556 3_556 ? Co1 Al5 Al3 112.37(4) 3 . ? Co1 Al5 Al3 112.37(4) 3_556 . ? Al8 Al5 Al3 100.70(5) 3_556 . ? Co1 Al5 Al2 58.18(3) 3 3_556 ? Co1 Al5 Al2 58.18(3) 3_556 3_556 ? Al8 Al5 Al2 59.02(4) 3_556 3_556 ? Al3 Al5 Al2 159.72(6) . 3_556 ? Co1 Al5 Al6 117.71(6) 3 3_556 ? Co1 Al5 Al6 50.44(3) 3_556 3_556 ? Al8 Al5 Al6 101.19(4) 3_556 3_556 ? Al3 Al5 Al6 129.49(4) . 3_556 ? Al2 Al5 Al6 60.89(4) 3_556 3_556 ? Co1 Al5 Al6 50.44(3) 3 3 ? Co1 Al5 Al6 117.71(6) 3_556 3 ? Al8 Al5 Al6 101.19(4) 3_556 3 ? Al3 Al5 Al6 129.49(4) . 3 ? Al2 Al5 Al6 60.89(4) 3_556 3 ? Al6 Al5 Al6 89.39(6) 3_556 3 ? Co1 Al5 Al1 109.03(4) 3 3_556 ? Co1 Al5 Al1 109.03(4) 3_556 3_556 ? Al8 Al5 Al1 148.70(6) 3_556 3_556 ? Al3 Al5 Al1 110.60(6) . 3_556 ? Al2 Al5 Al1 89.68(5) 3_556 3_556 ? Al6 Al5 Al1 58.60(4) 3_556 3_556 ? Al6 Al5 Al1 58.60(4) 3 3_556 ? Co1 Al5 Ce1 167.45(4) 3 1_556 ? Co1 Al5 Ce1 88.85(4) 3_556 1_556 ? Al8 Al5 Ce1 135.60(3) 3_556 1_556 ? Al3 Al5 Ce1 65.19(3) . 1_556 ? Al2 Al5 Ce1 128.18(4) 3_556 1_556 ? Al6 Al5 Ce1 67.29(4) 3_556 1_556 ? Al6 Al5 Ce1 120.55(5) 3 1_556 ? Al1 Al5 Ce1 62.69(3) 3_556 1_556 ? Co1 Al5 Ce1 88.85(4) 3 . ? Co1 Al5 Ce1 167.44(4) 3_556 . ? Al8 Al5 Ce1 135.60(3) 3_556 . ? Al3 Al5 Ce1 65.19(3) . . ? Al2 Al5 Ce1 128.18(4) 3_556 . ? Al6 Al5 Ce1 120.55(5) 3_556 . ? Al6 Al5 Ce1 67.29(4) 3 . ? Al1 Al5 Ce1 62.69(3) 3_556 . ? Ce1 Al5 Ce1 78.95(5) 1_556 . ? Co2 Al3 Co2 105.85(6) 1_556 . ? Co2 Al3 Al1 59.81(3) 1_556 . ? Co2 Al3 Al1 59.81(3) . . ? Co2 Al3 Al5 115.75(4) 1_556 . ? Co2 Al3 Al5 115.75(4) . . ? Al1 Al3 Al5 169.57(7) . . ? Co2 Al3 Al4 57.20(3) 1_556 7_655 ? Co2 Al3 Al4 57.20(3) . 7_655 ? Al1 Al3 Al4 59.50(5) . 7_655 ? Al5 Al3 Al4 110.07(6) . 7_655 ? Co2 Al3 Al6 118.19(6) 1_556 . ? Co2 Al3 Al6 50.81(3) . . ? Al1 Al3 Al6 59.89(4) . . ? Al5 Al3 Al6 125.97(4) . . ? Al4 Al3 Al6 101.10(5) 7_655 . ? Co2 Al3 Al6 50.81(3) 1_556 1_556 ? Co2 Al3 Al6 118.19(6) . 1_556 ? Al1 Al3 Al6 59.89(4) . 1_556 ? Al5 Al3 Al6 125.97(4) . 1_556 ? Al4 Al3 Al6 101.10(5) 7_655 1_556 ? Al6 Al3 Al6 87.59(6) . 1_556 ? Co2 Al3 Ce1 87.30(4) 1_556 1_556 ? Co2 Al3 Ce1 163.89(4) . 1_556 ? Al1 Al3 Ce1 122.79(4) . 1_556 ? Al5 Al3 Ce1 64.39(3) . 1_556 ? Al4 Al3 Ce1 138.84(3) 7_655 1_556 ? Al6 Al3 Ce1 114.89(5) . 1_556 ? Al6 Al3 Ce1 63.04(3) 1_556 1_556 ? Co2 Al3 Ce1 163.89(4) 1_556 . ? Co2 Al3 Ce1 87.30(4) . . ? Al1 Al3 Ce1 122.79(4) . . ? Al5 Al3 Ce1 64.40(3) . . ? Al4 Al3 Ce1 138.84(3) 7_655 . ? Al6 Al3 Ce1 63.04(3) . . ? Al6 Al3 Ce1 114.89(5) 1_556 . ? Ce1 Al3 Ce1 78.34(5) 1_556 . ? Co2 Al4 Co2 105.60(6) 7_666 7_665 ? Co2 Al4 Al2 115.28(4) 7_666 . ? Co2 Al4 Al2 115.28(4) 7_665 . ? Co2 Al4 Al1 59.72(3) 7_666 7_665 ? Co2 Al4 Al1 59.72(3) 7_665 7_665 ? Al2 Al4 Al1 168.42(7) . 7_665 ? Co2 Al4 Al3 57.05(3) 7_666 7_665 ? Co2 Al4 Al3 57.05(3) 7_665 7_665 ? Al2 Al4 Al3 109.03(6) . 7_665 ? Al1 Al4 Al3 59.39(5) 7_665 7_665 ? Co2 Al4 Al9 50.51(3) 7_666 3_556 ? Co2 Al4 Al9 117.65(5) 7_665 3_556 ? Al2 Al4 Al9 127.05(4) . 3_556 ? Al1 Al4 Al9 59.35(3) 7_665 3_556 ? Al3 Al4 Al9 100.49(4) 7_665 3_556 ? Co2 Al4 Al9 117.65(5) 7_666 3 ? Co2 Al4 Al9 50.51(3) 7_665 3 ? Al2 Al4 Al9 127.05(4) . 3 ? Al1 Al4 Al9 59.35(3) 7_665 3 ? Al3 Al4 Al9 100.49(4) 7_665 3 ? Al9 Al4 Al9 87.34(5) 3_556 3 ? Co2 Al4 Ce1 164.33(4) 7_666 . ? Co2 Al4 Ce1 87.84(4) 7_665 . ? Al2 Al4 Ce1 63.93(3) . . ? Al1 Al4 Ce1 124.02(4) 7_665 . ? Al3 Al4 Ce1 138.62(3) 7_665 . ? Al9 Al4 Ce1 116.20(5) 3_556 . ? Al9 Al4 Ce1 64.79(3) 3 . ? Co2 Al4 Ce1 87.84(4) 7_666 1_556 ? Co2 Al4 Ce1 164.33(4) 7_665 1_556 ? Al2 Al4 Ce1 63.93(3) . 1_556 ? Al1 Al4 Ce1 124.02(4) 7_665 1_556 ? Al3 Al4 Ce1 138.62(3) 7_665 1_556 ? Al9 Al4 Ce1 64.79(3) 3_556 1_556 ? Al9 Al4 Ce1 116.20(5) 3 1_556 ? Ce1 Al4 Ce1 77.82(5) . 1_556 ? Co2 Al1 Co2 101.18(6) . 1_556 ? Co2 Al1 Al3 56.82(3) . . ? Co2 Al1 Al3 56.82(3) 1_556 . ? Co2 Al1 Al4 56.89(3) . 7_655 ? Co2 Al1 Al4 56.89(3) 1_556 7_655 ? Al3 Al1 Al4 61.11(5) . 7_655 ? Co2 Al1 Al9 51.52(3) . . ? Co2 Al1 Al9 119.65(5) 1_556 . ? Al3 Al1 Al9 105.08(4) . . ? Al4 Al1 Al9 64.22(3) 7_655 . ? Co2 Al1 Al9 119.65(6) . 1_556 ? Co2 Al1 Al9 51.52(3) 1_556 1_556 ? Al3 Al1 Al9 105.08(4) . 1_556 ? Al4 Al1 Al9 64.22(3) 7_655 1_556 ? Al9 Al1 Al9 92.57(5) . 1_556 ? Co2 Al1 Al6 119.15(6) . 1_556 ? Co2 Al1 Al6 51.49(3) 1_556 1_556 ? Al3 Al1 Al6 63.86(4) . 1_556 ? Al4 Al1 Al6 104.99(5) 7_655 1_556 ? Al9 Al1 Al6 168.11(6) . 1_556 ? Al9 Al1 Al6 86.58(4) 1_556 1_556 ? Co2 Al1 Al6 51.49(4) . . ? Co2 Al1 Al6 119.15(6) 1_556 . ? Al3 Al1 Al6 63.86(4) . . ? Al4 Al1 Al6 104.99(5) 7_655 . ? Al9 Al1 Al6 86.58(4) . . ? Al9 Al1 Al6 168.10(6) 1_556 . ? Al6 Al1 Al6 91.81(6) 1_556 . ? Co2 Al1 Al5 112.12(4) . 3_456 ? Co2 Al1 Al5 112.12(4) 1_556 3_456 ? Al3 Al1 Al5 95.91(6) . 3_456 ? Al4 Al1 Al5 157.03(7) 7_655 3_456 ? Al9 Al1 Al5 127.59(3) . 3_456 ? Al9 Al1 Al5 127.59(3) 1_556 3_456 ? Al6 Al1 Al5 60.64(4) 1_556 3_456 ? Al6 Al1 Al5 60.64(4) . 3_456 ? Co2 Al1 Ce1 89.66(4) . 3_455 ? Co2 Al1 Ce1 169.15(4) 1_556 3_455 ? Al3 Al1 Ce1 131.85(4) . 3_455 ? Al4 Al1 Ce1 131.06(3) 7_655 3_455 ? Al9 Al1 Ce1 66.98(3) . 3_455 ? Al9 Al1 Ce1 122.22(5) 1_556 3_455 ? Al6 Al1 Ce1 123.19(5) 1_556 3_455 ? Al6 Al1 Ce1 68.23(4) . 3_455 ? Al5 Al1 Ce1 63.33(3) 3_456 3_455 ? Co2 Al1 Ce1 169.15(4) . 3_456 ? Co2 Al1 Ce1 89.66(4) 1_556 3_456 ? Al3 Al1 Ce1 131.85(4) . 3_456 ? Al4 Al1 Ce1 131.06(3) 7_655 3_456 ? Al9 Al1 Ce1 122.22(5) . 3_456 ? Al9 Al1 Ce1 66.98(3) 1_556 3_456 ? Al6 Al1 Ce1 68.22(4) 1_556 3_456 ? Al6 Al1 Ce1 123.19(5) . 3_456 ? Al5 Al1 Ce1 63.33(3) 3_456 3_456 ? Ce1 Al1 Ce1 79.49(5) 3_455 3_456 ? Co2 Al7 Co1 145.66(6) . 7_655 ? Co2 Al7 Co1 145.90(6) . 3 ? Co1 Al7 Co1 68.44(4) 7_655 3 ? Co2 Al7 Al8 136.19(2) . 3_556 ? Co1 Al7 Al8 53.36(3) 7_655 3_556 ? Co1 Al7 Al8 53.37(3) 3 3_556 ? Co2 Al7 Al8 136.19(2) . 3 ? Co1 Al7 Al8 53.36(3) 7_655 3 ? Co1 Al7 Al8 53.37(3) 3 3 ? Al8 Al7 Al8 87.61(5) 3_556 3 ? Co1 Al6 Co2 178.13(7) . . ? Co1 Al6 Al1 119.02(4) . 1_554 ? Co2 Al6 Al1 59.93(4) . 1_554 ? Co1 Al6 Al1 119.02(4) . . ? Co2 Al6 Al1 59.92(4) . . ? Al1 Al6 Al1 91.81(6) 1_554 . ? Co1 Al6 Al2 58.89(4) . . ? Co2 Al6 Al2 122.14(4) . . ? Al1 Al6 Al2 177.73(6) 1_554 . ? Al1 Al6 Al2 88.69(5) . . ? Co1 Al6 Al2 58.89(4) . 1_554 ? Co2 Al6 Al2 122.14(4) . 1_554 ? Al1 Al6 Al2 88.69(5) 1_554 1_554 ? Al1 Al6 Al2 177.73(6) . 1_554 ? Al2 Al6 Al2 90.73(6) . 1_554 ? Co1 Al6 Al5 58.26(3) . 3_455 ? Co2 Al6 Al5 120.68(4) . 3_455 ? Al1 Al6 Al5 60.76(4) 1_554 3_455 ? Al1 Al6 Al5 121.46(6) . 3_455 ? Al2 Al6 Al5 117.14(6) . 3_455 ? Al2 Al6 Al5 56.99(4) 1_554 3_455 ? Co1 Al6 Al5 58.26(3) . 3_456 ? Co2 Al6 Al5 120.68(4) . 3_456 ? Al1 Al6 Al5 121.46(6) 1_554 3_456 ? Al1 Al6 Al5 60.76(4) . 3_456 ? Al2 Al6 Al5 56.99(4) . 3_456 ? Al2 Al6 Al5 117.14(6) 1_554 3_456 ? Al5 Al6 Al5 89.39(6) 3_455 3_456 ? Co1 Al6 Al3 124.93(4) . 1_554 ? Co2 Al6 Al3 56.09(3) . 1_554 ? Al1 Al6 Al3 56.26(4) 1_554 1_554 ? Al1 Al6 Al3 116.02(6) . 1_554 ? Al2 Al6 Al3 125.38(6) . 1_554 ? Al2 Al6 Al3 66.05(4) 1_554 1_554 ? Al5 Al6 Al3 91.41(5) 3_455 1_554 ? Al5 Al6 Al3 176.49(6) 3_456 1_554 ? Co1 Al6 Al3 124.93(4) . . ? Co2 Al6 Al3 56.09(3) . . ? Al1 Al6 Al3 116.02(6) 1_554 . ? Al1 Al6 Al3 56.26(4) . . ? Al2 Al6 Al3 66.05(4) . . ? Al2 Al6 Al3 125.38(6) 1_554 . ? Al5 Al6 Al3 176.49(6) 3_455 . ? Al5 Al6 Al3 91.41(4) 3_456 . ? Al3 Al6 Al3 87.59(6) 1_554 . ? Co1 Al6 Ce1 91.87(4) . . ? Co2 Al6 Ce1 90.00(4) . . ? Al1 Al6 Ce1 118.87(4) 1_554 . ? Al1 Al6 Ce1 118.87(4) . . ? Al2 Al6 Ce1 62.68(3) . . ? Al2 Al6 Ce1 62.68(3) 1_554 . ? Al5 Al6 Ce1 119.67(4) 3_455 . ? Al5 Al6 Ce1 119.67(4) 3_456 . ? Al3 Al6 Ce1 62.74(4) 1_554 . ? Al3 Al6 Ce1 62.74(4) . . ? Co1 Al6 Ce1 88.74(4) . 3_455 ? Co2 Al6 Ce1 89.39(4) . 3_455 ? Al1 Al6 Ce1 60.79(4) 1_554 3_455 ? Al1 Al6 Ce1 60.79(4) . 3_455 ? Al2 Al6 Ce1 117.68(4) . 3_455 ? Al2 Al6 Ce1 117.68(4) 1_554 3_455 ? Al5 Al6 Ce1 60.69(4) 3_455 3_455 ? Al5 Al6 Ce1 60.69(4) 3_456 3_455 ? Al3 Al6 Ce1 116.88(4) 1_554 3_455 ? Al3 Al6 Ce1 116.88(4) . 3_455 ? Ce1 Al6 Ce1 179.39(4) . 3_455 ? _diffrn_measured_fraction_theta_max 0.996 _diffrn_reflns_theta_full 31.01 _diffrn_measured_fraction_theta_full 0.996 _refine_diff_density_max 1.221 _refine_diff_density_min -2.014 _refine_diff_density_rms 0.254