data_mj19295_0m _audit_creation_date 2019-05-08 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _shelx_SHELXL_version_number '2016/6' _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_name '' _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C37 H26 N2 O2' _chemical_formula_sum 'C37 H26 N2 O2' _chemical_formula_weight 530.60 _chemical_absolute_configuration rmad _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0148 0.0070 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0253 0.0136 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0412 0.0250 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'orthorhombic' _space_group_IT_number 19 _space_group_name_H-M_alt 'P 21 21 21' _space_group_name_Hall 'P 2ac 2ab' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' _cell_length_a 7.304(7) _cell_length_b 14.694(16) _cell_length_c 25.32(3) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 2717(5) _cell_formula_units_Z 4 _cell_measurement_reflns_used 1196 _cell_measurement_temperature 296(2) _cell_measurement_theta_max 45.80 _cell_measurement_theta_min 8.02 _shelx_estimated_absorpt_T_max 0.998 _shelx_estimated_absorpt_T_min 0.960 _exptl_absorpt_coefficient_mu 0.407 _exptl_absorpt_correction_T_max 0.7508 _exptl_absorpt_correction_T_min 0.4403 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1586 before and 0.1034 after correction. The Ratio of minimum to maximum transmission is 0.5864. The \l/2 correction factor is Not present.' _exptl_absorpt_special_details ? _exptl_crystal_colour yellow _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 1.297 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description 'needle' _exptl_crystal_F_000 1112 _exptl_crystal_size_max 0.1 _exptl_crystal_size_mid 0.03 _exptl_crystal_size_min 0.005 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.1687 _diffrn_reflns_av_unetI/netI 0.1483 _diffrn_reflns_Laue_measured_fraction_full 0.969 _diffrn_reflns_Laue_measured_fraction_max 0.965 _diffrn_reflns_limit_h_max 5 _diffrn_reflns_limit_h_min -8 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_l_max 30 _diffrn_reflns_limit_l_min -30 _diffrn_reflns_number 27385 _diffrn_reflns_point_group_measured_fraction_full 0.968 _diffrn_reflns_point_group_measured_fraction_max 0.963 _diffrn_reflns_theta_full 53.594 _diffrn_reflns_theta_max 55.597 _diffrn_reflns_theta_min 3.025 _diffrn_ambient_temperature 296 _diffrn_detector_area_resol_mean ? _diffrn_measured_fraction_theta_full 0.969 _diffrn_measured_fraction_theta_max 0.965 _diffrn_measurement_device_type 'Bruker D8 Venture' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type GaK\a _diffrn_radiation_wavelength 1.34139 _diffrn_source ? _diffrn_standards_number 0 _reflns_Friedel_coverage 0.747 _reflns_Friedel_fraction_full 0.967 _reflns_Friedel_fraction_max 0.961 _reflns_number_gt 1691 _reflns_number_total 5079 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'SAINT v8.37A (Bruker, 2015)' _computing_data_collection ? _computing_data_reduction 'SAINT v8.37A (Bruker, 2015)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _refine_diff_density_max 0.181 _refine_diff_density_min -0.181 _refine_diff_density_rms 0.044 _refine_ls_abs_structure_details ; Flack x determined using 432 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.4(8) _refine_ls_extinction_coef 0.027(3) _refine_ls_extinction_expression 'Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^' _refine_ls_extinction_method 'SHELXL-2016/6 (Sheldrick 2016)' _refine_ls_goodness_of_fit_ref 0.747 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 372 _refine_ls_number_reflns 5079 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.2512 _refine_ls_R_factor_gt 0.1094 _refine_ls_restrained_S_all 0.747 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0500P)^2^+10.0000P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2146 _refine_ls_wR_factor_ref 0.3180 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C25(H25) 2.b Secondary CH2 refined with riding coordinates: C26(H26A,H26B) 2.c Aromatic/amide H refined with riding coordinates: C2(H2), C4(H4), C5(H5), C9(H9), C10(H10), C12(H12), C15(H15), C16(H16), C17(H17), C18(H18), C20(H20), C21(H21), C22(H22), C23(H23), C28(H28), C29(H29), C31(H31), C32(H32), C33(H33), C34(H34) 2.d Idealised Me refined as rotating group: C37(H37A,H37B,H37C) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.0393(15) -0.7530(6) -0.4898(4) 0.132(4) Uani 1 1 d . . . . . O2 O 0.0573(17) -0.9653(7) -0.2575(5) 0.152(4) Uani 1 1 d . . . . . N1 N 0.030(2) -0.2573(10) -0.4615(8) 0.165(7) Uani 1 1 d . . . . . N2 N 0.046(2) -1.1455(10) -0.6739(7) 0.140(5) Uani 1 1 d . . . . . C1 C 0.003(2) -0.6967(9) -0.4469(7) 0.113(4) Uani 1 1 d . . . . . C2 C 0.030(2) -0.6059(8) -0.4594(6) 0.119(5) Uani 1 1 d . . . . . H2 H 0.075884 -0.590229 -0.492467 0.142 Uiso 1 1 calc R . . . . C3 C -0.010(2) -0.5393(8) -0.4238(7) 0.115(5) Uani 1 1 d . . . . . C4 C -0.083(2) -0.5684(10) -0.3746(7) 0.129(5) Uani 1 1 d . . . . . H4 H -0.115956 -0.524713 -0.349751 0.155 Uiso 1 1 calc R . . . . C5 C -0.1079(19) -0.6589(9) -0.3626(6) 0.123(5) Uani 1 1 d . . . . . H5 H -0.160562 -0.675351 -0.330529 0.148 Uiso 1 1 calc R . . . . C6 C -0.053(2) -0.7269(8) -0.3988(7) 0.114(5) Uani 1 1 d . . . . . C7 C -0.0808(19) -0.8254(9) -0.3892(7) 0.105(4) Uani 1 1 d . . . . . C8 C -0.0717(19) -0.8793(8) -0.4377(7) 0.111(4) Uani 1 1 d . . . . . C9 C -0.097(2) -0.9761(9) -0.4395(7) 0.120(5) Uani 1 1 d . . . . . H9 H -0.131529 -1.007884 -0.409340 0.144 Uiso 1 1 calc R . . . . C10 C -0.071(2) -1.0211(10) -0.4864(8) 0.119(5) Uani 1 1 d . . . . . H10 H -0.090335 -1.083679 -0.485703 0.143 Uiso 1 1 calc R . . . . C11 C -0.0213(18) -0.9859(9) -0.5330(7) 0.103(4) Uani 1 1 d . . . . . C12 C 0.0129(18) -0.8916(8) -0.5317(6) 0.111(4) Uani 1 1 d . . . . . H12 H 0.048677 -0.861518 -0.562353 0.133 Uiso 1 1 calc R . . . . C13 C -0.006(2) -0.8438(9) -0.4854(7) 0.112(4) Uani 1 1 d . . . . . C14 C 0.005(2) -0.4424(9) -0.4371(8) 0.121(5) Uani 1 1 d . . . . . C15 C -0.025(3) -0.4101(11) -0.4859(8) 0.143(6) Uani 1 1 d . . . . . H15 H -0.048513 -0.450803 -0.513174 0.172 Uiso 1 1 calc R . . . . C16 C -0.020(3) -0.3188(10) -0.4967(8) 0.164(8) Uani 1 1 d . . . . . H16 H -0.054068 -0.299229 -0.530231 0.197 Uiso 1 1 calc R . . . . C17 C 0.059(2) -0.2859(10) -0.4127(10) 0.151(7) Uani 1 1 d . . . . . H17 H 0.086145 -0.243780 -0.386464 0.181 Uiso 1 1 calc R . . . . C18 C 0.050(2) -0.3784(9) -0.3998(7) 0.138(6) Uani 1 1 d . . . . . H18 H 0.074675 -0.396757 -0.365429 0.166 Uiso 1 1 calc R . . . . C19 C -0.0005(19) -1.0356(10) -0.5818(8) 0.111(4) Uani 1 1 d . . . . . C20 C 0.058(2) -1.1267(10) -0.5808(8) 0.123(5) Uani 1 1 d . . . . . H20 H 0.085018 -1.154029 -0.548579 0.148 Uiso 1 1 calc R . . . . C21 C 0.075(2) -1.1738(11) -0.6246(9) 0.124(5) Uani 1 1 d . . . . . H21 H 0.112070 -1.233983 -0.620809 0.149 Uiso 1 1 calc R . . . . C22 C -0.007(2) -1.0577(14) -0.6752(7) 0.134(5) Uani 1 1 d . . . . . H22 H -0.029298 -1.030826 -0.707869 0.160 Uiso 1 1 calc R . . . . C23 C -0.030(2) -1.0061(10) -0.6303(9) 0.121(5) Uani 1 1 d . . . . . H23 H -0.069374 -0.946337 -0.634411 0.145 Uiso 1 1 calc R . . . . C24 C -0.092(2) -0.8546(10) -0.3385(8) 0.113(4) Uani 1 1 d . . . . . C25 C -0.018(2) -0.8127(9) -0.2921(7) 0.125(5) Uani 1 1 d . . . . . H25 H 0.045773 -0.756921 -0.302878 0.150 Uiso 1 1 calc R . . . . C26 C 0.127(2) -0.8807(9) -0.2725(7) 0.141(6) Uani 1 1 d . . . . . H26A H 0.216675 -0.889840 -0.300318 0.170 Uiso 1 1 calc R . . . . H26B H 0.190542 -0.854180 -0.242551 0.170 Uiso 1 1 calc R . . . . C27 C -0.098(2) -0.9899(11) -0.2814(8) 0.135(6) Uani 1 1 d . . . . . C28 C -0.159(3) -1.0765(12) -0.2654(7) 0.149(6) Uani 1 1 d . . . . . H28 H -0.088148 -1.111187 -0.242580 0.179 Uiso 1 1 calc R . . . . C29 C -0.326(3) -1.1109(12) -0.2835(7) 0.156(7) Uani 1 1 d . . . . . H29 H -0.373042 -1.165113 -0.270422 0.187 Uiso 1 1 calc R . . . . C30 C -0.422(3) -1.0591(10) -0.3235(8) 0.136(6) Uani 1 1 d . . . . . C31 C -0.592(3) -1.0886(12) -0.3429(8) 0.154(7) Uani 1 1 d . . . . . H31 H -0.638045 -1.144152 -0.331299 0.185 Uiso 1 1 calc R . . . . C32 C -0.689(2) -1.0409(12) -0.3768(9) 0.164(8) Uani 1 1 d . . . . . H32 H -0.798153 -1.064045 -0.390381 0.197 Uiso 1 1 calc R . . . . C33 C -0.627(2) -0.9552(10) -0.3922(8) 0.158(7) Uani 1 1 d . . . . . H33 H -0.699201 -0.918278 -0.413581 0.190 Uiso 1 1 calc R . . . . C34 C -0.461(2) -0.9264(10) -0.3756(7) 0.133(5) Uani 1 1 d . . . . . H34 H -0.415680 -0.871680 -0.388668 0.160 Uiso 1 1 calc R . . . . C35 C -0.353(2) -0.9757(9) -0.3396(7) 0.125(5) Uani 1 1 d . . . . . C36 C -0.176(2) -0.9444(10) -0.3226(7) 0.118(5) Uani 1 1 d . . . . . C37 C -0.140(3) -0.7899(11) -0.2461(7) 0.172(8) Uani 1 1 d . . . . . H37A H -0.227528 -0.837713 -0.241138 0.258 Uiso 1 1 calc GR . . . . H37B H -0.202538 -0.733739 -0.253002 0.258 Uiso 1 1 calc GR . . . . H37C H -0.066874 -0.783561 -0.214713 0.258 Uiso 1 1 calc GR . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.113(8) 0.075(5) 0.208(10) -0.007(6) 0.016(7) -0.020(6) O2 0.114(9) 0.102(7) 0.240(12) 0.023(7) -0.034(8) -0.010(7) N1 0.139(14) 0.093(10) 0.26(2) 0.021(12) -0.001(14) -0.001(10) N2 0.110(11) 0.098(9) 0.212(16) -0.012(10) 0.009(11) -0.020(8) C1 0.090(10) 0.085(9) 0.165(13) -0.020(9) 0.000(10) 0.014(8) C2 0.089(10) 0.078(8) 0.190(14) -0.017(9) 0.013(10) -0.007(8) C3 0.083(9) 0.075(8) 0.187(15) -0.013(9) -0.007(10) 0.010(7) C4 0.127(13) 0.089(10) 0.172(14) -0.014(9) -0.022(11) 0.019(9) C5 0.094(10) 0.083(9) 0.192(15) -0.033(9) -0.002(10) 0.011(7) C6 0.085(10) 0.084(9) 0.175(14) 0.010(9) -0.006(10) -0.003(8) C7 0.076(9) 0.091(9) 0.148(12) -0.016(9) 0.001(9) -0.001(7) C8 0.068(8) 0.070(8) 0.194(15) -0.005(9) -0.007(9) 0.010(7) C9 0.084(10) 0.081(9) 0.196(16) -0.004(9) -0.015(10) -0.014(7) C10 0.099(11) 0.089(9) 0.169(15) -0.010(10) -0.005(11) -0.004(9) C11 0.062(8) 0.105(10) 0.143(12) -0.010(10) -0.002(8) 0.005(7) C12 0.079(9) 0.083(8) 0.172(13) -0.005(8) 0.005(9) -0.015(7) C13 0.090(10) 0.098(10) 0.148(13) -0.011(10) -0.006(10) 0.005(8) C14 0.091(11) 0.085(9) 0.186(15) -0.013(10) 0.004(11) 0.006(8) C15 0.143(17) 0.105(11) 0.181(16) 0.005(11) 0.011(14) 0.005(11) C16 0.20(2) 0.066(8) 0.225(18) 0.016(10) 0.009(17) 0.014(11) C17 0.092(11) 0.079(10) 0.28(3) 0.004(12) 0.003(15) -0.014(8) C18 0.104(12) 0.090(10) 0.220(17) -0.014(11) -0.012(11) 0.010(9) C19 0.066(8) 0.113(12) 0.155(14) -0.013(11) 0.001(10) -0.025(8) C20 0.073(9) 0.106(11) 0.191(17) -0.017(11) 0.006(10) -0.004(8) C21 0.071(9) 0.107(11) 0.194(17) -0.011(13) 0.005(12) 0.004(8) C22 0.098(12) 0.153(15) 0.150(14) -0.008(12) 0.005(10) -0.024(12) C23 0.075(9) 0.105(10) 0.184(16) -0.014(12) 0.006(12) -0.015(8) C24 0.071(9) 0.116(11) 0.153(13) 0.000(11) -0.005(10) 0.009(8) C25 0.120(13) 0.087(9) 0.168(15) 0.004(9) 0.000(13) 0.017(9) C26 0.110(13) 0.082(9) 0.232(18) 0.003(10) -0.020(12) -0.012(9) C27 0.090(12) 0.093(10) 0.222(19) 0.015(11) -0.005(13) -0.023(9) C28 0.122(15) 0.097(11) 0.23(2) 0.003(11) -0.006(14) 0.017(11) C29 0.17(2) 0.103(12) 0.192(18) 0.009(12) -0.008(15) -0.002(13) C30 0.104(13) 0.089(10) 0.217(18) -0.007(11) 0.020(12) -0.010(9) C31 0.094(14) 0.116(13) 0.25(2) -0.008(13) 0.005(14) -0.019(11) C32 0.066(9) 0.121(14) 0.31(2) -0.021(15) -0.014(13) -0.002(9) C33 0.059(8) 0.088(10) 0.33(2) 0.006(12) -0.003(11) -0.008(8) C34 0.093(12) 0.111(10) 0.195(15) 0.001(10) 0.018(11) 0.007(9) C35 0.100(11) 0.072(8) 0.202(16) 0.022(9) -0.002(11) -0.006(8) C36 0.087(10) 0.091(9) 0.177(15) 0.000(10) 0.003(10) -0.020(8) C37 0.20(2) 0.123(13) 0.189(17) -0.011(12) 0.018(17) -0.054(14) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C1 1.391(16) . ? O1 C13 1.379(16) . ? O2 C26 1.397(15) . ? O2 C27 1.333(19) . ? N1 C16 1.32(2) . ? N1 C17 1.32(2) . ? N2 C21 1.333(18) . ? N2 C22 1.346(18) . ? C1 C2 1.386(17) . ? C1 C6 1.360(18) . ? C2 H2 0.9300 . ? C2 C3 1.363(17) . ? C3 C4 1.421(19) . ? C3 C14 1.467(19) . ? C4 H4 0.9300 . ? C4 C5 1.376(17) . ? C5 H5 0.9300 . ? C5 C6 1.414(18) . ? C6 C7 1.482(17) . ? C7 C8 1.462(18) . ? C7 C24 1.356(17) . ? C8 C9 1.435(16) . ? C8 C13 1.400(18) . ? C9 H9 0.9300 . ? C9 C10 1.372(18) . ? C10 H10 0.9300 . ? C10 C11 1.339(18) . ? C11 C12 1.409(16) . ? C11 C19 1.443(19) . ? C12 H12 0.9300 . ? C12 C13 1.374(17) . ? C14 C15 1.340(19) . ? C14 C18 1.373(18) . ? C15 H15 0.9300 . ? C15 C16 1.370(18) . ? C16 H16 0.9300 . ? C17 H17 0.9300 . ? C17 C18 1.398(19) . ? C18 H18 0.9300 . ? C19 C20 1.406(18) . ? C19 C23 1.319(18) . ? C20 H20 0.9300 . ? C20 C21 1.31(2) . ? C21 H21 0.9300 . ? C22 H22 0.9300 . ? C22 C23 1.378(19) . ? C23 H23 0.9300 . ? C24 C25 1.433(19) . ? C24 C36 1.512(18) . ? C25 H25 0.9800 . ? C25 C26 1.537(19) . ? C25 C37 1.51(2) . ? C26 H26A 0.9700 . ? C26 H26B 0.9700 . ? C27 C28 1.41(2) . ? C27 C36 1.37(2) . ? C28 H28 0.9300 . ? C28 C29 1.39(2) . ? C29 H29 0.9300 . ? C29 C30 1.45(2) . ? C30 C31 1.40(2) . ? C30 C35 1.386(18) . ? C31 H31 0.9300 . ? C31 C32 1.32(2) . ? C32 H32 0.9300 . ? C32 C33 1.39(2) . ? C33 H33 0.9300 . ? C33 C34 1.35(2) . ? C34 H34 0.9300 . ? C34 C35 1.40(2) . ? C35 C36 1.44(2) . ? C37 H37A 0.9600 . ? C37 H37B 0.9600 . ? C37 H37C 0.9600 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C13 O1 C1 117.8(12) . . ? C27 O2 C26 115.4(13) . . ? C16 N1 C17 117.2(16) . . ? C21 N2 C22 111.6(16) . . ? C2 C1 O1 111.5(15) . . ? C6 C1 O1 124.3(13) . . ? C6 C1 C2 124.1(14) . . ? C1 C2 H2 119.7 . . ? C3 C2 C1 120.6(15) . . ? C3 C2 H2 119.7 . . ? C2 C3 C4 116.4(13) . . ? C2 C3 C14 121.9(16) . . ? C4 C3 C14 121.4(14) . . ? C3 C4 H4 118.9 . . ? C5 C4 C3 122.3(14) . . ? C5 C4 H4 118.9 . . ? C4 C5 H5 119.9 . . ? C4 C5 C6 120.1(15) . . ? C6 C5 H5 119.9 . . ? C1 C6 C5 115.9(13) . . ? C1 C6 C7 120.4(14) . . ? C5 C6 C7 123.1(15) . . ? C8 C7 C6 112.7(14) . . ? C24 C7 C6 118.2(14) . . ? C24 C7 C8 128.7(13) . . ? C9 C8 C7 124.0(16) . . ? C13 C8 C7 122.5(12) . . ? C13 C8 C9 112.7(15) . . ? C8 C9 H9 120.4 . . ? C10 C9 C8 119.2(16) . . ? C10 C9 H9 120.4 . . ? C9 C10 H10 116.1 . . ? C11 C10 C9 127.9(15) . . ? C11 C10 H10 116.1 . . ? C10 C11 C12 114.1(14) . . ? C10 C11 C19 126.0(15) . . ? C12 C11 C19 119.9(16) . . ? C11 C12 H12 119.8 . . ? C13 C12 C11 120.3(15) . . ? C13 C12 H12 119.8 . . ? O1 C13 C8 120.8(13) . . ? C12 C13 O1 113.6(15) . . ? C12 C13 C8 125.5(14) . . ? C15 C14 C3 122.9(16) . . ? C15 C14 C18 115.4(15) . . ? C18 C14 C3 121.6(17) . . ? C14 C15 H15 119.1 . . ? C14 C15 C16 121.8(18) . . ? C16 C15 H15 119.1 . . ? N1 C16 C15 122.8(19) . . ? N1 C16 H16 118.6 . . ? C15 C16 H16 118.6 . . ? N1 C17 H17 119.4 . . ? N1 C17 C18 121.3(19) . . ? C18 C17 H17 119.4 . . ? C14 C18 C17 121.1(17) . . ? C14 C18 H18 119.4 . . ? C17 C18 H18 119.4 . . ? C20 C19 C11 119.8(18) . . ? C23 C19 C11 127.9(17) . . ? C23 C19 C20 112.3(16) . . ? C19 C20 H20 119.5 . . ? C21 C20 C19 121.0(17) . . ? C21 C20 H20 119.5 . . ? N2 C21 H21 116.2 . . ? C20 C21 N2 127.7(17) . . ? C20 C21 H21 116.2 . . ? N2 C22 H22 118.6 . . ? N2 C22 C23 122.8(16) . . ? C23 C22 H22 118.6 . . ? C19 C23 C22 124.6(16) . . ? C19 C23 H23 117.7 . . ? C22 C23 H23 117.7 . . ? C7 C24 C25 128.2(15) . . ? C7 C24 C36 123.5(16) . . ? C25 C24 C36 108.1(15) . . ? C24 C25 H25 108.0 . . ? C24 C25 C26 104.2(12) . . ? C24 C25 C37 120.4(16) . . ? C26 C25 H25 108.0 . . ? C37 C25 H25 108.0 . . ? C37 C25 C26 107.6(15) . . ? O2 C26 C25 114.5(13) . . ? O2 C26 H26A 108.6 . . ? O2 C26 H26B 108.6 . . ? C25 C26 H26A 108.6 . . ? C25 C26 H26B 108.6 . . ? H26A C26 H26B 107.6 . . ? O2 C27 C28 112.7(19) . . ? O2 C27 C36 124.8(14) . . ? C36 C27 C28 121.8(17) . . ? C27 C28 H28 119.6 . . ? C29 C28 C27 120.8(18) . . ? C29 C28 H28 119.6 . . ? C28 C29 H29 121.2 . . ? C28 C29 C30 117.6(17) . . ? C30 C29 H29 121.2 . . ? C31 C30 C29 120.8(18) . . ? C35 C30 C29 119.5(17) . . ? C35 C30 C31 119.4(19) . . ? C30 C31 H31 118.6 . . ? C32 C31 C30 122.7(18) . . ? C32 C31 H31 118.6 . . ? C31 C32 H32 120.4 . . ? C31 C32 C33 119.2(17) . . ? C33 C32 H32 120.4 . . ? C32 C33 H33 120.4 . . ? C34 C33 C32 119.2(17) . . ? C34 C33 H33 120.4 . . ? C33 C34 H34 118.6 . . ? C33 C34 C35 122.9(16) . . ? C35 C34 H34 118.6 . . ? C30 C35 C34 116.3(16) . . ? C30 C35 C36 121.4(16) . . ? C34 C35 C36 122.2(14) . . ? C27 C36 C24 117.3(14) . . ? C27 C36 C35 116.8(14) . . ? C35 C36 C24 124.6(16) . . ? C25 C37 H37A 109.5 . . ? C25 C37 H37B 109.5 . . ? C25 C37 H37C 109.5 . . ? H37A C37 H37B 109.5 . . ? H37A C37 H37C 109.5 . . ? H37B C37 H37C 109.5 . . ? _shelx_res_file ; TITL mj19295_0m_a.res in P2(1)2(1)2(1) mj19295_0m.res created by SHELXL-2016/6 at 10:12:40 on 08-May-2019 REM Old TITL mj19295_0m in P2(1)2(1)2(1) REM SHELXT solution in P2(1)2(1)2(1) REM R1 0.342, Rweak 0.149, Alpha 0.051, Orientation as input REM Flack x = -0.131 ( 0.610 ) from Parsons' quotients REM Formula found by SHELXT: C35 N5 O CELL 1.34139 7.3038 14.6936 25.3197 90 90 90 ZERR 4 0.0074 0.0156 0.0284 0 0 0 LATT -1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H N O DISP C 0.0148 0.007 57.7477 DISP H -0 0 0.6481 DISP N 0.0253 0.0136 110.5121 DISP O 0.0412 0.025 193.9543 UNIT 148 104 8 8 L.S. 4 PLAN 20 SIZE 0.005 0.03 0.1 TEMP 22.85 BOND $H list 4 fmap 2 acta OMIT 1 7 0 OMIT 4 10 0 OMIT 1 0 5 OMIT 0 14 1 OMIT 0 10 2 OMIT 0 8 0 OMIT 4 7 0 OMIT 4 3 0 OMIT 0 2 2 OMIT -2 13 2 OMIT 3 6 0 OMIT 3 12 0 OMIT 3 14 0 OMIT 2 13 2 OMIT 0 1 16 OMIT 1 0 4 OMIT 0 6 0 OMIT 2 0 2 OMIT 5 8 0 OMIT -4 7 2 OMIT 1 7 2 OMIT -4 10 2 OMIT 3 7 0 OMIT -1 7 1 OMIT 2 13 1 OMIT 0 14 3 OMIT -4 9 2 OMIT 1 1 4 OMIT 0 10 0 OMIT 4 9 0 OMIT 4 9 2 OMIT -1 7 2 OMIT -1 2 5 OMIT 1 0 21 OMIT 1 2 5 OMIT 1 7 1 OMIT -1 1 4 OMIT 0 2 0 OMIT -4 1 4 OMIT -2 1 2 OMIT 0 3 2 OMIT 4 6 0 OMIT 2 1 2 OMIT 4 7 2 OMIT 0 1 20 OMIT 3 9 1 OMIT -2 11 1 OMIT 6 4 2 OMIT -3 10 1 OMIT 4 1 1 OMIT 3 10 1 OMIT 2 14 1 OMIT 5 1 1 OMIT -6 4 3 OMIT 3 0 3 OMIT -2 13 1 OMIT 4 10 2 OMIT 2 3 11 OMIT 5 6 0 OMIT 5 15 0 OMIT 0 2 1 OMIT 2 11 1 OMIT -2 14 1 OMIT -4 5 1 OMIT -4 13 1 OMIT 0 9 13 OMIT 4 11 0 OMIT 3 7 2 OMIT 4 0 4 OMIT 0 10 11 OMIT 5 2 0 OMIT -3 7 1 OMIT -2 3 11 OMIT -5 1 3 OMIT 2 6 0 OMIT 4 13 1 OMIT 0 1 4 OMIT -4 9 1 OMIT 0 4 2 OMIT 3 14 2 OMIT 0 14 2 OMIT 1 14 1 OMIT 8 7 0 OMIT 3 8 0 OMIT 4 9 1 OMIT 7 0 19 OMIT 0 3 11 OMIT 2 8 0 OMIT 1 3 12 OMIT 1 3 10 OMIT 5 1 3 OMIT -6 1 4 OMIT 5 8 6 OMIT -6 4 4 OMIT 2 1 4 OMIT -1 2 7 OMIT 0 3 16 OMIT -1 1 3 OMIT 0 2 4 OMIT -3 7 2 REM REM REM WGHT 0.050000 10.000000 EXTI 0.027028 FVAR 0.60118 O1 4 0.039289 -0.753032 -0.489803 11.00000 0.11321 0.07505 = 0.20814 -0.00674 0.01573 -0.01959 O2 4 0.057321 -0.965329 -0.257541 11.00000 0.11355 0.10226 = 0.23979 0.02338 -0.03390 -0.01005 N1 3 0.030034 -0.257331 -0.461549 11.00000 0.13917 0.09324 = 0.26132 0.02077 -0.00055 -0.00066 N2 3 0.045541 -1.145497 -0.673912 11.00000 0.10969 0.09815 = 0.21240 -0.01192 0.00870 -0.02035 C1 1 0.003451 -0.696749 -0.446874 11.00000 0.08988 0.08473 = 0.16515 -0.02039 -0.00035 0.01430 C2 1 0.030098 -0.605899 -0.459422 11.00000 0.08895 0.07757 = 0.18959 -0.01718 0.01298 -0.00703 AFIX 43 H2 2 0.075884 -0.590229 -0.492467 11.00000 -1.20000 AFIX 0 C3 1 -0.010149 -0.539306 -0.423802 11.00000 0.08320 0.07473 = 0.18698 -0.01312 -0.00703 0.00977 C4 1 -0.083412 -0.568359 -0.374639 11.00000 0.12653 0.08946 = 0.17188 -0.01359 -0.02194 0.01879 AFIX 43 H4 2 -0.115956 -0.524713 -0.349751 11.00000 -1.20000 AFIX 0 C5 1 -0.107887 -0.658873 -0.362572 11.00000 0.09400 0.08274 = 0.19222 -0.03337 -0.00227 0.01086 AFIX 43 H5 2 -0.160562 -0.675351 -0.330529 11.00000 -1.20000 AFIX 0 C6 1 -0.053111 -0.726854 -0.398791 11.00000 0.08477 0.08393 = 0.17452 0.00954 -0.00568 -0.00304 C7 1 -0.080808 -0.825373 -0.389213 11.00000 0.07600 0.09111 = 0.14764 -0.01622 0.00098 -0.00087 C8 1 -0.071674 -0.879288 -0.437672 11.00000 0.06848 0.06953 = 0.19387 -0.00523 -0.00719 0.00983 C9 1 -0.097441 -0.976080 -0.439536 11.00000 0.08356 0.08076 = 0.19579 -0.00420 -0.01483 -0.01393 AFIX 43 H9 2 -0.131529 -1.007884 -0.409340 11.00000 -1.20000 AFIX 0 C10 1 -0.071182 -1.021118 -0.486393 11.00000 0.09857 0.08943 = 0.16862 -0.00998 -0.00501 -0.00388 AFIX 43 H10 2 -0.090335 -1.083679 -0.485703 11.00000 -1.20000 AFIX 0 C11 1 -0.021306 -0.985892 -0.533006 11.00000 0.06192 0.10492 = 0.14305 -0.00970 -0.00165 0.00493 C12 1 0.012905 -0.891569 -0.531718 11.00000 0.07862 0.08287 = 0.17212 -0.00515 0.00543 -0.01544 AFIX 43 H12 2 0.048677 -0.861518 -0.562353 11.00000 -1.20000 AFIX 0 C13 1 -0.006330 -0.843753 -0.485407 11.00000 0.08996 0.09799 = 0.14839 -0.01134 -0.00572 0.00511 C14 1 0.004885 -0.442402 -0.437137 11.00000 0.09146 0.08458 = 0.18558 -0.01290 0.00351 0.00596 C15 1 -0.024513 -0.410103 -0.485910 11.00000 0.14316 0.10491 = 0.18116 0.00539 0.01056 0.00487 AFIX 43 H15 2 -0.048513 -0.450803 -0.513174 11.00000 -1.20000 AFIX 0 C16 1 -0.020170 -0.318776 -0.496693 11.00000 0.20202 0.06595 = 0.22526 0.01568 0.00936 0.01358 AFIX 43 H16 2 -0.054068 -0.299229 -0.530231 11.00000 -1.20000 AFIX 0 C17 1 0.059087 -0.285945 -0.412721 11.00000 0.09165 0.07886 = 0.28119 0.00389 0.00322 -0.01415 AFIX 43 H17 2 0.086145 -0.243780 -0.386464 11.00000 -1.20000 AFIX 0 C18 1 0.049893 -0.378355 -0.399838 11.00000 0.10402 0.08989 = 0.21990 -0.01387 -0.01158 0.00955 AFIX 43 H18 2 0.074675 -0.396757 -0.365429 11.00000 -1.20000 AFIX 0 C19 1 -0.000472 -1.035552 -0.581813 11.00000 0.06616 0.11273 = 0.15502 -0.01305 0.00147 -0.02515 C20 1 0.057996 -1.126672 -0.580770 11.00000 0.07327 0.10582 = 0.19060 -0.01657 0.00582 -0.00431 AFIX 43 H20 2 0.085018 -1.154029 -0.548579 11.00000 -1.20000 AFIX 0 C21 1 0.075041 -1.173783 -0.624622 11.00000 0.07142 0.10736 = 0.19383 -0.01085 0.00518 0.00395 AFIX 43 H21 2 0.112070 -1.233983 -0.620809 11.00000 -1.20000 AFIX 0 C22 1 -0.007312 -1.057743 -0.675236 11.00000 0.09815 0.15295 = 0.14986 -0.00789 0.00518 -0.02438 AFIX 43 H22 2 -0.029298 -1.030826 -0.707869 11.00000 -1.20000 AFIX 0 C23 1 -0.030197 -1.006139 -0.630288 11.00000 0.07458 0.10512 = 0.18398 -0.01447 0.00556 -0.01461 AFIX 43 H23 2 -0.069374 -0.946337 -0.634411 11.00000 -1.20000 AFIX 0 C24 1 -0.091723 -0.854594 -0.338518 11.00000 0.07126 0.11579 = 0.15306 -0.00037 -0.00486 0.00921 C25 1 -0.017545 -0.812707 -0.292089 11.00000 0.11976 0.08709 = 0.16837 0.00432 -0.00021 0.01650 AFIX 13 H25 2 0.045773 -0.756921 -0.302878 11.00000 -1.20000 AFIX 0 C26 1 0.127209 -0.880678 -0.272509 11.00000 0.11038 0.08151 = 0.23192 0.00312 -0.01985 -0.01239 AFIX 23 H26A 2 0.216675 -0.889840 -0.300318 11.00000 -1.20000 H26B 2 0.190542 -0.854180 -0.242551 11.00000 -1.20000 AFIX 0 C27 1 -0.097831 -0.989915 -0.281353 11.00000 0.09036 0.09266 = 0.22201 0.01513 -0.00527 -0.02253 C28 1 -0.159382 -1.076538 -0.265439 11.00000 0.12154 0.09741 = 0.22814 0.00316 -0.00596 0.01658 AFIX 43 H28 2 -0.088148 -1.111187 -0.242580 11.00000 -1.20000 AFIX 0 C29 1 -0.325611 -1.110893 -0.283532 11.00000 0.17226 0.10347 = 0.19204 0.00895 -0.00761 -0.00189 AFIX 43 H29 2 -0.373042 -1.165113 -0.270422 11.00000 -1.20000 AFIX 0 C30 1 -0.422080 -1.059114 -0.323533 11.00000 0.10368 0.08858 = 0.21686 -0.00709 0.02049 -0.01038 C31 1 -0.592149 -1.088606 -0.342909 11.00000 0.09423 0.11609 = 0.25139 -0.00790 0.00546 -0.01924 AFIX 43 H31 2 -0.638045 -1.144152 -0.331299 11.00000 -1.20000 AFIX 0 C32 1 -0.689357 -1.040875 -0.376839 11.00000 0.06557 0.12066 = 0.30646 -0.02131 -0.01377 -0.00230 AFIX 43 H32 2 -0.798153 -1.064045 -0.390381 11.00000 -1.20000 AFIX 0 C33 1 -0.627189 -0.955243 -0.392193 11.00000 0.05889 0.08765 = 0.32740 0.00625 -0.00316 -0.00809 AFIX 43 H33 2 -0.699201 -0.918278 -0.413581 11.00000 -1.20000 AFIX 0 C34 1 -0.460754 -0.926443 -0.375627 11.00000 0.09317 0.11080 = 0.19491 0.00132 0.01771 0.00674 AFIX 43 H34 2 -0.415680 -0.871680 -0.388668 11.00000 -1.20000 AFIX 0 C35 1 -0.353241 -0.975662 -0.339613 11.00000 0.09961 0.07216 = 0.20232 0.02152 -0.00171 -0.00599 C36 1 -0.176492 -0.944404 -0.322619 11.00000 0.08653 0.09092 = 0.17707 -0.00040 0.00325 -0.02038 C37 1 -0.139684 -0.789861 -0.246067 11.00000 0.20342 0.12305 = 0.18942 -0.01105 0.01826 -0.05373 AFIX 137 H37A 2 -0.227528 -0.837713 -0.241138 11.00000 -1.50000 H37B 2 -0.202538 -0.733739 -0.253002 11.00000 -1.50000 H37C 2 -0.066874 -0.783561 -0.214713 11.00000 -1.50000 AFIX 0 HKLF 4 REM mj19295_0m_a.res in P2(1)2(1)2(1) REM R1 = 0.1094 for 1691 Fo > 4sig(Fo) and 0.2512 for all 5079 data REM 372 parameters refined using 0 restraints END WGHT 0.1648 0.5212 REM Highest difference peak 0.181, deepest hole -0.181, 1-sigma level 0.044 Q1 1 -0.0692 -0.8778 -0.3887 11.00000 0.05 0.18 Q2 1 0.0474 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6.60 -2 -3 -10 43.40 5.60 -2 -3 -10 27.40 5.40 -2 3 10 27.30 6.70 2 3 -10 53.59 8.10 -2 -3 10 44.60 7.90 2 3 10 48.20 5.70 -2 -3 10 21.00 6.80 2 -3 -10 41.90 5.90 -2 -3 10 20.90 9.30 2 -3 -10 38.20 7.80 -2 3 -10 32.30 6.50 -2 -3 10 39.30 6.50 -2 3 -10 40.10 6.70 -3 -3 -10 114.59 11.60 -3 3 10 90.99 12.30 -3 3 10 77.09 12.00 -3 3 10 88.69 12.50 3 3 -10 92.09 13.00 -3 3 -10 83.19 11.70 -3 -3 10 107.19 13.50 3 3 10 105.09 11.40 -3 -3 10 86.49 15.30 -3 -3 10 99.29 12.20 3 -3 -10 105.29 12.10 4 3 -10 0.20 4.50 -4 3 10 -5.20 3.90 -4 -3 -10 1.80 2.60 -4 -3 10 -3.90 5.30 -4 -3 10 9.20 7.80 -4 3 -10 2.00 3.40 4 -3 -10 0.40 2.90 -5 -3 -10 5.90 3.20 5 3 -10 2.90 3.90 -5 3 10 4.00 4.40 -5 -3 10 21.00 8.80 -5 -3 10 6.80 6.50 -6 3 10 1.60 4.30 -6 -3 -10 -0.70 2.10 -6 -3 10 -1.80 5.90 -7 -3 -10 0.10 2.20 -7 3 10 9.60 4.90 -7 -3 10 -8.40 6.30 -8 3 10 -3.50 3.40 -8 -3 -10 -1.20 2.50 -8 -3 10 2.90 7.10 0 4 10 10.00 3.30 0 4 -10 4.60 4.70 0 4 -10 9.10 5.30 0 -4 -10 3.50 4.30 0 -4 10 9.40 3.30 0 -4 10 8.70 6.90 0 4 -10 7.70 4.30 0 4 10 14.70 3.70 0 -4 -10 6.80 3.00 0 4 -10 8.50 5.90 0 -4 -10 9.30 3.00 1 4 -10 542.45 57.59 -1 4 10 502.45 57.49 -1 4 10 551.34 57.39 -1 4 10 423.66 57.29 -1 -4 -10 552.84 57.59 -1 4 10 526.55 57.39 1 4 -10 582.44 58.09 1 4 -10 464.55 58.09 -1 -4 -10 519.05 57.49 -1 -4 -10 521.55 57.29 -1 -4 -10 559.14 57.39 1 4 10 436.56 57.29 -1 4 -10 465.95 57.79 -1 -4 10 519.15 57.99 -1 -4 10 528.25 57.29 1 4 10 546.25 57.29 1 -4 -10 509.85 57.59 1 -4 -10 485.45 57.39 -1 4 -10 484.35 57.89 1 -4 -10 549.74 57.29 1 -4 -10 563.94 57.89 -1 -4 10 535.65 57.29 -2 -4 -10 86.49 11.80 2 4 -10 94.49 13.80 2 4 -10 95.99 13.00 2 4 -10 114.29 13.50 -2 4 10 95.09 12.20 -2 4 10 84.09 12.40 -2 -4 -10 94.59 11.90 -2 -4 10 101.59 12.30 -2 -4 10 115.19 12.40 -2 4 -10 84.49 12.40 2 4 10 113.19 11.90 2 -4 -10 110.59 12.20 -2 -4 10 83.49 13.10 3 4 -10 140.59 17.30 -3 -4 -10 129.29 15.20 -3 4 10 100.79 15.50 -3 -4 -10 149.99 15.20 -3 4 10 131.09 15.90 -3 4 10 125.09 15.90 3 4 10 141.79 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0 5 29 0.90 3.10 0 -5 -29 -2.40 3.10 -1 -5 -29 1.70 3.60 -1 -5 -29 -4.60 3.30 -1 5 29 -2.40 3.20 1 5 -29 -3.00 3.90 1 -5 29 -3.60 3.20 -1 5 -29 3.60 2.50 1 -5 -29 6.20 3.30 1 5 29 -2.80 3.40 -1 5 -29 4.40 4.80 -1 -5 29 4.70 4.50 0 6 -29 5.80 3.90 0 -6 -29 4.90 3.10 0 6 -29 -4.20 4.30 0 -6 29 0.80 4.10 0 6 29 4.00 3.30 0 0 30 8.10 4.10 0 0 -30 -1.00 3.70 0 0 -30 -9.10 5.10 -1 0 -30 6.80 4.10 -1 0 -30 0.50 3.20 1 0 -30 11.90 4.20 1 0 30 2.70 3.40 -1 0 30 0.10 3.60 -2 0 -30 3.00 3.20 -2 0 30 -6.00 3.40 2 0 -30 2.90 3.40 0 -1 -30 -6.00 3.40 0 -1 30 -3.90 3.40 0 1 -30 3.80 4.60 0 1 -30 -2.80 3.50 0 1 30 -1.70 3.50 -1 1 30 -0.20 3.50 -1 -1 -30 5.70 3.20 -1 -1 -30 2.40 4.10 1 -1 30 -1.80 3.20 1 1 -30 3.40 4.00 1 -1 -30 1.10 3.40 -1 -1 30 -3.20 3.40 -1 1 -30 -0.10 3.10 -1 1 -30 0.70 4.50 1 1 30 1.50 3.30 2 1 -30 5.60 3.70 -2 -1 30 2.90 3.80 2 -1 -30 0.90 3.30 0 2 30 2.00 3.50 0 2 -30 -2.10 4.40 0 2 -30 8.10 3.80 0 -2 30 -0.80 3.40 0 -2 -30 1.20 3.70 1 -2 30 -0.30 3.30 -1 -2 -30 -2.40 3.70 1 2 -30 -2.00 3.70 -1 2 30 0.00 3.50 1 2 30 2.20 3.40 -1 -2 30 3.90 4.00 1 -2 -30 -3.10 3.30 -1 2 -30 -5.60 3.30 -1 2 -30 -3.70 4.40 0 -3 30 1.20 3.90 0 3 30 3.00 3.50 0 3 -30 11.10 5.40 0 3 -30 -7.80 3.30 1 3 -30 -4.50 3.60 -1 -3 -30 6.60 3.90 1 -3 30 2.10 3.30 -1 -3 -30 -3.20 3.10 -1 3 30 -3.20 2.90 1 -3 -30 4.80 3.70 -1 -3 30 3.40 4.10 -1 3 -30 -1.00 5.10 -1 3 -30 7.70 3.60 1 3 30 4.10 3.40 0 4 -30 -3.80 7.40 0 4 30 -2.30 2.80 0 -4 -30 -3.80 3.00 0 -4 30 3.40 3.90 0 4 -30 3.00 3.80 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 956 _olex2_submission_special_instructions 'No special instructions were received'