_publ_requested_journal ' Inorg. Chem.' _publ_contact_author_name 'Prof. Jan J. Weigand' _publ_contact_author_address ;Department of Chemistry and Food Chemistry Chair Inorganic Molecular Chemistry TU Dresden 01062 Dresden, Germany ; _publ_contact_author_email jan.weigand@tu-dresden.de _publ_contact_author_phone +4935146342800 loop_ _publ_author_name _publ_author_address 'Weigand, Jan J. ' ;Department of Chemistry and Food Chemistry Chair Inorganic Molecular Chemistry TU Dresden 01062 Dresden, Germany ; 'Yogendra, Sivathmeehan' ;Department of Chemistry and Food Chemistry Chair Inorganic Molecular Chemistry TU Dresden 01062 Dresden, Germany ; 'Hennersdorf, Felix' ;Department of Chemistry and Food Chemistry Chair Inorganic Molecular Chemistry TU Dresden 01062 Dresden, Germany ; 'Chitnis, Saurabh S.' ;Department of Chemistry University of Victoria PO Box 3065 STN CSC Victoria BC V8W 3V6, Canada ; 'Burford, Neil' ;Department of Chemistry University of Victoria PO Box 3065 STN CSC Victoria BC V8W 3V6, Canada ; 'Fischer, Roland' ;Institut für Anorganische Chemie TU Graz Stremayrgasse 9 8010 Graz, Austria ; 'Bodensteiner, Michael' ;X-Ray Structure Analysis University of Regensburg 93053 Regensburg, Germany ; _audit_creation_date 2015-01-14 _audit_creation_method ; Olex2 1.2 (compiled 2015.01.12 svn.r3133 for OlexSys, GUI svn.r4987) ; _publ_contact_author_address ? _publ_contact_author_email ? _publ_contact_author_name '' _publ_contact_author_phone ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2008). Acta Cryst. A64, 112-122. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C4 H12 P2 Se' _chemical_formula_sum 'C4 H12 P2 Se' _chemical_formula_weight 201.04 _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'P' 'P' 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Se' 'Se' -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'tetragonal' _space_group_IT_number 135 _space_group_name_H-M_alt 'P 42/m b c' _space_group_name_Hall '-P 4c 2ab' loop_ _space_group_symop_operation_xyz 'x, y, z' '-y, x, z+1/2' 'y, -x, z+1/2' 'x+1/2, -y+1/2, -z' '-x+1/2, y+1/2, -z' '-x, -y, z' 'y+1/2, x+1/2, -z+1/2' '-y+1/2, -x+1/2, -z+1/2' '-x, -y, -z' 'y, -x, -z-1/2' '-y, x, -z-1/2' '-x-1/2, y-1/2, z' 'x-1/2, -y-1/2, z' 'x, y, -z' '-y-1/2, -x-1/2, z-1/2' 'y-1/2, x-1/2, z-1/2' _cell_length_a 12.5722(6) _cell_length_b 12.5722(6) _cell_length_c 10.7752(5) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 1703.13(18) _cell_formula_units_Z 8 _cell_measurement_reflns_used ? _cell_measurement_temperature 153.15 _cell_measurement_theta_max ? _cell_measurement_theta_min ? _shelx_estimated_absorpt_T_max 0.486 _shelx_estimated_absorpt_T_min 0.399 _exptl_absorpt_coefficient_mu 4.689 _exptl_absorpt_correction_T_max 0.7459 _exptl_absorpt_correction_T_min 0.3253 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2008/1 (Bruker,2008) was used for absorption correction. wR2(int) was 0.1363 before and 0.0509 after correction. The Ratio of minimum to maximum transmission is 0.4361. The \l/2 correction factor is 0.0000. ; _exptl_absorpt_special_details ? _exptl_crystal_colour 'clear colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.568 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description block _exptl_crystal_F_000 800 _exptl_crystal_size_max 0.24 _exptl_crystal_size_mid 0.21 _exptl_crystal_size_min 0.18 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0391 _diffrn_reflns_av_unetI/netI 0.0162 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 14 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_number 15850 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.862 _diffrn_reflns_theta_min 2.291 _diffrn_ambient_temperature 153.15 _diffrn_detector_area_resol_mean ? _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method 'Omega and Phi scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_source 'microfocus sealed tube' _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 1046 _reflns_number_total 1077 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'APEX2 Software Suit (v2012.4-3)' _computing_data_collection 'APEX2 Software Suit (v2012.4-3)' _computing_data_reduction 'APEX2 Software Suit (v2012.4-3)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2008)' _computing_structure_solution 'ShelXS (Sheldrick, 2008)' _refine_diff_density_max 1.057 _refine_diff_density_min -0.695 _refine_diff_density_rms 0.205 _refine_ls_extinction_coef 0.0088(8) _refine_ls_extinction_expression 'Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^' _refine_ls_extinction_method 'SHELXL-2014/7 (Sheldrick 2014' _refine_ls_goodness_of_fit_ref 1.308 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 40 _refine_ls_number_reflns 1077 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0286 _refine_ls_R_factor_gt 0.0272 _refine_ls_restrained_S_all 1.308 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0407P)^2^+0.8583P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0616 _refine_ls_wR_factor_ref 0.0783 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.5 times of: All C(H,H,H) groups 2.a Idealised Me refined as rotating group: C2(H2A,H2B,H2C), C1(H1A,H1B,H1C) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Se1 Se 0.88020(2) 0.30779(2) 0.0000 0.03098(16) Uani 1 2 d S T P . . P1 P 0.80212(5) 0.45719(5) 0.0000 0.01666(18) Uani 1 2 d S T P . . P2 P 0.62782(5) 0.45647(6) 0.0000 0.02208(19) Uani 1 2 d S T P . . C2 C 0.60744(17) 0.36549(17) -0.1298(2) 0.0299(4) Uani 1 1 d . . . . . H2A H 0.5339 0.3396 -0.1290 0.045 Uiso 1 1 calc GR . . . . H2B H 0.6563 0.3051 -0.1222 0.045 Uiso 1 1 calc GR . . . . H2C H 0.6212 0.4029 -0.2080 0.045 Uiso 1 1 calc GR . . . . C1 C 0.83494(17) 0.53826(18) 0.13253(19) 0.0295(4) Uani 1 1 d . . . . . H1A H 0.9098 0.5595 0.1278 0.044 Uiso 1 1 calc GR . . . . H1B H 0.8230 0.4975 0.2088 0.044 Uiso 1 1 calc GR . . . . H1C H 0.7898 0.6018 0.1330 0.044 Uiso 1 1 calc GR . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Se1 0.0257(2) 0.0284(2) 0.0389(2) 0.000 0.000 0.01475(11) P1 0.0118(3) 0.0174(3) 0.0208(3) 0.000 0.000 0.0005(2) P2 0.0117(3) 0.0144(3) 0.0401(4) 0.000 0.000 -0.0015(2) C2 0.0287(10) 0.0319(11) 0.0290(9) 0.0032(8) -0.0071(8) -0.0116(8) C1 0.0243(10) 0.0345(11) 0.0297(9) -0.0097(8) -0.0007(8) -0.0065(8) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Se1 P1 2.1194(7) . ? P1 P2 2.1914(8) . ? P1 C1 1.802(2) 14 ? P1 C1 1.802(2) . ? P2 C2 1.825(2) 14 ? P2 C2 1.825(2) . ? C2 H2A 0.9800 . ? C2 H2B 0.9800 . ? C2 H2C 0.9800 . ? C1 H1A 0.9800 . ? C1 H1B 0.9800 . ? C1 H1C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Se1 P1 P2 117.36(4) . . ? C1 P1 Se1 113.28(8) 14 . ? C1 P1 Se1 113.28(8) . . ? C1 P1 P2 103.37(7) . . ? C1 P1 P2 103.37(7) 14 . ? C1 P1 C1 104.80(15) . 14 ? C2 P2 P1 98.22(7) . . ? C2 P2 P1 98.22(7) 14 . ? C2 P2 C2 100.08(14) 14 . ? P2 C2 H2A 109.5 . . ? P2 C2 H2B 109.5 . . ? P2 C2 H2C 109.5 . . ? H2A C2 H2B 109.5 . . ? H2A C2 H2C 109.5 . . ? H2B C2 H2C 109.5 . . ? P1 C1 H1A 109.5 . . ? P1 C1 H1B 109.5 . . ? P1 C1 H1C 109.5 . . ? H1A C1 H1B 109.5 . . ? H1A C1 H1C 109.5 . . ? H1B C1 H1C 109.5 . . ? _shelx_res_file ; jjw0305.res created by SHELXL-2014/7 TITL jjw0305 in P4(2)/mbc CELL 0.71073 12.5722 12.5722 10.7752 90 90 90 ZERR 8 0.0006 0.0006 0.0005 0 0 0 LATT 1 SYMM -Y,+X,0.5+Z SYMM +Y,-X,0.5+Z SYMM 0.5+X,0.5-Y,-Z SYMM 0.5-X,0.5+Y,-Z SYMM -X,-Y,+Z SYMM 0.5+Y,0.5+X,0.5-Z SYMM 0.5-Y,0.5-X,0.5-Z SFAC C H P Se UNIT 32 96 16 8 L.S. 20 PLAN 20 SIZE 0.18 0.21 0.24 TEMP -120 BOND $H CONF fmap 2 acta MORE -1 MERG 2 SHEL 1000 0.76 REM REM REM WGHT 0.040700 0.858300 EXTI 0.008779 FVAR 0.44469 SE1 4 0.880203 0.307785 0.000000 10.50000 0.02572 0.02836 = 0.03886 0.00000 0.00000 0.01475 P1 3 0.802119 0.457190 0.000000 10.50000 0.01180 0.01741 = 0.02078 0.00000 0.00000 0.00050 P2 3 0.627816 0.456468 0.000000 10.50000 0.01173 0.01442 = 0.04010 0.00000 0.00000 -0.00149 C2 1 0.607441 0.365491 -0.129830 11.00000 0.02871 0.03191 = 0.02898 0.00318 -0.00713 -0.01159 AFIX 137 H2A 2 0.533910 0.339629 -0.129002 11.00000 -1.50000 H2B 2 0.656290 0.305098 -0.122205 11.00000 -1.50000 H2C 2 0.621184 0.402893 -0.207998 11.00000 -1.50000 AFIX 0 C1 1 0.834941 0.538265 0.132526 11.00000 0.02430 0.03453 = 0.02970 -0.00971 -0.00068 -0.00653 AFIX 137 H1A 2 0.909820 0.559548 0.127819 11.00000 -1.50000 H1B 2 0.823004 0.497487 0.208776 11.00000 -1.50000 H1C 2 0.789845 0.601844 0.133043 11.00000 -1.50000 AFIX 0 HKLF 4 REM jjw0305 in P4(2)/mbc REM R1 = 0.0272 for 1046 Fo > 4sig(Fo) and 0.0286 for all 1077 data REM 40 parameters refined using 0 restraints END WGHT 0.0407 0.8583 REM Highest difference peak 1.057, deepest hole -0.695, 1-sigma level 0.205 Q1 1 0.8793 0.3102 0.0778 11.00000 0.05 1.06 Q2 1 0.6176 0.4381 0.0789 11.00000 0.05 0.53 Q3 1 0.8085 0.4684 -0.0785 11.00000 0.05 0.48 Q4 1 0.8748 0.2502 0.0000 10.50000 0.05 0.38 Q5 1 0.6242 0.3642 -0.1980 11.00000 0.05 0.37 Q6 1 0.6202 0.3417 -0.1287 11.00000 0.05 0.34 Q7 1 0.5768 0.4098 -0.2286 11.00000 0.05 0.30 Q8 1 0.8236 0.5395 0.2114 11.00000 0.05 0.29 Q9 1 0.5967 0.4747 -0.2309 11.00000 0.05 0.28 Q10 1 0.9162 0.3033 0.0000 10.50000 0.05 0.26 Q11 1 0.5107 0.3585 -0.2357 11.00000 0.05 0.24 Q12 1 0.8153 0.6664 0.2471 11.00000 0.05 0.24 Q13 1 0.7707 0.6217 0.2494 11.00000 0.05 0.24 Q14 1 0.8675 0.5328 0.1462 11.00000 0.05 0.23 Q15 1 0.7013 0.4613 -0.2615 11.00000 0.05 0.22 Q16 1 0.7627 0.5099 0.2359 11.00000 0.05 0.21 Q17 1 0.7761 0.4029 0.2556 11.00000 0.05 0.21 Q18 1 0.8237 0.4509 0.2323 11.00000 0.05 0.20 Q19 1 0.8772 0.2395 0.0616 11.00000 0.05 0.20 Q20 1 0.6897 0.2770 -0.2449 11.00000 0.05 0.19 ; _shelx_res_checksum 17664 _shelx_hkl_file ; -1 0 0 0.01485 0.03315 3 0 -1 0 -0.0356 0.0297 2 0 -1 0 0.02923 0.04739 4 0 1 0 0.04980 0.03217 1 1 0 0 -0.0734 0.0314 1 1 0 0 0.01693 0.02934 2 -1 1 0 0.05503 0.03170 1 -1 1 0 0.02928 0.06230 3 1 -1 0 -0.0165 0.0661 2 1 -1 0 0.00087 0.04390 4 1 1 0 0.28376 0.09436 1 -1 -1 0 0.06444 0.04988 3 1 -2 0 5638.16 262.87 4 1 -2 0 5022.81 261.95 2 -1 2 0 5567.75 220.04 3 2 1 0 4687.27 235.53 1 0 2 0 24.6790 1.2490 1 2 0 0 23.0356 1.3380 2 2 -1 0 5048.97 267.81 2 2 -1 0 5106.70 268.42 4 -1 -2 0 5483.26 267.49 2 1 2 0 5543.47 241.08 1 -1 -2 0 5458.13 224.78 3 -2 1 0 5436.80 225.04 3 2 -2 0 2678.37 138.06 2 -2 2 0 2837.24 116.29 3 2 -2 0 2792.23 138.66 4 2 2 0 2459.59 124.06 1 -2 2 0 2794.88 124.08 1 -2 -2 0 2915.57 116.41 3 -2 -2 0 2857.41 138.25 2 -2 3 0 33.4439 1.8133 1 2 -3 0 34.6040 2.3100 2 2 -3 0 39.9508 2.0772 4 -3 -2 0 39.2114 1.8735 3 3 2 0 37.4360 2.0689 1 -2 3 0 36.4366 1.9406 3 -3 -1 0 1963.97 81.09 3 1 -3 0 2063.46 97.15 4 3 1 0 1858.30 86.78 1 -1 3 0 1906.94 86.85 1 1 -3 0 1856.97 96.60 2 3 0 0 0.88450 0.39629 2 -3 0 0 -0.4473 0.3916 3 0 -3 0 0.58645 0.45504 2 3 0 0 3.61512 0.48191 1 0 -3 0 1.21253 0.54936 4 -1 -3 0 2072.51 84.90 3 -1 -3 0 2072.45 101.08 2 3 -1 0 1982.79 101.13 2 1 3 0 2017.50 90.95 1 -1 -3 0 1948.33 101.69 4 -3 1 0 2005.94 84.97 3 3 -1 0 2049.35 90.88 1 3 -2 0 39.7590 2.0853 4 2 3 0 35.4752 2.1296 1 -2 -3 0 37.1093 1.8957 3 -2 -3 0 38.3403 2.1763 2 3 -2 0 36.7270 2.3613 2 -3 2 0 38.9002 2.0486 3 3 -3 0 211.039 10.998 4 3 -3 0 205.979 11.305 2 3 3 0 230.653 10.175 1 -3 -3 0 220.460 9.401 3 -3 3 0 215.180 9.506 3 -3 4 0 2050.28 86.91 3 3 -4 0 1962.34 103.48 2 -4 -3 0 2136.00 86.82 3 -3 4 0 2017.83 92.67 1 4 3 0 2014.59 92.98 1 3 -4 0 2193.88 103.64 4 2 -4 0 9.45099 0.93228 4 2 -4 0 9.68315 1.20268 2 -2 4 0 10.3295 0.8107 1 -4 -2 0 7.90879 0.90027 3 4 2 0 8.95528 1.03751 1 4 1 0 393.774 19.758 2 1 -4 0 332.085 19.880 2 4 1 0 385.719 17.865 1 1 -4 0 420.047 19.942 4 -4 -1 0 398.432 16.738 3 -1 4 0 414.754 17.821 1 4 0 0 4907.78 219.18 1 0 -4 0 5148.46 244.98 4 -4 0 0 4709.57 204.29 3 0 4 0 4904.00 219.16 1 4 0 0 4901.15 243.91 2 0 -4 0 4640.69 244.20 2 4 -1 0 393.363 19.828 2 1 4 0 383.451 17.888 1 -4 1 0 380.138 16.724 3 4 -1 0 368.314 17.692 1 -1 -4 0 393.038 16.643 3 -1 -4 0 423.419 20.072 4 -1 -4 0 390.524 19.794 2 -2 -4 0 8.11779 0.94112 2 -2 -4 0 8.44351 0.85852 3 2 4 0 10.1146 1.1082 1 -4 2 0 7.44285 0.95606 3 -2 -4 0 8.70188 1.28729 4 4 -2 0 10.1909 1.1602 2 -3 -4 0 1983.07 102.42 2 4 -3 0 2112.72 102.71 2 -3 -4 0 2144.75 86.13 3 4 -3 0 1995.18 102.78 4 3 4 0 2220.38 92.34 1 -4 3 0 1969.95 91.93 1 -4 3 0 1908.83 86.23 3 -4 4 0 145.187 6.613 3 -4 4 0 144.467 6.580 1 4 -4 0 137.348 7.836 2 4 -4 0 139.539 7.367 4 -4 -4 0 148.193 6.468 3 -4 5 0 102.936 5.015 3 4 -5 0 101.193 5.430 4 -4 5 0 104.235 4.832 1 4 -5 0 96.6670 5.9830 2 5 4 0 109.423 5.383 1 -5 -4 0 101.499 4.882 3 3 -5 0 155.137 8.810 2 -5 -3 0 166.527 7.309 3 5 3 0 152.465 7.847 1 -3 5 0 166.656 7.399 3 3 -5 0 165.123 8.449 4 -3 5 0 164.804 7.527 1 5 2 0 1598.73 79.36 2 -2 5 0 1518.49 71.34 1 -5 -2 0 1570.85 66.83 3 2 -5 0 1663.34 79.80 4 5 2 0 1572.31 71.52 1 -1 5 0 4164.57 192.62 1 1 -5 0 4035.16 214.43 2 -5 -1 0 4461.56 180.09 3 1 -5 0 4709.95 215.96 4 5 1 0 4167.63 214.93 2 5 1 0 4195.51 192.97 1 -5 0 0 0.59497 0.72748 3 0 5 0 0.91917 0.73385 1 5 0 0 3.11211 0.70564 1 0 -5 0 0.32368 0.75796 2 5 0 0 2.20305 0.72353 2 0 -5 0 0.83053 0.92283 4 -5 1 0 4271.55 176.19 3 5 -1 0 3993.47 188.64 1 5 -1 0 4199.45 209.99 2 -1 -5 0 4281.00 176.72 3 -1 -5 0 4330.41 210.83 4 -1 -5 0 4090.99 209.65 2 -2 -5 0 1574.65 80.81 4 5 -2 0 1575.29 80.31 2 -5 2 0 1575.50 67.51 3 2 5 0 1655.91 72.28 1 -2 -5 0 1617.57 80.19 2 -2 -5 0 1594.80 67.38 3 -5 3 0 147.402 7.192 3 -3 -5 0 163.428 8.766 4 -3 -5 0 156.311 8.262 2 3 5 0 164.367 7.747 1 -3 -5 0 153.908 7.037 3 5 -3 0 157.867 8.521 2 -5 4 0 102.001 4.793 1 5 -4 0 96.3720 5.3564 4 -4 -5 0 105.351 4.871 3 4 5 0 108.373 5.395 1 -5 4 0 101.847 5.047 3 -4 -5 0 106.509 6.201 4 -4 -5 0 99.3119 5.5519 2 5 -4 0 106.838 6.020 2 -5 -5 0 2487.48 135.32 4 5 -5 0 2663.56 134.58 4 5 5 0 2671.10 120.93 1 -5 5 0 2744.09 120.36 1 -5 5 0 2692.97 113.02 3 -5 -5 0 2712.62 112.83 3 5 -5 0 2787.78 134.58 2 -6 -5 0 45.4439 2.9803 3 -5 6 0 50.0286 3.2747 3 6 5 0 59.2838 3.5295 1 -5 6 0 56.9146 2.6409 1 -6 -5 0 50.4705 4.2697 4 5 -6 0 53.5878 3.9085 2 5 -6 0 48.2080 2.9855 4 6 4 0 32.0479 2.6018 1 -4 6 0 37.3651 2.6246 3 -6 -4 0 39.6444 2.4484 3 4 -6 0 38.3381 3.0396 2 -4 6 0 40.7453 2.1177 1 4 -6 0 37.7255 2.4136 4 -3 6 0 3511.60 147.24 1 6 3 0 3285.82 147.53 1 3 -6 0 3009.49 164.19 2 -6 -3 0 3307.89 137.82 3 3 -6 0 3262.99 164.61 4 -6 -2 0 528.673 23.488 3 6 2 0 545.948 27.713 2 -2 6 0 572.611 24.965 1 2 -6 0 577.492 27.939 4 2 -6 0 523.647 28.047 2 6 2 0 536.498 25.115 1 1 -6 0 173.528 9.861 2 1 -6 0 193.455 9.811 4 6 1 0 190.059 9.620 2 6 1 0 176.236 8.740 1 -1 6 0 185.191 8.725 1 0 -6 0 1084.44 53.62 4 6 0 0 1074.61 47.84 1 -6 0 0 1024.34 44.87 3 0 -6 0 1057.72 53.36 2 6 0 0 1064.60 53.23 2 0 6 0 1040.88 47.94 1 -1 -6 0 186.684 8.271 3 6 -1 0 177.621 9.766 2 1 6 0 185.978 8.918 1 -1 -6 0 188.650 9.825 2 6 -1 0 179.888 8.660 1 -6 1 0 180.984 8.394 3 -1 -6 0 196.207 10.044 4 -2 -6 0 547.217 23.732 3 -6 2 0 571.011 23.916 3 -2 -6 0 549.574 28.570 4 -2 -6 0 559.499 28.198 2 6 -2 0 546.603 28.301 2 6 -3 0 3235.12 163.09 2 -3 -6 0 3285.65 136.85 3 -6 3 0 2814.63 136.95 3 -3 -6 0 3349.04 162.88 2 -3 -6 0 3197.71 164.02 4 3 6 0 3647.12 146.71 1 4 6 0 39.8234 2.7171 1 -4 -6 0 37.9042 2.5177 2 -4 -6 0 38.0288 2.3237 3 -4 -6 0 38.2017 3.2574 4 -6 4 0 33.5860 1.9233 1 6 -4 0 38.6245 3.0706 2 -6 4 0 32.7603 2.6441 3 -6 5 0 49.4847 3.1024 3 6 -5 0 52.8810 3.8512 2 -5 -6 0 51.8119 2.9389 3 -6 5 0 48.6474 2.5017 1 5 6 0 53.5172 3.3896 1 -5 -6 0 48.2547 3.9460 4 6 6 0 133.052 7.083 1 -6 6 0 137.615 6.194 1 6 -6 0 143.341 7.852 2 -6 -6 0 127.746 6.368 3 -6 6 0 134.668 6.667 3 -6 -6 0 124.403 8.177 4 6 -6 0 132.111 6.952 4 -6 7 0 341.263 15.671 3 6 -7 0 354.465 18.620 2 -7 -6 0 360.785 19.107 4 -7 -6 0 346.612 15.453 3 7 6 0 346.878 16.731 1 5 -7 0 623.416 33.127 4 -7 -5 0 645.247 34.176 4 -7 -5 0 640.840 28.136 3 -5 7 0 745.018 29.647 1 7 5 0 643.206 30.227 1 -5 7 0 623.464 28.291 3 5 -7 0 651.538 33.726 2 4 -7 0 572.023 31.770 2 7 4 0 617.665 28.522 1 -7 -4 0 597.460 26.582 3 4 -7 0 595.094 31.378 4 -4 7 0 701.347 28.084 1 -3 7 0 106.181 4.843 1 3 -7 0 99.6298 5.4340 4 7 3 0 93.1075 5.1874 1 -7 -3 0 97.3443 4.8860 3 3 -7 0 94.8771 5.8874 2 7 3 0 88.3587 5.3124 2 -2 7 0 139.796 6.271 1 -7 -2 0 132.592 6.135 3 7 2 0 126.407 6.454 1 2 -7 0 113.804 7.227 2 7 2 0 122.793 6.846 2 2 -7 0 127.325 7.021 4 1 -7 0 1068.19 53.55 4 7 1 0 997.380 47.870 1 7 1 0 1048.72 53.16 2 1 -7 0 1038.32 53.45 2 -7 -1 0 1087.40 44.93 3 -1 7 0 1097.62 47.90 1 0 -7 0 0.16669 1.08250 2 0 7 0 -0.0932 1.0334 1 -7 0 0 2.60024 1.17550 3 7 0 0 6.04896 1.10591 1 0 -7 0 4.93230 1.47575 4 7 0 0 8.47713 1.26226 2 7 -1 0 1006.46 46.91 1 1 7 0 1035.57 47.19 1 -7 1 0 1063.31 44.18 3 7 -1 0 1028.06 52.34 2 -1 -7 0 1071.24 52.84 4 -1 -7 0 1022.70 44.02 3 -1 -7 0 1036.25 52.41 2 -2 -7 0 121.409 5.988 3 -2 -7 0 133.753 7.082 2 7 -2 0 127.178 7.185 2 -7 2 0 121.140 6.145 3 -2 -7 0 125.983 7.428 4 2 7 0 134.360 6.627 1 -3 -7 0 95.5392 5.6326 2 -3 -7 0 92.2457 4.8229 3 3 7 0 108.881 5.452 1 -7 3 0 90.8708 5.0361 3 -3 -7 0 106.641 6.187 4 7 -3 0 104.823 5.984 2 -7 4 0 559.015 26.161 3 -4 -7 0 621.852 30.780 2 4 7 0 661.165 28.075 1 -4 -7 0 584.470 31.399 4 7 -4 0 620.981 31.118 2 -4 -7 0 580.999 25.948 3 -7 5 0 639.634 29.118 1 -7 5 0 646.047 27.958 3 -5 -7 0 589.016 33.516 4 -5 -7 0 643.020 32.759 2 5 7 0 676.286 29.931 1 -5 -7 0 642.311 27.705 3 7 -5 0 679.018 33.222 2 -6 -7 0 327.666 18.694 4 6 7 0 346.720 16.536 1 7 -6 0 356.225 18.357 2 -7 6 0 352.372 15.556 3 -6 -7 0 342.044 15.239 3 -7 -7 0 133.068 7.991 4 -7 -7 0 122.285 6.049 3 7 -7 0 116.600 7.415 2 7 7 0 115.257 6.782 1 -7 7 0 119.920 6.370 3 8 7 0 536.510 24.080 1 -7 8 0 495.956 22.406 3 -8 -7 0 504.097 22.214 3 7 -8 0 506.356 26.704 2 -8 -7 0 499.557 27.224 4 -8 -6 0 174.643 10.558 4 8 6 0 175.197 8.963 1 6 -8 0 179.828 10.021 2 -8 -6 0 161.518 8.098 3 -5 8 0 37.6900 2.2297 1 -8 -5 0 32.0867 3.8909 4 -8 -5 0 53.1236 3.0272 3 5 -8 0 29.7230 3.4755 2 8 5 0 32.0960 3.0004 1 8 4 0 898.216 44.762 2 4 -8 0 788.715 45.272 2 -8 -4 0 901.929 37.983 3 8 4 0 879.925 40.663 1 -4 8 0 1002.17 40.22 1 4 -8 0 845.176 44.936 4 -8 -3 0 33.6817 2.4733 3 8 3 0 33.1461 2.5210 2 3 -8 0 26.2504 3.1264 2 3 -8 0 30.7910 2.6333 4 8 3 0 34.5284 2.8121 1 -3 8 0 40.9204 2.3608 1 2 -8 0 428.272 23.984 2 8 2 0 437.831 21.412 1 -2 8 0 496.820 21.295 1 8 2 0 458.840 23.572 2 -8 -2 0 473.058 20.186 3 2 -8 0 474.108 23.843 4 -8 -1 0 6.90870 1.54855 3 -1 8 0 4.21017 1.30421 1 1 -8 0 5.03576 1.63123 4 8 1 0 5.25375 1.30643 2 8 1 0 3.76974 1.26350 1 1 -8 0 2.60680 1.54709 2 0 -8 0 69.7644 4.5677 2 8 0 0 62.7885 4.2062 2 8 0 0 69.7671 3.8557 1 0 -8 0 74.0240 4.5755 4 0 8 0 68.5872 3.9677 1 -8 0 0 69.7438 3.9026 3 1 8 0 7.12860 1.55417 1 8 -1 0 6.48676 1.21173 1 -1 -8 0 2.45243 1.24990 3 -1 -8 0 5.10514 1.80906 4 -8 1 0 6.04180 1.51574 3 -1 -8 0 5.76328 1.57318 2 8 -1 0 13.3391 1.7885 2 8 -2 0 445.480 23.683 2 -2 -8 0 474.704 23.670 2 -8 2 0 454.333 20.132 3 -2 -8 0 447.587 19.909 3 -2 -8 0 459.536 24.058 4 2 8 0 471.106 21.430 1 -3 -8 0 27.3952 2.3307 3 -3 -8 0 32.6290 3.2806 4 8 -3 0 34.0825 3.0492 2 3 8 0 35.4514 2.7760 1 -8 3 0 36.9580 2.6754 3 -3 -8 0 29.4241 2.7256 2 8 -4 0 900.158 44.667 2 -4 -8 0 861.598 37.348 3 -4 -8 0 877.718 44.345 2 4 8 0 926.331 40.273 1 -4 -8 0 848.392 45.021 4 -8 4 0 834.799 37.610 3 5 8 0 27.5563 2.8236 1 -5 -8 0 31.6467 2.6522 2 8 -5 0 36.7980 3.4203 2 -5 -8 0 31.1194 3.6889 4 -8 5 0 31.8153 2.8138 3 -5 -8 0 29.0545 2.4375 3 8 -6 0 186.600 10.049 2 6 8 0 186.314 9.131 1 -6 -8 0 169.030 8.203 3 -8 6 0 163.312 8.450 3 -6 -8 0 166.239 10.360 4 7 8 0 546.779 24.536 1 8 -7 0 528.245 27.158 2 -8 7 0 504.214 22.900 3 -7 -8 0 498.030 27.607 4 -7 -8 0 514.101 22.625 3 8 -8 0 1500.67 73.60 2 -8 8 0 1403.36 61.80 3 8 8 0 1478.50 66.22 1 -8 -8 0 1452.30 61.58 3 -8 -8 0 1399.28 74.26 4 -9 -8 0 59.0052 6.0710 4 9 8 0 72.0512 5.0609 1 -9 -8 0 53.2443 4.0155 3 8 -9 0 68.0915 5.2549 2 -9 -7 0 6.76769 1.82717 3 9 7 0 10.1660 2.4661 1 7 -9 0 9.05718 2.64144 2 -9 -7 0 6.12060 3.46111 4 -9 -6 0 2435.80 125.54 4 -9 -6 0 2461.51 104.38 3 9 6 0 2464.65 111.87 1 6 -9 0 2516.37 124.58 2 9 5 0 173.401 8.953 1 -9 -5 0 183.458 10.674 4 5 -9 0 172.796 10.086 2 9 5 0 173.930 9.249 2 -9 -5 0 161.493 8.284 3 -9 -4 0 568.952 24.699 3 4 -9 0 553.476 29.584 2 4 -9 0 560.696 29.051 4 -4 9 0 635.159 25.966 1 9 4 0 537.311 28.875 2 9 4 0 547.431 26.447 1 9 3 0 529.122 26.648 1 9 3 0 589.007 29.307 2 -3 9 0 652.512 26.398 1 -9 -3 0 576.289 25.046 3 3 -9 0 513.384 29.844 2 3 -9 0 582.848 29.512 4 2 -9 0 1022.81 51.86 4 2 -9 0 962.996 51.945 2 9 2 0 987.669 46.508 1 9 2 0 989.155 51.472 2 -2 9 0 1141.13 46.40 1 -9 -2 0 1013.25 43.64 3 1 -9 0 55.3952 4.2211 2 -1 9 0 62.7690 3.5488 1 -9 -1 0 57.0372 3.6870 3 9 1 0 53.7500 3.7510 2 1 -9 0 54.0105 4.0172 4 9 1 0 55.6664 3.5290 1 9 0 0 2.49390 1.26513 1 0 -9 0 0.95736 1.71144 4 0 9 0 2.60861 1.48499 1 -9 0 0 -0.9049 1.3482 3 0 -9 0 1.34386 1.64771 2 9 0 0 1.52435 1.40414 2 9 -1 0 59.2895 4.0398 2 -1 -9 0 56.4339 4.1661 2 -1 -9 0 53.6496 3.4595 3 -1 -9 0 52.4902 4.3587 4 1 9 0 61.2523 3.8388 1 9 -1 0 62.7969 3.4742 1 -9 1 0 58.9141 3.6608 3 -2 -9 0 1056.71 51.95 2 9 -2 0 1027.00 51.98 2 -2 -9 0 981.376 52.337 4 2 9 0 1059.24 46.81 1 -2 -9 0 1043.67 43.68 3 -9 2 0 969.984 43.824 3 -3 -9 0 569.317 30.146 2 -3 -9 0 605.685 30.764 4 -3 -9 0 579.421 25.424 3 3 9 0 621.352 27.413 1 -9 3 0 554.240 25.650 3 9 -3 0 598.599 30.351 2 -4 -9 0 525.341 28.787 4 9 -4 0 551.680 28.495 2 -4 -9 0 535.493 23.794 3 -4 -9 0 533.476 28.176 2 4 9 0 571.478 25.757 1 -9 4 0 578.397 24.208 3 -5 -9 0 180.896 8.449 3 -9 5 0 174.793 8.776 3 -5 -9 0 170.246 10.540 4 5 9 0 183.473 9.338 1 9 -5 0 184.233 10.298 2 -5 -9 0 176.379 9.789 2 -6 -9 0 2266.17 124.66 4 6 9 0 2604.60 111.46 1 -9 6 0 2417.40 104.10 3 -6 -9 0 2421.21 103.84 3 9 -6 0 2580.81 123.91 2 7 9 0 10.0872 2.4568 1 9 -7 0 9.62763 2.52728 2 -7 -9 0 14.6118 3.3303 4 -9 7 0 8.34081 2.34361 3 -7 -9 0 7.61810 1.94684 3 -9 8 0 69.5246 4.5517 3 -8 -9 0 67.4256 4.2580 3 -8 -9 0 64.9886 6.2102 4 9 -8 0 60.5873 5.4457 2 8 9 0 72.5469 4.9945 1 -9 9 0 8.18264 2.59718 3 9 9 0 8.08903 2.96753 1 9 -9 0 10.3261 3.1503 2 -9 -9 0 6.65701 2.18734 3 -9 -9 0 3.55039 3.70779 4 10 9 0 576.454 27.980 1 -10 -9 0 553.769 31.650 4 -10 -9 0 612.084 25.868 3 9 -10 0 597.688 31.096 2 8 -10 0 54.9865 5.1497 2 10 8 0 49.4837 4.3910 1 -10 -8 0 40.3720 3.5843 3 -10 -8 0 40.3738 5.5966 4 10 7 0 209.045 10.798 1 -10 -7 0 199.712 9.684 3 7 -10 0 194.484 11.905 2 -10 -7 0 202.356 12.682 4 10 6 0 1.06644 2.31165 1 6 -10 0 2.84046 2.42278 2 -10 -6 0 -3.0694 3.2654 4 -10 -6 0 0.52626 1.86227 3 10 5 0 68.7569 4.6414 1 5 -10 0 67.3877 5.5887 2 -10 -5 0 65.8157 4.3622 3 -10 -5 0 78.8386 6.3404 4 -10 -4 0 184.003 11.483 4 10 4 0 192.410 10.128 2 -10 -4 0 198.705 9.069 3 4 -10 0 172.337 10.879 2 10 4 0 189.468 9.689 1 -10 -3 0 740.633 32.814 3 3 -10 0 700.489 39.093 2 10 3 0 725.951 34.961 1 -3 10 0 883.879 34.710 1 10 3 0 745.120 38.484 2 3 -10 0 747.422 38.757 4 2 -10 0 107.074 6.564 4 2 -10 0 104.128 6.832 2 10 2 0 100.606 6.207 2 -2 10 0 120.137 5.784 1 -10 -2 0 106.315 5.841 3 10 2 0 105.505 5.936 1 1 -10 0 351.760 18.333 4 1 -10 0 333.450 18.495 2 -1 10 0 387.915 16.387 1 10 1 0 327.939 17.998 2 -10 -1 0 337.111 15.571 3 10 1 0 335.029 16.317 1 10 0 0 280.611 14.281 1 10 0 0 286.888 15.931 2 0 10 0 324.077 14.484 1 0 -10 0 314.414 16.307 4 0 -10 0 301.752 16.328 2 -10 0 0 309.329 13.870 3 -10 1 0 331.048 15.427 3 -1 -10 0 355.582 18.371 4 -1 -10 0 317.558 15.195 3 10 -1 0 346.296 17.999 2 10 -1 0 329.562 15.989 1 1 10 0 364.491 16.328 1 -1 -10 0 345.575 18.208 2 -2 -10 0 103.208 6.681 2 10 -2 0 112.366 6.757 2 -10 2 0 107.616 5.908 3 -2 -10 0 117.864 7.175 4 -2 -10 0 99.4244 5.6455 3 2 10 0 116.276 6.241 1 -3 -10 0 725.066 32.259 3 10 -3 0 765.944 38.474 2 -3 -10 0 737.728 38.889 4 -10 3 0 727.361 32.583 3 -3 -10 0 756.274 38.360 2 3 10 0 780.554 34.737 1 10 -4 0 223.711 11.323 2 -10 4 0 201.249 9.674 3 -4 -10 0 188.362 9.254 3 -4 -10 0 191.535 10.886 2 -4 -10 0 184.088 11.668 4 4 10 0 194.750 10.240 1 -5 -10 0 62.1869 4.5684 2 10 -5 0 68.0942 4.9718 2 -5 -10 0 68.5886 5.8294 4 5 10 0 67.9651 4.6534 1 -5 -10 0 67.2244 4.1267 3 -10 5 0 70.4072 4.5602 3 10 -6 0 4.93391 2.53487 2 -6 -10 0 -2.7183 2.9374 4 -6 -10 0 -2.4195 1.6940 3 6 10 0 4.14634 2.43969 1 -10 6 0 2.62687 2.02793 3 -7 -10 0 182.353 9.209 3 -10 7 0 186.976 9.687 3 7 10 0 205.578 10.331 1 -7 -10 0 190.008 11.912 4 10 -7 0 195.565 11.189 2 -8 -10 0 43.4550 3.5304 3 10 -8 0 45.1171 4.6434 2 -8 -10 0 42.3618 5.1854 4 -10 8 0 39.4024 3.7704 3 8 10 0 43.9937 4.1917 1 10 -9 0 629.085 31.270 2 -9 -10 0 589.106 25.923 3 9 10 0 587.028 28.119 1 -9 -10 0 564.151 31.829 4 -10 9 0 575.630 26.243 3 -10 -10 0 52.7230 6.2985 4 10 -10 0 55.0303 5.4782 2 -10 -10 0 48.2200 4.0832 3 10 10 0 45.5859 4.7904 1 10 -11 0 96.5920 7.5195 2 -11 -10 0 101.166 8.739 4 -11 -10 0 88.7660 5.8579 3 11 10 0 99.8469 6.8302 1 9 -11 0 42.0306 4.6519 2 -11 -9 0 37.7387 5.5963 4 -11 -9 0 41.8765 3.7727 3 11 9 0 36.3801 4.2912 1 -11 -8 0 153.207 10.999 4 11 8 0 163.441 9.281 1 8 -11 0 171.830 10.327 2 -11 -8 0 165.834 8.493 3 -11 -7 0 357.801 20.285 4 -11 -7 0 357.629 16.184 3 7 -11 0 359.798 19.609 2 11 7 0 346.278 17.490 1 -11 -6 0 309.777 18.002 4 6 -11 0 320.037 17.543 2 11 6 0 301.748 15.492 1 -11 -6 0 316.865 14.418 3 -11 -5 0 1389.68 60.48 3 11 5 0 1376.92 64.71 1 5 -11 0 1430.06 72.29 2 -11 -5 0 1472.53 73.10 4 -11 -4 0 41.4990 5.0045 4 4 -11 0 40.8539 4.3150 2 -11 -4 0 38.7186 3.4535 3 11 4 0 39.8828 3.6024 1 -11 -3 0 142.235 7.180 3 11 3 0 134.768 7.519 1 3 -11 0 134.054 8.637 2 -11 -3 0 132.524 9.145 4 11 3 0 142.532 7.823 2 2 -11 0 1705.29 85.88 4 -2 11 0 1863.89 76.75 1 2 -11 0 1681.14 85.91 2 11 2 0 1658.24 85.27 2 -11 -2 0 1587.58 72.09 3 11 2 0 1663.80 76.91 1 1 -11 0 955.272 48.098 4 -11 -1 0 894.132 40.478 3 -1 11 0 983.886 42.916 1 11 1 0 929.680 47.623 2 1 -11 0 905.813 48.134 2 11 1 0 955.440 42.992 1 0 -11 0 2.60794 2.42344 4 -11 0 0 2.70758 2.06292 3 0 -11 0 6.03594 2.40226 2 11 0 0 4.02749 1.78300 1 11 0 0 0.85704 1.85140 2 0 11 0 6.56365 1.95161 1 -11 1 0 895.987 41.150 3 -1 -11 0 904.477 40.929 3 11 -1 0 930.979 48.600 2 1 11 0 1055.26 43.85 1 -1 -11 0 1007.81 49.15 4 -1 -11 0 927.247 48.785 2 -2 -11 0 1660.04 84.67 4 11 -2 0 1691.70 84.06 2 -2 -11 0 1652.59 84.11 2 -2 -11 0 1558.77 70.61 3 2 11 0 1751.17 75.67 1 -11 2 0 1661.99 70.93 3 -3 -11 0 136.188 8.156 2 -3 -11 0 139.523 8.617 4 -11 3 0 144.084 7.322 3 -3 -11 0 140.055 6.963 3 3 11 0 130.624 7.565 1 11 -3 0 127.508 8.199 2 -4 -11 0 42.1913 3.7685 2 -4 -11 0 36.2550 3.1882 3 -4 -11 0 35.0377 4.2499 4 -11 4 0 38.0346 3.6699 3 11 -4 0 42.2629 4.0645 2 4 11 0 41.0449 3.7301 1 5 11 0 1494.70 66.13 1 -11 5 0 1414.45 61.98 3 -5 -11 0 1424.03 74.10 4 11 -5 0 1457.51 73.42 2 -5 -11 0 1433.54 61.56 3 -6 -11 0 315.625 14.769 3 6 11 0 335.097 16.166 1 11 -6 0 339.567 17.837 2 -11 6 0 316.863 15.214 3 -6 -11 0 316.764 18.447 4 7 11 0 355.606 17.418 1 -7 -11 0 343.558 15.894 3 -11 7 0 339.474 16.361 3 11 -7 0 366.568 19.145 2 -7 -11 0 346.272 19.941 4 8 11 0 161.083 9.499 1 -8 -11 0 174.479 11.473 4 11 -8 0 170.842 10.343 2 -11 8 0 171.513 8.905 3 -8 -11 0 168.659 8.623 3 -9 -11 0 37.0167 5.7107 4 11 -9 0 44.1071 4.7190 2 -11 9 0 35.4944 3.8664 3 9 11 0 34.7845 4.5053 1 -9 -11 0 37.6992 3.6246 3 -11 10 0 83.1634 6.2294 3 10 11 0 96.8295 7.0218 1 11 -10 0 93.0592 7.4146 2 -10 -11 0 98.6057 8.7560 4 -10 -11 0 93.5954 5.8008 3 -11 -11 0 366.441 21.030 4 -11 -11 0 344.442 16.512 3 11 -11 0 351.395 19.811 2 11 11 0 356.499 18.081 1 11 -12 0 80.6036 7.5928 2 -12 -11 0 92.3241 9.0834 4 12 11 0 83.3188 7.0482 1 -12 -11 0 88.5625 5.9899 3 12 10 0 16.7147 4.0427 1 -12 -10 0 17.2615 3.3121 3 10 -12 0 17.0317 4.3614 2 -12 -10 0 20.9250 5.4296 4 -12 -9 0 3.38229 2.64670 3 12 9 0 4.72020 3.32561 1 9 -12 0 5.16487 3.65981 2 -12 -9 0 1.95754 4.29236 4 8 -12 0 141.600 9.634 2 12 8 0 139.478 8.744 1 -12 -8 0 153.370 10.635 4 -12 -8 0 148.966 7.925 3 -12 -7 0 24.2509 3.2630 3 7 -12 0 27.5559 4.2755 2 12 7 0 19.5889 3.3986 1 -12 -7 0 24.8942 5.3402 4 6 -12 0 240.823 13.838 2 12 6 0 220.078 11.995 1 -12 -6 0 232.118 14.516 4 -12 -6 0 236.351 11.236 3 -12 -5 0 -0.1071 3.7739 4 5 -12 0 2.39943 3.01757 2 -12 -5 0 4.92190 2.47958 3 12 5 0 3.55330 2.52491 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653.810 33.181 4 -2 3 -3 683.663 32.757 4 2 -3 -3 623.659 33.049 4 -3 -2 -3 668.621 27.419 3 3 2 -3 649.638 33.031 4 2 -3 -3 623.527 32.863 2 -2 3 3 583.537 27.384 3 -3 -2 3 676.110 27.580 3 2 -3 3 653.964 32.752 2 -2 3 3 672.917 29.572 1 3 2 3 640.383 29.516 1 3 1 -3 2035.70 96.06 2 1 -3 -3 1979.65 96.94 4 -1 3 -3 2024.34 96.66 4 -3 -1 -3 1950.10 80.81 3 3 1 -3 1802.56 96.83 4 -3 -1 -3 1932.84 96.88 4 1 -3 -3 1820.29 96.36 2 1 -3 3 1933.34 96.22 2 3 1 3 1869.92 86.55 1 -1 3 3 1892.12 86.64 1 -1 3 3 1915.49 80.67 3 -3 -1 3 1899.85 80.86 3 3 0 -3 1.19415 0.54880 2 0 3 -3 0.54267 0.66294 4 -3 0 -3 0.20051 0.56925 3 -3 0 -3 1.10696 0.81104 4 3 0 -3 0.36515 0.76217 4 0 -3 -3 0.15305 0.69232 2 0 -3 -3 0.95976 0.87717 4 3 0 3 0.52611 0.54510 1 -3 0 3 0.54074 0.54630 3 0 3 3 0.35850 0.65661 1 0 -3 3 2.29507 0.59696 2 -3 1 -3 1982.13 97.36 4 -1 -3 -3 2031.43 97.10 2 -1 -3 -3 1855.34 97.62 4 3 -1 -3 1861.17 97.51 4 1 3 -3 1987.40 97.44 4 3 -1 -3 1864.12 96.89 2 -3 1 -3 2060.85 81.50 3 -3 1 3 1960.32 81.38 3 -1 -3 3 1926.37 96.75 2 1 3 3 1870.02 87.24 1 -1 -3 3 1933.76 81.48 3 3 -1 3 1888.69 87.04 1 -2 -3 -3 656.057 32.859 2 -2 -3 -3 650.253 33.175 4 3 -2 -3 643.264 32.771 2 -3 2 -3 645.888 32.711 4 3 -2 -3 638.512 32.990 4 3 -2 3 627.983 29.268 1 -3 2 3 662.179 27.446 3 -2 -3 3 648.017 27.557 3 -2 -3 3 648.333 32.444 2 2 3 3 654.850 29.537 1 3 -2 3 646.388 32.750 2 -3 -3 -3 0.97326 1.12644 4 3 3 -3 1.46672 1.02047 1 3 -3 -3 0.80589 0.95473 4 -3 -3 -3 0.59079 0.47959 3 3 -3 -3 0.87330 0.89848 2 -3 3 -3 0.28056 0.51379 4 -3 3 3 0.38810 0.61869 3 -3 3 3 0.58469 0.76325 1 3 -3 3 2.13194 0.93954 2 3 -3 3 0.03051 0.48993 1 -3 -3 3 -0.0005 0.6690 3 3 3 3 1.09043 0.88234 1 -4 -3 -3 175.496 10.085 4 4 3 -3 179.967 9.006 1 3 -4 -3 185.457 9.854 4 3 -4 -3 186.402 9.948 2 -4 -3 -3 186.469 8.002 3 3 -4 3 179.501 9.677 2 -3 4 3 190.734 8.767 1 -3 4 3 183.799 8.097 3 -4 -3 3 172.660 8.187 3 4 3 3 184.814 8.756 1 2 -4 -3 746.343 36.347 2 -4 -2 -3 749.537 30.300 3 -4 -2 -3 667.834 36.541 4 2 -4 -3 719.245 36.462 4 4 2 3 703.132 32.492 1 2 -4 3 668.594 36.081 2 -4 -2 3 728.557 30.417 3 -2 4 3 725.297 30.251 3 -2 4 3 720.666 32.568 1 4 1 -3 29.8249 2.2637 4 1 -4 -3 30.2020 2.3329 2 -4 -1 -3 24.2475 2.2515 4 1 -4 -3 27.9602 2.3174 4 4 1 -3 31.5336 1.7639 2 -4 -1 -3 29.3376 1.8125 3 -1 4 3 29.7635 2.0585 1 -4 -1 3 30.7510 1.8176 3 1 -4 3 31.0098 2.0660 2 4 1 3 28.8587 1.8739 1 -1 4 3 29.9235 1.5676 3 4 0 -3 3719.80 198.49 2 -4 0 -3 4017.54 199.51 4 0 -4 -3 4341.19 198.72 2 0 -4 -3 4076.08 199.75 4 4 0 -3 3646.99 199.55 4 -4 0 -3 3934.18 166.77 3 -4 0 3 4397.30 167.57 3 4 0 3 3793.60 178.56 1 0 4 3 3823.30 178.53 1 0 -4 3 3971.69 198.61 2 4 -1 -3 26.5803 2.0937 2 -1 -4 -3 31.7167 2.5320 4 -4 1 -3 31.3200 2.1238 4 4 -1 -3 31.9092 2.3020 4 -4 1 -3 36.3229 2.0486 3 -1 -4 -3 30.5330 2.3989 2 -1 -4 -3 31.7497 1.4277 3 1 4 -3 31.1925 2.2179 1 -4 1 3 29.5308 1.8557 3 1 4 3 29.2865 2.0771 1 4 -1 3 29.1343 1.7941 1 4 -1 3 33.9619 2.3107 2 -1 -4 3 32.3091 1.9988 3 -1 -4 3 31.5352 1.9838 2 -4 2 -3 735.233 36.128 4 2 4 -3 728.594 32.782 1 4 -2 -3 728.579 36.242 2 4 -2 -3 710.780 36.422 4 -2 -4 -3 700.974 30.069 3 -2 -4 -3 726.607 36.317 2 -2 -4 -3 719.880 36.697 4 -4 2 -3 766.799 30.584 3 4 -2 3 713.369 36.206 2 -2 -4 3 698.782 30.472 3 -4 2 3 713.288 30.369 3 -2 -4 3 689.278 35.884 2 4 -2 3 702.066 32.279 1 2 4 3 682.473 32.609 1 4 -3 -3 188.135 9.912 2 4 -3 -3 178.275 9.838 4 -3 -4 -3 204.843 10.330 4 -3 -4 -3 186.877 7.901 3 3 4 -3 178.711 9.036 1 -4 3 -3 172.743 9.379 4 4 -3 3 177.361 9.754 2 -3 -4 3 176.079 8.255 3 -4 3 3 176.242 8.777 1 4 -3 3 178.968 8.394 1 -3 -4 3 194.789 9.267 2 -4 3 3 195.009 8.185 3 3 4 3 180.034 8.853 1 4 -4 -3 9.51377 1.46924 4 -4 -4 -3 0.90139 0.63726 3 4 -4 -3 0.62722 1.17411 2 4 4 -3 -0.9958 1.1779 1 -4 -4 -3 3.74660 1.72716 4 4 4 3 1.17224 1.05041 1 4 -4 3 0.27843 0.41053 1 4 -4 3 2.92651 1.18083 2 -4 -4 3 -0.5686 0.8027 3 -4 4 3 0.41048 0.85123 1 -4 4 3 2.12508 0.87306 3 4 -5 -3 733.458 35.934 2 -5 -4 -3 678.535 29.682 3 -5 -4 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1.06091 4 -5 0 -3 5.98996 1.04646 3 0 5 3 1.28767 0.91913 1 0 -5 3 2.32188 0.95209 2 -5 0 3 1.73233 0.88800 3 5 0 3 2.15176 0.76151 1 -1 -5 -3 326.278 13.448 3 -1 -5 -3 347.826 16.836 4 5 -1 -3 298.257 16.290 2 -1 -5 -3 289.862 16.467 2 -5 1 -3 343.654 16.360 4 -5 1 -3 332.842 13.941 3 1 5 -3 299.578 14.923 1 5 -1 -3 322.668 16.540 4 -5 1 3 311.640 13.777 3 5 -1 3 311.167 14.486 1 5 -1 3 320.239 16.428 2 1 5 3 298.110 14.816 1 -1 -5 3 305.108 16.172 2 -1 -5 3 331.379 13.913 3 -2 -5 -3 34.8662 2.8687 2 -5 2 -3 39.3930 2.3788 4 5 -2 -3 40.9463 2.7930 2 5 -2 -3 35.4666 2.7729 4 -5 2 -3 39.3275 2.4366 3 -2 -5 -3 39.0296 1.8576 3 2 5 -3 36.9224 2.7249 1 -2 -5 -3 39.1772 3.1552 4 -2 -5 3 37.1033 2.3056 2 5 -2 3 42.0123 2.7391 2 -2 -5 3 37.4894 2.3595 3 2 5 3 38.0376 2.5917 1 5 -2 3 36.3777 2.0022 1 -5 2 3 36.5937 2.3070 3 5 -3 -3 3802.24 199.47 2 3 5 -3 3659.41 179.45 1 -5 3 -3 3821.06 167.55 3 -5 3 -3 3938.54 199.83 4 -3 -5 -3 4069.60 199.43 2 -3 -5 -3 3939.33 200.72 4 -3 -5 -3 4173.63 167.29 3 5 -3 -3 4006.60 200.28 4 -3 -5 3 4269.07 198.95 2 5 -3 3 3630.96 178.71 1 -5 3 3 4053.48 167.38 3 5 -3 3 4153.36 199.36 2 3 5 3 3927.33 179.21 1 -3 -5 3 4313.49 167.51 3 -4 -5 -3 708.009 36.756 4 -4 -5 -3 714.098 29.961 3 5 -4 -3 723.309 36.321 2 5 -4 -3 696.579 36.138 4 -5 4 -3 762.738 30.540 3 4 5 -3 705.481 32.793 1 -5 4 3 680.970 32.284 1 -5 4 3 672.776 30.205 3 -4 -5 3 733.643 30.354 3 4 5 3 705.421 32.420 1 5 -4 3 688.962 35.987 2 -5 -5 -3 0.22237 2.04398 4 5 -5 -3 0.02447 1.28011 4 5 -5 -3 -1.2050 1.5000 2 -5 -5 -3 2.07234 0.84739 3 5 5 -3 1.92689 1.58260 1 -5 5 3 0.18440 1.05273 3 -5 -5 3 -0.9867 1.1021 3 5 5 3 -0.2612 1.1261 1 -5 5 3 0.53292 0.98327 1 5 -5 3 1.13973 1.36973 2 5 -6 -3 3787.71 195.19 4 -6 -5 -3 4064.78 163.03 3 -6 -5 -3 3529.68 195.94 4 5 -6 -3 3987.08 194.83 2 6 5 -3 3970.32 175.20 1 5 -6 3 3858.30 194.38 2 -6 -5 3 4068.16 163.32 3 6 5 3 3888.68 174.69 1 -5 6 3 3709.79 163.15 3 -5 6 3 3925.86 174.55 1 4 -6 -3 161.647 9.322 4 4 -6 -3 170.325 9.836 2 6 4 -3 175.433 8.881 1 -6 -4 -3 149.800 10.016 4 -6 -4 -3 176.374 7.717 3 4 -6 3 170.385 9.383 2 6 4 3 161.712 8.336 1 4 -6 3 189.799 8.700 4 -4 6 3 159.952 8.252 1 -4 6 3 174.053 7.810 3 -6 -4 3 164.502 7.927 3 3 -6 -3 27.7622 2.5591 4 -6 -3 -3 25.8084 1.8652 3 3 -6 -3 22.3005 2.7443 2 -6 -3 -3 23.7848 2.9479 4 6 3 -3 22.4486 2.4416 1 -6 -3 3 24.6437 2.0035 3 6 3 3 25.2528 2.0767 1 -3 6 3 26.6957 1.8974 3 3 -6 3 26.1912 2.4347 2 -3 6 3 25.9930 2.0601 1 2 -6 -3 1.74588 1.40833 2 6 2 -3 5.12761 1.37715 1 2 -6 -3 3.41784 1.43101 4 -6 -2 -3 3.81659 1.06001 3 -6 -2 -3 4.71170 1.67812 4 6 2 -3 2.73596 0.58959 2 -6 -2 3 1.37290 1.00643 3 -2 6 3 0.80313 1.04287 1 2 -6 3 2.84248 1.19441 2 6 2 3 3.64092 1.07240 1 -6 -1 -3 5799.44 311.74 4 -6 -1 -3 6317.04 260.46 3 1 -6 -3 6274.69 311.79 4 1 -6 -3 6828.98 311.37 2 6 1 -3 5800.30 309.98 2 -1 6 -3 5953.16 278.69 1 -6 -1 3 6080.10 260.43 3 1 -6 3 6117.76 310.01 2 6 1 3 6373.87 278.58 1 -1 6 3 6504.13 278.78 1 0 -6 -3 351.522 17.137 2 6 0 -3 312.802 16.983 4 6 0 -3 277.584 16.615 2 -6 0 -3 323.600 16.959 4 0 -6 -3 330.829 17.248 4 0 6 -3 314.075 15.303 1 -6 0 -3 329.922 14.325 3 -6 0 3 343.773 14.277 3 6 0 3 347.300 16.930 2 0 -6 3 332.577 16.758 2 0 6 3 320.878 15.226 1 6 0 3 321.626 14.948 1 -1 -6 -3 5980.64 311.81 2 -1 -6 -3 6700.23 261.64 3 -1 -6 -3 6320.83 313.53 4 1 6 -3 5773.57 280.35 1 6 -1 -3 5859.10 313.65 4 -6 1 -3 6490.21 313.04 4 6 -1 -3 5488.40 311.98 2 -6 1 -3 6417.71 261.91 3 1 6 3 6341.83 281.28 1 6 -1 3 6188.27 279.95 1 -6 1 3 6547.46 262.33 3 6 -1 3 6762.11 312.85 2 -1 -6 3 6113.22 311.64 2 -1 -6 3 6311.14 261.85 3 -2 -6 -3 2.98282 0.71184 3 -2 -6 -3 5.53705 1.53623 2 6 -2 -3 14.1025 1.6834 4 6 -2 -3 3.11511 1.35635 2 2 6 -3 1.74356 1.38487 1 -2 -6 -3 3.54797 1.70087 4 -6 2 -3 4.28600 1.00540 4 -6 2 -3 5.15831 1.26265 3 2 6 3 3.76119 1.31131 1 -6 2 3 2.84317 1.06546 3 6 -2 3 1.95404 1.24466 2 -2 -6 3 3.30704 1.22538 3 -2 -6 3 5.49956 1.00458 2 6 -3 -3 26.5713 2.3992 4 -6 3 -3 27.7809 2.3767 3 3 6 -3 28.1004 2.7811 1 -6 3 -3 26.7103 1.6690 4 -3 -6 -3 24.1313 2.4037 2 -3 -6 -3 25.8857 1.5735 3 -3 -6 -3 27.4684 3.0331 4 6 -3 -3 22.0649 2.4990 2 6 -3 3 24.1313 2.3723 2 3 6 3 25.0467 2.2241 1 6 -3 3 24.7767 1.3968 1 -3 -6 3 27.1904 1.8144 2 -6 3 3 23.8481 2.0349 3 -3 -6 3 25.0749 2.1278 3 -4 -6 -3 165.584 9.868 4 4 6 -3 169.114 8.755 1 6 -4 -3 165.569 9.068 4 -6 4 -3 158.807 7.905 3 -4 -6 -3 173.212 9.243 2 -4 -6 -3 166.964 7.331 3 6 -4 -3 147.237 9.354 2 -4 -6 3 172.274 7.826 3 6 -4 3 162.870 9.116 2 -4 -6 3 173.569 8.511 2 4 6 3 172.661 8.303 1 -6 4 3 157.428 8.063 1 -6 4 3 165.001 7.718 3 5 6 -3 3815.78 171.67 1 -5 -6 -3 3611.63 191.99 4 6 -5 -3 3873.69 191.20 4 6 -5 -3 3703.61 190.83 2 -6 5 -3 3730.31 160.15 3 -5 -6 -3 3938.62 159.62 3 6 -5 3 3998.43 190.45 2 -6 5 3 3596.29 159.88 3 -6 5 3 3812.66 170.98 1 -5 -6 3 3908.84 159.99 3 5 6 3 3804.12 171.19 1 6 6 -3 -0.1339 1.9750 1 -6 -6 -3 -0.1823 2.2269 4 -6 -6 -3 0.40201 1.12775 3 6 -6 -3 -0.3486 1.4331 4 6 -6 -3 0.78251 1.91521 2 -6 6 3 0.92450 1.33415 3 6 6 3 1.06901 1.38073 1 6 -6 3 0.41557 1.43614 2 -6 -6 3 6.79645 1.51520 3 -6 6 3 6.39698 1.31963 1 -7 -6 -3 247.432 16.176 4 6 -7 -3 286.048 15.893 2 -7 -6 -3 295.347 12.539 3 6 -7 -3 285.813 14.994 4 7 6 -3 272.664 14.242 1 7 6 3 283.052 13.651 1 -6 7 3 285.689 13.341 1 6 -7 3 264.838 15.134 2 -6 7 3 308.833 12.788 3 -7 -6 3 281.504 12.843 3 -7 -5 -3 75.1018 3.8891 3 5 -7 -3 68.7701 4.6486 4 5 -7 -3 74.1078 5.5514 2 -7 -5 -3 65.9360 5.9150 4 7 5 -3 70.3562 4.8307 1 7 5 3 68.2301 4.3185 1 -7 -5 3 66.1380 4.1206 3 5 -7 3 66.2384 4.8757 2 -5 7 3 76.3362 4.1006 1 -5 7 3 83.9430 4.0656 3 -7 -4 -3 1387.06 58.31 3 4 -7 -3 1368.04 70.03 2 4 -7 -3 1453.07 69.84 4 -7 -4 -3 1180.70 70.44 4 7 4 -3 1397.70 62.89 1 7 4 3 1379.45 62.44 1 4 -7 3 1376.97 69.55 2 -7 -4 3 1380.67 58.46 3 -4 7 3 1402.12 58.32 3 -4 7 3 1428.51 62.38 1 -7 -3 -3 1718.73 70.83 3 3 -7 -3 1664.99 84.78 2 7 3 -3 1709.63 76.17 1 3 -7 -3 1694.30 84.82 4 3 -7 3 1756.69 84.31 4 -3 7 3 1664.15 75.76 1 -7 -3 3 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6074.82 310.12 4 -2 -1 -4 5671.63 309.85 4 2 1 4 5950.05 276.69 1 -1 2 4 6734.74 258.81 3 -1 2 4 6222.10 277.23 1 -2 -1 4 6528.86 259.40 3 2 0 -4 363.662 18.941 4 2 0 -4 365.162 18.625 2 0 -2 -4 383.410 19.064 4 -2 0 -4 359.949 18.885 4 0 -2 -4 365.103 18.815 2 0 2 -4 365.845 18.819 4 0 2 4 358.197 16.964 1 2 0 4 358.914 16.856 1 -2 0 4 370.899 15.635 3 -1 -2 -4 5500.25 304.43 4 2 -1 -4 5275.68 304.35 4 1 2 -4 6442.11 305.59 4 -2 1 -4 5889.10 305.22 4 2 -1 4 6149.66 273.10 1 -1 -2 4 6583.69 254.91 3 -2 1 4 6681.93 254.89 3 1 2 4 6483.58 254.17 3 1 2 4 5549.90 273.23 1 2 2 -4 332.490 17.589 4 2 -2 -4 333.335 17.660 4 2 -2 -4 370.888 17.513 2 -2 -2 -4 339.750 17.721 4 -2 2 -4 333.606 17.401 4 2 -2 4 335.296 17.372 2 -2 2 4 353.006 15.836 1 -2 2 4 312.047 14.433 3 -2 -2 4 341.900 14.636 3 2 2 4 339.022 15.755 1 2 -2 4 341.180 15.632 1 -3 -2 -4 1.94492 0.59684 3 3 2 -4 3.31987 1.17997 4 -3 -2 -4 2.26686 1.18289 4 2 -3 -4 1.19721 1.07332 4 -2 3 -4 2.58243 0.82649 4 2 -3 -4 1.64722 0.94803 2 3 2 4 1.73925 0.87531 1 2 -3 4 2.03914 0.90531 2 -3 -2 4 1.19210 0.78202 3 -2 3 4 0.40907 0.86695 1 -2 3 4 2.56567 0.60731 3 1 -3 -4 1931.92 101.16 4 1 -3 -4 2210.20 100.66 2 3 1 -4 1933.95 101.08 4 -3 -1 -4 1930.33 101.09 4 -1 3 -4 2010.56 100.87 4 -3 -1 -4 2177.37 84.28 3 -1 3 4 1831.83 84.09 3 -3 -1 4 2061.27 84.37 3 1 -3 4 1997.38 100.38 2 3 1 4 1984.54 90.35 1 -1 3 4 1977.30 90.46 1 0 -3 -4 2.54173 1.25591 4 0 -3 -4 0.97879 0.92291 2 -3 0 -4 2.43936 1.04211 4 3 0 -4 3.12869 1.18021 4 3 0 -4 1.24711 0.72356 2 -3 0 4 2.30360 0.71980 3 0 -3 4 0.61175 0.68915 2 0 3 4 2.40989 0.90071 1 3 0 4 0.98341 0.69646 1 -1 -3 -4 1878.73 99.75 4 3 -1 -4 2142.93 99.01 2 -3 1 -4 2021.67 99.47 4 3 -1 -4 1902.17 99.64 4 -1 -3 -4 2018.90 99.18 2 1 3 -4 1997.50 99.52 4 3 -1 4 1961.63 88.95 1 -3 1 4 2038.45 83.07 3 -1 -3 4 1920.78 98.78 2 -1 -3 4 1974.68 83.20 3 1 3 4 1862.25 89.11 1 -3 2 -4 2.08895 0.81090 4 2 3 -4 2.59201 1.02061 4 3 -2 -4 2.69553 1.00487 2 3 -2 -4 4.54122 1.25050 4 -2 -3 -4 5.26233 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337.135 14.764 3 2 4 4 338.714 15.838 1 4 -2 4 335.852 15.484 1 -4 3 -4 1181.34 59.46 4 4 -3 -4 1204.57 59.93 4 -3 -4 -4 1207.80 60.21 4 -3 -4 -4 1093.19 49.61 3 4 -3 -4 1263.41 59.66 2 -4 3 4 1193.98 53.60 1 -3 -4 4 1068.72 59.03 2 -3 -4 4 1174.15 50.05 3 4 -3 4 1209.25 59.51 2 -4 3 4 1200.98 49.88 3 4 -3 4 1197.79 53.22 1 3 4 4 1181.81 53.59 1 -4 4 -4 526.759 25.975 4 -4 -4 -4 488.470 26.875 4 4 -4 -4 509.954 26.498 4 -4 -4 -4 512.199 21.798 3 4 -4 -4 540.610 26.557 2 4 -4 4 521.859 26.267 2 -4 -4 4 504.539 22.140 3 -4 4 4 499.334 23.668 1 4 -4 4 500.654 23.270 1 -4 4 4 528.913 21.980 3 4 4 4 505.883 23.681 1 -5 -4 -4 340.228 19.812 4 5 4 -4 376.592 17.798 1 4 -5 -4 400.366 19.666 2 4 -5 -4 371.673 19.421 4 -5 -4 -4 375.157 15.956 3 5 4 4 362.860 17.311 1 4 -5 4 372.535 19.225 2 -5 -4 4 375.802 16.264 3 -4 5 4 368.212 17.325 1 -4 5 4 388.473 16.079 3 4 -5 4 345.510 16.857 1 -5 -3 -4 497.722 29.329 4 3 -5 -4 582.703 29.192 4 -5 -3 -4 552.848 24.131 3 3 -5 -4 574.302 29.145 2 -3 5 4 639.038 24.140 3 -5 -3 4 561.941 24.301 3 5 3 4 567.269 25.951 1 3 -5 4 536.783 28.783 2 -3 5 4 564.259 26.023 1 2 -5 -4 1100.38 53.89 2 2 -5 -4 1087.52 54.12 4 -5 -2 -4 1006.52 54.13 4 -5 -2 -4 1059.57 44.99 3 -2 5 4 1091.66 44.81 3 -2 5 4 1092.61 48.30 1 2 -5 4 1039.60 53.52 2 -5 -2 4 1043.87 45.06 3 5 2 4 1033.25 48.15 1 -5 -1 -4 631.297 32.310 4 1 -5 -4 638.906 32.446 4 1 -5 -4 615.122 32.178 2 5 1 -4 623.707 31.648 2 -5 -1 -4 614.691 26.891 3 5 1 -4 627.583 32.294 4 1 -5 4 634.598 31.873 2 5 1 4 624.143 28.677 1 -5 -1 4 637.306 26.902 3 -1 5 4 639.499 28.884 1 5 0 -4 0.75997 0.80045 2 0 -5 -4 1.11155 1.37056 4 -5 0 -4 0.58221 1.03387 3 5 0 -4 2.33278 1.38042 4 0 -5 -4 1.51180 1.18037 2 -5 0 -4 1.24807 1.10941 4 5 0 4 -0.1732 0.7664 1 0 -5 4 0.60019 0.91411 2 -5 0 4 -0.3781 0.7629 3 0 5 4 1.02333 1.03646 1 5 -1 -4 649.692 32.567 2 5 -1 -4 627.861 32.947 4 -5 1 -4 652.851 27.587 3 -1 -5 -4 653.161 32.883 2 -5 1 -4 649.034 32.725 4 -1 -5 -4 647.280 33.213 4 -1 -5 4 640.117 27.575 3 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3.4349 4 2 -6 -4 40.6877 3.3673 4 -6 -2 -4 39.2719 2.5237 3 6 2 -4 39.1840 2.1267 2 6 2 4 35.4319 2.4441 1 -2 6 4 39.2014 2.1647 3 -2 6 4 33.2379 2.5715 1 2 -6 4 39.4358 2.8742 2 -6 -2 4 36.3417 2.4695 3 1 -6 -4 493.755 25.586 4 6 1 -4 466.981 25.390 4 -6 -1 -4 465.491 21.202 3 1 -6 -4 482.802 25.420 2 6 1 -4 484.471 24.764 2 -6 -1 -4 484.827 25.466 4 -1 6 4 533.484 22.802 1 1 -6 4 498.898 25.067 2 6 1 4 495.266 22.496 1 -6 -1 4 497.155 21.205 3 6 0 -4 129.443 7.288 4 -6 0 -4 131.322 6.099 3 0 -6 -4 109.741 7.260 2 0 -6 -4 124.206 7.528 4 6 0 -4 120.672 6.756 2 -6 0 -4 137.255 7.180 4 6 0 4 120.412 6.088 1 -6 0 4 126.195 5.977 3 0 -6 4 133.813 6.938 2 0 6 4 120.684 6.489 1 6 -1 -4 479.746 25.953 2 -1 -6 -4 529.018 21.446 3 -6 1 -4 520.728 26.095 4 -1 -6 -4 532.300 26.337 2 6 -1 -4 489.164 26.304 4 1 6 -4 475.173 23.707 1 -6 1 -4 504.858 22.092 3 -1 -6 -4 498.532 26.598 4 6 -1 4 514.815 26.137 2 1 6 4 523.722 23.627 1 -1 -6 4 500.631 22.080 3 -1 -6 4 536.295 25.862 2 6 -1 4 503.147 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24.5790 4.3951 4 3 -8 -10 15.0598 4.2649 4 -8 -3 10 19.2511 2.6928 3 3 -8 10 16.9061 2.9978 2 -3 8 10 25.2075 3.4153 1 3 -8 10 18.8732 3.3226 3 8 3 10 17.6422 3.0212 1 -8 -2 -10 53.3196 5.5984 4 8 2 -10 46.1395 4.9998 4 2 -8 -10 52.5488 5.9515 4 2 -8 -10 46.9552 5.3741 2 8 2 10 47.8983 4.0933 1 -8 -2 10 50.2313 3.6962 3 -2 8 10 52.1282 4.7294 1 2 -8 10 47.4612 4.4036 3 8 1 -10 7.87851 3.44718 4 1 -8 -10 7.87062 4.00432 4 1 -8 -10 8.78963 3.62065 2 -8 -1 -10 9.52427 3.47559 4 1 -8 10 3.69869 2.58299 3 8 1 10 11.1967 2.5572 1 -1 8 10 4.70376 2.66756 1 -8 -1 10 7.76542 2.28253 3 8 0 -10 72.1154 6.3525 4 0 -8 -10 69.4216 7.0721 4 0 -8 10 73.0826 5.3098 3 -8 0 10 72.4113 4.6501 3 0 8 10 64.9273 5.5741 1 8 0 10 85.7805 6.2051 2 8 -1 -10 5.27946 3.42617 4 -1 -8 -10 11.5346 4.2838 4 1 8 10 2.92828 2.77602 1 8 -1 10 5.49475 3.13858 2 -1 -8 10 8.57077 2.84825 3 -8 1 10 7.69623 2.21447 3 8 -2 -10 47.8339 5.3474 4 -2 -8 -10 44.5140 5.8379 4 8 -2 10 46.0802 4.7289 2 -8 2 10 44.2365 4.7741 1 2 8 10 52.7455 4.8008 1 -2 -8 10 52.8420 4.4211 3 -3 -8 -10 22.8996 4.7166 4 8 -3 -10 17.7096 3.8376 4 -3 -8 10 23.2212 3.2856 3 -8 3 10 21.4410 3.6116 1 3 8 10 15.3105 3.4159 1 8 -3 10 20.3334 3.4792 2 8 -4 -10 217.357 13.375 4 -4 -8 -10 203.225 14.360 4 8 -4 10 248.175 12.977 2 -4 -8 10 213.150 11.004 3 4 8 10 220.928 11.793 1 8 -5 -10 5.07775 3.31364 4 -5 -8 -10 4.00418 4.44966 4 -5 -8 10 4.55569 2.73673 3 -8 5 10 1.14080 2.74847 1 8 -5 10 6.00785 3.16975 2 5 8 10 2.93370 2.98389 1 8 -6 -10 27.3509 4.6950 2 -6 -8 -10 29.2190 5.7544 4 8 -6 -10 31.8252 4.8730 4 8 -6 10 32.3350 4.0983 2 -6 -8 10 30.8100 3.6919 3 6 8 10 27.0771 3.9375 1 -8 6 10 33.9168 4.0607 1 8 -7 -10 4.22438 3.98450 2 -7 -8 -10 4.59189 4.86913 4 8 -7 -10 2.04696 3.72820 4 -8 7 10 5.23480 3.03012 1 8 -7 10 8.04843 3.37282 2 -7 -8 10 0.87275 2.64746 3 7 8 10 0.94736 2.81123 1 8 -8 -10 293.883 16.090 4 -8 -8 -10 232.577 17.396 4 8 -8 -10 249.630 16.665 2 8 8 10 270.866 14.053 1 -8 8 10 271.229 14.121 1 -8 -8 10 267.645 13.323 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3.62144 3.69411 1 -5 2 13 5.25364 3.65143 1 -3 -5 -13 253.602 17.197 4 5 -3 -13 275.332 16.860 4 3 5 -13 291.178 16.275 4 -5 3 13 308.519 15.542 1 5 -3 13 307.801 16.304 2 -3 -5 13 254.962 15.469 1 3 5 13 272.175 14.962 1 5 -4 -13 63.1614 6.6912 4 -4 -5 -13 49.3046 6.8879 4 4 5 -13 62.4267 5.9144 4 -4 -5 13 66.7319 5.0250 3 -5 4 13 68.8383 6.4463 1 5 -4 13 60.5591 5.8178 2 4 5 13 45.1148 5.2110 1 -5 -5 -13 0.89797 4.47261 4 5 -5 -13 2.58595 4.34311 4 -5 -5 13 1.70125 3.04784 3 -5 5 13 -0.3149 3.2402 1 5 5 13 -0.8770 3.4513 1 5 -5 13 -3.3565 3.2389 2 5 -6 -13 216.077 14.356 4 -6 -5 -13 215.089 14.726 4 -5 6 13 219.713 12.557 1 6 5 13 208.741 12.059 1 -6 -5 13 235.192 11.314 3 5 -6 13 226.947 13.130 2 -6 -4 -13 25.6929 5.3621 4 6 4 -13 23.0413 4.5296 4 4 -6 -13 22.2901 5.4025 4 -4 6 13 21.8317 4.5155 1 4 -6 13 19.1456 3.9149 2 6 4 13 24.3719 4.1705 1 -6 -3 -13 17.3925 4.8444 4 3 -6 -13 21.5228 5.4066 4 6 3 -13 18.5313 4.5416 4 6 3 13 16.7540 3.7712 1 -6 -2 -13 4.09723 3.94181 4 6 2 -13 4.11184 3.67812 4 2 -6 -13 -0.5783 4.4367 4 6 2 13 3.33664 3.16368 1 -2 6 13 7.89167 3.74566 1 -6 -2 13 3.99625 3.81945 1 1 -6 -13 265.818 17.858 4 -6 -1 -13 307.396 17.371 4 6 1 -13 297.347 17.295 4 -6 -1 13 314.265 16.363 1 6 1 13 285.752 15.165 1 -1 6 13 303.396 15.691 1 0 -6 -13 9.23347 4.67983 4 6 0 -13 6.69291 4.15886 4 0 6 -13 3.71354 3.34362 4 0 6 13 6.44516 3.41793 1 -6 0 13 12.5292 3.9828 1 0 -6 13 7.18703 3.63438 1 1 6 -13 298.460 16.842 4 6 -1 -13 289.411 17.584 4 -1 -6 -13 275.641 18.285 4 -1 -6 13 303.268 14.390 3 1 6 13 298.472 15.751 1 6 -1 13 321.194 17.441 2 -6 1 13 325.077 16.422 1 -1 -6 13 279.351 15.821 1 2 6 -13 6.74171 3.48109 4 -2 -6 -13 3.70951 4.74144 4 6 -2 -13 5.48814 4.25831 4 -2 -6 13 6.20470 3.00702 3 2 6 13 6.86708 3.32261 1 -6 2 13 1.42783 3.78990 1 -2 -6 13 3.23558 3.83758 1 6 -2 13 8.50209 3.82525 2 -3 -6 -13 17.0113 5.2934 4 6 -3 -13 20.1783 4.6905 4 3 6 13 15.7759 3.7905 1 6 -3 13 15.5670 4.2761 2 -6 3 13 18.1519 4.2862 1 -3 -6 13 19.3032 3.5853 3 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2.49018 3.19483 3 8 -3 13 1.01904 3.93593 2 3 8 13 2.69261 3.37304 1 0 0 -14 1204.87 62.51 4 0 0 14 1195.45 56.23 1 0 -1 -14 3.08773 4.01747 4 -1 0 -14 -2.8538 3.6553 4 0 1 -14 -0.6943 3.6811 4 1 0 -14 3.69750 3.60458 4 0 1 14 -1.5581 3.5545 1 1 0 14 -0.0169 3.1833 1 0 -1 14 6.89321 3.92422 1 -1 0 14 -0.3253 3.7009 1 1 1 -14 12.4183 4.4310 4 1 -1 -14 13.3741 4.5089 4 -1 -1 -14 20.7550 4.7570 4 -1 1 -14 22.5438 4.6104 4 1 1 14 13.5290 4.1758 1 -1 -1 14 15.5165 4.1145 1 1 -1 14 19.0643 4.3778 1 -1 1 14 17.3764 4.1046 1 1 -2 -14 153.356 11.242 4 -2 -1 -14 158.752 11.128 4 2 1 -14 148.342 10.798 4 -1 2 -14 169.344 10.732 4 -1 2 14 161.945 10.335 1 2 1 14 157.293 9.742 1 -2 -1 14 166.809 10.528 1 1 -2 14 161.437 10.048 1 2 0 -14 6.51240 4.24016 4 0 2 -14 1.41953 3.66282 4 0 -2 -14 6.31695 4.09501 4 -2 0 -14 5.19778 4.01626 4 -2 0 14 6.22306 4.07871 1 0 -2 14 2.04294 3.39842 1 0 2 14 5.10333 3.58448 1 2 0 14 4.67181 3.70426 1 1 2 -14 156.848 10.650 4 2 -1 -14 170.875 11.487 4 -2 1 -14 163.927 10.906 4 -1 -2 -14 151.272 11.090 4 1 2 14 171.676 10.334 1 2 -1 14 173.926 10.116 1 -1 -2 14 157.145 10.422 1 -2 1 14 158.121 10.478 1 -2 2 -14 79.8786 6.9104 4 -2 -2 -14 76.9673 7.7294 4 2 2 -14 72.0668 7.1266 4 2 -2 -14 71.0288 7.3056 4 -2 2 14 81.3825 7.1656 1 2 -2 14 78.3771 6.6408 2 2 -2 14 84.5670 6.7597 1 2 2 14 67.6608 6.4490 1 -2 -2 14 74.0671 6.9386 1 -3 -2 -14 4.70869 4.30194 4 3 2 -14 -1.6071 3.8248 4 -2 3 -14 3.80586 3.41386 4 2 -3 -14 0.07727 3.91114 4 -3 -2 14 -1.0485 3.8375 1 2 -3 14 3.34173 3.35398 1 -2 3 14 -0.3337 3.7164 1 3 2 14 -4.1129 3.3020 1 1 -3 -14 71.8589 7.3078 4 3 1 -14 68.9820 6.8328 4 -3 -1 -14 67.3187 6.9850 4 -1 3 -14 62.2414 6.2088 4 -1 3 14 66.3183 6.3098 1 -3 -1 14 54.5287 6.2857 1 1 -3 14 58.5248 5.8610 1 3 1 14 61.8981 6.0387 1 0 -3 -14 0.81088 4.37197 4 -3 0 -14 3.61053 4.02751 4 3 0 -14 0.40307 3.60691 4 0 3 -14 -2.4167 3.4700 4 3 0 14 1.21488 3.49022 1 0 3 14 1.36783 3.74899 1 0 -3 14 -0.8208 3.6328 1 -3 0 14 -1.9521 3.4508 1 3 -1 -14 63.5117 7.0759 4 1 3 -14 61.4224 6.3455 4 -1 -3 -14 67.8332 7.4061 4 -3 1 -14 74.4704 6.6860 4 -1 -3 14 66.9577 6.6836 1 3 -1 14 61.8199 5.9469 1 1 3 14 68.0646 6.2239 1 -3 1 14 62.6411 6.6656 1 -2 -3 -14 -1.5516 3.8248 4 -3 2 -14 4.04654 3.89638 4 2 3 -14 -3.1673 3.2376 4 3 -2 -14 0.90698 3.87348 4 2 3 14 -2.1081 3.4528 1 -2 -3 14 -0.3161 3.4945 1 -3 2 14 -0.7575 3.5025 1 3 -2 14 2.89574 3.52903 2 3 -2 14 -1.4348 3.3028 1 3 -3 -14 5.14515 4.43952 4 -3 -3 -14 0.77173 3.81915 4 3 3 -14 4.19341 3.89510 4 -3 -3 14 -6.0459 3.8018 1 3 -3 14 5.00407 3.76215 2 -3 3 14 3.36213 3.91518 1 3 3 14 6.18466 3.70746 1 -4 -3 -14 84.3190 8.0659 4 4 3 -14 75.6533 7.2513 4 3 -4 -14 74.2457 7.7882 4 -3 4 14 87.6549 7.2358 1 4 3 14 72.8487 6.5498 1 -4 -3 14 79.6287 7.6723 1 4 2 -14 1.15135 4.07655 4 -4 -2 -14 -1.0753 4.0956 4 2 -4 -14 1.49128 4.62989 4 4 2 14 -1.3454 3.4525 1 -2 4 14 -1.6384 3.7534 1 -4 -2 14 2.23092 4.24560 1 4 1 -14 0.02713 4.07210 4 -4 -1 -14 1.89907 3.97771 4 1 -4 -14 -3.4217 4.3315 4 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4.72149 4 -4 4 14 10.9893 4.3172 1 4 4 14 6.70225 3.90692 1 -4 -4 14 8.43139 4.18094 1 4 -4 14 5.58981 3.73876 2 3 -5 -14 14.0735 5.3544 4 -5 -3 -14 12.4503 4.8087 4 5 3 -14 14.2477 4.5673 4 5 3 14 8.37952 3.81808 1 -3 5 14 13.7783 4.4333 1 -5 -3 14 10.3459 4.7131 1 5 2 -14 22.8414 4.6962 4 -5 -2 -14 22.5748 5.0874 4 2 -5 -14 20.4348 5.2071 4 -2 5 14 16.6259 4.3408 1 -5 -2 14 20.7081 4.8117 1 5 2 14 19.9989 4.2120 1 -5 -1 -14 105.411 8.676 4 5 1 -14 104.869 8.743 4 1 -5 -14 101.175 8.963 4 -5 -1 14 105.160 8.766 1 -1 5 14 109.599 8.215 1 5 1 14 100.323 7.312 1 0 5 -14 1.33113 3.37550 4 -5 0 -14 2.17725 4.20719 4 0 -5 -14 -0.8097 4.6073 4 5 0 -14 4.31247 3.97446 4 0 -5 14 1.43291 3.74555 1 0 5 14 0.38811 3.71904 1 -5 0 14 -3.7500 3.9743 1 5 -1 -14 114.909 9.194 4 1 5 -14 110.919 8.103 4 -1 -5 -14 89.9832 9.4088 4 -5 1 14 119.360 8.492 1 1 5 14 102.707 7.775 1 5 -1 14 123.282 8.856 2 -1 -5 14 104.614 8.276 1 2 5 -14 20.2426 4.3346 4 5 -2 -14 23.5384 5.2378 4 -2 -5 -14 18.2027 5.5158 4 5 -2 14 23.8212 4.8124 2 -2 -5 14 22.4337 4.9540 1 -5 2 14 19.2569 4.5628 1 2 5 14 18.9477 4.1260 1 3 5 -14 11.1339 4.1469 4 -3 -5 -14 10.6652 5.1567 4 5 -3 -14 14.4128 5.1111 4 5 -3 14 10.6406 4.1816 2 -5 3 14 9.44751 4.37548 1 -3 -5 14 9.17294 4.55066 1 3 5 14 10.7868 3.8449 1 6 1 -14 20.4301 5.1193 4 1 -6 -14 22.1635 5.5235 4 -1 6 14 29.0805 4.6923 1 -6 -1 14 27.6795 5.4097 1 6 0 -14 31.4074 5.6337 4 0 -6 -14 24.5955 6.0302 4 -6 0 14 30.8552 5.5185 1 6 0 14 39.0328 5.6692 2 0 6 14 30.6426 5.1181 1 1 6 -14 28.3457 4.4811 4 6 -1 -14 24.7358 5.0490 4 -1 -6 -14 26.2096 5.9298 4 -6 1 14 25.7553 4.9457 1 6 -1 14 19.1556 4.9208 2 -1 -6 14 15.9296 4.2973 1 1 6 14 24.6130 4.4625 1 0 0 15 2.65854 4.19231 1 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 81609 _shelx_SHELXL_version_number '2014/7' _olex2_diffrn_ambient_temperature_device 'Oxford Cryosystems' _olex2_exptl_crystal_mounting_method 'The crystal was mounted on a glass fibre in oil' _olex2_submission_original_sample_id jjw0305 _olex2_submission_special_instructions 'No special instructions were received'