data_209b2-295 _audit_creation_date 2021-03-22 _audit_creation_method ; Olex2 1.3 (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6272) ; _shelx_SHELXL_version_number '2018/3' loop_ _audit_author_name _audit_author_email _audit_author_address 'Straus, D.B.' dstraus@princeton.edu ; Princeton University Chemistry Frick Laboratory, Washington Road Princeton, NJ 08544 USA ; _audit_contact_author_address ; Princeton University Chemistry Frick Laboratory, Washington Road Princeton, NJ 08544 USA ; _audit_contact_author_email dstraus@princeton.edu _audit_contact_author_name 'Straus, D.B.' _audit_contact_author_phone '' _publ_contact_author_id_orcid 0000-0003-2977-5590 _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety '2(I4 Sn1), 0.893(C70)' _chemical_formula_sum 'C62.50 I8 Sn2' _chemical_formula_weight 2003.23 _chemical_absolute_configuration ad _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'I' 'I' -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Sn' 'Sn' -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'cubic' _space_group_IT_number 212 _space_group_name_H-M_alt 'P 43 3 2' _space_group_name_Hall 'P 4acd 2ab 3' loop_ _space_group_symop_operation_xyz 'x, y, z' '-y+3/4, x+1/4, z+3/4' '-x+1/2, -y, z+1/2' 'y+3/4, -x+3/4, z+1/4' 'x+3/4, -z+3/4, y+1/4' 'x+1/2, -y+1/2, -z' 'x+1/4, z+3/4, -y+3/4' 'z+1/4, y+3/4, -x+3/4' '-x, y+1/2, -z+1/2' '-z+3/4, y+1/4, x+3/4' 'z, x, y' 'y, z, x' '-y+1/2, -z, x+1/2' 'z+1/2, -x+1/2, -y' '-y, z+1/2, -x+1/2' '-z+1/2, -x, y+1/2' '-z, x+1/2, -y+1/2' 'y+1/2, -z+1/2, -x' 'y+1/4, x+3/4, -z+3/4' '-y+1/4, -x+1/4, -z+1/4' '-x+3/4, z+1/4, y+3/4' '-x+1/4, -z+1/4, -y+1/4' 'z+3/4, -y+3/4, x+1/4' '-z+1/4, -y+1/4, -x+1/4' _cell_length_a 16.7390(13) _cell_length_b 16.7390(13) _cell_length_c 16.7390(13) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 4690.2(11) _cell_formula_units_Z 4 _cell_measurement_reflns_used 5656 _cell_measurement_temperature 295 _cell_measurement_theta_max 29.14 _cell_measurement_theta_min 2.72 _shelx_estimated_absorpt_T_max 0.282 _shelx_estimated_absorpt_T_min 0.155 _exptl_absorpt_coefficient_mu 6.377 _exptl_absorpt_correction_T_max 1.0000 _exptl_absorpt_correction_T_min 0.7416 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2014/5 (Bruker,2014/5) was used for absorption correction. wR2(int) was 0.1431 before and 0.0461 after correction. The Ratio of minimum to maximum transmission is 0.7416. The \l/2 correction factor is 0.00150. ; _exptl_absorpt_special_details ? _exptl_crystal_colour black _exptl_crystal_colour_primary black _exptl_crystal_density_diffrn 2.837 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description irregular _exptl_crystal_F_000 3596 loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist -1.00 1.00 1.00 0.1870 1.00 -1.00 -1.00 0.1350 1.00 0.00 -1.00 0.1130 -1.00 0.00 1.00 0.1550 1.00 1.00 -1.00 0.1870 -1.00 -1.00 1.00 0.1200 -1.00 1.00 0.00 0.1000 -1.00 0.00 0.00 0.1330 1.00 0.00 0.00 0.1970 1.00 1.00 0.00 0.2350 -1.00 -1.00 0.00 0.1000 0.00 1.00 0.00 0.1990 0.00 -1.00 0.00 0.1350 -1.00 -1.00 -1.00 0.1430 1.00 1.00 1.00 0.2510 -1.00 0.00 -1.00 0.1260 1.00 0.00 1.00 0.1730 -1.00 1.00 -1.00 0.1290 1.00 -1.00 1.00 0.1140 0.00 -1.00 -1.00 0.1520 0.00 0.00 -1.00 0.1670 0.00 1.00 -1.00 0.1490 1.00 -1.00 2.00 0.1220 1.00 0.00 2.00 0.1590 1.00 -2.00 1.00 0.1050 2.00 -1.00 2.00 0.1150 -1.00 2.00 -1.00 0.1330 _exptl_crystal_size_max 0.467 _exptl_crystal_size_mid 0.308 _exptl_crystal_size_min 0.266 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0585 _diffrn_reflns_av_unetI/netI 0.0367 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 22 _diffrn_reflns_limit_h_min -20 _diffrn_reflns_limit_k_max 22 _diffrn_reflns_limit_k_min -22 _diffrn_reflns_limit_l_max 22 _diffrn_reflns_limit_l_min -8 _diffrn_reflns_number 18754 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 29.137 _diffrn_reflns_theta_min 1.720 _diffrn_ambient_temperature 295 _diffrn_detector_area_resol_mean ? _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_source 'sealed tube' _diffrn_source_current 30.0 _diffrn_source_power 1.5 _diffrn_source_voltage 50.0 _diffrn_standards_number 0 _reflns_Friedel_coverage 0.631 _reflns_Friedel_fraction_full 1.000 _reflns_Friedel_fraction_max 0.999 _reflns_number_gt 1380 _reflns_number_total 2127 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement ? _computing_data_collection ? _computing_data_reduction ? _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _refine_diff_density_max 0.903 _refine_diff_density_min -0.815 _refine_diff_density_rms 0.172 _refine_ls_abs_structure_details ; Flack x determined using 409 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.08(2) _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.163 _refine_ls_hydrogen_treatment undef _refine_ls_matrix_type full _refine_ls_number_parameters 42 _refine_ls_number_reflns 2127 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.1277 _refine_ls_R_factor_gt 0.0759 _refine_ls_restrained_S_all 1.163 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0471P)^2^+45.4265P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1507 _refine_ls_wR_factor_ref 0.1725 _refine_special_details ? _olex2_refinement_description ; 1. Uiso/Uaniso restraints and constraints Uiso(C13) = Uiso(C15) = Uiso(C16) = Uiso(C14) = Uiso(C23) = Uiso(C17) = Uiso(C21) = Uiso(C54) = Uiso(C24) = Uiso(C22) = Uiso(C18) = Uiso(C53) = Uiso(C20) = Uiso(C25) = Uiso(C12) = Uiso(C11) = Uiso(C35) = Uiso(C37) = Uiso(C19) = Uiso(C51) = Uiso(C52) = Uiso(C46) = Uiso(C26) = Uiso(C28) = Uiso(C10) = Uiso(C36) = Uiso(C34) = Uiso(C38) = Uiso(C48) = Uiso(C50) = Uiso(C55) = Uiso(C47) = Uiso(C27) = Uiso(C29) = Uiso(C9) = Uiso(C40) = Uiso(C33) = Uiso(C39) = Uiso(C49) = Uiso(C57) = Uiso(C56) = Uiso(C1) = Uiso(C31) = Uiso(C30) = Uiso(C8) = Uiso(C41) = Uiso(C32) = Uiso(C2) = Uiso(C59) = Uiso(C58) = Uiso(C60) = Uiso(C45) = Uiso(C7) = Uiso(C42) = Uiso(C43) = Uiso(C3) = Uiso(C6) = Uiso(C4) = Uiso(C44) = Uiso(C5) Uiso(C66) = Uiso(C72) = Uiso(C73) = Uiso(C130) = Uiso(C71) = Uiso(C74) = Uiso(C84) = Uiso(C129) = Uiso(C64) = Uiso(C127) = Uiso(C70) = Uiso(C75) = Uiso(C82) = Uiso(C85) = Uiso(C83) = Uiso(C128) = Uiso(C65) = Uiso(C63) = Uiso(C126) = Uiso(C69) = Uiso(C76) = Uiso(C81) = Uiso(C77) = Uiso(C86) = Uiso(C87) = Uiso(C102) = Uiso(C62) = Uiso(C123) = Uiso(C68) = Uiso(C101) = Uiso(C80) = Uiso(C78) = Uiso(C122) = Uiso(C88) = Uiso(C103) = Uiso(C61) = Uiso(C67) = Uiso(C104) = Uiso(C124) = Uiso(C125) = Uiso(C97) = Uiso(C79) = Uiso(C89) = Uiso(C98) = Uiso(C119) = Uiso(C120) = Uiso(C96) = Uiso(C110) = Uiso(C111) = Uiso(C105) = Uiso(C118) = Uiso(C112) = Uiso(C100) = Uiso(C90) = Uiso(C99) = Uiso(C121) = Uiso(C95) = Uiso(C109) = Uiso(C106) = Uiso(C117) = Uiso(C113) = Uiso(C91) = Uiso(C94) = Uiso(C116) = Uiso(C108) = Uiso(C107) = Uiso(C114) = Uiso(C92) = Uiso(C93) = Uiso(C115) 2. Others Sof(I2B)=1-FVAR(1) Sof(I2A)=FVAR(1) Fixed Sof: C72(0.04167) C81(0.04167) C91(0.04167) C108(0.04167) C66(0.04167) C65(0.04167) C73(0.04167) C80(0.04167) C92(0.04167) C109(0.04167) C102(0.04167) C123(0.04167) C101(0.04167) C122(0.04167) C97(0.04167) C119(0.04167) C96(0.04167) C118(0.04167) C103(0.04167) C124(0.04167) C128(0.04167) C126(0.04167) C76(0.04167) C86(0.04167) C98(0.04167) C120(0.04167) C95(0.04167) C117(0.04167) C104(0.04167) C125(0.04167) C129(0.04167) C127(0.04167) C77(0.04167) C87(0.04167) C99(0.04167) C121(0.04167) C106(0.04167) C113(0.04167) C62(0.04167) C68(0.04167) C63(0.04167) C69(0.04167) C75(0.04167) C85(0.04167) C78(0.04167) C88(0.04167) C94(0.04167) C116(0.04167) C105(0.04167) C112(0.04167) C130(0.04167) C71(0.04167) C82(0.04167) C83(0.04167) C100(0.04167) C90(0.04167) C107(0.04167) C114(0.04167) C61(0.04167) C67(0.04167) C64(0.04167) C70(0.04167) C74(0.04167) C84(0.04167) C79(0.04167) C89(0.04167) C93(0.04167) C115(0.04167) C110(0.04167) C111(0.04167) C15(0.125) C16(0.125) C14(0.125) C17(0.125) C18(0.125) C21(0.125) C20(0.125) C19(0.125) C25(0.125) C24(0.125) C13(0.125) C23(0.125) C22(0.125) C35(0.125) C36(0.125) C37(0.125) C28(0.125) C27(0.125) C12(0.125) C26(0.125) C34(0.125) C31(0.125) C32(0.125) C33(0.125) C10(0.125) C9(0.125) C11(0.125) C29(0.125) C30(0.125) C8(0.125) C7(0.125) C45(0.125) C53(0.125) C52(0.125) C54(0.125) C55(0.125) C56(0.125) C51(0.125) C50(0.125) C57(0.125) C5(0.125) C6(0.125) C58(0.125) C4(0.125) C42(0.125) C43(0.125) C44(0.125) C3(0.125) C39(0.125) C40(0.125) C41(0.125) C2(0.125) C47(0.125) C46(0.125) C38(0.125) C1(0.125) C59(0.125) C49(0.125) C48(0.125) C60(0.125) 3.a : C72(C81,C91,C108,C66,C65,C73,C80,C92,C109,C102,C123,C101,C122,C97,C119,C96, C118,C103,C124,C128,C126,C76,C86,C98,C120,C95,C117,C104,C125,C129,C127,C77,C87, C99,C121,C106,C113,C62,C68,C63,C69,C75,C85,C78,C88,C94,C116,C105,C112,C130,C71, C82,C83,C100,C90,C107,C114,C61,C67,C64,C70,C74,C84,C79,C89,C93,C115,C110,C111), C15(C16,C14,C17,C18,C21,C20,C19,C25,C24,C13,C23,C22,C35,C36,C37,C28,C27,C12, C26,C34,C31,C32,C33,C10,C9,C11,C29,C30,C8,C7,C45,C53,C52,C54,C55,C56,C51,C50, C57,C5,C6,C58,C4,C42,C43,C44,C3,C39,C40,C41,C2,C47,C46,C38,C1,C59,C49,C48,C60) ; _atom_sites_solution_hydrogens . _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Sn1 Sn -0.64883(7) -0.64883(7) -0.64883(7) 0.0512(5) Uani 1 3 d S T P . . I2A I -0.7190(13) -0.5177(12) -0.6018(12) 0.078(3) Uani 0.37(9) 1 d . . P A 2 I1 I -0.73977(8) -0.73977(8) -0.73977(8) 0.0922(9) Uani 1 3 d S T P A . I2B I -0.739(3) -0.5226(11) -0.6103(12) 0.093(4) Uani 0.63(9) 1 d . . P A 1 C72 C -0.870(4) -0.328(3) -0.678(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C81 C -0.695(3) -0.169(3) -0.714(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C91 C -0.774(3) 0.045(3) -0.644(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C108 C -0.998(3) 0.019(3) -0.565(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C66 C -1.058(3) -0.211(3) -0.586(4) 0.029(8) Uiso 0.0417 1 d G . P B -1 C65 C -1.015(3) -0.278(3) -0.615(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C73 C -0.794(4) -0.302(3) -0.702(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C80 C -0.691(3) -0.086(3) -0.700(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C92 C -0.848(4) 0.070(3) -0.611(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C109 C -1.048(3) -0.048(3) -0.559(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C102 C -0.825(4) -0.234(3) -0.432(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C123 C -0.982(4) -0.155(4) -0.850(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C101 C -0.750(4) -0.209(3) -0.455(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C122 C -0.907(4) -0.129(3) -0.873(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C97 C -0.745(4) -0.127(3) -0.442(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C119 C -0.902(4) -0.048(3) -0.859(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C96 C -0.817(4) -0.103(3) -0.410(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C118 C -0.974(4) -0.024(3) -0.827(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C103 C -0.867(4) -0.169(3) -0.404(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C124 C -1.023(4) -0.090(4) -0.821(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C128 C -0.863(4) -0.290(3) -0.474(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C126 C -0.990(4) -0.225(4) -0.814(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C76 C -0.716(4) -0.240(3) -0.520(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C86 C -0.843(4) -0.175(3) -0.860(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C98 C -0.707(4) -0.081(3) -0.493(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C120 C -0.834(4) -0.016(3) -0.833(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C95 C -0.848(4) -0.033(3) -0.431(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C117 C -0.975(4) 0.032(3) -0.771(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C104 C -0.944(4) -0.162(3) -0.419(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C125 C -1.072(3) -0.097(4) -0.759(4) 0.029(8) Uiso 0.0417 1 d G . P B -1 C129 C -0.827(4) -0.322(3) -0.542(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C127 C -0.924(4) -0.273(3) -0.799(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C77 C -0.676(4) -0.191(3) -0.574(4) 0.029(8) Uiso 0.0417 1 d G . P B -1 C87 C -0.773(3) -0.142(3) -0.831(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C99 C -0.739(4) -0.008(3) -0.516(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C121 C -0.836(4) 0.041(3) -0.773(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C106 C -0.929(4) -0.025(3) -0.448(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C113 C -1.025(3) 0.023(3) -0.705(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C62 C -0.983(4) -0.220(3) -0.464(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C68 C -1.080(3) -0.171(4) -0.721(4) 0.029(8) Uiso 0.0417 1 d G . P B -1 C63 C -0.944(4) -0.282(3) -0.491(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C69 C -1.040(3) -0.233(3) -0.748(4) 0.029(8) Uiso 0.0417 1 d G . P B -1 C75 C -0.756(4) -0.298(3) -0.565(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C85 C -0.852(4) -0.249(3) -0.822(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C78 C -0.672(4) -0.113(3) -0.561(4) 0.029(8) Uiso 0.0417 1 d G . P B -1 C88 C -0.768(3) -0.065(3) -0.818(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C94 C -0.808(4) 0.016(3) -0.485(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C116 C -0.904(4) 0.065(3) -0.742(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C105 C -0.976(4) -0.089(3) -0.442(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C112 C -1.072(3) -0.040(3) -0.699(4) 0.029(8) Uiso 0.0417 1 d G . P B -1 C130 C -0.887(4) -0.335(3) -0.599(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C71 C -0.935(4) -0.311(3) -0.726(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C82 C -0.691(3) -0.220(3) -0.650(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C83 C -0.739(3) -0.196(3) -0.778(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C100 C -0.722(4) 0.004(3) -0.596(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C90 C -0.770(3) 0.028(3) -0.723(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C107 C -0.938(4) 0.028(3) -0.511(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C114 C -0.985(3) 0.052(3) -0.638(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C61 C -1.039(4) -0.181(3) -0.512(4) 0.029(8) Uiso 0.0417 1 d G . P B -1 C67 C -1.087(3) -0.157(3) -0.640(4) 0.029(8) Uiso 0.0417 1 d G . P B -1 C64 C -0.957(4) -0.311(3) -0.568(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C70 C -1.005(3) -0.287(3) -0.695(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C74 C -0.739(4) -0.284(3) -0.645(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C84 C -0.786(3) -0.260(3) -0.772(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C79 C -0.682(3) -0.059(3) -0.623(4) 0.029(8) Uiso 0.0417 1 d G . P B -1 C89 C -0.729(3) -0.035(3) -0.751(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C93 C -0.865(4) 0.053(3) -0.533(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C115 C -0.913(4) 0.077(3) -0.661(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C110 C -1.035(4) -0.103(3) -0.499(3) 0.029(8) Uiso 0.0417 1 d G . P B -1 C111 C -1.083(3) -0.078(3) -0.626(4) 0.029(8) Uiso 0.0417 1 d G . P B -1 C15 C -0.7946(19) -0.1924(18) -0.4422(16) 0.061(4) Uiso 0.125 1 d G . P C -2 C16 C -0.7698(19) -0.1076(19) -0.4417(17) 0.061(4) Uiso 0.125 1 d G . P C -2 C14 C -0.7612(19) -0.2452(18) -0.4970(17) 0.061(4) Uiso 0.125 1 d G . P C -2 C17 C -0.7131(19) -0.0806(19) -0.4961(18) 0.061(4) Uiso 0.125 1 d G . P C -2 C18 C -0.724(2) -0.0028(19) -0.5364(18) 0.061(4) Uiso 0.125 1 d G . P C -2 C21 C -0.841(2) -0.0584(18) -0.4242(16) 0.061(4) Uiso 0.125 1 d G . P C -2 C20 C -0.851(2) 0.0148(18) -0.4621(17) 0.061(4) Uiso 0.125 1 d G . P C -2 C19 C -0.791(2) 0.0435(18) -0.5198(18) 0.061(4) Uiso 0.125 1 d G . P C -2 C25 C -0.8936(19) -0.3075(17) -0.5218(18) 0.061(4) Uiso 0.125 1 d G . P C -2 C24 C -0.9292(19) -0.2514(18) -0.4635(17) 0.061(4) Uiso 0.125 1 d G . P C -2 C13 C -0.812(2) -0.3045(17) -0.5380(17) 0.061(4) Uiso 0.125 1 d G . P C -2 C23 C -0.8812(19) -0.1956(18) -0.4249(16) 0.061(4) Uiso 0.125 1 d G . P C -2 C22 C -0.910(2) -0.1128(18) -0.4138(16) 0.061(4) Uiso 0.125 1 d G . P C -2 C35 C -1.0089(19) -0.2279(18) -0.4934(18) 0.061(4) Uiso 0.125 1 d G . P C -2 C36 C -1.0359(18) -0.1500(19) -0.4829(18) 0.061(4) Uiso 0.125 1 d G . P C -2 C37 C -0.9849(19) -0.0907(19) -0.4419(17) 0.061(4) Uiso 0.125 1 d G . P C -2 C28 C -0.838(2) -0.3230(17) -0.6831(18) 0.061(4) Uiso 0.125 1 d G . P C -2 C27 C -0.924(2) -0.3262(17) -0.6658(18) 0.061(4) Uiso 0.125 1 d G . P C -2 C12 C -0.783(2) -0.3124(18) -0.6211(17) 0.061(4) Uiso 0.125 1 d G . P C -2 C26 C -0.9514(19) -0.3187(17) -0.5876(19) 0.061(4) Uiso 0.125 1 d G . P C -2 C34 C -1.0227(19) -0.2695(18) -0.5701(19) 0.061(4) Uiso 0.125 1 d G . P C -2 C31 C -0.967(2) -0.2850(18) -0.7314(19) 0.061(4) Uiso 0.125 1 d G . P C -2 C32 C -1.0338(19) -0.2387(18) -0.7149(19) 0.061(4) Uiso 0.125 1 d G . P C -2 C33 C -1.0626(18) -0.2307(19) -0.632(2) 0.061(4) Uiso 0.125 1 d G . P C -2 C10 C -0.704(2) -0.2174(19) -0.7033(17) 0.061(4) Uiso 0.125 1 d G . P C -2 C9 C -0.762(2) -0.2286(19) -0.7691(17) 0.061(4) Uiso 0.125 1 d G . P C -2 C11 C -0.7146(19) -0.2581(19) -0.6315(17) 0.061(4) Uiso 0.125 1 d G . P C -2 C29 C -0.827(2) -0.2798(18) -0.7593(17) 0.061(4) Uiso 0.125 1 d G . P C -2 C30 C -0.906(2) -0.2563(18) -0.7892(17) 0.061(4) Uiso 0.125 1 d G . P C -2 C8 C -0.773(2) -0.1507(19) -0.8094(17) 0.061(4) Uiso 0.125 1 d G . P C -2 C7 C -0.848(2) -0.1286(19) -0.8375(16) 0.061(4) Uiso 0.125 1 d G . P C -2 C45 C -0.917(2) -0.1830(18) -0.8271(17) 0.061(4) Uiso 0.125 1 d G . P C -2 C53 C -0.6775(19) -0.137(2) -0.5544(18) 0.061(4) Uiso 0.125 1 d G . P C -2 C52 C -0.6665(19) -0.094(2) -0.6306(18) 0.061(4) Uiso 0.125 1 d G . P C -2 C54 C -0.7008(19) -0.2165(19) -0.5548(17) 0.061(4) Uiso 0.125 1 d G . P C -2 C55 C -0.679(2) -0.133(2) -0.7028(18) 0.061(4) Uiso 0.125 1 d G . P C -2 C56 C -0.722(2) -0.091(2) -0.7684(17) 0.061(4) Uiso 0.125 1 d G . P C -2 C51 C -0.695(2) -0.011(2) -0.6195(19) 0.061(4) Uiso 0.125 1 d G . P C -2 C50 C -0.735(2) 0.0280(19) -0.6812(18) 0.061(4) Uiso 0.125 1 d G . P C -2 C57 C -0.749(2) -0.0135(19) -0.7579(18) 0.061(4) Uiso 0.125 1 d G . P C -2 C5 C -0.963(2) -0.0491(18) -0.8091(17) 0.061(4) Uiso 0.125 1 d G . P C -2 C6 C -0.877(2) -0.0459(18) -0.8263(16) 0.061(4) Uiso 0.125 1 d G . P C -2 C58 C -0.829(2) 0.0099(18) -0.7878(17) 0.061(4) Uiso 0.125 1 d G . P C -2 C4 C -0.997(2) 0.0037(18) -0.7543(18) 0.061(4) Uiso 0.125 1 d G . P C -2 C42 C -1.0803(19) -0.1047(19) -0.6969(19) 0.061(4) Uiso 0.125 1 d G . P C -2 C43 C -1.045(2) -0.1608(19) -0.7552(19) 0.061(4) Uiso 0.125 1 d G . P C -2 C44 C -0.988(2) -0.1338(18) -0.8095(18) 0.061(4) Uiso 0.125 1 d G . P C -2 C3 C -1.057(2) -0.0250(19) -0.6965(18) 0.061(4) Uiso 0.125 1 d G . P C -2 C39 C -1.0536(19) -0.0240(19) -0.5480(18) 0.061(4) Uiso 0.125 1 d G . P C -2 C40 C -1.0784(18) -0.1088(19) -0.5485(19) 0.061(4) Uiso 0.125 1 d G . P C -2 C41 C -1.0913(18) -0.1479(19) -0.621(2) 0.061(4) Uiso 0.125 1 d G . P C -2 C2 C -1.043(2) 0.0166(18) -0.6198(18) 0.061(4) Uiso 0.125 1 d G . P C -2 C47 C -0.920(2) 0.0815(17) -0.5682(17) 0.061(4) Uiso 0.125 1 d G . P C -2 C46 C -0.931(2) 0.0383(18) -0.4919(17) 0.061(4) Uiso 0.125 1 d G . P C -2 C38 C -0.996(2) -0.0128(18) -0.4822(17) 0.061(4) Uiso 0.125 1 d G . P C -2 C1 C -0.974(2) 0.0710(17) -0.6302(18) 0.061(4) Uiso 0.125 1 d G . P C -2 C59 C -0.864(2) 0.0660(18) -0.7295(17) 0.061(4) Uiso 0.125 1 d G . P C -2 C49 C -0.806(2) 0.0772(18) -0.6636(18) 0.061(4) Uiso 0.125 1 d G . P C -2 C48 C -0.833(2) 0.0847(17) -0.5855(18) 0.061(4) Uiso 0.125 1 d G . P C -2 C60 C -0.946(2) 0.0630(17) -0.7133(17) 0.061(4) Uiso 0.125 1 d G . P C -2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Sn1 0.0512(5) 0.0512(5) 0.0512(5) 0.0033(5) 0.0033(5) 0.0033(5) I2A 0.080(7) 0.068(4) 0.086(7) -0.028(6) -0.008(5) 0.015(6) I1 0.0922(9) 0.0922(9) 0.0922(9) -0.0192(7) -0.0192(7) -0.0192(7) I2B 0.130(11) 0.081(5) 0.069(4) 0.000(3) 0.019(5) 0.050(5) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Sn1 I2A 2.61(2) . ? Sn1 I2A 2.61(2) 12 ? Sn1 I2A 2.61(2) 11 ? Sn1 I1 2.637(3) . ? Sn1 I2B 2.679(15) 12 ? Sn1 I2B 2.679(15) 11 ? Sn1 I2B 2.679(15) . ? C72 C73 1.408(14) . ? C72 C130 1.367(13) . ? C72 C71 1.367(13) . ? C81 C80 1.408(14) . ? C81 C82 1.368(13) . ? C81 C83 1.367(13) . ? C91 C92 1.408(14) . ? C91 C100 1.367(13) . ? C91 C90 1.367(13) . ? C108 C109 1.408(14) . ? C108 C107 1.367(13) . ? C108 C114 1.367(13) . ? C66 C65 1.408(14) . ? C66 C61 1.368(13) . ? C66 C67 1.367(13) . ? C65 C64 1.367(13) . ? C65 C70 1.368(13) . ? C73 C74 1.367(13) . ? C73 C84 1.367(13) . ? C80 C79 1.367(13) . ? C80 C89 1.367(13) . ? C92 C93 1.367(13) . ? C92 C115 1.368(13) . ? C109 C110 1.367(13) . ? C109 C111 1.367(13) . ? C102 C101 1.382(13) . ? C102 C103 1.382(13) . ? C102 C128 1.327(13) . ? C123 C122 1.382(13) . ? C123 C124 1.382(13) . ? C123 C126 1.326(13) . ? C101 C97 1.382(13) . ? C101 C76 1.327(13) . ? C122 C119 1.382(13) . ? C122 C86 1.327(13) . ? C97 C96 1.382(13) . ? C97 C98 1.327(13) . ? C119 C118 1.383(13) . ? C119 C120 1.327(13) . ? C96 C103 1.382(13) . ? C96 C95 1.327(13) . ? C118 C124 1.382(13) . ? C118 C117 1.327(13) . ? C103 C104 1.327(13) . ? C124 C125 1.327(13) . ? C128 C129 1.390(13) . ? C128 C63 1.390(13) . ? C126 C127 1.390(13) . ? C126 C69 1.390(14) . ? C76 C77 1.390(13) . ? C76 C75 1.390(13) . ? C86 C87 1.390(13) . ? C86 C85 1.390(13) . ? C98 C99 1.390(14) . ? C98 C78 1.390(13) . ? C120 C121 1.391(13) . ? C120 C88 1.390(13) . ? C95 C106 1.390(13) . ? C95 C94 1.390(13) . ? C117 C113 1.390(13) . ? C117 C116 1.390(13) . ? C104 C62 1.390(13) . ? C104 C105 1.390(13) . ? C125 C68 1.390(14) . ? C125 C112 1.390(13) . ? C129 C75 1.322(13) . ? C129 C130 1.389(14) . ? C127 C85 1.321(13) . ? C127 C71 1.390(14) . ? C77 C78 1.321(13) . ? C77 C82 1.389(13) . ? C87 C88 1.321(13) . ? C87 C83 1.390(13) . ? C99 C94 1.321(13) . ? C99 C100 1.389(13) . ? C121 C116 1.321(13) . ? C121 C90 1.390(14) . ? C106 C105 1.321(13) . ? C106 C107 1.390(13) . ? C113 C112 1.321(13) . ? C113 C114 1.389(13) . ? C62 C63 1.321(13) . ? C62 C61 1.390(13) . ? C68 C69 1.321(13) . ? C68 C67 1.389(13) . ? C63 C64 1.390(13) . ? C69 C70 1.389(13) . ? C75 C74 1.389(13) . ? C85 C84 1.389(13) . ? C78 C79 1.390(14) . ? C88 C89 1.390(13) . ? C94 C93 1.390(13) . ? C116 C115 1.390(13) . ? C105 C110 1.389(13) . ? C112 C111 1.389(14) . ? C130 C64 1.341(13) . ? C71 C70 1.341(13) . ? C82 C74 1.341(13) . ? C83 C84 1.341(13) . ? C100 C79 1.341(13) . ? C90 C89 1.341(13) . ? C107 C93 1.341(13) . ? C114 C115 1.341(13) . ? C61 C110 1.341(13) . ? C67 C111 1.341(13) . ? C15 C16 1.478(6) . ? C15 C14 1.391(6) . ? C15 C23 1.478(6) . ? C16 C17 1.391(6) . ? C16 C21 1.478(6) . ? C14 C13 1.479(6) . ? C14 C54 1.478(6) . ? C17 C18 1.478(6) . ? C17 C53 1.478(6) . ? C18 C19 1.391(6) . ? C18 C51 1.479(6) . ? C21 C20 1.391(6) . ? C21 C22 1.479(6) . ? C20 C19 1.478(6) . ? C20 C46 1.479(6) . ? C19 C48 1.479(6) . ? C25 C24 1.479(6) . ? C25 C13 1.391(6) . ? C25 C26 1.479(6) . ? C24 C23 1.391(6) . ? C24 C35 1.479(6) . ? C13 C12 1.479(6) . ? C23 C22 1.479(6) . ? C22 C37 1.391(6) . ? C35 C36 1.391(6) . ? C35 C34 1.479(6) . ? C36 C37 1.479(6) . ? C36 C40 1.479(6) . ? C37 C38 1.479(6) . ? C28 C27 1.479(6) . ? C28 C12 1.391(6) . ? C28 C29 1.478(6) . ? C27 C26 1.391(6) . ? C27 C31 1.478(6) . ? C12 C11 1.479(6) . ? C26 C34 1.479(6) . ? C34 C33 1.391(6) . ? C31 C32 1.391(6) . ? C31 C30 1.479(6) . ? C32 C33 1.479(6) . ? C32 C43 1.479(6) . ? C33 C41 1.479(6) . ? C10 C9 1.478(6) . ? C10 C11 1.391(6) . ? C10 C55 1.479(6) . ? C9 C29 1.391(6) . ? C9 C8 1.479(6) . ? C11 C54 1.479(6) . ? C29 C30 1.478(6) . ? C30 C45 1.391(6) . ? C8 C7 1.391(6) . ? C8 C56 1.478(6) . ? C7 C45 1.479(6) . ? C7 C6 1.478(6) . ? C45 C44 1.479(6) . ? C53 C52 1.479(6) . ? C53 C54 1.391(6) . ? C52 C55 1.391(6) . ? C52 C51 1.479(6) . ? C55 C56 1.478(6) . ? C56 C57 1.391(6) . ? C51 C50 1.391(6) . ? C50 C57 1.479(6) . ? C50 C49 1.478(6) . ? C57 C58 1.479(6) . ? C5 C6 1.479(6) . ? C5 C4 1.391(6) . ? C5 C44 1.479(6) . ? C6 C58 1.391(6) . ? C58 C59 1.478(6) . ? C4 C3 1.479(6) . ? C4 C60 1.479(6) . ? C42 C43 1.479(6) . ? C42 C3 1.391(6) . ? C42 C41 1.479(6) . ? C43 C44 1.391(6) . ? C3 C2 1.479(6) . ? C39 C40 1.479(6) . ? C39 C2 1.391(6) . ? C39 C38 1.479(6) . ? C40 C41 1.391(6) . ? C2 C1 1.478(6) . ? C47 C46 1.479(6) . ? C47 C1 1.391(6) . ? C47 C48 1.479(6) . ? C46 C38 1.391(6) . ? C1 C60 1.478(6) . ? C59 C49 1.479(6) . ? C59 C60 1.391(6) . ? C49 C48 1.391(6) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag I2A Sn1 I2A 105.1(5) . 12 ? I2A Sn1 I2A 105.1(5) . 11 ? I2A Sn1 I2A 105.1(5) 12 11 ? I2A Sn1 I1 113.6(4) . . ? I2A Sn1 I1 113.6(4) 12 . ? I2A Sn1 I1 113.6(4) 11 . ? I2A Sn1 I2B 108.8(8) . 12 ? I2A Sn1 I2B 110.3(10) . 11 ? I2A Sn1 I2B 108.8(8) 12 11 ? I2A Sn1 I2B 110.3(11) 11 12 ? I2A Sn1 I2B 8.1(8) 12 12 ? I2A Sn1 I2B 8.1(8) 11 11 ? I1 Sn1 I2B 105.5(10) . 11 ? I1 Sn1 I2B 105.5(10) . 12 ? I1 Sn1 I2B 105.5(10) . . ? I2B Sn1 I2B 113.1(9) 11 . ? I2B Sn1 I2B 113.1(9) 12 11 ? I2B Sn1 I2B 113.1(9) 12 . ? C130 C72 C73 119.0 . . ? C130 C72 C71 115.4 . . ? C71 C72 C73 119.0 . . ? C82 C81 C80 119.0 . . ? C83 C81 C80 119.0 . . ? C83 C81 C82 115.4 . . ? C100 C91 C92 119.0 . . ? C100 C91 C90 115.4 . . ? C90 C91 C92 119.0 . . ? C107 C108 C109 119.0 . . ? C107 C108 C114 115.4 . . ? C114 C108 C109 119.0 . . ? C61 C66 C65 119.0 . . ? C67 C66 C65 119.0 . . ? C67 C66 C61 115.4 . . ? C64 C65 C66 119.0 . . ? C64 C65 C70 115.4 . . ? C70 C65 C66 119.0 . . ? C74 C73 C72 119.0 . . ? C84 C73 C72 119.0 . . ? C84 C73 C74 115.4 . . ? C79 C80 C81 119.0 . . ? C79 C80 C89 115.4 . . ? C89 C80 C81 119.0 . . ? C93 C92 C91 119.0 . . ? C93 C92 C115 115.4 . . ? C115 C92 C91 119.0 . . ? C110 C109 C108 119.0 . . ? C111 C109 C108 119.0 . . ? C111 C109 C110 115.4 . . ? C101 C102 C103 108.0 . . ? C128 C102 C101 119.9 . . ? C128 C102 C103 119.8 . . ? C124 C123 C122 108.0 . . ? C126 C123 C122 119.9 . . ? C126 C123 C124 119.9 . . ? C102 C101 C97 108.0 . . ? C76 C101 C102 119.9 . . ? C76 C101 C97 119.9 . . ? C119 C122 C123 108.0 . . ? C86 C122 C123 119.8 . . ? C86 C122 C119 119.9 . . ? C101 C97 C96 108.0 . . ? C98 C97 C101 119.9 . . ? C98 C97 C96 119.8 . . ? C122 C119 C118 108.0 . . ? C120 C119 C122 119.8 . . ? C120 C119 C118 119.9 . . ? C97 C96 C103 108.0 . . ? C95 C96 C97 119.9 . . ? C95 C96 C103 119.9 . . ? C124 C118 C119 108.0 . . ? C117 C118 C119 119.8 . . ? C117 C118 C124 119.9 . . ? C96 C103 C102 108.0 . . ? C104 C103 C102 119.9 . . ? C104 C103 C96 119.9 . . ? C118 C124 C123 108.0 . . ? C125 C124 C123 119.8 . . ? C125 C124 C118 119.8 . . ? C102 C128 C129 120.3 . . ? C102 C128 C63 120.3 . . ? C129 C128 C63 106.4 . . ? C123 C126 C127 120.3 . . ? C123 C126 C69 120.3 . . ? C69 C126 C127 106.5 . . ? C101 C76 C77 120.3 . . ? C101 C76 C75 120.3 . . ? C77 C76 C75 106.4 . . ? C122 C86 C87 120.3 . . ? C122 C86 C85 120.3 . . ? C85 C86 C87 106.4 . . ? C97 C98 C99 120.4 . . ? C97 C98 C78 120.3 . . ? C99 C98 C78 106.4 . . ? C119 C120 C121 120.3 . . ? C119 C120 C88 120.3 . . ? C88 C120 C121 106.4 . . ? C96 C95 C106 120.3 . . ? C96 C95 C94 120.3 . . ? C94 C95 C106 106.4 . . ? C118 C117 C113 120.3 . . ? C118 C117 C116 120.3 . . ? C116 C117 C113 106.5 . . ? C103 C104 C62 120.3 . . ? C103 C104 C105 120.3 . . ? C62 C104 C105 106.5 . . ? C124 C125 C68 120.3 . . ? C124 C125 C112 120.3 . . ? C112 C125 C68 106.4 . . ? C75 C129 C128 119.8 . . ? C75 C129 C130 120.5 . . ? C130 C129 C128 108.2 . . ? C85 C127 C126 119.8 . . ? C85 C127 C71 120.5 . . ? C71 C127 C126 108.2 . . ? C78 C77 C76 119.8 . . ? C78 C77 C82 120.5 . . ? C82 C77 C76 108.2 . . ? C88 C87 C86 119.8 . . ? C88 C87 C83 120.5 . . ? C83 C87 C86 108.2 . . ? C94 C99 C98 119.8 . . ? C94 C99 C100 120.5 . . ? C100 C99 C98 108.2 . . ? C116 C121 C120 119.8 . . ? C116 C121 C90 120.6 . . ? C90 C121 C120 108.2 . . ? C105 C106 C95 119.8 . . ? C105 C106 C107 120.5 . . ? C107 C106 C95 108.2 . . ? C112 C113 C117 119.8 . . ? C112 C113 C114 120.5 . . ? C114 C113 C117 108.2 . . ? C63 C62 C104 119.8 . . ? C63 C62 C61 120.5 . . ? C61 C62 C104 108.2 . . ? C69 C68 C125 119.8 . . ? C69 C68 C67 120.5 . . ? C67 C68 C125 108.2 . . ? C62 C63 C128 119.8 . . ? C62 C63 C64 120.5 . . ? C64 C63 C128 108.2 . . ? C68 C69 C126 119.8 . . ? C68 C69 C70 120.5 . . ? C70 C69 C126 108.2 . . ? C129 C75 C76 119.8 . . ? C129 C75 C74 120.5 . . ? C74 C75 C76 108.2 . . ? C127 C85 C86 119.8 . . ? C127 C85 C84 120.5 . . ? C84 C85 C86 108.2 . . ? C77 C78 C98 119.8 . . ? C77 C78 C79 120.5 . . ? C79 C78 C98 108.2 . . ? C87 C88 C120 119.8 . . ? C87 C88 C89 120.5 . . ? C89 C88 C120 108.2 . . ? C99 C94 C95 119.8 . . ? C99 C94 C93 120.5 . . ? C93 C94 C95 108.2 . . ? C117 C116 C115 108.2 . . ? C121 C116 C117 119.8 . . ? C121 C116 C115 120.5 . . ? C106 C105 C104 119.8 . . ? C106 C105 C110 120.5 . . ? C110 C105 C104 108.2 . . ? C113 C112 C125 119.8 . . ? C113 C112 C111 120.5 . . ? C111 C112 C125 108.2 . . ? C72 C130 C129 120.4 . . ? C64 C130 C72 121.6 . . ? C64 C130 C129 108.6 . . ? C72 C71 C127 120.3 . . ? C70 C71 C72 121.7 . . ? C70 C71 C127 108.6 . . ? C81 C82 C77 120.3 . . ? C74 C82 C81 121.6 . . ? C74 C82 C77 108.6 . . ? C81 C83 C87 120.3 . . ? C84 C83 C81 121.7 . . ? C84 C83 C87 108.6 . . ? C91 C100 C99 120.3 . . ? C79 C100 C91 121.6 . . ? C79 C100 C99 108.6 . . ? C91 C90 C121 120.3 . . ? C89 C90 C91 121.6 . . ? C89 C90 C121 108.6 . . ? C108 C107 C106 120.3 . . ? C93 C107 C108 121.6 . . ? C93 C107 C106 108.6 . . ? C108 C114 C113 120.4 . . ? C115 C114 C108 121.6 . . ? C115 C114 C113 108.6 . . ? C66 C61 C62 120.3 . . ? C110 C61 C66 121.6 . . ? C110 C61 C62 108.6 . . ? C66 C67 C68 120.3 . . ? C111 C67 C66 121.7 . . ? C111 C67 C68 108.6 . . ? C65 C64 C63 120.3 . . ? C130 C64 C65 121.7 . . ? C130 C64 C63 108.6 . . ? C65 C70 C69 120.3 . . ? C71 C70 C65 121.6 . . ? C71 C70 C69 108.6 . . ? C73 C74 C75 120.3 . . ? C82 C74 C73 121.7 . . ? C82 C74 C75 108.6 . . ? C73 C84 C85 120.3 . . ? C83 C84 C73 121.7 . . ? C83 C84 C85 108.6 . . ? C80 C79 C78 120.3 . . ? C100 C79 C80 121.6 . . ? C100 C79 C78 108.6 . . ? C80 C89 C88 120.3 . . ? C90 C89 C80 121.6 . . ? C90 C89 C88 108.6 . . ? C92 C93 C94 120.3 . . ? C107 C93 C92 121.6 . . ? C107 C93 C94 108.6 . . ? C92 C115 C116 120.3 . . ? C114 C115 C92 121.6 . . ? C114 C115 C116 108.6 . . ? C109 C110 C105 120.4 . . ? C61 C110 C109 121.6 . . ? C61 C110 C105 108.6 . . ? C109 C111 C112 120.4 . . ? C67 C111 C109 121.6 . . ? C67 C111 C112 108.6 . . ? C14 C15 C16 120.0 . . ? C14 C15 C23 120.0 . . ? C23 C15 C16 108.0 . . ? C15 C16 C21 108.0 . . ? C17 C16 C15 120.0 . . ? C17 C16 C21 120.0 . . ? C15 C14 C13 120.0 . . ? C15 C14 C54 120.0 . . ? C54 C14 C13 108.0 . . ? C16 C17 C18 120.0 . . ? C16 C17 C53 120.0 . . ? C53 C17 C18 108.0 . . ? C17 C18 C51 108.0 . . ? C19 C18 C17 120.0 . . ? C19 C18 C51 120.0 . . ? C16 C21 C22 108.0 . . ? C20 C21 C16 120.0 . . ? C20 C21 C22 120.0 . . ? C21 C20 C19 120.0 . . ? C21 C20 C46 120.0 . . ? C19 C20 C46 108.0 . . ? C18 C19 C20 120.0 . . ? C18 C19 C48 120.0 . . ? C20 C19 C48 108.0 . . ? C24 C25 C26 108.0 . . ? C13 C25 C24 120.0 . . ? C13 C25 C26 120.0 . . ? C25 C24 C35 108.0 . . ? C23 C24 C25 120.0 . . ? C23 C24 C35 120.0 . . ? C25 C13 C14 120.0 . . ? C25 C13 C12 120.0 . . ? C12 C13 C14 108.0 . . ? C15 C23 C22 108.0 . . ? C24 C23 C15 120.0 . . ? C24 C23 C22 120.0 . . ? C23 C22 C21 108.0 . . ? C37 C22 C21 120.0 . . ? C37 C22 C23 120.0 . . ? C24 C35 C34 108.0 . . ? C36 C35 C24 120.0 . . ? C36 C35 C34 120.0 . . ? C35 C36 C37 120.0 . . ? C35 C36 C40 120.0 . . ? C40 C36 C37 108.0 . . ? C22 C37 C36 120.0 . . ? C22 C37 C38 120.0 . . ? C36 C37 C38 108.0 . . ? C12 C28 C27 120.0 . . ? C12 C28 C29 120.0 . . ? C29 C28 C27 108.0 . . ? C26 C27 C28 120.0 . . ? C26 C27 C31 120.0 . . ? C31 C27 C28 108.0 . . ? C13 C12 C11 108.0 . . ? C28 C12 C13 120.0 . . ? C28 C12 C11 120.0 . . ? C27 C26 C25 120.0 . . ? C27 C26 C34 120.0 . . ? C34 C26 C25 108.0 . . ? C26 C34 C35 108.0 . . ? C33 C34 C35 120.0 . . ? C33 C34 C26 120.0 . . ? C27 C31 C30 108.0 . . ? C32 C31 C27 120.0 . . ? C32 C31 C30 120.0 . . ? C31 C32 C33 120.0 . . ? C31 C32 C43 120.0 . . ? C33 C32 C43 108.0 . . ? C34 C33 C32 120.0 . . ? C34 C33 C41 120.0 . . ? C32 C33 C41 108.0 . . ? C9 C10 C55 108.0 . . ? C11 C10 C9 120.0 . . ? C11 C10 C55 120.0 . . ? C10 C9 C8 108.0 . . ? C29 C9 C10 120.0 . . ? C29 C9 C8 120.0 . . ? C12 C11 C54 108.0 . . ? C10 C11 C12 120.0 . . ? C10 C11 C54 120.0 . . ? C9 C29 C28 120.0 . . ? C9 C29 C30 120.0 . . ? C30 C29 C28 108.0 . . ? C29 C30 C31 108.0 . . ? C45 C30 C31 120.0 . . ? C45 C30 C29 120.0 . . ? C7 C8 C9 120.0 . . ? C7 C8 C56 120.0 . . ? C56 C8 C9 108.0 . . ? C8 C7 C45 120.0 . . ? C8 C7 C6 120.0 . . ? C6 C7 C45 108.0 . . ? C30 C45 C7 120.0 . . ? C30 C45 C44 120.0 . . ? C7 C45 C44 108.0 . . ? C17 C53 C52 108.0 . . ? C54 C53 C17 120.0 . . ? C54 C53 C52 120.0 . . ? C55 C52 C53 120.0 . . ? C55 C52 C51 120.0 . . ? C51 C52 C53 108.0 . . ? C14 C54 C11 108.0 . . ? C53 C54 C14 120.0 . . ? C53 C54 C11 120.0 . . ? C52 C55 C10 120.0 . . ? C52 C55 C56 120.0 . . ? C56 C55 C10 108.0 . . ? C55 C56 C8 108.0 . . ? C57 C56 C8 120.0 . . ? C57 C56 C55 120.0 . . ? C52 C51 C18 108.0 . . ? C50 C51 C18 120.0 . . ? C50 C51 C52 120.0 . . ? C51 C50 C57 120.0 . . ? C51 C50 C49 120.0 . . ? C49 C50 C57 108.0 . . ? C56 C57 C50 120.0 . . ? C56 C57 C58 120.0 . . ? C50 C57 C58 108.0 . . ? C4 C5 C6 120.0 . . ? C4 C5 C44 120.0 . . ? C44 C5 C6 108.0 . . ? C7 C6 C5 108.0 . . ? C58 C6 C7 120.0 . . ? C58 C6 C5 120.0 . . ? C6 C58 C57 120.0 . . ? C6 C58 C59 120.0 . . ? C59 C58 C57 108.0 . . ? C5 C4 C3 120.0 . . ? C5 C4 C60 120.0 . . ? C3 C4 C60 108.0 . . ? C3 C42 C43 120.0 . . ? C3 C42 C41 120.0 . . ? C41 C42 C43 108.0 . . ? C42 C43 C32 108.0 . . ? C44 C43 C32 120.0 . . ? C44 C43 C42 120.0 . . ? C5 C44 C45 108.0 . . ? C43 C44 C45 120.0 . . ? C43 C44 C5 120.0 . . ? C42 C3 C4 120.0 . . ? C42 C3 C2 120.0 . . ? C2 C3 C4 108.0 . . ? C40 C39 C38 108.0 . . ? C2 C39 C40 120.0 . . ? C2 C39 C38 120.0 . . ? C39 C40 C36 108.0 . . ? C41 C40 C36 120.0 . . ? C41 C40 C39 120.0 . . ? C42 C41 C33 108.0 . . ? C40 C41 C33 120.0 . . ? C40 C41 C42 120.0 . . ? C39 C2 C3 120.0 . . ? C39 C2 C1 120.0 . . ? C1 C2 C3 108.0 . . ? C1 C47 C46 120.0 . . ? C1 C47 C48 120.0 . . ? C48 C47 C46 108.0 . . ? C20 C46 C47 108.0 . . ? C38 C46 C20 120.0 . . ? C38 C46 C47 120.0 . . ? C39 C38 C37 108.0 . . ? C46 C38 C37 120.0 . . ? C46 C38 C39 120.0 . . ? C47 C1 C2 120.0 . . ? C47 C1 C60 120.0 . . ? C60 C1 C2 108.0 . . ? C58 C59 C49 108.0 . . ? C60 C59 C58 120.0 . . ? C60 C59 C49 120.0 . . ? C50 C49 C59 108.0 . . ? C48 C49 C50 120.0 . . ? C48 C49 C59 120.0 . . ? C47 C48 C19 108.0 . . ? C49 C48 C19 120.0 . . ? C49 C48 C47 120.0 . . ? C1 C60 C4 108.0 . . ? C59 C60 C4 120.0 . . ? C59 C60 C1 120.0 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C72 C73 C74 C75 4.5 . . . . ? C72 C73 C74 C82 -138.1 . . . . ? C72 C73 C84 C85 -4.5 . . . . ? C72 C73 C84 C83 138.1 . . . . ? C72 C130 C64 C65 0.0 . . . . ? C72 C130 C64 C63 -146.4 . . . . ? C72 C71 C70 C65 0.0 . . . . ? C72 C71 C70 C69 146.4 . . . . ? C81 C80 C79 C78 4.5 . . . . ? C81 C80 C79 C100 -138.1 . . . . ? C81 C80 C89 C88 -4.5 . . . . ? C81 C80 C89 C90 138.2 . . . . ? C81 C82 C74 C73 0.0 . . . . ? C81 C82 C74 C75 -146.5 . . . . ? C81 C83 C84 C73 0.0 . . . . ? C81 C83 C84 C85 146.4 . . . . ? C91 C92 C93 C94 4.5 . . . . ? C91 C92 C93 C107 -138.1 . . . . ? C91 C92 C115 C116 -4.5 . . . . ? C91 C92 C115 C114 138.1 . . . . ? C91 C100 C79 C80 0.0 . . . . ? C91 C100 C79 C78 -146.4 . . . . ? C91 C90 C89 C80 0.0 . . . . ? C91 C90 C89 C88 146.4 . . . . ? C108 C109 C110 C105 4.4 . . . . ? C108 C109 C110 C61 -138.2 . . . . ? C108 C109 C111 C112 -4.4 . . . . ? C108 C109 C111 C67 138.2 . . . . ? C108 C107 C93 C92 0.0 . . . . ? C108 C107 C93 C94 -146.4 . . . . ? C108 C114 C115 C92 0.0 . . . . ? C108 C114 C115 C116 146.4 . . . . ? C66 C65 C64 C63 4.5 . . . . ? C66 C65 C64 C130 -138.1 . . . . ? C66 C65 C70 C69 -4.5 . . . . ? C66 C65 C70 C71 138.2 . . . . ? C66 C61 C110 C109 0.0 . . . . ? C66 C61 C110 C105 -146.5 . . . . ? C66 C67 C111 C109 0.0 . . . . ? C66 C67 C111 C112 146.4 . . . . ? C65 C66 C61 C62 -4.5 . . . . ? C65 C66 C61 C110 138.2 . . . . ? C65 C66 C67 C68 4.5 . . . . ? C65 C66 C67 C111 -138.1 . . . . ? C73 C72 C130 C129 -4.4 . . . . ? C73 C72 C130 C64 138.2 . . . . ? C73 C72 C71 C127 4.4 . . . . ? C73 C72 C71 C70 -138.2 . . . . ? C80 C81 C82 C77 -4.4 . . . . ? C80 C81 C82 C74 138.2 . . . . ? C80 C81 C83 C87 4.4 . . . . ? C80 C81 C83 C84 -138.1 . . . . ? C92 C91 C100 C99 -4.4 . . . . ? C92 C91 C100 C79 138.2 . . . . ? C92 C91 C90 C121 4.4 . . . . ? C92 C91 C90 C89 -138.2 . . . . ? C109 C108 C107 C106 -4.5 . . . . ? C109 C108 C107 C93 138.1 . . . . ? C109 C108 C114 C113 4.5 . . . . ? C109 C108 C114 C115 -138.2 . . . . ? C102 C101 C97 C96 0.0 . . . . ? C102 C101 C97 C98 -142.2 . . . . ? C102 C101 C76 C77 137.0 . . . . ? C102 C101 C76 C75 0.8 . . . . ? C102 C103 C104 C62 -0.7 . . . . ? C102 C103 C104 C105 -137.0 . . . . ? C102 C128 C129 C75 0.7 . . . . ? C102 C128 C129 C130 -142.8 . . . . ? C102 C128 C63 C62 -0.8 . . . . ? C102 C128 C63 C64 142.8 . . . . ? C123 C122 C119 C118 0.0 . . . . ? C123 C122 C119 C120 142.2 . . . . ? C123 C122 C86 C87 -137.0 . . . . ? C123 C122 C86 C85 -0.8 . . . . ? C123 C124 C125 C68 0.7 . . . . ? C123 C124 C125 C112 137.0 . . . . ? C123 C126 C127 C85 -0.7 . . . . ? C123 C126 C127 C71 142.8 . . . . ? C123 C126 C69 C68 0.8 . . . . ? C123 C126 C69 C70 -142.8 . . . . ? C101 C102 C103 C96 0.0 . . . . ? C101 C102 C103 C104 142.2 . . . . ? C101 C102 C128 C129 -0.7 . . . . ? C101 C102 C128 C63 -137.0 . . . . ? C101 C97 C96 C103 0.0 . . . . ? C101 C97 C96 C95 -142.2 . . . . ? C101 C97 C98 C99 137.0 . . . . ? C101 C97 C98 C78 0.7 . . . . ? C101 C76 C77 C78 0.8 . . . . ? C101 C76 C77 C82 -142.8 . . . . ? C101 C76 C75 C129 -0.8 . . . . ? C101 C76 C75 C74 142.8 . . . . ? C122 C123 C124 C118 0.0 . . . . ? C122 C123 C124 C125 -142.2 . . . . ? C122 C123 C126 C127 0.8 . . . . ? C122 C123 C126 C69 137.0 . . . . ? C122 C119 C118 C124 0.0 . . . . ? C122 C119 C118 C117 142.2 . . . . ? C122 C119 C120 C121 -137.0 . . . . ? C122 C119 C120 C88 -0.8 . . . . ? C122 C86 C87 C88 -0.8 . . . . ? C122 C86 C87 C83 142.8 . . . . ? C122 C86 C85 C127 0.8 . . . . ? C122 C86 C85 C84 -142.8 . . . . ? C97 C101 C76 C77 -0.8 . . . . ? C97 C101 C76 C75 -137.0 . . . . ? C97 C96 C103 C102 0.0 . . . . ? C97 C96 C103 C104 -142.2 . . . . ? C97 C96 C95 C106 137.0 . . . . ? C97 C96 C95 C94 0.8 . . . . ? C97 C98 C99 C94 0.8 . . . . ? C97 C98 C99 C100 -142.8 . . . . ? C97 C98 C78 C77 -0.7 . . . . ? C97 C98 C78 C79 142.8 . . . . ? C119 C122 C86 C87 0.8 . . . . ? C119 C122 C86 C85 137.0 . . . . ? C119 C118 C124 C123 0.0 . . . . ? C119 C118 C124 C125 142.2 . . . . ? C119 C118 C117 C113 -137.0 . . . . ? C119 C118 C117 C116 -0.7 . . . . ? C119 C120 C121 C116 -0.8 . . . . ? C119 C120 C121 C90 142.8 . . . . ? C119 C120 C88 C87 0.8 . . . . ? C119 C120 C88 C89 -142.8 . . . . ? C96 C97 C98 C99 -0.8 . . . . ? C96 C97 C98 C78 -137.0 . . . . ? C96 C103 C104 C62 137.0 . . . . ? C96 C103 C104 C105 0.7 . . . . ? C96 C95 C106 C105 0.8 . . . . ? C96 C95 C106 C107 -142.8 . . . . ? C96 C95 C94 C99 -0.8 . . . . ? C96 C95 C94 C93 142.8 . . . . ? C118 C119 C120 C121 0.8 . . . . ? C118 C119 C120 C88 137.0 . . . . ? C118 C124 C125 C68 -137.0 . . . . ? C118 C124 C125 C112 -0.8 . . . . ? C118 C117 C113 C112 -0.7 . . . . ? C118 C117 C113 C114 142.8 . . . . ? C118 C117 C116 C121 0.7 . . . . ? C118 C117 C116 C115 -142.8 . . . . ? C103 C102 C101 C97 0.0 . . . . ? C103 C102 C101 C76 -142.2 . . . . ? C103 C102 C128 C129 137.0 . . . . ? C103 C102 C128 C63 0.8 . . . . ? C103 C96 C95 C106 -0.8 . . . . ? C103 C96 C95 C94 -137.0 . . . . ? C103 C104 C62 C63 0.7 . . . . ? C103 C104 C62 C61 -142.8 . . . . ? C103 C104 C105 C106 -0.7 . . . . ? C103 C104 C105 C110 142.8 . . . . ? C124 C123 C122 C119 0.0 . . . . ? C124 C123 C122 C86 142.2 . . . . ? C124 C123 C126 C127 -137.0 . . . . ? C124 C123 C126 C69 -0.8 . . . . ? C124 C118 C117 C113 0.7 . . . . ? C124 C118 C117 C116 137.0 . . . . ? C124 C125 C68 C69 -0.7 . . . . ? C124 C125 C68 C67 142.8 . . . . ? C124 C125 C112 C113 0.8 . . . . ? C124 C125 C112 C111 -142.8 . . . . ? C128 C102 C101 C97 142.2 . . . . ? C128 C102 C101 C76 0.0 . . . . ? C128 C102 C103 C96 -142.2 . . . . ? C128 C102 C103 C104 0.0 . . . . ? C128 C129 C75 C76 0.0 . . . . ? C128 C129 C75 C74 -139.0 . . . . ? C128 C129 C130 C72 147.7 . . . . ? C128 C129 C130 C64 0.8 . . . . ? C128 C63 C64 C65 -147.8 . . . . ? C128 C63 C64 C130 -0.8 . . . . ? C126 C123 C122 C119 -142.2 . . . . ? C126 C123 C122 C86 0.0 . . . . ? C126 C123 C124 C118 142.2 . . . . ? C126 C123 C124 C125 0.0 . . . . ? C126 C127 C85 C86 0.0 . . . . ? C126 C127 C85 C84 139.0 . . . . ? C126 C127 C71 C72 -147.7 . . . . ? C126 C127 C71 C70 -0.8 . . . . ? C126 C69 C70 C65 147.8 . . . . ? C126 C69 C70 C71 0.8 . . . . ? C76 C101 C97 C96 142.2 . . . . ? C76 C101 C97 C98 0.0 . . . . ? C76 C77 C78 C98 0.0 . . . . ? C76 C77 C78 C79 -139.0 . . . . ? C76 C77 C82 C81 147.7 . . . . ? C76 C77 C82 C74 0.8 . . . . ? C76 C75 C74 C73 -147.8 . . . . ? C76 C75 C74 C82 -0.8 . . . . ? C86 C122 C119 C118 -142.2 . . . . ? C86 C122 C119 C120 0.0 . . . . ? C86 C87 C88 C120 0.0 . . . . ? C86 C87 C88 C89 139.0 . . . . ? C86 C87 C83 C81 -147.7 . . . . ? C86 C87 C83 C84 -0.8 . . . . ? C86 C85 C84 C73 147.8 . . . . ? C86 C85 C84 C83 0.8 . . . . ? C98 C97 C96 C103 142.2 . . . . ? C98 C97 C96 C95 0.0 . . . . ? C98 C99 C94 C95 0.0 . . . . ? C98 C99 C94 C93 -139.1 . . . . ? C98 C99 C100 C91 147.7 . . . . ? C98 C99 C100 C79 0.8 . . . . ? C98 C78 C79 C80 -147.7 . . . . ? C98 C78 C79 C100 -0.8 . . . . ? C120 C119 C118 C124 -142.2 . . . . ? C120 C119 C118 C117 0.0 . . . . ? C120 C121 C116 C117 0.1 . . . . ? C120 C121 C116 C115 139.1 . . . . ? C120 C121 C90 C91 -147.7 . . . . ? C120 C121 C90 C89 -0.8 . . . . ? C120 C88 C89 C80 147.7 . . . . ? C120 C88 C89 C90 0.8 . . . . ? C95 C96 C103 C102 142.2 . . . . ? C95 C96 C103 C104 0.0 . . . . ? C95 C106 C105 C104 0.0 . . . . ? C95 C106 C105 C110 -139.0 . . . . ? C95 C106 C107 C108 147.7 . . . . ? C95 C106 C107 C93 0.8 . . . . ? C95 C94 C93 C92 -147.8 . . . . ? C95 C94 C93 C107 -0.8 . . . . ? C117 C118 C124 C123 -142.2 . . . . ? C117 C118 C124 C125 0.0 . . . . ? C117 C113 C112 C125 0.0 . . . . ? C117 C113 C112 C111 139.0 . . . . ? C117 C113 C114 C108 -147.7 . . . . ? C117 C113 C114 C115 -0.8 . . . . ? C117 C116 C115 C92 147.7 . . . . ? C117 C116 C115 C114 0.8 . . . . ? C104 C62 C63 C128 0.0 . . . . ? C104 C62 C63 C64 -139.0 . . . . ? C104 C62 C61 C66 147.8 . . . . ? C104 C62 C61 C110 0.8 . . . . ? C104 C105 C110 C109 -147.7 . . . . ? C104 C105 C110 C61 -0.8 . . . . ? C125 C68 C69 C126 0.0 . . . . ? C125 C68 C69 C70 139.0 . . . . ? C125 C68 C67 C66 -147.8 . . . . ? C125 C68 C67 C111 -0.8 . . . . ? C125 C112 C111 C109 147.7 . . . . ? C125 C112 C111 C67 0.8 . . . . ? C129 C128 C63 C62 -142.3 . . . . ? C129 C128 C63 C64 1.3 . . . . ? C129 C75 C74 C73 -4.6 . . . . ? C129 C75 C74 C82 142.4 . . . . ? C129 C130 C64 C65 146.4 . . . . ? C129 C130 C64 C63 0.0 . . . . ? C127 C126 C69 C68 142.3 . . . . ? C127 C126 C69 C70 -1.3 . . . . ? C127 C85 C84 C73 4.5 . . . . ? C127 C85 C84 C83 -142.4 . . . . ? C127 C71 C70 C65 -146.4 . . . . ? C127 C71 C70 C69 0.0 . . . . ? C77 C76 C75 C129 -142.3 . . . . ? C77 C76 C75 C74 1.3 . . . . ? C77 C78 C79 C80 -4.5 . . . . ? C77 C78 C79 C100 142.4 . . . . ? C77 C82 C74 C73 146.4 . . . . ? C77 C82 C74 C75 0.0 . . . . ? C87 C86 C85 C127 142.3 . . . . ? C87 C86 C85 C84 -1.3 . . . . ? C87 C88 C89 C80 4.5 . . . . ? C87 C88 C89 C90 -142.4 . . . . ? C87 C83 C84 C73 -146.5 . . . . ? C87 C83 C84 C85 0.0 . . . . ? C99 C98 C78 C77 -142.3 . . . . ? C99 C98 C78 C79 1.3 . . . . ? C99 C94 C93 C92 -4.5 . . . . ? C99 C94 C93 C107 142.4 . . . . ? C99 C100 C79 C80 146.4 . . . . ? C99 C100 C79 C78 0.0 . . . . ? C121 C120 C88 C87 142.2 . . . . ? C121 C120 C88 C89 -1.3 . . . . ? C121 C116 C115 C92 4.5 . . . . ? C121 C116 C115 C114 -142.4 . . . . ? C121 C90 C89 C80 -146.4 . . . . ? C121 C90 C89 C88 0.0 . . . . ? C106 C95 C94 C99 -142.3 . . . . ? C106 C95 C94 C93 1.3 . . . . ? C106 C105 C110 C109 -4.5 . . . . ? C106 C105 C110 C61 142.4 . . . . ? C106 C107 C93 C92 146.4 . . . . ? C106 C107 C93 C94 0.0 . . . . ? C113 C117 C116 C121 142.3 . . . . ? C113 C117 C116 C115 -1.3 . . . . ? C113 C112 C111 C109 4.5 . . . . ? C113 C112 C111 C67 -142.4 . . . . ? C113 C114 C115 C92 -146.4 . . . . ? C113 C114 C115 C116 0.0 . . . . ? C62 C104 C105 C106 -142.3 . . . . ? C62 C104 C105 C110 1.2 . . . . ? C62 C63 C64 C65 -4.5 . . . . ? C62 C63 C64 C130 142.4 . . . . ? C62 C61 C110 C109 146.4 . . . . ? C62 C61 C110 C105 0.0 . . . . ? C68 C125 C112 C113 142.3 . . . . ? C68 C125 C112 C111 -1.3 . . . . ? C68 C69 C70 C65 4.5 . . . . ? C68 C69 C70 C71 -142.4 . . . . ? C68 C67 C111 C109 -146.4 . . . . ? C68 C67 C111 C112 0.0 . . . . ? C63 C128 C129 C75 142.3 . . . . ? C63 C128 C129 C130 -1.3 . . . . ? C63 C62 C61 C66 4.6 . . . . ? C63 C62 C61 C110 -142.4 . . . . ? C69 C126 C127 C85 -142.3 . . . . ? C69 C126 C127 C71 1.3 . . . . ? C69 C68 C67 C66 -4.6 . . . . ? C69 C68 C67 C111 142.4 . . . . ? C75 C76 C77 C78 142.3 . . . . ? C75 C76 C77 C82 -1.3 . . . . ? C75 C129 C130 C72 4.5 . . . . ? C75 C129 C130 C64 -142.4 . . . . ? C85 C86 C87 C88 -142.3 . . . . ? C85 C86 C87 C83 1.3 . . . . ? C85 C127 C71 C72 -4.5 . . . . ? C85 C127 C71 C70 142.4 . . . . ? C78 C98 C99 C94 142.3 . . . . ? C78 C98 C99 C100 -1.3 . . . . ? C78 C77 C82 C81 4.5 . . . . ? C78 C77 C82 C74 -142.4 . . . . ? C88 C120 C121 C116 -142.3 . . . . ? C88 C120 C121 C90 1.3 . . . . ? C88 C87 C83 C81 -4.5 . . . . ? C88 C87 C83 C84 142.4 . . . . ? C94 C95 C106 C105 142.3 . . . . ? C94 C95 C106 C107 -1.3 . . . . ? C94 C99 C100 C91 4.5 . . . . ? C94 C99 C100 C79 -142.4 . . . . ? C116 C117 C113 C112 -142.3 . . . . ? C116 C117 C113 C114 1.2 . . . . ? C116 C121 C90 C91 -4.5 . . . . ? C116 C121 C90 C89 142.4 . . . . ? C105 C104 C62 C63 142.3 . . . . ? C105 C104 C62 C61 -1.2 . . . . ? C105 C106 C107 C108 4.5 . . . . ? C105 C106 C107 C93 -142.4 . . . . ? C112 C125 C68 C69 -142.3 . . . . ? C112 C125 C68 C67 1.3 . . . . ? C112 C113 C114 C108 -4.5 . . . . ? C112 C113 C114 C115 142.4 . . . . ? C130 C72 C73 C74 0.0 . . . . ? C130 C72 C73 C84 -150.1 . . . . ? C130 C72 C71 C127 155.6 . . . . ? C130 C72 C71 C70 13.0 . . . . ? C130 C129 C75 C76 139.0 . . . . ? C130 C129 C75 C74 0.0 . . . . ? C71 C72 C73 C74 150.1 . . . . ? C71 C72 C73 C84 0.0 . . . . ? C71 C72 C130 C129 -155.6 . . . . ? C71 C72 C130 C64 -13.0 . . . . ? C71 C127 C85 C86 -139.1 . . . . ? C71 C127 C85 C84 0.0 . . . . ? C82 C81 C80 C79 0.0 . . . . ? C82 C81 C80 C89 -150.1 . . . . ? C82 C81 C83 C87 155.6 . . . . ? C82 C81 C83 C84 13.0 . . . . ? C82 C77 C78 C98 139.0 . . . . ? C82 C77 C78 C79 0.0 . . . . ? C83 C81 C80 C79 150.1 . . . . ? C83 C81 C80 C89 0.0 . . . . ? C83 C81 C82 C77 -155.6 . . . . ? C83 C81 C82 C74 -13.0 . . . . ? C83 C87 C88 C120 -139.1 . . . . ? C83 C87 C88 C89 0.0 . . . . ? C100 C91 C92 C93 0.0 . . . . ? C100 C91 C92 C115 -150.1 . . . . ? C100 C91 C90 C121 155.6 . . . . ? C100 C91 C90 C89 13.0 . . . . ? C100 C99 C94 C95 139.1 . . . . ? C100 C99 C94 C93 0.0 . . . . ? C90 C91 C92 C93 150.1 . . . . ? C90 C91 C92 C115 0.0 . . . . ? C90 C91 C100 C99 -155.6 . . . . ? C90 C91 C100 C79 -13.0 . . . . ? C90 C121 C116 C117 -139.0 . . . . ? C90 C121 C116 C115 0.0 . . . . ? C107 C108 C109 C110 0.0 . . . . ? C107 C108 C109 C111 -150.1 . . . . ? C107 C108 C114 C113 155.6 . . . . ? C107 C108 C114 C115 13.0 . . . . ? C107 C106 C105 C104 139.0 . . . . ? C107 C106 C105 C110 0.0 . . . . ? C114 C108 C109 C110 150.1 . . . . ? C114 C108 C109 C111 0.0 . . . . ? C114 C108 C107 C106 -155.6 . . . . ? C114 C108 C107 C93 -13.0 . . . . ? C114 C113 C112 C125 -139.0 . . . . ? C114 C113 C112 C111 0.0 . . . . ? C61 C66 C65 C64 0.0 . . . . ? C61 C66 C65 C70 -150.1 . . . . ? C61 C66 C67 C68 155.6 . . . . ? C61 C66 C67 C111 13.0 . . . . ? C61 C62 C63 C128 139.0 . . . . ? C61 C62 C63 C64 0.0 . . . . ? C67 C66 C65 C64 150.1 . . . . ? C67 C66 C65 C70 0.0 . . . . ? C67 C66 C61 C62 -155.6 . . . . ? C67 C66 C61 C110 -13.0 . . . . ? C67 C68 C69 C126 -139.0 . . . . ? C67 C68 C69 C70 0.0 . . . . ? C64 C65 C70 C69 -155.6 . . . . ? C64 C65 C70 C71 -13.0 . . . . ? C70 C65 C64 C63 155.6 . . . . ? C70 C65 C64 C130 13.0 . . . . ? C74 C73 C84 C85 -155.6 . . . . ? C74 C73 C84 C83 -13.0 . . . . ? C84 C73 C74 C75 155.6 . . . . ? C84 C73 C74 C82 13.0 . . . . ? C79 C80 C89 C88 -155.6 . . . . ? C79 C80 C89 C90 -13.0 . . . . ? C89 C80 C79 C78 155.6 . . . . ? C89 C80 C79 C100 13.0 . . . . ? C93 C92 C115 C116 -155.6 . . . . ? C93 C92 C115 C114 -13.0 . . . . ? C115 C92 C93 C94 155.6 . . . . ? C115 C92 C93 C107 13.0 . . . . ? C110 C109 C111 C112 -155.6 . . . . ? C110 C109 C111 C67 -13.0 . . . . ? C111 C109 C110 C105 155.6 . . . . ? C111 C109 C110 C61 13.0 . . . . ? C15 C16 C17 C18 138.2 . . . . ? C15 C16 C17 C53 0.0 . . . . ? C15 C16 C21 C20 -142.6 . . . . ? C15 C16 C21 C22 0.0 . . . . ? C15 C14 C13 C25 0.0 . . . . ? C15 C14 C13 C12 142.6 . . . . ? C15 C14 C54 C11 -142.6 . . . . ? C15 C14 C54 C53 0.0 . . . . ? C15 C23 C22 C21 0.0 . . . . ? C15 C23 C22 C37 142.6 . . . . ? C16 C15 C14 C13 -138.2 . . . . ? C16 C15 C14 C54 0.0 . . . . ? C16 C15 C23 C24 142.6 . . . . ? C16 C15 C23 C22 0.0 . . . . ? C16 C17 C18 C19 0.0 . . . . ? C16 C17 C18 C51 -142.6 . . . . ? C16 C17 C53 C52 142.6 . . . . ? C16 C17 C53 C54 0.0 . . . . ? C16 C21 C20 C19 0.0 . . . . ? C16 C21 C20 C46 138.2 . . . . ? C16 C21 C22 C23 0.0 . . . . ? C16 C21 C22 C37 -142.6 . . . . ? C14 C15 C16 C17 0.0 . . . . ? C14 C15 C16 C21 142.6 . . . . ? C14 C15 C23 C24 0.0 . . . . ? C14 C15 C23 C22 -142.6 . . . . ? C14 C13 C12 C28 -142.6 . . . . ? C14 C13 C12 C11 0.0 . . . . ? C17 C16 C21 C20 0.0 . . . . ? C17 C16 C21 C22 142.6 . . . . ? C17 C18 C19 C20 0.0 . . . . ? C17 C18 C19 C48 -138.2 . . . . ? C17 C18 C51 C52 0.0 . . . . ? C17 C18 C51 C50 142.6 . . . . ? C17 C53 C52 C55 -142.6 . . . . ? C17 C53 C52 C51 0.0 . . . . ? C17 C53 C54 C14 0.0 . . . . ? C17 C53 C54 C11 138.2 . . . . ? C18 C17 C53 C52 0.0 . . . . ? C18 C17 C53 C54 -142.6 . . . . ? C18 C19 C48 C47 142.6 . . . . ? C18 C19 C48 C49 0.0 . . . . ? C18 C51 C50 C57 -138.2 . . . . ? C18 C51 C50 C49 0.0 . . . . ? C21 C16 C17 C18 0.0 . . . . ? C21 C16 C17 C53 -138.2 . . . . ? C21 C20 C19 C18 0.0 . . . . ? C21 C20 C19 C48 142.6 . . . . ? C21 C20 C46 C47 -142.6 . . . . ? C21 C20 C46 C38 0.0 . . . . ? C21 C22 C37 C36 138.2 . . . . ? C21 C22 C37 C38 0.0 . . . . ? C20 C21 C22 C23 142.6 . . . . ? C20 C21 C22 C37 0.0 . . . . ? C20 C19 C48 C47 0.0 . . . . ? C20 C19 C48 C49 -142.6 . . . . ? C20 C46 C38 C37 0.0 . . . . ? C20 C46 C38 C39 -138.2 . . . . ? C19 C18 C51 C52 -142.6 . . . . ? C19 C18 C51 C50 0.0 . . . . ? C19 C20 C46 C47 0.0 . . . . ? C19 C20 C46 C38 142.6 . . . . ? C25 C24 C23 C15 0.0 . . . . ? C25 C24 C23 C22 138.2 . . . . ? C25 C24 C35 C36 -142.6 . . . . ? C25 C24 C35 C34 0.0 . . . . ? C25 C13 C12 C28 0.0 . . . . ? C25 C13 C12 C11 142.6 . . . . ? C25 C26 C34 C35 0.0 . . . . ? C25 C26 C34 C33 142.6 . . . . ? C24 C25 C13 C14 0.0 . . . . ? C24 C25 C13 C12 -138.2 . . . . ? C24 C25 C26 C27 142.6 . . . . ? C24 C25 C26 C34 0.0 . . . . ? C24 C23 C22 C21 -142.6 . . . . ? C24 C23 C22 C37 0.0 . . . . ? C24 C35 C36 C37 0.0 . . . . ? C24 C35 C36 C40 138.2 . . . . ? C24 C35 C34 C26 0.0 . . . . ? C24 C35 C34 C33 -142.6 . . . . ? C13 C14 C54 C11 0.0 . . . . ? C13 C14 C54 C53 142.6 . . . . ? C13 C25 C24 C23 0.0 . . . . ? C13 C25 C24 C35 142.6 . . . . ? C13 C25 C26 C27 0.0 . . . . ? C13 C25 C26 C34 -142.6 . . . . ? C13 C12 C11 C10 -142.6 . . . . ? C13 C12 C11 C54 0.0 . . . . ? C23 C15 C16 C17 -142.6 . . . . ? C23 C15 C16 C21 0.0 . . . . ? C23 C15 C14 C13 0.0 . . . . ? C23 C15 C14 C54 138.2 . . . . ? C23 C24 C35 C36 0.0 . . . . ? C23 C24 C35 C34 142.6 . . . . ? C23 C22 C37 C36 0.0 . . . . ? C23 C22 C37 C38 -138.2 . . . . ? C22 C21 C20 C19 -138.2 . . . . ? C22 C21 C20 C46 0.0 . . . . ? C22 C37 C38 C39 142.6 . . . . ? C22 C37 C38 C46 0.0 . . . . ? C35 C24 C23 C15 -138.2 . . . . ? C35 C24 C23 C22 0.0 . . . . ? C35 C36 C37 C22 0.0 . . . . ? C35 C36 C37 C38 142.6 . . . . ? C35 C36 C40 C39 -142.6 . . . . ? C35 C36 C40 C41 0.0 . . . . ? C35 C34 C33 C32 138.2 . . . . ? C35 C34 C33 C41 0.0 . . . . ? C36 C35 C34 C26 142.6 . . . . ? C36 C35 C34 C33 0.0 . . . . ? C36 C37 C38 C39 0.0 . . . . ? C36 C37 C38 C46 -142.6 . . . . ? C36 C40 C41 C33 0.0 . . . . ? C36 C40 C41 C42 -138.2 . . . . ? C37 C36 C40 C39 0.0 . . . . ? C37 C36 C40 C41 142.6 . . . . ? C28 C27 C26 C25 0.0 . . . . ? C28 C27 C26 C34 138.2 . . . . ? C28 C27 C31 C32 -142.6 . . . . ? C28 C27 C31 C30 0.0 . . . . ? C28 C12 C11 C10 0.0 . . . . ? C28 C12 C11 C54 142.6 . . . . ? C28 C29 C30 C31 0.0 . . . . ? C28 C29 C30 C45 142.6 . . . . ? C27 C28 C12 C13 0.0 . . . . ? C27 C28 C12 C11 -138.2 . . . . ? C27 C28 C29 C9 142.6 . . . . ? C27 C28 C29 C30 0.0 . . . . ? C27 C26 C34 C35 -142.6 . . . . ? C27 C26 C34 C33 0.0 . . . . ? C27 C31 C32 C33 0.0 . . . . ? C27 C31 C32 C43 138.2 . . . . ? C27 C31 C30 C29 0.0 . . . . ? C27 C31 C30 C45 -142.6 . . . . ? C12 C28 C27 C26 0.0 . . . . ? C12 C28 C27 C31 142.6 . . . . ? C12 C28 C29 C9 0.0 . . . . ? C12 C28 C29 C30 -142.6 . . . . ? C12 C11 C54 C14 0.0 . . . . ? C12 C11 C54 C53 -142.6 . . . . ? C26 C25 C24 C23 -142.6 . . . . ? C26 C25 C24 C35 0.0 . . . . ? C26 C25 C13 C14 138.2 . . . . ? C26 C25 C13 C12 0.0 . . . . ? C26 C27 C31 C32 0.0 . . . . ? C26 C27 C31 C30 142.6 . . . . ? C26 C34 C33 C32 0.0 . . . . ? C26 C34 C33 C41 -138.2 . . . . ? C34 C35 C36 C37 -138.2 . . . . ? C34 C35 C36 C40 0.0 . . . . ? C34 C33 C41 C42 142.6 . . . . ? C34 C33 C41 C40 0.0 . . . . ? C31 C27 C26 C25 -138.2 . . . . ? C31 C27 C26 C34 0.0 . . . . ? C31 C32 C33 C34 0.0 . . . . ? C31 C32 C33 C41 142.6 . . . . ? C31 C32 C43 C42 -142.6 . . . . ? C31 C32 C43 C44 0.0 . . . . ? C31 C30 C45 C7 138.2 . . . . ? C31 C30 C45 C44 0.0 . . . . ? C32 C31 C30 C29 142.6 . . . . ? C32 C31 C30 C45 0.0 . . . . ? C32 C33 C41 C42 0.0 . . . . ? C32 C33 C41 C40 -142.6 . . . . ? C32 C43 C44 C45 0.0 . . . . ? C32 C43 C44 C5 -138.2 . . . . ? C33 C32 C43 C42 0.0 . . . . ? C33 C32 C43 C44 142.6 . . . . ? C10 C9 C29 C28 0.0 . . . . ? C10 C9 C29 C30 138.2 . . . . ? C10 C9 C8 C7 -142.6 . . . . ? C10 C9 C8 C56 0.0 . . . . ? C10 C11 C54 C14 142.6 . . . . ? C10 C11 C54 C53 0.0 . . . . ? C10 C55 C56 C8 0.0 . . . . ? C10 C55 C56 C57 142.6 . . . . ? C9 C10 C11 C12 0.0 . . . . ? C9 C10 C11 C54 -138.2 . . . . ? C9 C10 C55 C52 142.6 . . . . ? C9 C10 C55 C56 0.0 . . . . ? C9 C29 C30 C31 -142.6 . . . . ? C9 C29 C30 C45 0.0 . . . . ? C9 C8 C7 C45 0.0 . . . . ? C9 C8 C7 C6 138.2 . . . . ? C9 C8 C56 C55 0.0 . . . . ? C9 C8 C56 C57 -142.6 . . . . ? C11 C10 C9 C29 0.0 . . . . ? C11 C10 C9 C8 142.6 . . . . ? C11 C10 C55 C52 0.0 . . . . ? C11 C10 C55 C56 -142.6 . . . . ? C29 C28 C27 C26 -142.6 . . . . ? C29 C28 C27 C31 0.0 . . . . ? C29 C28 C12 C13 138.2 . . . . ? C29 C28 C12 C11 0.0 . . . . ? C29 C9 C8 C7 0.0 . . . . ? C29 C9 C8 C56 142.6 . . . . ? C29 C30 C45 C7 0.0 . . . . ? C29 C30 C45 C44 -138.2 . . . . ? C30 C31 C32 C33 -138.2 . . . . ? C30 C31 C32 C43 0.0 . . . . ? C30 C45 C44 C5 142.6 . . . . ? C30 C45 C44 C43 0.0 . . . . ? C8 C9 C29 C28 -138.2 . . . . ? C8 C9 C29 C30 0.0 . . . . ? C8 C7 C45 C30 0.0 . . . . ? C8 C7 C45 C44 142.6 . . . . ? C8 C7 C6 C5 -142.6 . . . . ? C8 C7 C6 C58 0.0 . . . . ? C8 C56 C57 C50 138.2 . . . . ? C8 C56 C57 C58 0.0 . . . . ? C7 C8 C56 C55 142.6 . . . . ? C7 C8 C56 C57 0.0 . . . . ? C7 C45 C44 C5 0.0 . . . . ? C7 C45 C44 C43 -142.6 . . . . ? C7 C6 C58 C57 0.0 . . . . ? C7 C6 C58 C59 -138.2 . . . . ? C45 C7 C6 C5 0.0 . . . . ? C45 C7 C6 C58 142.6 . . . . ? C53 C17 C18 C19 142.6 . . . . ? C53 C17 C18 C51 0.0 . . . . ? C53 C52 C55 C10 0.0 . . . . ? C53 C52 C55 C56 138.2 . . . . ? C53 C52 C51 C18 0.0 . . . . ? C53 C52 C51 C50 -142.6 . . . . ? C52 C53 C54 C14 -138.2 . . . . ? C52 C53 C54 C11 0.0 . . . . ? C52 C55 C56 C8 -142.6 . . . . ? C52 C55 C56 C57 0.0 . . . . ? C52 C51 C50 C57 0.0 . . . . ? C52 C51 C50 C49 138.2 . . . . ? C54 C14 C13 C25 -142.6 . . . . ? C54 C14 C13 C12 0.0 . . . . ? C54 C53 C52 C55 0.0 . . . . ? C54 C53 C52 C51 142.6 . . . . ? C55 C10 C9 C29 -142.6 . . . . ? C55 C10 C9 C8 0.0 . . . . ? C55 C10 C11 C12 138.2 . . . . ? C55 C10 C11 C54 0.0 . . . . ? C55 C52 C51 C18 142.6 . . . . ? C55 C52 C51 C50 0.0 . . . . ? C55 C56 C57 C50 0.0 . . . . ? C55 C56 C57 C58 -138.2 . . . . ? C56 C8 C7 C45 -138.2 . . . . ? C56 C8 C7 C6 0.0 . . . . ? C56 C57 C58 C6 0.0 . . . . ? C56 C57 C58 C59 142.6 . . . . ? C51 C18 C19 C20 138.2 . . . . ? C51 C18 C19 C48 0.0 . . . . ? C51 C52 C55 C10 -138.2 . . . . ? C51 C52 C55 C56 0.0 . . . . ? C51 C50 C57 C56 0.0 . . . . ? C51 C50 C57 C58 142.6 . . . . ? C51 C50 C49 C59 -142.6 . . . . ? C51 C50 C49 C48 0.0 . . . . ? C50 C57 C58 C6 -142.6 . . . . ? C50 C57 C58 C59 0.0 . . . . ? C50 C49 C48 C19 0.0 . . . . ? C50 C49 C48 C47 -138.2 . . . . ? C57 C50 C49 C59 0.0 . . . . ? C57 C50 C49 C48 142.6 . . . . ? C57 C58 C59 C49 0.0 . . . . ? C57 C58 C59 C60 -142.6 . . . . ? C5 C6 C58 C57 138.2 . . . . ? C5 C6 C58 C59 0.0 . . . . ? C5 C4 C3 C42 0.0 . . . . ? C5 C4 C3 C2 142.6 . . . . ? C5 C4 C60 C1 -142.6 . . . . ? C5 C4 C60 C59 0.0 . . . . ? C6 C7 C45 C30 -142.6 . . . . ? C6 C7 C45 C44 0.0 . . . . ? C6 C5 C4 C3 -138.2 . . . . ? C6 C5 C4 C60 0.0 . . . . ? C6 C5 C44 C45 0.0 . . . . ? C6 C5 C44 C43 142.6 . . . . ? C6 C58 C59 C49 142.6 . . . . ? C6 C58 C59 C60 0.0 . . . . ? C58 C59 C49 C50 0.0 . . . . ? C58 C59 C49 C48 -142.6 . . . . ? C58 C59 C60 C4 0.0 . . . . ? C58 C59 C60 C1 138.2 . . . . ? C4 C5 C6 C7 142.6 . . . . ? C4 C5 C6 C58 0.0 . . . . ? C4 C5 C44 C45 -142.6 . . . . ? C4 C5 C44 C43 0.0 . . . . ? C4 C3 C2 C39 -142.6 . . . . ? C4 C3 C2 C1 0.0 . . . . ? C42 C43 C44 C45 138.2 . . . . ? C42 C43 C44 C5 0.0 . . . . ? C42 C3 C2 C39 0.0 . . . . ? C42 C3 C2 C1 142.6 . . . . ? C43 C32 C33 C34 -142.6 . . . . ? C43 C32 C33 C41 0.0 . . . . ? C43 C42 C3 C4 0.0 . . . . ? C43 C42 C3 C2 -138.2 . . . . ? C43 C42 C41 C33 0.0 . . . . ? C43 C42 C41 C40 142.6 . . . . ? C44 C5 C6 C7 0.0 . . . . ? C44 C5 C6 C58 -142.6 . . . . ? C44 C5 C4 C3 0.0 . . . . ? C44 C5 C4 C60 138.2 . . . . ? C3 C4 C60 C1 0.0 . . . . ? C3 C4 C60 C59 142.6 . . . . ? C3 C42 C43 C32 142.6 . . . . ? C3 C42 C43 C44 0.0 . . . . ? C3 C42 C41 C33 -142.6 . . . . ? C3 C42 C41 C40 0.0 . . . . ? C3 C2 C1 C47 -142.6 . . . . ? C3 C2 C1 C60 0.0 . . . . ? C39 C40 C41 C33 138.2 . . . . ? C39 C40 C41 C42 0.0 . . . . ? C39 C2 C1 C47 0.0 . . . . ? C39 C2 C1 C60 142.6 . . . . ? C40 C36 C37 C22 -142.6 . . . . ? C40 C36 C37 C38 0.0 . . . . ? C40 C39 C2 C3 0.0 . . . . ? C40 C39 C2 C1 -138.2 . . . . ? C40 C39 C38 C37 0.0 . . . . ? C40 C39 C38 C46 142.6 . . . . ? C41 C42 C43 C32 0.0 . . . . ? C41 C42 C43 C44 -142.6 . . . . ? C41 C42 C3 C4 138.2 . . . . ? C41 C42 C3 C2 0.0 . . . . ? C2 C39 C40 C36 142.6 . . . . ? C2 C39 C40 C41 0.0 . . . . ? C2 C39 C38 C37 -142.6 . . . . ? C2 C39 C38 C46 0.0 . . . . ? C2 C1 C60 C4 0.0 . . . . ? C2 C1 C60 C59 -142.6 . . . . ? C47 C46 C38 C37 138.2 . . . . ? C47 C46 C38 C39 0.0 . . . . ? C47 C1 C60 C4 142.6 . . . . ? C47 C1 C60 C59 0.0 . . . . ? C46 C20 C19 C18 -142.6 . . . . ? C46 C20 C19 C48 0.0 . . . . ? C46 C47 C1 C2 0.0 . . . . ? C46 C47 C1 C60 -138.2 . . . . ? C46 C47 C48 C19 0.0 . . . . ? C46 C47 C48 C49 142.6 . . . . ? C38 C39 C40 C36 0.0 . . . . ? C38 C39 C40 C41 -142.6 . . . . ? C38 C39 C2 C3 138.2 . . . . ? C38 C39 C2 C1 0.0 . . . . ? C1 C47 C46 C20 142.6 . . . . ? C1 C47 C46 C38 0.0 . . . . ? C1 C47 C48 C19 -142.6 . . . . ? C1 C47 C48 C49 0.0 . . . . ? C59 C49 C48 C19 138.2 . . . . ? C59 C49 C48 C47 0.0 . . . . ? C49 C50 C57 C56 -142.6 . . . . ? C49 C50 C57 C58 0.0 . . . . ? C49 C59 C60 C4 -138.2 . . . . ? C49 C59 C60 C1 0.0 . . . . ? C48 C47 C46 C20 0.0 . . . . ? C48 C47 C46 C38 -142.6 . . . . ? C48 C47 C1 C2 138.2 . . . . ? C48 C47 C1 C60 0.0 . . . . ? C60 C4 C3 C42 -142.6 . . . . ? C60 C4 C3 C2 0.0 . . . . ? C60 C59 C49 C50 142.6 . . . . ? C60 C59 C49 C48 0.0 . . . . ? _shelx_res_file ; TITL 209b2-295_a.res in P4(1)32 209b2-295.res created by SHELXL-2018/3 at 14:42:22 on 22-Mar-2021 REM Old TITL 209b2-295_a.res in P4(1)32 REM SHELXT solution in P4(1)32: R1 0.265, Rweak 0.074, Alpha 0.009 REM 0.914 for 15 systematic absences, Orientation as input REM Flack x = 0.263 ( 0.044 ) from 425 Parsons' quotients REM Formula found by SHELXT: C91 I5 CELL 0.71073 16.739 16.739 16.739 90 90 90 ZERR 4 0.0013 0.0013 0.0013 0 0 0 LATT -1 SYMM 0.75-Y,0.25+X,0.75+Z SYMM 0.5-X,-Y,0.5+Z SYMM 0.75+Y,0.75-X,0.25+Z SYMM 0.75+X,0.75-Z,0.25+Y SYMM 0.5+X,0.5-Y,-Z SYMM 0.25+X,0.75+Z,0.75-Y SYMM 0.25+Z,0.75+Y,0.75-X SYMM -X,0.5+Y,0.5-Z SYMM 0.75-Z,0.25+Y,0.75+X SYMM +Z,+X,+Y SYMM +Y,+Z,+X SYMM 0.5-Y,-Z,0.5+X SYMM 0.5+Z,0.5-X,-Y SYMM -Y,0.5+Z,0.5-X SYMM 0.5-Z,-X,0.5+Y SYMM -Z,0.5+X,0.5-Y SYMM 0.5+Y,0.5-Z,-X SYMM 0.25+Y,0.75+X,0.75-Z SYMM 0.25-Y,0.25-X,0.25-Z SYMM 0.75-X,0.25+Z,0.75+Y SYMM 0.25-X,0.25-Z,0.25-Y SYMM 0.75+Z,0.75-Y,0.25+X SYMM 0.25-Z,0.25-Y,0.25-X SFAC C I Sn UNIT 250.01 32 8 EADP C13 C15 C16 C14 C23 C17 C21 C54 C24 C22 C18 C53 C20 C25 C12 C11 C35 = C37 C19 C51 C52 C46 C26 C28 C10 C36 C34 C38 C48 C50 C55 C47 C27 C29 C9 C40 = C33 C39 C49 C57 C56 C1 C31 C30 C8 C41 C32 C2 C59 C58 C60 C45 C7 C42 C43 C3 = C6 C4 C44 C5 EADP C66 C72 C73 C130 C71 C74 C84 C129 C64 C127 C70 C75 C82 C85 C83 C128 = C65 C63 C126 C69 C76 C81 C77 C86 C87 C102 C62 C123 C68 C101 C80 C78 C122 = C88 C103 C61 C67 C104 C124 C125 C97 C79 C89 C98 C119 C120 C96 C110 C111 = C105 C118 C112 C100 C90 C99 C121 C95 C109 C106 C117 C113 C91 C94 C116 C108 = C107 C114 C92 C93 C115 L.S. 40 0 0 PLAN 3 SIZE 0.266 0.308 0.467 TEMP 21.85 CONF list 4 MORE -1 fmap 2 53 ACTA REM REM REM WGHT 0.047100 45.426502 FVAR 0.15778 0.37358 SN1 3 -0.648826 -0.648826 -0.648826 10.33333 0.05122 0.05122 = 0.05122 0.00329 0.00329 0.00329 PART 2 I2A 2 -0.718956 -0.517689 -0.601837 21.00000 0.07952 0.06795 = 0.08565 -0.02752 -0.00824 0.01536 PART 0 I1 2 -0.739770 -0.739770 -0.739770 10.33333 0.09218 0.09218 = 0.09218 -0.01923 -0.01923 -0.01923 PART 1 I2B 2 -0.739477 -0.522631 -0.610345 -21.00000 0.13037 0.08051 = 0.06905 -0.00027 0.01926 0.04964 PART -1 AFIX 9 C72 1 -0.870420 -0.327726 -0.678442 10.04167 0.02920 C81 1 -0.695255 -0.169055 -0.714037 10.04167 0.02920 C91 1 -0.774289 0.045235 -0.643687 10.04167 0.02920 C108 1 -0.998335 0.019034 -0.564602 10.04167 0.02920 C66 1 -1.057755 -0.211486 -0.586091 10.04167 0.02920 C65 1 -1.015264 -0.278186 -0.614680 10.04167 0.02920 C73 1 -0.794057 -0.301706 -0.702167 10.04167 0.02920 C80 1 -0.690526 -0.086265 -0.700075 10.04167 0.02920 C92 1 -0.847751 0.070385 -0.611341 10.04167 0.02920 C109 1 -1.048445 -0.048246 -0.558586 10.04167 0.02920 C102 1 -0.824965 -0.234332 -0.432146 10.04167 0.02920 C123 1 -0.981588 -0.155080 -0.849546 10.04167 0.02920 C101 1 -0.749982 -0.208761 -0.455431 10.04167 0.02920 C122 1 -0.906596 -0.129500 -0.872841 10.04167 0.02920 C97 1 -0.745363 -0.127461 -0.441728 10.04167 0.02920 C119 1 -0.901966 -0.048190 -0.859139 10.04167 0.02920 C96 1 -0.817485 -0.102781 -0.409972 10.04167 0.02920 C118 1 -0.974109 -0.023510 -0.827383 10.04167 0.02920 C103 1 -0.866696 -0.168832 -0.404057 10.04167 0.02920 C124 1 -1.023299 -0.089560 -0.821478 10.04167 0.02920 C128 1 -0.862562 -0.289931 -0.474320 10.04167 0.02920 C126 1 -0.990021 -0.225411 -0.814038 10.04167 0.02920 C76 1 -0.715898 -0.239920 -0.519849 10.04167 0.02920 C86 1 -0.843367 -0.175421 -0.859578 10.04167 0.02920 C98 1 -0.706869 -0.080910 -0.493055 10.04167 0.02920 C120 1 -0.834297 -0.016421 -0.832784 10.04167 0.02920 C95 1 -0.847903 -0.032670 -0.430952 10.04167 0.02920 C117 1 -0.975362 0.031849 -0.770661 10.04167 0.02920 C104 1 -0.944156 -0.161841 -0.419392 10.04167 0.02920 C125 1 -1.071604 -0.097321 -0.759100 10.04167 0.02920 C129 1 -0.827318 -0.321959 -0.542348 10.04167 0.02920 C127 1 -0.923682 -0.273162 -0.799265 10.04167 0.02920 C77 1 -0.676354 -0.191099 -0.574136 10.04167 0.02920 C87 1 -0.772738 -0.142322 -0.831053 10.04167 0.02920 C99 1 -0.739137 -0.007859 -0.515805 10.04167 0.02920 C121 1 -0.835521 0.040918 -0.772682 10.04167 0.02920 C106 1 -0.928893 -0.025469 -0.447938 10.04167 0.02920 C113 1 -1.025286 0.023328 -0.704834 10.04167 0.02920 C62 1 -0.983383 -0.219590 -0.464346 10.04167 0.02920 C68 1 -1.079777 -0.170812 -0.721252 10.04167 0.02920 C63 1 -0.943512 -0.282189 -0.491215 10.04167 0.02920 C69 1 -1.039895 -0.233393 -0.748111 10.04167 0.02920 C75 1 -0.755616 -0.297519 -0.564623 10.04167 0.02920 C85 1 -0.852009 -0.248722 -0.821510 10.04167 0.02920 C78 1 -0.671914 -0.113379 -0.561053 10.04167 0.02920 C88 1 -0.768298 -0.064602 -0.817960 10.04167 0.02920 C94 1 -0.808070 0.015721 -0.485459 10.04167 0.02920 C116 1 -0.904473 0.064508 -0.742365 10.04167 0.02920 C105 1 -0.975944 -0.088599 -0.442282 10.04167 0.02920 C112 1 -1.072307 -0.039822 -0.699189 10.04167 0.02920 C130 1 -0.886825 -0.334858 -0.598743 10.04167 0.02920 C71 1 -0.934597 -0.310684 -0.726016 10.04167 0.02920 C82 1 -0.690850 -0.220217 -0.650498 10.04167 0.02920 C83 1 -0.738592 -0.196064 -0.777781 10.04167 0.02920 C100 1 -0.722162 0.004053 -0.596174 10.04167 0.02920 C90 1 -0.769894 0.028227 -0.723457 10.04167 0.02920 C107 1 -0.937528 0.028033 -0.510827 10.04167 0.02920 C114 1 -0.985280 0.052196 -0.638090 10.04167 0.02920 C61 1 -1.039279 -0.181418 -0.512409 10.04167 0.02920 C67 1 -1.087042 -0.157254 -0.639682 10.04167 0.02920 C64 1 -0.956817 -0.310918 -0.567957 10.04167 0.02920 C70 1 -1.004568 -0.286734 -0.695230 10.04167 0.02920 C74 1 -0.738591 -0.284297 -0.644773 10.04167 0.02920 C84 1 -0.786342 -0.260134 -0.772036 10.04167 0.02920 C79 1 -0.681680 -0.059477 -0.623433 10.04167 0.02920 C89 1 -0.729432 -0.035323 -0.750697 10.04167 0.02920 C93 1 -0.864766 0.052843 -0.533412 10.04167 0.02920 C115 1 -0.912538 0.077016 -0.660675 10.04167 0.02920 C110 1 -1.034799 -0.102548 -0.499117 10.04167 0.02920 C111 1 -1.082552 -0.078374 -0.626400 10.04167 0.02920 AFIX 9 PART -2 C15 1 -0.794600 -0.192383 -0.442191 10.12500 0.06148 C16 1 -0.769812 -0.107613 -0.441741 10.12500 0.06148 C14 1 -0.761170 -0.245153 -0.497001 10.12500 0.06148 C17 1 -0.713053 -0.080632 -0.496122 10.12500 0.06148 C18 1 -0.723965 -0.002763 -0.536352 10.12500 0.06148 C21 1 -0.841033 -0.058404 -0.424201 10.12500 0.06148 C20 1 -0.851305 0.014835 -0.462081 10.12500 0.06148 C19 1 -0.790976 0.043506 -0.519841 10.12500 0.06148 C25 1 -0.893649 -0.307476 -0.521759 10.12500 0.06148 C24 1 -0.929189 -0.251386 -0.463509 10.12500 0.06148 C13 1 -0.812219 -0.304464 -0.537990 10.12500 0.06148 C23 1 -0.881160 -0.195605 -0.424940 10.12500 0.06148 C22 1 -0.909882 -0.112806 -0.413830 10.12500 0.06148 C35 1 -1.008929 -0.227898 -0.493379 10.12500 0.06148 C36 1 -1.035941 -0.150028 -0.482909 10.12500 0.06148 C37 1 -0.984882 -0.090717 -0.441920 10.12500 0.06148 C28 1 -0.837760 -0.322965 -0.683099 10.12500 0.06148 C27 1 -0.924340 -0.326167 -0.665829 10.12500 0.06148 C12 1 -0.783430 -0.312444 -0.621120 10.12500 0.06148 C26 1 -0.951439 -0.318667 -0.587648 10.12500 0.06148 C34 1 -1.022679 -0.269478 -0.570098 10.12500 0.06148 C31 1 -0.966791 -0.284958 -0.731408 10.12500 0.06148 C32 1 -1.033801 -0.238699 -0.714928 10.12500 0.06148 C33 1 -1.062600 -0.230719 -0.631798 10.12500 0.06148 C10 1 -0.704182 -0.217423 -0.703251 10.12500 0.06148 C9 1 -0.761972 -0.228614 -0.769091 10.12500 0.06148 C11 1 -0.714591 -0.258062 -0.631511 10.12500 0.06148 C29 1 -0.826721 -0.279756 -0.759340 10.12500 0.06148 C30 1 -0.906452 -0.256277 -0.789219 10.12500 0.06148 C8 1 -0.772894 -0.150725 -0.809361 10.12500 0.06148 C7 1 -0.847895 -0.128636 -0.837470 10.12500 0.06148 C45 1 -0.916723 -0.183008 -0.827079 10.12500 0.06148 C53 1 -0.677523 -0.136732 -0.554352 10.12500 0.06148 C52 1 -0.666454 -0.093522 -0.630612 10.12500 0.06148 C54 1 -0.700841 -0.216472 -0.554781 10.12500 0.06148 C55 1 -0.679394 -0.132632 -0.702781 10.12500 0.06148 C56 1 -0.721845 -0.091434 -0.768372 10.12500 0.06148 C51 1 -0.695175 -0.010733 -0.619482 10.12500 0.06148 C50 1 -0.735116 0.028036 -0.681181 10.12500 0.06148 C57 1 -0.748846 -0.013544 -0.757892 10.12500 0.06148 C5 1 -0.963166 -0.049059 -0.809070 10.12500 0.06148 C6 1 -0.876586 -0.045857 -0.826330 10.12500 0.06148 C58 1 -0.828597 0.009944 -0.787751 10.12500 0.06148 C4 1 -0.996596 0.003701 -0.754290 10.12500 0.06148 C42 1 -1.080263 -0.104720 -0.696928 10.12500 0.06148 C43 1 -1.044713 -0.160820 -0.755179 10.12500 0.06148 C44 1 -0.987974 -0.133829 -0.809539 10.12500 0.06148 C3 1 -1.056935 -0.024980 -0.696478 10.12500 0.06148 C39 1 -1.053584 -0.024029 -0.548049 10.12500 0.06148 C40 1 -1.078382 -0.108809 -0.548509 10.12500 0.06148 C41 1 -1.091312 -0.147920 -0.620668 10.12500 0.06148 C2 1 -1.043185 0.016631 -0.619769 10.12500 0.06148 C47 1 -0.919996 0.081523 -0.568201 10.12500 0.06148 C46 1 -0.931065 0.038314 -0.491941 10.12500 0.06148 C38 1 -0.995794 -0.012838 -0.482180 10.12500 0.06148 C1 1 -0.974357 0.070992 -0.630160 10.12500 0.06148 C59 1 -0.864137 0.066034 -0.729511 10.12500 0.06148 C49 1 -0.806347 0.077225 -0.663641 10.12500 0.06148 C48 1 -0.833427 0.084735 -0.585451 10.12500 0.06148 C60 1 -0.945567 0.063022 -0.713270 10.12500 0.06148 AFIX 0 HKLF 4 REM 209b2-295_a.res in P4(1)32 REM wR2 = 0.1725, GooF = S = 1.163, Restrained GooF = 1.163 for all data REM R1 = 0.0759 for 1380 Fo > 4sig(Fo) and 0.1277 for all 2127 data REM 42 parameters refined using 0 restraints END WGHT 0.0470 45.4577 REM Highest difference peak 0.903, deepest hole -0.815, 1-sigma level 0.172 Q1 1 -0.7095 -0.5678 -0.6087 11.00000 0.05 0.90 Q2 1 -0.7021 -0.7765 -0.7197 11.00000 0.05 0.89 Q3 1 -0.7329 -0.5444 -0.6499 11.00000 0.05 0.89 ; _shelx_res_checksum 76350 _shelx_hkl_file ; 0 -1 0 0.20 0.50 0 1 0 0.00 0.40 1 0 0 0.90 0.60 -1 -1 0 3057.49 38.30 0 1 -1 3023.90 42.10 1 0 -1 3118.29 41.20 1 1 0 3126.99 56.79 -1 1 1 580.94 8.40 1 -1 1 559.84 8.70 1 1 1 592.84 8.10 -2 0 0 -4.80 1.10 0 0 2 -4.50 1.00 0 2 0 -2.00 1.40 2 0 0 -4.40 1.20 -2 0 1 231.68 4.40 -1 -2 0 241.28 3.90 -1 2 0 227.88 5.10 0 -1 2 231.08 4.40 0 1 2 236.98 4.60 1 2 0 242.98 3.80 2 0 1 230.38 4.80 -2 -1 0 238.78 4.00 -2 1 0 228.28 5.40 -1 0 2 226.08 4.30 0 -2 1 230.88 4.60 0 2 -1 231.78 4.70 0 2 1 234.98 4.60 1 0 2 231.48 4.70 2 1 0 228.78 3.90 -2 -1 1 2002.00 26.30 -2 1 1 1955.80 27.40 -1 -2 1 1975.60 26.30 -1 -2 1 1913.41 26.00 -1 -1 2 1976.70 51.79 -1 1 2 1961.50 28.00 -1 2 -1 1903.11 28.90 1 -2 1 1942.71 29.50 1 -1 2 1927.11 28.70 1 1 2 1995.90 28.60 1 2 1 1972.50 29.90 2 -1 1 1925.11 26.50 2 1 -1 1971.60 26.00 2 1 1 1948.31 28.10 -2 -2 0 84.59 2.00 -2 0 2 82.49 2.80 -2 2 0 83.89 4.00 0 -2 2 82.59 2.90 0 2 2 81.89 3.10 2 0 2 81.49 3.30 2 2 0 85.99 2.00 -2 -1 2 445.76 6.40 -2 1 2 452.15 7.60 -2 2 -1 430.76 8.70 -2 2 1 443.86 8.10 -1 -2 2 439.96 6.50 -1 2 2 449.36 7.80 1 -2 2 437.06 8.00 1 2 2 448.36 7.40 2 -2 1 433.56 8.60 2 -1 2 435.76 8.20 2 1 2 439.06 7.50 2 2 1 452.75 6.80 -2 -2 2 9999.00 147.39 -2 2 2 9904.61 131.29 2 -2 2 9174.18 132.99 2 2 -2 9425.56 160.48 2 2 2 9705.63 263.37 -3 0 0 0.60 1.60 0 0 3 3.30 1.50 0 3 0 1.10 1.30 3 0 0 0.80 1.60 -3 0 1 379.36 6.90 -1 3 0 368.36 7.30 0 -1 3 366.76 6.60 0 1 3 365.16 6.80 1 3 0 375.26 6.00 3 0 1 368.06 7.10 3 1 0 356.66 6.10 0 3 1 366.96 6.70 1 0 3 363.46 6.90 -1 0 3 362.46 6.40 0 3 -1 370.36 7.00 -3 1 0 358.76 7.80 -1 3 -1 427.96 8.60 3 -1 1 429.76 8.70 3 1 1 430.56 7.30 1 3 -1 433.76 7.00 1 3 1 436.16 7.10 1 1 3 429.26 7.70 -3 -1 1 433.46 7.00 -3 1 1 442.06 8.20 -1 -1 3 436.16 7.00 -1 1 3 435.76 7.70 1 -1 3 428.46 7.90 -1 3 1 438.76 8.10 3 0 2 1953.90 30.90 -3 0 2 1994.60 29.20 -2 3 0 1957.30 27.10 0 -2 3 1917.91 28.30 0 2 3 2021.80 30.30 2 3 0 1966.60 27.70 -2 0 3 1959.00 28.40 0 -3 2 1935.91 29.00 0 3 2 2007.60 27.40 2 0 3 1993.60 30.20 3 2 0 1939.21 27.50 -3 2 0 1996.40 27.60 -1 2 3 73.49 3.80 1 -2 3 75.49 3.80 -3 2 -1 68.09 4.40 2 3 -1 78.09 2.10 -2 3 1 71.69 4.20 3 -1 2 76.59 4.40 2 1 3 78.19 3.90 3 2 1 81.49 3.10 1 3 2 70.39 3.50 -3 1 2 70.89 3.60 -2 -1 3 70.19 2.80 -1 -3 2 73.19 2.80 2 3 1 66.79 2.80 1 2 3 73.99 3.70 -3 2 1 60.59 4.30 -2 -3 1 64.09 1.80 -2 1 3 65.59 3.50 -2 3 -1 67.09 4.70 1 -3 2 67.89 4.00 -3 -1 2 68.09 2.60 3 1 2 68.49 3.60 3 -2 1 62.99 4.30 3 2 -1 66.09 1.90 3 2 -1 71.49 2.00 -1 -2 3 71.29 2.90 -3 -2 2 183.48 3.30 -3 2 2 184.98 5.70 -2 -3 2 185.78 3.20 -2 -2 3 191.78 3.90 -2 2 3 183.38 5.50 2 -3 2 182.98 6.30 2 -2 3 182.78 5.90 2 2 3 188.88 5.20 2 3 2 184.28 4.80 3 -2 2 181.88 6.10 3 2 -2 184.58 3.10 3 2 2 179.08 4.80 -3 0 3 7537.55 101.69 -3 3 0 7568.44 110.99 0 -3 3 7342.17 102.49 0 3 3 7537.75 105.59 3 0 3 7323.57 106.89 3 3 0 7473.35 127.69 -3 -1 3 1160.08 15.20 -3 1 3 1101.99 16.30 -3 3 1 1095.79 17.50 -1 -3 3 1110.69 15.20 -1 3 3 1109.59 16.70 1 -3 3 1112.59 17.00 1 3 3 1135.49 16.40 3 -1 3 1079.89 17.20 3 1 3 1103.29 16.50 3 3 1 1118.59 14.90 -3 -2 3 11.80 2.00 -3 2 3 10.90 2.50 -3 3 2 6.40 2.60 -2 -3 3 14.70 2.00 -2 3 3 6.50 2.50 2 -3 3 16.50 3.20 2 3 3 11.70 2.30 3 -3 2 8.10 3.20 3 -2 3 13.50 3.20 3 2 3 14.30 2.50 3 3 2 11.90 2.10 -3 -3 3 8317.57 100.89 -3 3 3 8338.27 118.09 3 -3 3 7989.10 119.99 3 3 3 8089.89 113.69 0 0 4 6746.52 204.18 0 4 0 6764.42 95.39 4 0 0 6825.92 97.69 -4 0 1 22.50 3.60 -1 4 0 24.70 3.60 0 -1 4 29.50 3.20 0 1 4 26.10 3.00 1 4 0 27.40 2.60 4 0 1 27.70 3.70 0 4 -1 21.50 3.50 0 4 1 27.70 3.00 1 0 4 32.10 3.10 4 1 0 29.20 2.80 -4 1 0 23.00 3.90 -1 0 4 24.60 3.20 -1 -1 4 4289.87 65.79 -1 1 4 4264.57 62.29 -1 4 -1 4261.07 61.69 -1 4 1 4353.86 65.99 -4 -1 1 4264.27 61.79 -4 1 1 4370.76 67.89 4 1 1 4247.88 64.59 1 -1 4 4219.18 139.19 1 1 4 4305.27 145.29 1 4 -1 4318.57 60.99 1 4 1 4451.95 63.69 4 -1 1 4289.07 65.69 2 4 0 8383.06 204.28 -4 2 0 8365.76 123.49 -4 0 2 8442.96 115.89 -2 4 0 8472.45 123.39 0 -2 4 8419.46 246.18 0 2 4 8407.46 118.49 4 0 2 8269.87 119.19 0 4 2 8684.83 118.29 2 0 4 8252.47 119.49 4 2 0 8240.18 108.99 0 -4 2 8491.55 117.19 -2 0 4 8638.94 114.89 -2 -1 4 838.52 12.50 1 4 2 859.11 13.10 -4 2 -1 846.12 15.50 -4 1 2 844.12 13.80 -1 -4 2 857.91 12.70 -2 4 1 844.92 14.40 1 -2 4 833.62 13.80 2 1 4 843.12 13.80 2 4 -1 852.51 11.70 4 2 1 851.01 12.50 4 -1 2 846.72 14.70 -1 2 4 850.51 13.70 2 4 1 857.01 12.30 -4 2 1 856.11 14.80 -4 -1 2 876.41 12.60 1 2 4 848.42 13.70 4 -2 1 834.02 15.40 4 2 -1 844.12 11.60 1 -4 2 846.82 14.60 4 1 2 854.51 13.50 -1 4 2 858.81 14.00 -1 -2 4 837.52 12.60 -2 1 4 842.62 13.30 -2 4 -1 836.02 15.20 2 -1 4 837.72 14.10 2 -4 2 7627.64 112.89 -2 4 -2 7695.53 112.89 -2 4 2 7764.72 112.39 2 -2 4 7720.13 112.19 -2 2 4 7682.23 109.89 -4 -2 2 7949.50 99.59 -4 2 2 7656.73 110.29 -2 -4 2 7785.52 98.59 -2 -2 4 7642.14 102.19 4 2 2 7686.73 156.98 2 2 4 7833.52 137.89 2 4 2 7872.21 108.19 4 -2 2 7654.33 114.49 -3 4 0 571.14 12.40 4 0 3 566.64 11.10 0 -3 4 575.64 10.30 0 3 4 580.74 10.80 3 4 0 572.14 8.30 -4 3 0 566.24 12.40 -4 0 3 586.14 10.10 0 -4 3 563.84 10.40 0 4 3 576.74 10.70 3 0 4 563.14 11.10 4 3 0 577.74 8.30 -3 0 4 573.34 9.90 -3 4 1 2838.22 38.80 -1 3 4 2941.11 39.00 1 -3 4 2870.81 43.10 -1 -4 3 2892.71 40.30 3 4 -1 2873.31 37.30 -4 3 -1 2853.21 40.10 4 -1 3 2823.52 45.70 -3 -1 4 2920.71 41.20 3 1 4 2851.21 42.80 1 4 3 2856.11 40.90 -4 1 3 2874.41 41.60 4 3 1 2946.01 41.20 4 3 -1 2931.91 37.00 -3 1 4 2960.60 38.10 1 3 4 2987.70 43.40 -1 4 3 2995.50 47.00 1 -4 3 2917.41 43.60 -4 3 1 2958.20 44.20 4 1 3 2911.61 43.60 -1 -3 4 2922.21 91.29 -4 -1 3 3010.60 41.00 4 3 -1 2887.81 37.50 -3 -4 1 3000.40 36.60 -3 4 -1 2930.91 40.80 3 4 1 3026.70 43.50 3 -1 4 2873.31 44.50 -2 3 4 1376.36 20.60 -3 -2 4 1373.06 18.10 3 -4 2 1342.97 22.40 -3 4 2 1383.46 21.30 4 -2 3 1375.66 22.00 2 -3 4 1304.57 20.80 -2 -4 3 1376.36 17.80 -4 2 3 1407.26 20.80 3 2 4 1352.36 20.10 2 4 3 1374.46 19.70 4 3 2 1378.66 19.00 -4 3 2 1307.77 20.50 2 3 4 1296.97 19.30 -3 2 4 1298.67 19.60 -4 -2 3 1323.07 17.00 -2 4 3 1314.67 20.10 2 -4 3 1299.17 20.90 -2 -3 4 1294.97 17.40 3 -2 4 1295.47 20.60 3 4 2 1299.37 18.10 4 -3 2 1296.17 21.80 4 2 3 1286.27 19.00 -4 -3 3 663.63 9.00 -4 3 3 676.83 13.00 -3 -4 3 677.13 8.80 -3 -3 4 667.03 9.70 -3 3 4 668.03 12.70 -3 4 3 682.93 13.10 3 -4 3 647.04 13.80 3 -3 4 657.03 13.50 3 3 4 661.73 11.90 3 4 3 664.03 11.40 4 -3 3 658.83 14.00 4 3 3 664.43 11.50 -4 0 4 2978.80 41.20 -4 4 0 2945.61 41.40 0 -4 4 2884.91 42.80 0 4 4 2961.80 42.80 4 0 4 2956.50 41.50 4 4 0 2960.90 39.80 -4 -1 4 1204.78 16.90 -4 1 4 1204.78 18.10 -4 4 -1 1176.58 20.90 -4 4 1 1210.18 20.20 -1 -4 4 1172.18 17.10 -1 4 4 1206.78 18.80 1 -4 4 1164.48 18.70 1 4 4 1183.08 18.30 4 -1 4 1141.89 19.30 4 1 4 1183.28 18.70 4 4 1 1198.18 16.20 -4 -2 4 46.40 3.10 -4 2 4 49.99 4.50 -4 4 2 45.60 4.80 -2 -4 4 57.39 3.10 2 -4 4 44.20 4.90 2 4 4 46.00 4.20 4 -4 2 49.40 6.20 4 -2 4 64.09 5.60 4 2 4 49.60 4.70 4 4 2 46.30 3.40 -4 -3 4 188.78 4.30 -4 3 4 198.88 7.20 -4 4 3 199.48 7.60 -3 -4 4 193.98 4.30 -3 4 4 188.28 6.90 3 -4 4 188.28 8.10 3 4 4 195.68 6.40 4 -4 3 189.28 8.60 4 -3 4 191.28 8.10 4 3 4 181.38 6.20 4 4 3 189.98 6.00 -4 -4 4 4487.45 55.99 -4 4 4 4352.46 57.79 4 -4 4 4525.65 67.89 4 4 4 4348.37 68.99 0 0 5 6.40 2.60 0 5 0 2.80 2.30 5 0 0 3.50 2.70 -5 0 1 3289.37 42.80 -1 5 0 3252.37 49.40 0 -1 5 3221.48 44.50 0 1 5 3282.27 50.39 1 5 0 3297.27 49.10 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20.80 6.60 -3 0 11 8.90 5.00 0 -11 3 4.80 5.00 0 11 -3 7.20 5.30 0 11 3 5.60 5.10 3 0 11 5.80 5.70 11 -3 0 6.30 6.40 -11 0 3 -0.70 5.30 11 3 0 8.20 4.30 -1 11 -3 54.19 9.20 11 3 1 47.70 7.10 -11 1 3 45.30 7.40 -3 -1 11 47.30 7.50 1 11 3 42.20 6.00 11 1 -3 56.09 8.00 3 1 11 33.60 6.10 11 -3 -1 52.79 9.30 -1 -11 3 39.50 7.40 11 -1 3 52.69 9.50 3 11 -1 43.30 6.80 -1 3 11 45.40 7.40 -3 11 1 37.80 7.20 1 -3 11 40.80 6.50 1 3 11 51.59 8.80 11 -3 1 52.29 8.50 3 11 1 38.00 6.60 1 11 -3 47.30 7.70 -1 11 3 43.70 8.20 11 1 3 51.59 8.80 -3 1 11 49.99 8.10 3 -1 11 41.40 6.90 -1 -3 11 44.60 7.40 11 3 -1 45.00 6.80 1 -11 3 48.10 7.20 -11 3 1 38.20 7.90 -3 11 -1 42.00 7.40 -11 -1 3 48.20 6.80 -3 -2 11 104.89 8.80 2 -3 11 105.19 9.80 11 2 -3 101.99 8.60 11 3 2 119.69 8.70 3 2 11 114.29 10.10 -11 2 3 107.39 11.40 -2 -11 3 96.69 8.50 -2 11 -3 114.59 10.40 -3 11 2 92.69 10.60 -2 3 11 121.99 9.70 2 11 3 112.09 8.60 3 11 -2 95.49 7.80 11 -2 3 117.89 11.70 3 -2 11 104.79 10.20 3 11 2 107.39 7.90 11 3 -2 90.59 7.50 11 2 3 118.19 9.40 -3 2 11 116.29 9.30 -3 11 -2 109.09 11.00 -11 3 2 114.89 12.40 -2 -3 11 105.09 8.30 2 -11 3 111.89 10.90 -2 11 3 103.39 10.20 2 3 11 116.39 9.90 11 -3 2 104.39 12.20 3 3 11 1143.39 23.80 3 11 3 1187.18 21.80 3 -3 11 1152.68 24.20 -3 11 -3 1229.08 26.00 -3 3 11 1187.38 23.40 -3 -11 3 1127.59 20.40 11 3 -3 1162.78 20.40 11 3 3 1188.68 22.10 -3 -3 11 1157.18 21.50 -11 3 3 1214.28 26.60 11 -3 3 1213.28 27.30 -3 11 3 1182.88 25.00 3 -11 3 1210.88 26.00 -11 0 4 63.79 9.60 -11 4 0 66.59 9.80 11 4 0 61.99 6.80 11 0 4 75.29 9.80 0 4 11 72.09 9.40 -4 0 11 73.29 8.20 0 -11 4 69.29 9.10 0 11 4 71.69 8.70 4 0 11 83.09 9.90 11 -4 0 59.99 11.20 -4 11 0 50.79 8.30 0 -4 11 69.49 8.20 4 11 0 76.49 6.80 -4 -1 11 317.47 11.80 4 11 -1 316.07 9.70 1 11 4 309.67 11.80 -4 11 1 314.77 14.70 -11 1 4 326.07 14.10 -1 4 11 328.97 13.10 4 1 11 315.37 12.50 -1 -11 4 318.27 12.10 11 -1 4 320.07 14.30 1 -4 11 320.87 12.50 11 4 1 318.57 10.20 1 4 11 309.87 12.80 4 -1 11 306.37 13.50 -4 11 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5 8 47.20 10.30 -8 11 5 29.60 9.30 8 5 11 49.00 8.90 11 8 5 51.19 9.40 -5 8 11 42.00 8.90 -5 11 8 41.00 9.20 8 -5 11 45.50 9.90 11 -8 5 38.80 10.60 -8 5 11 42.80 8.90 5 -11 8 47.60 9.90 -11 8 5 39.90 10.60 8 11 5 51.59 9.30 5 8 11 42.50 8.00 11 5 8 47.20 8.20 -5 -8 11 49.60 8.20 6 11 8 149.88 12.90 8 6 11 166.88 13.50 -8 11 6 159.18 16.20 -8 -6 11 163.38 9.30 -6 8 11 156.28 13.80 8 -11 6 136.19 16.50 11 8 6 156.28 11.70 6 -8 11 156.38 15.30 11 -6 8 170.68 17.00 -11 6 8 161.28 15.50 -11 8 6 151.38 16.30 8 11 6 164.88 11.30 -6 11 8 168.28 14.70 6 -11 8 157.58 16.70 8 -6 11 157.98 15.60 -6 -8 11 166.68 8.90 11 6 8 151.38 13.30 6 8 11 166.38 14.00 -8 6 11 176.88 14.00 11 -8 6 150.08 17.20 11 8 7 64.69 8.70 7 -8 11 58.49 11.30 11 -7 8 53.39 11.90 7 11 8 60.49 11.50 -8 11 7 80.69 12.50 -7 8 11 67.19 10.50 -11 7 8 63.89 11.30 8 7 11 56.29 9.70 8 -11 7 57.99 12.20 8 11 7 60.89 10.70 7 8 11 54.79 9.00 11 7 8 59.69 9.10 11 -8 7 49.99 12.20 -7 11 8 60.79 11.10 7 -11 8 48.70 11.40 -8 7 11 52.39 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31.80 12.30 -1 10 12 25.40 9.10 -1 -12 10 22.80 7.40 10 1 12 26.00 10.40 -10 12 1 27.10 11.70 -10 -1 12 21.30 7.70 10 -12 1 31.50 10.10 1 10 12 23.50 9.30 -10 1 12 34.10 8.60 -12 10 1 28.00 11.40 10 -1 12 36.80 10.80 -12 -1 10 24.90 8.20 12 -10 1 31.00 10.80 -1 -10 12 20.20 7.90 -1 12 10 31.90 9.70 12 1 10 32.90 10.40 1 -12 10 31.00 8.50 -10 12 -1 29.70 12.00 -10 12 2 92.79 15.20 -2 -12 10 80.79 11.20 10 2 12 101.49 15.20 -2 10 12 89.79 13.70 2 12 10 95.49 13.40 -12 2 10 100.29 14.50 10 -12 2 106.79 15.70 -10 -2 12 95.89 11.50 12 -2 10 91.89 16.20 2 -10 12 71.19 13.50 -12 -2 10 89.09 11.60 -2 12 10 94.69 13.80 2 10 12 97.29 13.40 -10 12 -2 106.69 18.00 -2 -10 12 85.59 11.50 12 2 10 101.19 15.00 10 -2 12 94.19 15.50 -12 10 2 88.89 17.00 12 -10 2 106.39 16.50 -10 2 12 88.59 12.30 2 -12 10 89.49 13.60 3 -10 12 136.39 15.00 -3 -12 10 140.59 11.20 -10 -3 12 152.58 11.90 12 -3 10 150.28 17.40 -3 10 12 147.59 14.50 10 3 12 133.09 14.90 3 12 10 159.08 15.10 -12 3 10 142.19 16.00 -10 12 3 143.09 18.10 10 -12 3 138.29 16.90 -12 -3 10 155.68 11.90 12 -10 3 147.39 17.70 -12 10 3 156.88 18.50 3 10 12 142.89 14.20 -10 3 12 133.79 13.40 3 -12 10 126.99 15.00 10 -3 12 135.19 16.90 -3 -10 12 131.39 11.10 12 3 10 132.59 15.20 -3 12 10 141.79 14.70 12 10 4 24.60 6.00 10 -12 4 21.30 10.90 -12 4 10 29.70 10.50 4 12 10 24.50 8.90 4 -10 12 20.90 9.50 -10 -4 12 34.80 7.10 -10 12 4 24.50 11.70 -4 10 12 23.40 9.10 12 -4 10 21.80 11.60 10 4 12 26.40 10.00 -4 -10 12 20.30 6.80 -12 10 4 28.90 12.60 4 10 12 32.00 9.50 10 -4 12 20.50 10.30 12 4 10 24.40 9.90 12 -10 4 14.50 11.20 10 12 4 29.60 6.20 -10 4 12 24.80 9.20 4 -12 10 20.10 9.50 -4 12 10 24.80 9.40 -12 5 10 56.69 11.80 10 -12 5 46.10 11.70 12 10 5 56.09 10.20 5 -10 12 54.19 11.10 12 -5 10 55.99 12.80 10 5 12 65.29 11.60 -10 12 5 58.19 12.00 5 12 10 76.59 13.70 -5 10 12 53.99 10.40 5 10 12 62.59 10.50 -10 5 12 66.09 11.10 12 5 10 70.79 11.40 5 -12 10 54.29 11.00 -5 12 10 54.59 10.50 10 12 5 68.49 10.30 10 -5 12 47.10 10.90 12 -10 5 46.80 12.40 -12 10 5 68.29 13.90 -12 6 10 -3.60 11.10 -10 12 6 7.10 11.70 12 -6 10 6.50 11.40 -6 10 12 18.00 9.80 6 -10 12 2.40 9.50 10 -12 6 3.00 10.80 6 12 10 12.30 8.80 10 6 12 8.30 9.70 12 10 6 8.00 6.90 12 6 10 6.90 9.40 -10 6 12 10.20 10.00 10 -6 12 -1.40 9.60 6 10 12 9.70 8.70 12 -10 6 -4.90 11.20 -12 10 6 -2.60 10.90 10 12 6 11.40 7.20 6 -12 10 6.10 9.90 -6 12 10 5.20 9.50 12 -7 10 0.60 11.40 -12 7 10 -3.60 10.90 10 7 12 -5.00 9.80 12 10 7 -1.50 7.10 7 -10 12 0.60 9.70 -10 12 7 3.00 10.80 10 -12 7 -4.20 10.50 -7 10 12 -0.10 9.60 7 12 10 6.60 8.70 7 10 12 1.30 8.50 -10 7 12 3.30 10.00 -7 12 10 3.00 9.40 10 -7 12 -2.00 10.60 -12 10 7 7.20 12.10 12 7 10 -6.60 8.80 12 -10 7 -15.70 10.00 10 12 7 6.60 7.60 7 -12 10 -4.90 9.80 10 8 12 3.40 9.90 10 -12 8 -9.30 9.90 8 12 10 5.00 8.60 12 -8 10 -5.00 11.10 -10 12 8 5.80 11.60 -8 10 12 2.50 9.90 8 -10 12 -1.00 10.50 -12 8 10 7.30 12.00 12 10 8 2.20 7.70 8 10 12 6.30 9.00 8 -12 10 4.10 10.50 10 12 8 2.50 7.80 12 -10 8 2.80 11.30 -12 10 8 5.80 12.10 12 8 10 -2.40 9.40 -10 8 12 2.30 10.40 -8 12 10 9.00 10.30 10 -8 12 -2.40 10.50 12 -9 10 0.20 11.30 12 10 9 1.50 8.20 -10 12 9 11.20 12.20 10 -12 9 -9.80 11.10 -12 9 10 11.20 12.50 9 12 10 3.20 9.10 -9 10 12 0.80 10.50 10 9 12 1.40 9.00 9 -10 12 -7.70 10.90 12 -10 9 -1.90 11.50 10 -9 12 -7.40 11.20 -10 9 12 6.40 11.30 -12 10 9 4.50 12.30 12 9 10 -1.30 9.40 9 10 12 3.50 8.60 -9 12 10 9.60 11.40 10 12 9 -4.80 8.30 9 -12 10 -7.40 10.90 10 -10 12 3.50 12.40 10 12 10 14.60 9.00 -12 10 10 31.40 13.80 -10 10 12 23.50 12.60 -10 12 10 27.10 13.00 12 -10 10 9.40 12.20 10 10 12 17.40 9.90 10 -12 10 8.50 11.60 12 10 10 9.90 9.00 0 -11 12 42.60 9.00 -12 11 0 40.50 12.70 0 12 11 43.80 9.90 11 0 12 49.99 12.00 12 -11 0 38.40 10.60 0 11 12 42.00 9.70 12 0 11 44.60 11.80 -11 12 0 44.40 12.90 -11 0 12 49.30 9.40 0 -12 11 48.30 8.90 -12 0 11 49.20 9.70 -12 1 11 73.39 13.50 -1 11 12 62.89 10.80 1 -11 12 52.59 9.60 -11 -1 12 69.69 12.20 -1 -12 11 53.59 8.80 -11 12 1 64.79 13.40 11 -12 1 49.99 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273.77 13.70 0 1 13 262.37 13.00 1 13 0 269.17 12.70 13 0 -1 275.77 14.50 13 0 1 270.17 14.70 13 1 0 265.27 13.30 13 -1 0 279.97 15.60 1 0 13 268.27 13.40 -1 0 13 263.97 12.80 0 13 -1 268.87 13.70 0 13 1 265.87 12.90 13 1 1 3.40 6.70 13 1 -1 0.10 6.30 13 -1 1 0.90 7.90 -1 -1 13 6.80 6.30 -1 1 13 9.80 6.70 -1 13 -1 -3.00 7.00 -1 13 1 -5.30 6.90 1 -1 13 5.10 6.70 1 1 13 9.80 6.90 1 13 -1 1.60 6.20 1 13 1 -0.10 6.00 13 -1 -1 -2.50 7.60 -2 13 0 28.10 8.30 0 -2 13 37.20 7.50 0 2 13 48.20 9.00 0 13 2 30.20 7.40 2 0 13 46.30 8.10 13 -2 0 40.80 9.30 13 2 0 35.70 6.90 -2 0 13 37.60 7.20 0 13 -2 29.70 7.50 13 0 2 32.60 8.50 2 13 0 41.30 6.70 13 0 -2 33.10 8.00 13 1 -2 65.09 11.20 -1 2 13 69.39 10.70 2 1 13 80.09 11.20 13 2 1 73.09 10.50 13 -1 2 65.39 11.80 1 -2 13 81.99 10.80 -2 13 1 68.49 12.60 2 13 -1 65.79 9.90 1 13 2 74.09 10.40 -2 -1 13 68.19 10.60 13 -2 -1 72.89 10.10 -1 13 -2 64.29 11.80 -1 13 2 59.59 10.80 -2 1 13 72.49 10.20 2 13 1 66.89 10.00 2 -1 13 81.09 11.10 -2 13 -1 66.69 11.60 1 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14.60 8.50 -13 8 5 10.00 11.00 -5 -8 13 11.00 6.70 -8 5 13 15.70 8.70 -8 13 6 31.80 11.40 8 6 13 36.80 10.50 6 13 8 48.90 8.80 13 8 6 40.30 8.50 -6 8 13 27.90 9.70 -8 -6 13 40.90 7.20 8 -13 6 22.40 10.70 -13 6 8 33.70 11.90 13 -6 8 20.20 11.60 6 -8 13 29.90 10.30 13 -8 6 22.80 12.10 13 6 8 29.70 9.50 6 8 13 32.30 9.50 8 -6 13 30.00 10.60 -8 6 13 22.60 8.90 6 -13 8 24.50 10.70 -6 13 8 32.30 10.80 -13 8 6 42.20 12.10 8 13 6 41.90 7.70 -6 -8 13 35.20 6.90 -7 8 13 16.50 9.20 8 7 13 17.70 10.00 7 -8 13 22.90 10.50 -8 13 7 16.40 11.50 7 13 8 23.80 7.80 8 -13 7 18.10 11.00 -13 7 8 18.40 11.80 13 8 7 14.10 8.10 13 -7 8 6.40 11.90 7 8 13 10.80 8.80 -8 7 13 19.70 10.10 13 7 8 8.20 8.50 7 -13 8 1.20 9.80 8 -7 13 16.80 10.00 -13 8 7 29.70 12.20 -7 13 8 18.00 10.70 13 -8 7 8.40 11.80 8 13 7 22.40 7.40 8 13 8 13.90 7.80 13 -8 8 -4.50 11.20 8 8 13 7.50 9.00 -8 8 13 1.00 9.00 -13 8 8 9.90 11.60 8 -8 13 4.60 10.20 13 8 8 8.90 8.70 -8 13 8 15.60 11.30 8 -13 8 -0.10 9.80 0 13 9 124.59 14.10 13 -9 0 121.89 16.40 0 -13 9 118.59 12.20 0 -9 13 114.09 12.90 -9 13 0 132.09 18.20 0 9 13 127.49 14.00 13 0 9 122.99 16.30 -13 0 9 130.29 14.50 9 0 13 120.19 15.70 -13 9 0 132.59 18.60 -9 0 13 121.29 12.50 -13 1 9 38.10 9.80 9 1 13 44.90 10.60 -9 -1 13 40.60 8.30 -1 -13 9 34.70 7.80 -1 9 13 34.20 9.30 13 -1 9 44.60 11.90 1 -9 13 31.80 8.80 -9 13 1 33.10 11.10 1 13 9 45.50 9.80 -9 13 -1 27.80 11.40 13 -9 1 37.20 11.30 -9 1 13 43.00 8.80 9 -1 13 42.10 10.60 -1 13 9 36.30 9.60 -13 -1 9 36.30 8.90 1 -13 9 35.40 8.60 1 9 13 36.70 9.20 13 1 9 33.20 10.70 -13 9 1 35.70 11.80 -1 -9 13 30.00 8.30 2 -9 13 146.79 14.80 2 13 9 178.18 15.30 9 -13 2 168.08 16.40 -2 -13 9 154.08 11.60 -9 13 2 178.78 19.20 13 -2 9 157.38 17.20 -9 -2 13 161.98 12.00 9 2 13 150.88 15.40 -2 9 13 155.48 13.30 -13 2 9 171.18 15.70 -9 2 13 147.79 13.00 13 -9 2 181.08 18.30 2 9 13 168.28 14.80 2 -13 9 162.38 14.60 -2 -9 13 155.58 12.70 -13 -2 9 175.18 13.00 -2 13 9 159.18 14.90 13 2 9 163.18 16.10 9 -2 13 156.38 16.50 -13 9 2 182.58 18.70 -9 13 -2 168.18 19.00 -3 -13 9 26.60 7.10 -13 3 9 25.30 10.50 3 13 9 31.70 9.10 -3 9 13 26.50 9.10 3 -9 13 30.90 9.40 -9 13 3 29.50 12.30 9 3 13 22.20 9.80 -9 -3 13 27.00 7.60 9 -13 3 31.00 10.80 13 -3 9 23.30 12.20 3 -13 9 34.20 9.60 -13 -3 9 43.50 8.40 13 3 9 30.60 10.70 13 -9 3 36.40 11.90 3 9 13 37.00 9.70 -13 9 3 29.70 12.20 -9 3 13 27.60 8.80 9 -3 13 26.70 10.10 -3 -9 13 34.20 7.90 -3 13 9 25.80 9.60 -13 4 9 40.50 11.20 -9 13 4 39.50 12.70 4 13 9 44.70 9.40 -4 9 13 33.20 9.70 9 4 13 44.30 10.70 -9 -4 13 46.50 7.70 4 -9 13 35.20 9.80 13 -4 9 33.40 12.40 13 9 4 41.70 7.10 9 -13 4 47.20 11.60 -9 4 13 28.70 9.00 4 9 13 45.90 9.50 13 -9 4 42.60 12.40 -4 13 9 43.30 10.20 -13 9 4 37.50 12.40 13 4 9 30.40 10.70 9 -4 13 35.00 10.40 9 13 4 44.80 6.90 -4 -9 13 43.60 7.90 4 -13 9 33.10 10.40 13 -5 9 54.19 13.00 -9 13 5 68.49 13.30 5 -9 13 62.79 11.40 -13 5 9 62.09 11.90 9 -13 5 59.19 12.00 5 13 9 83.89 13.70 -5 9 13 77.69 14.00 13 9 5 59.89 8.30 9 5 13 58.09 11.70 -9 -5 13 71.69 10.10 -13 9 5 61.19 12.80 9 13 5 80.89 10.30 13 -9 5 53.59 13.20 9 -5 13 46.80 11.60 5 -13 9 53.89 11.10 -9 5 13 47.60 10.80 -5 13 9 54.99 10.90 13 5 9 50.79 10.50 5 9 13 48.60 10.20 -5 -9 13 67.49 10.20 -9 13 6 45.80 12.70 9 -13 6 41.10 11.80 6 -9 13 35.60 10.60 13 9 6 39.10 8.40 6 13 9 45.00 9.20 -13 6 9 37.80 12.30 -6 9 13 35.90 10.20 9 6 13 39.50 10.80 13 -6 9 35.40 12.90 13 6 9 38.10 10.30 9 -6 13 29.90 11.00 -13 9 6 52.89 13.20 13 -9 6 25.20 12.10 6 9 13 37.30 9.70 9 13 6 49.00 7.90 -9 6 13 38.30 10.50 6 -13 9 31.20 10.90 -6 13 9 40.50 11.10 -13 7 9 57.99 13.00 7 -9 13 42.70 11.30 -9 13 7 50.29 12.50 9 7 13 60.19 12.10 9 -13 7 40.60 12.40 7 13 9 71.19 13.10 13 -7 9 35.90 13.50 13 9 7 49.40 9.20 -7 9 13 42.10 11.10 13 7 9 48.60 10.50 7 -13 9 41.30 11.80 -13 9 7 65.19 13.90 9 -7 13 40.00 11.60 7 9 13 45.00 10.00 -7 13 9 55.79 12.00 13 -9 7 30.50 12.90 9 13 7 67.49 11.70 -9 7 13 50.49 11.00 -8 9 13 20.80 10.50 -9 13 8 32.60 12.70 8 -9 13 4.40 10.20 13 9 8 17.00 8.90 9 -13 8 5.60 10.20 13 -8 9 5.50 12.00 9 8 13 21.40 10.60 8 13 9 22.60 8.70 -13 8 9 22.20 12.60 9 -8 13 13.90 10.70 -8 13 9 23.60 10.90 -9 8 13 21.40 10.10 13 -9 8 5.30 12.00 8 -13 9 3.60 10.50 13 8 9 15.30 9.50 -13 9 8 28.40 13.10 8 9 13 12.60 9.40 9 13 8 22.90 8.30 13 9 9 0.00 9.10 -9 13 9 15.70 12.50 9 -13 9 -6.80 10.80 -13 9 9 18.80 13.30 -9 9 13 7.50 10.70 9 13 9 -0.30 8.60 13 -9 9 4.30 11.60 9 -9 13 -5.90 10.40 9 9 13 14.90 9.90 -13 0 10 19.40 8.60 0 13 10 20.60 9.70 13 0 10 26.00 11.70 -10 13 0 26.50 11.70 0 10 13 28.70 9.50 0 -10 13 19.00 8.40 -10 0 13 29.20 8.90 0 -13 10 24.30 8.20 -13 10 0 30.90 12.50 10 0 13 22.80 10.70 13 -10 0 23.90 10.30 10 -13 1 41.30 11.00 10 1 13 43.20 11.70 1 13 10 46.70 10.00 -1 10 13 26.40 8.70 -10 -1 13 48.00 9.00 13 -1 10 42.00 12.50 -1 -13 10 42.80 8.10 -13 1 10 41.70 9.90 1 -10 13 38.60 9.50 -10 13 1 44.30 12.60 -10 1 13 45.50 9.50 1 10 13 40.00 9.10 1 -13 10 39.70 9.30 -1 13 10 45.40 10.30 -10 13 -1 50.29 13.70 10 -1 13 38.60 11.20 -1 -10 13 41.70 8.90 13 1 10 48.90 12.30 -13 -1 10 41.50 9.40 13 -10 1 55.99 12.60 -13 10 1 46.90 12.50 10 -13 2 36.00 10.60 2 13 10 34.40 9.70 2 -10 13 19.90 9.30 -2 10 13 30.50 9.80 13 -2 10 24.40 11.90 -13 2 10 27.80 10.10 10 2 13 37.00 11.00 -10 -2 13 31.20 8.10 -2 -13 10 24.60 7.60 -10 13 2 35.00 12.70 13 -10 2 25.80 11.20 2 -13 10 27.60 9.50 -2 13 10 32.00 10.10 -13 10 2 36.70 12.80 -10 2 13 30.40 9.60 -13 -2 10 30.80 8.60 10 -2 13 25.10 11.00 2 10 13 33.90 9.70 -2 -10 13 21.90 7.80 -10 13 -2 26.70 12.00 13 2 10 23.50 11.20 -10 13 3 9.90 12.00 3 13 10 9.20 8.80 -13 3 10 -2.00 9.80 10 -13 3 7.00 10.30 13 -3 10 -1.70 11.20 -10 -3 13 5.30 7.10 -3 10 13 6.60 8.90 3 -10 13 -0.30 9.00 10 3 13 -0.50 10.00 10 -3 13 2.70 10.10 -3 13 10 6.60 8.80 3 10 13 12.10 9.20 13 -10 3 8.60 10.60 -13 10 3 8.40 11.80 3 -13 10 0.10 9.00 -10 3 13 4.90 9.00 -3 -10 13 -5.70 7.10 13 3 10 -2.10 10.40 -4 10 13 118.29 14.50 4 13 10 133.99 13.90 -13 4 10 124.09 16.90 10 4 13 101.29 15.60 4 -10 13 114.69 14.70 -10 13 4 138.09 18.90 10 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8.20 11.10 7 13 10 8.70 9.00 -13 7 10 10.70 12.10 -10 13 7 15.50 12.30 7 -10 13 -7.90 9.50 10 -13 7 -3.00 10.70 -7 10 13 6.80 9.80 13 -7 10 -2.10 12.20 -7 13 10 9.10 10.20 10 -7 13 -3.20 10.70 -10 7 13 8.60 10.90 13 7 10 -2.20 9.90 10 13 7 13.80 7.40 7 10 13 7.60 9.20 7 -13 10 -6.70 10.50 13 -10 7 -3.60 11.40 -13 10 7 10.80 12.60 13 -8 10 5.10 12.90 10 8 13 22.70 11.80 -10 13 8 10.70 11.60 -8 10 13 12.60 10.30 8 -10 13 -3.20 10.50 13 10 8 12.90 8.40 8 13 10 14.30 9.10 -13 8 10 17.30 12.20 10 -13 8 -1.10 11.00 8 10 13 18.40 9.80 -13 10 8 14.90 13.10 10 -8 13 2.20 10.50 13 8 10 3.30 10.20 -10 8 13 16.10 11.60 -8 13 10 20.90 11.60 8 -13 10 0.70 11.10 13 -10 8 5.00 12.30 10 13 8 19.00 8.70 9 -10 13 -6.00 11.20 -13 9 10 21.70 13.10 13 -9 10 5.60 12.80 13 10 9 12.30 9.00 -10 13 9 24.90 12.60 10 9 13 14.60 10.80 9 13 10 8.30 10.00 -9 10 13 13.40 12.20 10 -13 9 1.80 11.80 9 10 13 12.70 9.90 10 13 9 11.10 9.20 9 -13 10 -1.70 11.70 -13 10 9 19.80 13.90 -10 9 13 23.40 12.50 13 9 10 15.70 10.70 10 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13.60 11 -13 2 33.10 11.30 -2 -13 11 35.30 7.90 -2 11 13 29.20 9.50 13 -2 11 23.40 12.70 -13 11 2 37.90 13.10 2 -13 11 31.60 9.20 13 2 11 15.10 11.80 13 -11 2 23.80 11.30 -13 -2 11 39.00 8.20 2 11 13 31.00 10.00 -2 13 11 28.50 10.00 11 -2 13 22.30 11.20 -2 -11 13 27.80 8.00 -11 2 13 26.30 9.30 3 -11 13 57.69 10.70 -13 3 11 70.99 12.20 -11 13 3 78.49 14.80 11 3 13 65.79 12.80 13 -3 11 67.49 14.20 -3 11 13 79.49 14.30 3 13 11 84.49 14.00 11 -13 3 56.99 12.10 13 3 11 59.99 12.90 3 -13 11 64.19 11.00 -3 13 11 65.49 11.60 -3 -11 13 66.49 11.80 13 -11 3 68.49 13.60 -11 3 13 79.49 14.60 11 -3 13 53.99 12.90 -13 11 3 66.49 13.80 3 11 13 62.19 11.10 11 -13 4 8.40 10.20 13 -4 11 -10.10 11.00 4 13 11 15.50 9.10 4 -11 13 0.90 8.90 -4 11 13 12.30 9.40 -11 13 4 6.90 11.80 11 4 13 -4.30 10.60 -13 4 11 5.90 10.90 11 -4 13 -2.70 11.10 13 4 11 -2.10 10.20 -11 4 13 5.90 9.60 4 -13 11 0.20 9.60 13 -11 4 6.70 11.10 -4 13 11 7.00 8.90 -13 11 4 11.50 12.40 4 11 13 7.90 9.50 11 -13 5 -0.20 10.70 5 -11 13 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13.00 -8 11 13 -4.70 10.60 -13 8 11 15.30 13.20 11 -13 8 -16.70 10.80 8 13 11 -10.20 9.80 8 -11 13 -13.30 11.10 -11 13 8 0.30 14.00 11 8 13 -3.40 12.00 13 11 8 -11.30 7.50 13 8 11 -5.60 11.00 -13 11 8 1.70 14.10 8 -13 11 -15.60 11.00 8 11 13 -8.70 9.50 -11 8 13 8.60 12.90 -8 13 11 1.90 11.30 11 13 8 -13.00 8.10 13 -11 8 -2.60 11.80 11 -8 13 -18.70 11.10 11 -13 9 20.60 13.40 -13 9 11 42.50 15.20 -11 13 9 39.30 15.30 11 9 13 32.20 13.70 13 -9 11 11.10 14.30 13 11 9 26.60 9.10 9 13 11 22.20 11.10 -9 11 13 35.70 13.50 9 -11 13 3.70 12.60 -9 13 11 40.20 13.80 9 11 13 27.70 11.30 11 -9 13 10.10 13.40 9 -13 11 17.60 12.70 13 9 11 36.40 12.40 -11 9 13 41.40 14.40 11 13 9 45.80 10.80 13 -11 9 12.00 13.30 -13 11 9 31.00 15.70 -10 11 13 73.79 15.80 10 -11 13 27.50 14.40 10 13 11 56.29 12.50 11 -13 10 21.20 13.80 11 10 13 55.69 12.80 13 -10 11 20.50 14.80 -13 10 11 63.19 16.00 -11 13 10 67.19 16.80 13 11 10 44.60 10.60 13 10 11 41.90 11.50 11 13 10 58.39 11.60 -10 13 11 62.09 16.60 10 11 13 46.90 12.50 -11 10 13 70.89 15.90 13 -11 10 27.40 14.90 -13 11 10 65.29 16.80 13 -11 11 10.00 15.20 -11 13 11 46.70 17.00 13 11 11 27.10 10.90 -11 11 13 68.89 17.40 11 -13 11 5.80 13.50 11 11 13 35.10 12.60 11 13 11 41.90 12.40 -13 11 11 54.69 16.40 -13 0 12 8.10 9.20 13 -12 0 1.20 10.20 0 13 12 7.30 9.80 -12 0 13 13.20 8.80 0 -13 12 1.40 7.80 0 -12 13 3.00 8.30 12 0 13 -7.50 11.70 0 12 13 -2.20 8.80 13 0 12 -8.00 12.00 -12 13 0 9.20 13.10 12 -13 0 1.50 10.10 -13 12 0 5.70 12.10 12 -13 1 51.69 12.50 -1 -13 12 55.19 9.10 12 1 13 31.10 12.50 -13 1 12 80.69 14.20 1 13 12 47.90 11.10 -1 12 13 52.09 10.90 -12 13 1 55.79 14.30 13 -1 12 40.90 13.60 1 -12 13 39.00 9.70 -13 12 1 52.59 13.40 -12 13 -1 61.79 15.30 -1 -12 13 49.80 9.00 -1 13 12 39.90 10.70 1 -13 12 50.59 9.70 -13 -1 12 58.29 10.10 12 -1 13 37.50 13.20 -12 1 13 73.39 13.40 1 12 13 43.40 10.60 13 1 12 37.50 13.40 13 -12 1 42.70 12.10 -13 2 12 47.50 11.40 13 -2 12 13.50 13.20 12 -13 2 38.70 11.90 2 13 12 34.10 10.50 12 2 13 21.30 12.30 2 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13 -7.60 9.50 -13 5 12 9.80 12.10 12 5 13 1.10 12.40 -5 12 13 12.60 10.10 -12 13 5 -0.90 13.10 -12 5 13 10.30 12.00 13 -12 5 5.40 11.80 5 -13 12 -1.50 9.90 5 12 13 4.90 10.30 -13 12 5 7.40 13.60 12 -5 13 -9.00 11.90 -5 13 12 4.00 9.80 13 5 12 -2.20 11.80 12 -13 6 14.20 12.40 6 13 12 12.00 10.60 13 -6 12 -6.10 12.90 -6 12 13 19.40 11.10 12 6 13 14.00 13.10 -13 6 12 18.20 13.70 6 -12 13 7.60 10.70 -12 13 6 13.40 14.10 13 -12 6 11.30 12.20 6 12 13 19.10 10.60 12 -6 13 -4.90 13.00 -13 12 6 13.90 14.10 -12 6 13 14.00 13.30 -6 13 12 29.00 11.20 13 6 12 8.10 12.50 6 -13 12 3.30 11.40 13 -7 12 -18.70 13.20 12 -13 7 -4.70 11.30 -13 7 12 10.30 13.90 7 -12 13 -4.80 11.10 -7 12 13 10.10 10.30 12 7 13 1.90 13.30 -12 13 7 19.20 14.50 7 13 12 -1.90 10.20 -7 13 12 9.30 10.80 12 -7 13 -9.50 12.20 7 12 13 9.60 10.80 13 -12 7 -6.10 11.40 7 -13 12 -9.10 11.30 -13 12 7 9.10 15.20 13 7 12 -6.90 12.90 -12 7 13 17.30 13.50 12 -13 8 4.10 12.60 8 -12 13 -0.80 11.90 -13 8 12 32.70 15.10 -12 13 8 15.40 15.50 12 8 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27.80 10.20 -14 3 11 19.60 10.70 11 -14 3 18.00 10.70 -3 11 14 13.90 9.50 11 3 14 12.50 12.60 3 -14 11 10.30 9.50 -11 3 14 23.50 9.50 14 3 11 10.00 12.60 -3 -11 14 27.40 9.50 -3 14 11 23.90 10.00 3 11 14 16.10 10.10 14 -11 3 15.80 11.90 11 -3 14 12.60 11.90 -14 11 3 38.80 14.20 4 -11 14 31.80 11.00 11 -14 4 35.20 11.80 -11 14 4 52.59 15.00 -4 11 14 44.50 10.90 4 14 11 50.89 10.90 14 -4 11 28.80 14.40 -14 4 11 58.29 12.50 11 4 14 49.70 14.00 -14 11 4 66.39 15.80 -11 4 14 42.10 10.90 4 11 14 46.40 11.50 11 -4 14 21.10 12.30 -4 14 11 45.50 11.10 14 4 11 31.00 12.80 14 -11 4 37.50 12.80 4 -14 11 40.60 11.30 5 14 11 38.10 10.90 14 -5 11 19.10 15.10 11 5 14 46.80 13.90 11 -14 5 30.40 12.40 5 -11 14 23.70 10.90 -11 14 5 39.80 14.30 -14 5 11 50.59 13.00 -5 11 14 33.30 10.20 5 11 14 31.10 11.20 5 -14 11 31.30 11.40 -5 14 11 43.90 11.90 -14 11 5 43.70 14.80 14 5 11 31.60 12.70 -11 5 14 50.49 12.30 11 -5 14 29.20 13.00 14 -11 5 35.30 13.50 14 -6 11 14.00 15.50 -14 6 11 30.70 13.40 -11 14 6 34.50 14.60 11 -14 6 25.10 12.50 -6 11 14 30.70 11.70 11 6 14 26.00 13.40 6 14 11 30.10 10.50 6 -11 14 6.70 11.40 6 -14 11 20.50 11.70 14 6 11 13.20 12.10 -14 11 6 31.90 15.70 14 -11 6 26.40 13.80 11 -6 14 6.60 12.80 6 11 14 27.90 11.30 -11 6 14 32.60 12.60 -6 14 11 28.90 11.60 -7 11 14 18.50 11.30 -11 14 7 36.10 15.50 11 -14 7 13.00 12.70 -14 7 11 21.50 13.40 11 7 14 20.00 14.20 14 -7 11 6.30 13.80 7 -11 14 2.80 11.70 7 14 11 14.00 10.60 -14 11 7 13.30 15.00 11 -7 14 -1.10 12.50 7 11 14 19.20 11.10 -11 7 14 39.80 13.40 14 -11 7 15.10 13.40 -7 14 11 23.60 12.10 7 -14 11 9.00 12.30 14 7 11 11.00 12.90 11 -14 8 13.40 12.40 14 -8 11 29.90 16.50 11 8 14 30.40 14.50 -14 8 11 51.29 15.70 8 -11 14 2.60 12.10 -11 14 8 44.30 16.40 -8 11 14 31.50 12.30 8 14 11 31.00 11.20 -11 8 14 48.80 15.00 8 -14 11 13.20 12.60 8 11 14 23.00 12.10 -14 11 8 41.40 16.40 14 8 11 29.20 13.50 11 -8 14 4.80 13.50 14 -11 8 22.90 15.10 -8 14 11 37.00 14.00 9 -11 14 -15.50 11.60 9 14 11 5.60 11.00 14 11 9 16.00 9.80 11 9 14 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14 10.10 13.80 -14 3 12 47.10 12.50 12 -14 3 24.50 11.80 14 -3 12 0.60 14.70 -12 14 3 39.20 15.20 3 12 14 21.60 11.10 3 -14 12 25.70 10.10 14 3 12 18.60 14.00 12 -3 14 -3.80 12.70 14 -12 3 22.60 13.20 -12 3 14 30.30 11.50 -14 12 3 45.90 15.80 -3 14 12 36.10 11.50 12 -14 4 18.30 11.90 4 14 12 16.10 10.50 -12 14 4 18.80 14.60 4 -12 14 3.00 10.50 -14 4 12 16.10 12.60 12 4 14 0.60 13.70 14 -4 12 -21.40 14.30 -4 12 14 18.70 10.70 14 -12 4 4.70 12.40 -14 12 4 24.60 15.00 -4 14 12 18.70 10.90 -12 4 14 24.50 12.40 4 12 14 8.40 10.80 12 -4 14 -6.40 12.70 14 4 12 -10.70 13.00 4 -14 12 10.80 10.70 -12 14 5 37.30 16.00 -14 5 12 36.20 13.80 5 14 12 28.50 11.50 14 -5 12 -0.20 15.10 5 -12 14 18.00 11.10 12 -14 5 22.30 12.30 12 5 14 21.10 14.30 -5 12 14 24.40 10.60 12 -5 14 -1.30 13.00 5 12 14 22.80 11.50 -14 12 5 21.30 15.70 -12 5 14 37.00 13.90 14 -12 5 25.40 13.60 5 -14 12 16.70 11.10 -5 14 12 21.50 11.00 14 5 12 10.90 13.60 -14 6 12 26.40 13.80 12 6 14 -0.80 13.90 14 -6 12 -11.70 15.10 -6 12 14 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8.50 6.50 -4 -1 15 7.20 7.80 4 1 15 17.40 8.80 15 -4 -1 11.20 10.10 1 -4 15 11.90 8.00 4 15 -1 14.20 6.60 15 1 -4 13.90 8.00 -1 4 15 14.10 8.10 15 -1 4 10.80 10.50 -4 15 1 2.90 10.00 1 15 4 16.30 8.20 -1 -15 4 15.10 7.80 -1 15 4 16.10 9.00 1 4 15 21.60 8.50 15 -4 1 14.70 11.10 15 -1 -4 14.70 8.80 15 4 -1 14.60 6.40 4 -1 15 11.60 8.60 -4 15 -1 13.90 9.80 -4 1 15 16.20 8.00 -1 -4 15 13.00 7.80 15 1 4 13.70 9.60 4 15 1 19.40 7.20 1 -15 4 11.20 8.10 -2 4 15 111.39 13.00 2 -4 15 98.49 14.10 4 2 15 105.19 14.00 -15 2 4 104.49 16.00 15 -2 4 124.29 18.20 -4 -2 15 107.99 12.60 -4 15 2 116.39 16.10 4 15 -2 131.89 10.80 -2 -15 4 113.29 11.70 15 2 -4 115.99 12.00 15 -4 -2 136.19 17.00 2 15 4 127.09 12.90 15 4 2 102.79 12.00 4 -2 15 114.49 14.00 2 -15 4 114.79 14.60 -2 -4 15 119.29 12.10 4 15 2 117.79 11.80 2 4 15 116.59 13.60 15 4 -2 123.89 10.40 -2 15 4 117.79 14.40 15 2 4 113.59 14.50 15 -2 -4 113.59 14.30 -4 15 -2 116.99 15.30 15 -4 2 105.39 18.30 -4 2 15 117.29 12.80 15 -4 -3 20.50 10.00 15 3 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3 -5 15 29.10 9.10 15 -3 5 32.00 12.90 3 5 15 25.70 8.30 5 15 3 55.69 10.60 15 -5 3 33.00 12.80 -15 5 3 31.90 12.10 5 -3 15 30.40 9.60 -3 15 5 36.50 10.80 15 3 5 26.20 9.50 -5 15 -3 34.20 12.00 -3 -5 15 35.10 8.30 -5 3 15 25.70 8.70 3 -15 5 26.60 10.10 -5 15 4 26.40 11.40 -5 -4 15 20.70 7.80 5 4 15 23.30 9.30 4 -5 15 16.40 9.50 -4 5 15 15.90 8.60 15 -4 5 10.30 12.50 15 5 4 12.10 8.20 -15 4 5 22.20 11.20 4 15 5 28.00 7.50 5 -15 4 19.10 10.30 4 -15 5 16.90 10.10 -5 4 15 23.20 8.60 15 4 5 16.40 9.00 15 -5 4 6.10 12.10 -4 15 5 22.60 10.90 5 15 4 23.60 7.20 -15 5 4 22.90 11.80 5 -4 15 23.60 9.50 -4 -5 15 21.50 7.90 4 5 15 18.80 9.10 15 -5 5 6.80 12.30 -5 -5 15 12.40 7.70 5 5 15 5.10 9.10 5 15 5 15.90 7.30 5 -5 15 11.90 9.60 15 5 5 2.70 8.20 -5 15 5 11.10 10.60 -15 5 5 0.10 10.60 5 -15 5 7.50 10.10 -5 5 15 5.30 8.40 0 15 6 71.99 12.80 -15 0 6 72.79 13.80 -6 15 0 78.89 13.50 0 -6 15 51.29 9.50 15 0 6 63.79 12.60 6 0 15 55.19 10.50 0 -15 6 49.00 9.30 0 6 15 55.29 10.10 -6 0 15 50.79 9.30 15 -6 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67.89 12.40 -3 6 15 40.50 9.40 3 -6 15 56.09 10.30 3 15 6 80.69 12.60 -6 -3 15 69.89 11.70 -3 -6 15 77.29 12.20 -6 3 15 49.20 9.90 15 3 6 49.50 11.00 15 -6 3 50.59 13.60 -3 15 6 70.89 11.90 -15 6 3 58.99 13.20 6 15 3 74.09 10.70 6 -3 15 67.19 11.70 3 6 15 69.29 13.00 3 -15 6 51.59 10.60 -6 15 4 13.30 11.70 -6 -4 15 11.80 7.80 4 -6 15 6.40 9.30 15 6 4 -2.00 7.60 6 -15 4 7.00 9.70 15 -4 6 14.40 12.70 4 15 6 15.70 7.70 -15 4 6 8.60 10.80 6 4 15 5.50 8.90 -4 6 15 2.80 8.20 6 -4 15 9.20 9.70 -15 6 4 1.80 11.90 15 4 6 4.40 9.20 -6 4 15 0.80 8.20 -4 -6 15 8.00 7.70 15 -6 4 -2.50 12.10 6 15 4 13.30 6.30 -4 15 6 13.70 11.00 4 6 15 9.20 9.00 4 -15 6 -0.60 9.60 15 6 5 18.90 8.50 -15 5 6 33.90 12.10 15 -5 6 23.30 13.50 -6 -5 15 26.60 7.90 6 -15 5 29.70 11.40 -6 15 5 30.70 12.00 6 5 15 17.70 9.60 -5 6 15 13.30 8.80 5 15 6 34.30 8.30 5 -6 15 18.90 9.60 6 15 5 31.90 7.50 15 5 6 19.90 9.30 15 -6 5 11.80 12.30 -6 5 15 23.40 9.40 5 6 15 22.90 9.60 -15 6 5 21.70 12.60 6 -5 15 19.30 10.00 -5 -6 15 27.20 7.70 -5 15 6 27.30 11.70 5 -15 6 21.00 10.40 -15 6 6 2.00 12.00 6 15 6 7.60 7.30 -6 -6 15 -2.70 7.20 -6 6 15 -3.80 8.50 -6 15 6 4.80 11.60 6 6 15 -0.40 9.30 6 -6 15 -1.60 9.40 15 -6 6 -10.60 12.10 15 6 6 -12.00 7.60 6 -15 6 -7.30 9.50 7 0 15 145.79 15.90 0 -15 7 137.09 13.50 -7 0 15 148.29 13.90 0 15 7 165.08 14.20 15 0 7 117.89 16.60 0 -7 15 139.09 14.10 0 7 15 142.89 13.00 -7 15 0 173.78 18.30 15 -7 0 163.48 17.90 -15 0 7 156.58 14.20 1 15 7 -0.30 7.90 -7 15 1 6.90 11.70 15 -1 7 -12.20 11.50 7 1 15 -0.30 9.10 15 -7 -1 0.10 11.10 -7 -1 15 0.80 7.80 -1 7 15 -1.10 8.50 1 -7 15 -2.90 7.60 -1 -15 7 -2.10 6.80 -15 1 7 5.20 9.50 15 1 7 -15.70 10.40 -7 1 15 1.90 8.00 15 -7 1 1.90 11.10 -1 15 7 5.20 8.50 -7 15 -1 -7.70 10.90 -15 -1 7 3.30 7.60 7 -1 15 -3.90 9.00 1 7 15 3.70 8.60 1 -15 7 -12.80 7.30 -1 -7 15 0.50 7.70 7 2 15 8.30 9.90 15 -7 -2 8.10 11.00 15 -2 7 1.60 12.40 -2 7 15 7.80 9.00 2 -7 15 4.00 8.90 -2 -15 7 4.00 6.50 7 -15 2 10.40 9.40 -15 2 7 10.40 10.40 -7 -2 15 11.10 7.90 2 15 7 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29.20 12.70 -5 7 15 4.80 8.80 15 7 5 5.40 7.90 5 -7 15 10.10 9.70 -7 -5 15 24.30 7.80 7 -15 5 20.70 10.90 15 -5 7 10.00 13.20 -15 5 7 25.90 12.50 5 15 7 24.50 8.50 -7 15 5 26.00 12.40 7 5 15 14.30 10.20 15 -7 5 4.60 12.20 5 -15 7 12.40 10.50 -7 5 15 13.70 9.10 -15 7 5 22.60 12.80 7 15 5 27.40 7.50 5 7 15 10.90 9.40 -5 15 7 20.60 10.80 -5 -7 15 23.60 7.90 7 -5 15 13.30 9.80 15 5 7 10.00 9.70 6 15 7 12.10 8.10 -15 6 7 24.60 12.70 -7 -6 15 19.40 7.60 7 -15 6 5.70 10.20 15 7 6 -0.50 8.10 -7 15 6 16.50 12.10 6 -7 15 3.20 9.70 -6 7 15 10.50 9.00 15 -6 7 3.30 12.80 7 6 15 10.40 10.40 15 -7 6 10.20 13.30 -6 15 7 23.50 11.70 -6 -7 15 12.50 7.60 6 7 15 13.10 9.50 -7 6 15 10.70 8.80 -15 7 6 22.50 12.80 15 6 7 9.10 8.40 6 -15 7 8.50 10.10 7 -6 15 7.10 10.10 7 15 6 16.10 7.60 15 -7 7 25.10 14.80 15 7 7 35.50 9.60 7 -15 7 25.20 11.20 -7 15 7 44.90 13.40 -15 7 7 49.30 13.90 7 15 7 45.30 9.20 7 7 15 29.50 10.60 -7 7 15 35.90 10.10 7 -7 15 13.80 10.60 -8 15 0 7.10 12.00 8 0 15 0.20 9.30 0 8 15 -3.80 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10.10 20 -9 2 -20.00 19.10 -2 20 9 18.40 15.90 20 -9 -3 34.20 21.10 20 -3 9 -39.30 23.20 9 -20 3 -3.30 12.20 9 3 20 -21.40 18.40 -3 9 20 15.30 11.80 3 20 9 47.60 13.20 -3 20 9 11.60 17.30 -9 3 20 6.30 10.10 9 -3 20 -22.40 13.80 20 -9 3 11.20 20.00 3 9 20 0.50 12.70 20 -4 9 -29.10 23.20 -4 9 20 6.70 11.50 20 -9 -4 -17.30 18.10 -9 20 4 36.20 18.70 9 -20 4 -4.50 12.60 9 4 20 -28.00 17.90 -4 20 9 37.20 16.90 9 -4 20 -10.40 13.60 4 9 20 -18.20 12.80 20 -9 4 -12.80 19.60 -9 4 20 8.00 10.40 -9 20 5 63.49 20.70 20 -9 -5 15.20 18.80 5 9 20 0.30 13.90 -9 5 20 0.50 10.30 9 -5 20 -3.60 13.20 20 -9 -6 68.79 18.80 -9 20 6 69.69 18.60 -6 20 9 50.19 18.30 -10 0 20 8.30 10.30 0 20 10 59.59 16.40 10 -20 0 32.00 12.40 0 10 20 8.50 11.80 10 -20 1 9.50 12.90 -1 10 20 27.40 12.80 10 1 20 -8.70 17.00 -1 20 10 11.70 15.60 -10 1 20 13.00 10.70 1 10 20 8.20 12.50 10 -1 20 0.00 17.90 20 -10 1 -29.20 19.00 -2 10 20 22.80 12.30 20 -10 -2 -2.10 19.00 10 -20 2 21.20 12.30 2 20 10 45.20 13.80 10 2 20 -19.50 17.30 10 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18.20 11 -2 20 -0.70 18.90 2 11 20 33.60 14.50 -11 2 20 56.19 13.90 0 0 21 -5.80 10.10 1 0 21 10.50 11.20 -1 -1 21 2.80 10.80 1 1 21 1.60 10.90 0 21 2 26.00 13.50 0 2 21 -1.60 10.70 0 -2 21 0.60 11.00 -2 0 21 -6.40 10.30 2 0 21 -12.90 10.60 2 1 21 7.30 11.70 -2 -1 21 1.00 10.40 1 -2 21 -1.60 10.90 2 -21 1 38.70 10.50 -1 2 21 9.90 11.40 21 -2 -1 21.50 14.10 2 -1 21 2.30 11.70 -1 -2 21 14.70 10.80 -1 21 2 30.00 14.00 -2 1 21 12.40 11.30 1 -21 2 5.10 11.50 2 -2 21 -0.60 11.20 2 2 21 -5.80 11.00 -2 2 21 -5.70 10.70 -2 21 2 39.80 14.70 -2 -2 21 7.60 10.50 2 -21 2 -10.40 10.50 21 -2 -2 34.40 12.80 21 -3 0 14.60 15.90 -1 3 21 1.90 10.60 3 1 21 -6.60 11.30 1 -3 21 4.30 11.70 21 -3 -1 17.80 14.60 -3 -1 21 0.50 10.40 1 21 3 53.49 13.90 -3 1 21 -3.20 10.30 1 3 21 -0.60 11.00 -1 -3 21 7.20 11.10 3 -1 21 -0.90 11.20 3 -21 2 -5.80 10.80 3 2 21 1.00 12.00 -3 21 2 46.40 15.60 2 -3 21 14.30 11.50 -2 3 21 10.10 11.00 21 -3 -2 -11.90 14.70 -3 -2 21 10.10 11.00 2 3 21 -3.00 11.00 21 -3 2 -29.60 17.10 -3 2 21 11.10 10.80 -2 -3 21 15.20 10.90 2 -21 3 18.00 10.70 3 -2 21 4.60 11.50 21 -2 -3 -15.30 14.80 -3 3 21 21.40 11.10 3 -3 21 7.20 11.70 -3 -3 21 2.50 10.80 -3 21 3 37.10 16.00 3 3 21 5.20 11.70 21 -3 -3 -18.00 14.30 21 -3 3 -20.30 18.80 3 -21 3 15.30 10.90 21 -4 0 55.59 17.00 0 -4 21 23.90 12.00 0 21 4 53.29 15.10 4 1 21 -10.70 12.00 21 -4 -1 -20.20 16.40 -4 21 1 35.90 16.20 4 -21 1 26.40 10.90 1 21 4 23.70 13.30 1 -4 21 -4.10 11.10 -4 -1 21 4.80 10.60 -1 4 21 -8.80 10.60 4 -1 21 -16.80 11.90 -1 -4 21 0.20 10.20 -1 21 4 35.10 15.30 21 1 4 4.50 13.30 -4 1 21 4.90 10.50 1 4 21 -3.00 11.20 21 -4 -2 -28.00 15.40 2 -4 21 -10.90 11.50 -4 -2 21 9.70 11.00 4 -21 2 -10.40 11.00 4 2 21 -10.20 11.80 -2 4 21 -0.80 11.00 -4 2 21 7.20 11.00 -2 -4 21 -3.30 9.70 2 -21 4 -6.30 11.60 2 4 21 0.60 11.40 -2 21 4 37.70 14.70 4 -2 21 3.30 11.80 -4 21 3 40.00 16.60 4 3 21 1.80 12.50 -4 -3 21 -0.90 10.60 -3 4 21 7.00 10.90 3 -4 21 0.90 11.90 4 -21 3 18.90 11.30 21 -4 -3 -9.40 15.90 -4 3 21 11.30 10.90 -3 -4 21 5.60 10.60 3 4 21 10.70 12.00 4 -3 21 -1.70 11.50 3 -21 4 -10.70 11.20 21 -3 -4 -18.80 14.10 4 -4 21 7.50 11.90 21 -4 -4 -6.60 15.40 -4 4 21 23.60 11.60 -4 -4 21 10.70 11.00 4 4 21 12.90 12.60 4 -21 4 -6.50 11.50 0 -5 21 -3.40 10.60 0 5 21 -4.10 11.10 21 0 5 0.60 16.10 21 -5 0 -2.90 16.70 -5 0 21 15.50 11.10 0 21 5 22.50 14.40 5 0 21 -6.60 12.50 5 -21 1 14.60 10.40 5 1 21 -18.00 12.70 1 21 5 0.60 13.20 1 -5 21 -13.80 11.20 -5 -1 21 -2.80 10.60 -1 5 21 0.80 11.00 -5 1 21 1.80 10.50 21 -5 1 25.00 18.40 -1 21 5 19.10 15.30 -1 -5 21 -0.10 10.80 1 5 21 0.00 11.30 21 -5 -2 -29.60 16.80 -2 5 21 -9.10 10.30 2 -5 21 -4.20 10.90 -5 -2 21 -8.30 10.30 5 -21 2 -7.80 11.00 2 21 5 19.70 13.60 5 2 21 -9.80 12.80 5 -2 21 -12.30 11.60 -2 21 5 30.10 16.50 21 -5 2 -33.70 17.90 2 5 21 -9.10 11.50 -2 -5 21 0.40 10.70 -5 2 21 4.50 10.90 -5 21 3 37.90 16.80 -5 -3 21 -3.50 10.00 5 3 21 -7.10 12.10 5 -21 3 0.70 11.20 21 -5 -3 -12.20 16.70 3 -5 21 3.20 11.30 -3 5 21 7.40 10.90 21 -3 -5 -19.90 20.10 -3 -5 21 -4.00 9.60 -5 3 21 11.80 10.20 3 5 21 4.60 12.20 3 -21 5 -16.40 10.40 -3 21 5 39.80 17.30 5 -3 21 -4.60 12.10 -5 -4 21 7.50 10.60 4 -5 21 8.20 11.70 5 4 21 9.80 13.20 5 -21 4 8.50 12.40 21 -5 -4 11.00 17.70 -4 5 21 22.00 10.90 21 -5 4 -6.00 20.90 4 -21 5 -0.20 11.10 5 -4 21 8.20 12.30 4 5 21 15.50 12.90 -5 4 21 25.50 11.60 21 -4 -5 1.30 15.40 -4 -5 21 -0.60 10.50 5 -5 21 -9.00 11.80 -5 5 21 6.60 10.80 5 -21 5 -9.60 11.00 5 5 21 7.50 12.10 21 -5 -5 -14.60 16.40 -5 -5 21 -4.10 10.70 0 21 6 25.20 14.80 -6 0 21 10.70 10.20 6 0 21 -13.40 12.80 0 6 21 1.40 11.40 0 -6 21 -17.80 10.70 6 -21 1 23.00 11.50 1 -6 21 -9.50 11.10 -6 -1 21 0.10 10.40 6 1 21 -11.40 13.80 -1 6 21 -1.80 10.80 21 -6 -1 -8.40 17.40 21 -1 6 -15.20 18.70 1 6 21 -0.20 11.50 -6 21 -1 65.49 18.80 -1 21 6 27.50 15.70 21 -6 1 26.80 17.60 -6 1 21 21.70 10.30 6 2 21 -1.00 14.80 -2 6 21 13.70 11.50 21 -6 2 -3.90 20.60 -2 21 6 43.20 17.20 6 -2 21 -9.70 12.90 -6 2 21 14.80 11.20 -2 -6 21 -9.60 10.40 2 6 21 5.80 12.10 -6 21 3 64.79 18.60 -3 6 21 21.30 11.40 -6 -3 21 1.40 10.30 6 3 21 -1.80 15.10 21 -6 -3 1.00 18.70 6 -21 3 14.70 11.70 3 -6 21 2.00 11.40 -3 21 6 32.50 16.80 -3 -6 21 23.30 10.50 3 6 21 5.30 12.50 21 -6 3 -18.00 20.30 6 -3 21 11.10 12.90 -6 3 21 9.20 10.90 3 -21 6 -13.00 12.70 21 -6 -4 -12.10 18.00 6 -21 4 5.30 12.30 4 -6 21 -15.70 10.70 -6 21 4 39.90 19.20 -6 -4 21 -2.50 10.30 6 4 21 -6.30 13.70 -4 6 21 5.70 11.00 -4 21 6 26.70 17.20 4 6 21 1.20 12.50 6 -4 21 -4.60 12.00 21 -4 -6 1.70 15.40 4 -21 6 -14.40 10.50 -6 4 21 -9.90 10.20 -4 -6 21 -12.70 10.20 -5 6 21 14.60 11.40 21 -6 -5 39.10 17.50 21 -5 -6 28.30 16.60 6 -5 21 -8.60 12.10 5 6 21 -1.00 13.10 -6 5 21 -0.60 11.00 -5 21 6 38.90 19.00 6 -21 6 13.00 12.20 -6 6 21 19.80 11.50 6 6 21 35.30 13.70 21 -6 6 -33.80 21.60 6 -6 21 10.90 13.60 21 -6 -6 49.00 18.90 0 -7 21 -1.20 11.30 7 -21 0 21.00 11.00 -7 0 21 8.30 10.80 0 7 21 -3.00 11.40 7 0 21 -11.60 14.00 21 -7 -1 -21.90 18.00 7 1 21 -10.10 14.50 7 -21 1 1.20 10.90 21 -1 7 -27.30 20.40 -7 -1 21 15.10 10.70 -1 7 21 3.30 11.40 -7 21 -1 40.50 18.20 2 21 7 36.60 14.00 21 -7 -2 -25.70 19.30 7 -21 2 2.40 11.10 -2 7 21 14.10 11.60 -7 -2 21 20.90 10.40 7 2 21 -20.60 15.70 -7 2 21 -0.60 10.90 2 7 21 -17.40 11.70 -2 -7 21 -10.20 10.50 7 -2 21 -7.80 13.00 -2 21 7 48.40 17.50 21 -7 2 49.40 18.80 -7 -3 21 29.10 10.70 7 -21 3 11.20 12.40 21 -7 -3 -16.80 19.70 -3 7 21 20.40 11.30 3 21 7 30.80 17.00 7 3 21 -2.20 16.90 -3 21 7 39.30 18.10 -7 3 21 4.70 11.00 3 7 21 4.50 12.50 7 -3 21 4.50 13.70 21 -7 3 -30.20 22.10 -3 -7 21 7.20 10.80 21 -7 -4 -9.30 17.30 -4 7 21 0.40 11.10 7 -21 4 -15.20 12.10 7 4 21 -5.80 14.20 -4 21 7 42.90 17.50 4 7 21 0.40 13.20 7 -4 21 -20.90 12.50 -7 4 21 -8.70 10.20 -5 7 21 4.00 11.00 7 5 21 -2.40 15.00 21 -7 -5 31.30 17.80 -7 21 5 74.69 19.10 5 7 21 -4.80 13.50 -5 21 7 20.80 17.80 21 -5 -7 -4.20 16.70 -7 5 21 4.00 10.90 5 -21 7 27.50 10.80 -7 21 6 138.09 20.20 -6 21 7 55.69 20.60 0 21 8 30.80 15.10 0 8 21 13.20 12.20 8 -21 0 31.80 11.60 21 -8 0 -8.40 18.80 -8 0 21 6.40 10.80 1 21 8 35.50 15.20 8 -21 1 6.10 11.70 21 -8 1 -32.90 21.80 -8 1 21 3.90 10.80 -1 -8 21 -15.20 11.00 1 8 21 4.50 12.20 8 -1 21 -9.70 14.70 -8 -2 21 8.20 11.20 8 -21 2 10.30 11.50 21 -8 -2 -14.30 20.70 8 2 21 -7.40 16.20 -2 8 21 12.90 11.60 2 21 8 24.80 14.30 21 -8 2 37.90 19.70 8 -21 3 3.80 12.00 21 -3 8 -38.40 23.20 -3 8 21 11.70 11.50 3 -8 21 -15.60 11.20 21 -8 -3 -6.70 21.10 8 3 21 -20.20 16.50 3 21 8 28.10 14.30 -8 3 21 1.30 10.00 8 -3 21 -20.10 13.20 21 -8 3 -11.60 22.40 3 8 21 -8.10 12.70 8 4 21 -13.30 17.30 8 -21 4 -2.80 12.10 -8 21 4 61.09 19.50 21 -8 -4 22.30 21.20 -4 8 21 -3.50 10.80 -4 21 8 44.60 18.30 8 -4 21 -11.00 13.50 -8 4 21 2.60 10.10 4 8 21 -0.40 13.50 0 21 9 38.00 15.70 0 9 21 13.90 12.60 9 -21 0 13.80 11.20 21 -9 0 -24.10 21.90 9 0 21 -19.20 15.80 -9 0 21 11.40 10.80 -9 -1 21 8.10 11.10 9 -21 1 -10.70 11.90 1 -9 21 -19.90 10.30 21 -9 -1 -27.50 18.60 -1 9 21 14.80 11.90 9 1 21 -11.80 17.30 1 21 9 32.00 15.90 -9 1 21 15.20 10.70 -1 21 9 24.40 15.90 1 9 21 21.90 13.30 9 -1 21 -7.40 16.80 -1 -9 21 -12.50 11.30 21 -9 1 -24.20 20.60 -9 21 2 150.08 20.40 0 0 22 20.20 11.20 0 -1 22 23.60 11.30 0 1 22 15.90 11.30 1 0 22 16.20 11.30 -1 0 22 18.50 11.60 -1 -1 22 19.30 11.30 1 1 22 21.80 11.60 22 -1 1 -30.10 23.20 1 -1 22 27.30 11.60 -1 1 22 20.80 11.40 0 2 22 11.90 11.60 0 -2 22 8.20 11.10 -2 0 22 4.50 11.00 2 0 22 13.20 11.70 -1 2 22 21.40 11.50 1 -2 22 11.40 11.10 2 -22 1 30.70 11.10 -2 -1 22 29.10 11.90 2 1 22 12.40 11.70 -2 1 22 26.10 11.90 -1 -2 22 22.00 11.20 1 2 22 15.80 11.40 2 -1 22 11.10 11.40 2 -2 22 26.10 12.40 2 -22 2 17.70 14.60 -2 -2 22 24.90 11.60 -2 2 22 26.60 11.40 22 -2 2 -11.50 17.70 2 2 22 18.80 11.40 3 0 22 0.50 11.60 0 -3 22 -0.40 11.00 0 3 22 11.60 11.40 -3 0 22 21.60 11.00 -3 -1 22 11.40 11.40 1 -3 22 4.70 11.70 -1 3 22 6.50 11.30 3 -22 1 19.90 11.10 3 1 22 10.10 12.50 22 -3 -1 11.70 15.90 -3 1 22 1.60 10.50 -1 -3 22 10.20 10.70 22 -3 1 -31.10 17.60 3 -1 22 7.20 11.90 1 3 22 16.90 11.90 22 -3 -2 46.40 15.40 -3 2 22 2.60 10.70 3 -2 22 -3.90 12.30 -2 -3 22 -6.40 10.20 2 3 22 8.70 12.00 3 -3 22 -10.70 11.30 -3 -3 22 -3.70 10.80 3 3 22 -9.40 11.00 3 -22 3 -1.10 11.40 -3 3 22 0.60 10.50 4 0 22 -14.70 12.00 0 -4 22 -16.60 10.60 0 4 22 0.20 11.40 22 -4 0 9.10 17.50 -4 0 22 -4.30 10.90 -4 -1 22 -2.20 10.80 4 -22 1 10.20 11.00 4 1 22 -3.10 12.20 -1 4 22 3.10 11.00 1 -4 22 -9.40 10.90 22 -4 -1 48.10 17.30 -1 -4 22 4.90 10.90 22 -4 -2 -19.70 16.70 4 -22 2 -3.20 11.10 -4 -2 22 -10.80 10.10 4 2 22 -9.60 12.20 2 -4 22 -9.60 11.70 -2 4 22 1.30 11.10 -4 2 22 -3.10 10.80 4 -2 22 -4.20 11.90 2 4 22 -18.60 11.20 -2 -4 22 5.20 10.70 -3 4 22 -4.80 10.70 -4 -3 22 -5.00 10.20 4 3 22 -4.50 12.50 3 -4 22 -19.30 11.80 4 -22 3 0.50 11.90 3 4 22 -18.50 11.60 -3 -4 22 -13.80 10.50 3 -22 4 -19.30 15.40 -4 3 22 -8.00 10.40 4 -22 4 -17.80 12.00 4 4 22 -8.00 12.10 -4 4 22 -7.30 10.40 -4 -4 22 -8.80 10.40 22 0 5 -16.60 17.50 5 0 22 -1.90 13.20 -5 0 22 3.40 11.00 0 -5 22 -3.90 10.60 0 5 22 14.30 11.80 0 22 5 43.80 15.80 1 22 5 42.00 22.00 22 -5 -1 -4.50 18.20 22 -5 1 -31.60 20.10 5 -1 22 -20.20 12.10 1 5 22 -9.70 11.50 -1 -5 22 -5.80 11.00 -5 1 22 -4.30 10.20 -2 5 22 -13.00 10.50 -5 -2 22 -8.60 10.40 5 2 22 -11.00 12.80 5 -22 2 -5.80 11.10 2 5 22 -2.90 12.00 -2 -5 22 4.90 10.50 -5 2 22 2.90 10.20 5 -22 3 -5.10 11.70 5 3 22 -16.40 13.30 -5 -3 22 -5.80 10.70 -3 5 22 -9.10 10.90 3 -5 22 -16.40 11.50 5 -3 22 -10.80 12.50 3 5 22 -0.30 12.60 -5 3 22 11.60 11.20 -3 -5 22 -6.90 10.70 5 -22 4 -12.80 12.30 -5 -4 22 -0.80 11.10 5 4 22 -5.70 13.00 -4 5 22 12.40 11.20 4 -5 22 -6.10 12.20 5 -4 22 -6.70 12.00 -5 4 22 -1.80 10.90 4 5 22 -6.40 12.30 6 -22 0 41.20 11.70 -6 0 22 21.30 10.80 0 22 6 37.70 15.70 22 -6 0 28.50 20.10 1 22 6 38.40 15.40 -6 -1 22 12.20 11.00 22 -1 6 0.40 19.70 22 -6 1 33.00 19.10 -1 22 6 31.70 16.40 6 -1 22 -13.00 13.20 1 6 22 -6.80 11.80 -6 1 22 11.70 10.50 2 -6 22 -13.30 10.90 6 2 22 -13.50 15.80 6 -22 2 10.00 11.20 -6 -2 22 -0.20 10.90 -2 6 22 -7.50 11.00 -2 -6 22 -6.00 10.70 -6 2 22 0.70 10.70 -2 22 6 39.50 16.70 6 -2 22 -5.10 13.70 2 6 22 -11.20 12.00 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 7115 _olex2_submission_special_instructions 'No special instructions were received'