data_mo_l1r_1_0m_a
_audit_creation_date               2022-02-03
_audit_creation_method
;
Olex2 1.5
(compiled 2021.12.09 svn.r5202d8cf for OlexSys, GUI svn.r6439)
;
_shelx_SHELXL_version_number       '2018/3'
_audit_contact_author_address      ?
_audit_contact_author_email        ?
_audit_contact_author_name         ''
_audit_contact_author_phone        ?
_publ_contact_author_id_orcid      ?
_publ_section_references
;
Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H.
 (2009), J. Appl. Cryst. 42, 339-341.

Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8.
;
_chemical_name_common              ?
_chemical_name_systematic          ?
_chemical_formula_moiety           'C29 H24 N2 O2'
_chemical_formula_sum              'C29 H24 N2 O2'
_chemical_formula_weight           432.50
_chemical_melting_point            ?
loop_
  _atom_type_symbol
  _atom_type_description
  _atom_type_scat_dispersion_real
  _atom_type_scat_dispersion_imag
  _atom_type_scat_source
 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system        'monoclinic'
_space_group_IT_number             14
_space_group_name_H-M_alt          'P 1 21/c 1'
_space_group_name_Hall             '-P 2ybc'
loop_
  _space_group_symop_operation_xyz
 'x, y, z'
 '-x, y+1/2, -z+1/2'
 '-x, -y, -z'
 'x, -y-1/2, z-1/2'

_cell_length_a                     6.1666(7)
_cell_length_b                     19.363(2)
_cell_length_c                     18.960(2)
_cell_angle_alpha                  90
_cell_angle_beta                   93.007(4)
_cell_angle_gamma                  90
_cell_volume                       2260.8(5)
_cell_formula_units_Z              4
_cell_measurement_reflns_used      32652
_cell_measurement_temperature      200(2)
_cell_measurement_theta_max        55.15
_cell_measurement_theta_min 0 
_cell_measurement_theta_details
;
'We failed to resue theta min from the integration'
;
_shelx_estimated_absorpt_T_max     0.994
_shelx_estimated_absorpt_T_min     0.988
_exptl_absorpt_coefficient_mu      0.080
_exptl_absorpt_correction_T_max    ?
_exptl_absorpt_correction_T_min    ?
_exptl_absorpt_correction_type     ?
_exptl_absorpt_process_details     ?
_exptl_absorpt_special_details     ?
_exptl_crystal_colour              'clear light red'
_exptl_crystal_colour_lustre       clear
_exptl_crystal_colour_modifier     light
_exptl_crystal_colour_primary      red
_exptl_crystal_density_diffrn      1.271
_exptl_crystal_density_meas        ?
_exptl_crystal_density_method      ?
_exptl_crystal_description         block
_exptl_crystal_F_000               912
_exptl_crystal_preparation         ?
_exptl_crystal_recrystallization_method  ?
_exptl_crystal_size_max            0.15
_exptl_crystal_size_mid            0.1
_exptl_crystal_size_min            0.08
_exptl_transmission_factor_max     ?
_exptl_transmission_factor_min     ?
_diffrn_reflns_av_R_equivalents    0.1604
_diffrn_reflns_av_unetI/netI       0.1095
_diffrn_reflns_Laue_measured_fraction_full  0.999
_diffrn_reflns_Laue_measured_fraction_max  0.993
_diffrn_reflns_limit_h_max         8
_diffrn_reflns_limit_h_min         -7
_diffrn_reflns_limit_k_max         25
_diffrn_reflns_limit_k_min         -25
_diffrn_reflns_limit_l_max         24
_diffrn_reflns_limit_l_min         -24
_diffrn_reflns_number              32156
_diffrn_reflns_point_group_measured_fraction_full  0.999
_diffrn_reflns_point_group_measured_fraction_max  0.993
_diffrn_reflns_theta_full          25.242
_diffrn_reflns_theta_max           27.580
_diffrn_reflns_theta_min           2.363
_diffrn_ambient_temperature        199.97
_diffrn_detector_area_resol_mean   ?
_diffrn_measured_fraction_theta_full  0.999
_diffrn_measured_fraction_theta_max  0.993
_diffrn_measurement_device_type    'Bruker UNI-500'
_diffrn_measurement_method         ?
_diffrn_radiation_type             MoK\a
_diffrn_radiation_wavelength       0.71073
_diffrn_source                     ?
_diffrn_special_details            ?
_reflns_Friedel_coverage           0.000
_reflns_Friedel_fraction_full      .
_reflns_Friedel_fraction_max       .
_reflns_number_gt                  2526
_reflns_number_total               5195
_reflns_special_details
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression       'I > 2σ(I)'
_computing_cell_refinement         ?
_computing_data_collection         ?
_computing_data_reduction          ?
_computing_molecular_graphics      'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement    'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution      'SHELXT 2014/5 (Sheldrick, 2014)'
_refine_diff_density_max           0.185
_refine_diff_density_min           -0.228
_refine_diff_density_rms           0.048
_refine_ls_extinction_coef         .
_refine_ls_extinction_method       none
_refine_ls_goodness_of_fit_ref     1.038
_refine_ls_hydrogen_treatment      constr
_refine_ls_matrix_type             full
_refine_ls_number_parameters       298
_refine_ls_number_reflns           5195
_refine_ls_number_restraints       0
_refine_ls_R_factor_all            0.1728
_refine_ls_R_factor_gt             0.0726
_refine_ls_restrained_S_all        1.038
_refine_ls_shift/su_max            0.000
_refine_ls_shift/su_mean           0.000
_refine_ls_structure_factor_coef   Fsqd
_refine_ls_weighting_details      
 'w=1/[σ²(Fo²)+(0.0495P)²+0.4074P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme        calc
_refine_ls_wR_factor_gt            0.1292
_refine_ls_wR_factor_ref           0.1689
_refine_special_details            ?
_olex2_refinement_description
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups
2.a Secondary CH2 refined with riding coordinates:
 C1(H1A,H1B), C2(H2A,H2B), C3(H3A,H3B), C15(H15A,H15B), C16(H16A,H16B)
2.b Aromatic/amide H refined with riding coordinates:
 C6(H6), C11(H11), C12(H12), C17(H17), C18(H18), C19(H19), C20(H20), C22(H22),
 C23(H23), C25(H25), C26(H26), C27(H27), C28(H28), C29(H29)
;
_atom_sites_solution_hydrogens     geom
_atom_sites_solution_primary       ?
_atom_sites_solution_secondary     ?
loop_
  _atom_site_label
  _atom_site_type_symbol
  _atom_site_fract_x
  _atom_site_fract_y
  _atom_site_fract_z
  _atom_site_U_iso_or_equiv
  _atom_site_adp_type
  _atom_site_occupancy
  _atom_site_site_symmetry_order
  _atom_site_calc_flag
  _atom_site_refinement_flags_posn
  _atom_site_refinement_flags_adp
  _atom_site_refinement_flags_occupancy
  _atom_site_disorder_assembly
  _atom_site_disorder_group
 O1 O 0.5780(3) 0.08231(11) 0.27902(11) 0.0555(6) Uani 1 1 d . . . . .
 O2 O 0.3384(3) 0.16962(9) 0.28012(10) 0.0438(5) Uani 1 1 d . . . . .
 N1 N -0.0768(4) 0.39804(11) 0.28054(12) 0.0384(6) Uani 1 1 d . . . . .
 N2 N 1.4387(5) 0.03910(15) 0.58304(15) 0.0632(8) Uani 1 1 d . . . . .
 C1 C 0.0438(5) 0.53257(15) 0.33583(17) 0.0518(9) Uani 1 1 d . . . . .
 H1A H 0.081755 0.560121 0.378702 0.062 Uiso 1 1 calc R U . . .
 H1B H 0.051309 0.563285 0.294279 0.062 Uiso 1 1 calc R U . . .
 C2 C 0.2051(5) 0.47387(15) 0.33010(19) 0.0545(9) Uani 1 1 d . . . . .
 H2A H 0.351168 0.492973 0.322862 0.065 Uiso 1 1 calc R U . . .
 H2B H 0.212831 0.447044 0.374608 0.065 Uiso 1 1 calc R U . . .
 C3 C 0.1379(5) 0.42694(14) 0.26929(16) 0.0442(8) Uani 1 1 d . . . . .
 H3A H 0.133596 0.453326 0.224509 0.053 Uiso 1 1 calc R U . . .
 H3B H 0.244971 0.389146 0.265839 0.053 Uiso 1 1 calc R U . . .
 C4 C -0.1383(4) 0.33829(14) 0.24214(14) 0.0364(7) Uani 1 1 d . . . . .
 C5 C -0.0197(4) 0.27634(13) 0.25346(15) 0.0366(7) Uani 1 1 d . . . . .
 C6 C 0.1495(4) 0.27354(14) 0.30947(15) 0.0376(7) Uani 1 1 d . . . . .
 H6 H 0.150395 0.311205 0.341599 0.045 Uiso 1 1 calc R U . . .
 C7 C 0.3053(4) 0.22614(13) 0.32316(15) 0.0357(7) Uani 1 1 d . . . . .
 C8 C 0.4703(4) 0.22556(13) 0.38046(15) 0.0356(7) Uani 1 1 d . . . . .
 C9 C 0.6015(4) 0.17012(14) 0.37219(15) 0.0371(7) Uani 1 1 d . . . . .
 C10 C 0.7849(4) 0.14341(13) 0.41629(16) 0.0379(7) Uani 1 1 d . . . . .
 C11 C 0.9474(5) 0.10359(14) 0.38809(17) 0.0439(8) Uani 1 1 d . . . . .
 H11 H 0.941782 0.094750 0.338743 0.053 Uiso 1 1 calc R U . . .
 C12 C 1.1163(5) 0.07666(14) 0.43012(16) 0.0444(8) Uani 1 1 d . . . . .
 H12 H 1.224578 0.049257 0.409826 0.053 Uiso 1 1 calc R U . . .
 C13 C 1.1271(5) 0.08982(14) 0.50216(16) 0.0401(7) Uani 1 1 d . . . . .
 C14 C 1.3007(5) 0.06143(15) 0.54733(18) 0.0471(8) Uani 1 1 d . . . . .
 C15 C -0.1819(5) 0.50485(15) 0.33952(18) 0.0514(9) Uani 1 1 d . . . . .
 H15A H -0.286222 0.543709 0.336182 0.062 Uiso 1 1 calc R U . . .
 H15B H -0.196190 0.482137 0.385830 0.062 Uiso 1 1 calc R U . . .
 C16 C -0.2388(5) 0.45349(17) 0.28125(19) 0.0625(10) Uani 1 1 d . . . . .
 H16A H -0.383635 0.433403 0.288471 0.075 Uiso 1 1 calc R U . . .
 H16B H -0.245691 0.477534 0.235103 0.075 Uiso 1 1 calc R U . . .
 C17 C -0.0805(5) 0.21803(15) 0.21388(17) 0.0518(8) Uani 1 1 d . . . . .
 H17 H 0.003298 0.177004 0.219088 0.062 Uiso 1 1 calc R U . . .
 C18 C -0.2599(5) 0.21891(17) 0.16742(17) 0.0565(9) Uani 1 1 d . . . . .
 H18 H -0.300604 0.178445 0.141655 0.068 Uiso 1 1 calc R U . . .
 C19 C -0.3794(5) 0.27809(16) 0.15839(16) 0.0493(8) Uani 1 1 d . . . . .
 H19 H -0.504574 0.278359 0.126955 0.059 Uiso 1 1 calc R U . . .
 C20 C -0.3191(5) 0.33735(15) 0.19468(15) 0.0441(8) Uani 1 1 d . . . . .
 H20 H -0.402130 0.378279 0.187240 0.053 Uiso 1 1 calc R U . . .
 C21 C 0.5190(5) 0.13387(16) 0.30793(17) 0.0445(8) Uani 1 1 d . . . . .
 C22 C 0.9671(5) 0.12950(16) 0.53121(17) 0.0495(8) Uani 1 1 d . . . . .
 H22 H 0.973954 0.138495 0.580532 0.059 Uiso 1 1 calc R U . . .
 C23 C 0.7994(5) 0.15580(15) 0.48927(16) 0.0449(8) Uani 1 1 d . . . . .
 H23 H 0.691018 0.182875 0.509949 0.054 Uiso 1 1 calc R U . . .
 C24 C 0.4811(4) 0.28135(13) 0.43381(14) 0.0356(7) Uani 1 1 d . . . . .
 C25 C 0.6574(5) 0.32567(15) 0.43838(15) 0.0452(8) Uani 1 1 d . . . . .
 H25 H 0.774918 0.318319 0.408797 0.054 Uiso 1 1 calc R U . . .
 C26 C 0.6656(6) 0.38037(17) 0.48518(17) 0.0582(9) Uani 1 1 d . . . . .
 H26 H 0.787498 0.410458 0.487592 0.070 Uiso 1 1 calc R U . . .
 C27 C 0.4965(7) 0.39097(18) 0.52817(18) 0.0647(10) Uani 1 1 d . . . . .
 H27 H 0.500683 0.428865 0.560030 0.078 Uiso 1 1 calc R U . . .
 C28 C 0.3214(6) 0.34709(19) 0.52538(17) 0.0630(10) Uani 1 1 d . . . . .
 H28 H 0.206097 0.354464 0.555841 0.076 Uiso 1 1 calc R U . . .
 C29 C 0.3114(5) 0.29206(17) 0.47842(16) 0.0514(9) Uani 1 1 d . . . . .
 H29 H 0.189735 0.261878 0.476667 0.062 Uiso 1 1 calc R U . . .


_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
  _geom_bond_atom_site_label_1
  _geom_bond_atom_site_label_2
  _geom_bond_distance
  _geom_bond_site_symmetry_2
  _geom_bond_publ_flag
 O1 C21 1.204(3) . ?
 O2 C7 1.387(3) . ?
 O2 C21 1.391(3) . ?
 N1 C3 1.463(3) . ?
 N1 C4 1.409(3) . ?
 N1 C16 1.467(3) . ?
 N2 C14 1.144(4) . ?
 C1 H1A 0.9900 . ?
 C1 H1B 0.9900 . ?
 C1 C2 1.518(4) . ?
 C1 C15 1.497(4) . ?
 C2 H2A 0.9900 . ?
 C2 H2B 0.9900 . ?
 C2 C3 1.509(4) . ?
 C3 H3A 0.9900 . ?
 C3 H3B 0.9900 . ?
 C4 C5 1.416(4) . ?
 C4 C20 1.395(4) . ?
 C5 C6 1.450(4) . ?
 C5 C17 1.396(4) . ?
 C6 H6 0.9500 . ?
 C6 C7 1.344(4) . ?
 C7 C8 1.449(4) . ?
 C8 C9 1.358(4) . ?
 C8 C24 1.479(4) . ?
 C9 C10 1.465(4) . ?
 C9 C21 1.473(4) . ?
 C10 C11 1.393(4) . ?
 C10 C23 1.403(4) . ?
 C11 H11 0.9500 . ?
 C11 C12 1.380(4) . ?
 C12 H12 0.9500 . ?
 C12 C13 1.388(4) . ?
 C13 C14 1.444(4) . ?
 C13 C22 1.387(4) . ?
 C15 H15A 0.9900 . ?
 C15 H15B 0.9900 . ?
 C15 C16 1.514(4) . ?
 C16 H16A 0.9900 . ?
 C16 H16B 0.9900 . ?
 C17 H17 0.9500 . ?
 C17 C18 1.378(4) . ?
 C18 H18 0.9500 . ?
 C18 C19 1.368(4) . ?
 C19 H19 0.9500 . ?
 C19 C20 1.379(4) . ?
 C20 H20 0.9500 . ?
 C22 H22 0.9500 . ?
 C22 C23 1.369(4) . ?
 C23 H23 0.9500 . ?
 C24 C25 1.384(4) . ?
 C24 C29 1.395(4) . ?
 C25 H25 0.9500 . ?
 C25 C26 1.381(4) . ?
 C26 H26 0.9500 . ?
 C26 C27 1.372(5) . ?
 C27 H27 0.9500 . ?
 C27 C28 1.373(5) . ?
 C28 H28 0.9500 . ?
 C28 C29 1.388(4) . ?
 C29 H29 0.9500 . ?

loop_
  _geom_angle_atom_site_label_1
  _geom_angle_atom_site_label_2
  _geom_angle_atom_site_label_3
  _geom_angle
  _geom_angle_site_symmetry_1
  _geom_angle_site_symmetry_3
  _geom_angle_publ_flag
 C7 O2 C21 108.0(2) . . ?
 C3 N1 C16 110.1(2) . . ?
 C4 N1 C3 117.4(2) . . ?
 C4 N1 C16 116.1(2) . . ?
 H1A C1 H1B 108.1 . . ?
 C2 C1 H1A 109.6 . . ?
 C2 C1 H1B 109.6 . . ?
 C15 C1 H1A 109.6 . . ?
 C15 C1 H1B 109.6 . . ?
 C15 C1 C2 110.4(2) . . ?
 C1 C2 H2A 109.5 . . ?
 C1 C2 H2B 109.5 . . ?
 H2A C2 H2B 108.1 . . ?
 C3 C2 C1 110.6(3) . . ?
 C3 C2 H2A 109.5 . . ?
 C3 C2 H2B 109.5 . . ?
 N1 C3 C2 109.5(2) . . ?
 N1 C3 H3A 109.8 . . ?
 N1 C3 H3B 109.8 . . ?
 C2 C3 H3A 109.8 . . ?
 C2 C3 H3B 109.8 . . ?
 H3A C3 H3B 108.2 . . ?
 N1 C4 C5 119.6(3) . . ?
 C20 C4 N1 121.9(3) . . ?
 C20 C4 C5 118.4(3) . . ?
 C4 C5 C6 119.3(2) . . ?
 C17 C5 C4 118.8(3) . . ?
 C17 C5 C6 121.7(3) . . ?
 C5 C6 H6 114.9 . . ?
 C7 C6 C5 130.3(3) . . ?
 C7 C6 H6 114.9 . . ?
 O2 C7 C8 108.4(2) . . ?
 C6 C7 O2 123.4(3) . . ?
 C6 C7 C8 128.1(3) . . ?
 C7 C8 C24 120.8(2) . . ?
 C9 C8 C7 108.6(2) . . ?
 C9 C8 C24 130.6(3) . . ?
 C8 C9 C10 131.3(3) . . ?
 C8 C9 C21 106.9(3) . . ?
 C10 C9 C21 121.8(2) . . ?
 C11 C10 C9 121.7(3) . . ?
 C11 C10 C23 117.6(3) . . ?
 C23 C10 C9 120.7(2) . . ?
 C10 C11 H11 119.2 . . ?
 C12 C11 C10 121.6(3) . . ?
 C12 C11 H11 119.2 . . ?
 C11 C12 H12 120.2 . . ?
 C11 C12 C13 119.7(3) . . ?
 C13 C12 H12 120.2 . . ?
 C12 C13 C14 120.7(3) . . ?
 C22 C13 C12 119.6(3) . . ?
 C22 C13 C14 119.7(3) . . ?
 N2 C14 C13 179.8(4) . . ?
 C1 C15 H15A 109.1 . . ?
 C1 C15 H15B 109.1 . . ?
 C1 C15 C16 112.5(3) . . ?
 H15A C15 H15B 107.8 . . ?
 C16 C15 H15A 109.1 . . ?
 C16 C15 H15B 109.1 . . ?
 N1 C16 C15 110.8(3) . . ?
 N1 C16 H16A 109.5 . . ?
 N1 C16 H16B 109.5 . . ?
 C15 C16 H16A 109.5 . . ?
 C15 C16 H16B 109.5 . . ?
 H16A C16 H16B 108.1 . . ?
 C5 C17 H17 119.4 . . ?
 C18 C17 C5 121.2(3) . . ?
 C18 C17 H17 119.4 . . ?
 C17 C18 H18 120.0 . . ?
 C19 C18 C17 120.0(3) . . ?
 C19 C18 H18 120.0 . . ?
 C18 C19 H19 119.8 . . ?
 C18 C19 C20 120.3(3) . . ?
 C20 C19 H19 119.8 . . ?
 C4 C20 H20 119.4 . . ?
 C19 C20 C4 121.2(3) . . ?
 C19 C20 H20 119.4 . . ?
 O1 C21 O2 119.7(3) . . ?
 O1 C21 C9 132.2(3) . . ?
 O2 C21 C9 108.1(2) . . ?
 C13 C22 H22 119.8 . . ?
 C23 C22 C13 120.5(3) . . ?
 C23 C22 H22 119.8 . . ?
 C10 C23 H23 119.5 . . ?
 C22 C23 C10 121.1(3) . . ?
 C22 C23 H23 119.5 . . ?
 C25 C24 C8 120.2(2) . . ?
 C25 C24 C29 118.8(3) . . ?
 C29 C24 C8 121.0(3) . . ?
 C24 C25 H25 119.4 . . ?
 C26 C25 C24 121.2(3) . . ?
 C26 C25 H25 119.4 . . ?
 C25 C26 H26 120.2 . . ?
 C27 C26 C25 119.5(3) . . ?
 C27 C26 H26 120.2 . . ?
 C26 C27 H27 119.8 . . ?
 C26 C27 C28 120.4(3) . . ?
 C28 C27 H27 119.8 . . ?
 C27 C28 H28 119.7 . . ?
 C27 C28 C29 120.5(3) . . ?
 C29 C28 H28 119.7 . . ?
 C24 C29 H29 120.2 . . ?
 C28 C29 C24 119.6(3) . . ?
 C28 C29 H29 120.2 . . ?

loop_
  _geom_torsion_atom_site_label_1
  _geom_torsion_atom_site_label_2
  _geom_torsion_atom_site_label_3
  _geom_torsion_atom_site_label_4
  _geom_torsion
  _geom_torsion_site_symmetry_1
  _geom_torsion_site_symmetry_2
  _geom_torsion_site_symmetry_3
  _geom_torsion_site_symmetry_4
  _geom_torsion_publ_flag
 O2 C7 C8 C9 0.3(3) . . . . ?
 O2 C7 C8 C24 177.8(2) . . . . ?
 N1 C4 C5 C6 6.2(4) . . . . ?
 N1 C4 C5 C17 -178.7(3) . . . . ?
 N1 C4 C20 C19 -178.9(3) . . . . ?
 C1 C2 C3 N1 -59.9(3) . . . . ?
 C1 C15 C16 N1 53.9(4) . . . . ?
 C2 C1 C15 C16 -50.6(4) . . . . ?
 C3 N1 C4 C5 63.4(3) . . . . ?
 C3 N1 C4 C20 -119.1(3) . . . . ?
 C3 N1 C16 C15 -59.6(4) . . . . ?
 C4 N1 C3 C2 -161.1(3) . . . . ?
 C4 N1 C16 C15 163.9(3) . . . . ?
 C4 C5 C6 C7 -167.8(3) . . . . ?
 C4 C5 C17 C18 -3.7(4) . . . . ?
 C5 C4 C20 C19 -1.3(4) . . . . ?
 C5 C6 C7 O2 3.8(5) . . . . ?
 C5 C6 C7 C8 -179.5(3) . . . . ?
 C5 C17 C18 C19 1.3(5) . . . . ?
 C6 C5 C17 C18 171.2(3) . . . . ?
 C6 C7 C8 C9 -176.7(3) . . . . ?
 C6 C7 C8 C24 0.7(4) . . . . ?
 C7 O2 C21 O1 179.7(3) . . . . ?
 C7 O2 C21 C9 0.4(3) . . . . ?
 C7 C8 C9 C10 -176.6(3) . . . . ?
 C7 C8 C9 C21 -0.1(3) . . . . ?
 C7 C8 C24 C25 -114.1(3) . . . . ?
 C7 C8 C24 C29 63.4(4) . . . . ?
 C8 C9 C10 C11 -155.1(3) . . . . ?
 C8 C9 C10 C23 26.6(4) . . . . ?
 C8 C9 C21 O1 -179.4(3) . . . . ?
 C8 C9 C21 O2 -0.2(3) . . . . ?
 C8 C24 C25 C26 176.5(3) . . . . ?
 C8 C24 C29 C28 -176.6(3) . . . . ?
 C9 C8 C24 C25 62.7(4) . . . . ?
 C9 C8 C24 C29 -119.7(3) . . . . ?
 C9 C10 C11 C12 -177.9(3) . . . . ?
 C9 C10 C23 C22 178.2(3) . . . . ?
 C10 C9 C21 O1 -2.5(5) . . . . ?
 C10 C9 C21 O2 176.7(2) . . . . ?
 C10 C11 C12 C13 -0.6(4) . . . . ?
 C11 C10 C23 C22 -0.1(4) . . . . ?
 C11 C12 C13 C14 179.2(3) . . . . ?
 C11 C12 C13 C22 0.5(4) . . . . ?
 C12 C13 C22 C23 -0.1(4) . . . . ?
 C13 C22 C23 C10 0.0(5) . . . . ?
 C14 C13 C22 C23 -178.9(3) . . . . ?
 C15 C1 C2 C3 53.5(4) . . . . ?
 C16 N1 C3 C2 63.0(3) . . . . ?
 C16 N1 C4 C5 -163.4(3) . . . . ?
 C16 N1 C4 C20 14.2(4) . . . . ?
 C17 C5 C6 C7 17.3(5) . . . . ?
 C17 C18 C19 C20 1.1(5) . . . . ?
 C18 C19 C20 C4 -1.1(5) . . . . ?
 C20 C4 C5 C6 -171.5(2) . . . . ?
 C20 C4 C5 C17 3.6(4) . . . . ?
 C21 O2 C7 C6 176.8(3) . . . . ?
 C21 O2 C7 C8 -0.4(3) . . . . ?
 C21 C9 C10 C11 28.8(4) . . . . ?
 C21 C9 C10 C23 -149.5(3) . . . . ?
 C23 C10 C11 C12 0.5(4) . . . . ?
 C24 C8 C9 C10 6.3(5) . . . . ?
 C24 C8 C9 C21 -177.2(3) . . . . ?
 C24 C25 C26 C27 0.2(5) . . . . ?
 C25 C24 C29 C28 0.9(4) . . . . ?
 C25 C26 C27 C28 0.8(5) . . . . ?
 C26 C27 C28 C29 -0.9(5) . . . . ?
 C27 C28 C29 C24 0.1(5) . . . . ?
 C29 C24 C25 C26 -1.1(4) . . . . ?

_database_code_depnum_ccdc_archive  ?
_olex2_submission_special_instructions  'No special instructions were received'
