data_A20149_002 _audit_creation_method 'SHELXL-2018/3' _shelx_SHELXL_version_number '2018/3' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C30 H30 N Rh' _chemical_formula_weight 507.46 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Rh' 'Rh' -1.1178 0.9187 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 8.4358(3) _cell_length_b 11.8215(5) _cell_length_c 11.8878(5) _cell_angle_alpha 89.4274(14) _cell_angle_beta 84.7711(13) _cell_angle_gamma 88.9100(13) _cell_volume 1180.31(8) _cell_formula_units_Z 2 _cell_measurement_temperature 173(2) _cell_measurement_reflns_used 9655 _cell_measurement_theta_min 2.95 _cell_measurement_theta_max 27.52 _exptl_crystal_description 'plate' _exptl_crystal_colour 'yellow' _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.428 _exptl_crystal_F_000 524 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.314 _exptl_crystal_size_mid 0.212 _exptl_crystal_size_min 0.071 _exptl_absorpt_coefficient_mu 0.741 _shelx_estimated_absorpt_T_min 0.801 _shelx_estimated_absorpt_T_max 0.949 _exptl_absorpt_correction_type MULTI-SCAN _exptl_absorpt_correction_T_min 0.6560 _exptl_absorpt_correction_T_max 0.7456 _exptl_absorpt_process_details SADABS _exptl_absorpt_special_details ? _diffrn_ambient_temperature 173(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'fine-focus sealed tube' _diffrn_measurement_device_type 'CCD detector' _diffrn_measurement_method 'phi and omega scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 65125 _diffrn_reflns_av_unetI/netI 0.0130 _diffrn_reflns_av_R_equivalents 0.0293 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_theta_min 2.950 _diffrn_reflns_theta_max 27.538 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measured_fraction_theta_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_point_group_measured_fraction_full 0.997 _reflns_number_total 5417 _reflns_number_gt 5061 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Bruker APEX software' _computing_cell_refinement 'Bruker APEX software' _computing_data_reduction 'Bruker APEX software' _computing_structure_solution SHELXS _computing_structure_refinement SHELXL _computing_molecular_graphics ORTEP _computing_publication_material CIFTAB _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0068P)^2^+1.1892P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 5417 _refine_ls_number_parameters 295 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0271 _refine_ls_R_factor_gt 0.0229 _refine_ls_wR_factor_ref 0.0538 _refine_ls_wR_factor_gt 0.0494 _refine_ls_goodness_of_fit_ref 1.202 _refine_ls_restrained_S_all 1.202 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Rh1 Rh 0.38310(2) 0.81257(2) 0.73679(2) 0.01983(5) Uani 1 1 d . . . . . N2 N 0.54131(19) 0.71057(13) 0.63651(14) 0.0272(3) Uani 1 1 d . . . . . C3 C 0.6840(2) 0.66947(17) 0.6596(2) 0.0344(4) Uani 1 1 d . . . . . H3 H 0.719337 0.683325 0.731751 0.041 Uiso 1 1 calc R U . . . C4 C 0.7828(3) 0.60684(19) 0.5813(2) 0.0447(6) Uani 1 1 d . . . . . H4 H 0.884227 0.580451 0.599990 0.054 Uiso 1 1 calc R U . . . C5 C 0.7334(3) 0.58378(18) 0.4783(2) 0.0482(6) Uani 1 1 d . . . . . H5 H 0.799802 0.540878 0.425051 0.058 Uiso 1 1 calc R U . . . C6 C 0.5844(3) 0.62353(17) 0.45119(19) 0.0407(5) Uani 1 1 d . . . . . C7 C 0.5192(4) 0.6050(2) 0.3462(2) 0.0545(7) Uani 1 1 d . . . . . H7 H 0.579232 0.562335 0.289337 0.065 Uiso 1 1 calc R U . . . C8 C 0.3751(4) 0.6466(2) 0.3259(2) 0.0570(8) Uani 1 1 d . . . . . H8 H 0.335919 0.631968 0.255135 0.068 Uiso 1 1 calc R U . . . C9 C 0.2774(3) 0.71288(19) 0.40831(18) 0.0416(6) Uani 1 1 d . . . . . C10 C 0.1268(3) 0.7589(2) 0.3927(2) 0.0523(7) Uani 1 1 d . . . . . H10 H 0.079559 0.745232 0.324621 0.063 Uiso 1 1 calc R U . . . C11 C 0.0475(3) 0.8234(2) 0.4753(2) 0.0473(6) Uani 1 1 d . . . . . H11 H -0.054552 0.854269 0.463684 0.057 Uiso 1 1 calc R U . . . C12 C 0.1138(2) 0.84509(19) 0.57723(19) 0.0352(5) Uani 1 1 d . . . . . H12 H 0.056672 0.891511 0.632346 0.042 Uiso 1 1 calc R U . . . C13 C 0.2601(2) 0.80019(15) 0.59844(15) 0.0246(4) Uani 1 1 d . . . . . C14 C 0.3400(3) 0.73386(16) 0.51227(16) 0.0299(4) Uani 1 1 d . . . . . C15 C 0.4910(2) 0.68771(15) 0.53316(16) 0.0292(4) Uani 1 1 d . . . . . C16 C 0.2775(2) 0.95766(16) 0.82908(17) 0.0278(4) Uani 1 1 d . . . . . C17 C 0.3623(2) 0.89279(16) 0.90745(16) 0.0276(4) Uani 1 1 d . . . . . C18 C 0.5252(2) 0.88950(15) 0.86752(16) 0.0259(4) Uani 1 1 d . . . . . C19 C 0.5437(2) 0.95697(15) 0.76494(16) 0.0237(4) Uani 1 1 d . . . . . C20 C 0.3933(2) 1.00112(15) 0.74330(16) 0.0250(4) Uani 1 1 d . . . . . C21 C 0.1051(3) 0.9931(2) 0.8453(2) 0.0473(6) Uani 1 1 d . . . . . H21A H 0.091533 1.054140 0.900746 0.071 Uiso 1 1 calc R U . . . H21B H 0.041224 0.928395 0.872655 0.071 Uiso 1 1 calc R U . . . H21C H 0.070181 1.019925 0.773166 0.071 Uiso 1 1 calc R U . . . C22 C 0.2910(3) 0.8425(2) 1.01630(19) 0.0458(6) Uani 1 1 d . . . . . H22A H 0.297972 0.896623 1.077510 0.069 Uiso 1 1 calc R U . . . H22B H 0.349433 0.772796 1.032963 0.069 Uiso 1 1 calc R U . . . H22C H 0.179131 0.825272 1.009621 0.069 Uiso 1 1 calc R U . . . C23 C 0.6572(3) 0.83766(19) 0.9284(2) 0.0416(5) Uani 1 1 d . . . . . H23A H 0.684770 0.889171 0.987393 0.062 Uiso 1 1 calc R U . . . H23B H 0.750699 0.824315 0.874677 0.062 Uiso 1 1 calc R U . . . H23C H 0.622320 0.765627 0.962897 0.062 Uiso 1 1 calc R U . . . C24 C 0.6987(2) 0.97773(19) 0.69663(19) 0.0359(5) Uani 1 1 d . . . . . H24A H 0.759933 1.032336 0.735575 0.054 Uiso 1 1 calc R U . . . H24B H 0.678028 1.008019 0.622214 0.054 Uiso 1 1 calc R U . . . H24C H 0.759431 0.906433 0.687391 0.054 Uiso 1 1 calc R U . . . C25 C 0.3577(3) 1.08177(18) 0.6503(2) 0.0404(5) Uani 1 1 d . . . . . H25A H 0.339503 1.157944 0.681181 0.061 Uiso 1 1 calc R U . . . H25B H 0.262328 1.057543 0.616581 0.061 Uiso 1 1 calc R U . . . H25C H 0.448161 1.082507 0.592386 0.061 Uiso 1 1 calc R U . . . C26 C 0.2725(2) 0.66693(15) 0.79610(15) 0.0230(3) Uani 1 1 d . . . . . C27 C 0.1220(2) 0.63301(17) 0.77239(17) 0.0311(4) Uani 1 1 d . . . . . H27 H 0.061221 0.680626 0.727092 0.037 Uiso 1 1 calc R U . . . C28 C 0.0579(3) 0.53116(18) 0.81327(19) 0.0361(5) Uani 1 1 d . . . . . H28 H -0.044456 0.510640 0.793963 0.043 Uiso 1 1 calc R U . . . C29 C 0.1392(3) 0.45925(17) 0.88107(17) 0.0324(4) Uani 1 1 d . . . . . C30 C 0.2867(3) 0.49392(17) 0.90935(17) 0.0321(4) Uani 1 1 d . . . . . H30 H 0.344296 0.447972 0.958151 0.039 Uiso 1 1 calc R U . . . C31 C 0.3518(2) 0.59511(16) 0.86724(17) 0.0291(4) Uani 1 1 d . . . . . H31 H 0.453449 0.615897 0.887673 0.035 Uiso 1 1 calc R U . . . C32 C 0.0710(3) 0.34654(19) 0.9197(2) 0.0460(6) Uani 1 1 d . . . . . H32A H 0.084490 0.335055 1.000059 0.069 Uiso 1 1 calc R U . . . H32B H 0.126766 0.285728 0.875842 0.069 Uiso 1 1 calc R U . . . H32C H -0.042607 0.345805 0.908290 0.069 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Rh1 0.01810(7) 0.01892(7) 0.02241(7) -0.00080(5) -0.00090(5) -0.00320(5) N2 0.0279(8) 0.0213(7) 0.0313(8) -0.0011(6) 0.0045(6) -0.0044(6) C3 0.0284(10) 0.0271(10) 0.0462(12) -0.0014(9) 0.0045(9) 0.0003(8) C4 0.0354(12) 0.0291(11) 0.0661(16) -0.0046(11) 0.0142(11) 0.0025(9) C5 0.0534(15) 0.0254(10) 0.0600(16) -0.0080(10) 0.0277(12) -0.0040(10) C6 0.0599(15) 0.0231(10) 0.0356(11) -0.0067(8) 0.0176(10) -0.0156(9) C7 0.087(2) 0.0392(13) 0.0340(12) -0.0126(10) 0.0168(13) -0.0240(14) C8 0.100(2) 0.0474(14) 0.0241(11) -0.0050(10) -0.0022(13) -0.0403(16) C9 0.0644(15) 0.0357(11) 0.0266(10) 0.0047(9) -0.0088(10) -0.0282(11) C10 0.0714(18) 0.0545(15) 0.0359(12) 0.0141(11) -0.0270(12) -0.0357(14) C11 0.0424(13) 0.0532(14) 0.0503(14) 0.0235(12) -0.0246(11) -0.0212(11) C12 0.0312(10) 0.0373(11) 0.0385(11) 0.0102(9) -0.0099(9) -0.0097(9) C13 0.0276(9) 0.0224(8) 0.0246(9) 0.0051(7) -0.0050(7) -0.0102(7) C14 0.0419(11) 0.0250(9) 0.0231(9) 0.0026(7) -0.0020(8) -0.0161(8) C15 0.0408(11) 0.0185(8) 0.0268(9) -0.0017(7) 0.0073(8) -0.0111(8) C16 0.0232(9) 0.0254(9) 0.0342(10) -0.0103(8) 0.0015(7) -0.0023(7) C17 0.0357(10) 0.0222(9) 0.0244(9) -0.0059(7) 0.0025(8) -0.0094(7) C18 0.0298(9) 0.0218(9) 0.0273(9) -0.0038(7) -0.0080(7) -0.0045(7) C19 0.0219(8) 0.0213(8) 0.0281(9) -0.0029(7) -0.0021(7) -0.0063(7) C20 0.0258(9) 0.0178(8) 0.0317(10) -0.0014(7) -0.0045(7) -0.0037(7) C21 0.0256(11) 0.0504(14) 0.0648(16) -0.0201(12) 0.0045(10) 0.0011(10) C22 0.0677(16) 0.0379(12) 0.0299(11) -0.0070(9) 0.0115(11) -0.0194(11) C23 0.0473(13) 0.0331(11) 0.0482(13) -0.0001(10) -0.0244(11) -0.0015(9) C24 0.0264(10) 0.0389(11) 0.0415(12) -0.0026(9) 0.0038(8) -0.0118(8) C25 0.0457(13) 0.0283(10) 0.0493(13) 0.0093(9) -0.0150(10) -0.0036(9) C26 0.0267(9) 0.0209(8) 0.0209(8) -0.0023(7) 0.0012(7) -0.0036(7) C27 0.0306(10) 0.0302(10) 0.0329(10) 0.0083(8) -0.0045(8) -0.0075(8) C28 0.0315(10) 0.0379(11) 0.0397(12) 0.0071(9) -0.0051(9) -0.0147(9) C29 0.0416(11) 0.0254(10) 0.0292(10) 0.0018(8) 0.0032(8) -0.0085(8) C30 0.0419(11) 0.0249(9) 0.0296(10) 0.0035(8) -0.0039(8) -0.0009(8) C31 0.0312(10) 0.0260(9) 0.0305(10) -0.0011(8) -0.0042(8) -0.0040(8) C32 0.0568(15) 0.0313(11) 0.0503(14) 0.0104(10) -0.0042(11) -0.0167(10) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Rh1 C13 2.0308(18) . ? Rh1 C26 2.0612(18) . ? Rh1 N2 2.0818(16) . ? Rh1 C16 2.1772(18) . ? Rh1 C20 2.2347(17) . ? Rh1 C17 2.2390(18) . ? Rh1 C19 2.2459(17) . ? Rh1 C18 2.2559(18) . ? N2 C3 1.340(3) . ? N2 C15 1.367(3) . ? C3 C4 1.400(3) . ? C3 H3 0.9500 . ? C4 C5 1.361(4) . ? C4 H4 0.9500 . ? C5 C6 1.397(4) . ? C5 H5 0.9500 . ? C6 C15 1.414(3) . ? C6 C7 1.430(4) . ? C7 C8 1.344(4) . ? C7 H7 0.9500 . ? C8 C9 1.448(4) . ? C8 H8 0.9500 . ? C9 C10 1.400(4) . ? C9 C14 1.413(3) . ? C10 C11 1.367(4) . ? C10 H10 0.9500 . ? C11 C12 1.408(3) . ? C11 H11 0.9500 . ? C12 C13 1.377(3) . ? C12 H12 0.9500 . ? C13 C14 1.410(3) . ? C14 C15 1.418(3) . ? C16 C17 1.433(3) . ? C16 C20 1.444(3) . ? C16 C21 1.502(3) . ? C17 C18 1.413(3) . ? C17 C22 1.498(3) . ? C18 C19 1.448(3) . ? C18 C23 1.500(3) . ? C19 C20 1.407(3) . ? C19 C24 1.498(3) . ? C20 C25 1.500(3) . ? C21 H21A 0.9800 . ? C21 H21B 0.9800 . ? C21 H21C 0.9800 . ? C22 H22A 0.9800 . ? C22 H22B 0.9800 . ? C22 H22C 0.9800 . ? C23 H23A 0.9800 . ? C23 H23B 0.9800 . ? C23 H23C 0.9800 . ? C24 H24A 0.9800 . ? C24 H24B 0.9800 . ? C24 H24C 0.9800 . ? C25 H25A 0.9800 . ? C25 H25B 0.9800 . ? C25 H25C 0.9800 . ? C26 C27 1.393(3) . ? C26 C31 1.396(3) . ? C27 C28 1.394(3) . ? C27 H27 0.9500 . ? C28 C29 1.381(3) . ? C28 H28 0.9500 . ? C29 C30 1.389(3) . ? C29 C32 1.512(3) . ? C30 C31 1.395(3) . ? C30 H30 0.9500 . ? C31 H31 0.9500 . ? C32 H32A 0.9800 . ? C32 H32B 0.9800 . ? C32 H32C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C13 Rh1 C26 87.30(7) . . ? C13 Rh1 N2 80.37(7) . . ? C26 Rh1 N2 87.77(6) . . ? C13 Rh1 C16 105.25(8) . . ? C26 Rh1 C16 109.63(7) . . ? N2 Rh1 C16 161.74(7) . . ? C13 Rh1 C20 98.16(7) . . ? C26 Rh1 C20 147.68(7) . . ? N2 Rh1 C20 124.55(6) . . ? C16 Rh1 C20 38.17(7) . . ? C13 Rh1 C17 140.24(8) . . ? C26 Rh1 C17 93.25(7) . . ? N2 Rh1 C17 139.39(7) . . ? C16 Rh1 C17 37.83(7) . . ? C20 Rh1 C17 62.50(7) . . ? C13 Rh1 C19 123.34(7) . . ? C26 Rh1 C19 149.21(7) . . ? N2 Rh1 C19 99.45(6) . . ? C16 Rh1 C19 62.78(7) . . ? C20 Rh1 C19 36.62(7) . . ? C17 Rh1 C19 62.00(7) . . ? C13 Rh1 C18 159.75(7) . . ? C26 Rh1 C18 111.70(7) . . ? N2 Rh1 C18 106.38(7) . . ? C16 Rh1 C18 62.72(7) . . ? C20 Rh1 C18 62.10(7) . . ? C17 Rh1 C18 36.64(7) . . ? C19 Rh1 C18 37.54(7) . . ? C3 N2 C15 117.99(17) . . ? C3 N2 Rh1 128.33(14) . . ? C15 N2 Rh1 113.64(13) . . ? N2 C3 C4 122.4(2) . . ? N2 C3 H3 118.8 . . ? C4 C3 H3 118.8 . . ? C5 C4 C3 119.9(2) . . ? C5 C4 H4 120.0 . . ? C3 C4 H4 120.0 . . ? C4 C5 C6 119.6(2) . . ? C4 C5 H5 120.2 . . ? C6 C5 H5 120.2 . . ? C5 C6 C15 117.8(2) . . ? C5 C6 C7 125.0(2) . . ? C15 C6 C7 117.2(2) . . ? C8 C7 C6 121.6(2) . . ? C8 C7 H7 119.2 . . ? C6 C7 H7 119.2 . . ? C7 C8 C9 122.2(2) . . ? C7 C8 H8 118.9 . . ? C9 C8 H8 118.9 . . ? C10 C9 C14 117.5(2) . . ? C10 C9 C8 125.2(2) . . ? C14 C9 C8 117.4(2) . . ? C11 C10 C9 120.0(2) . . ? C11 C10 H10 120.0 . . ? C9 C10 H10 120.0 . . ? C10 C11 C12 121.5(2) . . ? C10 C11 H11 119.3 . . ? C12 C11 H11 119.3 . . ? C13 C12 C11 121.2(2) . . ? C13 C12 H12 119.4 . . ? C11 C12 H12 119.4 . . ? C12 C13 C14 116.54(18) . . ? C12 C13 Rh1 130.34(16) . . ? C14 C13 Rh1 113.12(14) . . ? C13 C14 C9 123.3(2) . . ? C13 C14 C15 116.94(17) . . ? C9 C14 C15 119.7(2) . . ? N2 C15 C6 122.2(2) . . ? N2 C15 C14 115.91(17) . . ? C6 C15 C14 121.8(2) . . ? C17 C16 C20 107.57(16) . . ? C17 C16 C21 125.9(2) . . ? C20 C16 C21 125.5(2) . . ? C17 C16 Rh1 73.42(11) . . ? C20 C16 Rh1 73.07(10) . . ? C21 C16 Rh1 128.12(14) . . ? C18 C17 C16 108.38(16) . . ? C18 C17 C22 125.9(2) . . ? C16 C17 C22 125.6(2) . . ? C18 C17 Rh1 72.33(10) . . ? C16 C17 Rh1 68.74(10) . . ? C22 C17 Rh1 127.17(13) . . ? C17 C18 C19 107.65(16) . . ? C17 C18 C23 125.77(19) . . ? C19 C18 C23 126.18(18) . . ? C17 C18 Rh1 71.03(10) . . ? C19 C18 Rh1 70.86(10) . . ? C23 C18 Rh1 129.25(14) . . ? C20 C19 C18 108.39(16) . . ? C20 C19 C24 126.58(18) . . ? C18 C19 C24 125.00(18) . . ? C20 C19 Rh1 71.26(10) . . ? C18 C19 Rh1 71.61(10) . . ? C24 C19 Rh1 124.26(13) . . ? C19 C20 C16 107.85(16) . . ? C19 C20 C25 126.76(18) . . ? C16 C20 C25 125.37(18) . . ? C19 C20 Rh1 72.12(10) . . ? C16 C20 Rh1 68.75(10) . . ? C25 C20 Rh1 125.96(14) . . ? C16 C21 H21A 109.5 . . ? C16 C21 H21B 109.5 . . ? H21A C21 H21B 109.5 . . ? C16 C21 H21C 109.5 . . ? H21A C21 H21C 109.5 . . ? H21B C21 H21C 109.5 . . ? C17 C22 H22A 109.5 . . ? C17 C22 H22B 109.5 . . ? H22A C22 H22B 109.5 . . ? C17 C22 H22C 109.5 . . ? H22A C22 H22C 109.5 . . ? H22B C22 H22C 109.5 . . ? C18 C23 H23A 109.5 . . ? C18 C23 H23B 109.5 . . ? H23A C23 H23B 109.5 . . ? C18 C23 H23C 109.5 . . ? H23A C23 H23C 109.5 . . ? H23B C23 H23C 109.5 . . ? C19 C24 H24A 109.5 . . ? C19 C24 H24B 109.5 . . ? H24A C24 H24B 109.5 . . ? C19 C24 H24C 109.5 . . ? H24A C24 H24C 109.5 . . ? H24B C24 H24C 109.5 . . ? C20 C25 H25A 109.5 . . ? C20 C25 H25B 109.5 . . ? H25A C25 H25B 109.5 . . ? C20 C25 H25C 109.5 . . ? H25A C25 H25C 109.5 . . ? H25B C25 H25C 109.5 . . ? C27 C26 C31 115.84(17) . . ? C27 C26 Rh1 125.55(14) . . ? C31 C26 Rh1 118.61(14) . . ? C26 C27 C28 121.83(19) . . ? C26 C27 H27 119.1 . . ? C28 C27 H27 119.1 . . ? C29 C28 C27 121.81(19) . . ? C29 C28 H28 119.1 . . ? C27 C28 H28 119.1 . . ? C28 C29 C30 117.11(18) . . ? C28 C29 C32 120.9(2) . . ? C30 C29 C32 122.0(2) . . ? C29 C30 C31 121.06(19) . . ? C29 C30 H30 119.5 . . ? C31 C30 H30 119.5 . . ? C30 C31 C26 122.26(18) . . ? C30 C31 H31 118.9 . . ? C26 C31 H31 118.9 . . ? C29 C32 H32A 109.5 . . ? C29 C32 H32B 109.5 . . ? H32A C32 H32B 109.5 . . ? C29 C32 H32C 109.5 . . ? H32A C32 H32C 109.5 . . ? H32B C32 H32C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C15 N2 C3 C4 1.4(3) . . . . ? Rh1 N2 C3 C4 -176.19(15) . . . . ? N2 C3 C4 C5 -1.4(3) . . . . ? C3 C4 C5 C6 0.4(3) . . . . ? C4 C5 C6 C15 0.5(3) . . . . ? C4 C5 C6 C7 180.0(2) . . . . ? C5 C6 C7 C8 -179.6(2) . . . . ? C15 C6 C7 C8 -0.1(3) . . . . ? C6 C7 C8 C9 0.3(4) . . . . ? C7 C8 C9 C10 179.8(2) . . . . ? C7 C8 C9 C14 0.6(3) . . . . ? C14 C9 C10 C11 1.4(3) . . . . ? C8 C9 C10 C11 -177.8(2) . . . . ? C9 C10 C11 C12 -0.1(3) . . . . ? C10 C11 C12 C13 -1.3(3) . . . . ? C11 C12 C13 C14 1.2(3) . . . . ? C11 C12 C13 Rh1 -178.30(15) . . . . ? C12 C13 C14 C9 0.2(3) . . . . ? Rh1 C13 C14 C9 179.77(15) . . . . ? C12 C13 C14 C15 179.73(17) . . . . ? Rh1 C13 C14 C15 -0.7(2) . . . . ? C10 C9 C14 C13 -1.5(3) . . . . ? C8 C9 C14 C13 177.82(18) . . . . ? C10 C9 C14 C15 178.98(18) . . . . ? C8 C9 C14 C15 -1.7(3) . . . . ? C3 N2 C15 C6 -0.4(3) . . . . ? Rh1 N2 C15 C6 177.51(14) . . . . ? C3 N2 C15 C14 -179.45(17) . . . . ? Rh1 N2 C15 C14 -1.5(2) . . . . ? C5 C6 C15 N2 -0.5(3) . . . . ? C7 C6 C15 N2 179.95(18) . . . . ? C5 C6 C15 C14 178.46(18) . . . . ? C7 C6 C15 C14 -1.1(3) . . . . ? C13 C14 C15 N2 1.5(2) . . . . ? C9 C14 C15 N2 -178.95(17) . . . . ? C13 C14 C15 C6 -177.55(17) . . . . ? C9 C14 C15 C6 2.0(3) . . . . ? C20 C16 C17 C18 -3.8(2) . . . . ? C21 C16 C17 C18 -172.77(19) . . . . ? Rh1 C16 C17 C18 61.80(13) . . . . ? C20 C16 C17 C22 173.14(18) . . . . ? C21 C16 C17 C22 4.2(3) . . . . ? Rh1 C16 C17 C22 -121.25(19) . . . . ? C20 C16 C17 Rh1 -65.61(12) . . . . ? C21 C16 C17 Rh1 125.4(2) . . . . ? C16 C17 C18 C19 2.2(2) . . . . ? C22 C17 C18 C19 -174.72(18) . . . . ? Rh1 C17 C18 C19 61.76(12) . . . . ? C16 C17 C18 C23 175.22(18) . . . . ? C22 C17 C18 C23 -1.7(3) . . . . ? Rh1 C17 C18 C23 -125.23(19) . . . . ? C16 C17 C18 Rh1 -59.54(12) . . . . ? C22 C17 C18 Rh1 123.52(19) . . . . ? C17 C18 C19 C20 0.3(2) . . . . ? C23 C18 C19 C20 -172.71(18) . . . . ? Rh1 C18 C19 C20 62.14(12) . . . . ? C17 C18 C19 C24 178.69(17) . . . . ? C23 C18 C19 C24 5.7(3) . . . . ? Rh1 C18 C19 C24 -119.44(18) . . . . ? C17 C18 C19 Rh1 -61.87(12) . . . . ? C23 C18 C19 Rh1 125.15(19) . . . . ? C18 C19 C20 C16 -2.6(2) . . . . ? C24 C19 C20 C16 178.99(18) . . . . ? Rh1 C19 C20 C16 59.74(12) . . . . ? C18 C19 C20 C25 175.69(18) . . . . ? C24 C19 C20 C25 -2.7(3) . . . . ? Rh1 C19 C20 C25 -121.9(2) . . . . ? C18 C19 C20 Rh1 -62.36(12) . . . . ? C24 C19 C20 Rh1 119.25(19) . . . . ? C17 C16 C20 C19 4.0(2) . . . . ? C21 C16 C20 C19 172.98(19) . . . . ? Rh1 C16 C20 C19 -61.89(13) . . . . ? C17 C16 C20 C25 -174.38(18) . . . . ? C21 C16 C20 C25 -5.4(3) . . . . ? Rh1 C16 C20 C25 119.77(19) . . . . ? C17 C16 C20 Rh1 65.85(12) . . . . ? C21 C16 C20 Rh1 -125.1(2) . . . . ? C31 C26 C27 C28 -2.7(3) . . . . ? Rh1 C26 C27 C28 177.96(16) . . . . ? C26 C27 C28 C29 1.1(3) . . . . ? C27 C28 C29 C30 1.5(3) . . . . ? C27 C28 C29 C32 -177.0(2) . . . . ? C28 C29 C30 C31 -2.3(3) . . . . ? C32 C29 C30 C31 176.1(2) . . . . ? C29 C30 C31 C26 0.6(3) . . . . ? C27 C26 C31 C30 1.9(3) . . . . ? Rh1 C26 C31 C30 -178.76(15) . . . . ? _refine_diff_density_max 1.022 _refine_diff_density_min -0.643 _refine_diff_density_rms 0.064 _shelx_res_file ; TITL A20149_002 in P-1 A20149_002.res created by SHELXL-2018/3 at 14:40:16 on 01-Jul-2020 CELL 0.71073 8.43580 11.82150 11.88780 89.4274 84.7711 88.9100 ZERR 2.00 0.00030 0.00050 0.00050 0.0014 0.0013 0.0013 LATT 1 SFAC C H N RH UNIT 60 60 2 2 ACTA OMIT -1 1 0 OMIT 1 0 1 TEMP -100.3 SIZE 0.071 0.212 0.314 CONF MERG 2 L.S. 12 BOND $H FMAP 2 PLAN 20 LIST 4 WGHT 0.006800 1.189200 FVAR 0.21982 RH1 4 0.383096 0.812570 0.736792 11.00000 0.01810 0.01892 = 0.02241 -0.00080 -0.00090 -0.00320 N2 3 0.541308 0.710575 0.636510 11.00000 0.02792 0.02134 = 0.03126 -0.00115 0.00448 -0.00439 C3 1 0.683977 0.669466 0.659614 11.00000 0.02844 0.02705 = 0.04620 -0.00139 0.00446 0.00034 AFIX 43 H3 2 0.719337 0.683325 0.731751 11.00000 -1.20000 AFIX 0 C4 1 0.782771 0.606836 0.581269 11.00000 0.03535 0.02913 = 0.06606 -0.00460 0.01422 0.00249 AFIX 43 H4 2 0.884227 0.580451 0.599990 11.00000 -1.20000 AFIX 0 C5 1 0.733362 0.583778 0.478267 11.00000 0.05338 0.02536 = 0.06000 -0.00804 0.02771 -0.00400 AFIX 43 H5 2 0.799802 0.540878 0.425051 11.00000 -1.20000 AFIX 0 C6 1 0.584388 0.623533 0.451187 11.00000 0.05990 0.02314 = 0.03562 -0.00669 0.01756 -0.01559 C7 1 0.519203 0.605035 0.346174 11.00000 0.08724 0.03923 = 0.03401 -0.01263 0.01678 -0.02397 AFIX 43 H7 2 0.579232 0.562335 0.289337 11.00000 -1.20000 AFIX 0 C8 1 0.375057 0.646589 0.325911 11.00000 0.10026 0.04740 = 0.02414 -0.00500 -0.00218 -0.04029 AFIX 43 H8 2 0.335919 0.631968 0.255135 11.00000 -1.20000 AFIX 0 C9 1 0.277426 0.712880 0.408310 11.00000 0.06440 0.03570 = 0.02663 0.00474 -0.00876 -0.02821 C10 1 0.126751 0.758865 0.392664 11.00000 0.07144 0.05454 = 0.03594 0.01412 -0.02705 -0.03567 AFIX 43 H10 2 0.079559 0.745232 0.324621 11.00000 -1.20000 AFIX 0 C11 1 0.047522 0.823389 0.475305 11.00000 0.04243 0.05319 = 0.05032 0.02351 -0.02458 -0.02118 AFIX 43 H11 2 -0.054552 0.854269 0.463684 11.00000 -1.20000 AFIX 0 C12 1 0.113826 0.845087 0.577228 11.00000 0.03117 0.03727 = 0.03846 0.01020 -0.00994 -0.00971 AFIX 43 H12 2 0.056672 0.891511 0.632346 11.00000 -1.20000 AFIX 0 C13 1 0.260118 0.800186 0.598440 11.00000 0.02763 0.02239 = 0.02459 0.00512 -0.00503 -0.01017 C14 1 0.339998 0.733855 0.512271 11.00000 0.04191 0.02499 = 0.02312 0.00261 -0.00204 -0.01610 C15 1 0.490967 0.687714 0.533163 11.00000 0.04079 0.01854 = 0.02681 -0.00174 0.00728 -0.01105 C16 1 0.277527 0.957661 0.829078 11.00000 0.02321 0.02543 = 0.03418 -0.01033 0.00146 -0.00230 C17 1 0.362253 0.892787 0.907455 11.00000 0.03573 0.02224 = 0.02444 -0.00586 0.00250 -0.00942 C18 1 0.525222 0.889504 0.867520 11.00000 0.02977 0.02185 = 0.02729 -0.00378 -0.00798 -0.00445 C19 1 0.543720 0.956967 0.764944 11.00000 0.02186 0.02129 = 0.02808 -0.00285 -0.00210 -0.00629 C20 1 0.393277 1.001124 0.743299 11.00000 0.02582 0.01778 = 0.03175 -0.00136 -0.00448 -0.00368 C21 1 0.105147 0.993108 0.845322 11.00000 0.02561 0.05036 = 0.06475 -0.02010 0.00455 0.00107 AFIX 137 H21A 2 0.091533 1.054140 0.900746 11.00000 -1.50000 H21B 2 0.041224 0.928395 0.872655 11.00000 -1.50000 H21C 2 0.070181 1.019925 0.773166 11.00000 -1.50000 AFIX 0 C22 1 0.291039 0.842523 1.016300 11.00000 0.06772 0.03786 = 0.02987 -0.00696 0.01149 -0.01939 AFIX 137 H22A 2 0.297972 0.896623 1.077510 11.00000 -1.50000 H22B 2 0.349433 0.772796 1.032963 11.00000 -1.50000 H22C 2 0.179131 0.825272 1.009621 11.00000 -1.50000 AFIX 0 C23 1 0.657195 0.837659 0.928400 11.00000 0.04734 0.03310 = 0.04817 -0.00012 -0.02438 -0.00152 AFIX 137 H23A 2 0.684770 0.889171 0.987393 11.00000 -1.50000 H23B 2 0.750699 0.824315 0.874677 11.00000 -1.50000 H23C 2 0.622320 0.765627 0.962897 11.00000 -1.50000 AFIX 0 C24 1 0.698668 0.977733 0.696627 11.00000 0.02644 0.03889 = 0.04153 -0.00259 0.00379 -0.01177 AFIX 137 H24A 2 0.759933 1.032336 0.735575 11.00000 -1.50000 H24B 2 0.678028 1.008019 0.622214 11.00000 -1.50000 H24C 2 0.759431 0.906433 0.687391 11.00000 -1.50000 AFIX 0 C25 1 0.357738 1.081767 0.650305 11.00000 0.04565 0.02830 = 0.04927 0.00935 -0.01503 -0.00362 AFIX 137 H25A 2 0.339503 1.157944 0.681181 11.00000 -1.50000 H25B 2 0.262328 1.057543 0.616581 11.00000 -1.50000 H25C 2 0.448161 1.082507 0.592386 11.00000 -1.50000 AFIX 0 C26 1 0.272518 0.666927 0.796099 11.00000 0.02672 0.02087 = 0.02087 -0.00228 0.00117 -0.00360 C27 1 0.121954 0.633013 0.772387 11.00000 0.03058 0.03018 = 0.03292 0.00830 -0.00451 -0.00747 AFIX 43 H27 2 0.061221 0.680626 0.727092 11.00000 -1.20000 AFIX 0 C28 1 0.057915 0.531157 0.813271 11.00000 0.03153 0.03785 = 0.03966 0.00707 -0.00512 -0.01471 AFIX 43 H28 2 -0.044456 0.510640 0.793963 11.00000 -1.20000 AFIX 0 C29 1 0.139201 0.459248 0.881074 11.00000 0.04159 0.02540 = 0.02920 0.00178 0.00318 -0.00847 C30 1 0.286726 0.493918 0.909346 11.00000 0.04189 0.02494 = 0.02955 0.00353 -0.00394 -0.00088 AFIX 43 H30 2 0.344296 0.447972 0.958151 11.00000 -1.20000 AFIX 0 C31 1 0.351753 0.595114 0.867244 11.00000 0.03119 0.02598 = 0.03051 -0.00115 -0.00417 -0.00403 AFIX 43 H31 2 0.453449 0.615897 0.887673 11.00000 -1.20000 AFIX 0 C32 1 0.070959 0.346545 0.919716 11.00000 0.05681 0.03127 = 0.05028 0.01039 -0.00424 -0.01666 AFIX 137 H32A 2 0.084490 0.335055 1.000059 11.00000 -1.50000 H32B 2 0.126766 0.285728 0.875842 11.00000 -1.50000 H32C 2 -0.042607 0.345805 0.908290 11.00000 -1.50000 REM ##### REM ##### AFIX 0 HKLF 4 REM A20149_002 in P-1 REM wR2 = 0.0538, GooF = S = 1.202, Restrained GooF = 1.202 for all data REM R1 = 0.0229 for 5061 Fo > 4sig(Fo) and 0.0271 for all 5417 data REM 295 parameters refined using 0 restraints END WGHT 0.0068 1.1892 REM Highest difference peak 1.022, deepest hole -0.643, 1-sigma level 0.064 Q1 1 -0.1453 0.5620 0.7879 11.00000 0.05 1.02 Q2 1 0.5413 0.9185 0.8153 11.00000 0.05 0.36 Q3 1 0.3057 0.7165 0.7754 11.00000 0.05 0.33 Q4 1 0.4731 0.9971 0.7635 11.00000 0.05 0.31 Q5 1 0.3369 0.9868 0.7930 11.00000 0.05 0.31 Q6 1 0.5254 0.6441 0.4978 11.00000 0.05 0.31 Q7 1 0.5119 0.6200 0.4176 11.00000 0.05 0.30 Q8 1 0.3865 1.0581 0.7149 11.00000 0.05 0.29 Q9 1 0.7209 0.5914 0.5359 11.00000 0.05 0.29 Q10 1 0.2980 0.8019 0.6410 11.00000 0.05 0.28 Q11 1 0.4939 0.9573 0.6804 11.00000 0.05 0.28 Q12 1 0.2224 0.7581 0.3946 11.00000 0.05 0.27 Q13 1 0.0305 0.2973 0.8466 11.00000 0.05 0.27 Q14 1 0.3132 0.9393 0.8799 11.00000 0.05 0.27 Q15 1 0.7481 0.6606 0.6050 11.00000 0.05 0.26 Q16 1 0.3259 0.7342 0.4546 11.00000 0.05 0.26 Q17 1 0.1931 0.6612 0.7953 11.00000 0.05 0.26 Q18 1 0.3239 0.3121 0.8402 11.00000 0.05 0.26 Q19 1 -0.0878 0.5553 0.8560 11.00000 0.05 0.26 Q20 1 0.1915 0.8034 0.6138 11.00000 0.05 0.26 ; _shelx_res_checksum 98647 _shelx_hkl_file ; -2 0 0 13.98 0.47 -2 0 0 14.90 0.48 -2 0 0 14.51 0.56 -2 0 0 13.02 0.55 -2 0 0 14.28 0.45 -2 0 0 15.52 0.66 -2 0 0 12.43 0.40 -2 0 0 14.97 0.43 -2 0 0 15.26 0.58 2 0 0 14.18 0.55 2 0 0 14.45 0.59 2 0 0 14.24 0.43 2 0 0 14.83 0.46 2 0 0 13.55 0.47 2 0 0 13.30 0.56 2 0 0 13.77 0.55 2 0 0 14.44 0.48 2 0 0 14.51 0.43 -3 0 0 282.64 6.26 -3 0 0 290.89 6.07 -3 0 0 280.80 5.93 -3 0 0 288.05 6.23 -3 0 0 295.22 6.03 -3 0 0 288.63 5.97 -3 0 0 284.84 6.01 -3 0 0 280.80 6.05 3 0 0 294.97 6.02 3 0 0 282.56 6.05 3 0 0 287.99 6.23 3 0 0 290.29 6.28 3 0 0 288.83 5.98 3 0 0 289.81 5.97 3 0 0 282.78 6.23 3 0 0 279.05 5.98 3 0 0 280.48 6.05 -4 0 0 187.30 4.05 -4 0 0 187.16 4.13 -4 0 0 179.89 4.30 -4 0 0 190.80 4.39 -4 0 0 183.69 3.93 -4 0 0 185.64 4.07 -4 0 0 180.78 4.09 -4 0 0 183.04 3.97 4 0 0 179.83 4.32 4 0 0 179.69 4.09 4 0 0 179.53 4.08 4 0 0 189.89 4.02 4 0 0 187.64 4.01 4 0 0 186.34 3.99 4 0 0 182.63 4.04 4 0 0 186.77 4.40 4 0 0 180.79 4.32 -5 0 0 0.08 0.14 -5 0 0 0.17 0.22 -5 0 0 0.13 0.11 -5 0 0 0.01 0.09 -5 0 0 0.23 0.15 -5 0 0 0.18 0.17 5 0 0 -0.03 0.18 5 0 0 0.20 0.13 5 0 0 0.06 0.14 5 0 0 0.15 0.22 5 0 0 0.02 0.15 5 0 0 0.32 0.25 5 0 0 0.11 0.12 5 0 0 0.40 0.15 5 0 0 0.18 0.12 -6 0 0 14.56 0.57 -6 0 0 16.03 0.95 -6 0 0 15.28 0.71 -6 0 0 15.40 0.72 -6 0 0 14.57 0.54 6 0 0 16.20 0.97 6 0 0 15.52 0.95 6 0 0 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34.18 1.05 2 -3 0 31.77 0.89 2 -3 0 33.43 0.87 2 -3 0 32.45 0.88 2 -3 0 33.57 0.89 2 -3 0 31.93 1.09 2 -3 0 31.66 0.86 -2 3 0 32.16 0.85 -2 3 0 33.31 0.86 -2 3 0 32.77 0.92 -2 3 0 34.26 0.93 -2 3 0 32.86 0.97 -2 3 0 32.18 1.13 -2 3 0 33.15 1.03 1 -3 0 220.56 4.68 1 -3 0 220.52 4.83 1 -3 0 215.28 4.71 1 -3 0 223.99 4.69 1 -3 0 218.19 4.72 1 -3 0 219.54 4.86 1 -3 0 225.26 4.77 1 -3 0 212.72 4.75 -1 3 0 224.90 4.75 -1 3 0 222.84 4.74 -1 3 0 214.31 4.86 -1 3 0 220.46 4.73 -1 3 0 225.74 4.84 -1 3 0 213.05 4.72 -1 3 0 219.52 4.66 0 -3 0 24.56 0.81 0 -3 0 25.78 0.80 0 -3 0 26.04 0.80 0 -3 0 24.07 0.63 0 -3 0 24.73 0.79 0 -3 0 25.52 0.82 0 -3 0 23.84 0.80 0 -3 0 24.89 0.78 0 -3 0 26.58 0.86 0 3 0 26.04 0.84 0 3 0 25.66 0.81 0 3 0 24.94 0.82 0 3 0 24.14 0.78 0 3 0 25.03 0.65 0 3 0 24.92 0.78 0 3 0 25.05 0.80 -1 -3 0 116.73 2.69 -1 -3 0 118.58 2.73 -1 -3 0 112.41 2.61 -1 -3 0 114.85 2.67 -1 -3 0 116.65 2.68 -1 -3 0 114.11 2.65 -1 -3 0 114.27 2.72 -1 -3 0 114.45 2.73 -1 -3 0 113.79 2.57 1 3 0 116.44 2.75 1 3 0 114.92 2.57 1 3 0 116.07 2.62 1 3 0 117.54 2.67 1 3 0 119.54 2.70 1 3 0 116.25 2.73 1 3 0 114.98 2.67 1 3 0 115.87 2.70 1 3 0 112.76 2.67 -2 -3 0 45.94 1.33 -2 -3 0 47.41 1.34 -2 -3 0 46.67 1.37 -2 -3 0 46.18 1.08 -2 -3 0 46.48 1.35 -2 -3 0 47.44 1.32 -2 -3 0 47.36 1.40 -2 -3 0 45.35 1.37 -2 -3 0 47.73 1.40 2 3 0 45.95 1.40 2 3 0 49.02 1.35 2 3 0 48.42 1.36 2 3 0 46.99 1.34 2 3 0 47.03 1.33 2 3 0 45.64 1.37 2 3 0 46.71 1.38 2 3 0 47.10 1.38 -3 -3 0 132.54 3.21 -3 -3 0 133.47 3.21 -3 -3 0 131.02 3.26 -3 -3 0 132.18 3.10 -3 -3 0 131.39 3.13 -3 -3 0 133.40 3.23 3 3 0 133.59 3.28 3 3 0 138.12 3.74 3 3 0 128.44 3.20 3 3 0 131.72 3.12 3 3 0 127.24 3.21 3 3 0 132.52 3.14 3 3 0 131.32 3.21 3 3 0 130.43 3.18 -4 -3 0 191.26 4.88 -4 -3 0 202.94 4.76 -4 -3 0 200.99 4.61 -4 -3 0 189.93 4.69 -4 -3 0 206.79 4.75 -4 -3 0 202.24 4.75 4 3 0 199.76 4.81 4 3 0 202.50 4.71 4 3 0 202.67 4.85 4 3 0 209.68 4.84 4 3 0 197.36 4.75 4 3 0 207.25 4.63 4 3 0 202.45 4.61 4 3 0 198.92 4.60 -5 -3 0 101.92 2.87 -5 -3 0 102.53 2.95 -5 -3 0 98.32 2.61 -5 -3 0 103.89 2.84 -5 -3 0 97.45 2.57 -5 -3 0 105.33 2.95 -5 -3 0 103.78 2.77 -5 -3 0 103.85 2.75 5 3 0 101.71 2.86 5 3 0 103.82 2.66 5 3 0 98.64 2.67 5 3 0 100.09 2.65 5 3 0 106.88 3.01 5 3 0 100.82 2.73 5 3 0 100.42 2.86 5 3 0 104.34 2.99 -6 -3 0 0.05 0.16 -6 -3 0 0.28 0.21 -6 -3 0 0.06 0.26 -6 -3 0 0.17 0.22 -6 -3 0 -0.10 0.19 -6 -3 0 -0.03 0.16 -6 -3 0 -0.03 0.28 6 3 0 -0.28 0.13 6 3 0 0.23 0.23 6 3 0 0.11 0.28 6 3 0 -0.07 0.22 6 3 0 0.02 0.17 6 3 0 -0.04 0.38 6 3 0 -0.13 0.16 6 3 0 -0.18 0.16 -7 -3 0 42.46 1.45 -7 -3 0 43.50 1.82 -7 -3 0 42.87 1.60 -7 -3 0 42.25 1.58 -7 -3 0 38.57 1.57 -7 -3 0 42.26 1.56 7 3 0 40.87 1.55 7 3 0 43.44 1.52 7 3 0 41.93 1.53 7 3 0 42.49 1.92 7 3 0 43.22 1.94 7 3 0 43.46 1.57 7 3 0 43.86 1.61 7 3 0 41.77 1.80 -8 -3 0 52.41 1.88 -8 -3 0 53.20 1.89 -8 -3 0 54.56 2.13 -8 -3 0 53.73 1.89 -8 -3 0 48.88 2.00 8 3 0 51.17 2.18 8 3 0 55.97 2.36 8 3 0 51.33 1.80 8 3 0 53.76 1.81 8 3 0 52.43 1.86 8 3 0 51.93 1.82 -9 -3 0 19.90 1.15 -9 -3 0 21.26 1.33 -9 -3 0 20.95 1.17 -9 -3 0 19.94 0.95 9 3 0 19.47 1.06 9 3 0 20.14 1.08 9 3 0 20.66 1.10 9 3 0 20.19 1.14 9 3 0 25.54 1.65 -10 -3 0 0.48 0.33 -10 -3 0 0.41 0.31 -10 -3 0 0.07 0.37 -10 -3 0 0.22 0.16 10 3 0 0.58 0.59 10 3 0 0.17 0.34 10 3 0 0.16 0.29 10 3 0 0.40 0.32 10 3 0 0.21 0.25 10 -4 0 11.07 0.80 10 -4 0 12.62 0.48 10 -4 0 10.83 1.24 10 -4 0 11.20 0.77 10 -4 0 12.17 0.48 10 -4 0 12.97 1.20 9 -4 0 0.74 0.16 9 -4 0 0.67 0.47 9 -4 0 0.54 0.55 9 -4 0 0.82 0.29 9 -4 0 0.24 0.28 9 -4 0 0.79 0.40 9 -4 0 0.69 0.41 8 -4 0 0.31 0.25 8 -4 0 0.00 0.36 8 -4 0 0.48 0.38 8 -4 0 -0.38 0.22 8 -4 0 -0.26 0.27 8 -4 0 0.28 0.30 8 -4 0 0.14 0.16 7 -4 0 8.79 0.89 7 -4 0 7.29 0.81 7 -4 0 9.19 0.65 7 -4 0 8.77 0.48 7 -4 0 8.13 0.77 7 -4 0 6.93 1.24 7 -4 0 8.69 0.79 7 -4 0 8.41 0.90 7 -4 0 9.50 0.67 -7 4 0 8.59 0.46 -7 4 0 9.34 0.48 -7 4 0 7.96 0.87 6 -4 0 52.93 1.80 6 -4 0 54.84 1.71 6 -4 0 54.92 2.08 6 -4 0 50.04 1.89 6 -4 0 51.01 1.60 6 -4 0 56.00 1.85 6 -4 0 56.37 1.53 6 -4 0 50.86 1.96 6 -4 0 53.92 2.03 -6 4 0 53.46 1.99 -6 4 0 53.85 1.77 -6 4 0 53.52 1.46 5 -4 0 21.82 1.11 5 -4 0 20.03 0.84 5 -4 0 20.22 0.73 5 -4 0 20.20 0.94 5 -4 0 20.99 1.08 5 -4 0 19.91 0.91 5 -4 0 18.34 1.06 5 -4 0 20.96 0.70 -5 4 0 20.44 1.12 -5 4 0 21.48 0.79 -5 4 0 20.55 0.73 4 -4 0 1.45 0.20 4 -4 0 1.07 0.33 4 -4 0 1.23 0.18 4 -4 0 1.23 0.17 4 -4 0 1.09 0.23 4 -4 0 1.59 0.22 4 -4 0 1.22 0.24 4 -4 0 1.01 0.24 4 -4 0 1.01 0.32 4 -4 0 1.16 0.31 4 -4 0 1.44 0.33 -4 4 0 1.14 0.34 -4 4 0 1.12 0.16 -4 4 0 1.26 0.22 -4 4 0 1.50 0.28 -4 4 0 1.20 0.15 -4 4 0 1.36 0.22 3 -4 0 215.91 5.28 3 -4 0 231.72 5.17 3 -4 0 223.22 4.88 3 -4 0 244.36 6.08 3 -4 0 232.80 4.90 3 -4 0 224.19 5.26 3 -4 0 224.62 4.85 3 -4 0 221.92 4.99 3 -4 0 224.03 4.88 3 -4 0 220.19 4.86 -3 4 0 220.74 5.31 -3 4 0 221.24 4.78 -3 4 0 225.00 5.02 -3 4 0 225.35 4.92 -3 4 0 240.19 5.31 -3 4 0 224.64 4.82 -3 4 0 225.47 5.13 2 -4 0 234.24 4.85 2 -4 0 233.43 5.04 2 -4 0 228.71 4.94 2 -4 0 229.35 5.04 2 -4 0 235.56 5.30 2 -4 0 242.38 5.21 2 -4 0 228.19 5.09 2 -4 0 226.66 5.32 2 -4 0 233.79 5.02 2 -4 0 233.18 5.03 -2 4 0 233.71 5.16 -2 4 0 228.96 5.08 -2 4 0 238.78 5.09 -2 4 0 235.61 5.12 -2 4 0 233.62 5.35 -2 4 0 230.55 4.98 1 -4 0 161.81 3.60 1 -4 0 154.75 3.63 1 -4 0 171.04 4.07 1 -4 0 154.91 3.76 1 -4 0 165.19 3.78 1 -4 0 160.71 3.60 1 -4 0 159.09 3.68 1 -4 0 158.47 3.64 -1 4 0 164.36 3.65 -1 4 0 155.52 3.73 -1 4 0 166.21 3.68 -1 4 0 162.52 3.65 -1 4 0 159.85 3.57 -1 4 0 156.52 3.78 0 -4 0 25.51 0.68 0 -4 0 24.40 0.88 0 -4 0 25.96 0.88 0 -4 0 25.89 0.87 0 -4 0 25.33 0.87 0 -4 0 25.48 0.91 0 -4 0 26.73 0.95 0 -4 0 25.48 0.91 0 -4 0 25.17 0.90 0 4 0 26.04 0.93 0 4 0 23.79 0.85 0 4 0 25.51 0.89 0 4 0 25.03 0.72 0 4 0 24.39 0.90 0 4 0 24.79 0.92 0 4 0 25.89 0.90 0 4 0 25.23 0.85 0 4 0 25.16 0.91 -1 -4 0 25.36 0.88 -1 -4 0 25.24 0.89 -1 -4 0 25.56 0.96 -1 -4 0 25.87 0.92 -1 -4 0 26.45 0.97 -1 -4 0 25.25 0.91 -1 -4 0 25.65 0.95 -1 -4 0 24.93 0.83 -1 -4 0 25.85 0.82 1 4 0 24.76 0.83 1 4 0 24.29 0.96 1 4 0 24.62 0.89 1 4 0 24.22 0.94 1 4 0 25.46 0.82 1 4 0 25.87 0.92 1 4 0 25.03 0.90 1 4 0 26.33 0.90 1 4 0 25.58 0.93 -2 -4 0 138.19 3.29 -2 -4 0 137.86 3.27 -2 -4 0 136.57 3.35 -2 -4 0 139.89 3.29 -2 -4 0 137.99 3.03 -2 -4 0 139.09 3.27 -2 -4 0 138.52 3.37 -2 -4 0 138.01 3.28 -2 -4 0 139.98 3.37 2 4 0 138.55 3.28 2 4 0 136.24 3.28 2 4 0 137.22 3.28 2 4 0 138.40 3.39 2 4 0 138.69 3.28 2 4 0 137.01 3.35 2 4 0 135.95 3.31 2 4 0 139.49 3.30 -3 -4 0 252.92 5.66 -3 -4 0 253.06 5.72 -3 -4 0 255.84 5.79 -3 -4 0 260.76 5.75 -3 -4 0 257.11 5.70 -3 -4 0 257.28 5.79 -3 -4 0 256.30 5.79 -3 -4 0 256.24 5.80 -3 -4 0 253.77 5.21 -3 -4 0 218.26 5.19 3 4 0 254.06 5.77 3 4 0 262.31 5.72 3 4 0 259.69 5.70 3 4 0 255.86 5.80 3 4 0 253.40 5.70 3 4 0 251.95 5.76 3 4 0 257.02 5.76 3 4 0 259.66 5.90 -4 -4 0 4.76 0.53 -4 -4 0 3.77 0.52 -4 -4 0 4.12 0.44 -4 -4 0 4.20 0.46 -4 -4 0 4.16 0.49 -4 -4 0 4.83 0.57 4 4 0 4.72 0.51 4 4 0 4.71 0.63 4 4 0 3.92 0.56 4 4 0 3.60 0.43 4 4 0 4.27 0.49 4 4 0 4.67 0.60 4 4 0 4.60 0.51 4 4 0 4.46 0.47 -5 -4 0 3.60 0.46 -5 -4 0 3.58 0.54 -5 -4 0 3.20 0.46 -5 -4 0 3.91 0.43 -5 -4 0 3.94 0.59 -5 -4 0 3.14 0.44 -5 -4 0 4.56 0.58 5 4 0 3.56 0.47 5 4 0 3.34 0.54 5 4 0 3.79 0.54 5 4 0 3.73 0.51 5 4 0 3.31 0.47 5 4 0 3.22 0.47 5 4 0 3.01 0.42 5 4 0 3.15 0.50 -6 -4 0 91.32 3.22 -6 -4 0 92.49 2.56 -6 -4 0 96.46 3.09 -6 -4 0 92.18 2.63 -6 -4 0 92.85 2.71 -6 -4 0 95.65 2.80 -6 -4 0 94.01 2.54 6 4 0 90.75 2.64 6 4 0 89.94 2.81 6 4 0 91.40 2.84 6 4 0 91.30 2.61 6 4 0 87.99 3.13 6 4 0 96.62 2.66 6 4 0 89.02 2.67 6 4 0 91.58 2.97 -7 -4 0 57.43 2.20 -7 -4 0 58.12 2.01 -7 -4 0 57.72 1.97 -7 -4 0 57.53 1.86 -7 -4 0 55.72 1.80 -7 -4 0 55.87 1.99 -7 -4 0 57.86 2.20 7 4 0 55.97 2.16 7 4 0 59.52 2.35 7 4 0 56.71 1.98 7 4 0 58.19 1.94 7 4 0 60.15 1.95 7 4 0 56.56 1.93 7 4 0 61.42 2.00 7 4 0 56.03 2.20 -8 -4 0 6.09 0.59 -8 -4 0 6.14 0.70 -8 -4 0 5.68 0.77 -8 -4 0 6.58 0.85 -8 -4 0 6.06 0.69 -8 -4 0 4.43 0.57 8 4 0 5.43 0.64 8 4 0 6.21 0.66 8 4 0 6.37 0.69 8 4 0 6.95 0.99 8 4 0 6.49 0.75 8 4 0 4.97 0.77 -9 -4 0 8.23 0.92 -9 -4 0 7.09 0.78 -9 -4 0 6.31 0.62 9 4 0 7.30 0.72 9 4 0 6.43 0.74 9 4 0 6.15 0.68 9 4 0 6.88 1.09 9 4 0 6.21 0.72 -10 -4 0 22.93 1.56 -10 -4 0 18.88 1.24 -10 -4 0 22.49 1.50 -10 -4 0 21.52 1.08 10 4 0 23.82 1.42 10 4 0 21.92 1.22 10 4 0 23.09 1.35 10 4 0 21.98 1.84 10 4 0 24.70 2.10 10 -5 0 -0.83 0.43 10 -5 0 0.11 0.59 10 -5 0 0.58 0.34 10 -5 0 -0.20 0.29 10 -5 0 0.84 0.45 9 -5 0 6.01 0.38 9 -5 0 5.17 0.82 9 -5 0 5.39 0.61 9 -5 0 5.36 0.59 9 -5 0 5.80 0.92 9 -5 0 5.79 0.89 9 -5 0 5.94 0.90 8 -5 0 51.64 2.25 8 -5 0 51.49 2.18 8 -5 0 50.38 1.75 8 -5 0 54.65 1.69 8 -5 0 54.06 2.26 8 -5 0 51.26 1.41 8 -5 0 51.41 1.70 8 -5 0 55.94 2.07 8 -5 0 50.80 2.00 -8 5 0 54.61 2.23 7 -5 0 31.66 1.41 7 -5 0 31.13 1.04 7 -5 0 32.61 1.01 7 -5 0 33.56 1.63 7 -5 0 31.75 1.22 7 -5 0 31.67 1.60 7 -5 0 31.82 1.53 7 -5 0 34.82 1.64 7 -5 0 34.24 1.71 7 -5 0 31.16 1.26 7 -5 0 32.34 1.66 -7 5 0 32.86 1.04 -7 5 0 33.59 1.02 -7 5 0 32.32 1.65 6 -5 0 11.84 0.80 6 -5 0 12.28 0.90 6 -5 0 13.05 0.58 6 -5 0 11.87 0.97 6 -5 0 12.45 0.88 6 -5 0 11.03 0.75 6 -5 0 13.06 1.03 6 -5 0 12.75 0.62 6 -5 0 14.30 1.29 6 -5 0 13.84 1.03 -6 5 0 12.22 0.59 -6 5 0 13.08 0.64 -6 5 0 13.57 1.07 5 -5 0 55.27 2.01 5 -5 0 57.02 1.37 5 -5 0 55.43 1.49 5 -5 0 53.54 1.65 5 -5 0 56.06 1.69 5 -5 0 54.91 1.68 5 -5 0 52.82 2.00 5 -5 0 54.14 1.41 5 -5 0 57.66 1.53 5 -5 0 55.22 2.02 5 -5 0 56.36 1.95 -5 5 0 57.47 1.55 -5 5 0 56.95 1.58 -5 5 0 52.84 2.02 -5 5 0 55.02 1.75 4 -5 0 204.10 5.11 4 -5 0 204.29 4.60 4 -5 0 213.49 5.11 4 -5 0 206.13 4.55 4 -5 0 208.48 4.55 4 -5 0 207.09 5.05 4 -5 0 210.78 4.96 4 -5 0 204.92 4.49 4 -5 0 202.40 4.60 4 -5 0 203.42 4.54 4 -5 0 203.36 4.70 -4 5 0 211.79 4.62 -4 5 0 207.71 5.13 -4 5 0 202.59 4.89 -4 5 0 202.51 4.43 -4 5 0 208.90 4.63 -4 5 0 208.35 4.77 -4 5 0 201.77 4.39 3 -5 0 109.58 2.64 3 -5 0 108.27 3.05 3 -5 0 110.48 3.01 3 -5 0 110.33 2.52 3 -5 0 109.51 2.52 3 -5 0 114.96 2.66 3 -5 0 108.97 2.75 3 -5 0 110.76 2.64 3 -5 0 115.34 2.93 -3 5 0 112.42 2.79 -3 5 0 113.10 2.87 -3 5 0 108.76 2.56 -3 5 0 108.89 3.06 -3 5 0 111.71 2.59 -3 5 0 117.09 2.74 -3 5 0 113.30 2.72 2 -5 0 28.37 1.09 2 -5 0 27.52 1.00 2 -5 0 27.17 1.15 2 -5 0 28.22 0.96 2 -5 0 26.44 1.57 2 -5 0 29.05 1.07 2 -5 0 26.37 0.94 -2 5 0 28.10 1.12 -2 5 0 28.40 1.05 -2 5 0 27.20 1.37 -2 5 0 27.71 0.90 -2 5 0 29.20 1.03 -2 5 0 27.91 0.91 -2 5 0 28.63 1.01 1 -5 0 1.57 0.30 1 -5 0 1.71 0.29 1 -5 0 1.19 0.21 1 -5 0 1.78 0.32 1 -5 0 1.36 0.23 1 -5 0 1.31 0.26 1 -5 0 1.11 0.21 1 -5 0 1.18 0.22 -1 5 0 1.18 0.20 -1 5 0 1.86 0.28 -1 5 0 1.76 0.34 -1 5 0 1.87 0.27 -1 5 0 1.68 0.29 -1 5 0 1.26 0.24 0 -5 0 207.08 4.78 0 -5 0 213.44 4.82 0 -5 0 209.02 4.70 0 -5 0 211.12 4.72 0 -5 0 211.55 4.71 0 -5 0 207.33 4.72 0 -5 0 216.24 5.34 0 -5 0 206.63 4.76 0 -5 0 205.11 4.40 0 5 0 208.54 4.79 0 5 0 205.57 4.79 0 5 0 202.85 4.72 0 5 0 208.73 4.40 0 5 0 211.68 4.74 0 5 0 209.21 4.79 0 5 0 204.01 4.68 0 5 0 208.05 4.77 -1 -5 0 155.00 3.51 -1 -5 0 155.34 3.69 -1 -5 0 155.87 3.78 -1 -5 0 156.44 3.68 -1 -5 0 151.06 3.74 -1 -5 0 151.25 3.59 -1 -5 0 159.73 3.78 -1 -5 0 163.05 3.66 -1 -5 0 158.90 3.71 1 5 0 151.39 3.66 1 5 0 154.34 3.76 1 5 0 152.74 3.60 1 5 0 156.18 3.69 1 5 0 155.48 3.73 1 5 0 157.28 3.71 1 5 0 159.06 3.81 1 5 0 155.71 3.52 1 5 0 155.17 3.67 -2 -5 0 12.42 0.73 -2 -5 0 12.01 0.67 -2 -5 0 11.16 0.54 -2 -5 0 11.65 0.64 -2 -5 0 11.84 0.66 -2 -5 0 12.59 0.76 -2 -5 0 10.99 0.66 -2 -5 0 13.04 0.71 2 5 0 11.98 0.68 2 5 0 11.71 0.66 2 5 0 12.73 0.71 2 5 0 11.93 0.75 2 5 0 11.21 0.54 2 5 0 11.45 0.66 2 5 0 11.93 0.72 2 5 0 12.32 0.71 2 5 0 11.61 0.67 -3 -5 0 3.94 0.60 -3 -5 0 4.05 0.27 -3 -5 0 3.80 0.27 -3 -5 0 3.91 0.56 -3 -5 0 3.20 0.45 -3 -5 0 3.91 0.50 -3 -5 0 4.29 0.46 -3 -5 0 4.04 0.49 -3 -5 0 4.65 0.58 -3 -5 0 4.53 0.49 3 5 0 6.52 0.80 3 5 0 3.98 0.46 3 5 0 4.36 0.48 3 5 0 4.38 0.69 3 5 0 4.11 0.49 3 5 0 4.11 0.53 3 5 0 4.06 0.49 3 5 0 4.68 0.49 -4 -5 0 81.81 2.45 -4 -5 0 82.50 2.36 -4 -5 0 85.17 2.45 -4 -5 0 80.30 2.29 -4 -5 0 81.18 2.33 -4 -5 0 80.81 2.39 -4 -5 0 80.51 2.42 -4 -5 0 83.42 2.44 4 5 0 82.38 2.41 4 5 0 81.50 2.40 4 5 0 82.50 2.35 4 5 0 82.19 2.34 4 5 0 83.80 2.48 4 5 0 80.77 2.32 4 5 0 80.68 2.41 4 5 0 76.36 2.60 -5 -5 0 143.75 3.75 -5 -5 0 143.74 3.74 -5 -5 0 136.90 3.71 -5 -5 0 140.91 3.75 -5 -5 0 137.41 3.82 -5 -5 0 140.55 3.62 -5 -5 0 136.82 3.54 5 5 0 138.34 3.75 5 5 0 138.76 3.68 5 5 0 139.80 3.73 5 5 0 145.79 3.89 5 5 0 135.49 3.59 5 5 0 135.24 3.72 5 5 0 144.07 3.64 5 5 0 141.72 3.62 -6 -5 0 39.79 1.60 -6 -5 0 37.25 1.43 -6 -5 0 38.29 1.51 -6 -5 0 39.36 1.64 -6 -5 0 37.91 1.45 -6 -5 0 40.25 1.68 6 5 0 40.16 1.55 6 5 0 39.35 1.66 6 5 0 39.00 1.52 6 5 0 37.01 1.52 6 5 0 38.37 1.67 6 5 0 40.18 1.54 6 5 0 39.57 1.77 6 5 0 37.86 1.58 -7 -5 0 1.04 0.36 -7 -5 0 1.66 0.50 -7 -5 0 1.36 0.44 -7 -5 0 1.13 0.34 -7 -5 0 1.28 0.31 -7 -5 0 1.37 0.35 -7 -5 0 1.09 0.30 7 5 0 1.63 0.41 7 5 0 1.47 0.49 7 5 0 0.88 0.60 7 5 0 1.42 0.35 7 5 0 1.11 0.40 7 5 0 0.21 0.40 7 5 0 0.77 0.31 7 5 0 0.89 0.32 -8 -5 0 24.23 1.32 -8 -5 0 23.96 1.18 -8 -5 0 23.79 1.30 -8 -5 0 25.70 1.42 -8 -5 0 28.01 1.56 8 5 0 25.16 1.27 8 5 0 25.89 1.31 8 5 0 25.07 1.32 8 5 0 24.80 1.27 8 5 0 21.56 1.45 8 5 0 23.62 1.57 -9 -5 0 39.20 1.78 -9 -5 0 43.10 1.97 -9 -5 0 43.18 1.85 9 5 0 41.23 1.74 9 5 0 42.47 1.81 9 5 0 42.24 1.76 9 5 0 42.34 1.81 9 5 0 43.81 2.25 -10 -5 0 22.39 1.85 -10 -5 0 24.23 1.57 10 5 0 22.06 2.07 10 5 0 22.39 1.32 10 5 0 22.55 1.31 10 5 0 22.96 1.71 10 5 0 21.85 1.31 9 -6 0 40.30 1.49 9 -6 0 42.22 1.23 9 -6 0 39.57 2.05 9 -6 0 40.10 1.80 9 -6 0 37.86 1.74 9 -6 0 38.13 1.53 9 -6 0 40.45 1.11 9 -6 0 41.28 2.15 8 -6 0 1.20 0.31 8 -6 0 1.57 0.67 8 -6 0 1.35 0.21 8 -6 0 1.24 0.34 8 -6 0 0.82 0.44 8 -6 0 1.07 0.38 8 -6 0 1.70 0.24 8 -6 0 1.23 0.47 -8 6 0 2.53 0.52 7 -6 0 16.72 1.12 7 -6 0 19.04 1.36 7 -6 0 17.96 0.92 7 -6 0 19.91 1.28 7 -6 0 19.50 1.30 7 -6 0 19.81 1.04 7 -6 0 18.21 0.79 7 -6 0 18.78 0.80 7 -6 0 18.67 1.04 -7 6 0 19.28 1.31 -7 6 0 17.09 1.09 -7 6 0 19.04 0.80 6 -6 0 36.31 1.46 6 -6 0 38.25 1.78 6 -6 0 37.29 1.83 6 -6 0 40.35 1.70 6 -6 0 37.82 1.23 6 -6 0 36.63 1.76 6 -6 0 37.47 1.36 6 -6 0 38.90 1.20 -6 6 0 39.87 1.24 -6 6 0 37.68 1.27 -6 6 0 38.88 1.79 5 -6 0 39.32 1.23 5 -6 0 39.55 1.15 5 -6 0 37.63 1.71 5 -6 0 40.10 1.29 5 -6 0 39.93 1.60 5 -6 0 38.97 1.16 5 -6 0 39.38 1.69 5 -6 0 38.64 1.22 5 -6 0 37.51 1.34 5 -6 0 37.43 1.68 5 -6 0 39.31 1.28 -5 6 0 37.97 0.99 -5 6 0 39.52 1.44 -5 6 0 39.10 1.31 -5 6 0 40.64 1.31 -5 6 0 37.82 0.98 -5 6 0 40.09 2.03 4 -6 0 24.11 0.89 4 -6 0 22.39 0.82 4 -6 0 23.15 1.21 4 -6 0 21.74 1.16 4 -6 0 18.98 1.33 4 -6 0 22.44 0.86 4 -6 0 19.96 1.18 4 -6 0 22.84 1.11 4 -6 0 22.20 0.78 4 -6 0 22.37 0.86 4 -6 0 21.61 0.77 -4 6 0 21.77 0.77 -4 6 0 22.00 0.75 -4 6 0 22.64 0.91 -4 6 0 22.54 1.24 -4 6 0 23.58 0.93 -4 6 0 22.47 1.17 -4 6 0 23.14 1.07 3 -6 0 0.97 0.33 3 -6 0 1.52 0.18 3 -6 0 1.50 0.31 3 -6 0 1.11 0.22 3 -6 0 1.64 0.19 3 -6 0 1.01 0.21 3 -6 0 1.26 0.31 3 -6 0 0.87 0.34 3 -6 0 1.11 0.22 -3 6 0 0.83 0.36 -3 6 0 0.83 0.30 -3 6 0 1.20 0.27 -3 6 0 1.19 0.21 -3 6 0 0.94 0.25 -3 6 0 1.25 0.20 2 -6 0 46.20 1.44 2 -6 0 45.52 1.41 2 -6 0 47.52 1.55 2 -6 0 46.31 1.41 2 -6 0 43.84 1.63 2 -6 0 44.28 1.41 2 -6 0 46.32 1.63 2 -6 0 45.96 1.47 -2 6 0 46.44 1.62 -2 6 0 46.07 1.49 -2 6 0 44.88 1.66 -2 6 0 45.00 1.35 -2 6 0 47.31 1.50 -2 6 0 46.18 1.49 -2 6 0 43.78 1.34 -2 6 0 45.62 1.47 1 -6 0 94.85 2.89 1 -6 0 103.95 2.71 1 -6 0 98.63 2.64 1 -6 0 99.33 2.62 1 -6 0 98.29 2.60 1 -6 0 100.62 2.81 1 -6 0 103.94 2.77 1 -6 0 96.38 3.00 -1 6 0 101.41 2.67 -1 6 0 104.08 3.53 -1 6 0 102.27 2.60 -1 6 0 99.56 2.58 -1 6 0 96.88 3.38 -1 6 0 102.82 2.93 0 -6 0 208.10 4.90 0 -6 0 217.33 4.95 0 -6 0 210.65 4.82 0 -6 0 202.88 4.90 0 -6 0 215.70 4.86 0 -6 0 207.08 4.86 0 -6 0 212.02 5.81 0 -6 0 218.03 4.84 0 6 0 206.28 4.92 0 6 0 209.70 4.85 0 6 0 205.24 4.90 0 6 0 211.87 4.46 0 6 0 197.11 4.82 0 6 0 205.45 4.91 0 6 0 207.93 4.81 0 6 0 220.07 5.65 -1 -6 0 11.51 0.65 -1 -6 0 12.29 0.93 -1 -6 0 11.11 0.68 -1 -6 0 12.83 0.92 -1 -6 0 11.33 0.70 -1 -6 0 12.57 0.69 -1 -6 0 10.90 0.71 -1 -6 0 10.90 0.54 -1 -6 0 11.73 0.73 1 6 0 10.93 0.65 1 6 0 11.93 0.78 1 6 0 10.98 0.72 1 6 0 11.17 0.56 1 6 0 11.73 0.69 1 6 0 11.14 0.72 1 6 0 11.55 0.71 1 6 0 11.00 0.68 1 6 0 11.08 0.68 -2 -6 0 33.63 1.24 -2 -6 0 31.72 1.30 -2 -6 0 31.90 1.29 -2 -6 0 30.77 1.54 -2 -6 0 32.97 1.25 -2 -6 0 32.80 1.15 -2 -6 0 32.83 1.23 -2 -6 0 32.09 1.07 -2 -6 0 31.58 1.22 2 6 0 31.35 1.28 2 6 0 33.31 1.26 2 6 0 30.91 1.22 2 6 0 33.38 1.25 2 6 0 32.48 1.08 2 6 0 31.44 1.20 2 6 0 32.87 1.17 2 6 0 31.39 1.46 -3 -6 0 182.81 4.40 -3 -6 0 181.51 4.40 -3 -6 0 179.85 4.53 -3 -6 0 180.85 4.52 -3 -6 0 180.17 4.00 -3 -6 0 177.90 4.40 -3 -6 0 179.74 4.41 -3 -6 0 191.32 5.17 3 6 0 178.16 4.41 3 6 0 181.17 4.41 3 6 0 183.14 4.53 3 6 0 174.10 4.49 3 6 0 185.60 4.44 3 6 0 182.21 4.41 3 6 0 179.99 4.56 3 6 0 178.86 4.45 -4 -6 0 86.37 2.64 -4 -6 0 88.31 2.57 -4 -6 0 89.80 2.55 -4 -6 0 91.52 2.68 -4 -6 0 90.11 2.66 -4 -6 0 88.23 2.55 -4 -6 0 83.37 2.48 -4 -6 0 85.40 1.90 -4 -6 0 87.11 2.61 4 6 0 87.57 2.54 4 6 0 91.45 2.58 4 6 0 85.36 2.57 4 6 0 87.51 2.67 4 6 0 83.38 2.59 4 6 0 85.29 2.52 4 6 0 87.45 2.60 4 6 0 89.22 2.65 -5 -6 0 2.32 0.43 -5 -6 0 2.75 0.49 -5 -6 0 2.63 0.49 -5 -6 0 1.48 0.32 -5 -6 0 2.03 0.37 -5 -6 0 1.69 0.33 -5 -6 0 2.39 0.37 -5 -6 0 2.35 0.51 5 6 0 1.77 0.36 5 6 0 2.60 0.47 5 6 0 1.84 0.41 5 6 0 3.07 0.52 5 6 0 2.25 0.50 5 6 0 2.24 0.47 5 6 0 1.83 0.41 5 6 0 1.76 0.36 -6 -6 0 -0.36 0.20 -6 -6 0 0.05 0.24 -6 -6 0 -0.33 0.16 -6 -6 0 0.07 0.24 -6 -6 0 0.25 0.56 -6 -6 0 -0.14 0.25 6 6 0 0.08 0.35 6 6 0 0.35 0.40 6 6 0 0.48 0.38 6 6 0 -0.09 0.20 6 6 0 0.00 0.30 6 6 0 0.05 0.21 6 6 0 0.15 0.24 6 6 0 -0.09 0.25 -7 -6 0 42.09 2.22 -7 -6 0 41.98 1.68 -7 -6 0 40.42 1.64 -7 -6 0 42.01 1.72 -7 -6 0 41.72 2.07 -7 -6 0 46.14 1.90 7 6 0 43.53 2.03 7 6 0 38.06 1.93 7 6 0 43.79 1.98 7 6 0 42.38 2.22 7 6 0 43.18 1.75 7 6 0 42.21 1.81 7 6 0 42.18 1.78 -8 -6 0 28.43 1.45 -8 -6 0 29.88 1.54 -8 -6 0 27.16 2.28 -8 -6 0 30.10 1.68 8 6 0 30.66 1.53 8 6 0 28.23 1.69 8 6 0 30.80 1.48 8 6 0 32.79 1.87 8 6 0 31.24 1.48 8 6 0 29.50 1.84 -9 -6 0 6.41 0.94 -9 -6 0 5.74 0.85 -9 -6 0 5.81 0.80 9 6 0 6.73 0.80 9 6 0 5.66 0.78 9 6 0 6.37 0.82 9 6 0 4.63 0.82 -10 -6 0 0.21 0.40 -10 -6 0 -0.10 0.23 -10 -6 0 -0.12 0.31 10 6 0 -0.06 0.32 10 6 0 0.06 0.29 10 6 0 0.14 0.32 10 6 0 -0.02 0.31 10 6 0 0.63 0.60 9 -7 0 0.72 0.53 9 -7 0 0.98 0.49 9 -7 0 0.67 0.37 9 -7 0 1.03 0.19 9 -7 0 0.32 0.32 9 -7 0 0.63 0.16 8 -7 0 19.74 0.82 8 -7 0 19.52 1.47 8 -7 0 16.89 0.97 8 -7 0 20.59 1.40 8 -7 0 17.89 1.05 8 -7 0 19.62 0.77 8 -7 0 18.10 1.06 8 -7 0 17.98 1.07 -8 7 0 19.21 0.74 -8 7 0 19.70 1.42 -8 7 0 18.93 0.75 7 -7 0 42.31 1.89 7 -7 0 46.03 1.47 7 -7 0 46.73 1.41 7 -7 0 47.72 2.16 7 -7 0 46.72 1.65 7 -7 0 43.96 1.62 7 -7 0 46.75 1.67 -7 7 0 48.62 1.44 -7 7 0 48.18 2.20 -7 7 0 48.01 1.50 6 -7 0 21.93 0.98 6 -7 0 22.65 1.61 6 -7 0 22.82 1.07 6 -7 0 23.59 1.02 6 -7 0 24.44 1.45 6 -7 0 25.34 0.99 6 -7 0 24.30 1.02 6 -7 0 24.73 1.37 6 -7 0 23.69 1.46 -6 7 0 23.29 1.46 -6 7 0 24.59 0.99 -6 7 0 26.89 1.06 -6 7 0 23.83 1.16 5 -7 0 11.12 1.01 5 -7 0 13.16 0.69 5 -7 0 12.53 1.23 5 -7 0 13.98 0.82 5 -7 0 15.00 1.00 5 -7 0 12.88 0.62 5 -7 0 14.54 0.72 5 -7 0 12.74 0.63 5 -7 0 14.11 0.66 5 -7 0 13.95 1.07 5 -7 0 13.29 0.67 -5 7 0 13.16 0.53 -5 7 0 13.93 0.86 -5 7 0 13.26 1.06 -5 7 0 13.62 0.56 -5 7 0 13.59 0.93 -5 7 0 12.46 0.73 -5 7 0 13.57 0.75 4 -7 0 26.26 1.02 4 -7 0 27.30 1.29 4 -7 0 25.85 1.32 4 -7 0 29.16 1.30 4 -7 0 26.81 1.00 4 -7 0 25.32 1.39 4 -7 0 27.56 1.89 4 -7 0 26.90 1.03 4 -7 0 26.07 0.79 4 -7 0 25.43 1.10 4 -7 0 27.00 0.82 -4 7 0 27.10 1.17 -4 7 0 26.55 0.94 -4 7 0 26.96 1.20 -4 7 0 26.70 1.62 -4 7 0 26.67 0.91 -4 7 0 25.49 2.02 -4 7 0 27.23 1.08 3 -7 0 66.05 2.09 3 -7 0 65.37 1.89 3 -7 0 65.65 1.97 3 -7 0 64.03 2.24 3 -7 0 65.84 1.88 3 -7 0 62.44 1.86 3 -7 0 66.77 2.23 -3 7 0 66.30 2.01 -3 7 0 64.67 1.96 -3 7 0 64.31 1.94 -3 7 0 62.39 2.25 -3 7 0 64.98 1.79 -3 7 0 66.34 2.00 2 -7 0 73.17 2.38 2 -7 0 63.83 1.95 2 -7 0 64.92 1.94 2 -7 0 65.37 1.91 2 -7 0 63.53 1.92 2 -7 0 63.27 2.16 2 -7 0 67.49 2.18 2 -7 0 65.54 1.90 -2 7 0 65.01 1.84 -2 7 0 64.36 1.97 -2 7 0 69.06 2.23 -2 7 0 65.57 2.00 -2 7 0 63.55 2.13 -2 7 0 66.46 1.99 -2 7 0 63.43 1.84 -2 7 0 63.07 2.17 1 -7 0 28.72 1.28 1 -7 0 28.29 1.15 1 -7 0 28.37 1.17 1 -7 0 28.41 1.28 1 -7 0 28.11 1.18 1 -7 0 27.20 1.14 1 -7 0 28.21 1.12 1 -7 0 29.60 1.15 -1 7 0 28.79 1.17 -1 7 0 27.33 1.25 -1 7 0 27.02 1.07 -1 7 0 26.92 1.17 -1 7 0 28.87 1.13 -1 7 0 29.77 1.23 -1 7 0 28.83 1.25 0 -7 0 7.84 0.60 0 -7 0 6.90 0.61 0 -7 0 7.99 0.71 0 -7 0 6.89 0.59 0 -7 0 5.96 0.93 0 -7 0 6.76 0.61 0 7 0 7.81 0.66 0 7 0 6.56 0.57 0 7 0 6.65 0.63 0 7 0 6.25 0.65 0 7 0 7.46 0.83 0 7 0 7.14 0.59 0 7 0 7.41 0.37 0 7 0 6.91 0.63 -1 -7 0 64.88 2.06 -1 -7 0 61.50 1.88 -1 -7 0 62.75 2.02 -1 -7 0 60.86 2.01 -1 -7 0 63.56 2.46 -1 -7 0 62.35 1.68 -1 -7 0 60.52 1.94 -1 -7 0 61.04 1.91 -1 -7 0 63.69 1.96 1 7 0 60.71 1.97 1 7 0 62.62 1.93 1 7 0 59.29 2.00 1 7 0 63.59 1.91 1 7 0 63.60 1.70 1 7 0 60.82 1.94 1 7 0 64.54 2.09 1 7 0 62.30 1.96 1 7 0 58.78 1.89 -2 -7 0 75.82 2.28 -2 -7 0 73.72 2.06 -2 -7 0 71.08 2.22 -2 -7 0 73.54 2.33 -2 -7 0 75.64 2.25 -2 -7 0 75.58 2.10 -2 -7 0 74.30 2.35 -2 -7 0 75.75 2.36 -2 -7 0 77.92 2.22 2 7 0 74.25 2.25 2 7 0 75.77 2.27 2 7 0 75.77 2.11 2 7 0 72.62 2.21 2 7 0 73.24 2.33 2 7 0 74.64 2.08 2 7 0 76.63 2.41 2 7 0 74.06 2.27 2 7 0 75.53 2.25 -3 -7 0 6.55 0.93 -3 -7 0 6.70 0.60 -3 -7 0 6.15 0.74 -3 -7 0 6.55 0.63 -3 -7 0 6.46 0.45 -3 -7 0 7.11 0.75 -3 -7 0 6.30 0.66 -3 -7 0 6.66 0.61 -3 -7 0 6.53 0.64 3 7 0 6.07 0.69 3 7 0 6.92 0.87 3 7 0 6.71 0.88 3 7 0 6.66 0.65 3 7 0 5.62 0.59 3 7 0 6.22 0.62 3 7 0 6.39 0.62 3 7 0 7.13 0.67 -4 -7 0 1.25 0.38 -4 -7 0 1.37 0.35 -4 -7 0 2.12 0.59 -4 -7 0 1.60 0.37 -4 -7 0 1.04 0.34 -4 -7 0 0.82 0.27 -4 -7 0 1.05 0.16 -4 -7 0 0.79 0.37 -4 -7 0 1.37 0.37 -4 -7 0 1.04 0.17 4 7 0 0.53 0.31 4 7 0 0.82 0.32 4 7 0 1.28 0.34 4 7 0 0.70 0.30 4 7 0 0.91 0.34 4 7 0 1.08 0.31 4 7 0 1.01 0.34 4 7 0 1.13 0.32 -5 -7 0 5.85 0.68 -5 -7 0 4.57 0.59 -5 -7 0 5.49 0.73 -5 -7 0 4.28 0.61 -5 -7 0 5.72 0.71 -5 -7 0 4.79 0.61 -5 -7 0 4.54 0.64 5 7 0 5.96 0.76 5 7 0 5.77 0.66 5 7 0 6.33 1.27 5 7 0 5.84 0.66 5 7 0 5.18 0.69 5 7 0 4.20 0.63 5 7 0 4.96 0.67 5 7 0 5.07 0.68 -6 -7 0 89.08 2.83 -6 -7 0 92.06 2.98 -6 -7 0 92.42 2.95 -6 -7 0 93.69 2.99 -6 -7 0 95.71 3.00 -6 -7 0 86.55 2.90 -6 -7 0 88.73 2.78 6 7 0 94.15 3.10 6 7 0 95.13 2.89 6 7 0 92.20 2.98 6 7 0 96.11 3.35 6 7 0 89.99 2.96 6 7 0 87.31 3.01 6 7 0 87.29 2.81 6 7 0 92.69 2.86 -7 -7 0 34.16 1.59 -7 -7 0 35.09 1.74 -7 -7 0 34.70 1.73 -7 -7 0 35.84 1.71 7 7 0 37.05 1.65 7 7 0 29.40 1.71 7 7 0 35.91 1.85 7 7 0 33.51 1.72 7 7 0 34.41 1.60 7 7 0 36.98 1.81 -8 -7 0 1.83 0.47 -8 -7 0 1.68 0.49 -8 -7 0 1.88 0.51 8 7 0 1.87 0.46 8 7 0 1.66 0.47 8 7 0 1.97 0.59 8 7 0 1.54 0.41 -9 -7 0 19.20 1.33 -9 -7 0 18.25 1.42 -9 -7 0 17.98 1.32 9 7 0 17.53 1.23 9 7 0 18.93 1.25 9 7 0 17.57 1.56 9 7 0 15.14 1.17 9 7 0 16.49 1.20 9 -8 0 23.01 1.22 9 -8 0 19.73 1.19 9 -8 0 20.53 1.20 9 -8 0 22.95 1.63 9 -8 0 22.74 0.83 9 -8 0 23.88 1.19 9 -8 0 24.02 1.88 9 -8 0 23.25 0.82 8 -8 0 19.46 1.51 8 -8 0 17.62 1.00 8 -8 0 17.29 1.02 8 -8 0 17.37 0.99 8 -8 0 16.53 1.15 8 -8 0 19.54 0.81 8 -8 0 19.06 0.87 8 -8 0 17.75 1.38 -8 8 0 20.37 0.81 -8 8 0 18.24 0.84 7 -8 0 4.55 0.46 7 -8 0 4.23 0.80 7 -8 0 4.23 0.52 7 -8 0 4.32 0.75 7 -8 0 3.51 0.65 7 -8 0 4.02 0.54 7 -8 0 5.49 0.54 -7 8 0 4.24 0.51 -7 8 0 4.10 0.77 -7 8 0 5.17 0.51 6 -8 0 2.76 0.32 6 -8 0 2.57 0.38 6 -8 0 2.43 0.32 6 -8 0 2.11 0.43 6 -8 0 2.34 0.51 6 -8 0 2.81 0.41 6 -8 0 2.45 0.35 6 -8 0 2.43 0.38 6 -8 0 2.39 0.60 -6 8 0 1.88 0.58 -6 8 0 2.99 0.42 -6 8 0 2.82 0.48 -6 8 0 2.48 0.41 5 -8 0 9.63 0.75 5 -8 0 10.92 0.63 5 -8 0 9.71 0.65 5 -8 0 10.90 0.70 5 -8 0 8.90 1.00 5 -8 0 11.51 0.52 5 -8 0 10.74 0.70 5 -8 0 10.83 0.98 5 -8 0 10.80 0.52 5 -8 0 10.54 0.97 5 -8 0 10.55 1.02 -5 8 0 10.25 0.53 -5 8 0 9.71 0.56 -5 8 0 9.91 0.84 -5 8 0 9.93 0.71 -5 8 0 10.86 0.81 -5 8 0 11.35 0.73 -5 8 0 10.88 1.05 4 -8 0 10.83 0.88 4 -8 0 10.99 0.94 4 -8 0 10.62 0.68 4 -8 0 9.04 0.89 4 -8 0 9.22 0.92 4 -8 0 10.69 0.66 4 -8 0 10.15 0.66 4 -8 0 9.93 0.67 4 -8 0 9.97 0.74 -4 8 0 11.31 0.81 -4 8 0 10.63 0.58 -4 8 0 9.55 0.97 -4 8 0 10.21 0.70 -4 8 0 10.50 0.74 -4 8 0 10.66 0.61 -4 8 0 10.31 0.77 3 -8 0 32.39 1.42 3 -8 0 31.88 1.53 3 -8 0 31.70 1.78 3 -8 0 30.84 1.22 3 -8 0 32.37 1.32 3 -8 0 33.73 1.25 3 -8 0 31.33 1.22 -3 8 0 32.37 1.32 -3 8 0 30.15 1.30 -3 8 0 30.96 1.13 -3 8 0 31.36 1.29 -3 8 0 32.82 2.29 2 -8 0 0.46 0.34 2 -8 0 1.26 0.35 2 -8 0 1.44 0.34 2 -8 0 1.34 0.41 2 -8 0 1.15 0.29 2 -8 0 0.60 0.23 2 -8 0 0.94 0.28 2 -8 0 1.30 0.32 -2 8 0 0.79 0.32 -2 8 0 1.35 0.28 -2 8 0 0.76 0.23 -2 8 0 1.09 0.30 -2 8 0 0.98 0.31 -2 8 0 1.18 0.38 -2 8 0 1.03 0.42 -2 8 0 1.01 0.30 1 -8 0 49.94 1.71 1 -8 0 47.53 1.69 1 -8 0 48.45 1.72 1 -8 0 49.34 1.68 1 -8 0 49.81 1.66 1 -8 0 47.39 1.70 1 -8 0 48.87 1.84 1 -8 0 52.21 1.88 -1 8 0 47.52 1.60 -1 8 0 51.20 1.81 -1 8 0 43.41 1.80 -1 8 0 48.21 1.73 -1 8 0 47.54 1.84 -1 8 0 48.03 1.65 -1 8 0 48.53 1.71 -1 8 0 48.23 1.79 0 -8 0 74.97 2.36 0 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1.47 -3 -8 0 38.94 1.67 3 8 0 35.55 1.52 3 8 0 36.20 1.49 3 8 0 35.21 1.44 3 8 0 38.08 1.78 3 8 0 37.21 1.65 3 8 0 33.66 1.49 3 8 0 34.83 1.57 3 8 0 35.96 1.51 -4 -8 0 52.62 2.02 -4 -8 0 49.96 1.84 -4 -8 0 48.04 1.85 -4 -8 0 48.74 1.97 -4 -8 0 49.23 1.38 -4 -8 0 48.53 1.97 -4 -8 0 51.11 1.87 -4 -8 0 50.48 1.90 -4 -8 0 48.82 1.39 4 8 0 46.93 1.84 4 8 0 47.84 1.94 4 8 0 50.50 2.01 4 8 0 50.37 1.88 4 8 0 51.74 1.89 4 8 0 49.24 1.90 4 8 0 48.94 1.87 4 8 0 49.73 1.89 -5 -8 0 67.09 2.45 -5 -8 0 68.74 2.30 -5 -8 0 62.83 2.88 -5 -8 0 55.46 2.64 -5 -8 0 65.95 2.32 -5 -8 0 70.13 2.48 -5 -8 0 66.04 2.29 5 8 0 64.38 2.37 5 8 0 68.98 2.36 5 8 0 72.14 2.46 5 8 0 73.13 2.62 5 8 0 66.20 2.41 5 8 0 64.46 2.35 5 8 0 66.66 2.33 -6 -8 0 2.32 0.52 -6 -8 0 2.66 0.61 -6 -8 0 1.34 0.45 -6 -8 0 2.01 0.43 -6 -8 0 2.77 0.74 -6 -8 0 1.80 0.43 -6 -8 0 1.68 0.42 6 8 0 2.45 0.57 6 8 0 1.92 0.45 6 8 0 2.14 0.54 6 8 0 2.68 0.78 6 8 0 2.80 0.61 6 8 0 2.17 0.52 6 8 0 2.28 0.50 6 8 0 2.13 0.49 -7 -8 0 5.90 0.82 -7 -8 0 4.25 0.66 -7 -8 0 3.60 0.84 7 8 0 5.45 0.77 7 8 0 4.37 0.63 7 8 0 5.35 0.80 7 8 0 5.01 0.83 7 8 0 4.04 0.62 -8 -8 0 22.42 1.45 -8 -8 0 21.81 1.49 -8 -8 0 23.31 1.46 8 8 0 22.87 1.38 8 8 0 20.91 1.34 8 8 0 22.13 1.37 8 8 0 22.26 1.44 8 8 0 20.18 1.59 -9 -8 0 34.05 1.95 -9 -8 0 27.84 2.26 -9 -8 0 30.47 1.74 9 8 0 31.37 1.66 9 8 0 29.79 2.13 9 8 0 30.19 1.67 9 8 0 27.11 1.64 9 8 0 27.07 2.43 8 -9 0 0.31 0.26 8 -9 0 0.51 0.49 8 -9 0 0.64 0.23 8 -9 0 0.93 0.26 8 -9 0 1.04 0.59 8 -9 0 0.51 0.55 8 -9 0 1.19 0.34 -8 9 0 1.25 0.30 7 -9 0 10.31 0.84 7 -9 0 9.76 0.61 7 -9 0 10.75 0.68 7 -9 0 9.34 0.69 7 -9 0 10.60 0.64 7 -9 0 8.63 1.02 -7 9 0 8.10 0.84 -7 9 0 11.76 1.22 -7 9 0 10.97 0.73 -7 9 0 9.68 0.89 6 -9 0 36.27 1.08 6 -9 0 34.98 1.52 6 -9 0 35.73 1.85 6 -9 0 38.99 1.43 6 -9 0 36.42 1.18 6 -9 0 39.43 1.98 6 -9 0 36.70 1.11 6 -9 0 38.13 1.39 -6 9 0 39.25 2.04 -6 9 0 38.38 1.45 -6 9 0 39.73 1.75 -6 9 0 38.75 1.50 5 -9 0 28.21 1.49 5 -9 0 29.62 1.21 5 -9 0 26.24 1.16 5 -9 0 27.28 1.29 5 -9 0 28.02 1.62 5 -9 0 26.54 1.09 -5 9 0 28.48 1.39 -5 9 0 26.92 1.23 -5 9 0 26.21 1.05 -5 9 0 25.95 1.55 -5 9 0 26.60 1.65 -5 9 0 26.64 0.97 -5 9 0 27.56 1.24 4 -9 0 -0.18 0.32 4 -9 0 0.15 0.36 4 -9 0 -0.24 0.27 4 -9 0 -0.26 0.18 4 -9 0 0.08 0.33 4 -9 0 -0.18 0.23 4 -9 0 0.36 0.36 4 -9 0 0.11 0.21 4 -9 0 -0.05 0.22 -4 9 0 -0.38 0.23 -4 9 0 -0.25 0.14 -4 9 0 -0.24 0.15 -4 9 0 -0.34 0.21 -4 9 0 -0.17 0.18 -4 9 0 -0.15 0.36 -4 9 0 -0.22 0.25 3 -9 0 13.82 1.01 3 -9 0 15.23 1.35 3 -9 0 15.75 0.89 3 -9 0 15.86 1.13 3 -9 0 14.62 1.03 3 -9 0 13.30 0.91 3 -9 0 13.66 0.86 3 -9 0 12.89 0.84 -3 9 0 14.73 0.94 -3 9 0 14.29 0.95 -3 9 0 13.17 0.76 -3 9 0 13.14 1.06 -3 9 0 14.41 0.91 -3 9 0 13.28 0.88 2 -9 0 71.78 2.28 2 -9 0 69.83 2.25 2 -9 0 74.34 2.52 2 -9 0 74.47 2.37 2 -9 0 69.66 2.52 2 -9 0 71.78 2.21 2 -9 0 66.43 2.51 2 -9 0 72.50 2.27 -2 9 0 73.84 2.63 -2 9 0 71.12 2.71 -2 9 0 69.39 2.12 -2 9 0 73.93 2.32 -2 9 0 71.72 2.22 -2 9 0 69.84 2.46 -2 9 0 67.56 2.11 1 -9 0 66.65 2.22 1 -9 0 68.94 2.17 1 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2.73 2 9 0 89.89 2.57 2 9 0 88.65 2.80 2 9 0 87.85 2.86 2 9 0 93.20 2.82 2 9 0 88.89 2.73 2 9 0 86.64 2.74 -3 -9 0 59.64 1.84 -3 -9 0 59.19 2.06 -3 -9 0 60.47 2.13 -3 -9 0 59.56 2.25 -3 -9 0 60.65 2.15 -3 -9 0 61.38 2.16 3 9 0 59.03 2.29 3 9 0 60.25 2.13 3 9 0 60.66 2.18 3 9 0 58.90 2.28 3 9 0 59.24 2.13 3 9 0 61.54 2.18 3 9 0 61.51 2.01 -4 -9 0 9.90 0.58 -4 -9 0 9.54 0.87 -4 -9 0 9.85 1.00 -4 -9 0 9.62 0.58 -4 -9 0 10.72 0.86 -4 -9 0 10.76 0.90 -4 -9 0 13.29 1.26 -4 -9 0 10.30 0.94 -4 -9 0 9.44 0.86 4 9 0 10.43 0.90 4 9 0 9.52 0.85 4 9 0 10.80 0.93 4 9 0 10.75 0.98 4 9 0 10.02 0.88 4 9 0 10.44 0.99 4 9 0 11.21 0.96 4 9 0 10.04 0.89 -5 -9 0 0.06 0.25 -5 -9 0 -0.25 0.12 -5 -9 0 0.02 0.36 -5 -9 0 -0.25 0.36 -5 -9 0 -0.14 0.24 -5 -9 0 -0.03 0.28 -5 -9 0 0.15 0.26 -5 -9 0 -0.21 0.24 5 9 0 0.27 0.29 5 9 0 0.20 0.38 5 9 0 -0.26 0.59 5 9 0 0.14 0.37 5 9 0 -0.15 0.28 5 9 0 0.18 0.28 5 9 0 0.02 0.33 5 9 0 -0.30 0.32 -6 -9 0 31.75 1.67 -6 -9 0 28.32 1.61 -6 -9 0 29.65 1.68 -6 -9 0 30.36 1.57 -6 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7.47 1.01 -5 10 0 6.43 0.84 -5 10 0 6.49 0.74 -5 10 0 6.70 0.54 4 -10 0 8.69 0.75 4 -10 0 8.10 0.83 4 -10 0 8.72 1.02 4 -10 0 9.90 0.76 4 -10 0 9.08 0.96 4 -10 0 9.78 0.79 -4 10 0 7.97 0.63 -4 10 0 9.50 0.84 -4 10 0 9.12 1.06 -4 10 0 8.05 0.80 -4 10 0 8.63 0.82 -4 10 0 8.29 0.77 3 -10 0 45.04 1.72 3 -10 0 44.16 2.08 3 -10 0 46.35 1.74 3 -10 0 43.74 1.69 3 -10 0 43.55 1.96 3 -10 0 47.75 1.88 3 -10 0 46.90 2.09 3 -10 0 45.05 1.79 -3 10 0 44.78 1.78 -3 10 0 45.94 1.59 -3 10 0 47.56 1.84 -3 10 0 45.25 2.10 -3 10 0 43.03 1.73 -3 10 0 44.89 1.80 2 -10 0 14.93 1.15 2 -10 0 14.65 1.00 2 -10 0 15.42 1.06 2 -10 0 15.83 0.99 2 -10 0 13.69 1.55 2 -10 0 14.54 0.95 2 -10 0 15.10 1.01 -2 10 0 13.95 1.04 -2 10 0 15.38 0.96 -2 10 0 13.78 1.12 -2 10 0 14.75 0.86 -2 10 0 13.18 1.03 -2 10 0 14.24 1.00 -2 10 0 13.11 1.11 1 -10 0 10.89 0.95 1 -10 0 11.27 1.04 1 -10 0 10.53 0.89 1 -10 0 11.87 0.86 1 -10 0 10.71 0.85 1 -10 0 13.03 0.92 1 -10 0 11.71 0.89 1 -10 0 12.00 0.91 -1 10 0 12.22 0.85 -1 10 0 12.27 0.93 -1 10 0 10.20 0.78 -1 10 0 11.79 1.07 -1 10 0 11.58 0.97 -1 10 0 11.91 0.91 -1 10 0 11.42 1.01 -1 10 0 11.17 0.81 0 -10 0 51.89 1.99 0 -10 0 49.41 1.92 0 -10 0 54.13 2.13 0 -10 0 49.39 1.90 0 -10 0 50.39 1.88 0 -10 0 51.14 1.98 0 -10 0 51.57 2.01 0 -10 0 53.18 1.88 0 10 0 51.24 1.87 0 10 0 49.29 1.27 0 10 0 48.74 1.84 0 10 0 51.59 2.02 0 10 0 52.39 2.08 0 10 0 52.10 1.97 0 10 0 50.14 1.84 0 10 0 50.10 2.02 0 10 0 51.36 2.02 0 10 0 51.20 1.30 -1 -10 0 141.24 3.91 -1 -10 0 143.48 4.70 -1 -10 0 148.88 4.17 -1 -10 0 137.79 3.87 -1 -10 0 146.47 3.99 -1 -10 0 144.85 3.83 -1 -10 0 142.51 4.07 -1 -10 0 142.94 4.06 1 10 0 139.85 3.89 1 10 0 140.37 4.02 1 10 0 143.02 3.92 1 10 0 146.71 4.17 1 10 0 143.62 3.99 1 10 0 143.84 3.91 1 10 0 143.28 3.93 1 10 0 145.40 4.11 1 10 0 140.99 3.40 -2 -10 0 35.79 1.74 -2 -10 0 34.46 1.93 -2 -10 0 35.43 1.67 -2 -10 0 29.63 1.51 -2 -10 0 35.08 1.67 -2 -10 0 36.52 1.46 -2 -10 0 35.01 1.59 -2 -10 0 35.72 1.51 2 10 0 33.84 1.73 2 10 0 34.26 2.05 2 10 0 34.55 1.60 2 10 0 33.27 1.60 2 10 0 34.69 1.56 2 10 0 33.04 1.51 2 10 0 32.39 1.55 -3 -10 0 2.36 0.49 -3 -10 0 1.18 0.50 -3 -10 0 1.40 0.44 -3 -10 0 1.19 0.37 -3 -10 0 2.07 0.51 -3 -10 0 2.06 0.43 -3 -10 0 1.51 0.35 -3 -10 0 2.01 0.64 3 10 0 1.90 0.48 3 10 0 2.02 0.59 3 10 0 1.46 0.41 3 10 0 1.70 0.64 3 10 0 1.55 0.39 3 10 0 1.23 0.38 3 10 0 2.45 0.53 -4 -10 0 15.21 0.79 -4 -10 0 16.15 1.12 -4 -10 0 15.56 1.13 -4 -10 0 15.48 1.10 -4 -10 0 14.61 1.26 -4 -10 0 15.82 1.22 -4 -10 0 15.70 1.21 -4 -10 0 15.53 0.79 -4 -10 0 16.61 1.11 4 10 0 15.86 1.13 4 10 0 16.63 1.17 4 10 0 13.77 1.14 4 10 0 16.09 1.61 4 10 0 16.24 1.32 4 10 0 16.69 1.14 4 10 0 15.47 1.28 -5 -10 0 40.92 2.36 -5 -10 0 42.06 1.23 -5 -10 0 45.72 1.97 -5 -10 0 46.88 2.12 -5 -10 0 48.17 2.34 5 10 0 44.55 2.31 5 10 0 47.11 1.99 5 10 0 45.50 2.01 5 10 0 46.18 2.14 5 10 0 45.87 1.96 5 10 0 44.29 1.97 5 10 0 49.18 2.05 5 10 0 37.85 2.20 -6 -10 0 25.75 2.12 -6 -10 0 25.55 1.58 -6 -10 0 28.50 1.55 -6 -10 0 24.23 1.52 6 10 0 28.28 1.56 6 10 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54.87 2.24 0 11 0 58.43 2.19 0 11 0 57.21 2.24 0 11 0 53.98 2.03 0 11 0 59.71 2.36 0 11 0 54.96 2.49 0 11 0 55.80 2.06 0 11 0 52.93 2.19 -1 -11 0 5.00 0.76 -1 -11 0 6.50 0.80 -1 -11 0 8.16 1.16 -1 -11 0 6.80 0.77 -1 -11 0 5.59 0.80 -1 -11 0 6.69 0.80 -1 -11 0 7.11 0.90 1 11 0 5.63 0.90 1 11 0 3.64 0.57 1 11 0 5.10 0.46 1 11 0 5.30 0.80 1 11 0 5.30 1.01 1 11 0 5.57 0.47 1 11 0 5.70 0.80 1 11 0 6.35 0.75 1 11 0 5.16 0.72 -2 -11 0 0.28 0.30 -2 -11 0 1.14 0.40 -2 -11 0 0.88 0.36 -2 -11 0 0.89 0.39 -2 -11 0 0.17 0.44 -2 -11 0 0.50 0.44 -2 -11 0 1.42 0.40 -2 -11 0 0.41 0.49 2 11 0 1.21 0.39 2 11 0 0.58 0.43 2 11 0 1.31 0.48 2 11 0 0.99 0.30 2 11 0 0.27 0.36 2 11 0 0.91 0.40 2 11 0 0.70 0.33 2 11 0 0.20 0.34 -3 -11 0 41.64 1.76 -3 -11 0 40.96 1.96 -3 -11 0 39.55 1.84 -3 -11 0 42.06 1.85 -3 -11 0 38.43 2.04 -3 -11 0 41.43 1.98 -3 -11 0 40.32 1.57 3 11 0 39.74 1.59 3 11 0 40.63 1.83 3 11 0 43.03 1.91 3 11 0 38.30 1.98 3 11 0 39.62 1.93 3 11 0 39.95 1.82 3 11 0 39.58 1.86 -4 -11 0 65.73 2.32 -4 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36.52 1.77 -1 -12 0 37.75 1.66 -1 -12 0 35.29 1.82 -1 -12 0 36.24 1.79 -1 -12 0 34.70 1.70 -1 -12 0 37.94 1.87 -1 -12 0 38.16 1.95 1 12 0 36.44 1.87 1 12 0 34.76 1.16 1 12 0 38.15 1.80 1 12 0 38.14 1.76 1 12 0 33.12 1.68 1 12 0 38.11 1.95 -2 -12 0 87.15 3.45 -2 -12 0 86.63 3.15 -2 -12 0 90.41 3.19 -2 -12 0 93.06 3.27 -2 -12 0 82.92 2.92 -2 -12 0 88.77 2.85 -2 -12 0 88.56 2.85 2 12 0 93.18 3.82 2 12 0 89.17 3.27 2 12 0 85.21 2.45 2 12 0 87.79 3.04 2 12 0 86.54 3.15 2 12 0 87.43 2.48 2 12 0 83.43 3.50 2 12 0 80.90 3.05 -3 -12 0 52.35 2.42 -3 -12 0 52.80 1.96 -3 -12 0 54.12 1.99 -3 -12 0 54.18 2.32 -3 -12 0 53.18 2.38 -3 -12 0 55.73 2.43 -3 -12 0 57.06 2.28 -3 -12 0 55.85 2.31 3 12 0 52.73 2.25 3 12 0 56.07 2.33 3 12 0 52.57 1.90 3 12 0 57.31 2.52 3 12 0 50.02 2.19 3 12 0 57.43 2.29 3 12 0 55.86 1.95 -4 -12 0 6.44 0.95 -4 -12 0 9.79 0.72 -4 -12 0 8.50 0.89 -4 -12 0 7.41 0.97 -4 -12 0 6.87 1.39 -4 -12 0 9.22 1.11 4 12 0 8.80 1.11 4 12 0 9.60 1.03 4 12 0 5.90 1.16 4 12 0 7.50 0.83 4 12 0 7.49 0.99 4 12 0 9.09 1.29 4 12 0 9.26 0.86 -5 -12 0 16.91 1.47 -5 -12 0 22.38 1.78 -5 -12 0 16.91 1.22 -5 -12 0 15.21 1.34 5 12 0 16.61 1.79 5 12 0 16.81 1.33 5 12 0 16.27 1.28 5 12 0 16.79 2.05 5 12 0 17.95 1.46 5 12 0 15.75 1.20 5 12 0 17.39 1.32 -6 -12 0 45.15 2.31 -6 -12 0 42.39 2.08 -6 -12 0 47.64 2.33 6 12 0 45.86 2.19 6 12 0 45.29 2.17 6 12 0 46.00 2.20 6 12 0 46.16 2.14 6 12 0 45.78 2.36 5 -13 0 3.49 0.79 5 -13 0 2.88 0.49 5 -13 0 2.94 0.56 5 -13 0 3.15 0.52 5 -13 0 1.78 0.54 -5 13 0 3.31 0.73 -5 13 0 3.19 0.63 4 -13 0 14.38 1.10 4 -13 0 11.87 1.30 4 -13 0 12.71 1.17 4 -13 0 13.03 1.04 4 -13 0 13.06 1.06 -4 13 0 12.00 1.32 -4 13 0 12.29 1.07 -4 13 0 14.75 1.17 3 -13 0 48.10 2.51 3 -13 0 46.75 2.02 3 -13 0 46.91 1.99 3 -13 0 46.05 1.97 3 -13 0 47.58 2.39 -3 13 0 47.03 2.09 -3 13 0 43.92 1.95 -3 13 0 50.33 2.45 -3 13 0 47.97 2.19 2 -13 0 5.90 0.84 2 -13 0 6.70 0.90 2 -13 0 7.27 1.08 2 -13 0 7.67 0.90 2 -13 0 8.49 0.89 -2 13 0 7.43 1.00 -2 13 0 6.63 0.88 -2 13 0 7.19 1.01 -2 13 0 4.90 0.72 1 -13 0 12.66 1.07 1 -13 0 11.22 1.23 1 -13 0 13.38 1.49 1 -13 0 13.60 1.11 1 -13 0 13.46 1.09 -1 13 0 12.56 1.12 -1 13 0 11.04 1.02 -1 13 0 14.36 1.24 0 -13 0 30.02 1.64 0 -13 0 28.78 1.57 0 -13 0 30.95 1.84 0 -13 0 30.82 1.72 0 -13 0 31.93 1.57 0 13 0 31.07 1.59 0 13 0 29.96 1.78 0 13 0 29.61 1.66 -1 -13 0 28.90 1.79 -1 -13 0 27.76 1.48 -1 -13 0 28.56 1.63 -1 -13 0 29.88 1.73 -1 -13 0 27.81 1.59 -1 -13 0 28.81 1.60 1 13 0 25.95 1.53 1 13 0 30.10 1.67 1 13 0 30.54 2.09 -2 -13 0 1.28 0.50 -2 -13 0 1.25 0.51 -2 -13 0 1.08 0.41 -2 -13 0 2.06 0.56 -2 -13 0 2.49 0.89 -2 -13 0 1.73 0.62 -2 -13 0 0.68 0.56 2 13 0 1.19 0.54 2 13 0 2.14 0.58 2 13 0 0.78 0.50 2 13 0 1.84 0.55 2 13 0 1.38 0.32 2 13 0 1.18 0.48 -3 -13 0 0.68 0.48 -3 -13 0 0.76 0.37 -3 -13 0 0.49 0.29 -3 -13 0 0.71 0.42 -3 -13 0 0.43 0.39 -3 -13 0 1.07 0.45 -3 -13 0 0.15 0.54 -3 -13 0 1.01 0.39 3 13 0 1.31 0.59 3 13 0 0.67 0.32 3 13 0 0.46 0.69 3 13 0 1.25 0.52 3 13 0 -0.02 0.20 3 13 0 0.51 0.50 -4 -13 0 6.36 1.13 -4 -13 0 3.50 0.62 -4 -13 0 4.96 0.75 -4 -13 0 2.89 0.80 4 13 0 2.23 0.62 4 13 0 4.45 0.80 4 13 0 2.80 0.53 4 13 0 4.24 0.95 4 13 0 3.33 0.70 -5 -13 0 18.55 1.29 -5 -13 0 15.07 1.48 5 13 0 19.99 1.60 5 13 0 17.73 1.52 5 13 0 16.31 2.04 5 13 0 17.39 1.25 4 -14 0 2.88 0.58 4 -14 0 2.38 0.60 4 -14 0 1.48 0.66 4 -14 0 2.81 0.56 4 -14 0 2.55 0.70 -4 14 0 2.82 0.60 -4 14 0 1.42 0.47 3 -14 0 1.32 0.47 3 -14 0 1.69 0.97 3 -14 0 0.10 0.31 3 -14 0 0.40 0.37 3 -14 0 0.65 0.43 -3 14 0 0.38 0.39 -3 14 0 0.10 0.24 -3 14 0 -0.06 0.21 -3 14 0 0.96 0.47 2 -14 0 32.35 1.69 2 -14 0 28.63 1.63 2 -14 0 31.83 2.02 2 -14 0 31.38 1.72 2 -14 0 32.24 1.74 -2 14 0 30.89 1.75 -2 14 0 32.99 1.92 1 -14 0 38.21 2.67 1 -14 0 38.78 1.92 1 -14 0 38.24 1.84 1 -14 0 41.23 1.98 1 -14 0 39.55 2.21 -1 14 0 40.44 2.00 -1 14 0 44.03 2.19 0 -14 0 21.93 1.69 0 -14 0 21.56 1.46 0 -14 0 24.13 1.42 0 -14 0 23.31 1.59 0 -14 0 21.92 1.48 0 14 0 24.68 1.56 0 14 0 23.77 1.68 -1 -14 0 -0.10 0.33 -1 -14 0 -0.18 0.31 -1 -14 0 0.14 0.38 -1 -14 0 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