data_PO19124_029 _audit_creation_method 'SHELXL-2018/3' _shelx_SHELXL_version_number '2018/3' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C20 H21 Cl3 Ir N O' _chemical_formula_weight 589.93 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0021 0.0012 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0044 0.0025 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0080 0.0047 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.1230 0.1255 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Ir' 'Ir' -0.7638 6.5985 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system orthorhombic _space_group_IT_number 29 _space_group_name_H-M_alt 'P c a 21' _space_group_name_Hall 'P 2c -2ac' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y, z' '-x+1/2, y, z+1/2' _cell_length_a 18.032(4) _cell_length_b 7.5130(15) _cell_length_c 14.966(3) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 2027.5(7) _cell_formula_units_Z 4 _cell_measurement_temperature 243(2) _cell_measurement_reflns_used 56592 _cell_measurement_theta_min 0.361 _cell_measurement_theta_max 33.548 _exptl_crystal_description 'plate' _exptl_crystal_colour 'orange' _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.933 _exptl_crystal_F_000 1136 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.052 _exptl_crystal_size_mid 0.040 _exptl_crystal_size_min 0.021 _exptl_absorpt_coefficient_mu 5.092 _shelx_estimated_absorpt_T_min 0.778 _shelx_estimated_absorpt_T_max 0.901 _exptl_absorpt_correction_type empirical _exptl_absorpt_correction_T_min 0.916 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_process_details 'HKL3000sm Scalepack' _exptl_absorpt_special_details ? _diffrn_ambient_temperature 243(2) _diffrn_radiation_wavelength 0.630 _diffrn_radiation_type synchrotron _diffrn_source 'PLSII 2D bending magnet' _diffrn_measurement_device_type 'Rayonix MX225HS CCD area detector' _diffrn_measurement_method 'omega scan' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 17646 _diffrn_reflns_av_unetI/netI 0.0358 _diffrn_reflns_av_R_equivalents 0.0539 _diffrn_reflns_limit_h_min -24 _diffrn_reflns_limit_h_max 24 _diffrn_reflns_limit_k_min -9 _diffrn_reflns_limit_k_max 9 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_limit_l_max 20 _diffrn_reflns_theta_min 2.002 _diffrn_reflns_theta_max 24.998 _diffrn_reflns_theta_full 22.210 _diffrn_measured_fraction_theta_max 0.995 _diffrn_measured_fraction_theta_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.995 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.993 _diffrn_reflns_point_group_measured_fraction_full 0.998 _reflns_number_total 5085 _reflns_number_gt 4873 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.922 _reflns_Friedel_fraction_max 0.991 _reflns_Friedel_fraction_full 0.997 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'PAL BL2D-SMDC Program' _computing_cell_refinement 'HKL3000sm' _computing_data_reduction 'HKL3000sm' _computing_structure_solution SHELXS _computing_structure_refinement SHELXL _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0288P)^2^] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_abs_structure_details ; Flack x determined using 2264 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.011(3) _chemical_absolute_configuration ? _refine_ls_number_reflns 5085 _refine_ls_number_parameters 241 _refine_ls_number_restraints 1 _refine_ls_R_factor_all 0.0221 _refine_ls_R_factor_gt 0.0212 _refine_ls_wR_factor_ref 0.0540 _refine_ls_wR_factor_gt 0.0536 _refine_ls_goodness_of_fit_ref 1.045 _refine_ls_restrained_S_all 1.045 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.48243(15) 0.7342(4) 0.4590(2) 0.0288(7) Uani 1 1 d . . . . . Ir01 Ir 0.39168(2) 0.60674(2) 0.40113(2) 0.02258(6) Uani 1 1 d . . . . . C2 C 0.4691(2) 0.7979(5) 0.5387(3) 0.0248(9) Uani 1 1 d . . . . . C3 C 0.5234(3) 0.8663(7) 0.5942(4) 0.0331(11) Uani 1 1 d . . . . . C4 C 0.5073(3) 0.9435(8) 0.6781(4) 0.0404(12) Uani 1 1 d . . . . . H4 H 0.545517 0.989771 0.713932 0.048 Uiso 1 1 calc R U . . . C5 C 0.4352(3) 0.9499(7) 0.7064(3) 0.0384(11) Uani 1 1 d . . . . . C6 C 0.3764(4) 0.8785(6) 0.6540(4) 0.0306(11) Uani 1 1 d . . . . . C7 C 0.3952(2) 0.8007(6) 0.5727(3) 0.0246(9) Uani 1 1 d . . . . . N8 N 0.34317(19) 0.7258(5) 0.5156(2) 0.0230(7) Uani 1 1 d . . . . . C9 C 0.2709(2) 0.7434(7) 0.5368(3) 0.0292(9) Uani 1 1 d . . . . . C10 C 0.2500(3) 0.8222(7) 0.6177(4) 0.0357(11) Uani 1 1 d . . . . . H10 H 0.199364 0.831271 0.631689 0.043 Uiso 1 1 calc R U . . . C11 C 0.3010(4) 0.8862(6) 0.6768(4) 0.0384(13) Uani 1 1 d . . . . . H11 H 0.285879 0.934659 0.731827 0.046 Uiso 1 1 calc R U . . . Cl12 Cl 0.61427(7) 0.8662(3) 0.55605(16) 0.0504(4) Uani 1 1 d . . . . . Cl13 Cl 0.41631(12) 1.0453(2) 0.80996(10) 0.0625(4) Uani 1 1 d . . . . . C14 C 0.2131(3) 0.6818(8) 0.4717(4) 0.0414(13) Uani 1 1 d . . . . . H14A H 0.167306 0.746109 0.482181 0.062 Uiso 1 1 calc R U . . . H14B H 0.204591 0.555275 0.479650 0.062 Uiso 1 1 calc R U . . . H14C H 0.230083 0.704032 0.411224 0.062 Uiso 1 1 calc R U . . . Cl15 Cl 0.35707(8) 0.88334(13) 0.33117(9) 0.0327(3) Uani 1 1 d . . . . . C16 C 0.4059(3) 0.4593(7) 0.2792(3) 0.0343(10) Uani 1 1 d . . . . . C17 C 0.4645(3) 0.4183(6) 0.3386(4) 0.0331(11) Uani 1 1 d . . . . . C18 C 0.4327(3) 0.3418(7) 0.4185(3) 0.0359(13) Uani 1 1 d . . . . . C19 C 0.3539(3) 0.3319(6) 0.4078(6) 0.0385(11) Uani 1 1 d . . . . . C20 C 0.3363(4) 0.4095(7) 0.3190(4) 0.0376(13) Uani 1 1 d . . . . . C21 C 0.4161(4) 0.5415(9) 0.1887(4) 0.0546(16) Uani 1 1 d . . . . . H21A H 0.448268 0.466635 0.152858 0.082 Uiso 1 1 calc R U . . . H21B H 0.438221 0.658428 0.195114 0.082 Uiso 1 1 calc R U . . . H21C H 0.368243 0.552589 0.159472 0.082 Uiso 1 1 calc R U . . . C22 C 0.5455(3) 0.4556(9) 0.3248(5) 0.0519(15) Uani 1 1 d . . . . . H22A H 0.573698 0.347460 0.334747 0.078 Uiso 1 1 calc R U . . . H22B H 0.561533 0.546350 0.366661 0.078 Uiso 1 1 calc R U . . . H22C H 0.553479 0.496990 0.264221 0.078 Uiso 1 1 calc R U . . . C23 C 0.4758(5) 0.2722(10) 0.4952(5) 0.066(2) Uani 1 1 d . . . . . H23A H 0.495458 0.155708 0.480399 0.099 Uiso 1 1 calc R U . . . H23B H 0.443823 0.262717 0.547076 0.099 Uiso 1 1 calc R U . . . H23C H 0.516445 0.352747 0.508304 0.099 Uiso 1 1 calc R U . . . C24 C 0.3014(4) 0.2519(9) 0.4711(5) 0.0628(18) Uani 1 1 d . . . . . H24A H 0.306911 0.123441 0.470345 0.094 Uiso 1 1 calc R U . . . H24B H 0.251166 0.283137 0.454099 0.094 Uiso 1 1 calc R U . . . H24C H 0.311455 0.296156 0.530798 0.094 Uiso 1 1 calc R U . . . C25 C 0.2626(4) 0.4070(9) 0.2733(6) 0.069(2) Uani 1 1 d . . . . . H25A H 0.264227 0.324519 0.223524 0.103 Uiso 1 1 calc R U . . . H25B H 0.251106 0.525404 0.251495 0.103 Uiso 1 1 calc R U . . . H25C H 0.224750 0.369579 0.315328 0.103 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0180(13) 0.0425(17) 0.0259(15) -0.0022(15) 0.0015(11) -0.0047(13) Ir01 0.02061(9) 0.02668(10) 0.02045(9) -0.00083(10) -0.00120(11) -0.00112(4) C2 0.025(2) 0.024(2) 0.025(2) 0.0036(16) -0.0059(16) -0.0009(17) C3 0.031(3) 0.035(2) 0.033(3) 0.005(2) -0.011(2) -0.005(2) C4 0.053(3) 0.034(2) 0.033(3) 0.002(2) -0.018(2) -0.009(3) C5 0.061(3) 0.030(2) 0.024(2) -0.006(2) -0.008(2) -0.002(3) C6 0.041(3) 0.030(2) 0.021(2) 0.0005(18) 0.002(2) 0.000(2) C7 0.028(2) 0.026(2) 0.019(2) 0.0009(19) -0.0006(15) 0.0002(16) N8 0.0210(17) 0.0269(17) 0.0212(17) 0.0013(15) -0.0009(13) -0.0001(14) C9 0.022(2) 0.034(2) 0.032(2) 0.003(2) 0.0035(17) 0.000(2) C10 0.031(3) 0.036(3) 0.039(2) 0.004(2) 0.009(2) 0.003(2) C11 0.046(3) 0.040(3) 0.029(3) 0.001(2) 0.007(3) 0.006(2) Cl12 0.0270(7) 0.0648(10) 0.0593(11) 0.0074(8) -0.0115(6) -0.0152(6) Cl13 0.1008(13) 0.0567(9) 0.0299(7) -0.0165(7) -0.0074(8) 0.0005(11) C14 0.020(2) 0.057(3) 0.047(3) -0.006(3) 0.000(2) -0.001(2) Cl15 0.0380(7) 0.0312(5) 0.0288(6) 0.0044(4) 0.0013(5) 0.0015(4) C16 0.050(3) 0.031(3) 0.023(2) -0.005(2) 0.001(2) 0.005(2) C17 0.037(3) 0.024(2) 0.038(3) -0.005(2) 0.000(2) 0.0049(19) C18 0.051(3) 0.029(2) 0.027(4) -0.002(2) -0.001(2) -0.002(2) C19 0.043(2) 0.028(2) 0.045(3) -0.001(3) -0.003(4) -0.0033(19) C20 0.043(3) 0.033(3) 0.037(3) -0.006(2) -0.007(3) -0.002(2) C21 0.093(5) 0.047(4) 0.024(3) -0.004(3) 0.003(3) 0.016(4) C22 0.039(3) 0.047(3) 0.069(4) -0.005(3) 0.012(3) 0.010(3) C23 0.088(5) 0.059(4) 0.052(4) 0.016(4) -0.009(4) 0.020(4) C24 0.067(4) 0.047(3) 0.075(5) 0.005(4) 0.028(4) -0.011(3) C25 0.052(4) 0.067(5) 0.087(6) -0.032(4) -0.032(4) 0.003(3) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C2 1.308(5) . ? O1 Ir01 2.084(3) . ? Ir01 N8 2.121(4) . ? Ir01 C18 2.139(5) . ? Ir01 C17 2.146(5) . ? Ir01 C16 2.150(5) . ? Ir01 C20 2.168(5) . ? Ir01 C19 2.177(5) . ? Ir01 Cl15 2.4092(12) . ? C2 C3 1.383(6) . ? C2 C7 1.426(6) . ? C3 C4 1.414(8) . ? C3 Cl12 1.735(6) . ? C4 C5 1.368(9) . ? C4 H4 0.9400 . ? C5 C6 1.423(8) . ? C5 Cl13 1.742(5) . ? C6 C7 1.393(7) . ? C6 C11 1.403(9) . ? C7 N8 1.389(6) . ? N8 C9 1.347(5) . ? C9 C10 1.400(7) . ? C9 C14 1.500(7) . ? C10 C11 1.363(8) . ? C10 H10 0.9400 . ? C11 H11 0.9400 . ? C14 H14A 0.9700 . ? C14 H14B 0.9700 . ? C14 H14C 0.9700 . ? C16 C17 1.415(8) . ? C16 C20 1.438(8) . ? C16 C21 1.500(8) . ? C17 C18 1.446(8) . ? C17 C22 1.501(8) . ? C18 C19 1.431(8) . ? C18 C23 1.482(8) . ? C19 C24 1.468(10) . ? C19 C20 1.485(10) . ? C20 C25 1.494(9) . ? C21 H21A 0.9700 . ? C21 H21B 0.9700 . ? C21 H21C 0.9700 . ? C22 H22A 0.9700 . ? C22 H22B 0.9700 . ? C22 H22C 0.9700 . ? C23 H23A 0.9700 . ? C23 H23B 0.9700 . ? C23 H23C 0.9700 . ? C24 H24A 0.9700 . ? C24 H24B 0.9700 . ? C24 H24C 0.9700 . ? C25 H25A 0.9700 . ? C25 H25B 0.9700 . ? C25 H25C 0.9700 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C2 O1 Ir01 113.8(3) . . ? O1 Ir01 N8 78.15(12) . . ? O1 Ir01 C18 96.06(18) . . ? N8 Ir01 C18 115.89(16) . . ? O1 Ir01 C17 90.21(17) . . ? N8 Ir01 C17 151.98(19) . . ? C18 Ir01 C17 39.4(2) . . ? O1 Ir01 C16 119.72(17) . . ? N8 Ir01 C16 162.13(18) . . ? C18 Ir01 C16 65.34(19) . . ? C17 Ir01 C16 38.5(2) . . ? O1 Ir01 C20 155.60(19) . . ? N8 Ir01 C20 123.8(2) . . ? C18 Ir01 C20 65.9(2) . . ? C17 Ir01 C20 65.4(2) . . ? C16 Ir01 C20 38.9(2) . . ? O1 Ir01 C19 131.48(19) . . ? N8 Ir01 C19 103.5(2) . . ? C18 Ir01 C19 38.7(2) . . ? C17 Ir01 C19 65.5(2) . . ? C16 Ir01 C19 65.6(3) . . ? C20 Ir01 C19 40.0(3) . . ? O1 Ir01 Cl15 89.30(10) . . ? N8 Ir01 Cl15 83.13(10) . . ? C18 Ir01 Cl15 160.91(13) . . ? C17 Ir01 Cl15 122.56(16) . . ? C16 Ir01 Cl15 96.11(15) . . ? C20 Ir01 Cl15 102.94(15) . . ? C19 Ir01 Cl15 139.22(18) . . ? O1 C2 C3 123.6(4) . . ? O1 C2 C7 120.2(4) . . ? C3 C2 C7 116.2(4) . . ? C2 C3 C4 122.7(5) . . ? C2 C3 Cl12 118.1(4) . . ? C4 C3 Cl12 119.1(4) . . ? C5 C4 C3 119.0(5) . . ? C5 C4 H4 120.5 . . ? C3 C4 H4 120.5 . . ? C4 C5 C6 121.7(5) . . ? C4 C5 Cl13 118.4(4) . . ? C6 C5 Cl13 119.9(5) . . ? C7 C6 C11 117.8(5) . . ? C7 C6 C5 117.2(5) . . ? C11 C6 C5 124.9(5) . . ? N8 C7 C6 122.9(4) . . ? N8 C7 C2 113.9(4) . . ? C6 C7 C2 123.1(4) . . ? C9 N8 C7 117.9(4) . . ? C9 N8 Ir01 129.1(3) . . ? C7 N8 Ir01 112.9(3) . . ? N8 C9 C10 120.4(4) . . ? N8 C9 C14 119.3(4) . . ? C10 C9 C14 120.3(4) . . ? C11 C10 C9 122.0(5) . . ? C11 C10 H10 119.0 . . ? C9 C10 H10 119.0 . . ? C10 C11 C6 118.7(5) . . ? C10 C11 H11 120.6 . . ? C6 C11 H11 120.6 . . ? C9 C14 H14A 109.5 . . ? C9 C14 H14B 109.5 . . ? H14A C14 H14B 109.5 . . ? C9 C14 H14C 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? C17 C16 C20 109.5(5) . . ? C17 C16 C21 124.4(6) . . ? C20 C16 C21 126.0(6) . . ? C17 C16 Ir01 70.6(3) . . ? C20 C16 Ir01 71.2(3) . . ? C21 C16 Ir01 124.7(4) . . ? C16 C17 C18 108.0(5) . . ? C16 C17 C22 126.8(6) . . ? C18 C17 C22 125.0(6) . . ? C16 C17 Ir01 70.9(3) . . ? C18 C17 Ir01 70.0(3) . . ? C22 C17 Ir01 122.1(4) . . ? C19 C18 C17 108.8(5) . . ? C19 C18 C23 126.1(6) . . ? C17 C18 C23 124.9(6) . . ? C19 C18 Ir01 72.1(3) . . ? C17 C18 Ir01 70.5(3) . . ? C23 C18 Ir01 127.2(4) . . ? C18 C19 C24 126.1(7) . . ? C18 C19 C20 107.0(5) . . ? C24 C19 C20 126.9(6) . . ? C18 C19 Ir01 69.2(2) . . ? C24 C19 Ir01 128.3(5) . . ? C20 C19 Ir01 69.7(3) . . ? C16 C20 C19 106.7(5) . . ? C16 C20 C25 126.1(7) . . ? C19 C20 C25 126.5(6) . . ? C16 C20 Ir01 69.9(3) . . ? C19 C20 Ir01 70.3(3) . . ? C25 C20 Ir01 132.6(4) . . ? C16 C21 H21A 109.5 . . ? C16 C21 H21B 109.5 . . ? H21A C21 H21B 109.5 . . ? C16 C21 H21C 109.5 . . ? H21A C21 H21C 109.5 . . ? H21B C21 H21C 109.5 . . ? C17 C22 H22A 109.5 . . ? C17 C22 H22B 109.5 . . ? H22A C22 H22B 109.5 . . ? C17 C22 H22C 109.5 . . ? H22A C22 H22C 109.5 . . ? H22B C22 H22C 109.5 . . ? C18 C23 H23A 109.5 . . ? C18 C23 H23B 109.5 . . ? H23A C23 H23B 109.5 . . ? C18 C23 H23C 109.5 . . ? H23A C23 H23C 109.5 . . ? H23B C23 H23C 109.5 . . ? C19 C24 H24A 109.5 . . ? C19 C24 H24B 109.5 . . ? H24A C24 H24B 109.5 . . ? C19 C24 H24C 109.5 . . ? H24A C24 H24C 109.5 . . ? H24B C24 H24C 109.5 . . ? C20 C25 H25A 109.5 . . ? C20 C25 H25B 109.5 . . ? H25A C25 H25B 109.5 . . ? C20 C25 H25C 109.5 . . ? H25A C25 H25C 109.5 . . ? H25B C25 H25C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Ir01 O1 C2 C3 171.1(4) . . . . ? Ir01 O1 C2 C7 -9.3(5) . . . . ? O1 C2 C3 C4 176.4(5) . . . . ? C7 C2 C3 C4 -3.2(7) . . . . ? O1 C2 C3 Cl12 -0.4(7) . . . . ? C7 C2 C3 Cl12 -180.0(4) . . . . ? C2 C3 C4 C5 0.6(8) . . . . ? Cl12 C3 C4 C5 177.4(4) . . . . ? C3 C4 C5 C6 0.9(8) . . . . ? C3 C4 C5 Cl13 179.9(4) . . . . ? C4 C5 C6 C7 0.3(8) . . . . ? Cl13 C5 C6 C7 -178.7(4) . . . . ? C4 C5 C6 C11 -177.4(5) . . . . ? Cl13 C5 C6 C11 3.7(7) . . . . ? C11 C6 C7 N8 -2.4(7) . . . . ? C5 C6 C7 N8 179.8(4) . . . . ? C11 C6 C7 C2 174.7(4) . . . . ? C5 C6 C7 C2 -3.1(7) . . . . ? O1 C2 C7 N8 2.2(6) . . . . ? C3 C2 C7 N8 -178.1(4) . . . . ? O1 C2 C7 C6 -175.1(4) . . . . ? C3 C2 C7 C6 4.5(7) . . . . ? C6 C7 N8 C9 5.9(7) . . . . ? C2 C7 N8 C9 -171.5(4) . . . . ? C6 C7 N8 Ir01 -176.8(4) . . . . ? C2 C7 N8 Ir01 5.9(5) . . . . ? C7 N8 C9 C10 -5.2(7) . . . . ? Ir01 N8 C9 C10 178.0(3) . . . . ? C7 N8 C9 C14 173.4(5) . . . . ? Ir01 N8 C9 C14 -3.5(7) . . . . ? N8 C9 C10 C11 1.2(8) . . . . ? C14 C9 C10 C11 -177.3(5) . . . . ? C9 C10 C11 C6 2.4(8) . . . . ? C7 C6 C11 C10 -1.7(7) . . . . ? C5 C6 C11 C10 175.9(5) . . . . ? C20 C16 C17 C18 -0.4(6) . . . . ? C21 C16 C17 C18 179.8(5) . . . . ? Ir01 C16 C17 C18 60.5(4) . . . . ? C20 C16 C17 C22 -177.2(5) . . . . ? C21 C16 C17 C22 3.0(9) . . . . ? Ir01 C16 C17 C22 -116.4(5) . . . . ? C20 C16 C17 Ir01 -60.9(4) . . . . ? C21 C16 C17 Ir01 119.3(6) . . . . ? C16 C17 C18 C19 1.2(6) . . . . ? C22 C17 C18 C19 178.2(5) . . . . ? Ir01 C17 C18 C19 62.3(3) . . . . ? C16 C17 C18 C23 176.6(6) . . . . ? C22 C17 C18 C23 -6.4(9) . . . . ? Ir01 C17 C18 C23 -122.3(6) . . . . ? C16 C17 C18 Ir01 -61.1(4) . . . . ? C22 C17 C18 Ir01 115.9(5) . . . . ? C17 C18 C19 C24 175.8(6) . . . . ? C23 C18 C19 C24 0.4(9) . . . . ? Ir01 C18 C19 C24 -122.9(7) . . . . ? C17 C18 C19 C20 -1.5(5) . . . . ? C23 C18 C19 C20 -176.9(6) . . . . ? Ir01 C18 C19 C20 59.8(3) . . . . ? C17 C18 C19 Ir01 -61.3(4) . . . . ? C23 C18 C19 Ir01 123.3(6) . . . . ? C17 C16 C20 C19 -0.6(6) . . . . ? C21 C16 C20 C19 179.2(5) . . . . ? Ir01 C16 C20 C19 -61.0(4) . . . . ? C17 C16 C20 C25 -170.8(5) . . . . ? C21 C16 C20 C25 9.0(9) . . . . ? Ir01 C16 C20 C25 128.7(5) . . . . ? C17 C16 C20 Ir01 60.5(4) . . . . ? C21 C16 C20 Ir01 -119.7(6) . . . . ? C18 C19 C20 C16 1.3(6) . . . . ? C24 C19 C20 C16 -176.0(6) . . . . ? Ir01 C19 C20 C16 60.7(4) . . . . ? C18 C19 C20 C25 171.5(5) . . . . ? C24 C19 C20 C25 -5.8(9) . . . . ? Ir01 C19 C20 C25 -129.0(6) . . . . ? C18 C19 C20 Ir01 -59.5(3) . . . . ? C24 C19 C20 Ir01 123.3(6) . . . . ? _refine_diff_density_max 1.696 _refine_diff_density_min -1.503 _refine_diff_density_rms 0.104 _shelx_res_file ; TITL PO19124_029 in Pca2(1) PO19124_029.res created by SHELXL-2018/3 at 16:27:38 on 31-Jul-2019 CELL 0.63000 18.03200 7.51300 14.96600 90.0000 90.0000 90.0000 ZERR 4.00 0.00361 0.00150 0.00299 0.0000 0.0000 0.0000 LATT -1 SYMM -X, -Y, 0.5+Z SYMM 0.5+X, -Y, Z SYMM 0.5-X, Y, 0.5+Z SFAC C H N O CL IR DISP C 0.0021 0.0012 9.00 DISP N 0.0044 0.0025 14.78 DISP O 0.0080 0.0047 23.75 DISP Cl 0.1230 0.1255 471.48 DISP Ir -0.7638 6.5985 24163.94 UNIT 80 84 4 4 12 4 ACTA SIZE 0.052 0.040 0.021 TEMP -30.15 CONF MERG 2 OMIT -3 50.00 L.S. 12 BOND $H FMAP 2 PLAN 20 LIST 4 WGHT 0.028800 FVAR 0.10874 O1 4 0.482425 0.734156 0.458983 11.00000 0.01805 0.04252 = 0.02589 -0.00219 0.00146 -0.00473 IR01 6 0.391677 0.606735 0.401132 11.00000 0.02061 0.02668 = 0.02045 -0.00083 -0.00120 -0.00112 C2 1 0.469089 0.797926 0.538678 11.00000 0.02466 0.02414 = 0.02548 0.00363 -0.00595 -0.00092 C3 1 0.523427 0.866278 0.594171 11.00000 0.03070 0.03507 = 0.03339 0.00480 -0.01119 -0.00530 C4 1 0.507287 0.943508 0.678101 11.00000 0.05346 0.03442 = 0.03325 0.00188 -0.01847 -0.00885 AFIX 43 H4 2 0.545517 0.989771 0.713932 11.00000 -1.20000 AFIX 0 C5 1 0.435214 0.949878 0.706359 11.00000 0.06063 0.03040 = 0.02411 -0.00585 -0.00806 -0.00155 C6 1 0.376384 0.878457 0.654043 11.00000 0.04080 0.02981 = 0.02132 0.00053 0.00187 -0.00040 C7 1 0.395204 0.800748 0.572660 11.00000 0.02815 0.02630 = 0.01925 0.00086 -0.00056 0.00019 N8 3 0.343165 0.725786 0.515561 11.00000 0.02096 0.02690 = 0.02125 0.00133 -0.00091 -0.00007 C9 1 0.270947 0.743416 0.536758 11.00000 0.02241 0.03378 = 0.03154 0.00349 0.00348 -0.00025 C10 1 0.250045 0.822228 0.617703 11.00000 0.03134 0.03644 = 0.03924 0.00424 0.00902 0.00261 AFIX 43 H10 2 0.199364 0.831271 0.631689 11.00000 -1.20000 AFIX 0 C11 1 0.300979 0.886243 0.676843 11.00000 0.04632 0.04027 = 0.02852 0.00066 0.00692 0.00619 AFIX 43 H11 2 0.285879 0.934659 0.731827 11.00000 -1.20000 AFIX 0 CL12 5 0.614270 0.866156 0.556048 11.00000 0.02697 0.06482 = 0.05934 0.00745 -0.01151 -0.01523 CL13 5 0.416312 1.045260 0.809958 11.00000 0.10077 0.05669 = 0.02994 -0.01646 -0.00744 0.00054 C14 1 0.213126 0.681763 0.471708 11.00000 0.02007 0.05725 = 0.04702 -0.00642 0.00033 -0.00104 AFIX 137 H14A 2 0.167306 0.746109 0.482181 11.00000 -1.50000 H14B 2 0.204591 0.555275 0.479650 11.00000 -1.50000 H14C 2 0.230083 0.704032 0.411224 11.00000 -1.50000 AFIX 0 CL15 5 0.357070 0.883341 0.331169 11.00000 0.03803 0.03118 = 0.02877 0.00437 0.00131 0.00148 C16 1 0.405875 0.459278 0.279192 11.00000 0.04970 0.03057 = 0.02278 -0.00482 0.00137 0.00524 C17 1 0.464505 0.418273 0.338611 11.00000 0.03745 0.02378 = 0.03798 -0.00511 0.00017 0.00492 C18 1 0.432652 0.341812 0.418523 11.00000 0.05137 0.02931 = 0.02690 -0.00167 -0.00080 -0.00184 C19 1 0.353909 0.331873 0.407800 11.00000 0.04301 0.02780 = 0.04462 -0.00052 -0.00296 -0.00325 C20 1 0.336323 0.409515 0.319026 11.00000 0.04332 0.03291 = 0.03655 -0.00587 -0.00663 -0.00168 C21 1 0.416051 0.541499 0.188658 11.00000 0.09299 0.04693 = 0.02399 -0.00370 0.00334 0.01599 AFIX 137 H21A 2 0.448268 0.466635 0.152858 11.00000 -1.50000 H21B 2 0.438221 0.658428 0.195114 11.00000 -1.50000 H21C 2 0.368243 0.552589 0.159472 11.00000 -1.50000 AFIX 0 C22 1 0.545460 0.455565 0.324843 11.00000 0.03948 0.04732 = 0.06887 -0.00539 0.01244 0.01031 AFIX 137 H22A 2 0.573698 0.347460 0.334747 11.00000 -1.50000 H22B 2 0.561533 0.546350 0.366661 11.00000 -1.50000 H22C 2 0.553479 0.496990 0.264221 11.00000 -1.50000 AFIX 0 C23 1 0.475823 0.272238 0.495197 11.00000 0.08770 0.05888 = 0.05227 0.01647 -0.00920 0.02047 AFIX 137 H23A 2 0.495458 0.155708 0.480399 11.00000 -1.50000 H23B 2 0.443823 0.262717 0.547076 11.00000 -1.50000 H23C 2 0.516445 0.352747 0.508304 11.00000 -1.50000 AFIX 0 C24 1 0.301405 0.251863 0.471135 11.00000 0.06659 0.04671 = 0.07523 0.00530 0.02785 -0.01130 AFIX 137 H24A 2 0.306911 0.123441 0.470345 11.00000 -1.50000 H24B 2 0.251166 0.283137 0.454099 11.00000 -1.50000 H24C 2 0.311455 0.296156 0.530798 11.00000 -1.50000 AFIX 0 C25 1 0.262637 0.407037 0.273335 11.00000 0.05234 0.06685 = 0.08716 -0.03241 -0.03220 0.00303 AFIX 137 H25A 2 0.264227 0.324519 0.223524 11.00000 -1.50000 H25B 2 0.251106 0.525404 0.251495 11.00000 -1.50000 H25C 2 0.224750 0.369579 0.315328 11.00000 -1.50000 AFIX 0 HKLF 4 REM PO19124_029 in Pca2(1) REM wR2 = 0.0540, GooF = S = 1.045, Restrained GooF = 1.045 for all data REM R1 = 0.0212 for 4873 Fo > 4sig(Fo) and 0.0221 for all 5085 data REM 241 parameters refined using 1 restraints END WGHT 0.0288 0.0000 REM Highest difference peak 1.696, deepest hole -1.503, 1-sigma level 0.104 Q1 1 0.3473 0.6099 0.3947 11.00000 0.05 1.70 Q2 1 0.3901 0.7131 0.4010 11.00000 0.05 1.43 Q3 1 0.3911 0.4953 0.4009 11.00000 0.05 1.23 Q4 1 0.4312 0.6074 0.4114 11.00000 0.05 1.14 Q5 1 0.3887 0.3509 0.4034 11.00000 0.05 0.77 Q6 1 0.4512 0.3975 0.3977 11.00000 0.05 0.70 Q7 1 0.3825 0.8570 0.3957 11.00000 0.05 0.58 Q8 1 0.3531 0.3812 0.4002 11.00000 0.05 0.47 Q9 1 0.3550 0.7774 0.3327 11.00000 0.05 0.45 Q10 1 0.3930 1.0095 0.4026 11.00000 0.05 0.44 Q11 1 0.3439 0.4157 0.3559 11.00000 0.05 0.37 Q12 1 0.3528 0.7723 0.4618 11.00000 0.05 0.36 Q13 1 0.3340 0.3588 0.3455 11.00000 0.05 0.35 Q14 1 0.3315 0.3518 0.4603 11.00000 0.05 0.33 Q15 1 0.3166 0.8639 0.3490 11.00000 0.05 0.33 Q16 1 0.5615 0.4435 0.3993 11.00000 0.05 0.33 Q17 1 0.5839 0.8810 0.5966 11.00000 0.05 0.32 Q18 1 0.4681 0.6626 0.4801 11.00000 0.05 0.31 Q19 1 0.3993 0.4086 0.3368 11.00000 0.05 0.31 Q20 1 0.4733 0.6407 0.3197 11.00000 0.05 0.31 ; _shelx_res_checksum 43155 _shelx_hkl_file ; 2 0 0 231.68 8.28 -2 0 0 225.41 7.96 3 0 0 0.08 0.06 -3 0 0 0.05 0.06 4 0 0 1025.18 23.77 -4 0 0 1057.53 35.64 5 0 0 0.03 0.09 -5 0 0 -0.13 0.17 6 0 0 395.60 10.17 -6 0 0 395.36 10.37 7 0 0 0.10 0.15 -7 0 0 -0.05 0.24 8 0 0 559.40 13.96 -8 0 0 567.59 20.99 9 0 0 0.13 0.15 -9 0 0 -0.01 0.15 10 0 0 347.84 8.97 -10 0 0 349.37 13.75 11 0 0 0.04 0.18 -11 0 0 0.26 0.28 12 0 0 53.17 1.67 -12 0 0 51.82 1.67 13 0 0 0.17 0.31 -13 0 0 -0.19 0.46 14 0 0 282.43 7.32 -14 0 0 294.90 7.39 15 0 0 0.20 0.26 -15 0 0 0.13 0.25 16 0 0 10.64 0.97 -16 0 0 10.88 0.70 17 0 0 0.02 0.31 -17 0 0 0.06 0.33 18 0 0 142.89 5.51 -18 0 0 144.64 3.99 19 0 0 0.57 0.72 -19 0 0 -0.25 0.41 20 0 0 33.61 1.40 -20 0 0 34.82 1.52 21 0 0 0.16 0.47 -21 0 0 0.30 0.63 22 0 0 87.08 2.95 -22 0 0 83.08 4.08 23 0 0 0.01 0.49 -23 0 0 0.14 0.52 24 0 0 58.20 2.26 -24 0 0 57.27 3.83 25 0 0 0.43 0.61 -25 0 0 0.22 0.64 26 0 0 12.15 1.01 -26 0 0 11.76 1.04 27 0 0 1.04 1.57 -27 0 0 -0.15 0.90 28 0 0 32.11 1.72 -28 0 0 33.09 1.85 -28 0 1 -0.23 0.93 28 0 -1 -0.11 0.86 -27 0 1 0.10 1.16 27 0 -1 0.81 0.84 -26 0 1 46.37 2.02 26 0 -1 43.60 1.87 -25 0 1 0.04 0.97 25 0 -1 -0.33 0.56 -24 0 1 20.02 1.84 24 0 -1 21.64 1.27 -23 0 1 -0.36 0.54 23 0 -1 -0.06 0.47 -22 0 1 63.81 3.18 22 0 -1 65.67 3.65 -21 0 1 0.53 0.67 21 0 -1 -0.11 0.62 -20 0 1 66.53 2.20 20 0 -1 73.20 2.56 -19 0 1 0.41 0.78 19 0 -1 -0.06 0.45 -18 0 1 23.06 1.17 18 0 -1 21.14 0.97 -17 0 1 -0.32 0.37 17 0 -1 -0.34 0.48 -16 0 1 152.67 4.37 16 0 -1 159.14 4.69 -15 0 1 -0.07 0.33 15 0 -1 -0.15 0.38 -14 0 1 3.24 0.49 14 0 -1 3.67 0.40 -13 0 1 0.21 0.21 13 0 -1 0.01 0.21 -12 0 1 260.02 6.65 12 0 -1 269.23 9.54 -11 0 1 0.03 0.18 11 0 -1 0.15 0.18 -10 0 1 205.07 8.57 10 0 -1 215.78 5.65 -9 0 1 0.09 0.19 9 0 -1 -0.02 0.32 -8 0 1 55.19 1.71 8 0 -1 55.27 1.70 -7 0 1 0.02 0.15 7 0 -1 0.14 0.27 -6 0 1 515.99 17.77 6 0 -1 579.42 14.27 -5 0 1 0.23 0.09 5 0 -1 -0.01 0.13 -4 0 1 35.46 1.70 4 0 -1 31.78 1.06 -3 0 1 -0.02 0.10 3 0 -1 0.00 0.09 -2 0 1 1681.34 63.11 2 0 -1 1638.86 60.07 1 0 -1 0.00 0.05 1 0 1 0.01 0.04 -1 0 -1 0.05 0.05 2 0 1 1621.02 43.20 -2 0 -1 1642.43 42.32 3 0 1 0.10 0.11 -3 0 -1 1.74 0.22 4 0 1 34.88 1.07 -4 0 -1 31.47 1.03 5 0 1 0.23 0.12 -5 0 -1 0.17 0.10 6 0 1 537.42 13.64 -6 0 -1 594.95 14.53 7 0 1 0.15 0.13 -7 0 -1 -0.05 0.12 8 0 1 54.74 2.29 -8 0 -1 54.61 1.83 9 0 1 0.24 0.32 -9 0 -1 0.44 0.21 10 0 1 203.87 5.38 -10 0 -1 203.96 5.64 11 0 1 0.17 0.19 -11 0 -1 0.27 0.28 12 0 1 255.31 6.51 -12 0 -1 262.36 6.73 13 0 1 -0.01 0.32 -13 0 -1 0.16 0.35 14 0 1 2.88 0.35 -14 0 -1 3.12 0.38 15 0 1 -0.01 0.27 -15 0 -1 -0.12 0.33 16 0 1 156.55 4.21 -16 0 -1 161.02 4.47 17 0 1 -0.19 0.59 -17 0 -1 0.24 0.40 18 0 1 24.15 1.58 -18 0 -1 20.89 0.99 19 0 1 0.29 0.45 -19 0 -1 0.07 0.50 20 0 1 66.82 2.13 -20 0 -1 73.00 2.51 21 0 1 -0.15 0.46 -21 0 -1 -0.16 0.86 22 0 1 64.77 2.46 -22 0 -1 66.96 3.09 23 0 1 -0.12 0.49 -23 0 -1 0.17 0.51 24 0 1 20.80 1.25 -24 0 -1 20.01 1.35 25 0 1 0.09 0.57 -25 0 -1 0.18 0.63 26 0 1 42.89 1.85 -26 0 -1 40.70 2.91 27 0 1 0.41 0.94 -27 0 -1 -0.43 1.51 28 0 1 0.28 0.91 -28 0 -1 -0.08 0.87 -28 0 2 27.68 2.17 28 0 -2 29.68 1.97 -27 0 2 0.31 0.85 27 0 -2 0.18 0.76 -26 0 2 6.39 1.05 26 0 -2 5.01 0.91 -25 0 2 0.16 0.74 25 0 -2 0.46 0.60 -24 0 2 51.02 2.98 24 0 -2 48.46 2.60 -23 0 2 -0.09 0.51 23 0 -2 -0.16 0.51 -22 0 2 53.85 2.60 22 0 -2 38.29 2.39 -21 0 2 0.20 0.53 21 0 -2 0.12 0.48 -20 0 2 35.41 1.55 20 0 -2 42.96 1.52 -19 0 2 -0.02 0.37 19 0 -2 0.00 0.53 -18 0 2 150.03 6.25 18 0 -2 125.16 3.67 -17 0 2 0.26 0.38 17 0 -2 0.06 0.60 -16 0 2 16.21 1.16 16 0 -2 16.89 0.76 -15 0 2 0.23 0.28 15 0 -2 0.25 0.29 -14 0 2 214.60 5.28 14 0 -2 183.13 6.76 -13 0 2 -0.05 0.22 13 0 -2 -0.12 0.22 -12 0 2 54.74 1.65 12 0 -2 42.51 1.42 -11 0 2 0.13 0.19 11 0 -2 -0.03 0.19 -10 0 2 248.67 6.56 10 0 -2 213.24 5.67 -9 0 2 0.01 0.15 9 0 -2 -0.05 0.25 -8 0 2 226.97 8.15 8 0 -2 189.61 5.06 -7 0 2 0.02 0.19 7 0 -2 0.11 0.18 -6 0 2 123.98 3.48 6 0 -2 177.73 4.86 -5 0 2 -0.11 0.15 5 0 -2 0.14 0.15 -4 0 2 848.79 28.38 4 0 -2 884.73 29.79 3 0 -2 0.06 0.12 -2 0 2 50.38 2.32 2 0 -2 52.77 2.30 -1 0 2 0.24 0.11 1 0 -2 -0.02 0.11 0 0 2 1254.99 31.64 0 0 -2 1266.20 32.43 1 0 2 0.01 0.06 -1 0 -2 0.04 0.06 2 0 2 49.34 1.45 -2 0 -2 54.47 1.51 3 0 2 0.27 0.12 -3 0 -2 -0.08 0.07 4 0 2 867.30 21.68 -4 0 -2 927.19 22.87 5 0 2 -0.06 0.10 -5 0 -2 0.12 0.11 6 0 2 131.88 5.94 -6 0 -2 166.23 4.75 7 0 2 -0.03 0.13 -7 0 -2 0.22 0.14 8 0 2 227.06 8.68 -8 0 -2 187.51 5.18 9 0 2 0.41 0.27 -9 0 -2 -0.19 0.16 10 0 2 247.08 6.64 -10 0 -2 212.22 6.00 11 0 2 0.02 0.18 -11 0 -2 0.01 0.27 12 0 2 55.27 1.67 -12 0 -2 44.70 1.91 13 0 2 0.10 0.22 -13 0 -2 0.01 0.22 14 0 2 206.23 5.49 -14 0 -2 173.66 4.71 15 0 2 -0.17 0.30 -15 0 -2 0.08 0.28 16 0 2 16.07 0.85 -16 0 -2 13.74 1.23 17 0 2 -0.12 0.30 -17 0 -2 0.22 0.46 18 0 2 137.42 3.91 -18 0 -2 116.56 3.48 19 0 2 0.02 0.37 -19 0 -2 -0.23 0.53 20 0 2 35.65 1.44 -20 0 -2 41.93 2.19 21 0 2 -0.09 0.57 -21 0 -2 0.15 0.45 22 0 2 52.00 1.95 -22 0 -2 39.19 2.70 23 0 2 0.19 0.49 -23 0 -2 -0.21 0.51 24 0 2 47.43 1.89 -24 0 -2 44.63 1.97 25 0 2 0.60 0.61 -25 0 -2 0.25 0.63 26 0 2 5.41 1.02 -26 0 -2 5.21 0.93 27 0 2 0.21 0.95 -27 0 -2 0.00 0.86 28 0 2 28.21 1.78 -28 0 -2 28.95 2.31 -28 0 3 1.73 1.42 28 0 -3 2.50 1.98 -27 0 3 -0.76 0.88 27 0 -3 0.42 0.83 -26 0 3 40.30 1.93 26 0 -3 41.34 2.65 -25 0 3 0.15 0.73 25 0 -3 0.16 0.70 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356.99 9.43 -4 0 -3 305.19 11.02 5 0 3 0.33 0.13 -5 0 -3 -0.02 0.13 6 0 3 665.19 16.33 -6 0 -3 762.75 18.75 7 0 3 0.09 0.15 -7 0 -3 0.16 0.19 8 0 3 251.04 9.52 -8 0 -3 248.59 6.36 9 0 3 -0.03 0.16 -9 0 -3 0.43 0.18 10 0 3 153.35 4.09 -10 0 -3 166.11 4.79 11 0 3 -0.18 0.19 -11 0 -3 -0.09 0.19 12 0 3 397.70 10.25 -12 0 -3 370.83 12.85 13 0 3 0.12 0.27 -13 0 -3 -0.12 0.33 14 0 3 30.28 1.04 -14 0 -3 34.54 1.19 15 0 3 -0.07 0.28 -15 0 -3 0.09 0.30 16 0 3 184.53 5.11 -16 0 -3 186.64 7.28 17 0 3 -0.05 0.33 -17 0 -3 0.11 0.34 18 0 3 8.19 0.86 -18 0 -3 12.03 0.78 19 0 3 0.27 0.45 -19 0 -3 -0.27 0.43 20 0 3 128.85 4.99 -20 0 -3 119.98 6.08 21 0 3 -0.30 0.42 -21 0 -3 0.07 0.42 22 0 3 43.16 1.67 -22 0 -3 41.75 2.14 23 0 3 0.12 0.70 -23 0 -3 0.04 0.73 24 0 3 29.00 1.41 -24 0 -3 28.77 1.97 25 0 3 0.34 0.63 -25 0 -3 0.04 0.62 26 0 3 34.13 1.69 -26 0 -3 42.47 2.59 27 0 3 -0.20 0.93 -27 0 -3 -0.05 0.82 28 0 3 2.76 1.46 -28 0 -3 2.20 1.40 -28 0 4 24.32 1.65 28 0 -4 30.54 1.80 -27 0 4 -0.09 1.05 27 0 -4 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15.21 1 0 4 -0.01 0.09 -1 0 -4 -0.06 0.09 2 0 4 34.19 1.15 -2 0 -4 39.89 1.30 3 0 4 0.06 0.10 -3 0 -4 -0.03 0.09 4 0 4 596.34 15.25 -4 0 -4 700.26 16.92 5 0 4 0.29 0.14 -5 0 -4 0.11 0.22 6 0 4 139.44 3.84 -6 0 -4 168.09 6.74 7 0 4 0.04 0.14 -7 0 -4 0.32 0.15 8 0 4 212.79 5.65 -8 0 -4 253.17 9.96 9 0 4 0.08 0.17 -9 0 -4 0.30 0.17 10 0 4 347.04 12.89 -10 0 -4 311.85 8.05 11 0 4 0.02 0.20 -11 0 -4 -0.09 0.21 12 0 4 33.33 1.08 -12 0 -4 37.04 1.19 13 0 4 0.04 0.23 -13 0 -4 -0.02 0.24 14 0 4 186.89 7.64 -14 0 -4 204.03 9.00 15 0 4 -0.14 0.60 -15 0 -4 0.32 0.38 16 0 4 1.14 0.40 -16 0 -4 2.70 0.42 17 0 4 0.06 0.50 -17 0 -4 0.01 0.39 18 0 4 117.08 4.72 -18 0 -4 112.30 3.50 19 0 4 -0.03 0.37 -19 0 -4 -0.15 0.38 20 0 4 36.44 1.54 -20 0 -4 45.49 2.43 21 0 4 0.10 0.45 -21 0 -4 0.49 0.71 22 0 4 42.14 1.69 -22 0 -4 39.44 1.71 23 0 4 0.49 0.60 -23 0 -4 0.62 0.79 24 0 4 36.08 2.33 -24 0 -4 37.89 1.69 25 0 4 0.23 0.69 -25 0 -4 -1.02 0.86 26 0 4 1.89 0.72 -26 0 -4 3.32 0.83 27 0 4 -0.02 1.62 -27 0 -4 0.42 1.09 28 0 4 22.74 2.30 -28 0 -4 25.02 1.78 28 0 -5 0.03 1.28 -27 0 5 -0.45 0.82 27 0 -5 -0.65 1.15 -26 0 5 29.08 1.73 26 0 -5 34.93 1.65 -25 0 5 0.36 0.97 25 0 -5 0.01 1.39 -24 0 5 16.00 1.08 24 0 -5 14.80 1.05 -23 0 5 0.66 0.66 23 0 -5 -0.10 0.61 -22 0 5 30.10 1.36 22 0 -5 28.43 1.21 -21 0 5 -0.36 0.70 21 0 -5 0.46 0.56 -20 0 5 99.36 3.26 20 0 -5 91.73 2.95 -19 0 5 -0.07 0.46 19 0 -5 0.38 0.47 -18 0 5 18.15 1.04 18 0 -5 22.25 1.05 -17 0 5 0.39 0.38 17 0 -5 -0.27 0.36 -16 0 5 208.19 5.62 16 0 -5 197.98 5.43 -15 0 5 0.10 0.43 15 0 -5 0.11 0.41 -14 0 5 14.68 0.99 14 0 -5 11.69 1.00 -13 0 5 0.17 0.25 13 0 -5 0.13 0.24 -12 0 5 331.12 8.18 12 0 -5 284.59 6.91 -11 0 5 0.07 0.24 11 0 -5 0.02 0.24 -10 0 5 49.75 1.55 10 0 -5 45.02 1.33 -9 0 5 -0.20 0.37 9 0 -5 0.01 0.19 8 0 -5 537.23 19.00 -7 0 5 0.04 0.21 7 0 -5 0.23 0.22 6 0 -5 432.55 15.51 5 0 -5 0.03 0.19 -4 0 5 340.85 8.84 4 0 -5 336.58 12.36 -3 0 5 0.03 0.12 3 0 -5 0.11 0.14 -2 0 5 646.87 15.91 2 0 -5 644.96 15.81 -1 0 5 0.05 0.12 1 0 -5 0.03 0.11 0 0 5 -0.14 0.11 0 0 -5 0.06 0.12 1 0 5 -0.02 0.12 -1 0 -5 -0.07 0.11 2 0 5 651.99 16.22 -2 0 -5 659.07 16.27 3 0 5 0.02 0.16 -3 0 -5 -0.07 0.17 4 0 5 351.78 9.11 -4 0 -5 330.03 8.37 5 0 5 0.10 0.15 -5 0 -5 -0.05 0.17 6 0 5 465.83 12.09 -6 0 -5 428.25 10.84 7 0 5 -0.14 0.15 -7 0 -5 -0.01 0.14 8 0 5 579.85 14.25 -8 0 -5 531.29 13.66 9 0 5 0.05 0.20 -9 0 -5 -0.07 0.17 10 0 5 50.55 1.69 -10 0 -5 43.12 1.46 11 0 5 0.15 0.20 -11 0 -5 -0.04 0.22 12 0 5 306.74 7.65 -12 0 -5 277.09 7.09 13 0 5 0.30 0.34 -13 0 -5 -0.34 0.34 14 0 5 14.24 1.29 -14 0 -5 12.87 0.72 15 0 5 -0.13 0.27 -15 0 -5 0.15 0.29 16 0 5 205.85 5.57 -16 0 -5 200.54 5.53 17 0 5 0.11 0.33 -17 0 -5 -0.13 0.46 18 0 5 18.00 0.92 -18 0 -5 23.16 1.65 19 0 5 0.06 0.36 -19 0 -5 -0.15 0.37 20 0 5 92.45 3.18 -20 0 -5 84.12 3.99 21 0 5 0.06 0.44 -21 0 -5 0.06 0.61 22 0 5 27.74 2.08 -22 0 -5 28.01 1.26 23 0 5 0.08 0.73 -23 0 -5 0.01 0.70 24 0 5 16.16 1.49 -24 0 -5 12.42 0.95 25 0 5 -0.01 0.62 -25 0 -5 0.04 0.72 26 0 5 30.19 1.54 -26 0 -5 32.44 1.65 27 0 5 0.47 0.82 -27 0 -5 -0.69 1.13 28 0 5 1.30 1.14 -28 0 -5 1.35 1.98 -27 0 6 -0.45 1.21 27 0 -6 -0.14 0.85 -26 0 6 11.06 1.35 26 0 -6 17.50 1.43 -25 0 6 -1.39 1.00 25 0 -6 0.13 0.66 -24 0 6 47.59 1.88 24 0 -6 48.02 2.79 -23 0 6 -0.13 0.57 23 0 -6 0.07 0.54 -22 0 6 62.41 2.10 22 0 -6 58.27 2.28 -21 0 6 -0.29 0.50 21 0 -6 0.00 0.57 -20 0 6 18.35 1.41 20 0 -6 19.28 1.11 -19 0 6 -0.21 0.57 19 0 -6 0.03 0.40 -18 0 6 210.31 8.87 18 0 -6 213.47 9.15 -17 0 6 -0.46 0.51 17 0 -6 -0.04 0.33 -16 0 6 0.10 0.33 16 0 -6 0.49 0.33 -15 0 6 0.17 0.31 15 0 -6 0.08 0.47 -14 0 6 368.70 9.05 14 0 -6 355.23 8.81 -13 0 6 0.17 0.38 13 0 -6 -0.30 0.56 -12 0 6 49.56 2.28 12 0 -6 57.24 2.30 -11 0 6 -0.08 0.22 11 0 -6 0.01 0.34 10 0 -6 345.88 12.14 9 0 -6 -0.03 0.25 -8 0 6 266.14 9.81 8 0 -6 255.89 9.40 -7 0 6 -0.05 0.24 7 0 -6 -0.11 0.22 -6 0 6 375.54 13.96 6 0 -6 350.28 12.68 -5 0 6 -0.23 0.22 5 0 -6 0.30 0.23 -4 0 6 578.76 20.12 4 0 -6 616.82 21.68 -3 0 6 0.02 0.13 3 0 -6 0.30 0.15 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0.67 -25 0 -6 0.39 0.67 26 0 6 11.14 1.16 -26 0 -6 12.52 1.21 27 0 6 -0.15 0.85 -27 0 -6 -0.29 0.86 28 0 6 13.47 2.37 -27 0 7 0.67 1.09 27 0 -7 1.53 1.83 -26 0 7 32.02 2.33 26 0 -7 29.90 1.76 -25 0 7 0.56 1.08 25 0 -7 -0.40 0.70 -24 0 7 16.07 1.22 24 0 -7 18.72 1.71 -23 0 7 0.16 0.59 23 0 -7 -0.17 0.54 -22 0 7 29.92 1.36 22 0 -7 26.66 1.28 -21 0 7 0.41 0.51 21 0 -7 -0.51 0.67 -20 0 7 59.95 2.10 20 0 -7 62.81 2.15 -19 0 7 0.11 0.39 19 0 -7 0.18 0.49 -18 0 7 19.37 0.93 18 0 -7 19.75 1.28 -17 0 7 -0.24 0.35 17 0 -7 0.21 0.38 -16 0 7 197.39 5.38 16 0 -7 203.73 5.40 -15 0 7 -0.09 0.48 15 0 -7 -0.03 0.36 -14 0 7 -0.16 0.43 14 0 -7 0.31 0.41 -13 0 7 0.30 0.27 13 0 -7 0.42 0.41 -12 0 7 220.09 9.39 12 0 -7 214.89 9.10 11 0 -7 0.18 0.34 10 0 -7 45.60 2.05 -9 0 7 0.25 0.31 9 0 -7 0.22 0.31 -8 0 7 378.33 13.38 8 0 -7 374.27 13.06 -7 0 7 0.07 0.22 7 0 -7 -0.01 0.28 -6 0 7 127.78 3.64 6 0 -7 134.20 3.72 -5 0 7 0.05 0.16 5 0 -7 0.05 0.24 -4 0 7 137.63 3.70 4 0 -7 142.15 4.08 -3 0 7 0.19 0.30 3 0 -7 0.06 0.22 -2 0 7 491.94 12.31 2 0 -7 532.37 18.69 -1 0 7 0.12 0.21 1 0 -7 -0.10 0.20 0 0 7 0.04 0.15 0 0 -7 0.11 0.16 1 0 7 0.02 0.14 -1 0 -7 0.14 0.15 2 0 7 511.24 12.62 -2 0 -7 529.08 13.25 3 0 7 0.17 0.16 -3 0 -7 0.14 0.17 4 0 7 143.83 5.73 -4 0 -7 140.89 3.96 5 0 7 -0.17 0.16 -5 0 -7 0.02 0.15 6 0 7 126.05 3.51 -6 0 -7 128.06 3.59 7 0 7 0.06 0.20 -7 0 -7 0.05 0.19 8 0 7 402.55 10.09 -8 0 -7 390.65 9.98 9 0 7 0.19 0.22 -9 0 -7 0.46 0.24 10 0 7 39.19 1.35 -10 0 -7 45.22 1.44 11 0 7 0.03 0.22 -11 0 -7 -0.13 0.22 12 0 7 190.52 5.45 -12 0 -7 210.57 5.30 13 0 7 0.30 0.28 -13 0 -7 -0.11 0.28 14 0 7 0.63 0.36 -14 0 -7 0.39 0.35 15 0 7 -0.15 0.31 -15 0 -7 0.06 0.31 16 0 7 187.44 5.13 -16 0 -7 189.78 5.23 17 0 7 -0.10 0.36 -17 0 -7 -0.18 0.35 18 0 7 17.33 1.34 -18 0 -7 18.46 0.96 19 0 7 0.18 0.50 -19 0 -7 0.56 0.78 20 0 7 62.82 2.18 -20 0 -7 59.67 2.11 21 0 7 -0.30 0.56 -21 0 -7 0.04 0.89 22 0 7 29.44 1.89 -22 0 -7 28.57 2.07 23 0 7 0.54 0.83 -23 0 -7 0.14 0.57 24 0 7 14.38 1.06 -24 0 -7 16.60 1.15 25 0 7 -0.25 0.69 -25 0 -7 -0.06 0.73 26 0 7 26.21 1.55 -26 0 -7 24.96 1.53 27 0 7 0.62 1.08 -27 0 -7 -0.88 1.29 -26 0 8 13.16 1.73 26 0 -8 9.97 1.11 -25 0 8 -0.69 0.86 25 0 -8 0.24 0.81 -24 0 8 27.89 1.42 24 0 -8 21.86 1.27 -23 0 8 0.29 0.62 23 0 -8 0.06 0.89 -22 0 8 38.19 1.57 22 0 -8 34.47 2.21 -21 0 8 -0.29 0.52 21 0 -8 -0.22 0.49 -20 0 8 15.31 0.91 20 0 -8 18.13 1.55 -19 0 8 -0.19 0.44 19 0 -8 -0.02 0.63 -18 0 8 137.49 3.95 18 0 -8 132.84 4.14 -17 0 8 -0.09 0.38 17 0 -8 0.02 0.38 -16 0 8 0.48 0.54 16 0 -8 0.38 0.53 -15 0 8 -0.24 0.50 15 0 -8 0.25 0.47 -14 0 8 230.22 6.17 14 0 -8 231.85 8.29 -13 0 8 0.30 0.31 13 0 -8 0.55 0.46 12 0 -8 17.07 1.19 -11 0 8 -0.17 0.34 11 0 -8 0.46 0.40 -10 0 8 233.45 8.33 10 0 -8 221.31 8.44 -9 0 8 0.06 0.25 -8 0 8 178.61 6.89 8 0 -8 178.90 6.38 -7 0 8 0.17 0.29 7 0 -8 -0.09 0.28 -6 0 8 249.92 9.20 6 0 -8 220.63 8.46 -5 0 8 -0.11 0.27 5 0 -8 0.00 0.28 -4 0 8 519.78 12.67 4 0 -8 472.62 11.83 -3 0 8 -0.17 0.17 3 0 -8 0.19 0.17 -2 0 8 33.13 1.08 2 0 -8 21.22 0.82 -1 0 8 0.23 0.18 1 0 -8 0.11 0.24 0 0 8 582.31 14.60 0 0 -8 466.85 17.17 1 0 8 -0.07 0.16 -1 0 -8 -0.02 0.23 2 0 8 29.79 0.98 -2 0 -8 21.73 1.37 3 0 8 -0.06 0.16 -3 0 -8 0.12 0.22 4 0 8 507.78 12.70 -4 0 -8 464.83 11.84 5 0 8 0.01 0.19 -5 0 -8 0.09 0.19 6 0 8 245.38 6.52 -6 0 -8 221.50 6.19 7 0 8 0.30 0.21 -7 0 -8 -0.16 0.22 8 0 8 178.09 4.88 -8 0 -8 168.88 4.37 9 0 8 0.22 0.25 -9 0 -8 -0.13 0.24 10 0 8 202.52 5.25 -10 0 -8 222.19 5.93 11 0 8 0.02 0.36 -11 0 -8 -0.12 0.25 12 0 8 16.76 0.84 -12 0 -8 14.52 0.77 13 0 8 -0.09 0.28 -13 0 -8 0.08 0.27 14 0 8 224.22 5.82 -14 0 -8 226.88 5.87 15 0 8 0.23 0.37 -15 0 -8 -0.15 0.39 16 0 8 0.17 0.36 -16 0 -8 1.05 0.40 17 0 8 -0.08 0.39 -17 0 -8 -0.11 0.37 18 0 8 136.64 3.96 -18 0 -8 129.53 5.79 19 0 8 -0.31 0.50 -19 0 -8 -0.23 0.49 20 0 8 15.74 1.01 -20 0 -8 16.33 0.91 21 0 8 -0.16 0.50 -21 0 -8 -0.01 0.49 22 0 8 37.14 1.51 -22 0 -8 34.62 1.45 23 0 8 0.20 0.58 -23 0 -8 0.40 0.88 24 0 8 23.70 1.34 -24 0 -8 22.54 1.35 25 0 8 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81.16 3.31 7 -4 4 76.92 2.12 -6 4 -4 97.24 4.01 6 -4 4 114.30 3.23 5 -4 4 24.51 0.74 4 -4 4 218.52 5.66 3 -4 4 39.78 1.14 2 -4 4 12.91 0.66 1 -4 4 65.75 1.80 0 4 -4 576.07 19.72 0 -4 4 499.57 16.63 1 4 -4 71.27 2.03 -1 -4 4 68.66 2.63 2 4 -4 16.43 0.60 -2 -4 4 14.21 0.74 3 4 -4 48.21 2.11 -3 -4 4 44.11 2.10 4 4 -4 246.23 6.41 -4 -4 4 245.96 6.58 5 4 -4 23.82 1.21 -5 -4 4 26.69 1.35 6 4 -4 103.34 3.02 -6 -4 4 122.68 5.19 7 4 -4 93.46 2.73 -7 -4 4 86.60 2.56 8 4 -4 108.52 4.14 -8 -4 4 85.70 2.48 9 4 -4 4.95 0.34 -9 -4 4 3.13 0.30 10 4 -4 142.20 3.83 -10 -4 4 147.66 5.87 11 4 -4 24.22 0.95 -11 -4 4 22.57 1.29 12 4 -4 13.80 0.71 -12 -4 4 11.04 0.65 13 4 -4 11.90 0.98 -13 -4 4 11.29 0.65 14 4 -4 125.06 3.31 -14 -4 4 120.45 3.52 15 4 -4 13.75 0.78 -15 -4 4 15.64 0.83 16 4 -4 4.13 0.62 -16 -4 4 5.06 0.92 17 4 -4 18.10 0.98 -17 -4 4 17.49 1.26 18 4 -4 67.81 4.00 -18 -4 4 72.60 2.65 19 4 -4 3.18 0.80 -19 -4 4 3.11 0.59 20 4 -4 14.71 0.89 -20 -4 4 15.07 0.96 21 4 -4 20.90 1.55 -21 -4 4 18.68 1.88 22 4 -4 30.56 1.51 -22 -4 4 26.50 1.95 23 4 -4 0.30 0.63 -23 -4 4 0.96 0.69 24 4 -4 28.90 1.58 -24 -4 4 21.81 1.45 25 4 -4 6.50 0.97 -25 -4 4 4.15 1.36 26 4 -4 4.62 1.42 -26 -4 4 3.29 1.48 -29 4 -3 0.92 1.03 29 -4 3 1.23 1.20 -28 4 -3 1.48 1.33 28 -4 3 1.67 1.55 -27 4 -3 2.89 1.25 27 -4 3 3.28 1.08 -26 4 -3 20.29 1.20 26 -4 3 19.55 1.25 -25 4 -3 0.49 0.88 25 -4 3 0.55 1.30 -24 4 -3 16.89 1.09 24 -4 3 16.37 1.13 -23 4 -3 10.09 0.86 23 -4 3 8.06 0.75 -22 4 -3 21.13 1.43 22 -4 3 18.51 0.99 -21 4 -3 -0.17 0.43 21 -4 3 0.30 0.65 -20 4 -3 49.70 1.70 20 -4 3 53.95 2.70 19 -4 3 16.89 0.90 -18 4 -3 7.49 0.54 18 -4 3 7.38 0.80 -17 4 -3 4.64 0.50 17 -4 3 3.04 0.39 -16 4 -3 84.11 3.68 16 -4 3 96.81 2.92 -15 4 -3 10.60 0.83 15 -4 3 12.07 0.63 -14 4 -3 1.59 0.35 14 -4 3 2.19 0.30 -13 4 -3 7.80 0.43 13 -4 3 8.12 0.49 -12 4 -3 143.02 5.44 12 -4 3 149.98 3.99 -11 4 -3 6.62 0.50 11 -4 3 7.30 0.53 10 -4 3 81.92 2.32 -9 4 -3 41.91 2.06 9 -4 3 41.29 1.26 -8 4 -3 143.42 5.28 8 -4 3 157.58 4.11 7 -4 3 4.84 0.26 6 -4 3 249.25 6.34 -5 4 -3 75.38 3.17 5 -4 3 80.32 2.16 4 -4 3 66.70 2.55 0 -4 3 -0.01 0.08 1 4 -3 70.84 2.88 -1 -4 3 94.73 2.65 2 4 -3 768.71 26.17 -2 -4 3 706.09 17.09 3 4 -3 42.99 1.28 -3 -4 3 41.95 1.27 4 4 -3 71.44 2.08 -4 -4 3 81.02 3.40 5 4 -3 81.82 3.36 -5 -4 3 85.36 3.32 6 4 -3 272.10 6.74 -6 -4 3 268.56 9.89 7 4 -3 5.70 0.30 -7 -4 3 5.64 0.34 8 4 -3 164.04 6.38 -8 -4 3 168.49 4.61 9 4 -3 46.08 1.44 -9 -4 3 47.41 1.40 10 4 -3 102.08 2.87 -10 -4 3 91.29 4.02 11 4 -3 6.76 0.44 -11 -4 3 8.55 0.64 12 4 -3 167.59 6.03 -12 -4 3 178.27 6.53 13 4 -3 11.59 0.88 -13 -4 3 10.60 0.60 14 4 -3 2.36 0.39 -14 -4 3 3.55 0.45 15 4 -3 18.79 1.30 -15 -4 3 17.42 0.83 16 4 -3 142.91 4.03 -16 -4 3 156.21 4.50 17 4 -3 6.87 0.59 -17 -4 3 5.67 0.61 18 4 -3 11.03 1.23 -18 -4 3 9.64 1.03 19 4 -3 19.77 1.06 -19 -4 3 20.02 1.20 20 4 -3 67.79 2.25 -20 -4 3 67.49 2.48 21 4 -3 0.42 0.78 -21 -4 3 0.54 0.84 22 4 -3 26.35 2.14 -22 -4 3 23.05 1.27 23 4 -3 11.98 0.97 -23 -4 3 11.70 1.02 24 4 -3 22.49 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1.38 0.82 22 5 -10 18.70 1.37 -22 -5 10 18.43 1.34 23 5 -10 -0.49 1.36 -23 -5 10 0.36 1.01 -26 5 -9 7.13 1.27 26 -5 9 4.87 0.83 -25 5 -9 0.30 0.87 25 -5 9 0.40 0.82 -24 5 -9 2.95 0.70 24 -5 9 3.27 0.72 -23 5 -9 0.20 0.81 23 -5 9 0.59 0.68 -22 5 -9 11.82 1.16 22 -5 9 11.35 0.88 -21 5 -9 -0.12 0.59 21 -5 9 -0.16 0.49 -20 5 -9 15.98 0.95 20 -5 9 17.20 0.95 -19 5 -9 0.54 0.48 19 -5 9 0.85 0.65 -18 5 -9 2.22 0.56 18 -5 9 2.45 0.52 -17 5 -9 1.06 0.49 17 -5 9 1.46 0.46 -16 5 -9 34.56 1.26 16 -5 9 39.38 1.39 -15 5 -9 2.61 0.63 15 -5 9 1.52 0.45 -14 5 -9 1.64 0.54 14 -5 9 1.15 0.39 -13 5 -9 4.42 0.61 13 -5 9 4.03 0.42 -12 5 -9 61.94 2.70 12 -5 9 67.40 2.04 -11 5 -9 5.13 0.40 11 -5 9 4.37 0.40 -10 5 -9 26.09 1.20 10 -5 9 26.62 0.88 -9 5 -9 9.34 0.65 9 -5 9 9.20 0.48 8 -5 9 57.42 1.80 -7 5 -9 5.01 0.52 7 -5 9 4.93 0.29 -6 5 -9 100.03 4.13 6 -5 9 96.18 2.77 -5 5 -9 1.27 0.29 5 -5 9 1.20 0.22 -4 5 -9 17.33 0.84 4 -5 9 19.72 1.15 -3 5 -9 2.25 0.36 3 -5 9 2.71 0.23 -2 5 -9 160.11 4.24 2 -5 9 155.25 4.26 -1 5 -9 1.60 0.21 1 -5 9 0.73 0.18 0 5 -9 0.10 0.21 0 -5 9 0.06 0.16 1 5 -9 1.86 0.26 -1 -5 9 0.83 0.21 2 5 -9 167.22 6.49 -2 -5 9 154.00 3.97 3 5 -9 1.79 0.32 -3 -5 9 2.84 0.26 4 5 -9 18.53 1.08 -4 -5 9 18.75 0.69 5 5 -9 1.64 0.37 -5 -5 9 0.96 0.33 6 5 -9 102.29 4.02 -6 -5 9 91.48 2.59 7 5 -9 5.00 0.38 -7 -5 9 4.26 0.52 8 5 -9 58.60 1.94 -8 -5 9 53.17 2.76 9 5 -9 9.13 0.88 -9 -5 9 7.73 0.64 10 5 -9 25.43 0.99 -10 -5 9 28.53 1.57 11 5 -9 5.02 0.52 -11 -5 9 4.47 0.46 12 5 -9 68.39 3.43 -12 -5 9 82.84 3.65 13 5 -9 3.91 0.48 -13 -5 9 4.98 0.56 14 5 -9 2.23 0.68 -14 -5 9 1.80 0.47 15 5 -9 2.67 0.56 -15 -5 9 2.16 0.60 16 5 -9 44.89 2.23 -16 -5 9 53.74 1.84 17 5 -9 1.69 0.52 -17 -5 9 2.19 0.62 18 5 -9 2.78 0.71 -18 -5 9 3.00 0.71 19 5 -9 1.19 0.63 -19 -5 9 1.66 0.62 20 5 -9 22.43 1.87 -20 -5 9 25.37 1.53 21 5 -9 -0.21 0.70 -21 -5 9 -0.55 0.73 22 5 -9 17.89 1.80 -22 -5 9 15.72 1.24 23 5 -9 0.88 0.92 -23 -5 9 0.42 0.98 24 5 -9 2.33 1.56 -24 -5 9 6.24 1.23 -27 5 -8 0.28 0.99 27 -5 8 0.39 1.07 -26 5 -8 0.77 1.17 26 -5 8 1.16 0.81 -25 5 -8 -0.08 1.52 25 -5 8 0.83 1.14 -24 5 -8 15.51 1.21 24 -5 8 15.16 1.57 -23 5 -8 -0.14 1.11 23 -5 8 0.04 0.86 -22 5 -8 11.15 0.86 22 -5 8 11.99 0.84 -21 5 -8 1.24 0.66 21 -5 8 1.05 0.51 -20 5 -8 10.38 0.76 20 -5 8 8.88 0.77 -19 5 -8 2.48 0.43 19 -5 8 1.29 0.49 -18 5 -8 29.75 1.57 18 -5 8 30.32 1.70 -17 5 -8 0.58 0.38 17 -5 8 0.81 0.36 -16 5 -8 1.39 0.58 16 -5 8 1.27 0.38 -15 5 -8 7.14 0.48 15 -5 8 5.63 0.47 -14 5 -8 57.56 1.92 14 -5 8 57.77 1.81 -13 5 -8 4.39 0.58 13 -5 8 5.18 0.51 -12 5 -8 12.03 0.79 12 -5 8 12.16 0.85 -11 5 -8 12.59 0.68 11 -5 8 10.60 0.49 -10 5 -8 74.68 3.04 10 -5 8 76.48 2.14 -9 5 -8 1.71 0.22 9 -5 8 1.51 0.23 -8 5 -8 81.59 2.30 8 -5 8 82.82 2.35 7 -5 8 7.37 0.33 -6 5 -8 40.68 1.32 6 -5 8 40.69 1.26 5 -5 8 2.57 0.21 -4 5 -8 128.97 4.76 4 -5 8 136.60 5.16 -3 5 -8 13.11 0.50 3 -5 8 13.73 0.51 2 -5 8 8.28 0.36 -1 5 -8 0.92 0.27 1 -5 8 0.21 0.12 0 5 -8 213.83 5.59 0 -5 8 210.53 7.48 1 5 -8 1.15 0.32 -1 -5 8 0.20 0.28 2 5 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1.37 0.84 23 -5 7 1.66 0.67 -22 5 -7 15.81 1.72 22 -5 7 16.99 1.13 -21 5 -7 1.60 0.87 21 -5 7 1.34 0.59 -20 5 -7 22.11 1.06 20 -5 7 25.44 1.69 -19 5 -7 1.72 0.58 19 -5 7 2.74 0.66 -18 5 -7 3.85 0.49 18 -5 7 4.81 0.55 -17 5 -7 2.56 0.54 17 -5 7 2.64 0.44 -16 5 -7 55.46 2.44 16 -5 7 54.69 1.68 15 -5 7 3.11 0.38 -14 5 -7 0.11 0.30 14 -5 7 0.28 0.28 -13 5 -7 9.05 0.46 13 -5 7 10.29 0.53 -12 5 -7 85.41 2.40 12 -5 7 94.27 2.68 -11 5 -7 6.65 0.55 11 -5 7 7.71 0.41 -10 5 -7 48.40 2.07 10 -5 7 50.23 2.09 -9 5 -7 21.93 1.11 9 -5 7 21.92 0.80 -8 5 -7 76.45 3.13 8 -5 7 78.28 3.09 -7 5 -7 3.62 0.24 7 -5 7 3.91 0.26 -6 5 -7 161.03 5.90 6 -5 7 167.38 4.59 5 -5 7 29.75 1.50 4 -5 7 44.63 1.35 -3 5 -7 2.28 0.27 3 -5 7 3.48 0.30 -2 5 -7 258.43 9.24 2 -5 7 276.06 6.90 1 -5 7 5.25 0.26 0 -5 7 0.16 0.12 1 5 -7 6.51 0.53 -1 -5 7 5.35 0.43 2 5 -7 267.24 6.78 -2 -5 7 288.77 10.32 3 5 -7 3.26 0.24 -3 -5 7 3.63 0.29 4 5 -7 49.56 1.64 -4 -5 7 48.89 1.50 5 5 -7 34.70 1.55 -5 -5 7 34.22 1.12 6 5 -7 179.02 4.52 -6 -5 7 184.62 4.54 7 5 -7 3.60 0.34 -7 -5 7 4.28 0.56 8 5 -7 81.63 3.18 -8 -5 7 80.22 2.27 9 5 -7 22.35 0.84 -9 -5 7 22.61 0.90 10 5 -7 46.17 2.34 -10 -5 7 49.04 1.62 11 5 -7 6.53 0.75 -11 -5 7 5.89 0.48 12 5 -7 96.82 3.87 -12 -5 7 115.87 4.37 13 5 -7 10.70 0.89 -13 -5 7 11.19 0.69 14 5 -7 0.13 0.36 -14 -5 7 0.87 0.39 15 5 -7 3.34 0.57 -15 -5 7 3.78 0.53 16 5 -7 75.30 2.27 -16 -5 7 78.47 3.46 17 5 -7 3.62 0.60 -17 -5 7 2.65 1.06 18 5 -7 4.74 0.61 -18 -5 7 8.43 1.15 19 5 -7 2.08 0.74 -19 -5 7 3.02 0.94 20 5 -7 31.41 1.46 -20 -5 7 37.28 2.44 21 5 -7 2.45 0.68 -21 -5 7 3.43 1.08 22 5 -7 19.92 1.88 -22 -5 7 25.55 1.43 23 5 -7 1.37 0.82 -23 -5 7 1.61 0.90 24 5 -7 7.80 1.27 -24 -5 7 8.12 1.36 25 5 -7 0.57 1.38 -25 -5 7 0.49 1.60 -28 5 -6 9.36 1.26 28 -5 6 9.11 1.58 -27 5 -6 -0.55 1.21 27 -5 6 0.62 1.36 26 -5 6 2.33 0.90 -25 5 -6 -0.05 0.93 25 -5 6 0.41 1.05 -24 5 -6 15.44 1.36 24 -5 6 15.71 1.08 -23 5 -6 -0.02 0.53 23 -5 6 -0.04 0.53 -22 5 -6 14.58 1.17 22 -5 6 14.86 0.96 -21 5 -6 1.05 0.46 21 -5 6 0.97 0.47 -20 5 -6 12.58 0.82 20 -5 6 12.67 0.79 -19 5 -6 0.25 0.47 19 -5 6 0.17 0.43 -18 5 -6 37.42 1.91 18 -5 6 40.81 1.45 -17 5 -6 3.40 0.71 17 -5 6 3.99 0.62 -16 5 -6 1.71 0.35 16 -5 6 1.47 0.30 -15 5 -6 4.39 0.57 15 -5 6 4.72 0.46 -14 5 -6 67.70 1.89 14 -5 6 65.67 1.95 -13 5 -6 2.37 0.36 13 -5 6 2.75 0.29 -12 5 -6 18.80 0.75 12 -5 6 17.86 0.96 -11 5 -6 6.23 0.49 11 -5 6 4.06 0.31 -10 5 -6 103.97 3.06 10 -5 6 101.40 2.87 -9 5 -6 1.89 0.28 9 -5 6 2.12 0.19 -8 5 -6 97.60 3.92 8 -5 6 104.78 2.99 7 -5 6 8.88 0.37 6 -5 6 47.12 1.43 5 -5 6 0.35 0.09 4 -5 6 200.47 5.04 3 -5 6 1.39 0.15 2 -5 6 13.94 0.47 1 -5 6 11.82 0.43 0 5 -6 315.43 11.78 0 -5 6 314.95 7.93 1 5 -6 10.38 0.42 -1 -5 6 12.15 0.45 2 5 -6 18.71 0.86 -2 -5 6 14.80 0.75 3 5 -6 0.66 0.19 -3 -5 6 1.56 0.18 4 5 -6 214.34 5.90 -4 -5 6 222.65 5.64 5 5 -6 0.51 0.25 -5 -5 6 0.35 0.20 6 5 -6 53.42 1.62 -6 -5 6 55.40 2.27 7 5 -6 5.86 0.50 -7 -5 6 8.47 0.63 8 5 -6 105.40 3.01 -8 -5 6 109.57 3.07 9 5 -6 2.40 0.30 -9 -5 6 2.13 0.34 10 5 -6 107.56 3.02 -10 -5 6 102.18 4.87 11 5 -6 5.89 0.51 -11 -5 6 3.80 0.47 12 5 -6 19.90 1.25 -12 -5 6 19.80 0.95 13 5 -6 3.42 0.42 -13 -5 6 3.71 0.47 14 5 -6 88.29 2.61 -14 -5 6 84.33 3.28 15 5 -6 4.90 0.62 -15 -5 6 6.17 0.74 16 5 -6 2.69 0.55 -16 -5 6 2.32 0.58 17 5 -6 5.16 1.12 -17 -5 6 5.99 0.82 18 5 -6 57.02 2.02 -18 -5 6 54.27 2.03 19 5 -6 0.39 0.61 -19 -5 6 0.42 0.61 20 5 -6 18.19 1.18 -20 -5 6 17.57 1.77 21 5 -6 1.90 0.65 -21 -5 6 0.85 0.99 22 5 -6 21.75 1.86 -22 -5 6 20.26 1.32 23 5 -6 0.32 0.77 -23 -5 6 0.05 0.84 24 5 -6 22.08 1.43 -24 -5 6 21.15 1.56 25 5 -6 0.69 1.20 -25 -5 6 0.81 2.12 -28 5 -5 -0.12 0.89 28 -5 5 0.29 1.17 27 -5 5 1.49 1.25 -26 5 -5 14.11 1.07 26 -5 5 13.47 1.11 -25 5 -5 0.31 0.73 25 -5 5 0.34 0.80 -24 5 -5 7.38 0.96 24 -5 5 5.51 0.74 -23 5 -5 2.63 0.74 23 -5 5 0.69 0.81 -22 5 -5 20.25 1.53 22 -5 5 21.65 1.71 -21 5 -5 1.81 0.55 21 -5 5 1.35 0.65 -20 5 -5 35.38 1.37 20 -5 5 34.82 1.80 -19 5 -5 1.52 0.71 19 -5 5 1.61 0.77 -18 5 -5 7.31 0.53 18 -5 5 7.36 0.84 -17 5 -5 3.48 0.43 17 -5 5 3.26 0.45 -16 5 -5 67.79 2.91 16 -5 5 61.25 1.87 -15 5 -5 3.27 0.39 15 -5 5 3.33 0.38 -14 5 -5 0.80 0.25 14 -5 5 0.57 0.27 -13 5 -5 3.06 0.44 13 -5 5 2.53 0.39 -12 5 -5 139.99 4.98 12 -5 5 120.33 3.37 -11 5 -5 3.88 0.30 11 -5 5 4.43 0.43 -10 5 -5 45.40 1.97 10 -5 5 44.77 1.42 -9 5 -5 15.56 0.81 9 -5 5 15.17 0.63 -8 5 -5 93.70 3.70 8 -5 5 93.76 3.79 -7 5 -5 7.62 0.44 7 -5 5 7.65 0.32 5 -5 5 9.98 0.55 1 -5 5 17.09 0.53 0 5 -5 0.04 0.12 1 5 -5 22.47 1.07 -1 -5 5 17.18 0.83 2 5 -5 330.45 8.38 -2 -5 5 329.94 11.36 -3 -5 5 1.28 0.22 4 5 -5 49.68 2.20 -4 -5 5 42.03 1.31 5 5 -5 13.63 0.89 -5 -5 5 13.70 0.81 6 5 -5 186.59 5.10 -6 -5 5 194.56 7.33 7 5 -5 9.02 0.45 -7 -5 5 9.59 0.62 8 5 -5 112.26 4.12 -8 -5 5 108.10 2.89 9 5 -5 15.84 0.67 -9 -5 5 16.65 0.67 10 5 -5 48.80 1.50 -10 -5 5 47.79 1.45 11 5 -5 4.03 0.67 -11 -5 5 3.90 0.59 12 5 -5 153.03 4.29 -12 -5 5 124.87 4.03 13 5 -5 3.50 0.44 -13 -5 5 3.15 0.56 14 5 -5 1.03 0.55 -14 -5 5 0.98 0.39 15 5 -5 3.40 0.51 -15 -5 5 3.73 0.49 16 5 -5 94.49 2.88 -16 -5 5 85.86 2.49 17 5 -5 4.43 0.83 -17 -5 5 3.64 0.54 18 5 -5 10.69 1.25 -18 -5 5 11.63 1.22 19 5 -5 3.51 0.62 -19 -5 5 2.83 0.91 20 5 -5 53.37 3.20 -20 -5 5 45.00 2.06 21 5 -5 1.85 0.90 -21 -5 5 2.20 1.01 22 5 -5 26.75 1.39 -22 -5 5 30.28 1.52 23 5 -5 2.20 0.89 -23 -5 5 3.71 1.01 24 5 -5 12.09 1.19 -24 -5 5 10.26 1.23 25 5 -5 -0.85 0.98 -25 -5 5 0.02 1.22 -28 5 -4 9.68 1.47 28 -5 4 11.14 1.69 -27 5 -4 0.00 1.09 27 -5 4 0.21 1.12 -26 5 -4 2.48 1.04 26 -5 4 2.34 0.79 -25 5 -4 1.61 0.92 25 -5 4 0.91 0.77 -24 5 -4 14.51 1.00 24 -5 4 19.24 1.73 -23 5 -4 1.02 1.01 23 -5 4 0.31 0.61 -22 5 -4 22.38 1.41 22 -5 4 19.19 1.10 -21 5 -4 1.87 0.48 21 -5 4 1.92 0.50 -20 5 -4 15.22 0.91 20 -5 4 16.75 0.85 -19 5 -4 3.13 0.60 19 -5 4 3.09 0.49 -18 5 -4 66.89 2.69 18 -5 4 62.83 1.95 -17 5 -4 2.21 0.50 17 -5 4 3.48 0.41 -16 5 -4 1.34 0.35 16 -5 4 1.61 0.35 -15 5 -4 9.91 0.87 15 -5 4 12.93 0.63 -14 5 -4 103.77 3.97 14 -5 4 96.44 3.94 13 -5 4 0.53 0.22 -12 5 -4 8.78 0.55 12 -5 4 10.36 0.47 -11 5 -4 22.37 1.02 11 -5 4 26.56 1.25 -10 5 -4 128.14 4.66 10 -5 4 118.89 3.24 -9 5 -4 2.88 0.30 9 -5 4 3.13 0.32 -8 5 -4 89.05 3.61 8 -5 4 97.97 3.91 -7 5 -4 15.62 0.78 7 -5 4 13.93 0.65 6 -5 4 77.31 2.04 0 -5 4 267.79 9.34 -1 -5 4 8.86 0.51 -2 -5 4 10.05 0.39 3 5 -4 11.58 0.67 -3 -5 4 6.58 0.45 4 5 -4 255.36 9.35 -4 -5 4 271.93 7.05 5 5 -4 5.07 0.27 -5 -5 4 5.12 0.41 6 5 -4 97.90 2.70 -6 -5 4 96.27 2.67 7 5 -4 16.32 0.65 -7 -5 4 17.40 0.73 8 5 -4 101.78 2.76 -8 -5 4 110.74 4.62 9 5 -4 4.35 0.46 -9 -5 4 3.15 0.35 10 5 -4 131.64 3.49 -10 -5 4 131.41 3.46 11 5 -4 23.47 0.86 -11 -5 4 27.57 1.04 12 5 -4 8.83 0.58 -12 -5 4 12.27 0.97 13 5 -4 1.72 0.36 -13 -5 4 0.72 0.51 14 5 -4 128.42 5.09 -14 -5 4 123.09 4.71 15 5 -4 12.46 1.08 -15 -5 4 16.28 1.25 16 5 -4 2.38 0.46 -16 -5 4 1.47 0.64 17 5 -4 5.34 0.89 -17 -5 4 5.25 0.65 18 5 -4 92.28 2.87 -18 -5 4 83.83 2.55 19 5 -4 4.42 0.62 -19 -5 4 4.39 0.61 20 5 -4 19.96 1.05 -20 -5 4 22.03 1.75 21 5 -4 2.64 0.87 -21 -5 4 3.10 0.93 22 5 -4 30.52 1.42 -22 -5 4 28.56 1.97 23 5 -4 1.59 0.76 -23 -5 4 0.63 0.74 24 5 -4 21.88 1.52 -24 -5 4 24.43 1.67 25 5 -4 1.83 1.06 -25 -5 4 1.71 1.17 -29 5 -3 -0.44 0.78 29 -5 3 0.41 1.07 -28 5 -3 -0.82 2.24 28 -5 3 0.69 1.12 -27 5 -3 0.28 0.87 27 -5 3 1.34 0.91 -26 5 -3 10.23 1.04 26 -5 3 12.59 1.12 -25 5 -3 0.79 1.16 25 -5 3 0.11 0.93 -24 5 -3 7.00 0.74 24 -5 3 5.73 0.79 -23 5 -3 0.67 0.59 23 -5 3 0.01 0.49 -22 5 -3 12.01 1.05 22 -5 3 12.11 0.87 -21 5 -3 0.04 0.48 21 -5 3 0.27 0.62 -20 5 -3 36.88 1.98 20 -5 3 34.39 1.35 -19 5 -3 1.54 0.75 19 -5 3 2.20 0.46 -18 5 -3 5.83 0.68 18 -5 3 6.95 0.60 -17 5 -3 0.50 0.44 17 -5 3 1.36 0.37 -16 5 -3 81.94 3.49 16 -5 3 74.84 2.21 -15 5 -3 3.74 0.47 15 -5 3 2.91 0.35 -14 5 -3 2.63 0.28 14 -5 3 3.90 0.35 -13 5 -3 1.05 0.28 13 -5 3 1.80 0.30 -12 5 -3 110.10 4.23 12 -5 3 105.92 2.82 -11 5 -3 4.86 0.41 11 -5 3 5.65 0.45 -10 5 -3 26.84 1.16 10 -5 3 29.92 1.38 9 -5 3 4.58 0.25 -8 5 -3 112.27 4.41 8 -5 3 111.01 2.98 -7 5 -3 5.65 0.35 7 -5 3 5.81 0.36 1 5 -3 2.51 0.20 -1 -5 3 0.88 0.12 2 5 -3 212.84 5.73 -2 -5 3 231.29 8.29 3 5 -3 9.13 0.54 -3 -5 3 8.00 0.46 4 5 -3 42.71 1.87 -4 -5 3 35.79 1.12 5 5 -3 4.53 0.27 -5 -5 3 7.06 0.54 6 5 -3 154.63 5.78 -6 -5 3 171.73 4.64 7 5 -3 7.23 0.38 -7 -5 3 6.20 0.51 8 5 -3 124.60 3.22 -8 -5 3 127.47 3.47 9 5 -3 4.02 0.33 -9 -5 3 4.56 0.51 10 5 -3 30.16 1.04 -10 -5 3 32.20 1.11 11 5 -3 5.44 0.40 -11 -5 3 6.29 0.44 12 5 -3 100.18 5.21 -12 -5 3 97.47 3.29 13 5 -3 1.23 0.38 -13 -5 3 1.79 0.43 14 5 -3 3.68 0.48 -14 -5 3 4.24 0.48 15 5 -3 3.78 0.49 -15 -5 3 4.39 0.73 16 5 -3 117.34 3.44 -16 -5 3 102.64 2.98 17 5 -3 1.19 0.79 -17 -5 3 2.26 0.68 18 5 -3 8.52 0.73 -18 -5 3 9.83 0.83 19 5 -3 2.02 0.53 -19 -5 3 1.98 0.56 20 5 -3 52.12 1.89 -20 -5 3 46.00 2.06 21 5 -3 -0.25 1.14 -21 -5 3 0.32 0.83 22 5 -3 17.06 1.65 -22 -5 3 17.39 1.57 23 5 -3 0.83 0.71 -23 -5 3 -0.17 0.73 24 5 -3 11.66 1.60 -24 -5 3 10.96 1.56 25 5 -3 -0.75 1.84 -25 -5 3 -0.33 1.05 -26 -5 3 10.13 2.04 -29 5 -2 0.61 1.72 29 -5 2 -0.36 1.05 -28 5 -2 9.36 1.56 28 -5 2 11.34 1.30 -27 5 -2 0.00 1.00 27 -5 2 0.72 0.91 -26 5 -2 2.94 1.07 26 -5 2 4.16 1.55 -25 5 -2 2.70 0.93 25 -5 2 1.28 0.71 -24 5 -2 12.98 1.31 24 -5 2 14.30 0.94 -23 5 -2 0.39 0.56 23 -5 2 0.16 1.01 -22 5 -2 26.77 1.64 22 -5 2 22.56 1.12 -21 5 -2 0.92 0.42 21 -5 2 1.43 0.64 -20 5 -2 11.14 0.70 20 -5 2 10.96 0.69 -19 5 -2 0.75 0.41 19 -5 2 0.64 0.53 -18 5 -2 75.91 2.46 18 -5 2 70.43 3.14 -17 5 -2 2.84 0.50 17 -5 2 3.11 0.50 -16 5 -2 1.03 0.33 16 -5 2 0.83 0.40 -15 5 -2 1.91 0.33 15 -5 2 3.16 0.40 -14 5 -2 138.08 3.75 14 -5 2 145.33 3.90 -13 5 -2 2.25 0.36 13 -5 2 1.73 0.26 -12 5 -2 15.77 1.04 12 -5 2 18.40 0.71 -11 5 -2 9.69 0.43 11 -5 2 7.97 0.55 -10 5 -2 172.10 4.59 10 -5 2 177.35 4.61 -9 5 -2 2.71 0.24 9 -5 2 2.79 0.27 -8 5 -2 75.67 3.00 8 -5 2 77.49 2.11 -7 5 -2 21.41 0.97 7 -5 2 19.59 0.84 1 5 -2 30.81 0.94 -1 -5 2 26.46 1.16 2 5 -2 22.07 0.94 -2 -5 2 23.78 1.11 3 5 -2 47.86 1.47 -3 -5 2 40.43 1.30 4 5 -2 249.84 9.08 -4 -5 2 259.63 7.03 5 5 -2 5.09 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5 7 86.46 2.46 12 -5 -7 94.75 4.08 -11 5 7 6.53 0.67 11 -5 -7 5.74 0.52 -10 5 7 52.67 2.20 10 -5 -7 48.58 2.26 -9 5 7 22.30 1.23 9 -5 -7 21.44 0.83 -8 5 7 84.50 3.06 8 -5 -7 80.56 2.29 -7 5 7 4.10 0.41 7 -5 -7 3.57 0.53 -6 5 7 189.04 4.75 6 -5 -7 179.77 6.82 -5 5 7 34.08 1.01 5 -5 -7 37.15 1.24 -4 5 7 52.20 1.62 4 -5 -7 51.92 1.60 -3 5 7 3.87 0.34 3 -5 -7 3.18 0.55 -2 5 7 315.45 7.86 2 -5 -7 289.78 11.15 -1 5 7 7.08 0.53 1 -5 -7 8.04 0.44 0 5 7 0.11 0.20 0 -5 -7 0.06 0.20 1 5 7 6.59 0.57 -1 -5 -7 7.75 0.47 2 5 7 322.01 7.94 -2 -5 -7 299.25 7.76 3 5 7 3.74 0.33 -3 -5 -7 2.21 0.30 4 5 7 51.84 1.69 -4 -5 -7 52.41 2.33 5 5 7 38.19 1.26 -5 -5 -7 38.69 1.91 6 5 7 199.97 5.25 -6 -5 -7 192.64 4.93 7 5 7 4.45 0.45 -7 -5 -7 4.54 0.45 8 5 7 93.45 2.77 -8 -5 -7 94.03 3.95 9 5 7 29.19 1.09 -9 -5 -7 27.26 1.36 10 5 7 68.79 2.56 -10 -5 -7 64.73 1.99 11 5 7 10.09 0.99 -11 -5 -7 8.35 0.63 12 5 7 129.52 3.80 -12 -5 -7 127.01 3.60 13 5 7 14.21 0.85 -13 -5 -7 12.85 0.82 14 5 7 0.57 0.48 -14 -5 -7 0.60 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