data_rjy10 _audit_creation_method 'SHELXL-2014/7' _shelx_SHELXL_version_number '2014/7' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C79 Co F12 N4 O23 Ru4 S4' _chemical_formula_weight 2192.28 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Co' 'Co' 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Ru' 'Ru' -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'F' 'F' 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/n' _space_group_name_Hall '-P 2yn' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 14.472(5) _cell_length_b 25.490(9) _cell_length_c 26.207(8) _cell_angle_alpha 90 _cell_angle_beta 93.01(2) _cell_angle_gamma 90 _cell_volume 9654(5) _cell_formula_units_Z 4 _cell_measurement_temperature 296(2) _cell_measurement_reflns_used ? _cell_measurement_theta_min ? _cell_measurement_theta_max ? _exptl_crystal_description ? _exptl_crystal_colour ? _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.508 _exptl_crystal_F_000 4244 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max ? _exptl_crystal_size_mid ? _exptl_crystal_size_min ? _exptl_absorpt_coefficient_mu 0.955 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type ? _exptl_absorpt_correction_T_min ? _exptl_absorpt_correction_T_max ? _exptl_absorpt_process_details ? _exptl_absorpt_special_details ? _diffrn_ambient_temperature 296(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source ? _diffrn_measurement_device_type ? _diffrn_measurement_method ? _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 22355 _diffrn_reflns_av_unetI/netI 0.0673 _diffrn_reflns_av_R_equivalents 0.0920 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_limit_l_max 20 _diffrn_reflns_theta_min 1.115 _diffrn_reflns_theta_max 15.849 _diffrn_reflns_theta_full 15.849 _diffrn_measured_fraction_theta_max 0.975 _diffrn_measured_fraction_theta_full 0.975 _diffrn_reflns_Laue_measured_fraction_max 0.975 _diffrn_reflns_Laue_measured_fraction_full 0.975 _diffrn_reflns_point_group_measured_fraction_max 0.975 _diffrn_reflns_point_group_measured_fraction_full 0.975 _reflns_number_total 4468 _reflns_number_gt 3123 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution ? _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1000P)^2^+0.5165P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens . _refine_ls_hydrogen_treatment undef _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 4468 _refine_ls_number_parameters 509 _refine_ls_number_restraints 32 _refine_ls_R_factor_all 0.1817 _refine_ls_R_factor_gt 0.1299 _refine_ls_wR_factor_ref 0.3583 _refine_ls_wR_factor_gt 0.3245 _refine_ls_goodness_of_fit_ref 2.441 _refine_ls_restrained_S_all 2.437 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ru1 Ru 0.5164(3) -0.18847(15) 0.21981(15) 0.0757(16) Uiso 1 1 d . . . . . Ru2 Ru 0.3851(2) 0.01180(14) 0.18600(14) 0.0691(15) Uiso 1 1 d . . . . . Ru3 Ru 0.1225(2) 0.18879(14) 0.50002(14) 0.0642(15) Uiso 1 1 d . . . . . Ru4 Ru 0.3928(2) 0.30005(14) 0.41081(14) 0.0642(15) Uiso 1 1 d . . . . . Co1 Co 0.3007(4) -0.0840(2) 0.4650(2) 0.054(2) Uiso 1 1 d . . . . . O1 O 0.3930(16) -0.1454(10) 0.2052(9) 0.061(8) Uiso 1 1 d . . . . . O2 O 0.5619(18) -0.1140(10) 0.2156(10) 0.076(9) Uiso 1 1 d . . . . . O3 O 0.3359(17) -0.0674(9) 0.1874(9) 0.052(8) Uiso 1 1 d . . . . . O4 O 0.5080(16) -0.0280(11) 0.2017(9) 0.066(8) Uiso 1 1 d . . . . . O5 O 0.1611(16) 0.2100(9) 0.4270(8) 0.050(7) Uiso 1 1 d . . . . . O6 O 0.2317(16) 0.2418(9) 0.5183(10) 0.064(8) Uiso 1 1 d . . . . . O7 O 0.2760(16) 0.2547(9) 0.3902(9) 0.060(8) Uiso 1 1 d . . . . . O8 O 0.3316(17) 0.2942(10) 0.4818(9) 0.066(8) Uiso 1 1 d . . . . . O9 O 0.4363(16) -0.0309(9) 0.5516(10) 0.058(8) Uiso 1 1 d . . . . . C1 C 0.181(2) -0.1184(14) 0.4375(14) 0.042(11) Uiso 1 1 d . . . . . C2 C 0.160(2) -0.0718(14) 0.4625(15) 0.054(12) Uiso 1 1 d . . . . . C3 C 0.200(2) -0.0825(15) 0.5120(15) 0.053(12) Uiso 1 1 d . . . . . C4 C 0.238(3) -0.1292(17) 0.5150(16) 0.069(13) Uiso 1 1 d . . . . . C5 C 0.228(3) -0.1515(15) 0.4692(16) 0.059(13) Uiso 1 1 d . . . . . C6 C 0.418(3) -0.0445(15) 0.5066(17) 0.055(12) Uiso 1 1 d . . . . . C7 C 0.437(2) -0.0956(14) 0.4839(14) 0.043(11) Uiso 1 1 d . . . . . C8 C 0.417(2) -0.0902(14) 0.4292(15) 0.045(11) Uiso 1 1 d . . . . . C9 C 0.377(2) -0.0393(15) 0.4213(15) 0.050(12) Uiso 1 1 d . . . . . C10 C 0.368(2) -0.0116(13) 0.4659(13) 0.028(10) Uiso 1 1 d . . . . . C11 C 0.476(2) -0.1425(15) 0.5128(16) 0.052(12) Uiso 1 1 d . . . . . C12 C 0.523(2) -0.1374(14) 0.5603(16) 0.052(12) Uiso 1 1 d . . . . . C13 C 0.554(2) -0.1826(16) 0.5833(14) 0.054(12) Uiso 1 1 d . . . . . C14 C 0.497(3) -0.2343(16) 0.5153(18) 0.075(14) Uiso 1 1 d . . . . . C15 C 0.462(2) -0.1905(15) 0.4875(14) 0.049(12) Uiso 1 1 d . . . . . C16 C 0.447(3) -0.1217(14) 0.3864(14) 0.045(11) Uiso 1 1 d . . . . . C17 C 0.381(2) -0.1527(13) 0.3577(14) 0.043(11) Uiso 1 1 d . . . . . C18 C 0.409(2) -0.1752(13) 0.3131(14) 0.044(11) Uiso 1 1 d . . . . . C19 C 0.558(3) -0.1407(16) 0.3223(16) 0.065(13) Uiso 1 1 d . . . . . C20 C 0.535(2) -0.1164(13) 0.3706(13) 0.044(11) Uiso 1 1 d . . . . . C21 C 0.369(3) -0.0205(13) 0.3687(14) 0.043(11) Uiso 1 1 d . . . . . C22 C 0.439(3) 0.0074(14) 0.3486(15) 0.052(12) Uiso 1 1 d . . . . . C23 C 0.437(3) 0.0214(14) 0.2965(16) 0.054(12) Uiso 1 1 d . . . . . C24 C 0.296(3) -0.0176(14) 0.2826(15) 0.053(12) Uiso 1 1 d . . . . . C25 C 0.291(2) -0.0324(13) 0.3344(14) 0.042(11) Uiso 1 1 d . . . . . C26 C 0.317(2) 0.0360(15) 0.4754(15) 0.046(12) Uiso 1 1 d . . . . . C27 C 0.259(3) 0.0558(16) 0.4372(16) 0.068(14) Uiso 1 1 d . . . . . C28 C 0.207(2) 0.1029(15) 0.4438(14) 0.049(12) Uiso 1 1 d . . . . . C29 C 0.278(2) 0.1084(14) 0.5290(14) 0.047(12) Uiso 1 1 d . . . . . C30 C 0.326(2) 0.0623(15) 0.5214(15) 0.051(12) Uiso 1 1 d . . . . . C31 C 0.403(3) -0.0947(16) 0.1958(14) 0.058(13) Uiso 1 1 d . . . . . C32 C 0.500(3) -0.0743(19) 0.2053(15) 0.068(14) Uiso 1 1 d . . . . . C33 C 0.487(4) -0.271(2) 0.218(2) 0.109(18) Uiso 1 1 d . . . . . C34 C 0.575(4) -0.2672(19) 0.2435(19) 0.104(17) Uiso 1 1 d . . . . . C35 C 0.638(4) -0.237(2) 0.219(2) 0.118(19) Uiso 1 1 d . . . . . C36 C 0.617(3) -0.2170(16) 0.1684(18) 0.079(14) Uiso 1 1 d . . . . . C37 C 0.529(3) -0.2240(16) 0.1468(15) 0.069(14) Uiso 1 1 d . . . . . C38 C 0.461(3) -0.253(2) 0.172(2) 0.109(18) Uiso 1 1 d . . . . . C39 C 0.698(5) -0.172(3) 0.145(3) 0.20(3) Uiso 1 1 d . . . . . C40 C 0.723(5) -0.223(3) 0.095(3) 0.20(3) Uiso 1 1 d . . . . . C41 C 0.766(5) -0.162(2) 0.182(3) 0.17(3) Uiso 1 1 d . . . . . C42 C 0.397(5) -0.295(3) 0.236(3) 0.19(3) Uiso 1 1 d . . . . . C43 C 0.272(3) 0.0436(16) 0.1397(16) 0.062(13) Uiso 1 1 d . . . . . C44 C 0.294(3) 0.0805(18) 0.1777(18) 0.086(15) Uiso 1 1 d . . . . . C45 C 0.390(3) 0.0956(16) 0.1845(16) 0.076(14) Uiso 1 1 d . . . . . C46 C 0.456(3) 0.0767(17) 0.1506(18) 0.083(15) Uiso 1 1 d . . . . . C47 C 0.433(3) 0.0386(18) 0.1127(18) 0.090(15) Uiso 1 1 d . . . . . C48 C 0.341(3) 0.0242(14) 0.1091(15) 0.058(12) Uiso 1 1 d . . . . . C49 C 0.179(4) 0.017(2) 0.133(2) 0.13(2) Uiso 1 1 d . . . . . C50 C 0.110(4) 0.031(2) 0.174(3) 0.17(3) Uiso 1 1 d . . . . . C51 C 0.121(4) 0.038(2) 0.082(3) 0.18(3) Uiso 1 1 d . . . . . C52 C 0.560(4) 0.087(2) 0.162(2) 0.14(2) Uiso 1 1 d . . . . . C53 C 0.230(3) 0.2413(15) 0.4310(16) 0.056(12) Uiso 1 1 d . . . . . C54 C 0.268(3) 0.2605(16) 0.4813(17) 0.060(13) Uiso 1 1 d . . . . . C55 C 0.057(3) 0.2011(19) 0.5720(18) 0.085(15) Uiso 1 1 d . . . . . C56 C 0.026(3) 0.2368(15) 0.5368(17) 0.062(13) Uiso 1 1 d . . . . . C57 C -0.012(3) 0.2201(17) 0.4889(17) 0.077(14) Uiso 1 1 d . . . . . C58 C -0.016(3) 0.1670(16) 0.4736(16) 0.062(13) Uiso 1 1 d . . . . . C59 C 0.020(3) 0.1291(15) 0.5111(16) 0.058(13) Uiso 1 1 d . . . . . C60 C 0.051(3) 0.1469(17) 0.5591(17) 0.069(14) Uiso 1 1 d . . . . . C61 C 0.103(3) 0.2240(17) 0.6199(19) 0.091(16) Uiso 1 1 d . . . . . C62 C 0.177(5) 0.189(3) 0.643(3) 0.20(3) Uiso 1 1 d . . . . . C63 C 0.029(5) 0.213(3) 0.662(3) 0.18(3) Uiso 1 1 d . . . . . C64 C -0.041(3) 0.1521(15) 0.4204(16) 0.077(14) Uiso 1 1 d . . . . . C65 C 0.392(3) 0.3335(15) 0.3336(15) 0.053(12) Uiso 1 1 d . . . . . C66 C 0.343(3) 0.3659(15) 0.3640(17) 0.064(13) Uiso 1 1 d . . . . . C67 C 0.384(3) 0.3806(16) 0.4106(17) 0.074(14) Uiso 1 1 d . . . . . C68 C 0.485(3) 0.3636(18) 0.4272(19) 0.091(16) Uiso 1 1 d . . . . . C69 C 0.527(3) 0.3332(15) 0.3942(16) 0.061(13) Uiso 1 1 d . . . . . C70 C 0.479(3) 0.3154(16) 0.3485(17) 0.074(14) Uiso 1 1 d . . . . . C71 C 0.340(3) 0.3091(17) 0.2869(17) 0.081(15) Uiso 1 1 d . . . . . C72 C 0.371(3) 0.2570(18) 0.2713(17) 0.092(15) Uiso 1 1 d . . . . . C73 C 0.348(3) 0.3508(18) 0.2438(18) 0.105(17) Uiso 1 1 d . . . . . C74 C 0.524(3) 0.384(2) 0.483(2) 0.13(2) Uiso 1 1 d . . . . . S1 S 0.1020(9) 0.3796(5) 0.4414(5) 0.090(4) Uiso 1 1 d . . . . . O10 O 0.1111(18) 0.3241(11) 0.4426(10) 0.089(10) Uiso 1 1 d . . . . . O11 O 0.184(2) 0.4093(12) 0.4513(12) 0.111(11) Uiso 1 1 d . . . . . O12 O 0.0323(19) 0.4011(11) 0.4018(11) 0.098(10) Uiso 1 1 d . . . . . C75 C 0.037(6) 0.389(3) 0.511(3) 0.19(3) Uiso 1 1 d . . . . . F1 F 0.098(3) 0.3786(16) 0.5405(18) 0.214(19) Uiso 1 1 d . . . . . F2 F 0.028(3) 0.4469(17) 0.4993(13) 0.198(15) Uiso 1 1 d . . . . . F3 F -0.044(3) 0.3698(16) 0.4928(16) 0.213(17) Uiso 1 1 d . . . . . S2 S 0.2745(10) 0.7189(6) 0.3861(6) 0.099(5) Uiso 1 1 d . . . . . O13 O 0.280(2) 0.6834(15) 0.3448(15) 0.147(14) Uiso 1 1 d . . . . . O14 O 0.353(2) 0.7253(12) 0.4174(13) 0.124(12) Uiso 1 1 d . . . . . O15 O 0.220(2) 0.7641(13) 0.3726(12) 0.120(12) Uiso 1 1 d . . . . . C76 C 0.194(5) 0.683(3) 0.426(3) 0.15(2) Uiso 1 1 d . . . . . F4 F 0.238(2) 0.6409(13) 0.4468(12) 0.149(12) Uiso 1 1 d . . . . . F5 F 0.1885(19) 0.7136(11) 0.4709(12) 0.133(10) Uiso 1 1 d . . . . . F6 F 0.114(2) 0.6779(12) 0.4047(12) 0.142(11) Uiso 1 1 d . . . . . S3 S 0.5994(13) 0.1730(7) 0.3038(7) 0.150(6) Uiso 1 1 d D . . . . O16 O 0.609(3) 0.2046(15) 0.3472(15) 0.188(17) Uiso 1 1 d D . . . . O17 O 0.642(3) 0.1958(17) 0.2547(17) 0.21(2) Uiso 1 1 d D . . . . O18 O 0.513(2) 0.1446(14) 0.2991(14) 0.163(15) Uiso 1 1 d D . . . . C77 C 0.695(2) 0.1276(13) 0.3186(14) 0.27(5) Uiso 1 1 d D . . . . F7 F 0.767(2) 0.1553(13) 0.3217(12) 0.172(13) Uiso 1 1 d D . . . . F8 F 0.693(2) 0.0930(14) 0.2836(14) 0.179(13) Uiso 1 1 d D . . . . F9 F 0.660(2) 0.1097(14) 0.3586(14) 0.206(16) Uiso 1 1 d D . . . . S4 S -0.0181(19) -0.0076(10) 0.3777(10) 0.233(11) Uiso 1 1 d D . . . . O19 O 0.037(3) 0.0252(18) 0.4090(17) 0.24(2) Uiso 1 1 d D . . . . O20 O 0.039(4) -0.055(2) 0.354(2) 0.32(3) Uiso 1 1 d D . . . . O21 O -0.106(3) -0.0212(17) 0.3984(17) 0.23(2) Uiso 1 1 d D . . . . C78 C -0.018(3) 0.0283(19) 0.3182(14) 1.2(4) Uiso 1 1 d D . . . . F10 F -0.079(4) 0.063(2) 0.322(2) 0.38(3) Uiso 1 1 d D . . . . F11 F -0.031(6) -0.004(3) 0.282(2) 0.56(6) Uiso 1 1 d D . . . . F12 F 0.067(3) 0.040(2) 0.3244(19) 0.30(2) Uiso 1 1 d D . . . . C102 C 0.693(4) 0.977(2) 0.320(2) 0.16(2) Uiso 1 1 d . . . . . N1 N 0.549(2) -0.2296(12) 0.5595(13) 0.062(10) Uiso 1 1 d . . . . . N2 N 0.493(2) -0.1685(11) 0.2959(11) 0.047(9) Uiso 1 1 d . . . . . N3 N 0.368(2) 0.0060(11) 0.2652(11) 0.045(9) Uiso 1 1 d . . . . . N4 N 0.2214(19) 0.1266(11) 0.4898(12) 0.044(9) Uiso 1 1 d . . . . . O31 O 0.733(3) 0.9340(17) 0.3530(16) 0.174(16) Uiso 1 1 d . . . . . O32 O 0.556(4) 0.718(3) 0.375(2) 0.32(3) Uiso 1 1 d . . . . . _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ru1 O2 2.01(3) . ? Ru1 N2 2.10(3) . ? Ru1 O1 2.11(2) . ? Ru1 C37 2.13(4) . ? Ru1 C35 2.15(5) . ? Ru1 C33 2.15(5) . ? Ru1 C36 2.15(4) . ? Ru1 C38 2.20(5) . ? Ru1 C34 2.25(5) . ? Ru2 O4 2.07(2) . ? Ru2 C48 2.11(4) . ? Ru2 N3 2.11(3) . ? Ru2 C45 2.14(4) . ? Ru2 O3 2.14(2) . ? Ru2 C43 2.15(4) . ? Ru2 C46 2.18(4) . ? Ru2 C47 2.19(5) . ? Ru2 C44 2.20(4) . ? Ru3 O5 2.09(2) . ? Ru3 C57 2.11(4) . ? Ru3 O6 2.11(2) . ? Ru3 C56 2.12(4) . ? Ru3 C58 2.15(4) . ? Ru3 C59 2.16(4) . ? Ru3 N4 2.16(3) . ? Ru3 C55 2.18(4) . ? Ru3 C60 2.19(4) . ? Ru4 C67 2.06(4) . ? Ru4 O7 2.10(2) . ? Ru4 O8 2.11(2) . ? Ru4 N1 2.12(3) 3_656 ? Ru4 C68 2.12(5) . ? Ru4 C70 2.15(4) . ? Ru4 C69 2.18(4) . ? Ru4 C66 2.18(4) . ? Ru4 C65 2.19(4) . ? Co1 C3 1.96(4) . ? Co1 C8 1.97(3) . ? Co1 C9 1.99(4) . ? Co1 C4 2.00(4) . ? Co1 C7 2.02(3) . ? Co1 C5 2.03(4) . ? Co1 C1 2.04(3) . ? Co1 C2 2.06(4) . ? Co1 C10 2.09(3) . ? Co1 C6 2.21(4) . ? O1 C31 1.33(4) . ? O2 C32 1.37(4) . ? O3 C31 1.21(4) . ? O4 C32 1.19(4) . ? O5 C53 1.28(4) . ? O6 C54 1.22(4) . ? O7 C53 1.33(4) . ? O8 C54 1.26(4) . ? O9 C6 1.24(4) . ? C1 C5 1.34(4) . ? C1 C2 1.40(4) . ? C2 C3 1.42(4) . ? C3 C4 1.31(4) . ? C4 C5 1.33(4) . ? C6 C7 1.46(4) . ? C6 C10 1.51(4) . ? C7 C8 1.45(4) . ? C7 C11 1.51(4) . ? C8 C9 1.43(4) . ? C8 C16 1.47(4) . ? C9 C10 1.38(4) . ? C9 C21 1.46(4) . ? C10 C26 1.45(4) . ? C11 C12 1.40(4) . ? C11 C15 1.40(4) . ? C12 C13 1.36(4) . ? C13 N1 1.35(4) . ? C14 N1 1.35(4) . ? C14 C15 1.41(5) . ? C16 C20 1.36(4) . ? C16 C17 1.42(4) . ? C17 C18 1.38(4) . ? C18 N2 1.34(4) . ? C19 N2 1.34(4) . ? C19 C20 1.46(4) . ? C21 C22 1.36(4) . ? C21 C25 1.44(4) . ? C22 C23 1.41(4) . ? C23 N3 1.32(4) . ? C24 N3 1.31(4) . ? C24 C25 1.41(4) . ? C26 C27 1.37(4) . ? C26 C30 1.38(4) . ? C27 C28 1.43(4) . ? C28 N4 1.35(4) . ? C29 N4 1.36(4) . ? C29 C30 1.39(4) . ? C31 C32 1.50(5) . ? C33 C38 1.33(6) . ? C33 C34 1.40(6) . ? C33 C42 1.53(7) . ? C34 C35 1.37(6) . ? C35 C36 1.45(6) . ? C36 C37 1.38(5) . ? C36 C39 1.78(8) . ? C37 C38 1.43(5) . ? C39 C41 1.36(8) . ? C39 C40 1.87(9) . ? C43 C44 1.39(5) . ? C43 C48 1.40(4) . ? C43 C49 1.51(6) . ? C44 C45 1.44(5) . ? C45 C46 1.42(5) . ? C46 C47 1.42(5) . ? C46 C52 1.54(6) . ? C47 C48 1.39(5) . ? C49 C50 1.55(7) . ? C49 C51 1.62(7) . ? C53 C54 1.48(5) . ? C55 C56 1.35(5) . ? C55 C60 1.42(5) . ? C55 C61 1.51(5) . ? C56 C57 1.41(5) . ? C57 C58 1.41(5) . ? C58 C59 1.45(5) . ? C58 C64 1.47(5) . ? C59 C60 1.39(4) . ? C61 C62 1.51(7) . ? C61 C63 1.59(7) . ? C65 C66 1.37(4) . ? C65 C70 1.38(5) . ? C65 C71 1.54(5) . ? C66 C67 1.38(5) . ? C67 C68 1.57(5) . ? C68 C69 1.33(5) . ? C68 C74 1.63(6) . ? C69 C70 1.42(5) . ? C71 C72 1.46(5) . ? C71 C73 1.56(5) . ? S1 O10 1.42(3) . ? S1 O11 1.42(3) . ? S1 O12 1.51(3) . ? S1 C75 2.10(8) . ? C75 F1 1.17(8) . ? C75 F3 1.33(8) . ? C75 F2 1.51(8) . ? S2 O14 1.37(3) . ? S2 O13 1.42(4) . ? S2 O15 1.43(3) . ? S2 C76 1.86(6) . ? C76 F6 1.26(6) . ? C76 F4 1.35(6) . ? C76 F5 1.40(6) . ? S3 O16 1.40(3) . ? S3 O18 1.45(3) . ? S3 O17 1.57(4) . ? S3 C77 1.83(3) . ? C77 F7 1.26(2) . ? C77 F8 1.27(2) . ? C77 F9 1.27(2) . ? S4 O19 1.39(4) . ? S4 O21 1.45(3) . ? S4 O20 1.61(4) . ? S4 C78 1.81(2) . ? C78 F10 1.26(3) . ? C78 F11 1.27(3) . ? C78 F12 1.27(3) . ? C102 O31 1.49(6) . ? N1 Ru4 2.12(3) 3_656 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O2 Ru1 N2 83.8(11) . . ? O2 Ru1 O1 77.1(10) . . ? N2 Ru1 O1 82.6(10) . . ? O2 Ru1 C37 107.9(14) . . ? N2 Ru1 C37 168.3(14) . . ? O1 Ru1 C37 99.7(13) . . ? O2 Ru1 C35 105.8(17) . . ? N2 Ru1 C35 108.4(17) . . ? O1 Ru1 C35 168.8(16) . . ? C37 Ru1 C35 69.2(18) . . ? O2 Ru1 C33 171.1(16) . . ? N2 Ru1 C33 102.3(17) . . ? O1 Ru1 C33 110.0(17) . . ? C37 Ru1 C33 66.1(17) . . ? C35 Ru1 C33 66(2) . . ? O2 Ru1 C36 92.9(13) . . ? N2 Ru1 C36 145.1(15) . . ? O1 Ru1 C36 130.6(15) . . ? C37 Ru1 C36 37.4(13) . . ? C35 Ru1 C36 39.3(15) . . ? C33 Ru1 C36 78.3(18) . . ? O2 Ru1 C38 142.1(17) . . ? N2 Ru1 C38 130.5(17) . . ? O1 Ru1 C38 90.4(15) . . ? C37 Ru1 C38 38.5(14) . . ? C35 Ru1 C38 80.8(18) . . ? C33 Ru1 C38 35.6(16) . . ? C36 Ru1 C38 68.3(17) . . ? O2 Ru1 C34 137.4(16) . . ? N2 Ru1 C34 91.8(15) . . ? O1 Ru1 C34 144.5(16) . . ? C37 Ru1 C34 79.7(16) . . ? C35 Ru1 C34 36.2(15) . . ? C33 Ru1 C34 37.1(15) . . ? C36 Ru1 C34 67.4(17) . . ? C38 Ru1 C34 66.9(18) . . ? O4 Ru2 C48 118.7(13) . . ? O4 Ru2 N3 84.9(10) . . ? C48 Ru2 N3 155.2(14) . . ? O4 Ru2 C45 117.7(14) . . ? C48 Ru2 C45 80.8(15) . . ? N3 Ru2 C45 95.4(14) . . ? O4 Ru2 O3 79.5(10) . . ? C48 Ru2 O3 94.2(12) . . ? N3 Ru2 O3 82.0(10) . . ? C45 Ru2 O3 162.4(14) . . ? O4 Ru2 C43 157.1(13) . . ? C48 Ru2 C43 38.5(12) . . ? N3 Ru2 C43 117.3(14) . . ? C45 Ru2 C43 68.6(16) . . ? O3 Ru2 C43 97.0(13) . . ? O4 Ru2 C46 92.2(14) . . ? C48 Ru2 C46 66.8(15) . . ? N3 Ru2 C46 123.6(15) . . ? C45 Ru2 C46 38.5(13) . . ? O3 Ru2 C46 152.6(14) . . ? C43 Ru2 C46 80.6(16) . . ? O4 Ru2 C47 91.0(14) . . ? C48 Ru2 C47 37.7(13) . . ? N3 Ru2 C47 161.0(16) . . ? C45 Ru2 C47 70.1(16) . . ? O3 Ru2 C47 115.5(14) . . ? C43 Ru2 C47 69.9(15) . . ? C46 Ru2 C47 37.9(14) . . ? O4 Ru2 C44 156.3(15) . . ? C48 Ru2 C44 68.5(15) . . ? N3 Ru2 C44 93.1(14) . . ? C45 Ru2 C44 38.9(14) . . ? O3 Ru2 C44 123.6(14) . . ? C43 Ru2 C44 37.4(13) . . ? C46 Ru2 C44 69.3(16) . . ? C47 Ru2 C44 83.3(16) . . ? O5 Ru3 C57 93.6(13) . . ? O5 Ru3 O6 79.0(10) . . ? C57 Ru3 O6 117.5(14) . . ? O5 Ru3 C56 118.6(13) . . ? C57 Ru3 C56 39.0(13) . . ? O6 Ru3 C56 91.7(12) . . ? O5 Ru3 C58 93.4(13) . . ? C57 Ru3 C58 38.7(13) . . ? O6 Ru3 C58 155.2(13) . . ? C56 Ru3 C58 71.0(15) . . ? O5 Ru3 C59 121.6(13) . . ? C57 Ru3 C59 69.4(15) . . ? O6 Ru3 C59 158.7(14) . . ? C56 Ru3 C59 82.6(14) . . ? C58 Ru3 C59 39.4(13) . . ? O5 Ru3 N4 82.3(10) . . ? C57 Ru3 N4 150.8(15) . . ? O6 Ru3 N4 90.2(10) . . ? C56 Ru3 N4 158.9(15) . . ? C58 Ru3 N4 112.4(14) . . ? C59 Ru3 N4 88.1(12) . . ? O5 Ru3 C55 154.6(14) . . ? C57 Ru3 C55 68.0(17) . . ? O6 Ru3 C55 93.8(15) . . ? C56 Ru3 C55 36.6(13) . . ? C58 Ru3 C55 82.9(17) . . ? C59 Ru3 C55 69.5(16) . . ? N4 Ru3 C55 122.3(15) . . ? O5 Ru3 C60 158.9(14) . . ? C57 Ru3 C60 79.3(15) . . ? O6 Ru3 C60 121.9(14) . . ? C56 Ru3 C60 67.2(15) . . ? C58 Ru3 C60 68.6(15) . . ? C59 Ru3 C60 37.3(12) . . ? N4 Ru3 C60 94.2(13) . . ? C55 Ru3 C60 38.1(13) . . ? C67 Ru4 O7 119.9(14) . . ? C67 Ru4 O8 92.5(13) . . ? O7 Ru4 O8 79.5(10) . . ? C67 Ru4 N1 150.7(16) . 3_656 ? O7 Ru4 N1 85.9(11) . 3_656 ? O8 Ru4 N1 78.1(11) . 3_656 ? C67 Ru4 C68 43.9(15) . . ? O7 Ru4 C68 163.8(14) . . ? O8 Ru4 C68 99.4(15) . . ? N1 Ru4 C68 109.8(16) 3_656 . ? C67 Ru4 C70 81.7(15) . . ? O7 Ru4 C70 113.5(14) . . ? O8 Ru4 C70 167.0(15) . . ? N1 Ru4 C70 101.3(14) 3_656 . ? C68 Ru4 C70 68.3(17) . . ? C67 Ru4 C69 70.7(15) . . ? O7 Ru4 C69 151.2(14) . . ? O8 Ru4 C69 128.6(14) . . ? N1 Ru4 C69 93.4(13) 3_656 . ? C68 Ru4 C69 35.9(13) . . ? C70 Ru4 C69 38.5(13) . . ? C67 Ru4 C66 37.9(13) . . ? O7 Ru4 C66 92.3(13) . . ? O8 Ru4 C66 114.2(13) . . ? N1 Ru4 C66 167.0(15) 3_656 . ? C68 Ru4 C66 73.3(16) . . ? C70 Ru4 C66 67.6(15) . . ? C69 Ru4 C66 81.9(14) . . ? C67 Ru4 C65 67.2(15) . . ? O7 Ru4 C65 90.8(12) . . ? O8 Ru4 C65 149.4(12) . . ? N1 Ru4 C65 130.5(14) 3_656 . ? C68 Ru4 C65 82.0(16) . . ? C70 Ru4 C65 37.0(12) . . ? C69 Ru4 C65 68.0(14) . . ? C66 Ru4 C65 36.6(12) . . ? C3 Co1 C8 168.9(16) . . ? C3 Co1 C9 143.7(16) . . ? C8 Co1 C9 42.2(13) . . ? C3 Co1 C4 38.8(13) . . ? C8 Co1 C4 133.8(17) . . ? C9 Co1 C4 172.6(16) . . ? C3 Co1 C7 126.5(16) . . ? C8 Co1 C7 42.6(12) . . ? C9 Co1 C7 70.2(14) . . ? C4 Co1 C7 102.9(16) . . ? C3 Co1 C5 64.8(15) . . ? C8 Co1 C5 114.7(15) . . ? C9 Co1 C5 145.5(16) . . ? C4 Co1 C5 38.6(13) . . ? C7 Co1 C5 111.4(15) . . ? C3 Co1 C1 65.4(14) . . ? C8 Co1 C1 121.8(14) . . ? C9 Co1 C1 122.1(15) . . ? C4 Co1 C1 65.0(16) . . ? C7 Co1 C1 145.1(15) . . ? C5 Co1 C1 38.5(12) . . ? C3 Co1 C2 41.3(13) . . ? C8 Co1 C2 149.7(16) . . ? C9 Co1 C2 118.4(15) . . ? C4 Co1 C2 68.0(15) . . ? C7 Co1 C2 167.6(16) . . ? C5 Co1 C2 67.1(15) . . ? C1 Co1 C2 39.8(12) . . ? C3 Co1 C10 109.8(14) . . ? C8 Co1 C10 70.6(14) . . ? C9 Co1 C10 39.4(12) . . ? C4 Co1 C10 136.9(16) . . ? C7 Co1 C10 71.3(13) . . ? C5 Co1 C10 174.6(15) . . ? C1 Co1 C10 140.6(14) . . ? C2 Co1 C10 109.2(14) . . ? C3 Co1 C6 105.0(15) . . ? C8 Co1 C6 67.6(15) . . ? C9 Co1 C6 65.6(15) . . ? C4 Co1 C6 107.6(16) . . ? C7 Co1 C6 40.1(12) . . ? C5 Co1 C6 138.5(16) . . ? C1 Co1 C6 170.4(14) . . ? C2 Co1 C6 132.9(15) . . ? C10 Co1 C6 41.0(12) . . ? C31 O1 Ru1 116(2) . . ? C32 O2 Ru1 120(3) . . ? C31 O3 Ru2 106(2) . . ? C32 O4 Ru2 114(3) . . ? C53 O5 Ru3 109(2) . . ? C54 O6 Ru3 114(3) . . ? C53 O7 Ru4 111(2) . . ? C54 O8 Ru4 112(3) . . ? C5 C1 C2 111(4) . . ? C5 C1 Co1 70(2) . . ? C2 C1 Co1 71(2) . . ? C1 C2 C3 100(3) . . ? C1 C2 Co1 69(2) . . ? C3 C2 Co1 65(2) . . ? C4 C3 C2 112(4) . . ? C4 C3 Co1 72(2) . . ? C2 C3 Co1 73(2) . . ? C3 C4 C5 108(4) . . ? C3 C4 Co1 69(2) . . ? C5 C4 Co1 72(3) . . ? C4 C5 C1 109(4) . . ? C4 C5 Co1 69(2) . . ? C1 C5 Co1 71(2) . . ? O9 C6 C7 127(4) . . ? O9 C6 C10 126(4) . . ? C7 C6 C10 107(4) . . ? O9 C6 Co1 135(3) . . ? C7 C6 Co1 63(2) . . ? C10 C6 Co1 65(2) . . ? C8 C7 C6 107(3) . . ? C8 C7 C11 128(3) . . ? C6 C7 C11 125(4) . . ? C8 C7 Co1 66.9(19) . . ? C6 C7 Co1 77(2) . . ? C11 C7 Co1 125(2) . . ? C9 C8 C7 107(3) . . ? C9 C8 C16 121(3) . . ? C7 C8 C16 131(3) . . ? C9 C8 Co1 70(2) . . ? C7 C8 Co1 71(2) . . ? C16 C8 Co1 135(3) . . ? C10 C9 C8 113(4) . . ? C10 C9 C21 129(3) . . ? C8 C9 C21 117(3) . . ? C10 C9 Co1 74(2) . . ? C8 C9 Co1 68(2) . . ? C21 C9 Co1 135(3) . . ? C9 C10 C26 130(3) . . ? C9 C10 C6 104(3) . . ? C26 C10 C6 125(3) . . ? C9 C10 Co1 67(2) . . ? C26 C10 Co1 120(2) . . ? C6 C10 Co1 74(2) . . ? C12 C11 C15 124(4) . . ? C12 C11 C7 122(4) . . ? C15 C11 C7 114(4) . . ? C13 C12 C11 117(4) . . ? N1 C13 C12 122(4) . . ? N1 C14 C15 123(4) . . ? C11 C15 C14 114(4) . . ? C20 C16 C17 120(3) . . ? C20 C16 C8 120(3) . . ? C17 C16 C8 119(3) . . ? C18 C17 C16 117(3) . . ? N2 C18 C17 123(3) . . ? N2 C19 C20 119(3) . . ? C16 C20 C19 119(3) . . ? C22 C21 C25 116(3) . . ? C22 C21 C9 121(3) . . ? C25 C21 C9 123(3) . . ? C21 C22 C23 122(4) . . ? N3 C23 C22 120(3) . . ? N3 C24 C25 122(3) . . ? C24 C25 C21 118(3) . . ? C27 C26 C30 119(4) . . ? C27 C26 C10 119(4) . . ? C30 C26 C10 122(4) . . ? C26 C27 C28 122(4) . . ? N4 C28 C27 115(3) . . ? N4 C29 C30 118(3) . . ? C26 C30 C29 121(4) . . ? O3 C31 O1 120(4) . . ? O3 C31 C32 124(4) . . ? O1 C31 C32 115(4) . . ? O4 C32 O2 133(4) . . ? O4 C32 C31 115(4) . . ? O2 C32 C31 112(4) . . ? C38 C33 C34 127(5) . . ? C38 C33 C42 102(5) . . ? C34 C33 C42 131(6) . . ? C38 C33 Ru1 74(3) . . ? C34 C33 Ru1 75(3) . . ? C42 C33 Ru1 124(4) . . ? C35 C34 C33 116(5) . . ? C35 C34 Ru1 68(3) . . ? C33 C34 Ru1 68(3) . . ? C34 C35 C36 121(5) . . ? C34 C35 Ru1 76(3) . . ? C36 C35 Ru1 71(3) . . ? C37 C36 C35 119(4) . . ? C37 C36 C39 124(5) . . ? C35 C36 C39 116(5) . . ? C37 C36 Ru1 70(2) . . ? C35 C36 Ru1 70(3) . . ? C39 C36 Ru1 119(3) . . ? C36 C37 C38 121(4) . . ? C36 C37 Ru1 72(3) . . ? C38 C37 Ru1 73(3) . . ? C33 C38 C37 116(5) . . ? C33 C38 Ru1 70(3) . . ? C37 C38 Ru1 68(3) . . ? C41 C39 C36 109(6) . . ? C41 C39 C40 118(6) . . ? C36 C39 C40 88(4) . . ? C44 C43 C48 120(4) . . ? C44 C43 C49 125(4) . . ? C48 C43 C49 115(4) . . ? C44 C43 Ru2 73(3) . . ? C48 C43 Ru2 69(2) . . ? C49 C43 Ru2 123(3) . . ? C43 C44 C45 117(4) . . ? C43 C44 Ru2 69(3) . . ? C45 C44 Ru2 68(2) . . ? C46 C45 C44 121(4) . . ? C46 C45 Ru2 72(2) . . ? C44 C45 Ru2 73(2) . . ? C47 C46 C45 122(4) . . ? C47 C46 C52 116(4) . . ? C45 C46 C52 120(4) . . ? C47 C46 Ru2 71(3) . . ? C45 C46 Ru2 69(2) . . ? C52 C46 Ru2 121(3) . . ? C48 C47 C46 115(4) . . ? C48 C47 Ru2 68(2) . . ? C46 C47 Ru2 71(3) . . ? C47 C48 C43 126(4) . . ? C47 C48 Ru2 74(3) . . ? C43 C48 Ru2 72(2) . . ? C43 C49 C50 114(5) . . ? C43 C49 C51 112(5) . . ? C50 C49 C51 99(5) . . ? O5 C53 O7 121(4) . . ? O5 C53 C54 122(4) . . ? O7 C53 C54 117(4) . . ? O6 C54 O8 127(4) . . ? O6 C54 C53 115(4) . . ? O8 C54 C53 118(4) . . ? C56 C55 C60 118(4) . . ? C56 C55 C61 115(5) . . ? C60 C55 C61 126(4) . . ? C56 C55 Ru3 69(3) . . ? C60 C55 Ru3 71(2) . . ? C61 C55 Ru3 126(3) . . ? C55 C56 C57 120(4) . . ? C55 C56 Ru3 74(3) . . ? C57 C56 Ru3 70(2) . . ? C56 C57 C58 123(4) . . ? C56 C57 Ru3 71(2) . . ? C58 C57 Ru3 72(2) . . ? C57 C58 C59 116(4) . . ? C57 C58 C64 121(4) . . ? C59 C58 C64 122(4) . . ? C57 C58 Ru3 69(2) . . ? C59 C58 Ru3 70(2) . . ? C64 C58 Ru3 123(3) . . ? C60 C59 C58 119(4) . . ? C60 C59 Ru3 72(2) . . ? C58 C59 Ru3 70(2) . . ? C59 C60 C55 123(4) . . ? C59 C60 Ru3 70(2) . . ? C55 C60 Ru3 71(2) . . ? C55 C61 C62 112(5) . . ? C55 C61 C63 103(4) . . ? C62 C61 C63 96(4) . . ? C66 C65 C70 122(4) . . ? C66 C65 C71 117(4) . . ? C70 C65 C71 119(4) . . ? C66 C65 Ru4 71(2) . . ? C70 C65 Ru4 70(2) . . ? C71 C65 Ru4 124(3) . . ? C65 C66 C67 118(4) . . ? C65 C66 Ru4 72(2) . . ? C67 C66 Ru4 66(2) . . ? C66 C67 C68 121(4) . . ? C66 C67 Ru4 76(2) . . ? C68 C67 Ru4 70(2) . . ? C69 C68 C67 116(4) . . ? C69 C68 C74 129(4) . . ? C67 C68 C74 116(4) . . ? C69 C68 Ru4 74(3) . . ? C67 C68 Ru4 66(2) . . ? C74 C68 Ru4 128(3) . . ? C68 C69 C70 121(4) . . ? C68 C69 Ru4 70(3) . . ? C70 C69 Ru4 70(2) . . ? C65 C70 C69 122(4) . . ? C65 C70 Ru4 73(2) . . ? C69 C70 Ru4 72(2) . . ? C72 C71 C65 117(4) . . ? C72 C71 C73 112(4) . . ? C65 C71 C73 104(4) . . ? O10 S1 O11 116.7(19) . . ? O10 S1 O12 115.6(18) . . ? O11 S1 O12 117.1(19) . . ? O10 S1 C75 98(3) . . ? O11 S1 C75 101(3) . . ? O12 S1 C75 104(3) . . ? F1 C75 F3 140(9) . . ? F1 C75 F2 114(8) . . ? F3 C75 F2 103(7) . . ? F1 C75 S1 102(6) . . ? F3 C75 S1 95(5) . . ? F2 C75 S1 89(4) . . ? O14 S2 O13 117(2) . . ? O14 S2 O15 119(2) . . ? O13 S2 O15 112(2) . . ? O14 S2 C76 104(3) . . ? O13 S2 C76 101(3) . . ? O15 S2 C76 100(3) . . ? F6 C76 F4 120(6) . . ? F6 C76 F5 110(5) . . ? F4 C76 F5 99(5) . . ? F6 C76 S2 112(5) . . ? F4 C76 S2 109(4) . . ? F5 C76 S2 105(4) . . ? O16 S3 O18 114(2) . . ? O16 S3 O17 115(3) . . ? O18 S3 O17 120(3) . . ? O16 S3 C77 98(2) . . ? O18 S3 C77 110.1(19) . . ? O17 S3 C77 95(2) . . ? F7 C77 F8 115(3) . . ? F7 C77 F9 121(4) . . ? F8 C77 F9 111(3) . . ? F7 C77 S3 106(3) . . ? F8 C77 S3 107(3) . . ? F9 C77 S3 94(2) . . ? O19 S4 O21 114(3) . . ? O19 S4 O20 113(3) . . ? O21 S4 O20 116(3) . . ? O19 S4 C78 100(3) . . ? O21 S4 C78 119(2) . . ? O20 S4 C78 91(2) . . ? F10 C78 F11 117(4) . . ? F10 C78 F12 120(4) . . ? F11 C78 F12 110(4) . . ? F10 C78 S4 105(3) . . ? F11 C78 S4 108(3) . . ? F12 C78 S4 93(2) . . ? C13 N1 C14 120(3) . . ? C13 N1 Ru4 125(3) . 3_656 ? C14 N1 Ru4 116(3) . 3_656 ? C19 N2 C18 121(3) . . ? C19 N2 Ru1 119(3) . . ? C18 N2 Ru1 119(2) . . ? C24 N3 C23 121(3) . . ? C24 N3 Ru2 121(3) . . ? C23 N3 Ru2 118(3) . . ? C28 N4 C29 125(3) . . ? C28 N4 Ru3 112(3) . . ? C29 N4 Ru3 122(2) . . ? _refine_diff_density_max 1.958 _refine_diff_density_min -0.901 _refine_diff_density_rms 0.218 _shelx_res_file ; rjy10.res created by SHELXL-2014/7 TITL rjy10 in P2(1)/n CELL 0.71073 14.4720 25.4897 26.2067 90.000 93.014 90.000 ZERR 4.00 0.0046 0.0087 0.0082 0.000 0.020 0.000 LATT 1 SYMM 0.5-X, 0.5+Y, 0.5-Z SFAC C N O Co Ru S F UNIT 316 16 92 4 16 16 48 L.S. 4 ACTA BOND FMAP 2 PLAN 30 SADI C78 F10 C78 F11 C78 F12 DFIX 1.8 S4 C78 TEMP 23.000 WGHT 0.100000 0.516466 FVAR 0.04622 MOLE 1 RU1 5 0.516430 -0.188471 0.219811 11.00000 0.07568 RU2 5 0.385078 0.011801 0.185996 11.00000 0.06907 RU3 5 0.122510 0.188786 0.500020 11.00000 0.06422 RU4 5 0.392838 0.300055 0.410809 11.00000 0.06425 CO1 4 0.300686 -0.083962 0.464986 11.00000 0.05416 O1 3 0.392978 -0.145414 0.205222 11.00000 0.06088 O2 3 0.561885 -0.113976 0.215553 11.00000 0.07573 O3 3 0.335949 -0.067443 0.187422 11.00000 0.05177 O4 3 0.507997 -0.027951 0.201749 11.00000 0.06565 O5 3 0.161086 0.210046 0.426963 11.00000 0.05028 O6 3 0.231729 0.241775 0.518319 11.00000 0.06369 O7 3 0.275974 0.254725 0.390193 11.00000 0.05979 O8 3 0.331639 0.294173 0.481825 11.00000 0.06581 O9 3 0.436340 -0.030925 0.551567 11.00000 0.05819 C1 1 0.180807 -0.118363 0.437513 11.00000 0.04202 C2 1 0.159632 -0.071794 0.462515 11.00000 0.05382 C3 1 0.199973 -0.082479 0.512046 11.00000 0.05294 C4 1 0.238096 -0.129205 0.514952 11.00000 0.06927 C5 1 0.227575 -0.151546 0.469166 11.00000 0.05886 C6 1 0.418181 -0.044494 0.506558 11.00000 0.05539 C7 1 0.436511 -0.095623 0.483885 11.00000 0.04251 C8 1 0.416834 -0.090195 0.429202 11.00000 0.04507 C9 1 0.377410 -0.039262 0.421305 11.00000 0.05028 C10 1 0.368202 -0.011552 0.465923 11.00000 0.02820 C11 1 0.475975 -0.142473 0.512780 11.00000 0.05218 C12 1 0.523435 -0.137391 0.560350 11.00000 0.05154 C13 1 0.554264 -0.182557 0.583272 11.00000 0.05419 C14 1 0.496940 -0.234333 0.515259 11.00000 0.07535 C15 1 0.461526 -0.190533 0.487526 11.00000 0.04870 C16 1 0.447379 -0.121688 0.386371 11.00000 0.04513 C17 1 0.381247 -0.152679 0.357741 11.00000 0.04304 C18 1 0.408744 -0.175150 0.313119 11.00000 0.04360 C19 1 0.557826 -0.140670 0.322308 11.00000 0.06536 C20 1 0.534864 -0.116449 0.370563 11.00000 0.04351 C21 1 0.369106 -0.020538 0.368708 11.00000 0.04317 C22 1 0.439011 0.007372 0.348614 11.00000 0.05180 C23 1 0.437430 0.021380 0.296470 11.00000 0.05355 C24 1 0.296056 -0.017595 0.282622 11.00000 0.05333 C25 1 0.291421 -0.032398 0.334356 11.00000 0.04163 C26 1 0.317402 0.035983 0.475361 11.00000 0.04575 C27 1 0.259177 0.055785 0.437164 11.00000 0.06838 C28 1 0.207419 0.102937 0.443839 11.00000 0.04909 C29 1 0.277623 0.108399 0.529047 11.00000 0.04665 C30 1 0.326349 0.062332 0.521359 11.00000 0.05114 C31 1 0.403436 -0.094740 0.195750 11.00000 0.05799 C32 1 0.499840 -0.074289 0.205340 11.00000 0.06811 C33 1 0.487126 -0.271241 0.218481 11.00000 0.10895 C34 1 0.574930 -0.267179 0.243467 11.00000 0.10429 C35 1 0.637620 -0.236927 0.219417 11.00000 0.11828 C36 1 0.616541 -0.216961 0.168444 11.00000 0.07911 C37 1 0.528756 -0.223973 0.146770 11.00000 0.06946 C38 1 0.460765 -0.253270 0.172294 11.00000 0.10922 C39 1 0.698293 -0.172297 0.144542 11.00000 0.20058 C40 1 0.723280 -0.222927 0.095248 11.00000 0.20140 C41 1 0.765523 -0.162321 0.181715 11.00000 0.16945 C42 1 0.397150 -0.294975 0.235921 11.00000 0.19452 C43 1 0.271555 0.043649 0.139750 11.00000 0.06224 C44 1 0.293674 0.080480 0.177735 11.00000 0.08626 C45 1 0.389728 0.095631 0.184472 11.00000 0.07630 C46 1 0.455918 0.076747 0.150616 11.00000 0.08295 C47 1 0.433225 0.038567 0.112703 11.00000 0.08977 C48 1 0.340553 0.024221 0.109094 11.00000 0.05791 C49 1 0.179108 0.016534 0.132588 11.00000 0.12909 C50 1 0.109996 0.031495 0.173618 11.00000 0.17184 C51 1 0.120908 0.037943 0.082420 11.00000 0.17519 C52 1 0.559748 0.086625 0.162035 11.00000 0.13936 C53 1 0.230006 0.241273 0.430995 11.00000 0.05570 C54 1 0.267502 0.260475 0.481347 11.00000 0.05958 C55 1 0.056865 0.201115 0.572018 11.00000 0.08536 C56 1 0.026210 0.236774 0.536846 11.00000 0.06201 C57 1 -0.011726 0.220137 0.488861 11.00000 0.07709 C58 1 -0.015680 0.167010 0.473552 11.00000 0.06195 C59 1 0.019615 0.129112 0.511107 11.00000 0.05762 C60 1 0.050707 0.146914 0.559123 11.00000 0.06856 C61 1 0.102583 0.224033 0.619895 11.00000 0.09110 C62 1 0.177440 0.189077 0.643096 11.00000 0.19895 C63 1 0.029137 0.212558 0.661681 11.00000 0.18488 C64 1 -0.040994 0.152062 0.420362 11.00000 0.07669 C65 1 0.392404 0.333477 0.333650 11.00000 0.05330 C66 1 0.343072 0.365879 0.363969 11.00000 0.06356 C67 1 0.383714 0.380640 0.410587 11.00000 0.07407 C68 1 0.484815 0.363551 0.427150 11.00000 0.09121 C69 1 0.526591 0.333182 0.394227 11.00000 0.06051 C70 1 0.479300 0.315388 0.348457 11.00000 0.07427 C71 1 0.340369 0.309070 0.286924 11.00000 0.08147 C72 1 0.370912 0.256978 0.271317 11.00000 0.09222 C73 1 0.348211 0.350794 0.243817 11.00000 0.10458 C74 1 0.524347 0.384493 0.482876 11.00000 0.13086 MOLE 2 S1 6 0.102017 0.379645 0.441401 11.00000 0.08987 O10 3 0.111108 0.324134 0.442561 11.00000 0.08851 O11 3 0.184227 0.409331 0.451339 11.00000 0.11101 O12 3 0.032341 0.401079 0.401829 11.00000 0.09759 C75 1 0.037155 0.388862 0.510609 11.00000 0.19269 F1 7 0.097759 0.378615 0.540507 11.00000 0.21358 F2 7 0.027541 0.446921 0.499314 11.00000 0.19803 F3 7 -0.043621 0.369832 0.492822 11.00000 0.21255 S2 6 0.274477 0.718945 0.386082 11.00000 0.09947 O13 3 0.280012 0.683444 0.344791 11.00000 0.14717 O14 3 0.352680 0.725264 0.417379 11.00000 0.12419 O15 3 0.219861 0.764115 0.372582 11.00000 0.11953 C76 1 0.193712 0.683173 0.426493 11.00000 0.14532 F4 7 0.237673 0.640885 0.446792 11.00000 0.14903 F5 7 0.188453 0.713617 0.470853 11.00000 0.13349 F6 7 0.114318 0.677937 0.404730 11.00000 0.14192 S3 6 0.599431 0.173004 0.303753 11.00000 0.14980 O16 3 0.609275 0.204580 0.347193 11.00000 0.18781 O17 3 0.642025 0.195790 0.254693 11.00000 0.21429 O18 3 0.512573 0.144605 0.299075 11.00000 0.16266 C77 1 0.695038 0.127584 0.318606 11.00000 0.27139 F7 7 0.767044 0.155281 0.321748 11.00000 0.17202 F8 7 0.693385 0.093041 0.283594 11.00000 0.17940 F9 7 0.660112 0.109729 0.358615 11.00000 0.20636 SAME S3 O16 O17 O18 C77 F7 F8 F9 S4 6 -0.018052 -0.007585 0.377706 11.00000 0.23321 O19 3 0.037012 0.025180 0.409009 11.00000 0.23752 O20 3 0.039088 -0.054986 0.353937 11.00000 0.32133 O21 3 -0.105890 -0.021213 0.398415 11.00000 0.23491 C78 1 -0.018331 0.028266 0.318161 11.00000 1.16101 F10 7 -0.079453 0.063027 0.321838 11.00000 0.37802 F11 7 -0.030739 -0.004473 0.282107 11.00000 0.55877 F12 7 0.066777 0.039961 0.324423 11.00000 0.29947 C102 1 0.692774 0.977096 0.320420 11.00000 0.15694 N1 2 0.548572 -0.229560 0.559542 11.00000 0.06153 N2 2 0.493401 -0.168457 0.295853 11.00000 0.04680 N3 2 0.368417 0.005992 0.265203 11.00000 0.04504 N4 2 0.221437 0.126646 0.489775 11.00000 0.04373 O31 3 0.733491 0.934003 0.352954 11.00000 0.17445 O32 3 0.555525 0.718374 0.375069 11.00000 0.31587 HKLF 4 REM rjy10 in P2(1)/n REM R1 = 0.1299 for 3123 Fo > 4sig(Fo) and 0.1817 for all 4468 data REM 509 parameters refined using 32 restraints END WGHT 0.2000 0.0000 REM Highest difference peak 1.958, deepest hole -0.901, 1-sigma level 0.218 Q1 1 0.3278 0.0172 0.1897 11.00000 0.05 1.96 Q2 1 0.4376 0.0069 0.1795 11.00000 0.05 1.60 Q3 1 0.4763 -0.2022 0.2227 11.00000 0.05 1.59 Q4 1 0.5745 -0.1736 0.2175 11.00000 0.05 1.53 Q5 1 0.0737 0.1952 0.4772 11.00000 0.05 1.34 Q6 1 0.2258 -0.3737 0.1911 11.00000 0.05 1.18 Q7 1 0.1581 0.1924 0.5269 11.00000 0.05 1.16 Q8 1 0.0654 -0.0190 0.2992 11.00000 0.05 1.14 Q9 1 -0.2078 0.4522 0.4534 11.00000 0.05 1.10 Q10 1 0.7659 0.1722 0.1839 11.00000 0.05 1.04 Q11 1 0.3948 0.2832 0.3961 11.00000 0.05 1.03 Q12 1 0.5914 0.1857 0.2774 11.00000 0.05 1.02 Q13 1 -0.0773 -0.0735 0.3033 11.00000 0.05 1.02 Q14 1 0.2972 0.4029 0.5698 11.00000 0.05 0.99 Q15 1 -0.0003 0.1001 0.3042 11.00000 0.05 0.96 Q16 1 0.3987 0.3224 0.4354 11.00000 0.05 0.96 Q17 1 0.7103 0.4732 0.4274 11.00000 0.05 0.87 Q18 1 0.1769 0.0774 0.3153 11.00000 0.05 0.86 Q19 1 0.5065 0.6896 0.3652 11.00000 0.05 0.86 Q20 1 0.6113 0.7341 0.3947 11.00000 0.05 0.84 Q21 1 0.0255 0.1856 0.5145 11.00000 0.05 0.83 Q22 1 0.7888 -0.0525 0.1229 11.00000 0.05 0.77 Q23 1 0.5580 -0.0932 0.2174 11.00000 0.05 0.77 Q24 1 -0.0533 0.0209 0.2883 11.00000 0.05 0.76 Q25 1 0.8240 0.1105 0.1894 11.00000 0.05 0.75 Q26 1 -0.1558 -0.0187 0.1831 11.00000 0.05 0.74 Q27 1 0.2224 0.0593 0.1649 11.00000 0.05 0.72 Q28 1 0.3201 0.6752 0.3596 11.00000 0.05 0.69 Q29 1 0.3788 0.0416 0.1205 11.00000 0.05 0.69 Q30 1 0.7048 0.1410 0.2612 11.00000 0.05 0.67 ; _shelx_res_checksum 51870 _shelx_hkl_file ; -1 0 0 -0.27 0.11 1 0 0 0.71 0.40 1 0 0 -0.33 0.59 1 0 0 -0.22 0.16 1 0 0 -0.25 0.18 -2 0 0 240.60 12.44 -2 0 0 251.48 8.75 -2 0 0 253.35 8.77 -2 0 0 243.77 20.61 2 0 0 254.18 12.48 2 0 0 258.08 8.79 2 0 0 245.81 20.64 2 0 0 262.10 9.17 -3 0 0 -1.43 0.81 -3 0 0 1.86 2.66 -3 0 0 1.01 0.82 3 0 0 -0.92 0.90 3 0 0 -1.03 0.79 3 0 0 -2.41 2.89 -4 0 0 9.03 3.73 -4 0 0 3.06 1.09 -4 0 0 0.81 2.44 -4 0 0 3.91 1.06 4 0 0 3.94 1.32 4 0 0 3.88 1.06 4 0 0 -1.06 2.56 4 0 0 -0.99 3.88 -5 0 0 0.86 1.18 -5 0 0 -0.05 2.83 -5 0 0 -1.28 4.16 -5 0 0 -0.13 1.13 5 0 0 0.05 1.06 5 0 0 -3.83 1.43 5 0 0 -4.12 4.37 5 0 0 -4.10 2.74 -6 0 0 -0.34 3.10 -6 0 0 4.25 1.41 -6 0 0 4.56 4.47 6 0 0 5.25 4.42 6 0 0 3.75 2.96 6 0 0 3.83 1.77 -7 0 0 2.55 3.81 -7 0 0 2.31 2.38 7 0 0 21.32 6.07 -8 0 0 120.92 5.62 -8 0 0 118.91 8.52 -8 0 0 114.96 6.29 8 0 0 109.35 6.09 -9 0 0 -3.41 2.66 -9 0 0 -5.02 4.78 -9 0 0 -5.22 1.75 9 0 0 -7.37 2.60 -10 0 0 55.30 5.18 -10 0 0 68.41 7.77 -10 0 0 68.88 4.34 10 0 0 59.41 5.00 -11 0 0 1.27 5.92 -11 0 0 0.19 2.13 -11 0 0 -5.15 3.20 -11 1 0 3.06 2.10 -11 1 0 -2.90 3.21 10 -1 0 -5.46 3.03 -10 1 0 1.35 2.07 -10 1 0 -5.17 3.03 -10 1 0 4.29 5.64 9 -1 0 9.30 4.14 9 -1 0 -3.68 2.69 -9 1 0 -0.47 1.89 -9 1 0 -4.13 5.03 -9 1 0 -3.03 2.68 8 -1 0 12.97 4.18 -8 1 0 11.31 4.83 -8 1 0 4.60 2.06 -8 1 0 24.25 7.60 7 -1 0 12.69 2.49 7 -1 0 18.98 5.76 -7 1 0 9.96 2.11 -7 1 0 14.25 6.19 -7 1 0 21.25 4.50 6 -1 0 22.14 2.46 6 -1 0 22.48 3.82 -6 1 0 19.60 2.28 -6 1 0 14.71 5.09 -6 1 0 23.33 4.06 5 -1 0 1.45 3.03 5 -1 0 -1.17 1.41 5 -1 0 -5.10 4.02 -5 1 0 1.08 1.09 -5 1 0 -0.57 1.16 -5 1 0 -0.95 3.89 -5 1 0 1.26 3.09 4 -1 0 -3.20 2.61 4 -1 0 -0.05 1.19 4 -1 0 -4.51 3.46 -4 1 0 1.10 0.90 -4 1 0 -2.86 2.67 -4 1 0 1.24 3.47 -4 1 0 -0.52 0.99 3 -1 0 30.52 1.89 3 -1 0 30.90 3.22 -3 1 0 26.70 1.95 -3 1 0 30.52 1.87 -3 1 0 27.98 3.15 2 -1 0 32.17 2.34 2 -1 0 29.79 1.55 2 -1 0 28.88 1.51 -2 1 0 32.86 2.31 -2 1 0 27.47 1.48 0 -1 0 0.01 0.03 0 -1 0 0.01 0.05 0 1 0 0.02 0.03 -2 -1 0 21.93 3.53 -2 -1 0 28.44 1.34 -2 -1 0 31.15 1.53 2 1 0 28.85 1.47 2 1 0 21.03 3.59 2 1 0 27.63 1.37 -3 -1 0 31.54 4.92 -3 -1 0 32.79 2.17 -3 -1 0 30.92 1.83 3 1 0 29.40 1.84 3 1 0 31.41 2.01 -4 -1 0 1.94 3.59 -4 -1 0 -4.07 2.22 -4 -1 0 0.14 0.92 -4 -1 0 -0.32 1.44 4 1 0 -4.03 4.00 4 1 0 -0.76 0.87 4 1 0 -0.15 1.29 -5 -1 0 -0.06 1.67 -5 -1 0 2.09 4.20 -5 -1 0 0.26 1.09 -5 -1 0 -5.64 2.65 5 1 0 1.14 1.07 5 1 0 -0.67 1.51 -6 -1 0 22.88 5.60 -6 -1 0 22.88 2.52 -6 -1 0 18.25 2.12 -6 -1 0 21.49 3.60 6 1 0 19.96 2.49 6 1 0 19.28 5.75 -7 -1 0 16.60 6.35 -7 -1 0 9.61 2.58 -7 -1 0 11.62 4.10 -7 -1 0 12.48 1.95 7 1 0 15.66 6.24 7 1 0 13.32 2.39 -8 -1 0 4.04 1.98 -8 -1 0 4.83 4.24 -8 -1 0 -0.86 2.71 8 1 0 2.31 2.58 -9 -1 0 0.27 1.92 -9 -1 0 0.90 4.63 -9 -1 0 -2.70 2.70 9 1 0 -3.92 2.62 -10 -1 0 7.63 5.18 -10 -1 0 -0.38 3.10 -10 -1 0 1.57 2.05 10 1 0 -2.01 3.14 -11 -1 0 1.79 3.42 -11 -1 0 3.73 2.14 -11 2 0 2.49 2.17 10 -2 0 -5.12 3.00 -10 2 0 0.70 2.05 -10 2 0 2.98 5.70 9 -2 0 40.09 4.11 -9 2 0 44.91 3.53 -9 2 0 41.21 6.64 8 -2 0 95.94 7.43 8 -2 0 71.59 4.98 -8 2 0 86.86 4.69 -8 2 0 86.06 7.83 7 -2 0 5.55 3.66 7 -2 0 -3.86 4.67 7 -2 0 0.94 1.94 -7 2 0 -2.41 5.21 -7 2 0 1.72 4.11 -7 2 0 -5.24 1.62 6 -2 0 0.28 1.50 6 -2 0 -3.64 2.97 -6 2 0 -1.22 1.29 -6 2 0 -6.37 3.40 5 -2 0 44.29 2.67 5 -2 0 44.30 2.93 5 -2 0 43.37 5.04 -5 2 0 40.48 2.62 -5 2 0 43.03 2.75 -5 2 0 40.92 5.22 4 -2 0 33.74 2.21 4 -2 0 30.07 4.24 4 -2 0 36.56 2.31 -4 2 0 29.44 4.36 -4 2 0 36.53 2.35 -4 2 0 31.75 2.13 3 -2 0 111.66 6.97 3 -2 0 132.41 4.86 3 -2 0 116.67 4.69 -3 2 0 119.39 4.72 -3 2 0 114.07 7.00 2 -2 0 48.11 2.10 2 -2 0 43.65 3.19 -2 2 0 40.08 3.13 -2 2 0 49.41 2.11 1 -2 0 51.41 3.00 1 -2 0 53.48 2.08 1 -2 0 51.14 2.07 -2 -2 0 37.33 1.88 -2 -2 0 36.19 1.72 2 2 0 38.61 1.85 2 2 0 34.39 1.71 -3 -2 0 115.91 4.69 -3 -2 0 104.35 4.24 3 2 0 105.26 4.52 3 2 0 107.91 4.29 -4 -2 0 31.28 6.23 -4 -2 0 32.93 2.06 -4 -2 0 33.51 2.54 4 2 0 35.77 2.44 4 2 0 30.24 2.07 -5 -2 0 44.99 7.39 -5 -2 0 43.87 2.57 -5 -2 0 41.93 3.06 5 2 0 41.61 2.60 5 2 0 31.56 7.78 5 2 0 44.23 2.98 -6 -2 0 -0.72 1.23 -6 -2 0 -0.11 2.73 -6 -2 0 -0.71 1.74 -6 -2 0 1.64 4.49 6 2 0 -4.43 4.77 6 2 0 -0.26 1.64 -7 -2 0 -0.92 2.17 -7 -2 0 -7.74 5.76 -7 -2 0 1.91 1.53 -7 -2 0 -4.06 3.55 7 2 0 1.13 2.10 7 2 0 5.90 5.52 -8 -2 0 81.25 4.29 -8 -2 0 79.86 6.78 -8 -2 0 78.50 5.17 8 2 0 81.52 5.11 -9 -2 0 36.34 6.01 -9 -2 0 36.96 3.20 -9 -2 0 40.52 4.42 9 2 0 34.54 3.99 -10 -2 0 7.01 5.11 -10 -2 0 4.04 1.99 -10 -2 0 1.89 3.12 10 2 0 -3.14 2.95 -11 -2 0 -2.46 1.99 10 -3 0 -0.27 2.97 -10 3 0 3.96 5.86 -10 3 0 3.12 2.13 9 -3 0 25.77 3.36 -9 3 0 27.32 6.18 -9 3 0 31.59 3.32 8 -3 0 10.24 4.24 8 -3 0 -1.77 2.19 -8 3 0 1.93 1.96 -8 3 0 7.85 4.92 7 -3 0 -2.33 1.85 7 -3 0 1.14 3.79 7 -3 0 -1.32 1.60 -7 3 0 4.77 4.38 -7 3 0 -1.57 1.56 6 -3 0 9.09 3.81 6 -3 0 12.98 1.87 6 -3 0 13.60 1.86 -6 3 0 11.55 1.79 -6 3 0 7.88 4.04 5 -3 0 31.21 2.53 5 -3 0 31.77 2.50 5 -3 0 30.73 4.44 -5 3 0 33.11 4.59 -5 3 0 32.65 2.45 4 -3 0 6.13 1.34 4 -3 0 1.18 3.15 4 -3 0 6.77 1.30 -4 3 0 6.47 1.22 -4 3 0 6.80 3.30 3 -3 0 534.79 26.91 3 -3 0 577.85 19.61 3 -3 0 540.19 18.80 -3 3 0 526.30 26.91 -3 3 0 527.45 18.79 2 -3 0 90.27 5.19 2 -3 0 88.09 3.50 2 -3 0 80.55 3.49 -2 3 0 82.85 3.47 -2 3 0 84.01 5.20 1 -3 0 13.08 1.03 1 -3 0 12.23 0.89 1 -3 0 9.03 1.63 -1 3 0 13.30 0.98 0 -3 0 0.62 0.41 0 -3 0 -0.48 0.36 0 3 0 0.24 0.38 -1 -3 0 11.87 0.94 -1 -3 0 10.24 0.84 1 3 0 10.92 0.85 -2 -3 0 76.49 3.07 -2 -3 0 79.41 3.33 2 3 0 77.63 3.09 -3 -3 0 567.66 19.24 -3 -3 0 513.38 18.14 3 3 0 523.59 19.11 3 3 0 502.28 18.13 -4 -3 0 4.91 4.05 -4 -3 0 3.53 1.18 -4 -3 0 5.44 1.64 4 3 0 -0.50 4.61 4 3 0 5.25 1.45 4 3 0 5.64 1.13 -5 -3 0 27.13 2.30 -5 -3 0 33.49 2.90 5 3 0 29.91 2.63 5 3 0 28.35 2.24 -6 -3 0 14.42 3.13 -6 -3 0 9.63 4.88 -6 -3 0 9.25 1.66 -6 -3 0 6.55 2.09 6 3 0 11.67 2.04 6 3 0 1.66 5.47 -7 -3 0 -2.05 6.18 -7 -3 0 -1.21 1.50 -7 -3 0 -6.30 3.20 -7 -3 0 -0.26 2.09 7 3 0 -2.68 2.00 -8 -3 0 7.19 3.89 -8 -3 0 3.79 1.86 -8 -3 0 3.54 2.58 8 3 0 3.02 2.47 -9 -3 0 30.59 5.32 -9 -3 0 18.56 3.44 -9 -3 0 30.70 3.10 9 3 0 26.61 3.50 -10 -3 0 8.81 4.90 -10 -3 0 -3.22 3.13 -10 -3 0 1.82 1.99 10 3 0 0.91 3.21 10 -4 0 1.24 2.78 -10 4 0 -1.07 5.96 -10 4 0 -0.06 1.99 9 -4 0 0.28 2.42 -9 4 0 0.14 1.88 -9 4 0 4.34 5.48 8 -4 0 36.50 3.28 8 -4 0 36.88 6.01 8 -4 0 34.11 3.50 -8 4 0 35.04 3.17 -8 4 0 33.97 5.99 7 -4 0 85.21 4.71 7 -4 0 92.51 7.67 7 -4 0 85.80 4.63 -7 4 0 92.73 4.73 -7 4 0 83.04 7.87 6 -4 0 3.10 1.65 6 -4 0 2.23 1.58 6 -4 0 2.70 3.66 -6 4 0 1.94 4.14 5 -4 0 -5.55 3.26 5 -4 0 0.23 1.29 5 -4 0 -0.21 1.17 -5 4 0 0.49 3.70 4 -4 0 74.21 6.21 4 -4 0 78.55 3.69 4 -4 0 84.15 3.79 -4 4 0 75.98 3.68 -4 4 0 80.99 6.46 3 -4 0 13.25 1.58 3 -4 0 13.82 3.11 3 -4 0 13.45 1.54 -3 4 0 15.27 3.35 -3 4 0 12.96 1.42 2 -4 0 0.35 0.92 2 -4 0 1.88 0.82 -2 4 0 2.61 0.94 -2 4 0 2.92 2.31 1 -4 0 22.43 1.40 1 -4 0 20.69 1.46 -1 4 0 20.01 1.39 0 -4 0 75.00 2.99 0 -4 0 66.37 2.84 0 4 0 66.79 2.84 -1 -4 0 21.35 1.42 -1 -4 0 19.83 1.29 1 4 0 20.35 1.29 -3 -4 0 12.98 1.52 -3 -4 0 14.38 1.59 3 4 0 13.12 1.26 -4 -4 0 78.52 3.97 -4 -4 0 79.75 3.52 4 4 0 80.09 3.90 4 4 0 73.86 3.47 -5 -4 0 6.25 4.50 -5 -4 0 -0.35 1.18 -5 -4 0 0.29 1.69 5 4 0 -5.85 5.15 5 4 0 -0.26 1.43 5 4 0 0.05 1.06 -6 -4 0 -1.85 2.01 -6 -4 0 11.41 5.41 -6 -4 0 -1.25 1.61 6 4 0 2.56 1.88 6 4 0 11.97 5.96 -7 -4 0 81.59 4.30 -7 -4 0 86.63 5.17 -7 -4 0 86.54 6.53 7 4 0 82.98 4.79 -8 -4 0 29.56 3.58 -8 -4 0 34.72 9.09 -8 -4 0 39.52 4.91 -8 -4 0 31.11 2.96 8 4 0 35.20 3.67 -9 -4 0 0.32 4.03 -9 -4 0 0.15 2.89 -9 -4 0 3.01 1.98 9 4 0 0.36 2.66 -10 -4 0 -6.39 3.20 -10 -4 0 4.89 2.24 -10 -4 0 6.30 4.91 10 4 0 0.12 3.20 10 -5 0 3.41 2.77 -10 5 0 2.98 6.45 -10 5 0 1.35 2.12 9 -5 0 0.81 2.42 9 -5 0 3.26 2.09 -9 5 0 3.14 1.95 -9 5 0 2.76 5.88 8 -5 0 2.68 2.18 8 -5 0 2.88 2.02 -8 5 0 3.89 5.39 -8 5 0 3.44 1.99 7 -5 0 36.57 5.92 7 -5 0 26.98 3.08 7 -5 0 25.62 2.99 -7 5 0 30.92 3.21 -7 5 0 26.53 5.71 6 -5 0 23.69 4.70 6 -5 0 27.96 2.63 6 -5 0 23.83 2.57 -6 5 0 26.83 5.21 5 -5 0 6.80 3.52 5 -5 0 7.32 1.61 5 -5 0 7.73 1.53 -5 5 0 7.25 3.97 4 -5 0 2.89 1.15 4 -5 0 1.49 3.23 4 -5 0 3.90 1.24 -4 5 0 1.56 1.05 -4 5 0 3.78 3.67 3 -5 0 45.55 2.45 3 -5 0 42.28 2.56 3 -5 0 35.83 4.96 -3 5 0 43.79 2.49 -3 5 0 33.81 5.20 2 -5 0 21.51 3.19 2 -5 0 17.94 1.56 2 -5 0 17.31 1.76 -2 5 0 18.27 1.73 1 -5 0 165.37 6.34 1 -5 0 175.80 6.57 -1 5 0 167.71 6.32 0 -5 0 0.23 0.75 0 -5 0 -0.46 0.72 0 5 0 0.03 0.71 -3 -5 0 43.71 2.68 -3 -5 0 41.76 2.33 3 5 0 41.16 2.27 -4 -5 0 1.09 1.11 -4 -5 0 3.82 4.17 -4 -5 0 3.22 1.48 4 5 0 1.13 0.92 4 5 0 -0.26 4.80 -5 -5 0 11.64 4.65 -5 -5 0 5.39 1.82 -5 -5 0 7.18 1.48 5 5 0 6.10 1.73 5 5 0 5.46 1.23 -6 -5 0 23.06 2.46 -6 -5 0 21.98 2.74 6 5 0 27.70 2.93 -7 -5 0 18.97 3.05 -7 -5 0 24.68 2.69 7 5 0 26.57 3.27 -8 -5 0 -1.94 1.85 -8 -5 0 12.19 3.81 -8 -5 0 2.81 2.73 8 5 0 3.53 2.57 -9 -5 0 8.80 4.20 -9 -5 0 5.27 2.09 -9 -5 0 8.69 3.12 9 5 0 4.50 2.74 -10 -5 0 9.40 4.76 -10 -5 0 2.17 2.33 -10 -5 0 -2.00 3.30 10 5 0 0.61 3.17 10 -6 0 5.22 2.79 10 -6 0 4.62 2.48 -10 6 0 -0.96 6.60 -10 6 0 5.71 2.36 9 -6 0 10.20 2.44 9 -6 0 11.53 2.69 -9 6 0 12.80 2.47 -9 6 0 10.03 6.37 8 -6 0 134.03 6.14 8 -6 0 127.86 6.38 -8 6 0 124.04 6.19 -8 6 0 130.40 10.26 7 -6 0 2.30 1.75 7 -6 0 7.93 4.21 7 -6 0 2.22 1.96 -7 6 0 3.85 5.04 6 -6 0 5.21 1.73 6 -6 0 4.51 1.92 6 -6 0 0.05 3.94 -6 6 0 3.56 4.76 5 -6 0 2.93 3.51 5 -6 0 4.00 1.53 5 -6 0 4.06 1.49 -5 6 0 -0.02 3.94 4 -6 0 148.16 6.12 4 -6 0 148.74 6.14 4 -6 0 149.88 9.36 -4 6 0 140.46 9.51 3 -6 0 6.69 1.26 3 -6 0 9.61 3.38 3 -6 0 7.21 1.36 -3 6 0 7.13 3.62 -3 6 0 6.55 1.25 2 -6 0 247.80 9.19 2 -6 0 240.05 13.44 2 -6 0 252.08 9.44 -2 6 0 252.02 9.16 1 -6 0 312.49 11.34 1 -6 0 300.28 10.90 -1 6 0 295.50 10.86 0 -6 0 236.86 8.84 0 -6 0 230.64 8.46 0 6 0 225.14 8.42 -1 -6 0 287.89 10.81 -1 -6 0 314.21 11.43 1 6 0 308.68 10.82 -2 -6 0 244.12 9.49 -2 -6 0 257.77 10.09 -2 -6 0 269.65 22.52 2 6 0 241.95 9.43 2 6 0 306.64 23.18 -3 -6 0 8.01 1.52 -3 -6 0 11.62 4.29 -3 -6 0 7.27 1.22 3 6 0 6.32 1.06 3 6 0 5.59 4.96 -4 -6 0 139.95 6.31 -4 -6 0 143.53 5.78 -4 -6 0 144.27 14.47 4 6 0 158.09 15.20 4 6 0 139.87 5.71 -6 -6 0 1.23 1.66 -6 -6 0 5.84 2.23 -6 -6 0 -0.89 5.48 6 6 0 5.67 2.00 -7 -6 0 3.66 1.74 -7 -6 0 4.69 2.42 7 6 0 1.75 2.24 -8 -6 0 130.42 5.87 -8 -6 0 123.50 8.42 -8 -6 0 127.24 6.81 8 6 0 127.60 6.51 -9 -6 0 12.21 3.27 -9 -6 0 11.69 2.37 -9 -6 0 20.10 4.60 9 6 0 16.14 3.20 -10 -6 0 3.10 3.40 -10 -6 0 14.35 4.65 -10 -6 0 7.92 2.36 10 6 0 5.17 3.24 10 -7 0 4.22 2.61 10 -7 0 4.11 2.42 -10 7 0 -0.04 2.16 -10 7 0 1.56 6.86 9 -7 0 20.69 2.99 9 -7 0 22.05 2.85 -9 7 0 22.68 2.88 -9 7 0 21.55 7.03 8 -7 0 1.95 2.03 8 -7 0 -0.67 2.10 -8 7 0 -3.32 5.60 7 -7 0 5.05 1.86 7 -7 0 3.91 2.02 -7 7 0 7.80 5.24 6 -7 0 42.28 6.05 6 -7 0 35.63 3.09 6 -7 0 41.72 3.23 -6 7 0 48.28 6.75 5 -7 0 247.28 9.81 5 -7 0 242.97 14.16 -5 7 0 249.29 14.43 4 -7 0 2.08 3.25 4 -7 0 0.41 1.16 4 -7 0 -0.97 1.15 -4 7 0 -2.84 3.80 3 -7 0 73.85 6.38 3 -7 0 72.35 3.54 3 -7 0 70.43 3.63 2 -7 0 -0.81 1.02 2 -7 0 -0.79 1.02 2 -7 0 0.27 2.99 -2 7 0 -2.16 0.97 1 -7 0 116.98 4.91 1 -7 0 113.61 4.80 -1 7 0 108.11 4.72 0 -7 0 -0.66 0.99 0 -7 0 -0.37 0.99 0 7 0 -0.13 0.91 -3 -7 0 66.99 3.53 -3 -7 0 67.98 3.23 3 7 0 65.62 3.13 -4 -7 0 5.27 4.52 -4 -7 0 0.69 1.46 -4 -7 0 1.13 1.14 4 7 0 1.00 5.18 4 7 0 0.37 0.97 -5 -7 0 267.11 23.18 -5 -7 0 243.53 9.72 -5 -7 0 230.90 10.46 5 7 0 299.05 24.34 -6 -7 0 36.47 2.82 -6 -7 0 31.81 3.24 -6 -7 0 28.24 8.08 -7 -7 0 8.17 2.44 -7 -7 0 6.04 1.80 -8 -7 0 3.01 2.78 -8 -7 0 5.70 2.01 8 7 0 -0.98 2.51 -9 -7 0 24.97 4.81 -9 -7 0 26.23 3.00 -9 -7 0 20.11 3.52 9 7 0 17.77 3.35 -10 -7 0 14.22 4.48 -10 -7 0 0.60 2.22 -10 -7 0 4.91 3.34 10 7 0 3.85 3.11 -10 8 0 28.23 7.86 -10 8 0 16.51 2.91 9 -8 0 11.84 2.82 9 -8 0 12.78 2.58 -9 8 0 9.79 6.88 8 -8 0 5.98 2.13 8 -8 0 1.06 2.15 -8 8 0 -0.82 6.15 7 -8 0 -1.05 1.77 7 -8 0 4.22 2.11 -7 8 0 -1.01 5.37 6 -8 0 16.78 4.58 6 -8 0 13.80 2.15 6 -8 0 11.29 2.14 -6 8 0 11.78 5.53 5 -8 0 1.46 1.55 5 -8 0 3.02 1.71 5 -8 0 -2.28 3.54 -5 8 0 -0.01 4.45 4 -8 0 33.10 2.76 4 -8 0 35.58 2.66 4 -8 0 28.51 4.71 3 -8 0 16.78 3.83 3 -8 0 15.82 1.95 3 -8 0 17.87 2.13 2 -8 0 2.73 1.15 2 -8 0 3.59 1.21 2 -8 0 5.18 3.27 1 -8 0 34.68 2.39 1 -8 0 33.82 2.40 -1 8 0 34.40 2.34 0 -8 0 16.70 1.70 0 -8 0 15.74 1.90 0 8 0 15.11 1.79 -1 -8 0 14.69 3.95 2 8 0 23.27 5.77 -3 -8 0 16.43 1.97 -3 -8 0 8.90 4.45 -3 -8 0 14.60 1.64 3 8 0 16.02 1.79 -4 -8 0 31.67 2.48 -4 -8 0 31.05 2.78 4 8 0 34.82 9.19 -5 -8 0 3.20 5.12 -5 -8 0 4.39 1.53 -5 -8 0 2.49 1.83 5 8 0 -0.58 5.75 -6 -8 0 13.42 2.01 -6 -8 0 0.62 6.36 -7 -8 0 -0.36 1.67 -7 -8 0 3.72 2.33 -8 -8 0 4.74 2.71 -8 -8 0 2.88 1.94 -9 -8 0 14.86 3.32 -9 -8 0 14.00 2.51 -10 -8 0 18.89 2.99 -10 -8 0 15.68 3.70 9 -9 0 -0.17 2.45 9 -9 0 1.14 2.17 -9 9 0 -3.16 6.83 8 -9 0 1.18 2.34 8 -9 0 2.47 2.03 -8 9 0 1.65 6.26 7 -9 0 -0.48 1.89 7 -9 0 2.12 2.12 -7 9 0 5.15 5.94 6 -9 0 0.08 1.54 6 -9 0 0.22 1.55 -6 9 0 -0.28 5.11 5 -9 0 48.76 3.43 5 -9 0 45.06 3.21 5 -9 0 42.99 6.12 4 -9 0 35.39 2.78 4 -9 0 30.25 2.97 4 -9 0 26.62 4.92 3 -9 0 7.95 3.65 3 -9 0 6.42 1.49 3 -9 0 4.14 1.60 2 -9 0 38.78 5.08 2 -9 0 36.08 2.52 2 -9 0 35.02 2.56 1 -9 0 2.05 1.31 1 -9 0 2.94 1.31 0 -9 0 0.51 1.16 0 -9 0 1.35 1.26 -1 -9 0 1.38 1.23 -1 -9 0 1.22 1.39 -1 -9 0 1.20 3.91 -2 -9 0 36.14 2.69 -2 -9 0 36.81 2.47 -3 -9 0 7.54 1.79 -3 -9 0 7.17 1.47 -4 -9 0 32.47 2.61 -4 -9 0 31.17 2.95 -5 -9 0 40.72 3.37 -5 -9 0 41.52 3.02 -6 -9 0 -2.28 1.91 -6 -9 0 0.02 1.59 -7 -9 0 4.09 2.57 -7 -9 0 4.88 1.93 -8 -9 0 4.16 1.98 -8 -9 0 2.52 2.68 -9 -9 0 1.69 2.87 -9 -9 0 1.79 2.08 9 -10 0 3.51 2.64 9 -10 0 5.37 2.34 -9 10 0 2.01 6.97 8 -10 0 5.95 2.16 8 -10 0 2.67 2.38 -8 10 0 10.27 6.68 7 -10 0 3.06 2.11 7 -10 0 2.03 2.00 -7 10 0 3.37 5.84 6 -10 0 4.06 1.85 6 -10 0 1.19 1.78 5 -10 0 -0.93 1.61 5 -10 0 -0.96 1.54 4 -10 0 160.44 7.00 4 -10 0 162.94 6.97 4 -10 0 159.38 10.68 3 -10 0 -0.96 1.45 3 -10 0 4.29 3.68 3 -10 0 0.52 1.50 2 -10 0 29.28 2.56 2 -10 0 33.31 4.57 2 -10 0 30.89 2.66 1 -10 0 51.39 3.20 1 -10 0 54.53 3.23 0 -10 0 330.32 12.89 0 -10 0 335.81 12.36 -1 -10 0 47.82 3.00 -1 -10 0 50.44 3.21 -2 -10 0 12.41 4.62 -3 -10 0 28.37 6.91 -4 -10 0 48.55 9.45 4 10 0 72.24 10.54 -5 -10 0 -3.81 1.81 -5 -10 0 1.32 6.00 -5 -10 0 -2.62 1.46 -6 -10 0 -1.84 1.65 -6 -10 0 -2.65 2.01 -7 -10 0 4.89 1.92 -7 -10 0 4.07 2.44 -8 -10 0 3.66 1.95 -8 -10 0 4.83 2.72 -9 -10 0 -0.48 3.00 -9 -10 0 4.31 2.35 -9 11 0 1.78 7.11 8 -11 0 -1.10 1.99 8 -11 0 -1.14 2.26 7 -11 0 4.73 2.15 7 -11 0 5.88 2.12 6 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3 67.61 6.81 -7 6 -3 18.84 5.39 7 -6 3 15.73 2.26 7 -6 3 17.54 2.37 -8 6 -3 -1.63 5.27 8 -6 3 2.61 1.80 8 -6 3 -0.91 1.99 -9 6 -3 0.71 1.95 -9 6 -3 8.87 6.12 9 -6 3 5.70 2.48 9 -6 3 -0.44 1.95 -10 6 -3 2.88 1.90 -10 6 -3 1.68 6.31 10 -6 3 3.07 2.75 10 -6 3 1.58 2.23 10 5 -3 -0.52 3.00 -10 -5 3 -5.01 3.06 -10 -5 3 -1.97 2.28 -10 -5 3 0.96 4.34 9 5 -3 5.48 2.89 -9 -5 3 10.17 2.37 -9 -5 3 7.30 3.16 -9 -5 3 7.92 4.10 8 5 -3 276.42 11.44 -8 -5 3 281.79 10.69 -8 -5 3 249.57 26.10 -8 -5 3 275.94 14.53 -8 -5 3 252.96 11.56 7 5 -3 3.67 2.15 -7 -5 3 2.47 2.72 -7 -5 3 -0.38 1.72 -7 -5 3 0.61 2.36 6 5 -3 -6.24 5.74 6 5 -3 7.85 2.02 -6 -5 3 7.14 1.76 -6 -5 3 -1.40 5.72 -6 -5 3 2.66 2.19 -5 -5 3 7.40 1.99 4 5 -3 8.32 1.74 -4 -5 3 9.82 1.55 -4 -5 3 10.50 1.97 3 5 -3 27.43 1.95 3 5 -3 25.19 2.24 -3 -5 3 26.36 2.11 -3 -5 3 25.11 2.44 2 5 -3 20.50 1.68 -2 -5 3 23.40 2.04 -2 -5 3 21.70 1.78 1 5 -3 4.79 0.88 -1 -5 3 5.12 1.01 -1 -5 3 5.09 1.13 0 5 -3 162.75 6.15 0 -5 3 171.96 6.43 0 -5 3 161.53 8.89 0 -5 3 162.28 6.22 -1 5 -3 0.56 0.77 -1 5 -3 2.36 2.52 1 -5 3 2.39 0.96 1 -5 3 0.48 0.80 1 -5 3 2.08 2.21 -2 5 -3 230.20 8.48 -2 5 -3 231.45 12.65 2 -5 3 222.38 8.50 2 -5 3 229.97 12.56 2 -5 3 237.58 8.67 -3 5 -3 9.55 1.22 -3 5 -3 9.35 3.60 3 -5 3 7.74 1.12 3 -5 3 7.50 3.51 3 -5 3 7.57 1.33 -4 5 -3 58.81 6.10 -4 5 -3 58.62 3.11 4 -5 3 57.94 5.98 4 -5 3 61.57 3.25 4 -5 3 61.59 3.07 -5 5 -3 -1.93 3.69 5 -5 3 1.63 1.29 5 -5 3 -1.92 3.30 5 -5 3 2.18 1.24 -6 5 -3 2.46 4.41 6 -5 3 5.24 4.02 6 -5 3 1.66 1.58 6 -5 3 1.29 1.57 -7 5 -3 13.66 5.07 7 -5 3 8.44 1.96 7 -5 3 6.40 1.92 -8 5 -3 13.07 5.50 -8 5 -3 10.91 2.06 8 -5 3 8.54 2.25 8 -5 3 10.62 2.17 -9 5 -3 2.19 5.64 -9 5 -3 3.86 1.86 9 -5 3 1.25 1.97 9 -5 3 1.30 2.43 -10 5 -3 -2.25 6.18 -10 5 -3 2.50 1.93 10 -5 3 -1.96 2.76 10 -5 3 1.81 2.05 10 4 -3 -1.43 2.90 -10 -4 3 -3.79 3.01 -10 -4 3 1.52 2.23 -10 -4 3 3.91 4.66 9 4 -3 16.33 3.28 -9 -4 3 21.30 2.70 -9 -4 3 10.47 4.49 -9 -4 3 18.21 3.41 8 4 -3 -4.58 2.62 -8 -4 3 -1.75 2.12 -8 -4 3 -4.15 2.72 7 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5 -4 3 5.30 1.27 5 -4 3 4.71 1.31 5 -4 3 2.93 3.48 -6 4 -3 131.59 9.14 6 -4 3 126.95 5.50 6 -4 3 121.74 5.56 6 -4 3 129.05 9.08 -7 4 -3 21.11 5.34 7 -4 3 23.53 5.17 7 -4 3 15.33 2.20 7 -4 3 18.35 2.32 -8 4 -3 2.15 1.68 -8 4 -3 1.81 5.00 8 -4 3 -1.01 1.73 8 -4 3 1.09 2.16 -9 4 -3 2.16 1.80 -9 4 -3 1.80 5.73 9 -4 3 2.76 2.01 9 -4 3 -6.11 2.39 -10 4 -3 4.89 1.96 -10 4 -3 1.98 6.07 10 -4 3 5.86 3.02 10 3 -3 0.27 2.97 -10 -3 3 1.45 2.07 -10 -3 3 0.54 4.92 -10 -3 3 4.39 3.13 9 3 -3 11.06 3.07 -9 -3 3 8.64 4.63 -9 -3 3 13.95 2.41 -9 -3 3 9.97 3.28 8 3 -3 43.62 4.07 -8 -3 3 41.66 4.23 -8 -3 3 43.17 3.56 -8 -3 3 58.18 5.38 7 3 -3 6.42 2.24 -7 -3 3 5.62 2.44 -7 -3 3 4.22 3.28 -7 -3 3 6.82 1.87 6 3 -3 38.92 9.21 6 3 -3 43.98 3.38 -6 -3 3 47.23 3.66 -6 -3 3 46.87 3.14 -6 -3 3 35.42 4.23 5 3 -3 0.47 1.62 -5 -3 3 0.87 1.33 -5 -3 3 0.05 1.87 4 3 -3 310.82 11.70 4 3 -3 291.23 11.05 -4 -3 3 303.83 11.78 -4 -3 3 312.38 11.10 3 3 -3 -3.29 3.90 3 3 -3 -0.67 1.10 3 3 -3 0.62 0.81 -3 -3 3 0.71 1.07 -3 -3 3 2.34 1.38 2 3 -3 109.57 4.52 2 3 -3 106.86 4.28 -2 -3 3 109.97 4.33 -2 -3 3 111.85 4.63 1 3 -3 17.11 1.23 1 3 -3 16.70 1.20 -1 -3 3 16.97 1.27 -1 -3 3 17.52 1.32 0 3 -3 76.30 4.41 0 3 -3 72.39 3.02 0 -3 3 81.22 3.13 0 -3 3 77.70 4.36 0 -3 3 82.35 3.15 -1 3 -3 242.53 12.50 -1 3 -3 248.60 8.67 1 -3 3 239.86 12.49 1 -3 3 237.85 8.68 1 -3 3 256.93 8.95 -2 3 -3 1.58 0.71 -2 3 -3 1.90 2.15 2 -3 3 1.03 0.56 2 -3 3 1.01 0.76 2 -3 3 1.40 2.12 -3 3 -3 18.85 1.55 -3 3 -3 17.85 3.54 3 -3 3 16.53 1.43 3 -3 3 15.52 3.51 3 -3 3 18.41 1.68 -4 3 -3 1.26 3.27 -4 3 -3 3.42 0.98 4 -3 3 1.54 1.05 4 -3 3 0.09 1.04 4 -3 3 -1.69 3.16 -5 3 -3 -0.50 0.95 -5 3 -3 -0.53 3.37 -5 3 -3 -1.13 3.71 5 -3 3 0.02 1.17 5 -3 3 -3.47 3.23 5 -3 3 -0.84 1.21 -6 3 -3 -1.57 4.59 -6 3 -3 3.92 4.28 6 -3 3 9.89 4.22 6 -3 3 7.65 1.77 6 -3 3 5.74 1.62 -7 3 -3 10.73 4.92 -7 3 -3 9.28 1.97 7 -3 3 15.69 2.34 7 -3 3 11.07 4.67 7 -3 3 8.51 2.00 -8 3 -3 5.43 1.76 -8 3 -3 6.99 4.99 8 -3 3 3.26 2.22 8 -3 3 4.26 1.88 -9 3 -3 9.93 5.86 -9 3 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