data_r20190409e _audit_creation_date 2019-04-10 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _shelx_SHELXL_version_number '2018/3' _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_name '' _audit_contact_author_phone ? _audit_update_record ; ???? ; _publ_contact_author_id_orcid ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C40 H38 N2 O2, 0.5(C3 H6 O)' _chemical_formula_sum 'C41.50 H41 N2 O2.50' _chemical_formula_weight 607.76 _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'monoclinic' _space_group_IT_number 14 _space_group_name_H-M_alt 'P 1 21/c 1' _space_group_name_Hall '-P 2ybc' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 21.705(8) _cell_length_b 18.455(6) _cell_length_c 17.774(7) _cell_angle_alpha 90 _cell_angle_beta 112.216(6) _cell_angle_gamma 90 _cell_volume 6591(4) _cell_formula_units_Z 8 _cell_measurement_reflns_used 17306 _cell_measurement_temperature 128.15 _cell_measurement_theta_max 27.9263 _cell_measurement_theta_min 1.4982 _shelx_estimated_absorpt_T_max 0.985 _shelx_estimated_absorpt_T_min 0.973 _exptl_absorpt_coefficient_mu 0.076 _exptl_absorpt_correction_T_max 1.0000 _exptl_absorpt_correction_T_min 0.9272 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'CrystalClear(Rigaku, 2008)' _exptl_absorpt_special_details ? _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.225 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description prism _exptl_crystal_F_000 2592 _exptl_crystal_size_max 0.36 _exptl_crystal_size_mid 0.22 _exptl_crystal_size_min 0.2 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0753 _diffrn_reflns_av_unetI/netI 0.0548 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.993 _diffrn_reflns_limit_h_max 28 _diffrn_reflns_limit_h_min -28 _diffrn_reflns_limit_k_max 24 _diffrn_reflns_limit_k_min -24 _diffrn_reflns_limit_l_max 23 _diffrn_reflns_limit_l_min -23 _diffrn_reflns_number 78677 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.993 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.927 _diffrn_reflns_theta_min 1.013 _diffrn_ambient_temperature 128.15 _diffrn_detector_area_resol_mean ? _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.993 _diffrn_measurement_device ; Saturn70 (4x4 bin mode) ; _diffrn_measurement_device_details ; AFC10: Fixed Chi 2 circle ; _diffrn_measurement_device_type 'Rigaku Saturn 70' _diffrn_measurement_method '\w scans' _diffrn_radiation_detector CCD _diffrn_radiation_monochromator Confocal _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71075 _diffrn_source 'Rotating Anode' _diffrn_standards_decay_% 0 _diffrn_standards_interval_count 0 _diffrn_standards_interval_time 0 _diffrn_standards_number 0 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 11898 _reflns_number_total 15706 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'CrystalClear (Rigaku Inc., 2008)' _computing_data_collection 'CrystalClear (Rigaku Inc., 2008)' _computing_data_reduction 'CrystalClear (Rigaku Inc., 2008)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _refine_diff_density_max 0.404 _refine_diff_density_min -0.310 _refine_diff_density_rms 0.044 _refine_ls_extinction_coef 0.0055(4) _refine_ls_extinction_expression 'Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^' _refine_ls_extinction_method 'SHELXL-2018/3 (Sheldrick 2018)' _refine_ls_goodness_of_fit_ref 1.138 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 836 _refine_ls_number_reflns 15706 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0907 _refine_ls_R_factor_gt 0.0647 _refine_ls_restrained_S_all 1.138 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0621P)^2^+0.5955P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1375 _refine_ls_wR_factor_ref 0.1531 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C1(H1), C3(H3), C4(H4), C5(H5), C6(H6), C8(H8), C9(H9), C10(H10), C41(H41), C43(H43), C44(H44), C45(H45), C47(H47), C48(H48), C49(H49), C50(H50) 2.b Secondary CH2 refined with riding coordinates: C27(H27A,H27B), C34(H34A,H34B), C67(H67A,H67B), C74(H74A,H74B) 2.c Aromatic/amide H refined with riding coordinates: C16(H16), C17(H17), C18(H18), C19(H19), C20(H20), C22(H22), C23(H23), C24(H24), C25(H25), C26(H26), C29(H29), C30(H30), C31(H31), C32(H32), C33(H33), C36(H36), C37(H37), C38(H38), C39(H39), C40(H40), C56(H56), C57(H57), C58(H58), C59(H59), C60(H60), C62(H62), C63(H63), C64(H64), C65(H65), C66(H66), C69(H69), C70(H70), C71(H71), C72(H72), C73(H73), C76(H76), C77(H77), C78(H78), C79(H79), C80(H80) 2.d Idealised Me refined as rotating group: C12(H12A,H12B,H12C), C14(H14A,H14B,H14C), C52(H52A,H52B,H52C), C54(H54A,H54B, H54C), C81(H81A,H81B,H81C), C83(H83A,H83B,H83C) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.83340(8) 0.07814(8) 0.84145(8) 0.0489(4) Uani 1 1 d . . . . . O2 O 0.83616(7) 0.42329(8) 0.78612(9) 0.0476(4) Uani 1 1 d . . . . . N1 N 0.82604(7) 0.25998(8) 0.92907(8) 0.0260(3) Uani 1 1 d . . . . . N2 N 0.93538(7) 0.25022(7) 0.82162(8) 0.0248(3) Uani 1 1 d . . . . . C1 C 0.88524(8) 0.21999(9) 0.97755(10) 0.0246(4) Uani 1 1 d . . . . . H1 H 0.878319 0.189663 1.020320 0.029 Uiso 1 1 calc R . . . . C2 C 0.90629(8) 0.17305(9) 0.91595(10) 0.0256(4) Uani 1 1 d . . . . . C3 C 0.98299(8) 0.17677(9) 0.95528(10) 0.0264(4) Uani 1 1 d . . . . . H3 H 0.995766 0.153947 1.010125 0.032 Uiso 1 1 calc R . . . . C4 C 0.99111(8) 0.25904(9) 0.97012(10) 0.0254(4) Uani 1 1 d . . . . . H4 H 1.038116 0.273063 1.003186 0.030 Uiso 1 1 calc R . . . . C5 C 0.94373(8) 0.27536(9) 1.01392(10) 0.0250(4) Uani 1 1 d . . . . . H5 H 0.966221 0.270761 1.074269 0.030 Uiso 1 1 calc R . . . . C6 C 0.92052(8) 0.35335(9) 0.98744(10) 0.0256(4) Uani 1 1 d . . . . . H6 H 0.961196 0.384565 1.006638 0.031 Uiso 1 1 calc R . . . . C7 C 0.89999(8) 0.34388(9) 0.89444(10) 0.0249(4) Uani 1 1 d . . . . . C8 C 0.84382(8) 0.28571(9) 0.86202(10) 0.0257(4) Uani 1 1 d . . . . . H8 H 0.804347 0.303947 0.815240 0.031 Uiso 1 1 calc R . . . . C9 C 0.87916(8) 0.22042(9) 0.83728(10) 0.0250(4) Uani 1 1 d . . . . . H9 H 0.847933 0.192894 0.789667 0.030 Uiso 1 1 calc R . . . . C10 C 0.96173(8) 0.30204(9) 0.88816(10) 0.0249(4) Uani 1 1 d . . . . . H10 H 0.995009 0.335720 0.880554 0.030 Uiso 1 1 calc R . . . . C11 C 0.87695(9) 0.09696(10) 0.90460(11) 0.0312(4) Uani 1 1 d . . . . . C12 C 0.90232(11) 0.04489(11) 0.97454(13) 0.0454(5) Uani 1 1 d . . . . . H12A H 0.877312 -0.000595 0.959731 0.068 Uiso 1 1 calc GR . . . . H12B H 0.896566 0.065966 1.022073 0.068 Uiso 1 1 calc GR . . . . H12C H 0.949634 0.035307 0.987467 0.068 Uiso 1 1 calc GR . . . . C13 C 0.88574(9) 0.41475(9) 0.84689(11) 0.0297(4) Uani 1 1 d . . . . . C14 C 0.93541(11) 0.47482(11) 0.87717(12) 0.0430(5) Uani 1 1 d . . . . . H14A H 0.928320 0.510242 0.833609 0.064 Uiso 1 1 calc GR . . . . H14B H 0.980508 0.454945 0.894168 0.064 Uiso 1 1 calc GR . . . . H14C H 0.929903 0.498575 0.923543 0.064 Uiso 1 1 calc GR . . . . C15 C 1.02564(9) 0.14057(9) 0.91537(11) 0.0292(4) Uani 1 1 d . . . . . C16 C 1.00007(10) 0.09486(10) 0.84829(11) 0.0359(4) Uani 1 1 d . . . . . H16 H 0.953421 0.086792 0.824430 0.043 Uiso 1 1 calc R . . . . C17 C 1.04146(11) 0.06073(11) 0.81546(13) 0.0430(5) Uani 1 1 d . . . . . H17 H 1.022815 0.030133 0.769396 0.052 Uiso 1 1 calc R . . . . C18 C 1.10931(12) 0.07114(12) 0.84948(13) 0.0482(6) Uani 1 1 d . . . . . H18 H 1.137599 0.047935 0.827133 0.058 Uiso 1 1 calc R . . . . C19 C 1.13585(11) 0.11601(12) 0.91688(14) 0.0467(5) Uani 1 1 d . . . . . H19 H 1.182567 0.123540 0.940899 0.056 Uiso 1 1 calc R . . . . C20 C 1.09420(10) 0.14992(11) 0.94925(12) 0.0375(4) Uani 1 1 d . . . . . H20 H 1.113058 0.180176 0.995583 0.045 Uiso 1 1 calc R . . . . C21 C 0.87174(9) 0.38668(9) 1.02019(10) 0.0278(4) Uani 1 1 d . . . . . C22 C 0.88825(10) 0.38870(10) 1.10415(11) 0.0357(4) Uani 1 1 d . . . . . H22 H 0.930286 0.370748 1.139400 0.043 Uiso 1 1 calc R . . . . C23 C 0.84435(11) 0.41648(11) 1.13726(12) 0.0438(5) Uani 1 1 d . . . . . H23 H 0.856196 0.415959 1.194476 0.053 Uiso 1 1 calc R . . . . C24 C 0.78409(11) 0.44462(11) 1.08773(12) 0.0418(5) Uani 1 1 d . . . . . H24 H 0.754003 0.463127 1.110310 0.050 Uiso 1 1 calc R . . . . C25 C 0.76757(10) 0.44571(10) 1.00408(12) 0.0361(4) Uani 1 1 d . . . . . H25 H 0.726587 0.466399 0.969390 0.043 Uiso 1 1 calc R . . . . C26 C 0.81068(9) 0.41677(9) 0.97137(11) 0.0309(4) Uani 1 1 d . . . . . H26 H 0.798409 0.417374 0.914092 0.037 Uiso 1 1 calc R . . . . C27 C 0.76337(9) 0.21954(11) 0.90340(11) 0.0335(4) Uani 1 1 d . . . . . H27A H 0.765764 0.177610 0.869876 0.040 Uiso 1 1 calc R . . . . H27B H 0.726465 0.251161 0.869511 0.040 Uiso 1 1 calc R . . . . C28 C 0.74929(8) 0.19294(10) 0.97576(11) 0.0315(4) Uani 1 1 d . . . . . C29 C 0.75237(9) 0.24022(11) 1.03789(11) 0.0346(4) Uani 1 1 d . . . . . H29 H 0.763964 0.289520 1.035183 0.042 Uiso 1 1 calc R . . . . C30 C 0.73861(10) 0.21604(13) 1.10412(12) 0.0437(5) Uani 1 1 d . . . . . H30 H 0.740384 0.248997 1.145950 0.052 Uiso 1 1 calc R . . . . C31 C 0.72243(12) 0.14444(15) 1.10922(14) 0.0573(7) Uani 1 1 d . . . . . H31 H 0.713353 0.127787 1.154556 0.069 Uiso 1 1 calc R . . . . C32 C 0.71956(14) 0.09731(14) 1.04786(15) 0.0643(7) Uani 1 1 d . . . . . H32 H 0.708235 0.047975 1.050974 0.077 Uiso 1 1 calc R . . . . C33 C 0.73298(11) 0.12101(12) 0.98167(13) 0.0479(5) Uani 1 1 d . . . . . H33 H 0.731017 0.087772 0.940008 0.058 Uiso 1 1 calc R . . . . C34 C 0.91764(8) 0.28036(10) 0.73964(10) 0.0275(4) Uani 1 1 d . . . . . H34A H 0.889707 0.324008 0.733890 0.033 Uiso 1 1 calc R . . . . H34B H 0.891228 0.244283 0.699020 0.033 Uiso 1 1 calc R . . . . C35 C 0.97870(9) 0.30022(10) 0.72318(10) 0.0281(4) Uani 1 1 d . . . . . C36 C 0.98383(10) 0.36734(10) 0.68976(11) 0.0356(4) Uani 1 1 d . . . . . H36 H 0.949113 0.401875 0.679212 0.043 Uiso 1 1 calc R . . . . C37 C 1.03896(11) 0.38415(12) 0.67180(12) 0.0437(5) Uani 1 1 d . . . . . H37 H 1.042089 0.430294 0.649826 0.052 Uiso 1 1 calc R . . . . C38 C 1.08946(10) 0.33404(13) 0.68574(12) 0.0457(5) Uani 1 1 d . . . . . H38 H 1.126759 0.345202 0.672231 0.055 Uiso 1 1 calc R . . . . C39 C 1.08531(9) 0.26765(12) 0.71942(11) 0.0396(5) Uani 1 1 d . . . . . H39 H 1.120017 0.233198 0.729310 0.048 Uiso 1 1 calc R . . . . C40 C 1.03077(9) 0.25094(10) 0.73890(11) 0.0328(4) Uani 1 1 d . . . . . H40 H 1.028907 0.205545 0.763155 0.039 Uiso 1 1 calc R . . . . O3 O 0.65392(7) 0.57176(7) 0.43642(9) 0.0431(3) Uani 1 1 d . . . . . O4 O 0.64735(7) 0.91998(7) 0.48453(9) 0.0456(4) Uani 1 1 d . . . . . N3 N 0.65963(7) 0.73549(8) 0.58466(8) 0.0245(3) Uani 1 1 d . . . . . N4 N 0.55103(7) 0.74461(8) 0.37595(8) 0.0253(3) Uani 1 1 d . . . . . C41 C 0.64229(8) 0.70994(9) 0.50107(10) 0.0246(4) Uani 1 1 d . . . . . H41 H 0.682027 0.692226 0.490981 0.029 Uiso 1 1 calc R . . . . C42 C 0.58684(8) 0.65107(9) 0.48170(10) 0.0246(4) Uani 1 1 d . . . . . C43 C 0.56541(8) 0.64128(9) 0.55478(10) 0.0250(4) Uani 1 1 d . . . . . H43 H 0.524489 0.610459 0.534920 0.030 Uiso 1 1 calc R . . . . C44 C 0.54176(8) 0.71889(9) 0.56022(10) 0.0244(3) Uani 1 1 d . . . . . H44 H 0.519041 0.723080 0.599592 0.029 Uiso 1 1 calc R . . . . C45 C 0.59969(8) 0.77516(9) 0.57768(10) 0.0238(3) Uani 1 1 d . . . . . H45 H 0.606151 0.805445 0.626752 0.029 Uiso 1 1 calc R . . . . C46 C 0.57893(8) 0.82209(9) 0.49715(10) 0.0249(4) Uani 1 1 d . . . . . C47 C 0.50218(8) 0.81746(9) 0.46588(10) 0.0255(4) Uani 1 1 d . . . . . H47 H 0.489469 0.839483 0.509367 0.031 Uiso 1 1 calc R . . . . C48 C 0.49475(8) 0.73500(9) 0.47258(10) 0.0249(4) Uani 1 1 d . . . . . H48 H 0.447804 0.720445 0.461884 0.030 Uiso 1 1 calc R . . . . C49 C 0.52493(8) 0.69218(9) 0.41789(10) 0.0249(4) Uani 1 1 d . . . . . H49 H 0.492091 0.658186 0.379459 0.030 Uiso 1 1 calc R . . . . C50 C 0.60650(8) 0.77508(9) 0.44346(10) 0.0243(3) Uani 1 1 d . . . . . H50 H 0.637618 0.802969 0.424828 0.029 Uiso 1 1 calc R . . . . C51 C 0.60344(9) 0.58011(10) 0.44942(10) 0.0297(4) Uani 1 1 d . . . . . C52 C 0.55537(11) 0.51824(11) 0.43586(13) 0.0451(5) Uani 1 1 d . . . . . H52A H 0.567599 0.479181 0.406794 0.068 Uiso 1 1 calc GR . . . . H52B H 0.510233 0.535021 0.403527 0.068 Uiso 1 1 calc GR . . . . H52C H 0.556957 0.500177 0.488409 0.068 Uiso 1 1 calc GR . . . . C53 C 0.60669(9) 0.89898(10) 0.51165(11) 0.0306(4) Uani 1 1 d . . . . . C54 C 0.58278(10) 0.94893(10) 0.56153(12) 0.0404(5) Uani 1 1 d . . . . . H54A H 0.595767 0.929504 0.616694 0.061 Uiso 1 1 calc GR . . . . H54B H 0.534197 0.952983 0.536617 0.061 Uiso 1 1 calc GR . . . . H54C H 0.602750 0.996914 0.563830 0.061 Uiso 1 1 calc GR . . . . C55 C 0.61247(9) 0.60592(9) 0.63226(10) 0.0277(4) Uani 1 1 d . . . . . C56 C 0.67411(9) 0.57733(10) 0.64108(11) 0.0341(4) Uani 1 1 d . . . . . H56 H 0.689647 0.582585 0.598070 0.041 Uiso 1 1 calc R . . . . C57 C 0.71314(11) 0.54150(12) 0.71101(12) 0.0443(5) Uani 1 1 d . . . . . H57 H 0.754774 0.521723 0.715392 0.053 Uiso 1 1 calc R . . . . C58 C 0.69177(12) 0.53432(13) 0.77474(13) 0.0534(6) Uani 1 1 d . . . . . H58 H 0.718557 0.509573 0.822884 0.064 Uiso 1 1 calc R . . . . C59 C 0.63129(13) 0.56333(14) 0.76796(13) 0.0564(6) Uani 1 1 d . . . . . H59 H 0.616669 0.559263 0.811863 0.068 Uiso 1 1 calc R . . . . C60 C 0.59192(10) 0.59835(11) 0.69719(11) 0.0388(5) Uani 1 1 d . . . . . H60 H 0.550111 0.617578 0.692854 0.047 Uiso 1 1 calc R . . . . C61 C 0.45950(9) 0.85474(9) 0.38755(10) 0.0289(4) Uani 1 1 d . . . . . C62 C 0.39038(9) 0.85148(10) 0.36358(12) 0.0365(4) Uani 1 1 d . . . . . H62 H 0.371639 0.824366 0.395118 0.044 Uiso 1 1 calc R . . . . C63 C 0.34874(11) 0.88726(12) 0.29438(13) 0.0480(6) Uani 1 1 d . . . . . H63 H 0.301852 0.884102 0.278791 0.058 Uiso 1 1 calc R . . . . C64 C 0.37504(12) 0.92758(12) 0.24784(12) 0.0484(6) Uani 1 1 d . . . . . H64 H 0.346501 0.952143 0.200528 0.058 Uiso 1 1 calc R . . . . C65 C 0.44300(11) 0.93156(11) 0.27105(12) 0.0430(5) Uani 1 1 d . . . . . H65 H 0.461474 0.959151 0.239573 0.052 Uiso 1 1 calc R . . . . C66 C 0.48494(10) 0.89553(10) 0.34024(11) 0.0353(4) Uani 1 1 d . . . . . H66 H 0.531770 0.898879 0.355378 0.042 Uiso 1 1 calc R . . . . C67 C 0.72193(8) 0.77715(10) 0.61489(10) 0.0298(4) Uani 1 1 d . . . . . H67A H 0.720790 0.814484 0.574387 0.036 Uiso 1 1 calc R . . . . H67B H 0.759805 0.744341 0.621949 0.036 Uiso 1 1 calc R . . . . C68 C 0.73209(8) 0.81316(10) 0.69461(11) 0.0304(4) Uani 1 1 d . . . . . C69 C 0.73147(9) 0.77331(11) 0.76097(11) 0.0364(4) Uani 1 1 d . . . . . H69 H 0.725526 0.722267 0.756656 0.044 Uiso 1 1 calc R . . . . C70 C 0.73953(10) 0.80813(14) 0.83337(12) 0.0475(6) Uani 1 1 d . . . . . H70 H 0.738408 0.780825 0.878140 0.057 Uiso 1 1 calc R . . . . C71 C 0.74922(10) 0.88262(15) 0.84077(14) 0.0533(6) Uani 1 1 d . . . . . H71 H 0.754988 0.906136 0.890530 0.064 Uiso 1 1 calc R . . . . C72 C 0.75041(10) 0.92209(13) 0.77584(15) 0.0516(6) Uani 1 1 d . . . . . H72 H 0.757326 0.972983 0.780728 0.062 Uiso 1 1 calc R . . . . C73 C 0.74151(9) 0.88761(11) 0.70311(13) 0.0388(5) Uani 1 1 d . . . . . H73 H 0.741872 0.915427 0.658309 0.047 Uiso 1 1 calc R . . . . C74 C 0.57028(9) 0.71452(10) 0.31124(10) 0.0281(4) Uani 1 1 d . . . . . H74A H 0.600641 0.672938 0.333010 0.034 Uiso 1 1 calc R . . . . H74B H 0.594580 0.751865 0.293399 0.034 Uiso 1 1 calc R . . . . C75 C 0.51083(9) 0.69005(10) 0.23974(10) 0.0281(4) Uani 1 1 d . . . . . C76 C 0.50720(11) 0.62060(11) 0.20859(12) 0.0416(5) Uani 1 1 d . . . . . H76 H 0.542323 0.587324 0.234101 0.050 Uiso 1 1 calc R . . . . C77 C 0.45307(13) 0.59901(14) 0.14077(13) 0.0558(6) Uani 1 1 d . . . . . H77 H 0.450726 0.550953 0.120705 0.067 Uiso 1 1 calc R . . . . C78 C 0.40271(12) 0.64751(16) 0.10263(13) 0.0578(7) Uani 1 1 d . . . . . H78 H 0.365912 0.633181 0.055561 0.069 Uiso 1 1 calc R . . . . C79 C 0.40561(10) 0.71685(14) 0.13262(12) 0.0476(6) Uani 1 1 d . . . . . H79 H 0.370978 0.750321 0.105872 0.057 Uiso 1 1 calc R . . . . C80 C 0.45876(9) 0.73785(11) 0.20151(11) 0.0355(4) Uani 1 1 d . . . . . H80 H 0.459724 0.785210 0.222876 0.043 Uiso 1 1 calc R . . . . O5 O 0.91123(10) 0.59322(12) 0.99920(13) 0.0843(7) Uani 1 1 d . . . . . C81 C 0.86986(14) 0.61444(19) 1.10067(17) 0.0806(9) Uani 1 1 d . . . . . H81A H 0.908945 0.586870 1.135085 0.121 Uiso 1 1 calc GR . . . . H81B H 0.829597 0.592599 1.103369 0.121 Uiso 1 1 calc GR . . . . H81C H 0.873764 0.664661 1.119847 0.121 Uiso 1 1 calc GR . . . . C82 C 0.86578(12) 0.61325(12) 1.01616(14) 0.0499(6) Uani 1 1 d . . . . . C83 C 0.80240(19) 0.6403(2) 0.9553(2) 0.1148(14) Uani 1 1 d . . . . . H83A H 0.796538 0.691313 0.966245 0.172 Uiso 1 1 calc GR . . . . H83B H 0.765361 0.611769 0.958425 0.172 Uiso 1 1 calc GR . . . . H83C H 0.803303 0.635640 0.900760 0.172 Uiso 1 1 calc GR . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0596(10) 0.0397(8) 0.0390(8) -0.0054(7) 0.0093(7) -0.0209(7) O2 0.0475(9) 0.0396(8) 0.0443(8) 0.0138(7) 0.0045(7) 0.0104(7) N1 0.0231(7) 0.0297(8) 0.0242(7) 0.0026(6) 0.0077(6) 0.0005(6) N2 0.0259(7) 0.0256(7) 0.0224(7) -0.0008(6) 0.0084(6) -0.0022(6) C1 0.0251(8) 0.0238(8) 0.0241(8) 0.0025(7) 0.0086(7) 0.0005(7) C2 0.0265(8) 0.0242(8) 0.0253(8) -0.0005(7) 0.0088(7) -0.0009(7) C3 0.0276(9) 0.0237(8) 0.0265(9) 0.0022(7) 0.0088(7) 0.0013(7) C4 0.0226(8) 0.0250(8) 0.0262(8) -0.0016(7) 0.0065(7) -0.0004(7) C5 0.0256(8) 0.0261(8) 0.0211(8) 0.0000(7) 0.0063(7) 0.0013(7) C6 0.0266(8) 0.0234(8) 0.0256(8) -0.0015(7) 0.0084(7) 0.0000(7) C7 0.0269(8) 0.0234(8) 0.0239(8) 0.0009(7) 0.0090(7) 0.0012(7) C8 0.0251(8) 0.0271(9) 0.0230(8) 0.0007(7) 0.0067(7) 0.0015(7) C9 0.0242(8) 0.0256(8) 0.0234(8) -0.0001(7) 0.0071(7) -0.0010(7) C10 0.0241(8) 0.0245(8) 0.0254(8) -0.0020(7) 0.0083(7) -0.0005(7) C11 0.0354(10) 0.0271(9) 0.0333(10) -0.0028(8) 0.0156(8) -0.0033(8) C12 0.0561(13) 0.0268(10) 0.0487(12) 0.0037(9) 0.0146(11) -0.0038(9) C13 0.0377(10) 0.0276(9) 0.0274(9) 0.0027(7) 0.0164(8) 0.0073(8) C14 0.0578(13) 0.0306(10) 0.0421(11) 0.0031(9) 0.0207(10) -0.0040(10) C15 0.0343(9) 0.0227(8) 0.0319(9) 0.0053(7) 0.0140(8) 0.0059(7) C16 0.0425(11) 0.0289(9) 0.0386(10) -0.0005(8) 0.0178(9) 0.0050(8) C17 0.0602(14) 0.0312(10) 0.0445(12) -0.0008(9) 0.0275(11) 0.0081(10) C18 0.0609(14) 0.0413(12) 0.0569(14) 0.0070(11) 0.0388(12) 0.0179(11) C19 0.0381(11) 0.0473(12) 0.0618(14) 0.0068(11) 0.0270(11) 0.0088(10) C20 0.0345(10) 0.0362(10) 0.0428(11) 0.0004(9) 0.0158(9) 0.0031(8) C21 0.0332(9) 0.0216(8) 0.0293(9) -0.0016(7) 0.0127(8) -0.0005(7) C22 0.0430(11) 0.0327(10) 0.0311(10) -0.0015(8) 0.0137(9) 0.0073(9) C23 0.0612(14) 0.0429(12) 0.0306(10) -0.0038(9) 0.0211(10) 0.0085(10) C24 0.0514(12) 0.0352(10) 0.0470(12) -0.0055(9) 0.0280(10) 0.0078(9) C25 0.0366(10) 0.0300(9) 0.0433(11) -0.0007(9) 0.0168(9) 0.0058(8) C26 0.0364(10) 0.0280(9) 0.0282(9) 0.0001(7) 0.0120(8) 0.0031(8) C27 0.0269(9) 0.0420(11) 0.0299(9) -0.0011(8) 0.0088(8) -0.0042(8) C28 0.0232(8) 0.0366(10) 0.0321(9) 0.0024(8) 0.0074(8) -0.0019(7) C29 0.0299(9) 0.0377(10) 0.0365(10) 0.0033(8) 0.0128(8) 0.0006(8) C30 0.0338(10) 0.0637(15) 0.0341(11) 0.0023(10) 0.0135(9) 0.0000(10) C31 0.0517(14) 0.0776(18) 0.0412(12) 0.0165(12) 0.0159(11) -0.0156(13) C32 0.0768(18) 0.0540(15) 0.0552(15) 0.0116(12) 0.0171(13) -0.0263(13) C33 0.0526(13) 0.0426(12) 0.0430(12) -0.0018(10) 0.0116(10) -0.0117(10) C34 0.0286(9) 0.0300(9) 0.0238(8) 0.0007(7) 0.0099(7) 0.0020(7) C35 0.0300(9) 0.0328(9) 0.0202(8) -0.0021(7) 0.0082(7) -0.0021(7) C36 0.0416(11) 0.0350(10) 0.0294(9) 0.0036(8) 0.0126(8) -0.0008(8) C37 0.0474(12) 0.0496(13) 0.0318(10) 0.0063(9) 0.0124(9) -0.0152(10) C38 0.0350(11) 0.0696(15) 0.0325(10) 0.0004(10) 0.0128(9) -0.0135(11) C39 0.0287(10) 0.0551(13) 0.0327(10) -0.0025(9) 0.0090(8) 0.0021(9) C40 0.0319(9) 0.0358(10) 0.0290(9) -0.0008(8) 0.0094(8) -0.0002(8) O3 0.0548(9) 0.0336(7) 0.0543(9) -0.0022(7) 0.0357(7) 0.0063(7) O4 0.0559(9) 0.0349(8) 0.0531(9) -0.0030(7) 0.0284(8) -0.0149(7) N3 0.0221(7) 0.0272(7) 0.0236(7) -0.0017(6) 0.0082(6) -0.0001(6) N4 0.0272(7) 0.0268(7) 0.0234(7) 0.0000(6) 0.0114(6) -0.0010(6) C41 0.0242(8) 0.0264(8) 0.0256(8) 0.0011(7) 0.0122(7) 0.0016(7) C42 0.0278(8) 0.0248(8) 0.0234(8) -0.0001(7) 0.0121(7) 0.0009(7) C43 0.0288(9) 0.0238(8) 0.0243(8) -0.0018(7) 0.0122(7) -0.0021(7) C44 0.0258(8) 0.0257(8) 0.0245(8) 0.0001(7) 0.0127(7) -0.0009(7) C45 0.0235(8) 0.0241(8) 0.0243(8) -0.0010(7) 0.0096(7) 0.0012(7) C46 0.0246(8) 0.0247(8) 0.0249(8) -0.0002(7) 0.0089(7) 0.0011(7) C47 0.0254(8) 0.0252(8) 0.0266(8) -0.0013(7) 0.0106(7) 0.0021(7) C48 0.0231(8) 0.0271(9) 0.0251(8) -0.0012(7) 0.0098(7) -0.0017(7) C49 0.0238(8) 0.0266(8) 0.0242(8) -0.0004(7) 0.0090(7) -0.0019(7) C50 0.0236(8) 0.0242(8) 0.0258(8) 0.0011(7) 0.0101(7) 0.0006(7) C51 0.0402(10) 0.0277(9) 0.0239(9) 0.0013(7) 0.0150(8) 0.0033(8) C52 0.0592(13) 0.0305(10) 0.0511(12) -0.0137(9) 0.0272(11) -0.0090(10) C53 0.0303(9) 0.0257(9) 0.0307(9) 0.0037(8) 0.0058(8) 0.0002(7) C54 0.0419(11) 0.0254(9) 0.0503(12) -0.0048(9) 0.0133(10) 0.0022(8) C55 0.0371(10) 0.0216(8) 0.0250(9) -0.0003(7) 0.0127(8) 0.0003(7) C56 0.0407(10) 0.0346(10) 0.0306(9) 0.0032(8) 0.0174(8) 0.0065(8) C57 0.0499(12) 0.0448(12) 0.0386(11) 0.0089(9) 0.0171(10) 0.0198(10) C58 0.0634(15) 0.0610(15) 0.0348(11) 0.0178(11) 0.0175(11) 0.0247(12) C59 0.0696(16) 0.0721(16) 0.0379(11) 0.0218(12) 0.0318(12) 0.0243(13) C60 0.0434(11) 0.0443(11) 0.0339(10) 0.0077(9) 0.0203(9) 0.0080(9) C61 0.0316(9) 0.0238(8) 0.0290(9) -0.0032(7) 0.0091(8) 0.0049(7) C62 0.0313(10) 0.0353(10) 0.0371(10) 0.0003(9) 0.0065(8) 0.0031(8) C63 0.0352(11) 0.0449(12) 0.0479(13) -0.0054(10) -0.0023(10) 0.0099(10) C64 0.0577(14) 0.0409(12) 0.0319(11) -0.0006(9) 0.0004(10) 0.0180(10) C65 0.0633(14) 0.0325(10) 0.0324(10) 0.0054(9) 0.0170(10) 0.0122(10) C66 0.0399(10) 0.0301(9) 0.0352(10) 0.0039(8) 0.0134(9) 0.0074(8) C67 0.0252(9) 0.0333(9) 0.0299(9) 0.0019(8) 0.0092(8) -0.0010(7) C68 0.0203(8) 0.0340(10) 0.0331(10) -0.0020(8) 0.0059(7) 0.0004(7) C69 0.0292(9) 0.0450(11) 0.0322(10) -0.0015(9) 0.0084(8) -0.0003(8) C70 0.0313(10) 0.0763(17) 0.0332(11) -0.0043(11) 0.0103(9) -0.0006(11) C71 0.0275(10) 0.0785(18) 0.0493(13) -0.0333(13) 0.0092(10) 0.0005(11) C72 0.0332(11) 0.0457(13) 0.0673(16) -0.0236(12) 0.0094(11) 0.0012(10) C73 0.0288(9) 0.0330(10) 0.0483(12) -0.0019(9) 0.0075(9) -0.0007(8) C74 0.0306(9) 0.0310(9) 0.0255(9) 0.0026(7) 0.0137(7) 0.0033(7) C75 0.0318(9) 0.0340(9) 0.0228(8) 0.0024(7) 0.0153(7) -0.0002(8) C76 0.0547(13) 0.0382(11) 0.0335(10) -0.0015(9) 0.0186(10) 0.0013(10) C77 0.0709(17) 0.0572(15) 0.0416(12) -0.0168(11) 0.0240(12) -0.0210(13) C78 0.0437(13) 0.095(2) 0.0343(11) -0.0122(13) 0.0141(10) -0.0257(14) C79 0.0290(10) 0.0782(17) 0.0355(11) 0.0042(11) 0.0119(9) 0.0009(11) C80 0.0323(10) 0.0442(11) 0.0335(10) 0.0035(9) 0.0163(8) 0.0032(8) O5 0.0671(12) 0.0974(15) 0.1037(15) -0.0549(13) 0.0498(12) -0.0296(11) C81 0.0586(17) 0.117(3) 0.0734(19) -0.0213(18) 0.0335(15) -0.0303(17) C82 0.0511(13) 0.0377(12) 0.0582(14) -0.0085(11) 0.0175(12) -0.0158(10) C83 0.098(3) 0.113(3) 0.098(3) 0.033(2) -0.002(2) -0.002(2) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C11 1.213(2) . ? O2 C13 1.213(2) . ? N1 C1 1.449(2) . ? N1 C8 1.464(2) . ? N1 C27 1.465(2) . ? N2 C9 1.458(2) . ? N2 C10 1.459(2) . ? N2 C34 1.468(2) . ? C1 H1 1.0000 . ? C1 C2 1.593(2) . ? C1 C5 1.566(2) . ? C2 C3 1.544(2) . ? C2 C9 1.563(2) . ? C2 C11 1.524(2) . ? C3 H3 1.0000 . ? C3 C4 1.540(2) . ? C3 C15 1.518(2) . ? C4 H4 1.0000 . ? C4 C5 1.536(2) . ? C4 C10 1.567(2) . ? C5 H5 1.0000 . ? C5 C6 1.539(2) . ? C6 H6 1.0000 . ? C6 C7 1.550(2) . ? C6 C21 1.518(2) . ? C7 C8 1.562(2) . ? C7 C10 1.587(2) . ? C7 C13 1.524(2) . ? C8 H8 1.0000 . ? C8 C9 1.578(2) . ? C9 H9 1.0000 . ? C10 H10 1.0000 . ? C11 C12 1.501(3) . ? C12 H12A 0.9800 . ? C12 H12B 0.9800 . ? C12 H12C 0.9800 . ? C13 C14 1.497(3) . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C14 H14C 0.9800 . ? C15 C16 1.393(3) . ? C15 C20 1.389(3) . ? C16 H16 0.9500 . ? C16 C17 1.393(3) . ? C17 H17 0.9500 . ? C17 C18 1.378(3) . ? C18 H18 0.9500 . ? C18 C19 1.389(3) . ? C19 H19 0.9500 . ? C19 C20 1.390(3) . ? C20 H20 0.9500 . ? C21 C22 1.397(2) . ? C21 C26 1.396(2) . ? C22 H22 0.9500 . ? C22 C23 1.393(3) . ? C23 H23 0.9500 . ? C23 C24 1.373(3) . ? C24 H24 0.9500 . ? C24 C25 1.391(3) . ? C25 H25 0.9500 . ? C25 C26 1.382(3) . ? C26 H26 0.9500 . ? C27 H27A 0.9900 . ? C27 H27B 0.9900 . ? C27 C28 1.512(3) . ? C28 C29 1.389(3) . ? C28 C33 1.388(3) . ? C29 H29 0.9500 . ? C29 C30 1.393(3) . ? C30 H30 0.9500 . ? C30 C31 1.379(3) . ? C31 H31 0.9500 . ? C31 C32 1.378(4) . ? C32 H32 0.9500 . ? C32 C33 1.385(3) . ? C33 H33 0.9500 . ? C34 H34A 0.9900 . ? C34 H34B 0.9900 . ? C34 C35 1.507(2) . ? C35 C36 1.396(3) . ? C35 C40 1.394(3) . ? C36 H36 0.9500 . ? C36 C37 1.385(3) . ? C37 H37 0.9500 . ? C37 C38 1.383(3) . ? C38 H38 0.9500 . ? C38 C39 1.381(3) . ? C39 H39 0.9500 . ? C39 C40 1.388(3) . ? C40 H40 0.9500 . ? O3 C51 1.212(2) . ? O4 C53 1.218(2) . ? N3 C41 1.466(2) . ? N3 C45 1.457(2) . ? N3 C67 1.469(2) . ? N4 C49 1.460(2) . ? N4 C50 1.454(2) . ? N4 C74 1.473(2) . ? C41 H41 1.0000 . ? C41 C42 1.560(2) . ? C41 C50 1.580(2) . ? C42 C43 1.547(2) . ? C42 C49 1.586(2) . ? C42 C51 1.527(2) . ? C43 H43 1.0000 . ? C43 C44 1.537(2) . ? C43 C55 1.517(2) . ? C44 H44 1.0000 . ? C44 C45 1.568(2) . ? C44 C48 1.534(2) . ? C45 H45 1.0000 . ? C45 C46 1.586(2) . ? C46 C47 1.546(2) . ? C46 C50 1.566(2) . ? C46 C53 1.525(2) . ? C47 H47 1.0000 . ? C47 C48 1.540(2) . ? C47 C61 1.515(2) . ? C48 H48 1.0000 . ? C48 C49 1.575(2) . ? C49 H49 1.0000 . ? C50 H50 1.0000 . ? C51 C52 1.503(3) . ? C52 H52A 0.9800 . ? C52 H52B 0.9800 . ? C52 H52C 0.9800 . ? C53 C54 1.501(3) . ? C54 H54A 0.9800 . ? C54 H54B 0.9800 . ? C54 H54C 0.9800 . ? C55 C56 1.391(3) . ? C55 C60 1.393(3) . ? C56 H56 0.9500 . ? C56 C57 1.380(3) . ? C57 H57 0.9500 . ? C57 C58 1.383(3) . ? C58 H58 0.9500 . ? C58 C59 1.380(3) . ? C59 H59 0.9500 . ? C59 C60 1.385(3) . ? C60 H60 0.9500 . ? C61 C62 1.397(3) . ? C61 C66 1.389(3) . ? C62 H62 0.9500 . ? C62 C63 1.388(3) . ? C63 H63 0.9500 . ? C63 C64 1.386(3) . ? C64 H64 0.9500 . ? C64 C65 1.375(3) . ? C65 H65 0.9500 . ? C65 C66 1.392(3) . ? C66 H66 0.9500 . ? C67 H67A 0.9900 . ? C67 H67B 0.9900 . ? C67 C68 1.504(2) . ? C68 C69 1.394(3) . ? C68 C73 1.389(3) . ? C69 H69 0.9500 . ? C69 C70 1.389(3) . ? C70 H70 0.9500 . ? C70 C71 1.389(3) . ? C71 H71 0.9500 . ? C71 C72 1.373(4) . ? C72 H72 0.9500 . ? C72 C73 1.387(3) . ? C73 H73 0.9500 . ? C74 H74A 0.9900 . ? C74 H74B 0.9900 . ? C74 C75 1.498(2) . ? C75 C76 1.387(3) . ? C75 C80 1.392(3) . ? C76 H76 0.9500 . ? C76 C77 1.386(3) . ? C77 H77 0.9500 . ? C77 C78 1.377(4) . ? C78 H78 0.9500 . ? C78 C79 1.378(4) . ? C79 H79 0.9500 . ? C79 C80 1.383(3) . ? C80 H80 0.9500 . ? O5 C82 1.194(3) . ? C81 H81A 0.9800 . ? C81 H81B 0.9800 . ? C81 H81C 0.9800 . ? C81 C82 1.471(3) . ? C82 C83 1.479(4) . ? C83 H83A 0.9800 . ? C83 H83B 0.9800 . ? C83 H83C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1 N1 C8 101.64(13) . . ? C1 N1 C27 115.85(14) . . ? C8 N1 C27 114.29(13) . . ? C9 N2 C10 101.09(13) . . ? C9 N2 C34 114.08(13) . . ? C10 N2 C34 115.55(14) . . ? N1 C1 H1 112.5 . . ? N1 C1 C2 106.77(13) . . ? N1 C1 C5 108.14(13) . . ? C2 C1 H1 112.5 . . ? C5 C1 H1 112.5 . . ? C5 C1 C2 103.89(13) . . ? C3 C2 C1 101.83(13) . . ? C3 C2 C9 110.93(14) . . ? C9 C2 C1 101.64(13) . . ? C11 C2 C1 112.22(14) . . ? C11 C2 C3 115.21(14) . . ? C11 C2 C9 113.57(14) . . ? C2 C3 H3 106.1 . . ? C4 C3 C2 98.94(13) . . ? C4 C3 H3 106.1 . . ? C15 C3 C2 120.83(15) . . ? C15 C3 H3 106.1 . . ? C15 C3 C4 117.62(15) . . ? C3 C4 H4 112.4 . . ? C3 C4 C10 111.11(13) . . ? C5 C4 C3 103.00(13) . . ? C5 C4 H4 112.4 . . ? C5 C4 C10 104.87(13) . . ? C10 C4 H4 112.4 . . ? C1 C5 H5 112.2 . . ? C4 C5 C1 104.86(13) . . ? C4 C5 H5 112.2 . . ? C4 C5 C6 103.47(13) . . ? C6 C5 C1 111.31(13) . . ? C6 C5 H5 112.2 . . ? C5 C6 H6 106.8 . . ? C5 C6 C7 98.60(13) . . ? C7 C6 H6 106.8 . . ? C21 C6 C5 117.18(14) . . ? C21 C6 H6 106.8 . . ? C21 C6 C7 119.58(14) . . ? C6 C7 C8 109.91(13) . . ? C6 C7 C10 102.70(13) . . ? C8 C7 C10 101.65(13) . . ? C13 C7 C6 114.24(14) . . ? C13 C7 C8 114.76(14) . . ? C13 C7 C10 112.22(14) . . ? N1 C8 C7 109.38(13) . . ? N1 C8 H8 112.3 . . ? N1 C8 C9 106.55(13) . . ? C7 C8 H8 112.3 . . ? C7 C8 C9 103.52(13) . . ? C9 C8 H8 112.3 . . ? N2 C9 C2 108.80(13) . . ? N2 C9 C8 107.18(13) . . ? N2 C9 H9 112.2 . . ? C2 C9 C8 103.67(13) . . ? C2 C9 H9 112.2 . . ? C8 C9 H9 112.2 . . ? N2 C10 C4 108.57(13) . . ? N2 C10 C7 107.05(13) . . ? N2 C10 H10 112.3 . . ? C4 C10 C7 103.80(13) . . ? C4 C10 H10 112.3 . . ? C7 C10 H10 112.3 . . ? O1 C11 C2 121.79(16) . . ? O1 C11 C12 119.76(17) . . ? C12 C11 C2 118.44(16) . . ? C11 C12 H12A 109.5 . . ? C11 C12 H12B 109.5 . . ? C11 C12 H12C 109.5 . . ? H12A C12 H12B 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? O2 C13 C7 122.08(17) . . ? O2 C13 C14 119.99(17) . . ? C14 C13 C7 117.93(15) . . ? C13 C14 H14A 109.5 . . ? C13 C14 H14B 109.5 . . ? C13 C14 H14C 109.5 . . ? H14A C14 H14B 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? C16 C15 C3 123.41(17) . . ? C20 C15 C3 119.05(16) . . ? C20 C15 C16 117.46(17) . . ? C15 C16 H16 119.3 . . ? C15 C16 C17 121.39(19) . . ? C17 C16 H16 119.3 . . ? C16 C17 H17 119.8 . . ? C18 C17 C16 120.3(2) . . ? C18 C17 H17 119.8 . . ? C17 C18 H18 120.4 . . ? C17 C18 C19 119.16(19) . . ? C19 C18 H18 120.4 . . ? C18 C19 H19 119.9 . . ? C18 C19 C20 120.2(2) . . ? C20 C19 H19 119.9 . . ? C15 C20 C19 121.49(19) . . ? C15 C20 H20 119.3 . . ? C19 C20 H20 119.3 . . ? C22 C21 C6 119.08(16) . . ? C26 C21 C6 123.97(15) . . ? C26 C21 C22 116.94(16) . . ? C21 C22 H22 119.3 . . ? C23 C22 C21 121.39(18) . . ? C23 C22 H22 119.3 . . ? C22 C23 H23 119.8 . . ? C24 C23 C22 120.41(18) . . ? C24 C23 H23 119.8 . . ? C23 C24 H24 120.4 . . ? C23 C24 C25 119.26(18) . . ? C25 C24 H24 120.4 . . ? C24 C25 H25 119.9 . . ? C26 C25 C24 120.12(18) . . ? C26 C25 H25 119.9 . . ? C21 C26 H26 119.1 . . ? C25 C26 C21 121.81(17) . . ? C25 C26 H26 119.1 . . ? N1 C27 H27A 109.4 . . ? N1 C27 H27B 109.4 . . ? N1 C27 C28 111.29(14) . . ? H27A C27 H27B 108.0 . . ? C28 C27 H27A 109.4 . . ? C28 C27 H27B 109.4 . . ? C29 C28 C27 120.52(17) . . ? C33 C28 C27 120.95(18) . . ? C33 C28 C29 118.53(18) . . ? C28 C29 H29 119.7 . . ? C28 C29 C30 120.62(19) . . ? C30 C29 H29 119.7 . . ? C29 C30 H30 119.9 . . ? C31 C30 C29 120.3(2) . . ? C31 C30 H30 119.9 . . ? C30 C31 H31 120.4 . . ? C32 C31 C30 119.3(2) . . ? C32 C31 H31 120.4 . . ? C31 C32 H32 119.6 . . ? C31 C32 C33 120.8(2) . . ? C33 C32 H32 119.6 . . ? C28 C33 H33 119.7 . . ? C32 C33 C28 120.5(2) . . ? C32 C33 H33 119.7 . . ? N2 C34 H34A 109.3 . . ? N2 C34 H34B 109.3 . . ? N2 C34 C35 111.41(14) . . ? H34A C34 H34B 108.0 . . ? C35 C34 H34A 109.3 . . ? C35 C34 H34B 109.3 . . ? C36 C35 C34 121.06(16) . . ? C40 C35 C34 120.56(16) . . ? C40 C35 C36 118.36(17) . . ? C35 C36 H36 119.6 . . ? C37 C36 C35 120.77(19) . . ? C37 C36 H36 119.6 . . ? C36 C37 H37 119.9 . . ? C38 C37 C36 120.3(2) . . ? C38 C37 H37 119.9 . . ? C37 C38 H38 120.2 . . ? C39 C38 C37 119.57(19) . . ? C39 C38 H38 120.2 . . ? C38 C39 H39 119.8 . . ? C38 C39 C40 120.44(19) . . ? C40 C39 H39 119.8 . . ? C35 C40 H40 119.7 . . ? C39 C40 C35 120.55(18) . . ? C39 C40 H40 119.7 . . ? C41 N3 C67 112.77(13) . . ? C45 N3 C41 101.34(12) . . ? C45 N3 C67 115.92(14) . . ? C49 N4 C74 115.35(14) . . ? C50 N4 C49 101.24(13) . . ? C50 N4 C74 113.54(14) . . ? N3 C41 H41 112.2 . . ? N3 C41 C42 109.19(13) . . ? N3 C41 C50 106.68(13) . . ? C42 C41 H41 112.2 . . ? C42 C41 C50 103.74(13) . . ? C50 C41 H41 112.2 . . ? C41 C42 C49 101.49(13) . . ? C43 C42 C41 110.36(13) . . ? C43 C42 C49 102.36(13) . . ? C51 C42 C41 114.09(14) . . ? C51 C42 C43 113.82(14) . . ? C51 C42 C49 113.47(14) . . ? C42 C43 H43 106.2 . . ? C44 C43 C42 99.06(13) . . ? C44 C43 H43 106.2 . . ? C55 C43 C42 119.97(15) . . ? C55 C43 H43 106.2 . . ? C55 C43 C44 118.03(14) . . ? C43 C44 H44 112.4 . . ? C43 C44 C45 111.57(13) . . ? C45 C44 H44 112.4 . . ? C48 C44 C43 103.09(13) . . ? C48 C44 H44 112.4 . . ? C48 C44 C45 104.38(13) . . ? N3 C45 C44 107.90(13) . . ? N3 C45 H45 112.4 . . ? N3 C45 C46 106.93(13) . . ? C44 C45 H45 112.4 . . ? C44 C45 C46 104.48(12) . . ? C46 C45 H45 112.4 . . ? C47 C46 C45 101.19(13) . . ? C47 C46 C50 110.99(13) . . ? C50 C46 C45 101.76(13) . . ? C53 C46 C45 113.36(13) . . ? C53 C46 C47 114.53(14) . . ? C53 C46 C50 113.63(14) . . ? C46 C47 H47 105.9 . . ? C48 C47 C46 99.03(13) . . ? C48 C47 H47 105.9 . . ? C61 C47 C46 120.45(14) . . ? C61 C47 H47 105.9 . . ? C61 C47 C48 118.32(14) . . ? C44 C48 C47 102.77(13) . . ? C44 C48 H48 112.3 . . ? C44 C48 C49 104.90(13) . . ? C47 C48 H48 112.3 . . ? C47 C48 C49 111.59(14) . . ? C49 C48 H48 112.3 . . ? N4 C49 C42 107.15(13) . . ? N4 C49 C48 108.35(13) . . ? N4 C49 H49 112.4 . . ? C42 C49 H49 112.4 . . ? C48 C49 C42 103.67(13) . . ? C48 C49 H49 112.4 . . ? N4 C50 C41 106.95(13) . . ? N4 C50 C46 109.22(13) . . ? N4 C50 H50 112.2 . . ? C41 C50 H50 112.2 . . ? C46 C50 C41 103.54(13) . . ? C46 C50 H50 112.2 . . ? O3 C51 C42 122.65(17) . . ? O3 C51 C52 119.70(17) . . ? C52 C51 C42 117.63(16) . . ? C51 C52 H52A 109.5 . . ? C51 C52 H52B 109.5 . . ? C51 C52 H52C 109.5 . . ? H52A C52 H52B 109.5 . . ? H52A C52 H52C 109.5 . . ? H52B C52 H52C 109.5 . . ? O4 C53 C46 121.89(17) . . ? O4 C53 C54 120.16(17) . . ? C54 C53 C46 117.94(16) . . ? C53 C54 H54A 109.5 . . ? C53 C54 H54B 109.5 . . ? C53 C54 H54C 109.5 . . ? H54A C54 H54B 109.5 . . ? H54A C54 H54C 109.5 . . ? H54B C54 H54C 109.5 . . ? C56 C55 C43 123.65(16) . . ? C56 C55 C60 117.67(16) . . ? C60 C55 C43 118.60(16) . . ? C55 C56 H56 119.3 . . ? C57 C56 C55 121.35(18) . . ? C57 C56 H56 119.3 . . ? C56 C57 H57 119.9 . . ? C56 C57 C58 120.1(2) . . ? C58 C57 H57 119.9 . . ? C57 C58 H58 120.2 . . ? C59 C58 C57 119.59(19) . . ? C59 C58 H58 120.2 . . ? C58 C59 H59 120.0 . . ? C58 C59 C60 120.0(2) . . ? C60 C59 H59 120.0 . . ? C55 C60 H60 119.4 . . ? C59 C60 C55 121.23(19) . . ? C59 C60 H60 119.4 . . ? C62 C61 C47 118.28(16) . . ? C66 C61 C47 123.87(16) . . ? C66 C61 C62 117.75(17) . . ? C61 C62 H62 119.5 . . ? C63 C62 C61 121.0(2) . . ? C63 C62 H62 119.5 . . ? C62 C63 H63 119.8 . . ? C64 C63 C62 120.5(2) . . ? C64 C63 H63 119.8 . . ? C63 C64 H64 120.4 . . ? C65 C64 C63 119.14(19) . . ? C65 C64 H64 120.4 . . ? C64 C65 H65 119.7 . . ? C64 C65 C66 120.6(2) . . ? C66 C65 H65 119.7 . . ? C61 C66 C65 121.12(19) . . ? C61 C66 H66 119.4 . . ? C65 C66 H66 119.4 . . ? N3 C67 H67A 109.4 . . ? N3 C67 H67B 109.4 . . ? N3 C67 C68 111.26(14) . . ? H67A C67 H67B 108.0 . . ? C68 C67 H67A 109.4 . . ? C68 C67 H67B 109.4 . . ? C69 C68 C67 121.26(17) . . ? C73 C68 C67 120.19(17) . . ? C73 C68 C69 118.54(18) . . ? C68 C69 H69 119.9 . . ? C70 C69 C68 120.1(2) . . ? C70 C69 H69 119.9 . . ? C69 C70 H70 119.8 . . ? C69 C70 C71 120.5(2) . . ? C71 C70 H70 119.8 . . ? C70 C71 H71 120.1 . . ? C72 C71 C70 119.7(2) . . ? C72 C71 H71 120.1 . . ? C71 C72 H72 120.0 . . ? C71 C72 C73 120.0(2) . . ? C73 C72 H72 120.0 . . ? C68 C73 H73 119.4 . . ? C72 C73 C68 121.2(2) . . ? C72 C73 H73 119.4 . . ? N4 C74 H74A 109.3 . . ? N4 C74 H74B 109.3 . . ? N4 C74 C75 111.61(14) . . ? H74A C74 H74B 108.0 . . ? C75 C74 H74A 109.3 . . ? C75 C74 H74B 109.3 . . ? C76 C75 C74 121.20(17) . . ? C76 C75 C80 118.55(17) . . ? C80 C75 C74 120.21(17) . . ? C75 C76 H76 119.5 . . ? C77 C76 C75 121.0(2) . . ? C77 C76 H76 119.5 . . ? C76 C77 H77 120.2 . . ? C78 C77 C76 119.7(2) . . ? C78 C77 H77 120.2 . . ? C77 C78 H78 120.0 . . ? C77 C78 C79 120.1(2) . . ? C79 C78 H78 120.0 . . ? C78 C79 H79 119.9 . . ? C78 C79 C80 120.2(2) . . ? C80 C79 H79 119.9 . . ? C75 C80 H80 119.8 . . ? C79 C80 C75 120.4(2) . . ? C79 C80 H80 119.8 . . ? H81A C81 H81B 109.5 . . ? H81A C81 H81C 109.5 . . ? H81B C81 H81C 109.5 . . ? C82 C81 H81A 109.5 . . ? C82 C81 H81B 109.5 . . ? C82 C81 H81C 109.5 . . ? O5 C82 C81 121.7(2) . . ? O5 C82 C83 123.3(3) . . ? C81 C82 C83 115.0(3) . . ? C82 C83 H83A 109.5 . . ? C82 C83 H83B 109.5 . . ? C82 C83 H83C 109.5 . . ? H83A C83 H83B 109.5 . . ? H83A C83 H83C 109.5 . . ? H83B C83 H83C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag N1 C1 C2 C3 143.06(13) . . . . ? N1 C1 C2 C9 28.50(16) . . . . ? N1 C1 C2 C11 -93.18(16) . . . . ? N1 C1 C5 C4 -111.16(14) . . . . ? N1 C1 C5 C6 0.07(18) . . . . ? N1 C8 C9 N2 -138.99(13) . . . . ? N1 C8 C9 C2 -24.00(16) . . . . ? N1 C27 C28 C29 50.4(2) . . . . ? N1 C27 C28 C33 -129.67(19) . . . . ? N2 C34 C35 C36 -132.29(17) . . . . ? N2 C34 C35 C40 49.6(2) . . . . ? C1 N1 C8 C7 -69.12(15) . . . . ? C1 N1 C8 C9 42.17(15) . . . . ? C1 N1 C27 C28 60.7(2) . . . . ? C1 C2 C3 C4 -48.40(15) . . . . ? C1 C2 C3 C15 -178.22(14) . . . . ? C1 C2 C9 N2 111.48(14) . . . . ? C1 C2 C9 C8 -2.35(15) . . . . ? C1 C2 C11 O1 109.8(2) . . . . ? C1 C2 C11 C12 -69.1(2) . . . . ? C1 C5 C6 C7 -62.23(16) . . . . ? C1 C5 C6 C21 67.48(18) . . . . ? C2 C1 C5 C4 2.03(16) . . . . ? C2 C1 C5 C6 113.26(14) . . . . ? C2 C3 C4 C5 50.64(15) . . . . ? C2 C3 C4 C10 -61.17(16) . . . . ? C2 C3 C15 C16 -8.5(3) . . . . ? C2 C3 C15 C20 174.99(16) . . . . ? C3 C2 C9 N2 3.85(18) . . . . ? C3 C2 C9 C8 -109.98(15) . . . . ? C3 C2 C11 O1 -134.26(19) . . . . ? C3 C2 C11 C12 46.8(2) . . . . ? C3 C4 C5 C1 -32.52(16) . . . . ? C3 C4 C5 C6 -149.27(13) . . . . ? C3 C4 C10 N2 -0.17(18) . . . . ? C3 C4 C10 C7 113.47(14) . . . . ? C3 C15 C16 C17 -177.65(17) . . . . ? C3 C15 C20 C19 177.76(18) . . . . ? C4 C3 C15 C16 -129.57(18) . . . . ? C4 C3 C15 C20 53.9(2) . . . . ? C4 C5 C6 C7 49.89(15) . . . . ? C4 C5 C6 C21 179.59(14) . . . . ? C5 C1 C2 C3 28.89(15) . . . . ? C5 C1 C2 C9 -85.68(14) . . . . ? C5 C1 C2 C11 152.64(14) . . . . ? C5 C4 C10 N2 -110.78(14) . . . . ? C5 C4 C10 C7 2.86(16) . . . . ? C5 C6 C7 C8 60.25(16) . . . . ? C5 C6 C7 C10 -47.31(15) . . . . ? C5 C6 C7 C13 -169.09(14) . . . . ? C5 C6 C21 C22 55.0(2) . . . . ? C5 C6 C21 C26 -125.77(18) . . . . ? C6 C7 C8 N1 2.14(18) . . . . ? C6 C7 C8 C9 -111.14(14) . . . . ? C6 C7 C10 N2 142.52(13) . . . . ? C6 C7 C10 C4 27.79(16) . . . . ? C6 C7 C13 O2 -132.03(18) . . . . ? C6 C7 C13 C14 48.2(2) . . . . ? C6 C21 C22 C23 -177.84(18) . . . . ? C6 C21 C26 C25 179.20(17) . . . . ? C7 C6 C21 C22 173.99(16) . . . . ? C7 C6 C21 C26 -6.8(2) . . . . ? C7 C8 C9 N2 -23.68(16) . . . . ? C7 C8 C9 C2 91.31(14) . . . . ? C8 N1 C1 C2 -44.05(15) . . . . ? C8 N1 C1 C5 67.20(15) . . . . ? C8 N1 C27 C28 178.38(15) . . . . ? C8 C7 C10 N2 28.76(16) . . . . ? C8 C7 C10 C4 -85.97(14) . . . . ? C8 C7 C13 O2 -3.8(2) . . . . ? C8 C7 C13 C14 176.46(16) . . . . ? C9 N2 C10 C4 67.63(15) . . . . ? C9 N2 C10 C7 -43.86(15) . . . . ? C9 N2 C34 C35 -171.72(14) . . . . ? C9 C2 C3 C4 59.11(16) . . . . ? C9 C2 C3 C15 -70.72(19) . . . . ? C9 C2 C11 O1 -4.8(3) . . . . ? C9 C2 C11 C12 176.32(16) . . . . ? C10 N2 C9 C2 -69.84(15) . . . . ? C10 N2 C9 C8 41.66(15) . . . . ? C10 N2 C34 C35 71.71(18) . . . . ? C10 C4 C5 C1 83.83(15) . . . . ? C10 C4 C5 C6 -32.92(16) . . . . ? C10 C7 C8 N1 110.41(14) . . . . ? C10 C7 C8 C9 -2.87(15) . . . . ? C10 C7 C13 O2 111.58(19) . . . . ? C10 C7 C13 C14 -68.2(2) . . . . ? C11 C2 C3 C4 -170.11(14) . . . . ? C11 C2 C3 C15 60.1(2) . . . . ? C11 C2 C9 N2 -127.79(15) . . . . ? C11 C2 C9 C8 118.39(15) . . . . ? C13 C7 C8 N1 -128.24(15) . . . . ? C13 C7 C8 C9 118.48(15) . . . . ? C13 C7 C10 N2 -94.34(16) . . . . ? C13 C7 C10 C4 150.93(14) . . . . ? C15 C3 C4 C5 -177.46(14) . . . . ? C15 C3 C4 C10 70.73(18) . . . . ? C15 C16 C17 C18 0.6(3) . . . . ? C16 C15 C20 C19 1.0(3) . . . . ? C16 C17 C18 C19 0.0(3) . . . . ? C17 C18 C19 C20 -0.1(3) . . . . ? C18 C19 C20 C15 -0.5(3) . . . . ? C20 C15 C16 C17 -1.1(3) . . . . ? C21 C6 C7 C8 -67.85(19) . . . . ? C21 C6 C7 C10 -175.41(14) . . . . ? C21 C6 C7 C13 62.8(2) . . . . ? C21 C22 C23 C24 -1.8(3) . . . . ? C22 C21 C26 C25 -1.5(3) . . . . ? C22 C23 C24 C25 -0.6(3) . . . . ? C23 C24 C25 C26 1.9(3) . . . . ? C24 C25 C26 C21 -0.8(3) . . . . ? C26 C21 C22 C23 2.9(3) . . . . ? C27 N1 C1 C2 80.45(17) . . . . ? C27 N1 C1 C5 -168.29(14) . . . . ? C27 N1 C8 C7 165.34(14) . . . . ? C27 N1 C8 C9 -83.37(17) . . . . ? C27 C28 C29 C30 179.20(17) . . . . ? C27 C28 C33 C32 -179.4(2) . . . . ? C28 C29 C30 C31 0.7(3) . . . . ? C29 C28 C33 C32 0.6(3) . . . . ? C29 C30 C31 C32 -0.5(3) . . . . ? C30 C31 C32 C33 0.3(4) . . . . ? C31 C32 C33 C28 -0.3(4) . . . . ? C33 C28 C29 C30 -0.7(3) . . . . ? C34 N2 C9 C2 165.47(13) . . . . ? C34 N2 C9 C8 -83.02(16) . . . . ? C34 N2 C10 C4 -168.69(13) . . . . ? C34 N2 C10 C7 79.82(16) . . . . ? C34 C35 C36 C37 -177.44(17) . . . . ? C34 C35 C40 C39 176.29(16) . . . . ? C35 C36 C37 C38 0.9(3) . . . . ? C36 C35 C40 C39 -1.9(3) . . . . ? C36 C37 C38 C39 -1.5(3) . . . . ? C37 C38 C39 C40 0.3(3) . . . . ? C38 C39 C40 C35 1.4(3) . . . . ? C40 C35 C36 C37 0.8(3) . . . . ? N3 C41 C42 C43 2.86(18) . . . . ? N3 C41 C42 C49 110.82(14) . . . . ? N3 C41 C42 C51 -126.77(14) . . . . ? N3 C41 C50 N4 -139.09(13) . . . . ? N3 C41 C50 C46 -23.79(16) . . . . ? N3 C45 C46 C47 143.30(13) . . . . ? N3 C45 C46 C50 28.83(16) . . . . ? N3 C45 C46 C53 -93.58(16) . . . . ? N3 C67 C68 C69 55.0(2) . . . . ? N3 C67 C68 C73 -124.16(17) . . . . ? N4 C74 C75 C76 -127.07(18) . . . . ? N4 C74 C75 C80 55.0(2) . . . . ? C41 N3 C45 C44 67.74(15) . . . . ? C41 N3 C45 C46 -44.16(15) . . . . ? C41 N3 C67 C68 170.21(14) . . . . ? C41 C42 C43 C44 59.53(16) . . . . ? C41 C42 C43 C55 -70.36(19) . . . . ? C41 C42 C49 N4 28.46(16) . . . . ? C41 C42 C49 C48 -86.00(14) . . . . ? C41 C42 C51 O3 -3.4(2) . . . . ? C41 C42 C51 C52 174.94(15) . . . . ? C42 C41 C50 N4 -23.85(16) . . . . ? C42 C41 C50 C46 91.46(14) . . . . ? C42 C43 C44 C45 -61.23(16) . . . . ? C42 C43 C44 C48 50.25(15) . . . . ? C42 C43 C55 C56 -3.6(3) . . . . ? C42 C43 C55 C60 179.54(16) . . . . ? C43 C42 C49 N4 142.53(13) . . . . ? C43 C42 C49 C48 28.07(16) . . . . ? C43 C42 C51 O3 -131.24(18) . . . . ? C43 C42 C51 C52 47.1(2) . . . . ? C43 C44 C45 N3 -0.80(18) . . . . ? C43 C44 C45 C46 112.74(14) . . . . ? C43 C44 C48 C47 -149.56(13) . . . . ? C43 C44 C48 C49 -32.77(16) . . . . ? C43 C55 C56 C57 -175.68(18) . . . . ? C43 C55 C60 C59 176.8(2) . . . . ? C44 C43 C55 C56 -124.48(18) . . . . ? C44 C43 C55 C60 58.7(2) . . . . ? C44 C45 C46 C47 29.06(15) . . . . ? C44 C45 C46 C50 -85.40(14) . . . . ? C44 C45 C46 C53 152.19(14) . . . . ? C44 C48 C49 N4 -110.97(14) . . . . ? C44 C48 C49 C42 2.63(16) . . . . ? C45 N3 C41 C42 -69.58(15) . . . . ? C45 N3 C41 C50 41.95(15) . . . . ? C45 N3 C67 C68 54.04(19) . . . . ? C45 C44 C48 C47 -32.86(16) . . . . ? C45 C44 C48 C49 83.93(15) . . . . ? C45 C46 C47 C48 -48.82(15) . . . . ? C45 C46 C47 C61 -179.41(14) . . . . ? C45 C46 C50 N4 110.96(14) . . . . ? C45 C46 C50 C41 -2.71(15) . . . . ? C45 C46 C53 O4 114.29(19) . . . . ? C45 C46 C53 C54 -65.2(2) . . . . ? C46 C47 C48 C44 51.35(15) . . . . ? C46 C47 C48 C49 -60.57(16) . . . . ? C46 C47 C61 C62 -177.41(16) . . . . ? C46 C47 C61 C66 -1.2(3) . . . . ? C47 C46 C50 N4 3.97(18) . . . . ? C47 C46 C50 C41 -109.70(14) . . . . ? C47 C46 C53 O4 -130.28(18) . . . . ? C47 C46 C53 C54 50.2(2) . . . . ? C47 C48 C49 N4 -0.40(18) . . . . ? C47 C48 C49 C42 113.20(14) . . . . ? C47 C61 C62 C63 177.10(17) . . . . ? C47 C61 C66 C65 -176.64(17) . . . . ? C48 C44 C45 N3 -111.46(14) . . . . ? C48 C44 C45 C46 2.08(16) . . . . ? C48 C47 C61 C62 61.0(2) . . . . ? C48 C47 C61 C66 -122.73(19) . . . . ? C49 N4 C50 C41 41.61(16) . . . . ? C49 N4 C50 C46 -69.82(15) . . . . ? C49 N4 C74 C75 69.05(18) . . . . ? C49 C42 C43 C44 -47.85(15) . . . . ? C49 C42 C43 C55 -177.74(14) . . . . ? C49 C42 C51 O3 112.23(19) . . . . ? C49 C42 C51 C52 -69.5(2) . . . . ? C50 N4 C49 C42 -43.82(15) . . . . ? C50 N4 C49 C48 67.46(15) . . . . ? C50 N4 C74 C75 -174.73(14) . . . . ? C50 C41 C42 C43 -110.59(14) . . . . ? C50 C41 C42 C49 -2.63(15) . . . . ? C50 C41 C42 C51 119.78(15) . . . . ? C50 C46 C47 C48 58.54(16) . . . . ? C50 C46 C47 C61 -72.05(19) . . . . ? C50 C46 C53 O4 -1.3(2) . . . . ? C50 C46 C53 C54 179.22(15) . . . . ? C51 C42 C43 C44 -170.69(14) . . . . ? C51 C42 C43 C55 59.4(2) . . . . ? C51 C42 C49 N4 -94.38(16) . . . . ? C51 C42 C49 C48 151.15(14) . . . . ? C53 C46 C47 C48 -171.14(14) . . . . ? C53 C46 C47 C61 58.3(2) . . . . ? C53 C46 C50 N4 -126.82(15) . . . . ? C53 C46 C50 C41 119.51(14) . . . . ? C55 C43 C44 C45 69.92(19) . . . . ? C55 C43 C44 C48 -178.60(14) . . . . ? C55 C56 C57 C58 -1.0(3) . . . . ? C56 C55 C60 C59 -0.3(3) . . . . ? C56 C57 C58 C59 -0.1(4) . . . . ? C57 C58 C59 C60 1.0(4) . . . . ? C58 C59 C60 C55 -0.8(4) . . . . ? C60 C55 C56 C57 1.2(3) . . . . ? C61 C47 C48 C44 -176.70(14) . . . . ? C61 C47 C48 C49 71.38(19) . . . . ? C61 C62 C63 C64 -0.5(3) . . . . ? C62 C61 C66 C65 -0.4(3) . . . . ? C62 C63 C64 C65 0.1(3) . . . . ? C63 C64 C65 C66 0.1(3) . . . . ? C64 C65 C66 C61 0.0(3) . . . . ? C66 C61 C62 C63 0.6(3) . . . . ? C67 N3 C41 C42 165.84(13) . . . . ? C67 N3 C41 C50 -82.64(16) . . . . ? C67 N3 C45 C44 -169.83(13) . . . . ? C67 N3 C45 C46 78.27(16) . . . . ? C67 C68 C69 C70 -178.59(16) . . . . ? C67 C68 C73 C72 179.43(17) . . . . ? C68 C69 C70 C71 -0.9(3) . . . . ? C69 C68 C73 C72 0.2(3) . . . . ? C69 C70 C71 C72 0.4(3) . . . . ? C70 C71 C72 C73 0.4(3) . . . . ? C71 C72 C73 C68 -0.8(3) . . . . ? C73 C68 C69 C70 0.6(3) . . . . ? C74 N4 C49 C42 79.19(16) . . . . ? C74 N4 C49 C48 -169.53(13) . . . . ? C74 N4 C50 C41 -82.64(16) . . . . ? C74 N4 C50 C46 165.92(13) . . . . ? C74 C75 C76 C77 -177.84(18) . . . . ? C74 C75 C80 C79 176.18(17) . . . . ? C75 C76 C77 C78 1.3(3) . . . . ? C76 C75 C80 C79 -1.8(3) . . . . ? C76 C77 C78 C79 -1.1(3) . . . . ? C77 C78 C79 C80 -0.6(3) . . . . ? C78 C79 C80 C75 2.1(3) . . . . ? C80 C75 C76 C77 0.1(3) . . . . ? _shelx_res_file ; TITL r20190409e_a.res in P2(1)/c r20190409e.res created by SHELXL-2018/3 at 08:00:13 on 10-Apr-2019 REM Old TITL r20190409e REM SHELXT solution in P2(1)/c: R1 0.166, Rweak 0.130, Alpha 0.043 REM 1.053 for 449 systematic absences, Orientation as input REM Formula found by SHELXT: C83 N4 O5 CELL 0.71075 21.7055 18.4546 17.7735 90 112.216 90 ZERR 8 0.0078 0.0059 0.0065 0 0.006 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H N O UNIT 332 328 16 20 L.S. 4 0 0 PLAN 20 SIZE 0.36 0.22 0.2 TEMP -145 BOND $h conf htab fmap 2 53 acta REM REM REM WGHT 0.062100 0.595500 EXTI 0.005533 FVAR 0.38801 O1 4 0.833399 0.078141 0.841451 11.00000 0.05963 0.03969 = 0.03904 -0.00536 0.00925 -0.02091 O2 4 0.836156 0.423287 0.786125 11.00000 0.04754 0.03960 = 0.04428 0.01378 0.00451 0.01037 N1 3 0.826040 0.259976 0.929074 11.00000 0.02312 0.02970 = 0.02421 0.00256 0.00774 0.00046 N2 3 0.935375 0.250221 0.821617 11.00000 0.02587 0.02559 = 0.02236 -0.00080 0.00840 -0.00221 C1 1 0.885236 0.219995 0.977552 11.00000 0.02512 0.02384 = 0.02409 0.00252 0.00857 0.00049 AFIX 13 H1 2 0.878319 0.189663 1.020320 11.00000 -1.20000 AFIX 0 C2 1 0.906292 0.173052 0.915947 11.00000 0.02647 0.02422 = 0.02529 -0.00051 0.00877 -0.00095 C3 1 0.982989 0.176771 0.955284 11.00000 0.02759 0.02368 = 0.02654 0.00220 0.00877 0.00130 AFIX 13 H3 2 0.995766 0.153947 1.010125 11.00000 -1.20000 AFIX 0 C4 1 0.991109 0.259035 0.970123 11.00000 0.02263 0.02503 = 0.02618 -0.00159 0.00653 -0.00038 AFIX 13 H4 2 1.038116 0.273063 1.003186 11.00000 -1.20000 AFIX 0 C5 1 0.943732 0.275360 1.013921 11.00000 0.02563 0.02611 = 0.02106 -0.00002 0.00633 0.00127 AFIX 13 H5 2 0.966221 0.270761 1.074269 11.00000 -1.20000 AFIX 0 C6 1 0.920516 0.353354 0.987436 11.00000 0.02662 0.02344 = 0.02556 -0.00150 0.00838 0.00004 AFIX 13 H6 2 0.961196 0.384565 1.006638 11.00000 -1.20000 AFIX 0 C7 1 0.899986 0.343875 0.894444 11.00000 0.02693 0.02345 = 0.02386 0.00088 0.00904 0.00119 C8 1 0.843821 0.285711 0.862021 11.00000 0.02505 0.02708 = 0.02295 0.00072 0.00668 0.00154 AFIX 13 H8 2 0.804347 0.303947 0.815240 11.00000 -1.20000 AFIX 0 C9 1 0.879163 0.220422 0.837283 11.00000 0.02422 0.02564 = 0.02342 -0.00014 0.00708 -0.00097 AFIX 13 H9 2 0.847933 0.192894 0.789667 11.00000 -1.20000 AFIX 0 C10 1 0.961734 0.302045 0.888161 11.00000 0.02408 0.02445 = 0.02536 -0.00201 0.00835 -0.00045 AFIX 13 H10 2 0.995009 0.335720 0.880554 11.00000 -1.20000 AFIX 0 C11 1 0.876952 0.096958 0.904603 11.00000 0.03540 0.02713 = 0.03326 -0.00277 0.01556 -0.00334 C12 1 0.902318 0.044888 0.974540 11.00000 0.05610 0.02680 = 0.04871 0.00374 0.01461 -0.00381 AFIX 137 H12A 2 0.877312 -0.000595 0.959731 11.00000 -1.50000 H12B 2 0.896566 0.065966 1.022073 11.00000 -1.50000 H12C 2 0.949634 0.035307 0.987467 11.00000 -1.50000 AFIX 0 C13 1 0.885736 0.414746 0.846888 11.00000 0.03769 0.02761 = 0.02737 0.00267 0.01635 0.00727 C14 1 0.935407 0.474816 0.877168 11.00000 0.05780 0.03064 = 0.04210 0.00310 0.02069 -0.00402 AFIX 137 H14A 2 0.928320 0.510242 0.833609 11.00000 -1.50000 H14B 2 0.980508 0.454945 0.894168 11.00000 -1.50000 H14C 2 0.929903 0.498575 0.923543 11.00000 -1.50000 AFIX 0 C15 1 1.025636 0.140566 0.915373 11.00000 0.03428 0.02267 = 0.03190 0.00533 0.01403 0.00589 C16 1 1.000069 0.094860 0.848293 11.00000 0.04248 0.02893 = 0.03859 -0.00055 0.01784 0.00498 AFIX 43 H16 2 0.953421 0.086792 0.824430 11.00000 -1.20000 AFIX 0 C17 1 1.041465 0.060732 0.815463 11.00000 0.06023 0.03121 = 0.04446 -0.00076 0.02750 0.00811 AFIX 43 H17 2 1.022815 0.030133 0.769396 11.00000 -1.20000 AFIX 0 C18 1 1.109312 0.071142 0.849476 11.00000 0.06091 0.04132 = 0.05693 0.00699 0.03885 0.01793 AFIX 43 H18 2 1.137599 0.047935 0.827133 11.00000 -1.20000 AFIX 0 C19 1 1.135848 0.116012 0.916875 11.00000 0.03814 0.04726 = 0.06175 0.00676 0.02702 0.00878 AFIX 43 H19 2 1.182567 0.123540 0.940899 11.00000 -1.20000 AFIX 0 C20 1 1.094198 0.149924 0.949250 11.00000 0.03454 0.03616 = 0.04282 0.00038 0.01581 0.00315 AFIX 43 H20 2 1.113058 0.180176 0.995583 11.00000 -1.20000 AFIX 0 C21 1 0.871744 0.386678 1.020194 11.00000 0.03321 0.02162 = 0.02929 -0.00164 0.01270 -0.00051 C22 1 0.888249 0.388698 1.104152 11.00000 0.04300 0.03274 = 0.03108 -0.00147 0.01370 0.00729 AFIX 43 H22 2 0.930286 0.370748 1.139400 11.00000 -1.20000 AFIX 0 C23 1 0.844353 0.416483 1.137264 11.00000 0.06116 0.04287 = 0.03056 -0.00381 0.02112 0.00853 AFIX 43 H23 2 0.856196 0.415959 1.194476 11.00000 -1.20000 AFIX 0 C24 1 0.784092 0.444615 1.087729 11.00000 0.05144 0.03521 = 0.04705 -0.00553 0.02803 0.00783 AFIX 43 H24 2 0.754003 0.463127 1.110310 11.00000 -1.20000 AFIX 0 C25 1 0.767572 0.445714 1.004080 11.00000 0.03658 0.02998 = 0.04333 -0.00074 0.01682 0.00579 AFIX 43 H25 2 0.726587 0.466399 0.969390 11.00000 -1.20000 AFIX 0 C26 1 0.810675 0.416772 0.971372 11.00000 0.03639 0.02801 = 0.02820 0.00011 0.01197 0.00307 AFIX 43 H26 2 0.798409 0.417374 0.914092 11.00000 -1.20000 AFIX 0 C27 1 0.763370 0.219543 0.903405 11.00000 0.02687 0.04202 = 0.02994 -0.00113 0.00879 -0.00424 AFIX 23 H27A 2 0.765764 0.177610 0.869876 11.00000 -1.20000 H27B 2 0.726465 0.251161 0.869511 11.00000 -1.20000 AFIX 0 C28 1 0.749288 0.192941 0.975759 11.00000 0.02323 0.03661 = 0.03213 0.00242 0.00744 -0.00193 C29 1 0.752366 0.240223 1.037891 11.00000 0.02985 0.03774 = 0.03646 0.00334 0.01280 0.00056 AFIX 43 H29 2 0.763964 0.289520 1.035183 11.00000 -1.20000 AFIX 0 C30 1 0.738611 0.216038 1.104122 11.00000 0.03381 0.06375 = 0.03412 0.00229 0.01355 -0.00002 AFIX 43 H30 2 0.740384 0.248997 1.145950 11.00000 -1.20000 AFIX 0 C31 1 0.722426 0.144438 1.109220 11.00000 0.05168 0.07762 = 0.04117 0.01647 0.01592 -0.01559 AFIX 43 H31 2 0.713353 0.127787 1.154556 11.00000 -1.20000 AFIX 0 C32 1 0.719555 0.097305 1.047860 11.00000 0.07684 0.05396 = 0.05520 0.01159 0.01709 -0.02632 AFIX 43 H32 2 0.708235 0.047975 1.050974 11.00000 -1.20000 AFIX 0 C33 1 0.732984 0.121010 0.981671 11.00000 0.05256 0.04258 = 0.04296 -0.00182 0.01164 -0.01170 AFIX 43 H33 2 0.731017 0.087772 0.940008 11.00000 -1.20000 AFIX 0 C34 1 0.917638 0.280355 0.739644 11.00000 0.02859 0.03004 = 0.02375 0.00069 0.00990 0.00199 AFIX 23 H34A 2 0.889707 0.324008 0.733890 11.00000 -1.20000 H34B 2 0.891228 0.244283 0.699020 11.00000 -1.20000 AFIX 0 C35 1 0.978705 0.300219 0.723182 11.00000 0.02996 0.03283 = 0.02023 -0.00213 0.00819 -0.00206 C36 1 0.983834 0.367338 0.689759 11.00000 0.04161 0.03504 = 0.02944 0.00363 0.01263 -0.00084 AFIX 43 H36 2 0.949113 0.401875 0.679212 11.00000 -1.20000 AFIX 0 C37 1 1.038957 0.384149 0.671804 11.00000 0.04742 0.04958 = 0.03183 0.00631 0.01243 -0.01516 AFIX 43 H37 2 1.042089 0.430294 0.649826 11.00000 -1.20000 AFIX 0 C38 1 1.089458 0.334039 0.685736 11.00000 0.03497 0.06963 = 0.03254 0.00036 0.01280 -0.01348 AFIX 43 H38 2 1.126759 0.345202 0.672231 11.00000 -1.20000 AFIX 0 C39 1 1.085308 0.267648 0.719418 11.00000 0.02871 0.05510 = 0.03274 -0.00255 0.00903 0.00211 AFIX 43 H39 2 1.120017 0.233198 0.729310 11.00000 -1.20000 AFIX 0 C40 1 1.030772 0.250942 0.738902 11.00000 0.03186 0.03575 = 0.02896 -0.00075 0.00944 -0.00023 AFIX 43 H40 2 1.028907 0.205545 0.763155 11.00000 -1.20000 AFIX 0 O3 4 0.653922 0.571761 0.436423 11.00000 0.05477 0.03364 = 0.05431 -0.00216 0.03568 0.00628 O4 4 0.647349 0.919985 0.484528 11.00000 0.05590 0.03487 = 0.05311 -0.00303 0.02845 -0.01490 N3 3 0.659626 0.735491 0.584662 11.00000 0.02215 0.02723 = 0.02365 -0.00174 0.00820 -0.00015 N4 3 0.551026 0.744610 0.375946 11.00000 0.02721 0.02682 = 0.02342 0.00001 0.01142 -0.00104 C41 1 0.642288 0.709938 0.501070 11.00000 0.02417 0.02636 = 0.02562 0.00107 0.01218 0.00157 AFIX 13 H41 2 0.682027 0.692226 0.490981 11.00000 -1.20000 AFIX 0 C42 1 0.586837 0.651074 0.481699 11.00000 0.02784 0.02476 = 0.02342 -0.00007 0.01205 0.00090 C43 1 0.565412 0.641279 0.554778 11.00000 0.02881 0.02377 = 0.02430 -0.00184 0.01221 -0.00208 AFIX 13 H43 2 0.524489 0.610459 0.534920 11.00000 -1.20000 AFIX 0 C44 1 0.541763 0.718895 0.560215 11.00000 0.02575 0.02569 = 0.02453 0.00011 0.01269 -0.00090 AFIX 13 H44 2 0.519041 0.723080 0.599592 11.00000 -1.20000 AFIX 0 C45 1 0.599685 0.775163 0.577684 11.00000 0.02350 0.02414 = 0.02431 -0.00098 0.00960 0.00116 AFIX 13 H45 2 0.606151 0.805445 0.626752 11.00000 -1.20000 AFIX 0 C46 1 0.578932 0.822095 0.497154 11.00000 0.02461 0.02473 = 0.02488 -0.00025 0.00891 0.00108 C47 1 0.502180 0.817464 0.465877 11.00000 0.02540 0.02516 = 0.02657 -0.00126 0.01057 0.00212 AFIX 13 H47 2 0.489469 0.839483 0.509367 11.00000 -1.20000 AFIX 0 C48 1 0.494747 0.734996 0.472577 11.00000 0.02310 0.02710 = 0.02507 -0.00119 0.00978 -0.00169 AFIX 13 H48 2 0.447804 0.720445 0.461884 11.00000 -1.20000 AFIX 0 C49 1 0.524933 0.692177 0.417891 11.00000 0.02376 0.02658 = 0.02419 -0.00035 0.00900 -0.00191 AFIX 13 H49 2 0.492091 0.658186 0.379459 11.00000 -1.20000 AFIX 0 C50 1 0.606498 0.775079 0.443460 11.00000 0.02361 0.02421 = 0.02576 0.00110 0.01005 0.00058 AFIX 13 H50 2 0.637618 0.802969 0.424828 11.00000 -1.20000 AFIX 0 C51 1 0.603440 0.580111 0.449423 11.00000 0.04018 0.02766 = 0.02388 0.00131 0.01503 0.00334 C52 1 0.555373 0.518237 0.435858 11.00000 0.05915 0.03051 = 0.05113 -0.01374 0.02721 -0.00899 AFIX 137 H52A 2 0.567599 0.479181 0.406794 11.00000 -1.50000 H52B 2 0.510233 0.535021 0.403527 11.00000 -1.50000 H52C 2 0.556957 0.500177 0.488409 11.00000 -1.50000 AFIX 0 C53 1 0.606686 0.898982 0.511651 11.00000 0.03034 0.02566 = 0.03067 0.00369 0.00576 0.00016 C54 1 0.582775 0.948929 0.561525 11.00000 0.04187 0.02543 = 0.05029 -0.00485 0.01330 0.00223 AFIX 137 H54A 2 0.595767 0.929504 0.616694 11.00000 -1.50000 H54B 2 0.534197 0.952983 0.536617 11.00000 -1.50000 H54C 2 0.602750 0.996914 0.563830 11.00000 -1.50000 AFIX 0 C55 1 0.612469 0.605921 0.632264 11.00000 0.03712 0.02159 = 0.02505 -0.00032 0.01265 0.00033 C56 1 0.674106 0.577333 0.641078 11.00000 0.04067 0.03460 = 0.03064 0.00317 0.01744 0.00653 AFIX 43 H56 2 0.689647 0.582585 0.598070 11.00000 -1.20000 AFIX 0 C57 1 0.713144 0.541498 0.711008 11.00000 0.04993 0.04479 = 0.03859 0.00888 0.01715 0.01982 AFIX 43 H57 2 0.754774 0.521723 0.715392 11.00000 -1.20000 AFIX 0 C58 1 0.691772 0.534318 0.774743 11.00000 0.06341 0.06097 = 0.03482 0.01777 0.01746 0.02472 AFIX 43 H58 2 0.718557 0.509573 0.822884 11.00000 -1.20000 AFIX 0 C59 1 0.631293 0.563326 0.767962 11.00000 0.06957 0.07206 = 0.03786 0.02178 0.03184 0.02426 AFIX 43 H59 2 0.616669 0.559263 0.811863 11.00000 -1.20000 AFIX 0 C60 1 0.591922 0.598351 0.697195 11.00000 0.04338 0.04427 = 0.03387 0.00768 0.02032 0.00798 AFIX 43 H60 2 0.550111 0.617578 0.692854 11.00000 -1.20000 AFIX 0 C61 1 0.459496 0.854742 0.387548 11.00000 0.03164 0.02385 = 0.02899 -0.00315 0.00909 0.00491 C62 1 0.390384 0.851477 0.363581 11.00000 0.03127 0.03534 = 0.03709 0.00030 0.00652 0.00307 AFIX 43 H62 2 0.371639 0.824366 0.395118 11.00000 -1.20000 AFIX 0 C63 1 0.348735 0.887259 0.294383 11.00000 0.03519 0.04490 = 0.04787 -0.00540 -0.00234 0.00991 AFIX 43 H63 2 0.301852 0.884102 0.278791 11.00000 -1.20000 AFIX 0 C64 1 0.375043 0.927579 0.247842 11.00000 0.05773 0.04092 = 0.03193 -0.00058 0.00040 0.01803 AFIX 43 H64 2 0.346501 0.952143 0.200528 11.00000 -1.20000 AFIX 0 C65 1 0.443001 0.931563 0.271047 11.00000 0.06326 0.03248 = 0.03238 0.00539 0.01700 0.01218 AFIX 43 H65 2 0.461474 0.959151 0.239573 11.00000 -1.20000 AFIX 0 C66 1 0.484943 0.895529 0.340240 11.00000 0.03995 0.03007 = 0.03516 0.00393 0.01339 0.00741 AFIX 43 H66 2 0.531770 0.898879 0.355378 11.00000 -1.20000 AFIX 0 C67 1 0.721928 0.777145 0.614886 11.00000 0.02520 0.03335 = 0.02989 0.00194 0.00915 -0.00103 AFIX 23 H67A 2 0.720790 0.814484 0.574387 11.00000 -1.20000 H67B 2 0.759805 0.744341 0.621949 11.00000 -1.20000 AFIX 0 C68 1 0.732095 0.813165 0.694608 11.00000 0.02026 0.03403 = 0.03315 -0.00197 0.00588 0.00037 C69 1 0.731471 0.773313 0.760969 11.00000 0.02923 0.04499 = 0.03221 -0.00154 0.00842 -0.00033 AFIX 43 H69 2 0.725526 0.722267 0.756656 11.00000 -1.20000 AFIX 0 C70 1 0.739529 0.808135 0.833367 11.00000 0.03131 0.07631 = 0.03317 -0.00429 0.01028 -0.00065 AFIX 43 H70 2 0.738408 0.780825 0.878140 11.00000 -1.20000 AFIX 0 C71 1 0.749216 0.882615 0.840770 11.00000 0.02754 0.07849 = 0.04929 -0.03335 0.00925 0.00051 AFIX 43 H71 2 0.754988 0.906136 0.890530 11.00000 -1.20000 AFIX 0 C72 1 0.750410 0.922086 0.775843 11.00000 0.03324 0.04572 = 0.06735 -0.02356 0.00944 0.00121 AFIX 43 H72 2 0.757326 0.972983 0.780728 11.00000 -1.20000 AFIX 0 C73 1 0.741514 0.887607 0.703115 11.00000 0.02878 0.03298 = 0.04831 -0.00189 0.00746 -0.00068 AFIX 43 H73 2 0.741872 0.915427 0.658309 11.00000 -1.20000 AFIX 0 C74 1 0.570281 0.714522 0.311238 11.00000 0.03058 0.03101 = 0.02555 0.00255 0.01370 0.00333 AFIX 23 H74A 2 0.600641 0.672938 0.333010 11.00000 -1.20000 H74B 2 0.594580 0.751865 0.293399 11.00000 -1.20000 AFIX 0 C75 1 0.510828 0.690053 0.239736 11.00000 0.03185 0.03397 = 0.02281 0.00235 0.01533 -0.00018 C76 1 0.507198 0.620597 0.208588 11.00000 0.05468 0.03825 = 0.03348 -0.00152 0.01860 0.00135 AFIX 43 H76 2 0.542323 0.587324 0.234101 11.00000 -1.20000 AFIX 0 C77 1 0.453068 0.599006 0.140772 11.00000 0.07088 0.05719 = 0.04164 -0.01679 0.02395 -0.02104 AFIX 43 H77 2 0.450726 0.550953 0.120705 11.00000 -1.20000 AFIX 0 C78 1 0.402713 0.647514 0.102626 11.00000 0.04371 0.09490 = 0.03429 -0.01218 0.01414 -0.02571 AFIX 43 H78 2 0.365912 0.633181 0.055561 11.00000 -1.20000 AFIX 0 C79 1 0.405613 0.716849 0.132622 11.00000 0.02903 0.07815 = 0.03546 0.00423 0.01185 0.00095 AFIX 43 H79 2 0.370978 0.750321 0.105872 11.00000 -1.20000 AFIX 0 C80 1 0.458755 0.737851 0.201508 11.00000 0.03231 0.04417 = 0.03351 0.00348 0.01628 0.00319 AFIX 43 H80 2 0.459724 0.785210 0.222876 11.00000 -1.20000 AFIX 0 O5 4 0.911233 0.593225 0.999196 11.00000 0.06712 0.09738 = 0.10370 -0.05489 0.04976 -0.02960 C81 1 0.869861 0.614444 1.100666 11.00000 0.05858 0.11728 = 0.07335 -0.02134 0.03347 -0.03029 AFIX 137 H81A 2 0.908945 0.586870 1.135085 11.00000 -1.50000 H81B 2 0.829597 0.592599 1.103369 11.00000 -1.50000 H81C 2 0.873764 0.664661 1.119847 11.00000 -1.50000 AFIX 0 C82 1 0.865778 0.613246 1.016156 11.00000 0.05106 0.03774 = 0.05820 -0.00852 0.01750 -0.01578 C83 1 0.802402 0.640270 0.955262 11.00000 0.09814 0.11290 = 0.09843 0.03330 -0.00233 -0.00187 AFIX 137 H83A 2 0.796538 0.691313 0.966245 11.00000 -1.50000 H83B 2 0.765361 0.611769 0.958425 11.00000 -1.50000 H83C 2 0.803303 0.635640 0.900760 11.00000 -1.50000 AFIX 0 HKLF 4 REM r20190409e_a.res in P2(1)/c REM wR2 = 0.1531, GooF = S = 1.138, Restrained GooF = 1.138 for all data REM R1 = 0.0647 for 11898 Fo > 4sig(Fo) and 0.0907 for all 15706 data REM 836 parameters refined using 0 restraints END WGHT 0.0621 0.5955 REM Instructions for potential hydrogen bonds EQIV $1 -x+2, -y+1, -z+2 HTAB C14 O5_$1 HTAB C14 O5 HTAB C27 O1 HTAB C34 O2 HTAB C67 O4 HTAB C74 O3 REM Highest difference peak 0.404, deepest hole -0.310, 1-sigma level 0.044 Q1 1 0.8389 0.6250 0.9138 11.00000 0.05 0.40 Q2 1 0.6182 0.6812 0.4980 11.00000 0.05 0.23 Q3 1 0.5948 0.7981 0.4770 11.00000 0.05 0.23 Q4 1 0.9353 0.0624 1.0274 11.00000 0.05 0.23 Q5 1 0.5772 0.7447 0.5735 11.00000 0.05 0.21 Q6 1 0.8760 0.3174 0.8779 11.00000 0.05 0.20 Q7 1 0.5968 0.6339 0.6025 11.00000 0.05 0.20 Q8 1 0.9989 0.2797 0.7220 11.00000 0.05 0.19 Q9 1 0.6254 0.7395 0.4682 11.00000 0.05 0.18 Q10 1 0.5385 0.7185 0.3964 11.00000 0.05 0.18 Q11 1 0.5436 0.8232 0.4775 11.00000 0.05 0.18 Q12 1 1.0033 0.1616 0.9256 11.00000 0.05 0.18 Q13 1 0.8558 0.6576 1.0624 11.00000 0.05 0.17 Q14 1 0.5042 0.6588 0.2096 11.00000 0.05 0.17 Q15 1 0.9282 0.3223 0.8808 11.00000 0.05 0.17 Q16 1 0.5562 0.6805 0.5673 11.00000 0.05 0.17 Q17 1 0.8932 0.3754 0.8753 11.00000 0.05 0.17 Q18 1 0.7545 0.8414 0.7008 11.00000 0.05 0.17 Q19 1 0.5790 0.6440 0.5228 11.00000 0.05 0.17 Q20 1 0.8998 0.1980 0.9534 11.00000 0.05 0.17 ; _shelx_res_checksum 44151 _shelx_hkl_file ; -1 0 0 37.40 0.88 0 1 0 -0.04 0.41 0 0 -1 -0.01 0.31 0 0 -1 0.46 0.79 0 0 -1 -0.03 0.37 1 0 -1 0.19 0.62 -1 1 0 1.92 0.69 1 -1 0 2.03 0.59 -1 1 0 2.53 2.23 -1 1 0 1.37 1.22 -1 -1 0 1.13 0.81 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32.44 5.61 12 5 -6 30.66 13.49 -8 6 9 16.69 9.01 -8 6 9 2.76 9.34 8 -6 -9 8.00 7.53 -8 -6 9 2.16 6.29 -8 -6 9 13.18 7.95 -9 1 -5 8.69 2.59 -9 -1 -5 3.47 2.30 9 -1 5 4.03 1.59 -9 -1 -5 8.06 4.70 9 1 5 6.56 4.51 9 -1 5 5.25 2.93 -9 1 -5 11.75 7.38 -9 -1 -5 15.72 7.97 -11 3 9 26.88 9.87 -11 -3 9 8.00 5.83 -11 3 9 17.74 12.15 11 3 -9 14.93 4.21 -11 -3 9 22.81 5.89 11 -3 -9 7.92 4.82 11 3 -9 20.53 17.77 8 -8 -7 76.22 8.83 -8 8 7 62.83 9.28 -8 8 7 72.71 7.73 -8 -8 7 68.51 1.39 -8 -8 7 80.03 8.75 -8 -8 7 63.10 5.33 5 8 5 43.73 8.20 -5 8 -5 39.54 7.95 5 -8 5 39.95 1.80 5 -8 5 40.73 1.47 -5 -8 -5 35.30 10.70 5 -8 5 37.26 7.02 -7 6 -5 190.11 22.69 7 6 5 174.77 28.36 7 -6 5 196.39 13.20 -7 -6 -5 178.20 19.23 -12 -2 -1 91.89 5.70 -12 2 -1 85.58 5.57 12 2 1 90.60 6.23 12 -2 1 74.19 7.08 -12 2 -1 85.67 9.19 -12 -2 -1 78.18 6.34 -13 3 6 147.13 13.51 -13 -3 6 224.50 11.79 13 -3 -6 170.89 14.95 -13 3 6 194.47 14.70 -13 -3 6 154.05 12.20 13 3 -6 169.99 12.62 1 -10 5 0.76 2.62 -1 10 -5 0.03 3.99 1 -10 5 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68.83 6.65 2 -9 6 66.63 21.30 -2 9 -6 70.62 3.56 -2 -9 -6 69.14 9.12 -11 -5 8 2.56 4.19 -11 5 8 15.90 7.53 -11 -5 8 5.26 3.44 -11 5 8 13.59 9.00 -11 -5 8 11.40 3.57 11 -5 -8 13.34 8.72 11 5 -8 15.04 6.09 -11 0 -3 3.41 4.52 11 0 3 0.72 2.05 -11 0 -3 0.66 1.36 -1 -8 8 1.81 3.86 1 -8 -8 8.08 6.34 -1 8 8 1.95 2.08 -1 -8 8 11.51 3.63 -1 8 8 9.72 8.31 1 8 -8 5.60 1.66 1 -8 -8 6.04 2.39 1 8 -8 1.95 3.11 6 -7 -9 688.03 35.03 -6 7 9 717.53 33.45 -6 -7 9 631.05 29.20 6 -7 -9 652.18 28.14 -6 -7 9 642.54 27.54 12 0 -9 0.34 4.24 -12 0 9 -1.15 5.64 -12 0 9 2.43 3.49 -2 -10 6 117.55 14.69 2 -10 -6 106.75 11.20 2 10 -6 107.14 8.38 -2 10 6 111.95 16.34 -2 -10 6 109.61 7.20 2 -10 -6 125.70 16.35 -5 -11 2 93.02 10.30 -5 -11 2 86.12 6.88 -5 11 2 108.37 11.82 5 11 -2 91.77 8.63 5 -11 -2 110.31 10.09 5 -11 -2 115.04 9.37 13 -4 -5 407.26 32.89 -13 -4 5 408.62 21.42 13 4 -5 359.34 20.63 -13 4 5 380.78 22.38 -13 4 5 393.39 22.50 -13 -4 5 416.56 23.44 3 -11 -4 66.37 6.67 -3 -11 4 70.12 21.93 3 -11 -4 65.51 8.50 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2 -4 96.64 5.05 7 -10 -4 14.50 11.68 -7 10 4 11.88 12.42 7 -10 -4 20.27 7.13 -7 -10 4 17.63 7.68 -7 -10 4 19.27 5.18 7 10 -4 16.05 5.99 -11 -7 5 18.14 7.41 -11 7 5 9.26 11.00 -11 -7 5 22.07 8.76 -11 -7 5 27.03 9.80 11 -7 -5 20.20 14.24 -11 7 5 12.92 9.65 -11 -7 5 24.55 14.90 -6 -6 -6 11.56 6.73 -6 6 -6 21.11 13.42 6 -6 6 30.31 10.46 6 6 6 5.93 10.52 11 -6 -7 132.40 10.89 -11 6 7 126.23 12.35 -11 6 7 141.95 18.86 -11 -6 7 111.78 4.24 -11 -6 7 119.77 12.88 -11 -6 7 129.21 10.32 -2 8 -7 25.98 4.07 2 -8 7 28.91 3.92 -2 8 -7 24.68 5.93 2 -8 7 42.28 7.67 -2 -8 -7 26.42 3.70 2 8 7 26.08 6.11 -2 -8 -7 39.88 8.91 2 8 7 14.32 7.14 -9 4 10 91.38 13.98 -9 -4 10 100.23 7.31 -9 -4 10 91.15 10.90 9 -4 -10 98.93 10.68 -9 4 10 110.83 10.96 11 -1 3 17.59 7.01 -11 1 -3 8.31 7.80 -11 -1 -3 6.06 4.93 -11 -1 -3 9.42 6.39 -11 1 -3 14.87 7.00 11 1 3 5.85 4.44 -4 10 6 242.39 21.74 4 -10 -6 229.47 12.28 4 -10 -6 237.78 16.21 4 10 -6 234.18 16.52 -4 -10 6 225.70 10.73 -4 -10 6 244.92 21.50 -4 -10 6 214.12 12.73 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5.97 -2 11 -3 125.47 20.13 2 11 3 117.71 12.00 -4 -3 11 13.99 5.77 -4 -3 11 19.98 7.97 4 3 -11 16.81 5.32 -4 3 11 18.81 8.21 4 3 -11 10.77 3.78 -4 3 11 12.52 9.91 4 -3 -11 10.11 4.39 10 -7 -7 339.36 19.48 -10 7 7 362.18 31.30 -10 7 7 286.03 19.10 -10 -7 7 357.77 19.95 -10 -7 7 339.18 16.59 -10 -7 7 316.70 15.15 -10 -7 7 314.99 18.78 -9 8 -1 44.94 17.14 9 -8 1 46.90 15.51 9 -8 1 46.74 10.70 -9 -8 -1 56.89 7.73 9 8 1 50.26 10.49 9 8 1 52.27 21.59 -8 -2 -6 143.63 9.80 -8 2 -6 128.79 7.72 -8 -2 -6 159.99 12.25 -8 -2 -6 143.04 8.48 -8 2 -6 128.10 13.30 8 -2 6 88.41 15.19 8 2 6 101.05 4.32 8 -2 6 132.71 7.93 -6 -4 -7 419.49 22.04 -6 4 -7 491.88 23.10 6 -4 7 472.06 22.23 6 4 7 452.26 23.26 12 -6 -3 27.10 6.16 -12 6 3 40.97 17.25 -12 6 3 35.65 13.94 -12 -6 3 46.30 18.56 -12 -6 3 37.93 10.67 12 6 -3 45.52 8.65 -10 8 5 498.19 25.74 -10 8 5 463.38 23.02 10 -8 -5 463.03 22.10 -10 -8 5 442.64 11.94 -10 -8 5 449.08 21.22 -10 -8 5 454.09 20.70 -10 -8 5 427.14 7.73 -10 6 -2 332.02 16.96 -10 6 -2 335.69 29.26 10 -6 2 341.66 17.22 10 -6 2 351.26 25.30 -10 -6 -2 295.41 17.26 10 6 2 321.41 16.90 10 6 2 336.74 17.18 -10 -6 -2 326.55 19.66 12 3 1 184.60 10.59 12 -3 1 182.62 12.03 -12 3 -1 158.62 18.21 -12 -3 -1 176.30 12.60 -12 3 -1 182.45 14.99 -12 -3 -1 166.53 10.93 0 -11 4 60.80 8.64 0 -11 -4 59.16 12.14 0 11 -4 69.07 7.36 0 -11 -4 57.75 7.37 0 11 4 86.98 12.24 0 -11 4 67.58 8.32 -10 -5 9 0.33 4.34 10 -5 -9 3.29 3.49 -10 5 9 3.38 6.05 -10 -5 9 12.95 14.89 -10 5 9 1.86 3.10 -7 0 -7 1.73 2.14 -7 0 -7 1.30 1.44 -7 0 -7 4.94 5.67 7 0 7 1.87 2.27 7 0 7 1.58 2.03 10 3 -10 357.10 17.26 -10 3 10 386.55 23.30 10 -3 -10 348.50 21.26 -10 -3 10 358.21 17.61 10 3 -10 355.33 22.97 -10 3 10 406.58 23.81 -10 -3 10 356.36 21.00 -7 10 0 184.33 31.95 7 -10 0 143.39 13.06 7 -10 0 140.90 10.77 7 10 0 159.93 13.26 -7 -10 0 134.34 12.07 -7 -10 0 136.75 10.16 -9 9 4 251.51 29.63 -9 9 4 243.48 14.66 9 -9 -4 255.06 14.32 9 9 -4 251.97 15.19 -9 -9 4 258.45 9.58 -9 -9 4 260.16 23.43 1 -10 -6 279.39 15.61 1 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1 -6 355.41 17.83 -9 1 -6 390.20 22.30 -14 -1 1 248.76 14.05 -14 1 1 240.57 14.63 -14 1 1 246.45 13.27 -14 -1 1 296.07 16.85 14 -1 -1 266.14 21.46 14 1 -1 248.87 14.48 -9 8 8 6.56 6.30 -9 -8 8 3.43 4.62 -9 8 8 0.88 2.80 9 -8 -8 4.41 4.63 -9 -8 8 4.13 5.38 3 0 10 34.92 12.22 -3 0 -10 34.50 7.61 -3 0 -10 29.48 7.86 5 -10 4 241.34 10.92 5 10 4 241.53 28.28 5 10 4 234.80 11.72 -5 10 -4 269.75 14.31 -5 -10 -4 231.43 14.33 -5 -10 -4 251.46 13.17 5 -10 4 250.83 15.56 5 -10 4 252.89 11.71 -12 7 2 177.80 13.07 -12 7 2 167.98 39.04 12 -7 -2 168.77 12.90 -12 -7 2 164.98 11.99 -12 -7 2 200.53 12.01 12 7 -2 155.52 12.02 -2 9 -7 136.36 19.95 2 -9 7 137.31 7.76 2 -9 7 126.82 12.14 -2 9 -7 122.45 7.31 -2 -9 -7 98.05 7.96 2 9 7 108.58 10.64 -2 -9 -7 107.26 4.67 5 -7 -10 178.09 18.94 5 7 -10 163.29 9.13 5 -7 -10 203.47 19.20 -5 -7 10 161.15 13.03 -5 7 10 195.59 14.71 5 7 -10 177.74 4.42 -5 -7 10 162.18 11.06 -1 -10 7 24.17 15.54 -1 -10 7 40.65 8.50 1 10 -7 42.07 7.37 -1 10 7 42.01 18.84 1 -10 -7 20.24 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259.36 10.06 -13 -6 2 184.13 17.17 -2 12 -3 32.42 9.18 2 12 3 34.61 9.88 -2 -12 -3 30.84 15.10 -2 -12 -3 48.78 19.78 2 -12 3 31.17 8.27 2 -12 3 49.86 9.68 -2 5 11 287.99 18.79 2 5 -11 332.79 17.45 2 -5 -11 358.08 18.56 -2 -5 11 290.13 17.82 2 -5 -11 289.67 18.12 -2 -5 11 305.93 16.54 2 -11 5 55.47 8.76 2 -11 5 42.64 5.62 -2 11 -5 52.78 21.87 2 11 5 70.67 10.17 -2 -11 -5 41.39 3.97 -2 -11 -5 64.76 10.40 -10 3 -5 5.96 7.27 -10 -3 -5 10.48 3.18 -10 3 -5 4.70 4.24 10 -3 5 6.53 2.89 -10 -3 -5 8.71 4.93 10 -3 5 11.71 9.27 10 3 5 6.26 3.52 -10 -3 -5 5.39 2.52 -8 8 9 28.29 9.71 -8 8 9 29.40 12.44 8 -8 -9 27.62 13.34 -8 -8 9 21.11 6.31 -8 -8 9 30.04 8.55 -15 1 5 6.34 4.85 15 1 -5 45.13 7.37 -15 1 5 30.76 8.28 -15 -1 5 36.61 8.60 -15 -1 5 42.16 14.78 15 -1 -5 47.12 7.43 -10 9 6 294.26 22.34 -10 9 6 349.15 21.47 10 -9 -6 281.61 26.41 -10 -9 6 310.07 16.35 -10 -9 6 300.34 16.41 -10 -9 6 339.74 19.07 -10 -9 6 315.93 19.17 5 11 -6 67.32 9.20 -5 -11 6 73.31 11.55 -5 11 6 72.91 12.43 5 -11 -6 70.41 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4 20.37 9.12 8 -2 -12 496.57 23.85 -8 2 12 493.60 23.59 -8 -2 12 505.55 30.45 -8 2 12 525.15 32.88 8 2 -12 524.63 26.21 8 2 -12 481.60 20.33 -8 -2 12 535.18 23.43 6 3 -12 20.87 4.82 -6 3 12 15.54 4.99 6 3 -12 12.87 7.44 -6 3 12 24.90 11.99 -6 -3 12 21.44 12.75 -6 -3 12 23.02 12.74 6 -3 -12 15.60 9.60 5 -3 -12 1.09 2.96 -5 -3 12 3.13 3.24 -5 3 12 3.35 6.45 -5 -3 12 5.13 3.77 -5 3 12 6.45 5.27 5 3 -12 3.01 3.08 5 3 -12 6.95 3.10 14 -4 -2 3.17 5.06 -14 4 2 2.28 6.02 -14 -4 2 1.60 3.99 -14 4 2 3.21 2.69 -14 -4 2 6.54 3.82 14 4 -2 4.79 5.58 -9 -3 -6 1200.04 46.17 9 3 6 1058.49 40.94 9 -3 6 1163.05 53.00 -9 3 -6 1246.88 26.50 -9 -3 -6 1082.59 43.88 -9 -3 -6 1081.35 45.45 -9 3 -6 1202.22 45.83 14 3 -1 149.21 18.91 -14 3 1 149.45 13.26 -14 -3 1 109.75 13.21 -14 -3 1 163.34 12.12 14 -3 -1 178.66 11.72 -14 3 1 165.16 14.46 9 -8 3 25.88 2.83 9 -8 3 21.62 9.63 -9 8 -3 12.85 9.15 -9 -8 -3 29.53 5.35 9 8 3 21.99 2.58 9 8 3 34.50 7.15 9 8 3 17.20 7.59 -3 -2 12 621.70 27.27 3 2 -12 556.89 24.05 -3 2 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5.09 11 8 0 0.81 2.91 -11 8 0 1.15 0.82 -11 -8 0 2.57 4.16 -11 8 0 -0.44 7.22 -7 -5 -7 1.76 3.57 -7 5 -7 7.31 4.67 7 5 7 5.57 9.40 7 -5 7 8.29 6.98 6 9 5 4.01 1.54 6 9 5 3.28 1.52 6 -9 5 4.09 5.75 -6 -9 -5 6.65 5.18 6 -9 5 2.59 1.91 -6 9 -5 -2.36 5.53 6 9 5 12.96 5.76 4 3 -12 16.84 7.79 -4 3 12 6.29 8.53 -4 -3 12 22.27 11.57 -4 3 12 23.19 9.33 4 -3 -12 16.87 6.53 -4 -3 12 16.95 16.49 0 -11 -6 73.69 9.98 0 -11 6 55.43 4.73 0 11 -6 73.13 8.21 0 11 6 73.18 10.60 0 -11 -6 69.36 7.55 0 -11 6 69.66 12.25 14 -1 0 535.21 24.60 14 1 0 449.19 23.29 -14 -1 0 421.14 22.36 -14 1 0 470.54 21.31 -14 1 0 443.63 24.16 -9 1 12 512.45 29.66 -9 -1 12 472.81 20.56 9 1 -12 532.70 26.75 9 1 -12 465.43 20.69 9 -1 -12 508.42 31.09 -9 -1 12 474.24 25.28 -9 1 12 416.21 23.71 -5 -6 11 15.10 5.25 5 -6 -11 3.46 3.12 5 -6 -11 10.92 6.92 -5 6 11 16.04 8.74 -5 -6 11 23.92 7.49 5 6 -11 14.73 4.85 5 6 -11 18.02 5.65 7 -1 8 12.17 3.78 -7 -1 -8 13.79 2.59 7 1 8 9.83 4.90 -7 -1 -8 13.32 5.17 -7 1 -8 13.20 3.98 -7 1 -8 12.97 4.72 -7 -1 -8 19.56 6.78 -7 1 -8 12.14 4.65 -8 7 10 18.19 11.03 -8 7 10 2.42 4.86 -8 -7 10 8.36 4.83 -8 -7 10 5.64 5.78 8 -7 -10 2.76 3.82 7 -11 -5 20.13 7.32 -7 11 5 16.08 11.15 7 -11 -5 29.22 10.13 7 11 -5 21.82 9.91 -7 -11 5 21.08 6.24 -7 -11 5 13.04 9.09 -3 6 -9 78.30 16.27 3 -6 9 79.45 9.31 3 6 9 59.96 13.46 -3 -6 -9 58.50 8.86 -10 8 8 36.96 7.69 -10 8 8 37.12 13.59 10 -8 -8 38.24 8.52 -10 -8 8 28.05 16.20 -10 -8 8 35.55 13.28 -3 -9 -7 25.69 9.11 -3 9 -7 23.63 12.00 3 9 7 30.16 13.78 3 -9 7 29.98 5.23 3 -9 7 29.63 14.25 -3 -9 -7 26.16 3.31 -14 -4 7 6.66 7.40 -14 4 7 7.19 5.25 -14 -4 7 4.62 3.51 -14 4 7 4.01 5.95 14 4 -7 -1.00 5.87 14 -4 -7 5.04 5.98 -12 7 7 19.47 13.88 -12 7 7 24.44 6.86 12 -7 -7 20.62 9.06 -12 -7 7 20.58 6.45 -12 -7 7 19.98 9.12 -12 -7 7 21.33 7.54 15 -2 -5 202.45 16.25 15 2 -5 187.64 12.73 -15 2 5 161.43 13.13 -15 -2 5 205.25 16.68 -15 -2 5 185.97 11.82 -15 2 5 218.72 22.22 -2 1 12 609.01 25.68 -2 -1 12 589.40 23.65 2 1 -12 574.29 23.52 -2 -1 12 607.02 24.12 2 -1 -12 548.81 23.05 14 5 -4 5.65 7.40 14 -5 -4 9.33 5.35 -14 5 4 1.88 6.59 -14 -5 4 4.50 2.36 -14 5 4 4.78 3.81 -14 -5 4 6.15 4.93 -10 4 11 30.28 7.60 -10 4 11 26.67 10.29 -10 -4 11 34.90 7.98 10 -4 -11 20.36 6.39 3 -10 6 96.48 4.98 -3 10 -6 83.30 9.55 -3 -10 -6 125.99 21.27 -3 10 -6 99.06 15.30 3 10 6 108.58 11.54 3 -10 6 106.14 10.34 -3 -10 -6 89.82 4.31 -5 -3 -9 37.71 6.59 -5 3 -9 57.60 6.94 -5 3 -9 43.32 3.91 -5 3 -9 41.10 4.52 -5 -3 -9 51.32 14.35 5 3 9 46.74 3.70 5 -3 9 47.70 7.00 -5 -3 -9 44.90 3.92 -13 5 8 111.32 10.91 13 -5 -8 100.25 12.96 -13 5 8 101.30 11.78 -13 -5 8 96.80 9.79 -13 -5 8 106.93 4.35 -13 -5 8 96.80 17.08 13 5 -8 103.51 10.27 -15 1 3 20.68 6.65 -15 1 3 36.69 15.55 15 1 -3 15.45 11.51 15 -1 -3 33.10 14.81 -15 -1 3 36.76 7.38 -15 -1 3 49.59 15.56 -13 0 10 41.08 16.07 13 0 -10 63.24 17.35 -13 0 10 32.06 14.37 -4 -11 -4 15.62 8.11 4 11 4 10.44 5.59 -4 11 -4 10.57 7.68 4 -11 4 12.10 5.12 4 11 4 9.29 3.42 4 -11 4 22.30 8.70 -4 -11 -4 14.83 6.03 -6 6 11 65.56 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1 50.70 23.62 12 7 1 64.43 5.42 -12 -7 -1 67.02 18.22 -12 7 -1 61.59 10.47 -3 -12 -4 37.26 13.53 3 -12 4 28.89 14.55 -3 12 -4 35.48 15.33 -3 -12 -4 36.75 17.12 3 -12 4 28.91 9.03 3 12 4 21.43 8.56 -7 -12 1 2.28 7.97 7 -12 -1 4.45 4.01 7 -12 -1 13.14 5.49 -7 -12 1 6.78 6.45 7 12 -1 12.96 11.35 -7 12 1 4.17 5.32 0 0 -12 6.84 4.46 0 0 -12 13.54 3.77 0 0 12 9.59 3.61 14 6 -6 15.90 7.23 14 -6 -6 11.85 5.72 -14 -6 6 18.73 14.53 -14 6 6 24.33 11.66 -14 -6 6 20.36 9.33 -14 6 6 5.23 10.43 -12 -6 -2 124.87 9.17 -12 6 -2 125.13 5.32 -12 -6 -2 117.22 8.12 -12 6 -2 160.79 21.23 12 -6 2 118.49 8.81 12 6 2 129.77 6.02 -10 -7 10 155.33 16.50 -10 7 10 154.11 31.09 -10 -7 10 137.25 18.90 10 -7 -10 143.06 10.55 -10 7 10 150.00 26.11 4 13 -2 2.68 3.94 -4 13 2 4.17 6.14 -4 -13 2 3.00 5.23 4 -13 -2 3.60 4.58 -4 -13 2 1.49 6.86 4 -13 -2 -0.25 5.14 14 4 0 5.75 3.09 14 -4 0 9.73 7.38 -14 -4 0 5.08 6.16 -14 4 0 4.69 2.10 -14 -4 0 7.63 4.47 -14 4 0 11.25 8.33 9 -4 -12 85.79 29.53 -9 -4 12 98.84 9.47 -9 -4 12 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48.71 9.83 8 10 3 54.06 23.68 8 -10 3 55.57 9.12 8 -10 3 57.33 9.34 8 10 3 55.30 4.46 -7 1 13 49.26 11.17 -7 1 13 38.76 15.30 7 1 -13 39.96 8.53 -7 -1 13 44.89 14.71 7 -1 -13 46.18 6.72 -7 -1 13 36.57 19.02 -5 -1 13 4.06 6.54 -5 -1 13 1.79 3.15 -5 1 13 2.25 2.78 -5 1 13 3.60 4.76 -5 -1 13 -0.01 2.90 5 -1 -13 4.15 4.39 4 -12 -6 20.95 6.97 4 -12 -6 25.22 8.78 -4 -12 6 26.60 13.74 -4 12 6 26.06 11.88 4 12 -6 18.28 4.80 -4 -12 6 21.75 16.19 -8 5 -7 284.13 16.36 -8 -5 -7 279.62 15.54 -8 -5 -7 263.14 23.74 8 -5 7 266.58 17.22 13 0 3 -0.22 1.57 -13 0 -3 1.33 1.56 -13 0 -3 2.92 2.79 6 -6 8 2.36 6.03 6 6 8 4.52 6.10 -6 6 -8 5.02 5.41 -6 -6 -8 5.78 3.23 -8 0 -8 4.53 6.18 -8 0 -8 2.64 2.63 8 0 8 8.78 3.72 10 -10 0 60.10 8.69 -10 -10 0 73.20 6.27 10 -10 0 60.85 8.25 -10 -10 0 74.36 9.46 10 10 0 69.04 10.98 -10 10 0 52.16 10.49 -13 -1 11 53.97 8.73 13 1 -11 71.51 9.24 -13 1 11 63.57 7.22 -13 -1 11 61.03 6.02 -13 1 11 43.74 21.07 13 -1 -11 64.14 8.88 -11 2 12 3.57 6.32 11 2 -12 2.06 1.77 11 2 -12 7.42 6.12 11 -2 -12 5.53 4.85 -11 2 12 5.12 6.07 -11 -2 12 4.71 6.29 -11 -2 12 4.33 3.52 -4 -13 3 197.87 13.01 4 13 -3 186.39 12.74 -4 13 3 182.61 25.78 4 -13 -3 176.35 12.02 -4 -13 3 162.52 21.76 4 -13 -3 182.17 21.40 -14 6 2 86.40 16.13 -14 -6 2 87.06 9.29 -14 6 2 93.87 16.12 14 6 -2 88.71 17.71 14 -6 -2 98.83 9.56 -14 -6 2 118.13 10.42 -10 7 -4 80.12 8.74 10 -7 4 86.25 2.68 -10 -7 -4 84.52 13.42 10 7 4 78.38 3.20 -10 -7 -4 111.89 14.49 10 7 4 85.01 3.32 10 -7 4 77.52 19.73 10 -7 4 72.73 2.95 -8 -10 8 5.85 5.68 8 -10 -8 2.23 5.48 -8 -10 8 3.53 4.65 -8 -10 8 1.53 1.14 -8 10 8 9.67 5.96 8 -10 -8 3.21 3.16 -8 -10 8 1.76 0.88 6 -9 6 81.32 18.36 -6 9 -6 81.38 11.77 6 9 6 88.60 14.86 -6 -9 -6 84.61 10.62 -11 9 7 4.58 4.74 -11 -9 7 0.29 1.13 -11 9 7 9.78 12.30 -11 -9 7 16.28 14.17 -11 -9 7 3.61 4.75 11 -9 -7 -0.46 3.05 11 -5 -11 494.18 22.82 -11 -5 11 464.93 28.96 -11 -5 11 452.98 21.49 -11 5 11 502.16 24.81 -11 5 11 410.26 20.79 16 0 -5 1.99 5.77 -16 0 5 8.25 5.94 -16 0 5 4.76 4.64 14 4 -9 264.41 13.35 14 4 -9 276.54 16.42 -14 4 9 249.67 17.04 -14 -4 9 267.14 17.06 14 -4 -9 262.83 20.58 -14 -4 9 258.29 14.39 -14 4 9 239.94 26.86 0 2 -12 9.54 5.71 0 2 12 9.07 11.63 0 -2 -12 14.01 6.74 0 -2 12 9.39 7.77 0 2 -12 13.73 4.53 0 -2 -12 15.05 5.92 6 -10 5 0.57 1.14 -6 10 -5 8.19 7.29 6 -10 5 12.59 11.67 6 -10 5 0.00 1.01 -6 -10 -5 -0.59 4.97 -6 -10 -5 0.94 0.69 6 10 5 1.66 5.33 -12 -9 4 129.35 9.81 -12 -9 4 148.72 18.56 -12 -9 4 147.20 10.51 -12 9 4 139.72 11.67 -12 9 4 124.99 14.22 12 -9 -4 144.25 11.51 -13 -1 -3 4.06 3.00 -13 1 -3 2.67 2.36 -13 -1 -3 2.45 4.66 -13 1 -3 1.39 4.46 13 1 3 2.85 2.72 13 -1 3 2.58 2.29 -7 -12 0 96.19 23.55 7 -12 0 113.52 7.49 7 12 0 130.05 10.70 -7 -12 0 113.74 8.16 -7 12 0 131.97 12.31 7 -12 0 97.03 18.64 -8 1 -8 9.03 6.19 -8 -1 -8 0.00 5.02 -8 1 -8 6.81 2.06 -8 -1 -8 3.91 4.26 8 -1 8 8.97 2.78 8 1 8 8.12 3.48 8 -1 8 3.85 3.57 -8 -1 -8 5.60 2.92 8 -5 -12 167.54 14.69 -8 -5 12 139.37 21.00 -8 5 12 136.92 13.60 -8 5 12 133.72 12.99 -8 -5 12 160.91 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103.69 13.85 8 -7 6 87.24 9.11 3 -5 -12 153.97 9.32 3 -5 -12 143.06 13.38 3 5 -12 133.81 7.79 -3 5 12 142.18 11.76 -3 -5 12 139.55 13.68 -3 -5 12 133.02 10.64 -9 11 5 140.96 46.54 9 -11 -5 160.07 12.70 -9 -11 5 156.45 16.49 9 -11 -5 162.47 11.21 -9 -11 5 149.67 17.56 9 11 -5 139.00 13.21 -12 -9 3 19.12 7.49 -12 9 3 27.93 14.94 12 -9 -3 20.22 7.73 12 9 -3 26.36 10.67 -12 -9 3 32.51 9.24 -12 9 3 29.39 13.91 -7 -11 7 35.80 7.60 -7 11 7 44.75 21.31 7 11 -7 38.41 8.56 7 -11 -7 42.13 6.15 -7 -11 7 44.48 17.24 -7 -11 7 41.40 16.72 7 -11 -7 19.69 6.71 15 -3 -8 3.93 8.45 -15 -3 8 1.87 2.18 -15 3 8 2.64 4.97 -15 -3 8 2.03 2.64 15 3 -8 11.06 7.02 -15 3 8 2.64 5.68 -12 -5 -3 76.53 21.42 12 5 3 94.09 9.18 12 -5 3 101.09 8.16 -12 5 -3 97.27 29.43 12 -5 3 73.10 3.28 -12 -5 -3 92.90 7.88 -12 5 -3 88.13 6.47 5 0 10 181.53 11.15 -5 0 -10 210.35 11.75 -5 0 -10 224.17 14.24 -10 9 -2 181.14 17.61 10 -9 2 167.19 19.34 10 9 2 161.39 18.03 10 9 2 155.85 12.13 10 -9 2 153.12 7.60 -10 -9 -2 163.68 11.84 10 -9 2 169.49 9.08 16 1 -5 3.99 5.71 -16 1 5 8.80 12.13 -16 1 5 11.19 4.80 -16 -1 5 10.52 4.12 16 -1 -5 10.35 6.45 -16 -1 5 20.46 7.08 -14 2 10 27.76 12.42 -14 -2 10 26.40 5.94 14 -2 -10 32.85 10.85 -14 -2 10 22.52 9.46 -14 2 10 13.29 13.93 14 2 -10 33.02 8.93 -13 8 4 8.83 6.28 -13 8 4 3.08 7.60 13 -8 -4 1.14 3.84 -13 -8 4 -3.48 2.15 13 8 -4 7.76 6.45 -13 -8 4 2.42 3.40 6 -2 -13 12.29 5.73 -6 -2 13 6.11 3.12 -6 -2 13 2.93 4.49 -6 -2 13 5.63 5.41 -6 2 13 5.73 5.11 -6 2 13 5.07 4.87 -16 0 4 77.47 14.98 -16 0 4 83.03 11.06 16 0 -4 71.85 12.01 2 -13 -4 12.38 8.54 -2 -13 4 9.31 6.22 2 13 -4 17.61 6.75 -2 13 4 1.69 6.17 -2 -13 4 16.59 7.34 2 -13 -4 6.54 9.92 -3 13 -2 123.73 23.05 3 -13 2 112.68 7.72 3 13 2 98.13 13.66 -3 -13 -2 136.75 13.21 3 -13 2 129.94 12.89 -3 -13 -2 141.53 11.46 16 0 -6 955.25 37.83 -16 0 6 1026.78 39.88 -16 0 6 1078.55 43.58 -4 -4 -10 50.14 7.97 4 -4 10 43.82 6.95 -4 4 -10 45.02 1.80 4 4 10 49.06 24.83 -4 4 -10 66.34 13.64 -4 -4 -10 47.64 2.70 -4 4 -10 47.89 2.17 -14 3 -1 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7.02 6.34 4 -9 8 7.35 6.75 -4 0 -11 4.21 4.31 -4 0 -11 -0.89 2.30 4 0 11 1.20 1.37 -16 2 2 54.49 8.97 -16 2 2 39.06 20.94 -16 -2 2 58.13 10.71 -16 -2 2 57.81 13.44 16 2 -2 52.22 11.81 16 -2 -2 42.90 19.78 10 9 3 267.52 28.78 10 9 3 195.57 8.28 10 -9 3 237.21 21.59 10 9 3 180.33 7.45 10 -9 3 247.63 15.10 -10 -9 -3 199.09 11.48 -10 9 -3 221.44 28.10 7 10 5 141.88 16.08 7 10 5 152.59 3.34 7 -10 5 163.65 14.01 -7 -10 -5 145.93 12.86 7 -10 5 139.35 3.41 7 -10 5 148.03 3.16 -7 10 -5 144.88 15.31 13 -4 3 23.22 6.78 -13 4 -3 16.77 8.37 -13 -4 -3 21.37 7.98 -13 -4 -3 25.74 5.39 13 4 3 26.78 5.76 -13 4 -3 21.14 9.44 -2 9 -9 51.80 3.31 2 -9 9 61.40 9.95 2 -9 9 57.97 3.36 -2 9 -9 64.57 7.43 2 9 9 69.55 10.58 -2 -9 -9 69.05 13.85 -1 14 2 13.15 7.40 1 14 -2 15.45 5.43 1 -14 -2 18.05 10.63 -1 -14 2 26.17 9.22 -1 -14 2 18.96 5.92 1 -14 -2 15.64 6.99 -7 9 -6 7.14 7.43 7 -9 6 0.92 6.23 -7 -9 -6 4.66 4.36 7 9 6 3.72 5.79 1 3 12 220.12 14.59 -1 3 -12 211.25 11.70 -1 -3 -12 216.02 11.14 -1 3 -12 198.02 9.09 1 -3 12 207.44 15.55 -1 -3 -12 195.55 8.39 -1 -3 -12 175.03 21.26 8 -4 8 2.91 4.29 -8 -4 -8 0.68 3.12 -8 -4 -8 9.01 7.93 -8 4 -8 -0.11 2.57 0 13 -5 5.05 4.17 0 -13 -5 -0.24 2.42 0 -13 5 -1.46 7.21 0 -13 -5 8.46 5.86 0 -13 5 3.00 3.35 0 13 5 2.20 6.75 -10 0 -7 0.99 1.39 -10 0 -7 -2.79 5.21 10 0 7 3.17 2.89 12 1 5 1.67 2.26 -12 1 -5 1.36 3.63 -12 -1 -5 3.05 5.09 -12 1 -5 0.92 1.81 -12 -1 -5 1.84 2.03 12 -1 5 4.86 3.70 -8 -8 -6 19.56 7.42 8 -8 6 18.19 8.00 8 8 6 9.87 10.41 -8 8 -6 12.28 3.74 9 10 3 36.06 13.47 9 10 3 42.42 9.95 9 10 3 27.24 7.56 9 -10 3 39.54 4.10 -9 -10 -3 35.63 22.40 9 -10 3 36.80 6.89 9 -10 3 42.51 20.01 -9 10 -3 48.53 9.32 16 2 -8 -3.01 6.72 -16 2 8 7.64 6.14 -16 -2 8 1.39 3.09 -16 -2 8 2.74 3.18 -16 2 8 3.18 5.67 16 -2 -8 0.79 5.28 -5 -12 -4 655.37 33.95 5 -12 4 617.85 30.35 -5 12 -4 604.02 32.96 5 12 4 540.76 30.45 5 -12 4 555.45 29.96 -5 -12 -4 629.79 29.92 6 13 -4 124.24 7.87 -6 -13 4 127.51 7.84 -6 13 4 129.84 16.79 6 -13 -4 138.65 9.43 -6 -13 4 136.55 19.90 6 -13 -4 140.49 10.11 -15 6 6 8.00 11.53 -15 -6 6 8.75 3.08 -15 -6 6 8.93 9.39 -15 6 6 4.08 3.99 15 -6 -6 9.74 5.29 15 6 -6 8.90 6.67 -4 -1 -11 4.59 2.68 4 1 11 10.07 5.97 4 -1 11 11.85 6.39 -4 1 -11 19.37 6.23 -4 -1 -11 10.69 6.65 -4 1 -11 11.78 4.35 1 -12 -7 73.62 9.32 -1 -12 7 77.08 10.45 1 -12 -7 77.15 7.86 -1 -12 7 68.95 4.79 -1 12 7 69.44 12.38 1 12 -7 76.01 10.05 0 -14 -2 6.53 6.41 0 -14 2 -0.17 5.56 0 14 -2 7.98 6.09 0 -14 -2 5.45 5.82 0 14 2 0.94 3.07 0 -14 2 1.73 3.37 -16 4 5 2.44 4.68 16 -4 -5 3.33 5.83 16 4 -5 3.93 4.74 -16 4 5 1.53 4.54 -16 -4 5 2.13 1.79 -16 -4 5 3.24 4.39 14 3 2 82.57 13.40 14 -3 2 92.59 10.06 -14 -3 -2 95.46 8.60 -14 3 -2 95.49 5.75 -14 3 -2 78.10 12.00 -14 -3 -2 112.26 9.51 0 -7 -11 3.52 5.00 0 7 11 11.54 10.10 0 7 -11 0.63 2.07 0 -7 11 3.15 2.04 0 7 -11 2.59 1.30 0 -7 11 3.99 4.34 0 -7 -11 2.41 1.95 -7 -12 -2 25.21 4.95 7 12 2 37.29 9.81 -7 12 -2 18.60 10.34 7 -12 2 19.80 6.65 -7 -12 -2 26.55 13.33 7 -12 2 18.75 6.35 2 -14 -2 1.76 3.76 -2 -14 2 2.93 2.97 2 14 -2 0.43 4.70 -2 -14 2 5.61 5.35 2 -14 -2 4.12 3.31 -2 14 2 1.80 6.53 -7 3 -9 91.92 2.42 -7 -3 -9 95.70 10.26 -7 -3 -9 99.58 5.48 -7 3 -9 101.44 2.11 -7 -3 -9 94.50 7.48 7 -3 9 91.88 7.44 7 3 9 99.24 4.19 -7 3 -9 114.07 13.61 -14 6 0 143.29 11.08 -14 -6 0 138.44 23.93 -14 6 0 151.01 11.22 -14 -6 0 167.41 9.94 14 -6 0 156.76 11.76 14 6 0 167.33 9.28 -9 6 12 32.09 13.49 -9 -6 12 20.78 14.86 -9 6 12 20.00 6.62 -9 -6 12 25.55 12.15 9 -6 -12 33.58 13.16 -11 -5 -5 123.60 9.71 11 5 5 129.35 4.55 11 -5 5 117.33 8.48 -11 5 -5 121.63 18.60 11 -5 5 120.11 3.29 -11 -5 -5 113.84 14.00 -11 5 -5 117.55 3.31 10 -5 6 59.88 23.12 10 5 6 51.35 1.69 -10 -5 -6 56.96 19.62 -10 -5 -6 64.66 27.31 -10 5 -6 71.48 10.81 7 -6 8 39.13 8.56 -7 -6 -8 26.74 5.67 -7 6 -8 34.78 18.92 7 6 8 37.41 16.84 3 4 11 978.64 52.15 -3 -4 -11 1013.25 45.57 -3 -4 -11 863.23 38.87 3 -4 11 1068.03 54.54 -3 4 -11 1017.69 48.50 -3 -4 -11 1180.43 55.96 -3 4 -11 995.70 44.63 0 -11 8 15.22 7.63 0 -11 -8 14.19 5.84 0 -11 8 12.98 11.05 0 -11 -8 7.40 6.46 0 11 -8 5.32 6.61 0 11 8 6.53 6.99 -10 -1 -7 3.55 3.09 -10 1 -7 2.98 2.34 -10 1 -7 2.25 4.88 -10 -1 -7 2.73 3.81 10 -1 7 9.86 4.02 10 1 7 1.96 2.02 -8 -4 13 92.91 8.47 -8 4 13 113.25 10.62 -8 4 13 95.11 37.15 8 4 -13 101.93 3.30 8 4 -13 94.39 7.13 8 -4 -13 94.19 8.36 -8 -4 13 88.83 12.10 14 2 -11 52.64 18.15 -14 2 11 50.40 22.74 14 -2 -11 55.73 12.77 -14 -2 11 48.62 9.61 -14 2 11 56.59 18.79 -14 -2 11 55.12 13.56 14 2 -11 38.52 5.40 4 -4 -13 54.09 20.80 -4 -4 13 101.01 9.01 4 -4 -13 80.24 8.50 -4 -4 13 55.52 4.91 -4 4 13 92.61 13.87 4 4 -13 79.85 10.30 -8 8 11 3.26 6.20 -8 -8 11 -0.96 3.65 8 -8 -11 6.24 8.08 -8 -8 11 9.59 7.11 8 -8 -11 1.79 1.48 -15 5 8 102.83 12.38 -15 -5 8 106.74 8.69 -15 -5 8 142.11 12.45 -15 5 8 120.00 12.17 15 5 -8 123.88 11.72 15 -5 -8 108.09 10.14 -2 6 12 32.30 7.37 2 6 -12 37.75 8.75 2 -6 -12 35.59 7.60 -2 -6 12 35.66 4.88 2 -6 -12 34.95 8.77 -2 -6 12 33.97 10.19 -5 4 -10 128.69 18.74 5 -4 10 133.11 8.95 -5 -4 -10 137.22 9.12 5 4 10 170.15 21.76 -9 -11 7 46.13 6.93 9 11 -7 53.88 6.29 9 -11 -7 56.51 6.75 -9 -11 7 67.20 8.67 9 -11 -7 68.89 31.22 -9 11 7 55.62 16.87 0 10 -9 167.99 22.11 0 10 9 173.29 26.04 0 -10 -9 166.87 7.48 0 -10 -9 158.71 10.76 0 -10 9 157.98 22.09 0 10 -9 161.70 6.61 0 10 9 162.03 5.61 0 -10 9 169.66 7.54 2 12 6 33.41 9.72 -2 12 -6 41.51 21.33 2 -12 6 36.20 7.44 -2 -12 -6 39.05 9.19 -2 -12 -6 33.32 10.54 2 -12 6 29.56 9.90 -15 6 3 35.47 28.92 -15 -6 3 27.32 14.47 15 6 -3 37.50 7.82 -15 6 3 35.19 8.52 -15 -6 3 29.60 16.16 15 -6 -3 40.20 8.47 11 10 0 85.29 6.86 11 10 0 115.03 10.88 -11 10 0 99.09 20.43 -11 -10 0 113.02 9.53 11 -10 0 78.14 6.14 11 -10 0 100.61 9.52 5 -13 -5 10.67 5.39 -5 -13 5 8.15 9.86 -5 -13 5 7.98 5.67 -5 13 5 7.64 13.17 5 13 -5 6.99 5.41 5 -13 -5 12.99 6.49 -13 0 12 11.97 5.97 -13 0 12 13.99 5.37 13 0 -12 13.53 7.93 2 14 1 36.30 8.30 2 -14 1 18.27 11.71 -2 -14 -1 37.25 7.36 2 -14 1 33.74 24.72 -2 -14 -1 38.87 14.09 -2 14 -1 29.76 14.53 16 -4 -4 12.87 12.39 -16 4 4 6.84 8.22 -16 -4 4 7.34 6.92 -16 4 4 24.82 7.56 -16 -4 4 6.94 4.19 16 4 -4 18.52 5.85 -13 7 9 12.95 6.75 13 -7 -9 1.96 4.15 -13 -7 9 0.61 0.63 -13 -7 9 3.11 4.26 13 7 -9 1.25 9.78 -13 7 9 8.50 12.12 -16 4 6 176.94 13.11 -16 4 6 148.20 10.98 -16 -4 6 179.59 12.56 16 -4 -6 174.08 12.18 -16 -4 6 166.53 9.37 16 4 -6 168.85 13.13 2 -8 -11 59.13 9.85 -2 8 11 80.94 21.26 2 -8 -11 35.58 8.94 -2 -8 11 48.42 23.81 -2 -8 11 57.71 7.37 2 8 -11 57.81 6.59 -12 9 0 149.82 12.92 -12 -9 0 136.57 15.52 12 -9 0 149.14 11.05 12 9 0 143.62 9.24 -12 9 0 165.17 42.35 -12 -9 0 146.57 8.95 -14 5 -1 0.53 1.90 14 -5 1 1.66 3.02 -14 -5 -1 5.47 3.67 14 5 1 6.05 4.54 -14 -5 -1 4.53 4.09 -14 5 -1 6.45 5.63 3 -14 -1 172.39 21.23 3 14 -1 208.26 23.75 -3 14 1 190.03 19.16 -3 -14 1 197.45 12.35 3 -14 -1 204.22 11.26 -3 -14 1 212.49 13.91 15 4 -9 46.82 9.81 -15 -4 9 42.45 10.12 -15 4 9 46.31 8.15 -15 -4 9 13.57 5.90 -15 4 9 37.20 13.83 15 -4 -9 53.68 11.13 -10 10 8 10.17 12.66 -10 -10 8 0.51 2.92 10 -10 -8 2.46 4.18 -10 -10 8 2.87 3.90 10 -10 -8 3.39 7.38 9 -12 -3 131.45 12.09 -9 -12 3 166.75 11.55 9 -12 -3 141.22 19.13 -9 -12 3 133.99 18.42 -9 12 3 107.47 13.40 9 12 -3 142.71 14.74 15 0 1 6.28 6.33 -15 0 -1 1.79 5.48 -15 0 -1 -0.15 3.19 -15 2 10 6.91 5.60 15 2 -10 6.77 7.49 15 -2 -10 8.69 8.88 -15 -2 10 15.74 6.84 -15 2 10 15.61 8.51 -15 -2 10 12.16 5.49 -11 -2 -6 126.09 9.72 -11 2 -6 150.74 10.53 -11 -2 -6 159.82 10.79 11 -2 6 134.57 5.42 11 2 6 140.10 7.04 11 -2 6 169.02 9.78 -11 2 -6 151.41 5.11 12 -7 -10 96.16 8.33 -12 -7 10 93.99 10.47 -12 7 10 84.36 17.14 -12 7 10 109.88 14.66 -12 -7 10 86.33 10.18 6 0 10 524.33 25.62 -6 0 -10 592.14 28.25 -6 0 -10 525.29 33.74 5 13 2 8.86 8.51 -5 13 -2 17.68 6.59 5 -13 2 11.22 6.79 -5 -13 -2 8.55 4.63 5 -13 2 6.16 3.44 -5 -13 -2 8.74 5.03 13 -7 1 22.73 8.52 -13 7 -1 25.35 8.96 -13 -7 -1 33.82 11.99 -13 -7 -1 28.70 13.47 13 7 1 28.63 8.30 -13 7 -1 30.36 5.96 -13 -6 10 8.27 6.58 13 -6 -10 -1.21 4.27 13 6 -10 -1.33 6.25 -13 6 10 6.42 6.38 -13 6 10 3.60 3.28 11 8 3 83.94 8.76 11 -8 3 68.23 8.90 -11 -8 -3 79.81 9.56 -11 8 -3 74.26 10.31 -11 -8 -3 70.11 12.68 11 8 3 76.91 8.53 11 -8 3 79.65 15.81 4 -13 3 2.71 2.78 -4 13 -3 0.17 5.50 4 13 3 2.26 3.21 -4 -13 -3 8.95 8.72 4 -13 3 8.70 7.03 -4 -13 -3 1.22 2.96 13 -9 -4 14.64 6.02 -13 9 4 17.73 11.41 -13 9 4 4.94 6.67 -13 -9 4 5.61 5.89 13 9 -4 9.95 4.91 -13 -9 4 4.36 3.06 13 1 -12 269.41 20.48 13 -1 -12 275.69 24.50 -13 -1 12 253.26 16.46 -13 -1 12 240.52 14.14 -13 1 12 271.54 34.91 -13 1 12 280.16 18.76 13 0 4 786.36 38.35 -13 0 -4 770.65 36.61 -13 0 -4 593.78 31.26 2 0 12 2.24 3.14 -2 0 -12 -1.64 3.54 -2 0 -12 2.19 2.79 -12 -8 9 1.01 2.82 -12 -8 9 0.95 5.89 -12 8 9 -1.05 5.40 -12 8 9 4.12 7.90 12 -8 -9 -0.52 3.15 -11 0 13 10.68 6.32 11 0 -13 3.56 4.71 -11 0 13 0.19 2.03 6 12 -7 160.83 6.97 -6 -12 7 149.68 5.38 6 -12 -7 178.96 17.42 -6 -12 7 160.15 35.30 -6 -12 7 164.35 10.05 6 -12 -7 175.01 15.41 -6 12 7 214.58 18.85 1 0 -13 1.06 3.79 1 0 -13 1.04 2.82 -1 0 13 1.67 1.78 9 12 -2 0.08 1.93 -9 -12 2 4.88 4.17 9 -12 -2 8.44 3.86 -9 -12 2 0.87 3.84 9 -12 -2 2.69 3.44 -9 12 2 1.87 5.02 -1 -14 -2 209.95 15.61 1 -14 2 221.88 14.16 -1 14 -2 233.37 17.20 1 -14 2 238.86 10.34 -1 -14 -2 253.77 18.27 1 14 2 209.42 22.47 -3 -14 0 19.70 11.87 -3 -14 0 15.08 6.80 3 -14 0 14.97 8.74 3 -14 0 15.22 7.45 3 14 0 15.02 7.30 -3 14 0 14.10 11.80 -12 2 -5 71.29 11.00 -12 -2 -5 69.74 8.47 12 -2 5 64.83 12.68 -12 -2 -5 66.64 10.88 12 2 5 60.59 7.31 -12 2 -5 71.40 4.33 6 -10 6 44.42 20.88 -6 -10 -6 55.46 19.30 -6 10 -6 51.83 9.65 6 10 6 52.60 9.06 -11 -10 7 4.60 5.27 -11 10 7 -0.33 5.65 -11 -10 7 3.22 2.43 -11 10 7 12.39 12.34 11 -10 -7 3.48 3.31 -11 -10 7 0.73 4.06 -15 -1 -1 -0.52 3.28 -15 -1 -1 1.02 5.92 -15 1 -1 2.00 2.01 -15 1 -1 -1.71 6.10 15 -1 1 -0.31 3.21 15 1 1 1.58 2.97 10 7 5 0.96 0.60 -10 -7 -5 3.61 4.62 -10 -7 -5 6.64 4.34 -10 7 -5 10.70 7.04 10 -7 5 13.07 6.94 10 7 5 2.76 0.89 -13 -6 -2 31.09 8.06 -13 -6 -2 32.58 13.71 13 -6 2 46.08 20.45 -13 6 -2 32.97 15.91 13 6 2 34.17 8.28 -13 6 -2 36.92 10.14 -6 1 -10 19.49 6.87 -6 1 -10 10.16 3.01 -6 -1 -10 19.63 5.91 6 -1 10 13.51 3.99 6 1 10 18.80 7.84 -6 1 -10 12.55 4.66 -6 -1 -10 14.13 5.01 10 -11 -6 60.02 7.32 -10 -11 6 59.58 9.52 10 -11 -6 76.52 9.28 -10 11 6 86.85 13.12 -10 -11 6 65.12 13.39 10 11 -6 53.46 10.19 -10 -11 6 66.14 8.24 3 14 -2 63.82 13.28 -3 -14 2 41.50 18.99 3 -14 -2 59.19 7.58 3 -14 -2 55.61 23.23 -3 14 2 66.10 12.42 -3 -14 2 58.17 23.21 -12 5 -4 22.27 4.61 -12 -5 -4 25.98 4.91 -12 -5 -4 29.45 9.14 -12 5 -4 36.24 10.16 12 -5 4 21.99 3.56 12 5 4 20.31 5.39 12 -5 4 18.23 5.83 12 5 4 18.82 7.53 4 2 11 111.58 7.07 -4 2 -11 125.61 5.09 -4 -2 -11 106.42 6.18 -4 2 -11 122.07 17.94 -4 2 -11 104.64 4.17 -4 -2 -11 107.56 4.02 4 -2 11 104.09 7.17 -4 -2 -11 100.29 9.24 -9 5 -7 41.45 17.85 -9 -5 -7 39.27 14.57 9 -5 7 44.48 20.75 -9 -5 -7 44.84 13.19 13 1 4 33.87 7.44 -13 1 -4 41.89 7.20 -13 1 -4 43.54 7.12 -13 -1 -4 49.54 6.13 13 -1 4 35.19 6.49 -13 -1 -4 41.58 17.28 12 -10 -4 67.48 24.70 -12 10 4 68.86 12.68 -12 10 4 58.69 6.63 -12 -10 4 65.20 8.74 -12 -10 4 76.76 15.84 -12 -10 4 69.27 9.39 -2 -1 -12 33.36 11.14 2 -1 12 26.75 4.38 2 1 12 22.72 6.07 -2 1 -12 29.29 4.23 -2 1 -12 20.40 6.77 -2 -1 -12 20.51 8.03 11 -1 -13 246.94 18.82 -11 -1 13 278.21 17.98 -11 -1 13 299.62 20.97 11 1 -13 279.36 24.34 -11 1 13 325.38 23.09 -11 1 13 291.86 19.41 7 11 4 251.28 15.04 7 -11 4 273.19 23.16 7 -11 4 251.42 15.82 7 11 4 251.67 29.85 -7 -11 -4 236.00 9.94 7 -11 4 244.47 14.55 -7 11 -4 235.18 26.18 -7 -11 -4 292.14 20.06 -1 1 13 436.87 22.85 -1 1 13 434.47 27.09 1 1 -13 412.02 22.01 -1 -1 13 399.57 20.97 1 -1 -13 366.41 25.85 1 1 -13 404.01 21.73 -15 -5 1 17.93 5.25 -15 5 1 18.15 6.64 -15 -5 1 21.23 7.40 15 5 -1 20.22 4.70 15 -5 -1 22.74 11.97 -15 5 1 24.66 8.17 13 -9 -5 258.19 18.56 -13 9 5 227.79 12.76 -13 9 5 248.27 20.98 -13 -9 5 259.23 18.05 -13 -9 5 289.68 17.64 13 9 -5 248.98 20.47 -9 -12 4 232.73 12.63 9 -12 -4 271.43 19.29 -9 -12 4 253.21 17.52 9 -12 -4 263.75 18.54 -9 12 4 263.04 21.25 9 12 -4 256.39 18.84 6 -7 -12 45.57 5.40 -6 7 12 40.20 13.45 6 7 -12 39.22 2.08 -6 -7 12 40.51 15.45 6 7 -12 36.16 6.90 6 -7 -12 44.73 8.38 -6 -7 12 26.61 7.09 -7 -13 2 172.19 19.41 -7 -13 2 127.99 9.50 7 13 -2 163.62 10.89 7 -13 -2 154.22 22.56 7 -13 -2 182.69 12.02 -7 13 2 170.08 15.93 13 -9 -3 194.63 27.10 -13 9 3 185.58 15.37 -13 9 3 194.29 15.67 13 9 -3 182.48 11.82 -13 -9 3 178.64 17.07 -13 -9 3 188.85 9.83 5 7 -12 38.97 2.81 5 -7 -12 34.67 11.97 5 -7 -12 36.95 8.84 5 7 -12 37.43 7.40 -5 -7 12 38.45 11.14 -5 -7 12 52.73 10.64 -5 7 12 44.43 11.87 -10 2 -7 9.51 3.23 -10 -2 -7 11.24 5.62 -10 2 -7 8.29 4.93 -10 -2 -7 8.02 3.50 10 2 7 10.64 4.11 10 -2 7 8.86 2.08 10 -2 7 12.45 4.18 -10 -2 -7 5.79 4.51 4 12 5 0.96 1.27 4 -12 5 -3.05 5.93 -4 -12 -5 2.09 1.96 -4 -12 -5 9.44 6.43 4 -12 5 1.83 1.91 -4 12 -5 1.21 6.09 4 12 5 5.67 6.13 -9 -7 -6 8.81 5.43 9 -7 6 5.89 6.04 9 7 6 2.69 6.10 -9 7 -6 0.84 5.43 -14 7 1 121.78 8.58 -14 7 1 119.57 14.89 -14 -7 1 124.33 11.61 -14 -7 1 111.03 7.81 14 -7 -1 127.32 22.29 14 7 -1 113.36 7.20 -10 -3 13 25.39 7.16 -10 -3 13 19.60 6.50 -10 3 13 17.78 16.75 10 3 -13 20.53 2.35 10 3 -13 34.25 9.67 -10 3 13 26.22 6.49 10 -3 -13 21.18 10.57 2 3 -13 29.76 4.19 -2 3 13 28.08 7.05 -2 -3 13 31.97 6.91 2 -3 -13 32.55 4.91 -2 -3 13 34.69 13.55 2 -3 -13 26.45 11.43 -16 0 1 -1.20 7.10 -16 0 1 0.46 2.87 16 0 -1 1.88 2.84 12 -10 -3 13.00 7.48 -12 10 3 3.90 7.40 -12 10 3 9.24 6.09 -12 -10 3 14.85 4.21 -12 -10 3 8.32 7.08 -12 -10 3 8.10 7.78 -9 0 -8 119.21 12.81 9 0 8 159.06 6.86 -9 0 -8 122.90 7.56 10 -10 2 358.62 21.40 -10 10 -2 385.22 23.44 -10 -10 -2 370.37 24.47 10 10 2 415.74 25.89 10 -10 2 367.58 25.39 10 10 2 369.29 22.25 -8 11 -3 46.61 12.21 8 11 3 9.27 4.28 8 11 3 15.85 8.30 8 -11 3 10.74 6.88 -8 -11 -3 16.75 4.40 8 -11 3 19.07 3.90 -8 -11 -3 2.42 3.51 9 -9 -10 106.05 14.53 -9 -9 10 128.38 12.30 -9 9 10 103.38 15.17 -9 -9 10 129.29 12.31 9 -9 -10 122.62 9.11 16 -3 -2 143.09 9.78 16 3 -2 178.43 11.65 -16 3 2 194.22 14.43 -16 3 2 170.22 16.39 -16 -3 2 140.56 12.42 -16 -3 2 174.46 17.54 -14 6 9 173.83 17.88 -14 -6 9 135.46 9.06 14 6 -9 157.92 28.66 14 -6 -9 142.24 10.02 -14 -6 9 136.44 10.39 -7 8 -7 20.51 8.66 7 -8 7 18.53 10.03 -7 -8 -7 17.30 5.89 7 8 7 29.28 17.92 -1 -13 -5 79.50 9.69 -1 13 -5 71.51 10.51 1 13 5 73.94 19.64 1 -13 5 61.99 4.85 1 -13 5 86.89 26.78 -1 -13 -5 70.51 14.71 11 9 2 3.64 2.07 11 -9 2 6.98 7.11 11 -9 2 6.83 2.73 -11 9 -2 2.16 4.15 11 9 2 2.51 2.74 7 -13 -3 421.58 23.71 7 -13 -3 401.06 23.39 -7 -13 3 453.29 25.18 7 13 -3 399.36 21.68 -7 13 3 328.17 25.31 -7 -13 3 428.05 23.06 6 13 1 14.07 6.26 -6 -13 -1 18.82 6.08 6 -13 1 18.59 8.81 -6 -13 -1 19.76 8.66 -6 13 -1 13.11 8.21 6 -13 1 18.40 3.98 -10 11 0 703.43 38.69 -10 -11 0 628.23 32.07 10 -11 0 576.85 32.77 -10 -11 0 611.67 30.50 10 -11 0 571.20 30.58 10 11 0 620.36 32.30 -11 -5 12 5.08 5.05 -11 -5 12 -0.01 5.45 -11 5 12 3.22 5.59 11 -5 -12 1.65 2.77 -11 5 12 6.10 6.30 11 7 4 30.44 7.93 -11 -7 -4 41.21 9.31 11 -7 4 36.22 3.75 11 -7 4 31.91 5.60 -11 7 -4 43.45 8.88 11 -7 4 32.94 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8.87 -2 -14 3 50.27 6.75 -2 14 3 49.04 9.82 2 14 -3 51.52 9.07 7 -7 -12 4.22 6.98 -7 -7 12 6.69 6.20 7 -7 -12 4.07 4.20 -7 -7 12 4.94 3.27 -7 7 12 3.06 2.98 -13 8 8 4.99 8.33 -13 -8 8 6.82 3.47 -13 8 8 17.05 12.38 13 -8 -8 8.25 4.60 -13 -8 8 11.67 7.11 -13 -8 8 5.60 2.31 -3 -13 -4 270.65 17.17 3 -13 4 264.73 18.40 3 -13 4 268.32 25.74 -3 13 -4 282.71 24.74 3 13 4 259.96 20.17 -3 -13 -4 259.72 18.75 7 13 -1 3.18 4.69 -7 13 1 4.77 8.71 -7 -13 1 5.11 6.05 7 -13 -1 3.73 3.92 7 -13 -1 1.43 5.23 -7 -13 1 4.07 6.08 0 -5 -12 179.77 8.89 0 -5 12 184.16 10.02 0 5 12 198.03 20.50 0 5 -12 178.14 15.06 0 -5 -12 179.22 7.63 0 -5 12 169.13 11.43 0 -5 -12 187.02 13.92 0 5 -12 186.54 7.38 -11 8 10 2.26 6.73 11 -8 -10 -1.06 4.64 -11 8 10 -0.88 5.77 -11 -8 10 2.41 3.27 -11 -8 10 1.87 4.90 12 -10 -5 5.09 5.94 -12 10 5 -0.47 3.96 -12 10 5 -1.19 7.85 -12 -10 5 4.93 5.64 -12 -10 5 1.98 2.11 -12 -10 5 2.53 1.86 -13 -2 12 140.36 26.68 13 2 -12 131.59 18.37 13 -2 -12 121.33 26.91 -13 -2 12 118.41 10.11 -13 2 12 113.78 9.09 13 2 -12 112.82 4.45 -13 2 12 128.25 13.42 6 -11 5 80.44 21.30 -6 -11 -5 61.09 4.66 6 11 5 80.48 10.62 -6 11 -5 66.43 10.63 6 -11 5 65.29 3.30 -6 -11 -5 80.43 11.21 14 8 -5 38.26 9.30 -14 8 5 36.16 12.88 14 -8 -5 22.95 7.43 -14 -8 5 49.69 17.89 -14 8 5 33.25 7.35 -14 -8 5 37.48 6.54 4 -7 -12 98.41 9.27 -4 -7 12 90.70 14.98 4 -7 -12 62.06 26.90 -4 -7 12 82.12 8.66 4 7 -12 73.66 8.00 -4 7 12 91.80 17.47 4 7 -12 86.09 4.34 -16 -4 7 173.03 22.86 -16 4 7 198.31 14.65 -16 -4 7 155.31 9.82 16 4 -7 171.17 15.28 -16 4 7 173.22 17.43 16 -4 -7 204.10 21.46 -12 -4 12 7.68 14.06 -12 4 12 29.33 7.83 -12 4 12 27.67 8.38 12 -4 -12 10.78 5.86 12 4 -12 31.76 9.98 -4 6 -10 55.99 17.79 4 6 10 53.76 21.36 -4 -6 -10 56.89 10.81 4 -6 10 41.32 16.56 -13 8 0 13.19 9.22 13 -8 0 26.65 9.93 -13 -8 0 23.34 8.34 -13 8 0 21.15 4.55 -13 -8 0 27.56 5.85 13 8 0 26.71 7.98 -9 -12 1 26.78 6.53 9 12 -1 19.85 11.21 -9 12 1 21.48 13.39 -9 -12 1 17.13 9.79 9 -12 -1 22.25 9.73 9 -12 -1 32.37 6.71 -14 -3 11 3.82 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1.21 5 10 -10 1.51 1.70 -5 -10 10 3.82 4.59 -5 10 10 -1.38 8.22 5 -10 -10 -0.61 6.76 5 -10 -10 5.07 2.72 -10 -6 12 3.26 2.75 -10 -6 12 5.60 5.86 -10 6 12 6.15 6.69 -10 6 12 3.86 4.63 10 -6 -12 10.91 6.67 -7 -5 13 17.28 13.57 -7 5 13 14.98 5.70 -7 -5 13 20.74 5.17 -7 5 13 16.41 12.18 7 -5 -13 23.17 7.12 7 5 -13 15.12 5.75 7 5 -13 20.23 5.74 -5 -5 13 14.78 7.19 5 -5 -13 20.24 8.13 5 -5 -13 18.18 14.16 -5 5 13 20.64 6.42 -5 -5 13 13.86 5.67 5 5 -13 16.53 6.63 5 5 -13 9.65 4.73 -13 9 6 38.31 8.89 13 -9 -6 33.51 8.87 -13 9 6 21.97 10.20 -13 -9 6 31.18 10.81 -13 -9 6 46.78 4.09 -4 -10 10 279.58 29.16 -4 -10 10 289.52 18.59 -4 -10 10 283.88 16.65 4 10 -10 293.07 18.04 4 -10 -10 326.56 19.91 4 -10 -10 324.47 23.57 -4 10 10 337.88 26.13 14 -4 2 188.09 14.22 -14 -4 -2 217.95 11.74 -14 4 -2 242.55 8.29 -14 -4 -2 223.55 14.10 -14 4 -2 278.05 20.15 14 4 2 286.13 17.85 -12 9 8 1.23 5.21 -12 -9 8 9.99 5.37 -12 -9 8 3.03 1.20 12 -9 -8 4.62 5.31 -12 -9 8 6.62 5.24 -12 9 8 2.68 3.51 -8 7 -7 4.98 7.19 8 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-11 -8 23.28 8.43 1 -11 8 12.98 7.34 -1 -11 -8 19.29 8.03 1 -11 8 21.11 4.55 1 11 8 16.42 10.03 1 11 8 19.97 3.54 -1 11 -8 18.85 7.30 1 6 -12 5.01 3.09 -1 6 12 5.86 8.37 1 -6 -12 4.48 2.35 1 -6 -12 7.29 3.49 -1 -6 12 13.38 4.97 1 -6 -12 10.90 6.91 -1 -6 12 1.31 5.53 -12 -3 -5 48.81 8.35 -12 3 -5 33.69 5.02 -12 -3 -5 31.60 6.88 12 3 5 42.37 8.03 12 -3 5 42.90 15.58 12 -3 5 35.11 6.23 -12 3 -5 29.31 15.53 7 -13 -4 298.01 23.26 -7 -13 4 279.72 21.94 7 -13 -4 318.69 26.64 -7 13 4 260.57 35.66 -7 -13 4 289.10 19.56 7 13 -4 284.16 18.91 11 -11 -3 39.72 8.33 11 -11 -3 45.05 19.29 -11 11 3 48.53 23.68 -11 -11 3 42.66 16.50 -11 -11 3 59.92 22.33 11 11 -3 48.86 17.22 -9 12 5 2.16 3.56 9 12 -5 0.72 3.05 9 -12 -5 -1.83 4.75 -9 -12 5 -1.34 5.03 9 -12 -5 1.58 3.20 -9 -12 5 4.28 8.70 2 6 11 149.50 15.78 2 -6 11 126.79 10.69 -2 6 -11 111.26 20.62 -2 6 -11 121.71 2.31 -2 -6 -11 127.11 10.10 16 -2 -1 -0.32 2.97 -16 2 1 1.81 5.65 16 2 -1 1.47 3.27 -16 -2 1 2.84 3.47 -16 2 1 1.55 2.71 -16 -2 1 1.51 3.24 2 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12.15 6.78 0 6 -12 13.05 5.65 -4 -14 4 3.39 3.67 -4 14 4 0.96 7.56 4 14 -4 3.58 2.94 -4 -14 4 7.49 8.63 4 -14 -4 3.98 4.25 4 -14 -4 5.03 5.12 -14 -5 -2 14.06 15.30 -14 5 -2 17.96 5.70 -14 -5 -2 24.80 14.95 -14 5 -2 24.20 8.18 14 5 2 16.21 6.15 14 -5 2 15.13 4.71 7 -5 9 76.84 7.88 -7 5 -9 55.96 23.62 -7 -5 -9 51.56 8.25 -7 -5 -9 53.34 17.25 8 2 -14 242.99 17.41 -8 2 14 204.49 22.35 -8 -2 14 228.67 13.44 -8 2 14 218.87 12.38 -8 -2 14 227.35 12.23 8 -2 -14 229.13 13.52 13 -8 -9 117.96 11.92 -13 -8 9 133.81 17.36 -13 -8 9 122.21 11.57 -13 8 9 98.10 13.44 -13 8 9 146.96 11.01 10 -12 -4 101.08 10.25 10 -12 -4 111.48 15.08 -10 12 4 116.42 16.99 10 12 -4 108.48 20.16 -10 -12 4 111.95 12.01 -10 -12 4 121.04 9.28 -2 -11 -8 44.53 6.15 2 11 8 48.96 29.21 -2 11 -8 42.69 8.33 2 -11 8 48.81 12.23 2 -11 8 40.56 5.97 -2 -11 -8 35.06 9.87 -4 1 14 58.80 25.87 4 -1 -14 65.85 9.67 -4 -1 14 56.09 6.66 -4 -1 14 56.11 16.47 -4 1 14 58.17 19.10 4 1 -14 72.57 8.71 -8 -10 10 4.72 5.20 -8 -10 10 8.73 11.34 -8 10 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6.32 9 -12 2 -1.29 5.70 -9 12 -2 6.87 5.63 9 -12 2 0.83 1.33 9 12 2 9.60 7.10 4 10 -11 77.96 5.48 -4 -10 11 68.91 10.34 -4 -10 11 54.06 29.04 -4 10 11 79.22 43.92 4 -10 -11 67.83 8.78 4 -10 -11 82.76 13.70 7 14 -2 908.07 31.61 -7 -14 2 953.54 32.00 -7 14 2 866.28 40.46 -7 -14 2 914.77 30.97 7 -14 -2 869.98 30.09 7 -14 -2 853.05 43.33 3 -15 -1 3.56 6.18 3 -15 -1 10.00 7.27 -3 -15 1 3.73 3.57 3 15 -1 0.90 2.73 -3 15 1 -1.94 7.21 -3 -15 1 3.12 3.94 -9 13 1 63.98 35.81 9 -13 -1 47.26 15.44 9 -13 -1 59.58 23.10 -9 -13 1 69.82 14.45 -9 -13 1 52.47 7.09 9 13 -1 57.69 11.04 1 -12 8 -0.39 6.58 -1 12 -8 6.19 3.89 1 -12 8 0.14 0.67 -1 -12 -8 6.59 6.24 -1 -12 -8 1.24 1.50 1 12 8 0.27 4.45 14 4 -12 1.10 5.23 -14 4 12 3.82 3.22 -14 4 12 -0.62 5.21 -14 -4 12 3.93 6.65 -14 -4 12 0.52 1.18 14 -4 -12 4.02 5.36 14 -9 -7 200.23 26.65 -14 9 7 226.53 19.13 -14 9 7 255.72 42.86 -14 -9 7 197.32 20.49 -14 -9 7 175.74 6.04 14 9 -7 186.75 25.79 12 -11 -6 243.86 14.52 -12 11 6 212.10 17.48 12 -11 -6 228.81 34.56 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183.31 15.31 -16 -7 7 236.52 11.33 -16 7 7 230.59 16.11 12 -7 -12 104.87 10.57 -12 7 12 102.34 12.06 -12 7 12 110.36 27.73 -12 -7 12 113.96 17.22 -12 -7 12 122.57 17.10 5 13 -8 1022.22 30.80 -5 -13 8 1167.66 35.47 -5 -13 8 1047.10 48.56 5 -13 -8 1168.14 39.38 -5 13 8 914.96 36.02 5 -13 -8 1073.66 37.97 13 -4 -13 16.53 8.31 -13 4 13 11.25 5.08 -13 4 13 3.62 5.76 -13 -4 13 4.07 5.07 13 4 -13 5.79 4.97 -1 15 -3 23.21 9.41 1 -15 3 20.10 11.92 -1 -15 -3 22.62 7.46 1 -15 3 26.49 10.46 1 15 3 33.85 18.46 -1 -15 -3 27.08 7.88 1 4 13 17.00 11.65 -1 -4 -13 7.54 6.12 -1 4 -13 13.97 4.99 1 -4 13 20.54 9.30 -1 -4 -13 16.23 6.26 -1 4 -13 11.87 7.66 -14 9 8 234.85 15.06 -14 9 8 206.62 21.19 14 -9 -8 208.39 17.12 -14 -9 8 218.32 14.44 14 9 -8 215.43 15.81 -14 -9 8 196.32 5.69 -11 4 -7 15.82 6.07 -11 4 -7 15.37 3.74 -11 -4 -7 16.93 8.82 11 -4 7 6.07 9.03 -15 -3 12 20.27 8.53 -15 3 12 25.65 12.49 -15 3 12 23.36 13.44 -15 -3 12 44.35 9.04 15 -3 -12 29.45 8.68 15 3 -12 37.71 10.30 1 12 -9 20.31 10.34 -1 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208.57 15.02 14 -10 -5 213.48 15.03 -14 -10 5 192.02 7.24 14 10 -5 239.44 15.33 -14 -10 5 241.21 14.56 -2 15 4 8.64 7.75 2 -15 -4 27.29 8.75 -2 -15 4 3.60 4.46 2 15 -4 8.87 5.72 -2 -15 4 6.07 8.08 2 -15 -4 7.32 4.41 3 15 2 172.46 37.52 -3 15 -2 174.42 14.40 -3 -15 -2 148.39 11.84 3 -15 2 173.14 8.16 -3 -15 -2 153.21 12.50 3 -15 2 158.46 11.51 9 3 9 128.86 3.90 -9 -3 -9 124.77 6.71 -9 3 -9 118.69 15.61 -9 -3 -9 142.86 10.74 -9 3 -9 131.02 2.65 9 -3 9 145.73 8.72 10 -13 -4 34.97 13.87 10 -13 -4 34.40 14.00 -10 13 4 50.01 24.11 -10 -13 4 41.97 6.46 -10 -13 4 39.74 24.48 10 13 -4 44.17 7.03 -12 11 0 207.88 37.46 12 -11 0 185.78 22.68 12 -11 0 210.33 11.60 -12 -11 0 188.02 10.69 12 11 0 204.36 11.50 12 11 0 188.26 27.98 -17 -4 9 0.58 3.75 17 -4 -9 3.01 3.90 17 4 -9 9.59 7.37 -17 4 9 1.53 5.95 -17 -4 9 1.20 2.74 -17 4 9 1.18 5.71 -6 -13 8 56.89 21.18 6 13 -8 58.63 13.26 -6 -13 8 54.61 28.83 -6 13 8 74.57 13.60 6 -13 -8 68.94 11.96 6 -13 -8 66.26 10.32 -18 0 3 0.92 3.10 -18 0 3 0.58 3.50 18 0 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34.52 10.70 4 -15 1 32.10 12.05 -12 -8 -4 7.56 4.06 -12 8 -4 8.42 8.33 12 -8 4 2.12 1.72 12 -8 4 7.37 9.47 12 8 4 6.51 3.65 -12 -8 -4 9.95 9.57 6 3 11 160.46 3.98 -6 -3 -11 189.38 15.40 -6 3 -11 165.54 16.40 -6 -3 -11 152.63 10.11 6 -3 11 157.72 9.55 9 -8 7 76.66 12.51 9 8 7 91.03 43.68 -9 -8 -7 104.78 9.39 -9 8 -7 92.78 10.35 8 -12 4 12.76 8.88 8 -12 4 17.10 5.06 -8 -12 -4 7.70 3.69 8 12 4 20.41 9.24 -8 12 -4 10.98 7.41 -8 -12 -4 13.88 9.75 8 1 10 0.40 1.18 8 -1 10 4.12 3.80 -8 -1 -10 10.16 7.22 -8 1 -10 -1.29 5.07 -8 1 -10 2.30 2.16 -8 -1 -10 2.54 2.73 13 -11 -4 23.74 10.46 -13 11 4 11.98 8.66 13 -11 -4 16.48 11.29 -13 -11 4 30.60 16.63 -13 -11 4 24.31 8.44 -13 -11 4 10.94 7.84 10 -4 8 39.06 5.25 -10 4 -8 54.27 6.58 -10 -4 -8 63.65 22.42 -10 -4 -8 55.69 9.35 10 4 8 61.15 2.71 15 5 2 84.91 5.93 15 -5 2 79.98 11.99 -15 -5 -2 93.31 13.17 -15 5 -2 78.53 9.84 -15 -5 -2 78.00 14.85 -15 5 -2 71.62 10.07 -6 0 15 2.61 3.24 -6 0 15 2.79 4.53 6 0 -15 3.70 4.95 -5 -15 2 24.19 12.15 5 15 -2 25.66 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216.18 24.46 8 0 -15 1.88 4.28 -8 0 15 6.31 5.92 -8 0 15 0.06 1.86 -7 1 15 93.31 7.72 -7 1 15 91.93 12.55 -7 -1 15 92.81 6.40 -7 -1 15 89.35 17.15 7 -1 -15 87.90 9.46 7 1 -15 100.89 10.77 6 -14 -6 45.68 7.78 -6 14 6 46.07 12.28 6 -14 -6 55.28 9.54 -6 -14 6 40.16 24.62 6 14 -6 57.38 12.93 -6 -14 6 41.52 16.36 -18 3 5 1.66 5.41 18 -3 -5 0.38 5.80 18 3 -5 5.01 4.58 -18 -3 5 5.33 4.01 -18 -3 5 4.17 4.92 -18 3 5 3.92 6.27 17 0 0 21.33 11.10 -17 0 0 32.89 6.27 -17 0 0 31.38 8.73 -8 -12 9 69.03 25.78 -8 -12 9 58.59 10.57 8 -12 -9 55.81 7.72 -8 12 9 78.49 12.80 8 -12 -9 52.93 10.33 -15 9 5 230.32 41.38 15 -9 -5 268.70 19.35 -15 9 5 241.23 22.62 -15 -9 5 310.06 16.79 -15 -9 5 273.65 19.79 15 9 -5 281.87 21.53 -14 10 3 12.09 10.47 14 -10 -3 3.56 4.59 -14 10 3 1.93 2.59 14 10 -3 3.72 4.28 -14 -10 3 4.57 4.84 -14 -10 3 1.48 2.38 7 -14 1 16.51 11.17 7 14 1 7.12 5.12 -7 14 -1 19.67 8.28 -7 -14 -1 22.39 9.37 7 -14 1 8.12 4.11 -7 -14 -1 12.08 6.81 7 -12 5 57.47 6.79 -7 -12 -5 62.92 3.24 -7 -12 -5 70.53 11.14 -7 12 -5 67.60 35.58 7 -12 5 61.16 11.29 7 12 5 66.15 10.02 1 13 -8 314.46 20.16 -1 -13 8 294.09 16.58 -1 -13 8 275.56 19.89 -1 13 8 289.23 55.96 1 -13 -8 303.15 16.78 1 -13 -8 290.35 20.63 2 -4 -14 126.74 15.32 -2 -4 14 119.67 9.20 -2 -4 14 126.60 9.18 2 -4 -14 115.88 12.39 2 4 -14 120.43 9.20 -2 4 14 116.96 9.70 15 -9 -4 88.37 12.16 -15 9 4 117.31 37.02 -15 9 4 83.32 8.27 15 9 -4 89.99 9.10 -15 -9 4 112.50 21.78 -15 -9 4 82.63 5.98 -6 1 15 77.69 11.54 -6 -1 15 90.67 9.49 -6 1 15 68.25 28.36 6 -1 -15 60.97 19.49 6 1 -15 93.45 11.81 -6 -1 15 73.78 7.75 -13 11 5 147.88 13.42 -13 11 5 118.21 29.46 13 -11 -5 128.69 14.18 -13 -11 5 162.80 24.79 -13 -11 5 130.17 7.81 -13 -11 5 146.18 16.30 2 15 3 11.19 7.93 -2 -15 -3 6.18 5.89 2 -15 3 2.38 7.06 -2 -15 -3 15.10 8.89 2 -15 3 7.70 3.78 -2 15 -3 6.91 5.65 -11 -8 12 284.02 18.70 -11 8 12 287.18 20.72 -11 -8 12 290.56 21.74 11 -8 -12 288.87 32.72 -11 8 12 308.03 44.02 -1 -10 11 514.34 24.59 -1 -10 11 550.65 17.80 1 10 -11 567.96 20.38 1 -10 -11 512.00 16.93 1 -10 -11 583.23 23.62 -1 10 11 528.65 25.90 -13 11 3 275.66 20.89 13 -11 -3 274.94 17.61 13 -11 -3 257.79 15.27 -13 -11 3 238.54 12.05 -13 -11 3 336.37 20.23 13 11 -3 281.75 17.82 8 1 -15 7.52 4.59 -8 1 15 2.25 4.15 -8 -1 15 4.28 3.18 -8 1 15 11.29 5.89 -8 -1 15 11.36 6.13 8 -1 -15 7.99 4.56 -11 4 14 319.56 20.39 11 4 -14 335.67 23.33 11 -4 -14 380.59 35.86 -11 4 14 364.52 23.60 -11 -4 14 349.92 21.43 9 12 3 138.63 11.53 -9 12 -3 141.09 17.37 -9 -12 -3 160.72 18.26 9 -12 3 143.51 6.36 9 -12 3 148.82 12.10 -10 7 13 3.50 6.26 -10 -7 13 7.71 5.52 -10 7 13 0.10 6.03 -10 -7 13 2.89 2.03 10 -7 -13 0.40 1.95 -2 -7 13 4.12 6.31 2 -7 -13 15.49 8.11 -2 -7 13 0.90 3.24 2 -7 -13 2.49 2.40 -2 7 13 8.57 9.02 2 7 -13 2.30 3.92 -2 10 -10 67.88 7.65 2 -10 10 55.43 3.21 2 -10 10 67.14 25.27 -2 -10 -10 57.86 8.57 2 10 10 61.18 20.42 -17 1 0 2.71 3.21 -17 -1 0 4.16 7.06 -17 1 0 14.08 9.92 -17 -1 0 -0.19 3.20 17 -1 0 8.26 5.85 17 1 0 7.04 5.24 2 13 7 14.27 10.01 -2 13 -7 11.26 4.58 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181.50 12.19 -14 3 -5 52.20 11.19 -14 -3 -5 42.30 4.13 14 -3 5 35.84 16.99 14 3 5 40.03 12.29 -14 3 -5 47.17 9.48 -14 -3 -5 47.04 12.70 -1 -16 2 2.00 5.85 1 -16 -2 7.63 4.98 -1 -16 2 5.64 6.02 -1 16 2 11.91 15.35 1 16 -2 13.97 7.00 1 -16 -2 6.49 9.79 10 2 9 1.05 1.09 -10 -2 -9 1.43 2.57 -10 2 -9 1.67 1.36 -10 -2 -9 0.17 3.60 -10 2 -9 -3.34 5.28 10 -2 9 3.93 3.28 -8 -10 12 38.49 9.10 -8 -10 12 38.94 17.27 8 -10 -12 33.57 15.89 8 -10 -12 45.90 10.19 -8 10 12 41.55 25.06 -15 9 1 90.46 14.43 15 -9 -1 81.49 21.25 -15 9 1 101.65 28.48 -15 -9 1 108.69 9.90 15 9 -1 111.52 13.41 -15 -9 1 85.68 15.12 7 -15 -2 28.91 13.98 7 -15 -2 27.58 13.60 -7 -15 2 7.93 11.10 -7 -15 2 29.82 14.27 -7 15 2 27.75 12.68 7 15 -2 40.91 8.90 10 -13 -7 127.64 15.68 10 -13 -7 100.03 24.75 -10 13 7 117.45 51.64 10 13 -7 129.63 6.05 -10 -13 7 112.88 19.31 -10 -13 7 143.65 12.22 -9 -12 -4 16.58 6.89 -9 12 -4 17.49 8.55 9 -12 4 20.08 5.45 9 -12 4 12.72 9.33 9 12 4 21.59 5.47 9 12 4 17.44 7.30 6 7 -14 111.26 4.33 -6 -7 14 124.53 12.04 -6 -7 14 110.32 7.60 6 -7 -14 131.37 20.66 6 -7 -14 122.56 10.19 -6 7 14 126.31 10.59 -18 0 1 1.48 2.79 -18 0 1 4.13 5.27 18 0 -1 2.43 2.93 -7 -7 14 4.66 9.44 -7 -7 14 2.09 3.19 -7 7 14 -2.83 5.14 7 -7 -14 12.69 6.84 7 -7 -14 5.52 4.04 -11 2 15 21.17 9.27 -11 -2 15 26.91 6.99 11 -2 -15 31.00 7.95 11 2 -15 33.41 9.81 -11 -2 15 16.67 6.31 -11 2 15 12.33 3.63 -8 12 -5 231.21 14.06 8 12 5 254.17 20.94 8 -12 5 208.52 5.24 -8 -12 -5 263.26 18.78 8 -12 5 238.72 17.09 8 12 5 225.90 5.17 13 6 5 112.09 4.29 13 -6 5 98.15 16.50 -13 -6 -5 134.65 11.14 -13 -6 -5 125.20 13.50 -13 6 -5 114.02 12.11 -15 2 -4 2.51 1.71 -15 -2 -4 5.23 4.40 -15 -2 -4 4.33 3.04 15 -2 4 6.36 5.26 15 2 4 4.91 4.42 -15 2 -4 13.55 9.33 -3 -10 12 659.71 33.39 -3 -10 12 633.12 27.88 3 10 -12 634.26 30.66 3 -10 -12 617.42 26.38 3 -10 -12 588.89 30.19 -3 10 12 680.76 36.42 -9 14 5 126.09 31.75 9 -14 -5 131.53 10.94 9 -14 -5 121.03 10.93 -9 -14 5 122.37 9.81 -9 -14 5 110.86 18.28 9 14 -5 123.40 7.56 16 -8 -8 91.20 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1.76 -15 -8 -1 -0.67 3.49 -15 -8 -1 2.15 4.66 -5 -9 -10 18.53 8.88 5 9 10 29.12 8.41 -5 9 -10 27.30 7.03 5 -9 10 19.24 5.72 -6 8 -10 306.57 19.78 -6 -8 -10 327.91 31.20 6 8 10 320.52 22.98 6 -8 10 293.36 24.40 -17 1 12 10.77 5.76 -17 -1 12 9.63 6.27 17 -1 -12 6.14 4.42 -17 1 12 8.66 8.68 17 1 -12 2.78 6.03 -17 -1 12 6.27 6.88 2 -2 -15 110.78 18.13 -2 2 15 106.25 9.77 -2 -2 15 101.12 8.83 2 2 -15 112.84 20.79 2 2 -15 119.81 11.71 2 -2 -15 136.90 10.66 -16 6 11 4.56 6.07 16 -6 -11 0.79 4.91 16 6 -11 9.27 7.77 -16 6 11 2.47 5.82 -16 -6 11 -0.06 0.75 -16 -6 11 2.74 5.11 13 -10 -10 328.44 21.96 -13 10 10 327.24 41.93 -13 10 10 318.40 29.13 -13 -10 10 330.87 21.58 -13 -10 10 315.41 25.24 -8 -5 -10 62.34 29.46 -8 -5 -10 52.92 15.87 8 -5 10 84.15 8.87 -8 5 -10 48.36 8.84 -11 -4 -8 36.69 7.72 -11 -4 -8 37.46 8.24 -11 4 -8 35.56 13.85 11 -4 8 44.06 10.36 -13 -8 -4 10.23 5.73 -13 8 -4 20.42 10.25 13 8 4 20.48 6.78 13 -8 4 14.88 8.72 13 -8 4 17.44 5.45 -13 -8 -4 19.19 10.50 -15 7 -2 106.84 5.98 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13.93 -2 15 -5 78.46 8.91 2 -15 5 71.82 5.88 -2 -15 -5 62.00 9.27 -4 16 1 -2.91 8.29 -4 -16 1 9.66 5.25 4 -16 -1 1.96 2.23 -4 -16 1 4.10 3.35 4 -16 -1 6.33 6.59 4 16 -1 4.77 4.87 17 6 -1 8.11 6.67 -17 6 1 0.95 4.44 -17 -6 1 5.75 4.69 -17 -6 1 6.58 6.05 17 -6 -1 6.23 6.63 -17 6 1 2.16 6.83 13 -10 2 13.86 4.68 13 -10 2 16.49 11.63 -13 10 -2 13.24 9.01 -13 -10 -2 7.72 11.95 -13 -10 -2 10.28 7.72 13 10 2 4.75 6.17 -18 -3 10 72.59 31.21 18 -3 -10 62.43 10.64 18 3 -10 49.78 21.80 -18 3 10 34.69 25.08 -18 -3 10 43.97 16.06 -18 3 10 68.62 26.38 3 -16 -3 129.70 10.50 3 -16 -3 102.71 13.32 -3 -16 3 117.54 9.09 -3 16 3 80.66 12.77 3 16 -3 96.10 21.06 -3 -16 3 122.99 18.18 8 14 -7 2.42 2.26 -8 -14 7 5.83 4.76 -8 -14 7 3.26 5.31 8 -14 -7 5.38 4.77 -8 14 7 2.37 7.72 8 -14 -7 2.59 6.55 5 -15 -6 4.07 8.46 5 15 -6 2.53 1.75 -5 -15 6 2.55 3.14 -5 -15 6 1.95 4.38 5 -15 -6 -0.63 4.35 -5 15 6 3.79 8.50 -5 -14 -5 432.20 23.01 5 -14 5 408.18 18.42 -5 14 -5 418.31 31.55 5 14 5 435.78 28.32 5 -14 5 395.16 34.97 -5 -14 -5 360.31 21.97 -9 -12 10 81.65 35.17 -9 -12 10 75.60 7.28 -9 12 10 60.01 13.91 9 -12 -10 88.08 8.53 9 -12 -10 85.87 12.09 -4 -6 -12 4.73 6.04 4 -6 12 6.95 5.25 4 6 12 7.40 6.30 -4 6 -12 2.46 3.52 -8 13 -4 81.11 16.52 8 -13 4 78.40 21.70 -8 -13 -4 85.94 10.48 8 -13 4 91.99 4.79 -8 -13 -4 105.64 11.57 8 13 4 95.17 14.74 14 -3 -14 73.52 26.78 -14 -3 14 68.23 5.40 -14 -3 14 65.67 12.72 14 3 -14 74.44 15.63 -14 3 14 79.41 9.03 -14 3 14 65.02 9.74 9 -2 10 1.37 2.74 9 2 10 0.50 0.79 -9 -2 -10 2.70 0.95 -9 2 -10 0.36 0.78 -9 -2 -10 3.08 5.96 -9 2 -10 3.55 3.33 -11 12 -2 4.29 8.07 11 -12 2 4.02 4.45 11 -12 2 8.01 8.07 -11 -12 -2 2.98 5.85 11 12 2 5.48 2.52 11 12 2 8.62 4.02 -12 2 15 22.99 6.66 -12 2 15 29.64 9.09 12 2 -15 14.46 8.47 12 -2 -15 17.80 17.30 -12 -2 15 30.30 11.02 -12 -2 15 27.02 7.00 -4 -16 2 21.20 6.91 -4 -16 2 19.84 9.02 4 -16 -2 13.19 8.20 4 16 -2 19.36 13.68 -4 16 2 32.88 16.37 4 -16 -2 30.44 15.49 -6 5 15 272.44 20.42 6 5 -15 279.41 15.78 6 -5 -15 273.93 17.53 -6 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20.49 0 -12 -10 330.99 18.32 0 12 10 266.57 20.69 10 -14 -2 3.62 6.00 -10 14 2 8.56 9.75 10 -14 -2 -4.84 5.97 10 14 -2 4.70 2.62 -10 -14 2 4.77 4.30 -10 -14 2 4.79 4.63 -19 3 6 7.46 4.00 19 -3 -6 15.67 8.42 -19 3 6 5.81 5.12 -19 -3 6 2.07 2.47 19 3 -6 -3.41 4.20 -19 -3 6 7.22 7.12 6 -6 11 67.76 9.09 -6 -6 -11 58.77 19.50 -6 6 -11 75.60 14.57 6 6 11 58.05 28.13 -17 -2 12 230.21 14.03 -17 2 12 159.11 11.37 -17 -2 12 213.16 9.99 -17 2 12 201.54 35.07 17 -2 -12 198.04 23.58 17 2 -12 239.81 36.98 0 -15 -6 248.07 16.17 0 15 -6 260.27 18.37 0 -15 6 248.03 14.98 0 15 6 286.78 24.52 0 -15 -6 275.82 20.57 0 -15 6 260.09 36.03 -3 -7 14 79.95 14.12 -3 -7 14 64.07 6.26 3 7 -14 80.22 15.74 -3 7 14 69.27 30.67 3 -7 -14 70.16 8.18 3 -7 -14 85.60 12.28 -18 6 6 2.93 4.48 18 6 -6 3.05 3.03 18 -6 -6 3.25 5.93 -18 -6 6 1.18 3.32 -18 -6 6 10.29 7.11 -18 6 6 7.22 6.22 -4 10 -10 54.96 8.02 4 -10 10 54.81 10.23 -4 -10 -10 56.16 8.79 4 10 10 69.63 10.89 -16 -2 13 77.69 7.11 -16 -2 13 74.60 13.66 -16 2 13 78.97 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196.66 25.80 8 15 0 216.90 27.43 -8 -15 0 205.02 11.84 -8 -15 0 218.41 10.59 -5 13 -7 383.54 40.10 5 13 7 466.98 27.66 5 -13 7 409.69 24.83 -5 -13 -7 381.01 54.86 3 13 -10 1.32 2.49 -3 -13 10 2.34 3.61 -3 -13 10 2.93 4.78 3 -13 -10 0.66 4.46 3 -13 -10 3.02 2.31 -3 13 10 5.89 6.17 -5 11 -9 78.42 17.13 5 -11 9 90.32 11.16 5 11 9 63.61 29.74 -5 -11 -9 77.66 24.66 9 10 7 25.67 17.57 -9 10 -7 28.60 9.53 9 -10 7 15.23 9.48 -9 -10 -7 16.41 6.51 2 -4 -15 14.39 6.66 -2 -4 15 3.71 5.91 2 4 -15 8.29 5.02 2 -4 -15 11.43 4.01 -2 -4 15 13.43 6.36 -2 4 15 6.51 5.47 13 -2 7 114.48 8.28 -13 2 -7 118.69 5.03 -13 2 -7 96.90 10.43 -13 -2 -7 116.93 11.26 -13 -2 -7 112.64 6.69 13 2 7 143.20 7.02 -2 -15 7 22.19 8.58 -2 -15 7 34.08 12.06 2 15 -7 28.06 15.22 2 -15 -7 37.18 13.83 2 -15 -7 46.23 10.41 -2 15 7 34.98 13.28 9 1 -16 3.81 5.30 9 -1 -16 1.75 6.93 -9 -1 16 10.36 7.93 -9 1 16 0.03 2.22 -9 -1 16 1.82 3.81 -9 1 16 1.78 3.66 -7 -14 -4 118.28 6.05 7 14 4 138.63 14.61 7 -14 4 111.23 15.97 -7 14 -4 105.18 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-2.20 5.93 10 -12 4 140.40 12.43 10 -12 4 191.05 4.96 -10 12 -4 213.78 30.51 10 12 4 189.93 5.55 -10 -12 -4 141.84 28.05 10 12 4 198.28 28.48 15 0 5 0.68 2.12 -15 0 -5 -1.38 2.20 -15 0 -5 3.28 5.70 12 -13 -6 29.45 8.87 12 -13 -6 24.83 8.33 -12 13 6 39.78 20.17 -12 -13 6 19.74 7.35 -12 -13 6 23.52 9.93 -12 -13 6 28.21 10.31 -15 7 12 219.92 28.18 -15 -7 12 196.42 11.97 15 -7 -12 184.29 14.10 15 7 -12 200.94 19.41 -15 7 12 201.48 23.82 15 -9 -10 82.71 9.61 -15 9 10 88.19 36.52 -15 9 10 83.94 31.46 15 9 -10 84.79 14.17 -15 -9 10 81.05 9.51 -11 -9 -6 7.86 6.44 11 -9 6 33.43 12.71 -11 9 -6 22.48 11.03 -11 -9 -6 11.60 6.69 17 6 0 275.95 17.66 -17 6 0 233.67 16.26 -17 -6 0 299.79 19.66 -17 6 0 220.83 9.63 -17 -6 0 251.32 17.47 17 -6 0 234.55 11.64 -19 0 2 484.41 24.65 19 0 -2 410.34 27.18 -19 0 2 460.30 24.67 16 -8 0 123.18 10.94 -16 8 0 136.84 19.28 -16 8 0 126.39 13.41 16 8 0 112.51 7.61 -16 -8 0 119.58 19.81 -16 -8 0 109.50 15.34 8 14 3 141.85 14.01 8 -14 3 151.79 20.46 -8 -14 -3 145.57 6.60 8 -14 3 146.70 6.94 -8 -14 -3 133.44 25.72 -8 14 -3 131.99 14.49 -14 2 -6 352.95 32.85 -14 -2 -6 450.31 24.54 -14 2 -6 432.20 20.32 14 2 6 474.81 21.54 14 -2 6 473.07 22.90 -14 -2 -6 440.47 23.82 16 7 -11 59.55 21.56 -16 7 11 70.30 15.68 -16 7 11 63.44 15.70 -16 -7 11 54.29 20.74 16 -7 -11 53.06 12.67 -1 -16 -4 19.02 11.74 1 -16 4 31.78 10.69 -1 -16 -4 16.68 16.23 1 -16 4 18.42 8.16 -1 16 -4 25.71 10.29 1 16 4 18.47 11.71 -7 -2 16 41.04 11.71 -7 2 16 45.14 21.42 7 2 -16 51.72 8.92 7 2 -16 42.67 6.83 7 -2 -16 30.00 6.04 -7 2 16 39.86 22.44 5 8 11 64.69 30.89 -5 8 -11 55.52 9.78 -5 -8 -11 35.52 9.86 5 -8 11 34.91 7.69 -9 4 -10 19.55 17.16 9 -4 10 6.57 5.26 -9 -4 -10 8.38 6.58 -9 -4 -10 20.45 7.29 8 -11 7 128.39 11.33 8 11 7 114.73 19.70 -8 11 -7 124.81 11.52 -8 -11 -7 125.73 23.80 -18 3 11 113.46 18.44 -18 -3 11 86.45 14.75 -18 -3 11 112.11 15.00 18 3 -11 88.78 12.59 18 -3 -11 111.64 11.89 -18 3 11 132.34 11.56 12 4 -15 -2.91 7.11 -12 -4 15 2.01 4.50 -12 4 15 4.65 6.22 -12 4 15 7.50 4.14 12 -4 -15 1.38 5.60 -8 2 16 318.96 20.77 -8 -2 16 314.16 21.14 8 -2 -16 292.35 19.86 -8 2 16 307.08 21.59 8 2 -16 298.09 17.22 8 2 -16 309.30 33.80 -10 14 0 74.51 11.95 10 -14 0 109.01 24.25 10 -14 0 94.85 7.50 10 14 0 101.51 13.53 -10 -14 0 75.05 28.01 -10 -14 0 103.84 15.99 -11 -10 12 220.12 30.26 11 -10 -12 232.99 14.08 -11 -10 12 203.05 11.48 -11 10 12 227.69 16.59 11 -10 -12 229.01 12.63 19 -3 -3 59.06 13.51 19 3 -3 79.51 14.11 -19 3 3 58.77 12.89 -19 -3 3 58.84 11.48 -19 -3 3 75.42 10.50 -19 3 3 57.30 16.92 4 8 -14 34.06 7.02 -4 -8 14 32.07 16.63 -4 -8 14 58.66 11.18 -4 8 14 36.21 10.18 4 -8 -14 37.88 7.60 4 -8 -14 32.16 9.38 -5 -15 7 83.06 11.26 -5 -15 7 72.64 12.12 5 15 -7 77.65 10.22 5 -15 -7 78.21 8.81 5 -15 -7 94.56 15.63 -5 15 7 69.03 31.82 -3 -5 15 107.36 9.82 3 -5 -15 81.88 10.86 -3 -5 15 73.22 13.94 3 -5 -15 93.73 11.33 3 5 -15 76.40 10.05 -3 5 15 98.70 9.92 -16 4 -3 23.98 13.28 -16 4 -3 32.88 4.25 -16 -4 -3 36.52 6.00 16 -4 3 42.30 18.48 16 4 3 34.26 13.68 -16 -4 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12.40 4.11 0 -10 12 17.31 11.53 0 10 -12 17.26 5.18 0 -10 -12 18.87 6.54 0 10 12 19.79 16.97 6 14 5 1.96 6.59 6 -14 5 7.15 6.88 -6 -14 -5 11.78 6.64 -6 -14 -5 1.05 2.93 -6 14 -5 8.65 6.52 6 -14 5 2.36 1.28 -1 3 15 38.42 14.86 1 -3 -15 52.98 8.66 -1 -3 15 50.18 21.85 1 3 -15 54.11 9.10 1 -3 -15 50.81 7.23 1 3 -15 53.69 16.32 -10 5 -9 5.90 6.01 10 -5 9 8.54 4.81 -10 -5 -9 5.07 3.06 -10 -5 -9 14.61 5.62 8 -11 -12 9.27 6.76 -8 -11 12 7.61 4.74 -8 11 12 28.52 13.31 -8 -11 12 4.26 5.54 8 -11 -12 13.72 5.87 -19 4 4 69.15 14.03 -19 -4 4 54.48 17.33 19 4 -4 59.79 21.36 19 -4 -4 80.96 22.39 -19 4 4 56.19 10.86 -19 -4 4 55.24 8.94 10 9 7 1.51 7.61 -10 9 -7 7.95 6.30 10 -9 7 9.92 4.94 -10 -9 -7 4.04 5.73 11 5 -15 39.99 10.51 -11 5 15 33.42 17.92 -11 -5 15 49.43 11.99 11 -5 -15 42.38 9.05 -11 5 15 38.04 16.06 3 -14 7 0.62 1.31 -3 14 -7 8.24 6.13 3 -14 7 1.93 6.58 -3 -14 -7 -0.23 1.62 -3 -14 -7 6.08 5.90 3 14 7 3.05 4.22 -7 -13 10 3.45 7.25 -7 -13 10 6.82 3.55 7 -13 -10 3.92 4.08 -7 13 10 11.12 7.35 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30.34 17.15 11 1 9 32.18 15.04 -11 -1 -9 27.90 10.83 -11 -1 -9 24.46 13.33 -11 1 -9 28.53 6.24 11 -1 9 30.79 13.74 15 -8 2 76.91 21.27 -15 8 -2 63.26 11.45 -15 8 -2 65.97 11.32 -15 -8 -2 70.32 10.97 -15 -8 -2 69.80 17.64 15 8 2 70.81 5.73 19 3 -9 12.07 8.42 -19 3 9 25.27 9.44 19 -3 -9 16.86 6.59 -19 -3 9 6.41 5.60 -19 3 9 5.84 6.42 -19 -3 9 14.69 7.22 -9 2 16 38.15 11.53 -9 -2 16 38.45 8.32 9 2 -16 37.84 8.84 -9 2 16 36.34 5.98 9 -2 -16 42.58 9.63 -9 -2 16 41.33 16.43 -6 10 13 61.83 16.79 6 -10 -13 78.99 7.97 -6 -10 13 85.75 10.84 -6 -10 13 70.39 6.70 6 -10 -13 87.79 16.20 -9 6 15 243.11 17.10 -9 6 15 232.03 25.86 -9 -6 15 252.65 14.64 -9 -6 15 255.98 14.98 9 -6 -15 239.62 17.28 -5 16 -1 71.77 14.80 -5 -16 -1 61.04 28.71 5 -16 1 73.11 7.09 5 -16 1 70.33 15.06 -5 -16 -1 66.34 11.38 5 16 1 90.84 13.94 -7 -15 -2 3.54 2.93 7 -15 2 5.75 4.89 -7 15 -2 7.27 8.06 -7 -15 -2 7.67 5.52 7 -15 2 12.94 10.69 7 15 2 8.06 6.26 -18 3 0 27.11 8.96 -18 -3 0 28.32 12.75 -18 3 0 41.45 8.07 -18 -3 0 35.93 17.34 18 -3 0 33.22 9.64 18 3 0 17.65 12.29 -19 0 10 285.27 18.83 19 0 -10 334.29 17.35 -19 0 10 354.47 16.89 -9 -7 -9 53.55 18.86 -9 -7 -9 49.35 7.26 9 -7 9 53.46 28.22 -9 7 -9 70.48 11.09 -17 8 8 77.53 11.73 -17 8 8 110.08 10.91 17 -8 -8 74.57 28.84 -17 -8 8 99.07 6.09 17 8 -8 63.13 10.63 -17 -8 8 92.31 8.76 -12 13 1 8.11 11.63 12 -13 -1 8.61 7.14 12 -13 -1 2.69 3.47 12 13 -1 3.73 6.34 -12 -13 1 3.49 3.99 -12 -13 1 1.20 2.51 -2 -12 11 8.99 13.02 2 12 -11 7.90 3.69 -2 -12 11 11.58 5.93 2 -12 -11 15.39 10.98 2 -12 -11 11.10 5.11 -2 12 11 34.68 11.19 16 4 -13 106.69 15.67 16 -4 -13 119.13 26.09 -16 4 13 125.46 12.83 -16 -4 13 129.95 11.36 -16 4 13 134.87 23.92 0 -6 14 125.83 9.94 0 6 14 111.75 10.92 0 6 -14 136.41 8.97 0 -6 -14 162.91 11.48 0 6 -14 117.30 12.32 -2 -13 10 8.10 8.17 2 13 -10 4.59 4.70 -2 -13 10 5.04 5.62 2 -13 -10 4.04 6.74 -2 13 10 1.38 7.29 2 -13 -10 3.11 3.63 -4 -4 -13 -3.89 4.72 4 -4 13 0.18 2.05 -4 -4 -13 4.41 3.64 -4 4 -13 1.88 3.70 19 4 -8 222.06 14.09 -19 -4 8 212.99 13.98 19 -4 -8 194.43 13.41 -19 4 8 217.91 20.29 -19 -4 8 189.31 11.19 -19 4 8 245.78 15.38 1 -11 11 30.63 18.71 -1 11 -11 39.20 7.79 -1 -11 -11 32.54 14.51 1 11 11 40.63 10.00 -13 3 15 28.19 6.56 13 3 -15 25.39 10.37 13 -3 -15 43.66 10.50 -13 -3 15 34.25 7.77 -13 3 15 49.22 10.65 -10 -1 16 39.70 10.33 -10 1 16 41.64 14.53 -10 -1 16 27.88 13.00 -10 1 16 40.13 16.90 10 -1 -16 40.84 7.79 10 1 -16 50.25 8.83 6 -16 -1 52.02 8.35 6 16 -1 54.03 11.47 -6 16 1 51.60 15.80 -6 -16 1 41.74 20.70 -6 -16 1 43.63 19.08 6 -16 -1 49.18 19.84 6 7 11 30.53 14.66 -6 -7 -11 45.76 13.58 -6 7 -11 31.68 14.02 6 -7 11 44.05 12.42 -2 -15 -6 55.52 10.92 2 -15 6 49.63 15.03 2 15 6 55.20 11.61 -2 15 -6 54.86 15.20 -2 -15 -6 48.20 14.11 2 -15 6 56.55 11.39 11 -13 -8 34.68 10.68 11 -13 -8 20.84 12.71 -11 13 8 20.21 13.60 -11 -13 8 21.04 10.29 -11 -13 8 14.82 12.33 2 16 -5 5.66 6.37 -2 -16 5 5.19 2.93 2 -16 -5 1.30 7.03 -2 -16 5 1.78 6.36 2 -16 -5 5.05 3.84 -2 16 5 2.02 9.23 0 0 15 1.50 1.71 0 0 -15 0.83 3.02 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3.73 4.28 -14 -12 5 6.80 5.96 -14 -12 5 2.39 2.51 -18 -6 2 427.85 17.33 18 -6 -2 455.81 18.83 18 6 -2 477.63 17.94 -18 6 2 477.43 17.93 -18 -6 2 403.50 16.61 -18 6 2 476.32 22.95 -19 -2 10 2.06 4.55 -19 2 10 5.65 6.31 -19 -2 10 6.32 8.33 19 -2 -10 15.22 7.06 19 2 -10 4.76 8.35 -19 2 10 3.37 4.87 -17 8 2 99.07 22.04 -17 8 2 111.49 18.48 17 -8 -2 117.30 18.00 -17 -8 2 113.80 8.11 17 8 -2 102.86 8.98 -17 -8 2 112.85 24.59 -17 -6 11 135.60 29.65 17 -6 -11 109.10 11.90 17 6 -11 92.11 21.82 -17 6 11 98.87 16.90 -17 6 11 112.46 12.41 -14 11 0 132.79 32.43 14 -11 0 130.08 11.84 14 -11 0 132.54 8.19 14 11 0 126.95 8.47 -14 -11 0 123.08 10.49 -14 -11 0 126.40 12.95 -18 7 4 -2.76 7.60 18 -7 -4 9.82 8.30 -18 7 4 5.32 5.54 18 7 -4 4.79 4.42 -18 -7 4 1.42 5.38 -18 -7 4 3.30 2.77 -9 11 12 2.01 5.57 -9 -11 12 7.04 7.83 9 -11 -12 -1.26 6.55 -9 -11 12 2.14 5.74 9 -11 -12 -0.65 3.19 -6 -16 0 275.02 13.29 6 -16 0 242.58 12.00 -6 -16 0 271.19 19.32 -6 16 0 276.41 40.59 6 16 0 249.39 13.92 6 -16 0 289.30 15.67 16 -10 -6 89.79 10.16 -16 10 6 111.00 24.37 -16 10 6 65.94 43.24 -16 -10 6 99.77 10.36 16 10 -6 107.09 11.78 -16 -10 6 112.95 6.99 -7 11 -8 106.97 18.47 -7 -11 -8 106.20 12.14 7 -11 8 87.87 12.50 7 11 8 87.48 12.80 8 -13 -10 6.06 10.75 -8 -13 10 4.59 5.73 8 -13 -10 6.63 3.58 -8 -13 10 2.51 3.93 -8 13 10 7.03 7.27 8 -15 1 1.34 8.20 8 -15 1 6.31 5.07 -8 15 -1 7.75 7.74 -8 -15 -1 7.04 6.62 -8 -15 -1 0.01 6.32 8 15 1 18.52 9.56 -15 6 13 52.57 10.87 -15 6 13 44.11 19.53 15 6 -13 48.39 22.83 15 -6 -13 57.43 9.98 -15 -6 13 61.12 27.49 15 -10 -9 28.62 9.41 -15 10 9 33.39 19.15 -15 10 9 39.55 20.91 -15 -10 9 31.42 11.07 15 10 -9 38.47 10.89 -10 6 15 5.73 6.31 -10 6 15 5.91 6.52 -10 -6 15 9.49 9.97 -10 -6 15 5.88 6.52 10 -6 -15 10.35 5.50 -13 12 0 33.83 15.33 13 -12 0 34.54 5.86 13 -12 0 44.34 11.91 -13 -12 0 44.63 6.93 13 12 0 44.11 12.38 -13 -12 0 44.87 25.77 -3 6 -13 98.06 10.81 3 6 13 87.40 35.07 -3 -6 -13 83.96 10.54 3 -6 13 126.58 21.73 6 3 -16 3.48 2.59 -6 3 16 4.91 3.85 -6 -3 16 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7.84 5.99 -15 1 15 -0.16 4.84 -15 -1 15 -0.55 2.16 2 16 5 -1.87 6.54 2 -16 5 0.47 2.69 -2 16 -5 7.71 5.29 -2 -16 -5 1.24 6.57 -2 -16 -5 2.57 3.02 2 -16 5 1.72 7.81 -18 8 5 4.82 7.40 18 -8 -5 3.05 4.46 -18 8 5 1.27 4.38 18 8 -5 4.82 5.49 -18 -8 5 -1.08 5.75 -18 -8 5 2.73 3.38 -9 -1 -11 73.58 9.64 9 1 11 57.54 7.35 9 -1 11 71.52 13.95 -9 -1 -11 65.97 11.39 -9 1 -11 68.63 11.96 13 5 -15 29.38 9.95 13 -5 -15 44.65 9.38 -13 5 15 41.92 21.75 -13 5 15 41.90 7.96 -13 -5 15 30.04 19.42 15 -10 -10 92.21 13.35 -15 10 10 97.48 32.54 -15 10 10 126.36 14.12 15 10 -10 108.94 14.85 -15 -10 10 85.02 18.89 -10 12 -5 123.95 22.23 10 -12 5 119.71 23.76 10 12 5 133.45 17.86 -10 -12 -5 150.68 12.88 -11 -10 -6 120.04 18.41 -11 10 -6 138.71 15.81 11 10 6 140.66 27.87 11 -10 6 102.87 23.87 4 7 -15 8.33 5.37 -4 -7 15 7.74 4.09 -4 7 15 2.05 9.40 4 -7 -15 14.96 6.85 -4 -7 15 11.19 7.22 4 -7 -15 7.97 6.19 10 -15 -2 16.93 10.80 10 -15 -2 -1.33 4.07 -10 15 2 3.35 8.68 -10 -15 2 3.98 6.35 -10 -15 2 5.59 3.61 10 15 -2 2.19 3.31 -17 -2 -3 415.17 14.99 17 2 3 413.85 17.97 17 -2 3 452.92 17.43 -17 2 -3 398.79 14.45 -17 2 -3 500.33 22.02 -17 -2 -3 434.94 19.40 -1 -17 3 2.34 4.80 1 -17 -3 5.69 5.97 -1 -17 3 5.82 7.52 1 17 -3 9.64 4.45 -1 17 3 3.23 7.38 1 -17 -3 6.18 6.88 20 -3 -7 154.53 11.79 20 3 -7 125.17 10.60 -20 3 7 140.81 18.79 -20 -3 7 135.71 10.72 -20 3 7 144.70 13.13 -20 -3 7 121.35 19.44 -5 -16 6 98.23 32.20 5 16 -6 85.60 10.13 -5 -16 6 84.32 21.35 5 -16 -6 74.79 28.59 5 -16 -6 85.30 11.39 -5 16 6 80.81 20.72 -2 -17 3 4.00 5.34 2 -17 -3 2.52 5.48 2 -17 -3 1.95 3.95 -2 -17 3 -1.99 6.21 -2 17 3 5.03 6.22 2 17 -3 -1.83 3.90 0 -4 -15 2.01 2.56 0 4 -15 3.38 1.25 0 -4 -15 5.76 3.59 0 4 15 5.87 4.37 0 4 -15 6.96 2.75 0 -4 15 5.98 4.17 -2 -6 15 2.66 3.58 2 -6 -15 8.70 3.67 -2 6 15 2.38 3.94 2 6 -15 2.32 2.45 -2 -6 15 2.21 3.70 2 -6 -15 0.85 4.88 20 0 -9 3.53 5.95 -20 0 9 6.75 6.72 -20 0 9 4.92 6.16 15 -9 2 56.61 26.77 -15 9 -2 61.37 9.73 -15 9 -2 71.27 17.44 15 9 2 66.86 14.00 -15 -9 -2 60.16 12.54 -15 -9 -2 51.01 8.38 20 2 -4 1.62 4.40 -20 -2 4 1.70 5.29 -20 2 4 -0.15 4.67 20 -2 -4 5.09 4.86 -20 -2 4 4.01 5.95 -20 2 4 1.94 5.36 -18 7 2 85.34 12.92 18 -7 -2 97.86 9.76 -18 7 2 61.46 27.53 -18 -7 2 95.56 14.18 18 7 -2 75.76 13.96 -18 -7 2 77.02 9.56 -17 7 11 3.55 6.60 17 -7 -11 2.87 6.33 -17 7 11 4.84 8.44 -17 -7 11 3.92 6.11 17 7 -11 -7.75 6.34 17 -9 -8 83.10 33.52 -17 9 8 84.63 10.10 -17 9 8 75.73 20.43 -17 -9 8 123.21 22.43 17 9 -8 98.66 10.45 -17 -9 8 80.22 5.42 6 -12 -12 14.20 8.41 6 -12 -12 16.27 10.26 -6 -12 12 10.54 7.57 -6 -12 12 19.42 6.90 -6 12 12 15.59 11.94 -5 13 11 826.74 33.23 5 -13 -11 947.77 26.55 5 -13 -11 944.61 32.65 -5 -13 11 931.44 32.50 -5 -13 11 883.52 29.52 -15 7 13 10.84 9.06 -15 -7 13 7.61 8.09 -15 7 13 7.53 8.59 15 -7 -13 15.86 8.97 15 7 -13 18.87 11.00 -5 -12 12 153.74 25.98 -5 12 12 148.27 25.73 -5 -12 12 156.98 13.55 5 -12 -12 165.43 16.19 5 -12 -12 130.93 15.13 3 -13 9 10.64 7.28 -3 13 -9 4.18 4.18 -3 -13 -9 -0.12 6.83 3 13 9 5.96 7.08 -10 -7 15 11.56 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6.26 -19 -6 9 9.48 8.65 19 6 -9 19.83 8.92 17 5 -13 43.59 10.78 -17 5 13 23.98 11.81 -17 5 13 32.38 9.65 -17 -5 13 16.80 15.38 17 -5 -13 33.93 9.71 -20 -4 8 7.71 6.26 20 4 -8 13.44 8.74 20 -4 -8 2.18 3.87 -20 4 8 9.14 8.57 -20 -4 8 2.63 4.01 -20 4 8 0.35 2.90 -18 -6 0 265.68 16.69 18 -6 0 236.52 17.01 18 6 0 228.09 15.14 -18 6 0 267.49 15.52 -18 -6 0 279.20 17.68 -18 6 0 246.43 19.35 5 -5 13 96.03 8.36 -5 5 -13 116.26 9.14 -5 -5 -13 109.18 9.75 -5 -5 -13 115.93 8.27 14 -12 0 34.43 17.16 -14 12 0 50.02 19.47 14 -12 0 44.62 11.67 -14 -12 0 34.70 7.05 14 12 0 16.90 5.36 -14 -12 0 32.39 10.84 4 16 -7 108.93 15.01 -4 -16 7 111.97 33.67 -4 -16 7 111.18 7.88 4 -16 -7 91.31 10.12 4 -16 -7 87.16 10.16 -4 16 7 142.32 25.38 -9 -12 12 10.63 8.01 9 -12 -12 7.07 4.01 -9 -12 12 2.51 3.32 -9 12 12 16.03 10.62 9 -12 -12 16.39 9.63 10 -15 0 101.68 7.92 -10 15 0 94.14 16.95 10 -15 0 123.79 16.43 -10 -15 0 104.31 9.35 10 15 0 103.05 17.53 -10 -15 0 88.75 13.05 -14 10 -3 8.88 9.26 14 -10 3 10.80 9.85 -14 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11 187.27 29.26 19 4 -11 188.93 15.44 -19 -4 11 151.36 9.52 -12 4 16 135.65 10.58 -12 4 16 160.21 14.34 -12 -4 16 158.85 12.60 12 -4 -16 178.13 26.51 12 4 -16 160.31 14.97 -19 7 6 15.38 9.00 19 -7 -6 3.01 7.83 -19 7 6 12.57 7.80 -19 -7 6 12.11 11.25 -19 -7 6 6.04 5.65 19 7 -6 7.01 6.66 8 -16 0 29.63 6.41 -8 16 0 27.06 17.34 8 -16 0 29.41 13.84 8 16 0 18.62 9.33 -8 -16 0 10.62 9.12 -8 -16 0 17.18 9.33 11 -14 -8 295.78 20.67 11 -14 -8 317.68 19.47 -11 14 8 315.31 23.91 -11 -14 8 303.86 19.62 -11 -14 8 309.02 20.94 15 -12 -3 106.81 36.65 15 -12 -3 97.00 10.45 -15 12 3 84.40 36.33 -15 -12 3 82.89 16.64 15 12 -3 75.57 8.67 -15 -12 3 106.63 19.76 14 -9 4 5.47 4.65 -14 9 -4 7.70 7.58 -14 -9 -4 8.09 7.77 -14 -9 -4 2.12 5.49 5 17 0 4.14 5.39 -5 -17 0 -1.74 5.77 5 -17 0 1.47 2.87 5 -17 0 5.78 5.04 -5 -17 0 -0.48 3.59 -5 17 0 1.84 5.05 -2 -16 7 1.55 3.20 2 16 -7 2.01 2.51 -2 -16 7 8.53 7.23 2 -16 -7 8.64 8.99 2 -16 -7 0.75 3.36 -2 16 7 3.57 8.26 7 13 7 95.00 22.12 -7 13 -7 171.31 13.34 7 -13 7 148.51 12.32 -7 -13 -7 159.49 30.45 -4 -17 4 239.10 14.75 4 -17 -4 238.46 15.99 4 17 -4 265.51 35.83 -4 -17 4 236.74 30.71 -4 17 4 234.18 19.66 4 -17 -4 212.14 15.44 -6 -15 -5 12.71 6.33 6 -15 5 30.62 9.78 -6 15 -5 45.89 11.25 6 15 5 44.65 16.10 6 -15 5 37.67 9.77 -9 8 15 169.16 17.33 -9 -8 15 183.65 10.37 9 -8 -15 171.93 23.57 9 -8 -15 155.46 25.63 -9 -8 15 189.54 12.17 -8 16 5 18.95 10.50 8 -16 -5 9.43 8.09 8 -16 -5 14.69 7.78 -8 -16 5 4.90 4.85 8 16 -5 13.12 7.12 -8 -16 5 12.40 8.49 -18 -2 -2 58.73 9.89 -18 2 -2 68.48 6.11 -18 -2 -2 77.13 12.62 -18 2 -2 59.26 18.86 18 2 2 53.06 23.06 18 -2 2 63.26 21.65 -1 0 16 533.70 27.79 1 0 -16 490.68 25.50 1 0 -16 569.86 15.66 0 8 -14 26.06 7.04 0 -8 14 27.55 9.08 0 8 14 16.84 7.20 0 -8 -14 15.97 7.09 3 -15 7 5.40 7.57 -3 15 -7 11.54 5.07 3 -15 7 14.71 7.67 -3 -15 -7 19.50 9.29 3 15 7 19.48 10.58 -16 9 -1 522.03 31.89 -16 9 -1 478.50 25.63 16 -9 1 523.05 29.25 -16 -9 -1 512.77 27.44 -16 -9 -1 487.06 28.87 16 9 1 500.40 24.84 -4 -5 16 424.89 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2 10 1.47 5.01 1 1 -16 104.27 6.99 1 -1 -16 120.93 9.00 1 1 -16 111.22 20.25 -1 -1 16 89.45 12.43 1 -1 -16 128.26 9.47 1 -1 -16 121.19 10.16 -12 11 12 0.02 8.25 12 -11 -12 2.01 6.15 12 -11 -12 8.21 6.35 -12 -11 12 0.23 4.60 -12 -11 12 1.09 4.76 5 16 -7 114.80 18.18 -5 -16 7 119.88 16.59 -5 -16 7 113.27 11.07 -5 16 7 88.41 14.17 5 -16 -7 124.79 11.35 5 -16 -7 130.03 22.33 -12 -2 -9 52.71 10.78 12 -2 9 44.61 22.78 -12 -2 -9 45.80 5.60 -12 2 -9 51.58 20.40 -6 10 14 3.32 6.63 -6 -10 14 0.37 2.92 6 -10 -14 5.13 7.74 -6 -10 14 15.27 8.17 6 -10 -14 0.18 2.25 -16 8 12 13.13 7.55 -16 8 12 9.61 6.73 16 -8 -12 2.23 5.17 16 8 -12 6.36 5.88 -16 -8 12 5.53 6.62 -19 7 7 18.13 11.79 19 -7 -7 4.75 5.96 -19 -7 7 2.01 3.14 -19 -7 7 1.33 5.13 19 7 -7 6.32 6.57 13 -13 0 25.20 9.15 13 -13 0 34.38 7.55 -13 13 0 32.37 15.12 13 13 0 20.99 9.37 13 13 0 9.22 3.93 -13 -13 0 33.65 11.56 -7 -10 14 0.24 5.55 -7 10 14 -1.56 6.48 7 -10 -14 9.01 10.26 -7 -10 14 2.15 3.51 7 -10 -14 2.56 2.79 -13 3 16 22.02 8.97 -13 -3 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2 12 5.54 6.34 -19 -2 12 0.30 4.10 19 2 -12 0.91 6.87 19 -2 -12 6.22 6.97 2 7 -15 218.97 16.22 -2 -7 15 219.61 12.49 -2 -7 15 239.22 16.67 2 -7 -15 211.81 14.50 -2 7 15 234.86 17.90 16 -9 -11 31.55 12.21 -16 9 11 18.09 7.01 -16 9 11 7.89 4.62 16 9 -11 18.84 6.74 -16 -9 11 21.79 10.44 7 -6 -16 0.67 3.83 7 -6 -16 8.42 6.48 -7 -6 16 -0.33 5.35 -7 -6 16 1.94 4.67 -7 6 16 4.02 6.63 10 -14 -9 133.70 12.08 -10 14 9 159.49 32.48 10 -14 -9 114.60 28.36 -10 -14 9 125.96 20.24 -10 -14 9 143.99 12.19 -7 0 17 1.10 5.21 -7 0 17 1.61 3.22 7 0 -17 6.53 4.60 -20 1 2 2.13 1.82 -20 -1 2 1.88 3.39 20 -1 -2 1.56 4.64 20 1 -2 2.80 4.28 -20 -1 2 4.45 4.99 -20 1 2 0.28 7.12 -14 -3 -7 35.92 19.93 14 3 7 32.68 10.38 -14 3 -7 20.99 7.19 14 -3 7 35.36 11.85 -14 -3 -7 47.69 14.57 8 -6 -16 59.67 8.76 -8 -6 16 62.16 13.36 8 -6 -16 48.95 12.67 -8 -6 16 54.55 15.86 -8 6 16 63.81 10.97 1 -11 12 77.39 15.64 -1 11 -12 63.66 10.79 -1 -11 -12 59.54 9.00 1 11 12 50.28 10.96 -4 -15 9 25.72 7.99 -4 -15 9 35.95 19.49 4 15 -9 25.77 5.33 -4 15 9 22.34 9.62 4 -15 -9 35.85 11.40 4 -15 -9 26.15 10.90 -9 15 -2 7.01 6.69 9 -15 2 0.99 2.56 9 -15 2 -2.61 6.89 9 15 2 3.74 4.35 -9 -15 -2 -7.71 6.66 -9 -15 -2 -1.80 2.14 9 -13 -11 66.81 8.86 9 -13 -11 72.82 13.52 -9 13 11 53.58 14.65 -9 -13 11 67.35 16.28 -9 -13 11 69.96 14.63 4 -13 9 136.97 12.46 -4 13 -9 125.83 13.77 4 13 9 122.81 14.22 -4 -13 -9 127.41 10.61 -9 14 -4 52.18 11.40 9 -14 4 50.28 10.85 9 -14 4 41.90 14.60 -9 -14 -4 29.45 16.47 9 14 4 62.50 11.59 -12 8 -7 0.52 5.51 -12 -8 -7 4.18 6.22 12 -8 7 3.30 5.69 -12 -8 -7 1.44 4.34 -12 10 13 49.09 12.18 12 -10 -13 46.50 7.96 12 -10 -13 51.30 9.85 -12 -10 13 42.67 13.24 -12 -10 13 50.71 17.17 1 -15 8 31.93 11.97 -1 15 -8 22.44 6.40 1 -15 8 40.93 13.55 -1 -15 -8 22.75 8.82 -1 -15 -8 19.53 8.19 1 15 8 35.29 11.56 8 -14 5 152.10 30.97 -8 -14 -5 159.63 14.40 8 14 5 142.86 22.09 -8 14 -5 173.49 14.06 -13 -8 -6 153.79 15.29 -13 8 -6 142.48 15.73 -13 -8 -6 111.44 10.04 13 -8 6 178.62 11.35 8 -1 -17 5.27 3.47 -8 -1 17 3.29 3.17 -8 1 17 0.19 3.58 -8 1 17 3.70 5.55 -8 -1 17 2.60 5.13 8 1 -17 6.63 5.86 0 -10 13 6.56 8.03 0 10 -13 2.32 2.05 0 10 13 3.40 3.80 0 -10 -13 3.35 5.10 -18 -3 13 14.43 8.64 -18 3 13 4.94 5.69 18 -3 -13 13.46 9.48 18 3 -13 17.73 15.02 -18 -3 13 6.43 4.30 -18 3 13 6.66 7.44 -4 3 -14 13.72 6.03 4 -3 14 7.59 6.28 -4 -3 -14 10.57 8.88 -4 -3 -14 17.53 8.28 11 -15 -3 33.02 17.97 11 -15 -3 32.86 20.10 -11 15 3 52.24 18.63 -11 -15 3 29.83 6.50 -11 -15 3 27.17 11.08 11 15 -3 38.02 7.59 9 0 -17 8.13 8.63 -9 0 17 0.38 3.83 -9 0 17 5.36 4.41 17 -10 -7 0.59 3.88 -17 10 7 8.92 7.55 -17 10 7 1.42 3.58 -17 -10 7 1.71 5.38 17 10 -7 4.56 5.31 -17 -10 7 -0.02 2.30 -6 3 -13 99.34 20.36 -6 -3 -13 84.88 11.80 -6 -3 -13 99.51 9.24 6 -3 13 99.64 11.52 -12 -6 -8 111.80 11.07 -12 6 -8 135.28 12.56 -12 -6 -8 104.53 8.86 12 -6 8 147.42 11.13 -17 9 1 19.92 4.97 -17 9 1 7.83 8.79 17 -9 -1 10.01 6.64 -17 -9 1 12.79 10.93 -17 -9 1 5.54 4.73 17 9 -1 14.75 8.48 -5 -16 -4 9.73 5.88 5 -16 4 23.66 11.57 -5 -16 -4 8.24 5.76 5 16 4 4.33 7.07 -5 16 -4 12.26 9.20 5 -16 4 4.23 3.00 14 0 -16 236.36 17.61 -14 0 16 202.20 9.40 -14 0 16 238.03 17.60 7 -5 12 9.10 4.51 -7 -5 -12 4.74 3.66 -7 -5 -12 13.45 8.79 -7 5 -12 -2.31 5.08 -11 15 4 31.40 14.23 11 -15 -4 28.80 7.88 11 -15 -4 42.79 10.05 -11 -15 4 28.66 7.76 -11 -15 4 31.88 15.08 11 15 -4 25.32 14.16 14 -13 -3 15.07 6.01 -14 13 3 8.21 8.76 14 -13 -3 17.36 9.25 -14 -13 3 15.19 7.02 -14 -13 3 21.58 12.08 14 13 -3 28.56 7.24 -5 -15 9 24.95 14.79 5 -15 -9 39.00 6.99 5 -15 -9 33.74 21.47 -5 -15 9 27.35 13.42 5 -8 12 12.14 7.76 -5 8 -12 8.51 10.00 -5 -8 -12 9.34 7.37 5 8 12 15.87 10.02 -18 8 9 56.73 34.37 -18 8 9 73.11 13.20 18 -8 -9 66.12 9.99 -18 -8 9 67.36 5.94 18 8 -9 75.09 29.57 -18 -8 9 80.63 12.18 -16 5 14 113.73 21.03 16 -5 -14 115.68 15.72 16 5 -14 109.35 35.44 -16 -5 14 101.88 22.12 -16 5 14 135.94 13.82 -16 1 15 8.15 9.99 -16 -1 15 24.47 15.24 16 -1 -15 17.95 8.03 16 1 -15 19.23 10.59 -16 -1 15 7.02 4.89 -16 1 15 13.78 8.99 -4 9 -12 63.66 6.97 4 -9 12 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5.37 7 -16 2 7.44 13.68 -7 -16 -2 1.44 2.46 7 -16 2 1.46 2.62 -7 -16 -2 5.06 5.73 7 16 2 0.46 5.01 -7 16 -2 6.80 7.35 -12 7 15 551.55 22.21 -12 -7 15 501.16 34.40 12 -7 -15 511.53 28.54 -12 -7 15 499.01 36.73 -12 7 15 482.25 38.20 -7 11 -9 4.53 4.55 7 -11 9 -0.53 6.23 7 11 9 4.14 5.65 -7 -11 -9 1.71 4.34 -8 -10 14 26.78 9.13 -8 10 14 34.20 11.44 8 -10 -14 30.98 5.58 -8 -10 14 17.35 5.16 8 -10 -14 23.68 10.37 -3 -15 9 69.02 24.12 -3 -15 9 61.04 14.43 3 15 -9 65.71 12.20 3 -15 -9 48.64 13.51 3 -15 -9 60.01 10.74 -3 15 9 63.45 12.91 8 -14 -10 41.26 12.28 -8 -14 10 17.28 11.02 -8 14 10 52.68 13.76 8 -14 -10 26.35 8.33 -8 -14 10 31.82 12.06 15 -10 -11 122.22 24.52 -15 10 11 139.89 23.04 -15 10 11 112.00 25.14 15 10 -11 125.14 14.18 -15 -10 11 86.30 19.87 -1 -13 11 16.34 7.95 1 13 -11 21.00 5.61 -1 -13 11 13.93 8.33 1 -13 -11 27.93 10.28 -1 13 11 28.10 8.94 -19 -3 0 139.03 10.89 -19 3 0 112.68 10.63 -19 -3 0 132.69 17.28 19 3 0 129.41 9.01 -19 3 0 107.06 15.37 19 -3 0 112.13 9.37 11 0 10 1.14 1.66 -11 0 -10 3.77 8.38 -11 0 -10 7.37 2.65 -15 -4 15 61.32 20.95 -15 4 15 37.57 10.16 -15 4 15 64.65 13.03 15 4 -15 42.25 29.21 15 -4 -15 58.28 10.11 -18 -5 -1 56.20 9.57 18 -5 1 52.93 11.85 -18 5 -1 94.02 12.34 -18 -5 -1 70.04 9.62 18 5 1 46.09 16.59 -18 5 -1 69.24 12.25 -6 -6 16 108.45 11.06 6 -6 -16 94.31 17.24 -6 -6 16 96.84 8.60 -6 6 16 91.15 19.18 6 -6 -16 88.55 19.09 -15 12 7 27.90 12.31 -15 12 7 11.07 9.96 15 -12 -7 14.64 9.87 -15 -12 7 12.61 4.84 -15 -12 7 20.26 9.05 -16 7 -3 3.04 4.90 16 7 3 2.59 2.91 16 -7 3 3.20 5.82 -16 -7 -3 1.08 2.60 -16 -7 -3 4.74 4.09 9 -4 11 253.06 15.74 -9 -4 -11 247.13 21.51 -9 4 -11 300.74 19.89 -9 -4 -11 242.03 14.13 -12 14 7 156.51 15.63 12 -14 -7 163.48 12.59 12 -14 -7 154.64 12.34 -12 -14 7 178.61 11.92 -12 -14 7 168.96 19.40 -12 -14 7 149.65 6.13 -9 -1 17 67.75 5.95 -9 1 17 69.73 20.00 -9 -1 17 79.11 19.50 9 -1 -17 72.93 10.00 9 1 -17 80.73 11.40 -9 1 17 62.98 15.91 -16 -2 -5 133.22 7.90 16 2 5 114.21 16.40 16 -2 5 131.85 9.04 -16 2 -5 136.35 6.42 -16 -2 -5 102.62 12.19 -16 2 -5 122.23 24.53 2 -13 10 90.87 21.96 -2 13 -10 90.52 13.11 2 13 10 113.11 12.57 -2 -13 -10 117.33 35.88 4 17 2 0.17 4.76 4 -17 2 4.82 7.82 -4 -17 -2 -1.18 3.68 4 -17 2 3.37 3.72 -4 17 -2 3.51 4.29 -4 -17 -2 7.63 5.83 -2 2 -15 6.93 5.62 -2 -2 -15 4.98 3.40 2 -2 15 8.47 4.88 -2 2 -15 12.19 4.31 -2 -2 -15 5.58 4.34 -2 -2 -15 11.96 4.86 -4 -8 15 32.31 14.67 4 -8 -15 40.31 6.43 -4 8 15 47.30 21.44 4 -8 -15 54.79 9.72 -4 -8 15 37.78 12.52 14 -1 -16 150.01 30.23 14 1 -16 143.30 12.27 -14 -1 16 143.13 26.34 -14 -1 16 144.68 9.67 -14 1 16 171.63 9.73 -14 1 16 222.32 17.38 -8 -2 -12 -0.59 2.45 -8 2 -12 2.21 4.90 -8 -2 -12 2.36 3.09 8 -2 12 1.72 2.57 -17 -3 14 31.70 8.57 -17 3 14 28.22 13.11 17 -3 -14 43.79 8.77 17 3 -14 52.78 14.41 -17 3 14 26.48 15.64 2 -16 6 234.89 33.64 -2 16 -6 214.42 15.97 2 -16 6 199.38 7.88 -2 -16 -6 217.83 13.24 2 16 6 222.63 18.46 -2 -16 -6 199.87 32.49 -15 -3 -6 17.86 12.14 15 3 6 12.92 6.61 15 -3 6 24.35 13.69 -15 3 -6 47.19 11.94 -15 -3 -6 26.07 15.95 14 -13 -6 0.32 4.43 -14 13 6 9.67 13.28 14 -13 -6 7.09 6.72 -14 -13 6 2.91 2.73 -14 -13 6 5.75 4.71 -14 -13 6 6.22 7.40 12 -13 2 73.38 5.64 12 -13 2 54.57 38.06 -12 13 -2 59.04 29.23 12 13 2 66.83 27.52 12 13 2 73.14 13.33 -12 -13 -2 86.58 12.66 -9 -6 16 53.39 13.03 -9 6 16 58.35 26.64 -9 -6 16 47.87 24.44 9 -6 -16 46.59 7.39 -9 6 16 58.75 21.77 20 5 -6 26.05 14.46 20 -5 -6 17.58 8.11 -20 -5 6 20.63 10.11 -20 5 6 17.84 15.27 -20 -5 6 18.64 5.68 -20 5 6 14.89 7.78 18 -8 -2 80.85 14.36 -18 8 2 81.31 20.58 -18 8 2 91.85 7.91 18 8 -2 83.05 8.05 -18 -8 2 71.50 8.55 -18 -8 2 102.86 9.31 9 -9 9 7.26 7.81 -9 9 -9 5.16 5.50 -9 -9 -9 -0.66 4.14 9 9 9 2.23 7.20 17 -8 -11 175.13 12.18 -17 8 11 195.29 15.66 -17 8 11 131.18 13.32 17 8 -11 179.27 14.09 -17 -8 11 206.93 13.40 1 -2 -16 2.20 4.58 1 2 -16 4.08 3.79 -1 -2 16 6.08 6.53 1 -2 -16 2.82 4.20 1 -2 -16 8.66 4.91 1 2 -16 3.27 2.90 19 -7 -4 37.16 9.72 -19 7 4 20.24 8.87 -19 7 4 18.28 8.72 19 7 -4 27.97 7.92 -19 -7 4 29.18 12.12 -19 -7 4 22.76 8.89 -4 12 -10 35.61 10.24 4 -12 10 40.25 10.93 4 12 10 37.56 9.80 -4 -12 -10 40.26 7.83 -6 0 17 4.26 3.07 6 0 -17 7.42 4.16 -6 0 17 1.75 4.25 -15 8 13 38.44 21.51 15 -8 -13 54.15 17.57 -15 8 13 70.36 28.47 15 8 -13 55.97 13.21 -15 -8 13 69.20 30.35 -11 -1 -10 18.62 14.83 -11 -1 -10 22.86 11.85 11 1 10 15.05 9.31 11 -1 10 21.47 5.68 -11 1 -10 35.99 17.81 -10 -8 15 32.78 17.16 10 -8 -15 53.17 11.15 -10 -8 15 30.63 12.19 -10 8 15 16.63 7.12 10 -8 -15 36.62 14.28 -3 8 -13 5.06 4.28 3 -8 13 -0.56 5.07 3 8 13 6.19 3.43 -3 -8 -13 4.21 4.51 9 -16 -3 58.37 30.29 -9 16 3 61.47 31.72 9 -16 -3 74.75 10.21 -9 -16 3 75.18 15.28 -9 -16 3 69.91 14.29 9 16 -3 72.42 12.12 5 -17 -4 132.80 18.40 -5 -17 4 131.55 10.45 -5 17 4 147.63 14.77 5 17 -4 132.02 25.76 5 -17 -4 141.44 16.63 -5 -17 4 121.98 18.82 -5 15 -6 3.36 5.62 -5 -15 -6 4.71 4.72 5 -15 6 10.05 7.10 5 15 6 10.37 7.52 5 -15 6 2.23 2.39 -1 -14 10 54.48 23.71 -1 -14 10 58.41 4.80 1 14 -10 68.21 9.08 1 -14 -10 72.58 10.70 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2 6.29 5.21 20 4 -9 2.99 8.17 -20 -4 9 19.35 9.73 -20 4 9 6.38 6.98 20 -4 -9 18.76 9.38 -20 4 9 13.69 6.03 -20 -4 9 4.94 4.44 -11 -8 -8 23.83 8.14 -11 -8 -8 30.10 15.78 -11 8 -8 32.73 16.06 11 -8 8 23.94 8.10 -6 -15 9 7.65 7.43 -6 -15 9 2.03 3.32 6 -15 -9 0.39 3.67 6 -15 -9 9.05 7.43 -6 15 9 15.73 8.66 5 -17 1 226.15 22.27 -5 -17 -1 230.93 15.58 5 17 1 239.46 24.21 5 -17 1 234.88 22.87 -5 17 -1 202.21 14.21 -5 -17 -1 262.65 16.11 -20 -2 2 189.99 31.23 20 -2 -2 179.31 15.05 -20 2 2 219.86 17.96 -20 -2 2 184.53 20.81 -20 2 2 206.20 10.81 20 2 -2 196.92 12.05 -2 14 -9 26.26 12.84 2 -14 9 6.36 6.37 2 14 9 28.84 9.98 -2 -14 -9 27.84 14.72 -6 16 7 11.85 9.21 -6 -16 7 4.90 6.42 6 -16 -7 3.17 5.48 -6 -16 7 4.76 7.17 6 16 -7 9.51 5.13 6 -16 -7 3.41 3.83 14 -8 5 3.06 5.39 -14 -8 -5 3.03 5.06 -14 8 -5 3.16 7.44 -14 -8 -5 2.42 3.64 7 14 6 21.90 10.83 -7 14 -6 44.93 10.19 -7 -14 -6 29.64 9.56 7 -14 6 29.82 16.64 9 -16 -2 74.98 9.29 9 -16 -2 77.57 18.59 -9 16 2 77.14 13.47 9 16 -2 74.71 10.79 -9 -16 2 67.08 10.45 -9 -16 2 95.80 15.15 18 3 2 8.35 4.43 18 -3 2 16.24 8.80 -18 -3 -2 11.06 4.34 -18 3 -2 7.27 5.37 -18 -3 -2 7.67 4.01 -18 3 -2 10.17 9.73 -17 10 3 43.26 6.73 -17 10 3 38.18 10.17 17 -10 -3 43.82 21.16 -17 -10 3 35.51 24.71 -17 -10 3 31.10 14.14 17 10 -3 38.39 7.01 -15 12 2 22.89 13.09 15 -12 -2 4.73 3.39 15 -12 -2 4.66 5.31 -15 -12 2 8.17 3.47 -15 -12 2 6.46 5.91 15 12 -2 6.33 6.02 -18 9 6 145.83 29.85 -18 9 6 174.45 19.99 18 -9 -6 156.08 13.18 18 9 -6 165.15 12.78 -18 -9 6 126.04 16.43 -18 -9 6 163.29 10.93 6 1 -17 0.93 0.89 -6 1 17 2.32 5.80 6 1 -17 5.19 4.67 6 -1 -17 4.39 3.82 -6 1 17 1.79 4.12 -6 -1 17 3.42 2.57 10 0 -17 6.22 5.02 -10 0 17 2.95 6.05 -10 0 17 6.69 3.55 -16 -7 13 0.73 5.45 16 -7 -13 2.13 5.79 16 7 -13 9.56 10.34 -16 7 13 3.48 8.84 -16 7 13 0.45 7.01 -8 -2 17 6.29 5.28 -8 2 17 5.71 6.20 8 2 -17 0.71 2.22 8 -2 -17 2.01 3.72 -8 2 17 4.43 5.86 8 2 -17 5.04 5.59 4 -7 13 15.06 11.17 -4 -7 -13 23.34 6.68 -4 7 -13 26.45 6.96 4 7 13 16.29 7.66 -19 7 8 52.40 8.71 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1.74 3.81 19 -5 -1 33.28 15.52 -19 -5 1 36.41 17.22 -19 5 1 34.48 18.46 -19 5 1 23.97 10.16 -19 -5 1 34.82 11.37 19 5 -1 34.29 16.64 10 -12 -12 20.20 6.28 10 -12 -12 5.82 15.30 -10 12 12 9.50 11.11 -10 -12 12 11.60 8.88 -10 -12 12 19.57 9.11 -16 2 15 7.94 7.24 -16 -2 15 8.63 6.12 16 -2 -15 8.87 5.87 16 2 -15 18.10 8.06 -16 2 15 -2.68 6.41 -2 17 5 5.66 8.68 2 17 -5 15.11 6.39 -2 -17 5 10.49 8.68 2 -17 -5 11.70 5.37 2 -17 -5 14.61 4.51 -2 -17 5 13.00 7.39 -5 10 -11 123.59 15.65 5 -10 11 119.09 26.66 5 10 11 119.74 35.70 -5 -10 -11 91.08 9.12 7 2 -17 4.31 3.14 7 -2 -17 4.79 3.60 -7 -2 17 2.30 6.90 7 2 -17 4.73 7.99 -7 2 17 7.16 4.81 -7 2 17 3.96 5.03 2 15 -9 2.37 2.58 -2 -15 9 6.61 8.18 -2 -15 9 0.33 1.88 2 -15 -9 5.08 7.12 2 -15 -9 3.09 3.45 -2 15 9 2.50 8.61 3 17 -5 4.78 6.13 -3 17 5 4.91 8.04 -3 -17 5 1.79 3.43 3 -17 -5 -0.47 5.54 -3 -17 5 6.77 5.48 3 -17 -5 11.31 5.90 20 -3 -10 0.46 6.94 -20 -3 10 5.10 6.67 -20 3 10 -3.67 7.99 -20 -3 10 1.45 3.10 -20 3 10 6.68 7.51 20 3 -10 16.25 8.60 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15.95 17 5 3 32.38 9.38 17 -5 3 34.51 17.60 -10 13 11 18.60 10.01 10 -13 -11 9.53 7.53 10 -13 -11 14.66 9.54 -10 -13 11 18.96 12.74 -10 -13 11 20.45 7.60 -11 0 17 2.69 3.39 -11 0 17 1.82 3.86 11 0 -17 4.50 4.81 9 -14 -10 2.98 8.94 9 -14 -10 8.30 5.02 -9 14 10 14.47 8.86 -9 -14 10 9.54 5.23 -9 -14 10 5.06 4.68 -13 -4 -8 73.10 6.50 -13 4 -8 72.27 14.28 -13 -4 -8 79.89 29.27 13 -4 8 73.42 7.76 -21 1 7 19.71 8.06 -21 -1 7 19.56 9.07 21 1 -7 16.39 8.66 21 -1 -7 17.90 6.19 -21 -1 7 17.67 7.19 -21 1 6 297.51 18.97 -21 -1 6 303.98 19.66 21 1 -6 313.62 20.83 21 -1 -6 316.45 20.63 -21 -1 6 322.36 21.55 -21 1 6 376.28 23.78 -20 5 4 6.74 4.61 20 5 -4 4.72 4.75 20 -5 -4 2.55 4.03 -20 -5 4 5.92 6.58 -20 5 4 2.57 5.83 -20 -5 4 -0.53 4.22 -17 6 13 38.98 25.47 -17 6 13 33.58 11.17 17 6 -13 30.78 11.55 17 -6 -13 29.34 11.67 -17 -6 13 42.45 20.89 -11 14 -2 13.86 7.65 11 -14 2 14.37 9.60 11 -14 2 4.52 3.29 -11 -14 -2 12.74 11.07 11 14 2 4.82 3.01 11 14 2 7.21 5.11 -20 3 2 12.02 6.55 -20 -3 2 37.38 9.50 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19.25 9.35 5 -17 -6 6.69 6.16 4 -10 12 3.85 4.47 -4 10 -12 4.66 5.53 -4 -10 -12 7.94 4.98 4 10 12 4.17 7.57 0 7 -15 127.40 8.47 0 -7 15 149.70 11.58 0 -7 -15 128.37 11.71 0 7 15 171.94 13.88 -20 3 1 51.65 13.10 -20 -3 1 73.31 10.45 -20 3 1 57.78 10.70 20 3 -1 45.41 20.33 20 -3 -1 57.83 8.34 -20 -3 1 67.12 8.76 11 -9 8 9.84 6.09 -11 9 -8 11.89 11.51 -11 -9 -8 9.32 6.44 -11 -9 -8 2.58 4.15 9 -15 -9 32.85 16.48 9 -15 -9 22.32 8.86 -9 15 9 61.33 16.65 -9 -15 9 44.99 10.67 -9 -15 9 33.45 10.35 -17 2 15 9.26 6.07 -17 2 15 4.88 7.04 -17 -2 15 15.25 8.27 17 -2 -15 7.97 5.77 17 2 -15 3.07 6.04 15 -13 -4 3.66 5.12 -15 13 4 4.45 9.02 15 -13 -4 0.62 2.45 15 13 -4 7.11 7.29 -15 -13 4 -0.14 2.94 -15 -13 4 5.32 4.62 14 -9 5 28.04 11.83 -14 9 -5 19.12 7.85 -14 -9 -5 19.31 9.57 -14 -9 -5 20.61 8.74 20 -5 -10 61.09 19.65 -20 -5 10 59.53 33.64 -20 -5 10 62.85 20.78 -20 5 10 59.51 30.80 -20 5 10 84.24 15.60 20 5 -10 88.13 27.24 3 -1 -17 35.69 7.74 3 -1 -17 45.09 12.96 3 -1 -17 40.02 5.78 3 1 -17 24.97 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39.23 16.19 -15 3 16 61.69 12.12 15 -3 -16 33.47 12.22 13 0 -17 -1.50 5.69 -13 0 17 3.66 5.21 -13 0 17 2.42 4.45 15 -13 -6 7.02 4.05 -15 13 6 8.09 7.97 15 -13 -6 14.39 8.56 -15 -13 6 8.99 11.11 -15 -13 6 5.41 3.14 6 -10 11 10.28 8.89 -6 10 -11 3.27 2.82 -6 -10 -11 11.11 5.08 6 10 11 7.84 6.45 -2 18 3 19.58 20.13 -2 -18 3 23.18 16.50 2 -18 -3 28.11 12.90 -2 -18 3 37.78 14.52 2 -18 -3 18.09 12.49 2 18 -3 20.68 11.12 -14 -1 -8 6.17 9.95 -14 1 -8 1.53 4.35 14 1 8 1.92 2.01 14 -1 8 2.62 3.42 -5 -11 14 43.13 9.62 5 -11 -14 34.67 6.06 5 -11 -14 42.36 11.81 -5 -11 14 37.21 12.14 -5 11 14 29.50 8.02 -21 0 10 9.72 11.03 -21 0 10 9.30 3.69 21 0 -10 11.37 9.22 -15 -1 -7 12.05 5.00 15 -1 7 7.19 4.35 15 1 7 8.98 6.24 -15 1 -7 15.30 9.52 -15 -1 -7 10.97 8.44 -21 0 3 10.39 6.46 -21 0 3 0.85 4.45 21 0 -3 2.47 3.58 -7 -16 8 44.10 8.57 7 -16 -8 50.19 18.51 -7 -16 8 51.20 16.63 -7 16 8 67.19 15.69 7 -16 -8 38.72 16.58 -20 4 11 27.47 27.89 -20 -4 11 25.33 22.17 20 -4 -11 23.64 10.88 20 4 -11 27.99 10.00 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16.67 18 10 -6 78.88 10.70 -18 -10 6 86.98 19.81 -2 -14 11 7.08 7.47 -2 -14 11 10.31 3.58 -2 14 11 17.75 9.22 2 14 -11 12.60 4.13 2 -14 -11 12.70 9.37 7 -13 8 1.95 5.74 -7 13 -8 -1.29 6.10 -7 -13 -8 -1.00 5.68 7 13 8 -1.53 6.51 -15 11 11 75.27 38.15 -15 11 11 86.28 19.78 15 -11 -11 76.93 10.93 -15 -11 11 90.28 23.41 -15 -11 11 77.34 10.55 7 -17 -5 5.45 4.74 -7 17 5 9.87 13.06 7 -17 -5 12.58 7.89 -7 -17 5 3.41 6.89 7 17 -5 2.99 1.57 -7 -17 5 -0.97 4.71 7 -9 11 31.28 12.68 -7 9 -11 21.23 15.74 7 9 11 26.49 9.80 -7 -9 -11 19.48 16.77 -9 1 -12 393.83 16.85 -9 -1 -12 433.06 25.01 9 -1 12 402.56 15.42 -9 -1 -12 396.95 12.85 18 -10 -5 18.70 10.12 -18 10 5 25.45 16.13 -18 10 5 14.88 8.05 -18 -10 5 15.76 9.47 18 10 -5 36.67 7.97 -18 -10 5 20.79 9.32 -4 -7 16 3.41 5.23 4 -7 -16 7.33 9.08 -4 -7 16 -0.26 2.75 -4 7 16 2.31 5.96 4 -7 -16 0.61 1.30 3 -3 15 70.00 7.82 -3 -3 -15 79.04 22.45 -3 3 -15 74.85 9.04 -3 -3 -15 68.19 11.27 -16 -5 -5 134.49 16.71 -16 5 -5 100.48 18.53 -16 -5 -5 89.29 13.40 16 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7.49 -15 -13 2 33.82 18.64 15 13 -2 33.57 6.96 -10 5 17 10.53 9.62 10 -5 -17 8.82 5.36 -10 -5 17 3.65 5.68 -10 5 17 -1.02 6.02 -1 -14 11 22.55 28.88 1 14 -11 20.41 12.83 -1 14 11 22.21 17.78 1 -14 -11 25.72 9.74 19 -6 0 73.85 24.30 -19 6 0 44.70 12.38 -19 6 0 79.92 7.26 19 6 0 60.43 21.62 -19 -6 0 61.23 10.15 -19 -6 0 64.56 8.14 -20 3 12 49.45 10.69 -20 -3 12 47.51 32.26 20 -3 -12 59.67 10.86 20 3 -12 38.09 14.90 -20 3 12 31.51 13.40 -20 -3 12 43.22 13.16 -8 -16 8 12.19 5.47 8 -16 -8 -0.05 4.63 8 -16 -8 5.50 6.46 -8 -16 8 4.69 3.88 -8 16 8 2.77 5.44 19 -4 -13 3.66 6.49 -19 4 13 6.25 5.80 -19 4 13 -0.89 6.45 -19 -4 13 7.13 13.06 19 4 -13 8.72 8.26 12 0 10 109.80 7.14 -12 0 -10 74.30 18.70 -16 -12 8 -1.11 4.71 16 -12 -8 8.69 8.93 16 12 -8 3.78 5.15 -16 12 8 -2.97 4.49 -16 12 8 4.80 4.23 -12 -8 -8 15.09 13.03 12 -8 8 9.49 7.29 -12 8 -8 34.48 9.44 -12 -8 -8 16.45 6.42 2 -14 10 4.10 7.87 2 14 10 13.05 10.71 -2 -14 -10 5.37 3.21 -2 14 -10 7.76 4.44 -7 4 -13 3.12 4.20 -7 -4 -13 1.08 3.37 7 -4 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15.91 8.72 -19 -6 12 12.56 6.43 -19 6 12 9.58 8.22 -2 -9 15 0.02 5.67 2 -9 -15 3.12 5.55 2 9 -15 7.16 3.26 -2 9 15 4.42 7.16 -21 -5 7 79.42 8.24 -21 5 7 60.88 10.24 -21 -5 7 61.82 13.30 21 5 -7 37.92 20.48 21 -5 -7 51.96 9.07 -21 5 7 54.72 11.31 21 -5 -6 45.43 8.34 -21 -5 6 26.91 16.03 -21 5 6 30.60 19.93 -21 5 6 31.95 17.81 -21 -5 6 37.62 8.64 21 5 -6 44.07 8.00 0 18 -4 2.89 2.55 0 -18 -4 3.91 7.78 0 -18 4 8.64 7.88 0 -18 4 4.10 6.12 0 18 4 24.24 9.75 0 -18 -4 15.69 8.10 -17 -4 15 16.99 13.50 -17 4 15 16.73 6.57 17 4 -15 1.88 7.32 -17 4 15 13.65 14.98 -20 -7 4 21.96 7.07 -20 7 4 19.10 11.51 20 7 -4 26.92 8.55 -20 7 4 23.50 7.99 20 -7 -4 13.69 7.78 -20 -7 4 19.54 13.19 -21 0 11 5.82 6.14 21 0 -11 7.37 7.08 -21 0 11 -3.78 6.23 -6 14 -8 16.37 7.75 -6 -14 -8 29.36 9.31 6 14 8 1.18 5.47 6 -14 8 4.87 6.93 -4 -1 -15 2.32 7.40 4 -1 15 8.68 4.94 4 1 15 1.72 2.22 -4 -1 -15 1.91 2.02 -4 1 -15 8.05 5.97 -21 0 2 74.11 15.54 21 0 -2 92.76 10.75 -21 0 2 72.98 15.41 2 -15 9 26.08 8.65 -2 15 -9 51.00 10.24 -2 -15 -9 51.19 10.46 2 15 9 49.51 37.18 -7 15 -6 43.33 24.65 -7 -15 -6 41.84 10.22 7 15 6 41.73 11.06 7 -15 6 34.33 11.90 -1 3 -16 8.27 4.47 -1 -3 -16 11.15 6.15 1 -3 16 3.02 3.21 -1 -3 -16 0.79 2.67 2 -2 -17 40.29 7.86 2 2 -17 36.87 8.29 2 2 -17 28.54 4.82 2 -2 -17 40.53 8.55 -2 -2 17 48.65 7.90 2 -2 -17 48.86 7.78 -3 -16 9 1.59 2.32 3 16 -9 2.56 3.26 -3 16 9 6.72 7.83 3 -16 -9 0.73 6.93 -3 -16 9 1.77 3.81 3 -16 -9 0.48 3.00 -5 -17 7 31.15 8.55 5 -17 -7 29.79 11.51 -5 -17 7 26.52 13.42 5 -17 -7 38.38 11.95 -5 17 7 38.68 10.87 5 17 -7 26.45 12.60 14 -1 -17 9.71 8.52 -14 -1 17 17.20 7.18 -14 1 17 3.01 4.72 -14 1 17 13.45 7.87 14 1 -17 0.70 5.50 13 -11 -13 114.09 15.57 -13 -11 13 121.08 21.81 -13 -11 13 106.90 37.23 13 -11 -13 107.36 11.93 -13 11 13 141.21 27.01 -10 12 -7 -1.31 5.66 -10 -12 -7 2.10 5.70 10 -12 7 5.31 8.93 10 12 7 11.70 9.27 -14 -14 2 86.97 19.88 14 -14 -2 88.34 8.85 14 -14 -2 89.62 32.28 14 14 -2 89.20 9.97 -14 14 2 57.22 37.85 -14 -14 2 91.19 14.45 1 -11 13 71.12 38.08 -1 -11 -13 85.60 13.02 -1 11 -13 61.63 14.06 1 11 13 75.56 13.72 -1 -7 -15 3.17 8.43 -1 7 -15 14.19 4.41 1 7 15 12.50 7.63 1 -7 15 9.12 6.94 13 -3 9 26.82 12.45 -13 -3 -9 27.76 5.43 -13 -3 -9 37.91 8.36 -13 3 -9 37.89 15.90 -11 11 -7 41.80 12.01 11 11 7 19.21 11.52 11 -11 7 41.27 17.45 -11 -11 -7 23.07 10.52 6 17 3 14.30 5.90 -6 17 -3 12.93 9.16 6 -17 3 17.08 9.16 -6 -17 -3 21.95 12.50 -6 -17 -3 13.72 7.32 6 -17 3 20.04 14.93 -5 -18 3 129.90 16.46 5 -18 -3 118.76 17.40 -5 -18 3 136.49 18.11 5 -18 -3 124.67 11.54 -5 18 3 141.41 18.41 5 18 -3 112.62 19.74 12 -2 10 19.98 8.72 -12 -2 -10 24.49 10.20 -12 -2 -10 35.27 13.05 -12 2 -10 36.26 17.83 -5 8 16 8.57 8.21 5 -8 -16 7.89 4.22 -5 -8 16 16.44 8.59 5 -8 -16 11.19 6.40 -5 -8 16 11.65 6.07 -19 1 14 306.61 24.15 19 1 -14 282.05 20.63 19 -1 -14 284.71 20.56 -19 -1 14 269.10 19.96 -19 1 14 242.94 14.23 -19 -1 14 288.92 13.04 -11 -5 17 209.45 13.13 -11 5 17 235.32 13.56 -11 5 17 160.77 12.88 11 -5 -17 193.19 19.63 11 5 -17 210.63 18.36 16 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3.27 -17 -2 -5 58.90 10.06 -17 -2 -5 61.40 22.45 -17 2 -5 34.00 10.62 17 -2 5 45.74 11.79 17 2 5 64.09 17.31 -19 -5 -1 104.36 12.42 19 -5 1 106.25 9.76 -19 5 -1 114.62 18.21 -19 -5 -1 96.64 9.52 -19 5 -1 107.46 33.81 19 5 1 111.31 8.80 -13 11 -5 71.37 10.74 -13 -11 -5 69.70 16.10 13 -11 5 55.57 22.74 -13 -11 -5 61.40 27.68 -16 -9 -3 8.38 4.80 -16 -9 -3 9.91 5.59 16 -9 3 12.55 13.60 -16 9 -3 8.33 6.89 -16 -6 -5 21.10 10.59 16 -6 5 28.85 12.05 -16 -6 -5 20.25 10.12 -16 6 -5 27.32 7.65 -5 10 15 41.09 10.21 5 -10 -15 45.14 4.63 -5 -10 15 42.98 9.74 5 -10 -15 35.38 9.29 -5 -10 15 33.62 15.73 5 -16 6 11.44 9.80 -5 16 -6 6.05 10.31 -5 -16 -6 8.87 7.25 5 16 6 3.66 5.77 -10 8 16 3.21 3.84 -10 -8 16 6.60 4.79 -10 -8 16 5.73 3.50 10 -8 -16 6.81 5.65 2 6 15 188.94 15.15 -2 6 -15 128.33 16.67 -2 -6 -15 124.82 17.79 2 -6 15 143.44 10.47 -5 17 -4 116.61 18.08 5 17 4 108.47 14.15 -5 -17 -4 115.55 22.40 5 -17 4 88.02 16.99 -5 -17 -4 126.56 16.28 5 -17 4 103.70 14.79 15 -13 -8 8.81 8.02 -15 13 8 14.23 9.15 -15 -13 8 7.87 7.71 15 -13 -8 10.28 8.83 -15 -13 8 3.00 2.66 16 -10 2 51.78 25.68 -16 -10 -2 52.26 16.38 -16 10 -2 40.42 17.13 -16 -10 -2 58.43 9.15 -8 -6 -12 63.55 8.04 -8 6 -12 77.55 13.28 -8 -6 -12 67.47 30.79 8 -6 12 69.57 16.41 -11 16 2 13.55 7.99 -11 -16 2 9.26 7.09 11 16 -2 6.31 7.25 11 -16 -2 14.79 7.11 -11 -16 2 14.71 8.67 11 -16 -2 7.12 6.81 18 0 -15 7.99 11.13 -18 0 15 6.90 6.39 -18 0 15 -1.21 2.94 1 -17 -7 19.83 6.10 1 17 -7 14.07 10.32 -1 -17 7 16.70 9.47 -1 17 7 28.91 9.11 -1 -17 7 30.39 17.90 1 -17 -7 17.85 8.32 -13 12 12 90.94 15.61 13 -12 -12 86.37 14.05 -13 -12 12 104.82 35.05 -13 -12 12 115.89 18.65 13 -12 -12 65.95 38.86 -6 -16 9 58.30 29.57 -6 16 9 93.22 18.49 -6 -16 9 84.01 8.20 6 -16 -9 106.96 18.99 6 -16 -9 90.84 12.83 -9 10 15 56.39 21.57 -9 -10 15 39.27 22.17 -9 -10 15 50.62 13.85 9 -10 -15 50.75 29.89 9 -10 -15 54.94 7.01 -7 17 -2 83.68 39.73 -7 -17 -2 136.36 7.92 7 17 2 106.46 31.49 -7 -17 -2 95.75 15.89 7 -17 2 131.81 23.83 7 -17 2 116.67 16.00 19 -8 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91.23 21.97 21 2 -11 113.33 25.98 21 -2 -11 156.85 17.70 -21 2 2 3.46 3.86 -21 2 2 0.47 7.95 -21 -2 2 15.10 8.04 21 -2 -2 3.36 4.51 21 2 -2 8.16 5.68 -21 -2 2 3.10 3.74 6 17 -7 82.53 17.19 -6 17 7 60.07 13.55 6 -17 -7 87.82 19.66 -6 -17 7 87.36 25.81 -6 -17 7 62.75 28.82 6 -17 -7 79.54 13.98 5 8 13 29.13 15.55 -5 8 -13 25.63 6.19 -5 -8 -13 20.24 6.60 5 -8 13 16.02 14.70 -9 -17 2 71.94 27.38 9 17 -2 81.26 15.83 9 -17 -2 78.02 17.91 -9 -17 2 100.24 9.50 9 -17 -2 80.47 8.70 -9 17 2 61.85 31.80 -15 -13 1 42.24 12.48 -15 13 1 65.02 16.76 15 -13 -1 64.68 31.12 -15 -13 1 60.62 19.22 15 -13 -1 41.49 15.53 15 13 -1 60.02 8.14 13 -15 -5 30.46 12.57 -13 -15 5 22.55 9.69 -13 -15 5 32.60 16.94 13 -15 -5 20.08 11.35 -13 15 5 54.81 15.36 -13 -15 5 29.26 14.68 20 1 -13 16.71 7.86 -20 -1 13 11.05 10.01 -20 1 13 20.61 11.06 -20 1 13 19.45 9.02 -20 -1 13 27.55 11.84 20 -1 -13 25.36 10.07 13 -15 -3 79.57 8.61 -13 -15 3 92.74 17.41 13 15 -3 81.35 10.89 -13 15 3 65.31 13.19 13 -15 -3 103.15 14.57 -13 -15 3 92.81 9.48 -11 0 -11 4.20 5.42 12 -10 7 27.26 12.80 -12 -10 -7 26.76 6.63 -12 -10 -7 30.17 8.10 -12 10 -7 21.83 9.52 -18 -5 14 138.22 24.65 -18 5 14 122.12 12.09 -18 5 14 138.83 14.32 18 5 -14 100.93 35.63 18 -5 -14 146.38 14.71 -8 -1 -13 4.12 4.92 -8 1 -13 1.11 4.24 8 -1 13 1.78 3.74 13 -10 6 45.79 19.96 -13 -10 -6 52.43 23.36 -13 -10 -6 52.21 21.52 -13 10 -6 68.57 11.65 -6 -9 -12 1.93 5.15 6 9 12 5.69 11.06 6 -9 12 4.21 6.55 -6 9 -12 1.56 4.83 -9 -6 17 164.44 18.25 9 -6 -17 223.64 17.61 9 -6 -17 196.01 11.14 -9 -6 17 155.89 12.08 -9 6 17 162.33 28.33 -16 12 1 83.91 24.34 -16 -12 1 63.93 19.50 16 12 -1 84.95 8.61 16 -12 -1 68.24 32.91 -16 -12 1 80.28 22.03 16 -12 -1 71.03 22.47 -9 -16 8 183.28 11.47 9 -16 -8 171.66 30.94 -9 -16 8 191.07 14.13 9 -16 -8 158.21 24.92 -9 16 8 157.93 17.72 -4 -18 -2 29.07 14.44 4 18 2 34.30 9.69 -4 18 -2 9.54 6.84 4 -18 2 20.02 7.76 -4 -18 -2 22.76 8.53 4 -18 2 18.85 6.60 14 -8 -15 60.29 10.13 -14 -8 15 52.68 12.75 -14 8 15 58.46 29.67 -14 8 15 35.90 21.69 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9 159.21 12.31 13 -14 -9 163.87 16.35 -13 14 9 125.49 52.49 11 -13 -12 38.03 9.38 -11 -13 12 25.89 17.63 -11 13 12 27.33 10.96 11 -13 -12 28.80 10.21 -11 -13 12 25.69 6.89 -8 0 18 144.59 9.30 -8 0 18 169.13 15.56 8 0 -18 133.93 22.20 -10 -16 -1 36.42 10.79 10 16 1 33.52 18.11 10 -16 1 46.29 20.08 -10 -16 -1 37.66 7.33 -10 16 -1 39.40 28.50 10 -16 1 35.04 17.28 9 17 -4 6.55 3.86 -9 -17 4 6.41 4.92 9 -17 -4 11.61 6.83 -9 -17 4 7.51 5.36 9 -17 -4 7.87 7.88 -9 17 4 6.88 5.30 2 -3 -17 23.47 5.94 2 -3 -17 20.62 4.94 -2 -3 17 25.10 13.45 2 3 -17 15.79 7.23 2 3 -17 20.98 4.52 -2 3 17 21.92 17.81 -2 7 16 40.90 29.44 2 7 -16 38.99 11.63 2 -7 -16 43.50 16.28 -2 -7 16 37.35 14.94 18 0 4 409.18 20.34 -18 0 -4 361.72 22.09 -18 0 -4 392.45 18.29 -11 -1 -11 9.29 6.08 -11 1 -11 15.90 6.78 11 -1 11 11.79 6.84 -4 -17 -5 1.66 3.32 4 -17 5 5.49 8.16 4 17 5 3.36 4.80 -4 -17 -5 18.87 11.51 4 -17 5 3.06 5.12 -4 17 -5 7.10 4.91 -11 6 -10 112.22 18.55 -11 -6 -10 120.18 26.63 -11 -6 -10 114.63 17.40 11 -6 10 102.75 21.90 -9 -4 -12 121.07 7.69 -9 4 -12 159.68 19.36 -9 -4 -12 142.43 32.40 9 -4 12 142.56 9.50 5 18 -4 7.09 4.01 -5 18 4 15.73 10.62 -5 -18 4 2.11 3.62 5 -18 -4 5.50 5.65 -5 -18 4 3.79 4.36 5 -18 -4 4.51 4.96 -16 12 9 45.80 16.16 -16 12 9 51.89 12.86 16 -12 -9 42.94 16.23 16 12 -9 71.44 13.37 -16 -12 9 25.56 12.99 11 -11 -14 4.52 4.63 -11 11 14 3.32 9.73 -11 -11 14 6.10 4.14 11 -11 -14 11.17 10.17 -11 -11 14 6.14 9.74 -4 8 16 5.40 3.23 -4 -8 16 8.73 5.47 -4 -8 16 -1.84 2.59 4 -8 -16 1.91 5.55 19 -5 -13 148.25 17.41 19 5 -13 155.76 15.66 -19 -5 13 148.34 33.44 -19 5 13 93.85 9.89 -19 5 13 107.38 25.23 9 0 -18 15.98 7.17 -9 0 18 4.35 4.92 -9 0 18 12.23 8.37 6 -15 7 7.41 7.80 -6 15 -7 7.12 6.05 -6 -15 -7 1.44 6.62 6 15 7 11.67 6.50 -12 3 -10 84.83 14.71 -12 -3 -10 81.74 7.71 12 -3 10 92.07 10.78 -12 -3 -10 107.89 11.28 -12 14 10 14.65 9.86 12 -14 -10 1.15 4.23 -12 -14 10 -0.38 5.10 12 -14 -10 2.19 5.67 -12 -14 10 4.94 4.81 -4 -10 15 0.02 1.16 4 -10 -15 1.27 5.75 -4 10 15 0.95 4.26 -4 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86.41 11.35 -4 18 7 48.93 28.27 4 18 -7 59.77 9.97 -4 -18 7 60.07 8.93 4 -18 -7 44.82 24.09 -10 11 -9 24.64 7.00 10 -11 9 31.67 11.61 -10 -11 -9 21.35 10.04 10 11 9 48.50 24.98 -17 -6 -5 15.39 6.97 -17 -6 -5 8.65 10.42 -17 6 -5 26.46 8.07 17 -6 5 8.82 9.14 3 -17 -9 5.32 4.67 -3 -17 9 2.46 3.38 -3 -17 9 4.47 8.83 3 -17 -9 4.34 6.90 -3 17 9 11.55 7.88 12 16 0 3.49 6.72 -12 -16 0 -0.24 2.86 12 -16 0 2.94 4.35 -12 -16 0 3.57 4.40 -12 16 0 6.39 8.30 12 -16 0 4.25 4.34 -12 1 -11 17.35 9.27 -12 -1 -11 6.99 9.15 17 -3 6 2.57 3.47 -17 3 -6 4.05 6.63 -17 -3 -6 9.16 6.24 -17 -3 -6 2.68 1.71 -11 -8 -10 8.26 5.11 -11 -8 -10 9.60 9.04 -11 8 -10 7.50 4.36 11 -8 10 8.67 5.53 -11 -11 15 183.98 14.31 11 -11 -15 189.90 11.42 -11 11 15 167.77 35.39 -11 -11 15 206.49 11.82 11 -11 -15 224.72 15.84 -20 -2 -2 121.83 8.75 20 -2 2 96.66 10.96 20 2 2 91.25 16.98 -20 2 -2 116.02 14.91 -20 -2 -2 87.08 23.40 -20 2 -2 103.81 7.88 -14 1 18 64.72 11.13 -14 -1 18 52.82 8.99 14 -1 -18 67.48 29.07 14 1 -18 73.63 11.92 -6 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6.05 5 -18 -8 7.43 3.99 -2 16 11 11.79 8.67 2 -16 -11 15.42 6.49 -2 -16 11 -0.04 5.48 -10 2 19 44.81 19.49 10 2 -19 69.13 13.51 10 -2 -19 41.03 20.77 -10 -2 19 53.47 25.12 -10 2 19 66.68 16.57 -15 -12 13 1.20 5.35 15 -12 -13 9.33 6.68 15 -12 -13 -1.91 4.29 -15 -12 13 5.59 7.38 -15 12 13 7.82 9.08 11 -9 10 10.35 5.59 -11 9 -10 5.66 7.26 -11 -9 -10 11.36 10.38 -11 -9 -10 0.35 3.79 -10 12 15 41.26 31.39 -10 -12 15 25.00 16.09 10 -12 -15 29.35 16.98 -10 -12 15 35.73 21.37 10 -12 -15 30.06 17.05 -5 -6 18 17.40 9.52 -5 6 18 9.39 8.91 5 -6 -18 14.99 10.64 -5 -6 18 19.55 13.06 3 -12 13 43.45 18.60 -3 12 -13 27.35 14.37 -3 -12 -13 48.69 10.29 3 12 13 32.14 17.31 -13 -5 -10 -0.64 5.98 -13 -5 -10 5.30 2.69 -13 5 -10 3.99 5.19 13 -5 10 3.70 3.89 15 -15 -7 3.45 5.12 -15 15 7 9.86 15.69 15 -15 -7 -2.54 4.76 -15 -15 7 6.13 3.78 -15 -15 7 6.36 4.76 23 0 -4 191.59 22.75 -23 0 4 194.40 16.72 -23 0 4 151.24 30.59 13 -11 -15 26.71 10.74 -13 11 15 18.13 7.87 13 -11 -15 38.20 13.42 -13 -11 15 30.18 6.67 -13 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2.12 4.97 -17 5 17 4.54 4.39 -17 5 17 12.88 10.45 17 -5 -17 8.56 7.48 17 5 -17 -0.07 6.66 -17 -5 17 2.20 6.21 -6 -15 13 2.03 2.43 -6 -15 13 9.33 6.95 6 -15 -13 10.68 6.83 -6 15 13 -0.38 8.30 -10 -3 -13 47.30 9.25 -10 3 -13 32.96 13.98 10 -3 13 52.48 15.03 -7 18 -4 4.81 4.71 7 18 4 8.18 7.63 7 -18 4 1.68 6.53 -7 -18 -4 4.84 5.34 4 -8 15 79.68 9.63 4 8 15 65.32 20.59 -4 8 -15 68.79 8.38 -4 -8 -15 79.61 10.85 20 10 -10 9.16 8.49 -20 10 10 4.96 5.32 -20 -10 10 5.98 6.50 20 -10 -10 14.75 8.34 -20 10 10 4.43 7.39 23 5 -7 6.65 5.01 23 -5 -7 5.11 5.87 -23 5 7 7.08 8.47 -23 -5 7 0.84 3.69 -23 -5 7 1.71 5.32 -23 5 7 10.79 6.36 -1 -20 -2 36.98 12.22 1 -20 2 51.47 13.34 1 20 2 33.24 21.69 -1 20 -2 44.70 9.55 -1 -20 -2 34.90 18.13 1 -20 2 49.92 11.24 -18 3 17 13.75 7.71 18 -3 -17 20.11 10.79 -18 -3 17 30.74 18.30 18 3 -17 13.25 7.44 -18 3 17 19.74 8.92 -12 -10 -9 53.89 16.55 12 -10 9 56.54 20.85 -12 10 -9 53.65 18.47 -12 -10 -9 52.04 23.88 -14 8 17 5.70 6.09 14 -8 -17 4.16 5.08 14 8 -17 6.72 4.82 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18.50 7.04 17 5 -22 14.77 7.17 -17 -5 22 11.60 10.96 -17 5 22 11.07 4.66 -3 -13 19 3.43 5.98 3 -13 -19 2.92 5.03 -3 13 19 3.66 5.34 23 -11 1 4.08 9.10 -23 11 -1 5.26 16.43 -23 -11 -1 5.05 5.00 -23 -11 -1 8.73 7.89 11 -8 -22 3.38 5.70 -11 8 22 5.51 5.50 11 8 -22 9.38 7.16 16 -20 -6 3.22 3.89 -16 20 6 7.53 10.46 16 -20 -6 5.18 6.91 -16 -20 6 3.35 5.82 -16 -20 6 2.62 4.71 11 -4 -23 1.70 4.04 11 4 -23 2.58 4.85 -27 2 15 8.68 6.76 27 -2 -15 6.25 10.67 -27 -2 15 9.41 8.20 27 2 -15 13.23 9.51 10 -14 -19 12.49 10.07 -10 -14 19 -0.31 5.87 -10 14 19 0.56 7.28 -13 3 -15 3.10 5.32 -13 -3 -15 2.36 4.79 -15 0 23 5.27 6.95 15 0 -23 2.67 5.28 15 -20 -9 7.36 5.80 15 -20 -9 3.81 7.06 -15 20 9 10.39 7.29 -15 -20 9 1.86 4.84 -15 -20 9 5.53 5.14 19 -18 -7 3.38 7.29 -19 18 7 2.34 12.32 19 -18 -7 5.21 4.99 19 18 -7 1.32 4.23 -19 -18 7 1.33 3.93 -10 -22 8 5.37 4.01 10 -22 -8 1.56 4.52 10 -22 -8 5.72 5.61 -10 22 8 4.15 7.27 -10 -22 8 5.20 4.39 15 -17 -15 25.46 10.38 -15 17 15 5.28 4.43 15 -17 -15 2.03 3.69 -15 -17 15 0.38 4.18 -15 -17 15 6.15 5.35 -16 -6 22 2.58 4.83 -16 6 22 -1.67 6.07 16 6 -22 6.66 6.34 16 -6 -22 8.04 5.50 25 -10 -13 16.51 13.84 -25 10 13 42.50 14.09 -25 10 13 44.83 10.04 25 10 -13 21.31 8.63 -25 -10 13 31.60 16.16 25 7 -16 -2.17 7.09 -25 -7 16 9.54 8.59 -25 7 16 13.50 9.79 -25 7 16 2.35 5.94 25 -7 -16 15.87 9.54 10 -4 -23 13.76 5.26 10 4 -23 9.29 6.91 -9 17 -11 9.96 8.65 9 -17 11 2.73 7.17 9 17 11 8.79 9.00 -9 -17 -11 13.09 7.00 24 -12 -12 14.01 7.87 -24 12 12 4.05 8.19 -24 12 12 12.94 12.04 24 12 -12 7.24 6.54 -24 -12 12 5.71 9.04 -2 -7 -20 5.48 4.37 2 -7 20 23.39 8.17 -13 -10 -13 11.50 8.70 13 -10 13 8.57 5.91 -13 -10 -13 33.23 10.23 -13 10 -13 13.27 12.89 -24 9 -1 64.71 23.59 -24 -9 -1 43.42 27.11 -24 -9 -1 56.27 14.94 24 -9 1 40.57 21.52 -27 3 2 3.47 4.64 27 -3 -2 8.82 7.60 27 3 -2 9.54 4.25 -27 -3 2 6.63 4.57 27 -6 -4 8.93 8.66 27 6 -4 14.12 5.67 -27 6 4 13.16 9.95 -27 -6 4 13.23 6.86 -27 -6 4 12.88 7.14 -9 -8 22 10.01 8.16 -9 8 22 8.24 5.60 9 -8 -22 4.28 7.76 2 -3 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-21 -2 21 48.02 10.33 -21 2 21 20.51 15.06 -19 -3 -10 23.00 23.58 -19 3 -10 35.45 29.87 0 -24 3 60.08 14.80 0 24 3 36.12 27.21 0 24 -3 42.93 14.77 0 -24 3 57.75 20.95 0 -24 -3 71.21 10.61 -21 -2 -8 22.17 19.24 -21 2 -8 40.02 25.78 16 -11 10 4.27 7.42 -16 -11 -10 8.72 5.97 -16 -11 -10 4.16 2.98 -16 11 -10 3.69 6.50 -3 -16 17 43.40 24.26 -3 16 17 20.07 9.22 -8 -8 -17 58.49 10.14 -8 8 -17 61.30 16.00 17 -19 -9 17.99 8.09 -17 19 9 19.97 9.07 -17 -19 9 15.27 12.24 15 1 -23 13.49 5.45 -15 -1 23 6.41 7.05 -15 1 23 7.25 9.24 15 -1 -23 4.43 4.55 -2 -24 -2 17.48 8.74 2 -24 2 13.22 11.35 -2 24 -2 24.35 23.67 2 24 2 22.45 8.12 2 -24 2 23.61 8.68 5 -15 15 3.60 5.49 -5 -15 -15 1.96 3.32 5 15 15 14.06 12.38 -20 16 12 10.81 9.44 20 -16 -12 7.49 7.05 20 -16 -12 1.72 4.51 -20 -16 12 10.32 9.02 20 16 -12 11.85 12.59 -9 23 3 16.02 8.79 -9 -23 3 18.64 6.84 -9 -23 3 4.65 10.19 9 -23 -3 10.19 7.15 4 -24 -1 9.68 4.75 -4 -24 1 13.64 8.08 -4 24 1 10.23 12.42 4 24 -1 8.86 4.37 4 -24 -1 7.15 5.37 -4 -24 1 -0.20 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-10 10.88 9.23 9 -18 10 18.95 12.66 9 18 10 9.99 8.27 -1 7 21 7.87 5.41 -1 -7 21 1.55 3.73 -18 -7 -10 9.15 8.72 -18 7 -10 12.78 12.26 -12 18 15 4.77 6.35 -12 -18 15 1.81 4.25 -12 -18 15 5.56 5.25 -6 23 7 -0.64 6.86 -6 -23 7 -0.35 3.30 6 -23 -7 5.82 4.70 -6 -23 7 2.39 7.31 4 -24 -2 1.90 5.66 -4 24 2 2.05 6.97 -4 -24 2 3.62 5.22 -4 -24 2 2.43 4.46 -9 23 2 11.46 10.71 -9 -23 2 5.48 3.50 9 -23 -2 0.11 4.21 -22 14 1 4.33 10.66 22 -14 -1 4.45 6.96 -22 -14 1 3.29 4.82 -22 -14 1 7.57 7.07 -1 10 20 8.56 12.68 -24 10 15 9.14 11.00 -24 10 15 21.19 10.94 24 10 -15 2.55 7.33 -24 -10 15 1.99 3.96 24 -13 -9 25.85 25.39 -24 13 9 53.70 14.46 24 13 -9 72.63 12.87 -20 3 -9 21.12 8.92 -20 -3 -9 13.63 10.10 0 -15 17 3.76 6.42 0 -15 -17 7.53 10.02 0 15 17 14.78 8.05 19 -7 9 11.05 8.49 -19 -7 -9 8.75 8.85 -19 7 -9 35.53 9.94 -16 18 -3 91.93 30.29 -16 -18 -3 54.77 18.99 -16 -18 -3 49.57 33.60 26 -10 -8 15.55 11.15 -26 10 8 16.68 8.06 -26 -10 8 34.80 12.01 26 10 -8 13.60 6.80 -18 3 -11 6.47 9.57 -18 -3 -11 10.09 7.23 -12 22 3 -0.77 7.48 -12 -22 3 3.94 6.37 -15 -15 -8 6.47 7.41 -15 15 -8 5.04 6.86 -15 -15 -8 7.45 5.01 -20 13 -4 6.41 12.35 -20 -13 -4 11.81 13.58 -20 -13 -4 17.41 8.40 -23 14 10 22.91 28.31 23 -14 -10 29.48 13.27 23 -14 -10 30.93 8.30 23 14 -10 38.69 11.10 10 22 2 13.30 7.65 -10 -22 -2 6.96 6.22 -10 22 -2 4.81 5.98 -14 -16 -8 0.86 5.42 -14 -16 -8 11.61 10.02 -14 16 -8 7.87 9.56 -20 -9 -7 9.44 14.46 -20 -9 -7 19.50 7.26 -20 9 -7 36.51 11.06 2 -19 -14 11.64 5.99 -13 -12 -12 3.03 8.09 -13 -12 -12 5.72 4.07 -13 12 -12 3.85 4.24 -15 16 -7 30.96 10.43 -15 -16 -7 44.12 12.59 -15 -16 -7 23.84 12.45 7 15 14 9.37 13.49 -7 -15 -14 4.56 7.25 -24 6 -3 25.03 11.30 -24 -6 -3 1.77 5.22 -24 -6 -3 5.77 4.74 24 -6 3 3.94 5.62 -6 -21 -8 4.53 5.78 -6 21 -8 3.00 5.18 6 21 8 13.56 9.76 -6 -4 -19 0.49 7.10 -6 4 -19 1.93 3.32 -10 3 -17 0.98 6.14 -10 -3 -17 3.06 6.48 -22 8 -5 23.87 10.89 22 -8 5 5.23 4.95 -22 -8 -5 12.32 5.64 -24 11 1 -3.99 8.35 24 -11 -1 3.05 5.51 -24 -11 1 1.28 3.72 2 14 17 31.86 12.37 -2 -14 -17 20.54 10.81 9 -23 -4 -0.54 5.28 -2 8 21 1.95 4.52 -4 23 -5 14.70 8.35 -14 -21 2 10.50 6.37 -14 -5 -14 7.51 4.92 -14 5 -14 12.18 8.50 -11 11 -14 37.03 8.83 -11 -11 -14 14.40 9.74 -11 -11 -14 25.16 7.30 -9 16 -12 10.13 5.46 9 16 12 23.40 7.51 -9 -16 -12 21.67 13.29 -8 4 -18 17.64 17.44 -24 -3 -4 21.92 9.73 -24 3 -4 -0.39 5.91 -15 -20 0 4.00 6.29 -16 15 -7 7.95 8.38 -16 -15 -7 5.65 5.25 -16 -15 -7 8.13 6.80 -22 0 -7 6.52 6.30 -25 9 1 10.97 12.65 -25 -9 1 15.20 9.46 25 -9 -1 20.49 12.76 -25 -9 1 13.25 13.09 -26 10 7 18.31 14.83 14 19 4 1.42 4.30 27 7 -5 7.43 4.89 -27 -7 5 3.55 4.62 -27 -7 5 4.84 4.47 -27 7 5 -5.95 7.54 27 -7 -5 6.58 5.60 -23 12 0 5.99 11.01 -23 -12 0 9.10 4.34 -15 -6 -13 4.43 5.88 -15 6 -13 11.05 6.72 26 -9 -4 2.97 2.58 -26 9 4 5.09 9.42 -26 -9 4 4.32 6.32 -14 -15 -9 11.42 6.66 -14 15 -9 17.94 8.81 -25 11 4 12.64 14.78 -16 0 -13 5.23 6.55 -17 -7 -11 32.10 21.47 -17 7 -11 41.04 13.99 -20 12 -5 -1.70 6.91 -20 -12 -5 4.01 5.73 -19 -11 -7 7.86 5.76 -19 11 -7 7.62 7.66 -22 1 -7 6.41 8.79 -22 -1 -7 18.80 14.47 -20 7 -8 25.48 9.31 -20 -7 -8 21.51 8.78 -16 -1 -13 3.24 3.40 -16 1 -13 11.31 10.49 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 15894 _olex2_submission_special_instructions 'No special instructions were received'