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data_darr027
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   'P 21/c'
_symmetry_Int_Tables_number      14
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 x,y,z
2 -x,1/2+y,1/2-z
3 -x,-y,-z
4 x,1/2-y,1/2+z
_cell_length_a                   10.133(3)
_cell_length_b                   10.2962(16)
_cell_length_c                   21.998(5)
_cell_angle_alpha                90.00
_cell_angle_beta                 96.612(9)
_cell_angle_gamma                90.00
_cell_volume                     2279.82
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
Ga Ga 0.21030(2) 0.63496(2) 0.097059(9)
Cl1 Cl 0.13588(6) 0.66627(5) 0.18691(2)
Cl2 Cl 0.25034(5) 0.42816(5) 0.09273(2)
Cl3 Cl 0.05703(5) 0.69892(5) 0.02709(2)
Cl4 Cl 0.39031(5) 0.74696(5) 0.09198(3)
P P 0.01974(5) 0.42340(5) 0.25943(2)
N1 N 0.16377(16) 0.35968(15) 0.28379(7)
N2 N -0.02486(16) 0.34400(15) 0.19605(7)
C1 C 0.2968(2) 0.5185(2) 0.34860(10)
H1A H 0.3121 0.5659 0.3130
C2 C 0.3500(2) 0.5604(2) 0.40649(11)
H2A H 0.4018 0.6375 0.4106
C3 C 0.3277(2) 0.4906(2) 0.45810(10)
H3A H 0.3638 0.5202 0.4974
C4 C 0.2529(2) 0.3776(2) 0.45261(10)
H4A H 0.2385 0.3297 0.4882
C5 C 0.1988(2) 0.3340(2) 0.39514(9)
H5A H 0.1477 0.2565 0.3911
C6 C 0.22076(19) 0.40563(19) 0.34407(9)
C7 C 0.23641(19) 0.26452(18) 0.25350(9)
C8 C 0.3640(2) 0.2329(2) 0.27713(9)
H8A H 0.4048 0.2751 0.3128
C9 C 0.4337(2) 0.1367(2) 0.24777(11)
H9A H 0.5224 0.1158 0.2635
C10 C 0.3753(2) 0.0736(2) 0.19716(10)
H10A H 0.4232 0.0080 0.1787
C11 C 0.2440(2) 0.10459(19) 0.17169(9)
C12 C 0.1815(2) 0.03981(19) 0.11912(9)
H12A H 0.2275 -0.0274 0.1008
C13 C 0.0563(2) 0.07259(19) 0.09457(9)
H13A H 0.0157 0.0271 0.0598
C14 C -0.0135(2) 0.17354(19) 0.12034(9)
H14A H -0.1002 0.1965 0.1025
C15 C 0.04381(19) 0.23840(18) 0.17109(8)
C16 C 0.17308(19) 0.20454(18) 0.19941(9)
C17 C -0.2689(2) 0.3628(2) 0.18500(10)
H17A H -0.2704 0.3188 0.2229
C18 C -0.3872(2) 0.4022(2) 0.15105(11)
H18A H -0.4699 0.3851 0.1659
C19 C -0.3840(2) 0.4660(2) 0.09593(10)
H19A H -0.4648 0.4915 0.0727
C20 C -0.2634(2) 0.4933(2) 0.07423(9)
H20A H -0.2620 0.5382 0.0366
C21 C -0.1446(2) 0.4546(2) 0.10772(9)
H21A H -0.0617 0.4729 0.0933
C22 C -0.14972(19) 0.38882(19) 0.16258(8)

#END
