data_shelx _audit_creation_method 'SHELXL-2018/3' _shelx_SHELXL_version_number '2018/3' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C53 H58 Ge N4' _chemical_formula_weight 823.62 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Ge' 'Ge' 0.1547 1.8001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/n' _space_group_name_Hall '-P 2yn' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 13.9768(2) _cell_length_b 14.7308(3) _cell_length_c 22.7506(4) _cell_angle_alpha 90 _cell_angle_beta 91.1630(10) _cell_angle_gamma 90 _cell_volume 4683.14(14) _cell_formula_units_Z 4 _cell_measurement_temperature 200(2) _cell_measurement_reflns_used 9947 _cell_measurement_theta_min 2.19 _cell_measurement_theta_max 27.75 _exptl_crystal_description 'block' _exptl_crystal_colour 'red' _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.168 _exptl_crystal_F_000 1744 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.600 _exptl_crystal_size_mid 0.443 _exptl_crystal_size_min 0.236 _exptl_absorpt_coefficient_mu 0.692 _shelx_estimated_absorpt_T_min 0.681 _shelx_estimated_absorpt_T_max 0.854 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.6749 _exptl_absorpt_correction_T_max 0.7460 _exptl_absorpt_process_details 'SADABS, Bruker (2003)' _exptl_absorpt_special_details ? _diffrn_ambient_temperature 200(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source ? _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 42740 _diffrn_reflns_av_unetI/netI 0.0286 _diffrn_reflns_av_R_equivalents 0.0264 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_k_max 19 _diffrn_reflns_limit_l_min -29 _diffrn_reflns_limit_l_max 29 _diffrn_reflns_theta_min 1.647 _diffrn_reflns_theta_max 30.165 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.794 _diffrn_measured_fraction_theta_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.794 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.794 _diffrn_reflns_point_group_measured_fraction_full 1.000 _reflns_number_total 11015 _reflns_number_gt 8466 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'APEX II, Bruker (2009)' _computing_cell_refinement 'APEX II, Bruker (2009)' _computing_data_reduction 'XPREP, Bruker (2009)' _computing_structure_solution 'SHELXS-03 (Sheldrick, 2003)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics 'Mercury (Macrae et al., 2008)' _computing_publication_material 'CIFTAB (Sheldrick, 1997)' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0396P)^2^+1.7568P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 11015 _refine_ls_number_parameters 548 _refine_ls_number_restraints 108 _refine_ls_R_factor_all 0.0547 _refine_ls_R_factor_gt 0.0347 _refine_ls_wR_factor_ref 0.0900 _refine_ls_wR_factor_gt 0.0814 _refine_ls_goodness_of_fit_ref 1.018 _refine_ls_restrained_S_all 1.018 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ge1 Ge 0.32937(2) 0.30358(2) 0.73454(2) 0.02927(6) Uani 0.9547(4) 1 d . . P A 1 Ge2 Ge 0.3894(3) 0.2907(2) 0.73008(17) 0.02927(6) Uani 0.0453(4) 1 d . . P A 2 N1 N 0.39737(8) 0.14838(8) 0.65672(5) 0.0261(3) Uani 1 1 d . . . . . N2 N 0.24592(8) 0.15029(8) 0.68221(5) 0.0244(3) Uani 1 1 d . . . . . N3 N 0.19150(9) 0.26580(8) 0.73468(5) 0.0247(3) Uani 1 1 d . . . . . N4 N 0.51328(9) 0.23664(9) 0.69581(5) 0.0281(3) Uani 1 1 d . . . . . C1 C 0.33165(10) 0.19680(10) 0.68928(6) 0.0247(3) Uani 1 1 d . . . . . C2 C 0.35134(11) 0.07365(10) 0.63101(7) 0.0292(3) Uani 1 1 d . . . . . H2 H 0.380709 0.029383 0.606955 0.035 Uiso 1 1 calc R U . . . C3 C 0.25957(11) 0.07457(10) 0.64573(7) 0.0286(3) Uani 1 1 d . . . . . H3 H 0.212082 0.031887 0.633769 0.034 Uiso 1 1 calc R U . . . C4 C 0.16845(10) 0.18699(10) 0.70843(6) 0.0240(3) Uani 1 1 d . . . . . C5 C 0.07668(10) 0.13838(10) 0.71008(6) 0.0261(3) Uani 1 1 d . . . . . C6 C -0.01002(11) 0.18327(11) 0.70053(8) 0.0346(4) Uani 1 1 d . . . . . H6 H -0.010204 0.246006 0.690868 0.042 Uiso 1 1 calc R U . . . C7 C -0.09575(12) 0.13722(13) 0.70502(9) 0.0454(5) Uani 1 1 d . . . . . H7 H -0.154377 0.168656 0.698586 0.054 Uiso 1 1 calc R U . . . C8 C -0.09688(12) 0.04596(13) 0.71876(9) 0.0450(5) Uani 1 1 d . . . . . H8 H -0.156003 0.014717 0.721986 0.054 Uiso 1 1 calc R U . . . C9 C -0.01174(12) 0.00052(12) 0.72778(8) 0.0386(4) Uani 1 1 d . . . . . H9 H -0.012210 -0.062427 0.736840 0.046 Uiso 1 1 calc R U . . . C10 C 0.07434(11) 0.04594(11) 0.72371(7) 0.0317(3) Uani 1 1 d . . . . . H10 H 0.132612 0.013961 0.730262 0.038 Uiso 1 1 calc R U . . . C11 C 0.49356(10) 0.17278(10) 0.65911(6) 0.0251(3) Uani 1 1 d . . . . . C12 C 0.55889(10) 0.12660(10) 0.61798(7) 0.0269(3) Uani 1 1 d . . . . . C13 C 0.64763(11) 0.09446(11) 0.63786(8) 0.0324(3) Uani 1 1 d . . . . . H13 H 0.665619 0.099852 0.678200 0.039 Uiso 1 1 calc R U . . . C14 C 0.70947(12) 0.05468(13) 0.59865(9) 0.0437(4) Uani 1 1 d . . . . . H14 H 0.769730 0.032401 0.612265 0.052 Uiso 1 1 calc R U . . . C15 C 0.68408(14) 0.04722(14) 0.54001(9) 0.0484(5) Uani 1 1 d . . . . . H15 H 0.726937 0.020140 0.513276 0.058 Uiso 1 1 calc R U . . . C16 C 0.59663(14) 0.07902(13) 0.52016(8) 0.0442(4) Uani 1 1 d . . . . . H16 H 0.579196 0.073615 0.479730 0.053 Uiso 1 1 calc R U . . . C17 C 0.53396(12) 0.11885(11) 0.55885(7) 0.0349(4) Uani 1 1 d . . . . . H17 H 0.473807 0.140893 0.544883 0.042 Uiso 1 1 calc R U . . . C18 C 0.12506(10) 0.30929(10) 0.77249(6) 0.0237(3) Uani 1 1 d . . . . . C19 C 0.07564(10) 0.38690(10) 0.75247(7) 0.0259(3) Uani 1 1 d . . . . . C20 C 0.01191(11) 0.42759(11) 0.79038(7) 0.0313(3) Uani 1 1 d . . . . . H20 H -0.022177 0.480156 0.777833 0.038 Uiso 1 1 calc R U . . . C21 C -0.00299(12) 0.39329(11) 0.84594(7) 0.0350(4) Uani 1 1 d . . . . . H21 H -0.048773 0.420726 0.870615 0.042 Uiso 1 1 calc R U . . . C22 C 0.04883(12) 0.31899(11) 0.86558(7) 0.0345(4) Uani 1 1 d . . . . . H22 H 0.039281 0.296608 0.904183 0.041 Uiso 1 1 calc R U . . . C23 C 0.11480(11) 0.27633(11) 0.82980(7) 0.0295(3) Uani 1 1 d . . . . . C24 C 0.17490(13) 0.19854(12) 0.85380(8) 0.0395(4) Uani 1 1 d . . . . . H24 H 0.211463 0.172603 0.820408 0.047 Uiso 1 1 calc R U . . . C25 C 0.11387(17) 0.12294(14) 0.87877(10) 0.0579(6) Uani 1 1 d . . . . . H25A H 0.155434 0.074225 0.893742 0.087 Uiso 1 1 calc R U . . . H25B H 0.075612 0.146919 0.910878 0.087 Uiso 1 1 calc R U . . . H25C H 0.071232 0.098923 0.847776 0.087 Uiso 1 1 calc R U . . . C26 C 0.24749(16) 0.23431(17) 0.89924(10) 0.0599(6) Uani 1 1 d . . . . . H26A H 0.286145 0.183789 0.914608 0.090 Uiso 1 1 calc R U . . . H26B H 0.289293 0.278883 0.880689 0.090 Uiso 1 1 calc R U . . . H26C H 0.213621 0.263216 0.931561 0.090 Uiso 1 1 calc R U . . . C27 C 0.09209(11) 0.42603(11) 0.69178(7) 0.0317(3) Uani 1 1 d . . . . . H27 H 0.128365 0.380047 0.668797 0.038 Uiso 1 1 calc R U . . . C28 C 0.15281(16) 0.51160(15) 0.69600(10) 0.0586(6) Uani 1 1 d . . . . . H28A H 0.162685 0.535891 0.656485 0.088 Uiso 1 1 calc R U . . . H28B H 0.119966 0.557002 0.719770 0.088 Uiso 1 1 calc R U . . . H28C H 0.214875 0.497033 0.714472 0.088 Uiso 1 1 calc R U . . . C29 C -0.00070(14) 0.44658(14) 0.65801(8) 0.0477(5) Uani 1 1 d . . . . . H29A H 0.014171 0.471575 0.619330 0.072 Uiso 1 1 calc R U . . . H29B H -0.037749 0.390534 0.652999 0.072 Uiso 1 1 calc R U . . . H29C H -0.038193 0.490860 0.679977 0.072 Uiso 1 1 calc R U . . . C30 C 0.60608(10) 0.27428(10) 0.70426(7) 0.0276(3) Uani 1 1 d . . . . . C31 C 0.65261(11) 0.25737(11) 0.75861(7) 0.0332(4) Uani 1 1 d . . . . . C32 C 0.73838(12) 0.30221(13) 0.77081(8) 0.0415(4) Uani 1 1 d . . . . . H32 H 0.770499 0.292064 0.807425 0.050 Uiso 1 1 calc R U . . . C33 C 0.77749(13) 0.36079(13) 0.73102(9) 0.0471(5) Uani 1 1 d . . . . . H33 H 0.835929 0.391009 0.740241 0.056 Uiso 1 1 calc R U . . . C34 C 0.73205(13) 0.37558(12) 0.67797(9) 0.0423(4) Uani 1 1 d . . . . . H34 H 0.760340 0.415538 0.650529 0.051 Uiso 1 1 calc R U . . . C35 C 0.64571(12) 0.33376(11) 0.66315(7) 0.0334(4) Uani 1 1 d . . . . . C36 C 0.59663(14) 0.35555(13) 0.60496(8) 0.0421(4) Uani 1 1 d . . . . . H36 H 0.539194 0.315362 0.601022 0.051 Uiso 1 1 calc R U . . . C37 C 0.5615(2) 0.45327(17) 0.60472(12) 0.0851(9) Uani 1 1 d . . . . . H37A H 0.529888 0.466651 0.566876 0.128 Uiso 1 1 calc R U . . . H37B H 0.516027 0.461837 0.636459 0.128 Uiso 1 1 calc R U . . . H37C H 0.616068 0.494298 0.610679 0.128 Uiso 1 1 calc R U . . . C38 C 0.6608(2) 0.3357(2) 0.55334(10) 0.0808(8) Uani 1 1 d . . . . . H38A H 0.626693 0.350595 0.516525 0.121 Uiso 1 1 calc R U . . . H38B H 0.719007 0.372529 0.556808 0.121 Uiso 1 1 calc R U . . . H38C H 0.677949 0.271209 0.553423 0.121 Uiso 1 1 calc R U . . . C39 C 0.61021(13) 0.19337(13) 0.80318(8) 0.0417(4) Uani 1 1 d . . . . . H39 H 0.564434 0.152700 0.781440 0.050 Uiso 1 1 calc R U . . . C40 C 0.55342(17) 0.24492(19) 0.84831(10) 0.0693(7) Uani 1 1 d . . . . . H40A H 0.526786 0.202077 0.876588 0.104 Uiso 1 1 calc R U . . . H40B H 0.595515 0.288005 0.869054 0.104 Uiso 1 1 calc R U . . . H40C H 0.501205 0.278037 0.828496 0.104 Uiso 1 1 calc R U . . . C41 C 0.68498(16) 0.13281(14) 0.83321(10) 0.0561(5) Uani 1 1 d . . . . . H41A H 0.653701 0.092973 0.861474 0.084 Uiso 1 1 calc R U . . . H41B H 0.716805 0.095856 0.803590 0.084 Uiso 1 1 calc R U . . . H41C H 0.732499 0.170683 0.853863 0.084 Uiso 1 1 calc R U . . . C42 C 0.027(2) 0.4136(13) 0.4941(7) 0.083(5) Uani 0.54(3) 1 d D . P B 1 H42 H 0.046346 0.352281 0.489528 0.100 Uiso 0.54(3) 1 calc R U P B 1 C43 C 0.0965(11) 0.480(2) 0.4953(8) 0.096(6) Uani 0.54(3) 1 d D . P B 1 H43 H 0.162300 0.464336 0.492292 0.115 Uiso 0.54(3) 1 calc R U P B 1 C44 C 0.0678(16) 0.5688(19) 0.5010(6) 0.084(4) Uani 0.54(3) 1 d D . P B 1 H44 H 0.113280 0.616768 0.501491 0.100 Uiso 0.54(3) 1 calc R U P B 1 C45 C 0.0634(19) 0.4287(12) 0.4896(7) 0.067(4) Uani 0.46(3) 1 d D . P B 2 H45 H 0.106141 0.380276 0.481708 0.081 Uiso 0.46(3) 1 calc R U P B 2 C46 C 0.0963(12) 0.5145(17) 0.5017(10) 0.070(4) Uani 0.46(3) 1 d D . P B 2 H46 H 0.163221 0.525732 0.503867 0.084 Uiso 0.46(3) 1 calc R U P B 2 C47 C 0.033(2) 0.5843(9) 0.5107(7) 0.063(4) Uani 0.46(3) 1 d D . P B 2 H47 H 0.057310 0.643723 0.517290 0.075 Uiso 0.46(3) 1 calc R U P B 2 C48 C 0.3646(3) 0.3377(3) 0.50095(18) 0.0991(17) Uani 0.616(4) 1 d G . P C 1 H48 H 0.412322 0.383197 0.497500 0.119 Uiso 0.616(4) 1 calc R U P C 1 C49 C 0.3096(4) 0.3335(2) 0.55110(13) 0.0846(15) Uani 0.616(4) 1 d G . P C 1 H49 H 0.319734 0.376113 0.581925 0.101 Uiso 0.616(4) 1 calc R U P C 1 C50 C 0.2398(3) 0.2669(3) 0.55614(13) 0.0756(13) Uani 0.616(4) 1 d G . P C 1 H50 H 0.202239 0.263980 0.590419 0.091 Uiso 0.616(4) 1 calc R U P C 1 C51 C 0.2250(3) 0.2045(2) 0.51104(19) 0.0868(14) Uani 0.616(4) 1 d G . P C 1 H51 H 0.177330 0.158930 0.514489 0.104 Uiso 0.616(4) 1 calc R U P C 1 C52 C 0.2800(4) 0.2087(3) 0.46089(15) 0.0889(15) Uani 0.616(4) 1 d G . P C 1 H52 H 0.269917 0.166012 0.430064 0.107 Uiso 0.616(4) 1 calc R U P C 1 C53 C 0.3498(3) 0.2753(4) 0.45584(13) 0.0952(16) Uani 0.616(4) 1 d G . P C 1 H53 H 0.387413 0.278145 0.421569 0.114 Uiso 0.616(4) 1 calc R U P C 1 C54 C 0.3331(5) 0.3372(4) 0.5305(3) 0.0991(17) Uani 0.384(4) 1 d G . P C 2 H54 H 0.367373 0.387992 0.545691 0.119 Uiso 0.384(4) 1 calc R U P C 2 C55 C 0.2542(6) 0.3041(5) 0.5599(2) 0.0846(15) Uani 0.384(4) 1 d G . P C 2 H55 H 0.234524 0.332288 0.595218 0.101 Uiso 0.384(4) 1 calc R U P C 2 C56 C 0.2041(4) 0.2298(5) 0.5377(3) 0.0756(13) Uani 0.384(4) 1 d G . P C 2 H56 H 0.150120 0.207142 0.557761 0.091 Uiso 0.384(4) 1 calc R U P C 2 C57 C 0.2328(6) 0.1885(4) 0.4860(3) 0.0868(14) Uani 0.384(4) 1 d G . P C 2 H57 H 0.198565 0.137698 0.470777 0.104 Uiso 0.384(4) 1 calc R U P C 2 C58 C 0.3117(7) 0.2216(6) 0.4566(3) 0.0889(15) Uani 0.384(4) 1 d G . P C 2 H58 H 0.331413 0.193400 0.421248 0.107 Uiso 0.384(4) 1 calc R U P C 2 C59 C 0.3619(5) 0.2959(6) 0.4788(3) 0.0952(16) Uani 0.384(4) 1 d G . P C 2 H59 H 0.415818 0.318546 0.458704 0.114 Uiso 0.384(4) 1 calc R U P C 2 C60 C 1.0324(6) -0.0490(9) 0.5499(4) 0.1159(12) Uani 0.562(6) 1 d D . P D 1 H60 H 1.053655 -0.084142 0.582604 0.139 Uiso 0.562(6) 1 calc R U P D 1 C61 C 0.9909(7) 0.0327(10) 0.5570(5) 0.1159(12) Uani 0.562(6) 1 d D . P D 1 H61 H 0.984757 0.057869 0.595168 0.139 Uiso 0.562(6) 1 calc R U P D 1 C62 C 0.9573(5) 0.0798(6) 0.5077(6) 0.1159(12) Uani 0.562(6) 1 d D . P D 1 H62 H 0.925559 0.136006 0.513596 0.139 Uiso 0.562(6) 1 calc R U P D 1 C63 C 0.9976(11) -0.0061(11) 0.5570(6) 0.1159(12) Uani 0.438(6) 1 d D . P D 2 H63 H 0.995865 -0.013741 0.598424 0.139 Uiso 0.438(6) 1 calc R U P D 2 C64 C 0.9629(8) 0.0740(10) 0.5364(7) 0.1159(12) Uani 0.438(6) 1 d D . P D 2 H64 H 0.940484 0.121006 0.561225 0.139 Uiso 0.438(6) 1 calc R U P D 2 C65 C 0.9635(6) 0.0807(9) 0.4749(7) 0.1159(12) Uani 0.438(6) 1 d D . P D 2 H65 H 0.938936 0.132796 0.455128 0.139 Uiso 0.438(6) 1 calc R U P D 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ge1 0.02578(11) 0.02597(9) 0.03614(10) -0.00712(7) 0.00230(7) -0.00608(7) Ge2 0.02578(11) 0.02597(9) 0.03614(10) -0.00712(7) 0.00230(7) -0.00608(7) N1 0.0202(6) 0.0274(7) 0.0307(7) -0.0047(5) 0.0006(5) 0.0003(5) N2 0.0195(6) 0.0230(6) 0.0308(6) -0.0043(5) -0.0011(5) -0.0008(5) N3 0.0226(6) 0.0219(6) 0.0296(6) -0.0027(5) 0.0021(5) -0.0009(5) N4 0.0230(6) 0.0311(7) 0.0303(7) -0.0036(6) 0.0020(5) -0.0009(5) C1 0.0202(7) 0.0249(7) 0.0290(7) -0.0016(6) 0.0010(6) -0.0009(6) C2 0.0260(8) 0.0281(8) 0.0335(8) -0.0080(6) -0.0014(6) 0.0020(6) C3 0.0260(8) 0.0245(7) 0.0353(8) -0.0079(6) -0.0007(6) -0.0016(6) C4 0.0208(7) 0.0236(7) 0.0275(7) -0.0003(6) 0.0002(6) 0.0008(6) C5 0.0234(7) 0.0262(7) 0.0286(7) -0.0048(6) 0.0005(6) -0.0022(6) C6 0.0256(8) 0.0270(8) 0.0511(10) -0.0074(7) -0.0025(7) 0.0006(6) C7 0.0211(8) 0.0440(10) 0.0710(13) -0.0141(9) -0.0014(8) -0.0004(7) C8 0.0301(9) 0.0464(11) 0.0587(12) -0.0105(9) 0.0077(8) -0.0148(8) C9 0.0410(9) 0.0311(9) 0.0437(10) 0.0009(7) 0.0037(8) -0.0110(7) C10 0.0292(8) 0.0295(8) 0.0364(8) 0.0018(7) -0.0020(7) -0.0018(6) C11 0.0210(7) 0.0278(7) 0.0265(7) 0.0014(6) 0.0004(6) 0.0007(6) C12 0.0236(7) 0.0248(7) 0.0325(8) -0.0014(6) 0.0038(6) -0.0033(6) C13 0.0248(8) 0.0322(8) 0.0403(9) -0.0050(7) 0.0006(7) -0.0011(6) C14 0.0278(8) 0.0428(10) 0.0608(12) -0.0113(9) 0.0054(8) 0.0044(8) C15 0.0438(11) 0.0473(11) 0.0548(12) -0.0158(9) 0.0207(9) 0.0013(9) C16 0.0518(11) 0.0461(11) 0.0350(9) -0.0091(8) 0.0105(8) -0.0039(9) C17 0.0341(9) 0.0362(9) 0.0346(9) -0.0024(7) 0.0028(7) 0.0002(7) C18 0.0192(7) 0.0223(7) 0.0296(7) -0.0053(6) 0.0012(6) -0.0030(6) C19 0.0233(7) 0.0238(7) 0.0304(8) -0.0036(6) -0.0018(6) -0.0033(6) C20 0.0282(8) 0.0257(8) 0.0399(9) -0.0059(7) -0.0003(7) 0.0028(6) C21 0.0323(8) 0.0339(9) 0.0392(9) -0.0105(7) 0.0097(7) 0.0007(7) C22 0.0398(9) 0.0352(9) 0.0288(8) -0.0024(7) 0.0081(7) -0.0026(7) C23 0.0301(8) 0.0269(7) 0.0316(8) -0.0011(6) 0.0005(6) -0.0023(6) C24 0.0475(10) 0.0359(9) 0.0352(9) 0.0058(7) 0.0025(8) 0.0083(8) C25 0.0809(16) 0.0384(11) 0.0544(12) 0.0125(9) 0.0055(11) 0.0008(10) C26 0.0547(13) 0.0699(15) 0.0545(12) 0.0093(11) -0.0119(10) 0.0102(11) C27 0.0328(8) 0.0284(8) 0.0338(8) 0.0001(7) 0.0011(7) 0.0016(7) C28 0.0641(13) 0.0565(13) 0.0550(12) 0.0153(10) -0.0064(10) -0.0276(11) C29 0.0464(11) 0.0544(12) 0.0420(10) 0.0101(9) -0.0070(8) 0.0006(9) C30 0.0218(7) 0.0269(7) 0.0343(8) -0.0085(6) 0.0028(6) -0.0002(6) C31 0.0290(8) 0.0320(9) 0.0385(9) -0.0066(7) 0.0003(7) -0.0019(7) C32 0.0315(9) 0.0440(10) 0.0487(10) -0.0067(8) -0.0091(8) -0.0050(8) C33 0.0295(9) 0.0456(11) 0.0660(13) -0.0087(9) -0.0010(9) -0.0138(8) C34 0.0360(9) 0.0366(9) 0.0546(11) -0.0026(8) 0.0105(8) -0.0098(8) C35 0.0320(8) 0.0289(8) 0.0395(9) -0.0060(7) 0.0071(7) -0.0014(7) C36 0.0489(11) 0.0395(10) 0.0380(9) 0.0035(8) 0.0041(8) -0.0063(8) C37 0.125(2) 0.0528(14) 0.0762(17) 0.0065(13) -0.0293(17) 0.0203(15) C38 0.0890(19) 0.108(2) 0.0456(13) -0.0017(13) 0.0178(12) -0.0148(17) C39 0.0392(9) 0.0478(11) 0.0377(9) 0.0044(8) -0.0072(7) -0.0110(8) C40 0.0632(14) 0.0933(19) 0.0519(13) 0.0187(13) 0.0149(11) 0.0152(13) C41 0.0593(13) 0.0465(12) 0.0619(13) 0.0086(10) -0.0102(10) -0.0028(10) C42 0.085(14) 0.103(7) 0.061(5) -0.011(5) 0.004(8) 0.024(8) C43 0.071(9) 0.163(17) 0.053(4) -0.026(10) -0.012(4) 0.030(10) C44 0.062(9) 0.135(13) 0.053(5) -0.016(7) -0.001(5) -0.008(7) C45 0.067(12) 0.093(9) 0.041(5) 0.003(5) -0.007(6) 0.015(7) C46 0.057(7) 0.104(11) 0.050(7) 0.003(8) 0.000(5) 0.005(7) C47 0.075(13) 0.068(5) 0.045(5) 0.002(4) 0.001(7) -0.013(7) C48 0.077(3) 0.158(4) 0.062(3) 0.007(3) -0.011(2) 0.001(3) C49 0.118(5) 0.086(3) 0.049(2) 0.020(2) -0.005(2) 0.000(3) C50 0.120(4) 0.053(3) 0.053(2) 0.0127(18) -0.001(2) 0.013(2) C51 0.138(3) 0.070(3) 0.052(3) 0.007(2) 0.001(3) 0.031(2) C52 0.101(4) 0.102(3) 0.0628(19) 0.0054(19) -0.005(2) 0.046(3) C53 0.068(2) 0.149(5) 0.068(3) -0.004(3) -0.013(2) 0.039(2) C54 0.077(3) 0.158(4) 0.062(3) 0.007(3) -0.011(2) 0.001(3) C55 0.118(5) 0.086(3) 0.049(2) 0.020(2) -0.005(2) 0.000(3) C56 0.120(4) 0.053(3) 0.053(2) 0.0127(18) -0.001(2) 0.013(2) C57 0.138(3) 0.070(3) 0.052(3) 0.007(2) 0.001(3) 0.031(2) C58 0.101(4) 0.102(3) 0.0628(19) 0.0054(19) -0.005(2) 0.046(3) C59 0.068(2) 0.149(5) 0.068(3) -0.004(3) -0.013(2) 0.039(2) C60 0.104(2) 0.181(4) 0.063(2) -0.027(3) 0.0180(18) -0.029(2) C61 0.104(2) 0.181(4) 0.063(2) -0.027(3) 0.0180(18) -0.029(2) C62 0.104(2) 0.181(4) 0.063(2) -0.027(3) 0.0180(18) -0.029(2) C63 0.104(2) 0.181(4) 0.063(2) -0.027(3) 0.0180(18) -0.029(2) C64 0.104(2) 0.181(4) 0.063(2) -0.027(3) 0.0180(18) -0.029(2) C65 0.104(2) 0.181(4) 0.063(2) -0.027(3) 0.0180(18) -0.029(2) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ge1 C1 1.8806(14) . ? Ge1 N3 2.0058(12) . ? Ge2 C1 1.844(4) . ? Ge2 N4 2.072(5) . ? N1 C1 1.3889(18) . ? N1 C11 1.3916(18) . ? N1 C2 1.3973(19) . ? N2 C4 1.3589(18) . ? N2 C1 1.3868(18) . ? N2 C3 1.4056(19) . ? N3 C4 1.3418(18) . ? N3 C18 1.4301(18) . ? N4 C11 1.2842(19) . ? N4 C30 1.4200(19) . ? C2 C3 1.332(2) . ? C2 H2 0.9500 . ? C3 H3 0.9500 . ? C4 C5 1.470(2) . ? C5 C6 1.394(2) . ? C5 C10 1.397(2) . ? C6 C7 1.382(2) . ? C6 H6 0.9500 . ? C7 C8 1.380(3) . ? C7 H7 0.9500 . ? C8 C9 1.377(3) . ? C8 H8 0.9500 . ? C9 C10 1.381(2) . ? C9 H9 0.9500 . ? C10 H10 0.9500 . ? C11 C12 1.485(2) . ? C12 C17 1.388(2) . ? C12 C13 1.394(2) . ? C13 C14 1.385(2) . ? C13 H13 0.9500 . ? C14 C15 1.378(3) . ? C14 H14 0.9500 . ? C15 C16 1.377(3) . ? C15 H15 0.9500 . ? C16 C17 1.385(2) . ? C16 H16 0.9500 . ? C17 H17 0.9500 . ? C18 C23 1.401(2) . ? C18 C19 1.407(2) . ? C19 C20 1.389(2) . ? C19 C27 1.518(2) . ? C20 C21 1.381(2) . ? C20 H20 0.9500 . ? C21 C22 1.382(2) . ? C21 H21 0.9500 . ? C22 C23 1.392(2) . ? C22 H22 0.9500 . ? C23 C24 1.516(2) . ? C24 C25 1.520(3) . ? C24 C26 1.527(3) . ? C24 H24 1.0000 . ? C25 H25A 0.9800 . ? C25 H25B 0.9800 . ? C25 H25C 0.9800 . ? C26 H26A 0.9800 . ? C26 H26B 0.9800 . ? C26 H26C 0.9800 . ? C27 C28 1.522(2) . ? C27 C29 1.524(2) . ? C27 H27 1.0000 . ? C28 H28A 0.9800 . ? C28 H28B 0.9800 . ? C28 H28C 0.9800 . ? C29 H29A 0.9800 . ? C29 H29B 0.9800 . ? C29 H29C 0.9800 . ? C30 C35 1.404(2) . ? C30 C31 1.408(2) . ? C31 C32 1.392(2) . ? C31 C39 1.514(2) . ? C32 C33 1.372(3) . ? C32 H32 0.9500 . ? C33 C34 1.370(3) . ? C33 H33 0.9500 . ? C34 C35 1.390(2) . ? C34 H34 0.9500 . ? C35 C36 1.513(2) . ? C36 C38 1.520(3) . ? C36 C37 1.521(3) . ? C36 H36 1.0000 . ? C37 H37A 0.9800 . ? C37 H37B 0.9800 . ? C37 H37C 0.9800 . ? C38 H38A 0.9800 . ? C38 H38B 0.9800 . ? C38 H38C 0.9800 . ? C39 C40 1.515(3) . ? C39 C41 1.525(3) . ? C39 H39 1.0000 . ? C40 H40A 0.9800 . ? C40 H40B 0.9800 . ? C40 H40C 0.9800 . ? C41 H41A 0.9800 . ? C41 H41B 0.9800 . ? C41 H41C 0.9800 . ? C42 C44 1.356(13) 3_566 ? C42 C43 1.375(8) . ? C42 H42 0.9500 . ? C43 C44 1.381(8) . ? C43 H43 0.9500 . ? C44 H44 0.9500 . ? C45 C47 1.360(16) 3_566 ? C45 C46 1.371(10) . ? C45 H45 0.9500 . ? C46 C47 1.376(9) . ? C46 H46 0.9500 . ? C47 H47 0.9500 . ? C48 C49 1.3900 . ? C48 C53 1.3900 . ? C48 H48 0.9500 . ? C49 C50 1.3900 . ? C49 H49 0.9500 . ? C50 C51 1.3900 . ? C50 H50 0.9500 . ? C51 C52 1.3900 . ? C51 H51 0.9500 . ? C52 C53 1.3900 . ? C52 H52 0.9500 . ? C53 H53 0.9500 . ? C54 C55 1.3900 . ? C54 C59 1.3900 . ? C54 H54 0.9500 . ? C55 C56 1.3900 . ? C55 H55 0.9500 . ? C56 C57 1.3900 . ? C56 H56 0.9500 . ? C57 C58 1.3900 . ? C57 H57 0.9500 . ? C58 C59 1.3900 . ? C58 H58 0.9500 . ? C59 H59 0.9500 . ? C60 C61 1.346(9) . ? C60 C62 1.397(9) 3_756 ? C60 H60 0.9500 . ? C61 C62 1.392(10) . ? C61 H61 0.9500 . ? C62 H62 0.9500 . ? C63 C64 1.355(11) . ? C63 C65 1.430(16) 3_756 ? C63 H63 0.9500 . ? C64 C65 1.405(9) . ? C64 H64 0.9500 . ? C65 H65 0.9500 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1 Ge1 N3 78.21(5) . . ? C1 Ge2 N4 83.26(16) . . ? C1 N1 C11 119.70(12) . . ? C1 N1 C2 108.90(12) . . ? C11 N1 C2 131.00(13) . . ? C4 N2 C1 116.53(12) . . ? C4 N2 C3 133.93(12) . . ? C1 N2 C3 109.47(12) . . ? C4 N3 C18 120.16(12) . . ? C4 N3 Ge1 117.48(9) . . ? C18 N3 Ge1 120.81(9) . . ? C11 N4 C30 123.88(13) . . ? C11 N4 Ge2 110.89(14) . . ? C30 N4 Ge2 124.51(14) . . ? N2 C1 N1 105.29(12) . . ? N2 C1 Ge2 142.93(18) . . ? N1 C1 Ge2 111.49(17) . . ? N2 C1 Ge1 116.91(10) . . ? N1 C1 Ge1 137.76(11) . . ? C3 C2 N1 108.93(13) . . ? C3 C2 H2 125.5 . . ? N1 C2 H2 125.5 . . ? C2 C3 N2 107.42(13) . . ? C2 C3 H3 126.3 . . ? N2 C3 H3 126.3 . . ? N3 C4 N2 110.69(12) . . ? N3 C4 C5 127.72(13) . . ? N2 C4 C5 121.38(13) . . ? C6 C5 C10 118.22(14) . . ? C6 C5 C4 121.41(14) . . ? C10 C5 C4 120.31(13) . . ? C7 C6 C5 120.52(16) . . ? C7 C6 H6 119.7 . . ? C5 C6 H6 119.7 . . ? C8 C7 C6 120.56(16) . . ? C8 C7 H7 119.7 . . ? C6 C7 H7 119.7 . . ? C9 C8 C7 119.55(16) . . ? C9 C8 H8 120.2 . . ? C7 C8 H8 120.2 . . ? C8 C9 C10 120.38(16) . . ? C8 C9 H9 119.8 . . ? C10 C9 H9 119.8 . . ? C9 C10 C5 120.74(15) . . ? C9 C10 H10 119.6 . . ? C5 C10 H10 119.6 . . ? N4 C11 N1 114.14(13) . . ? N4 C11 C12 128.21(13) . . ? N1 C11 C12 117.57(13) . . ? C17 C12 C13 119.39(14) . . ? C17 C12 C11 120.19(14) . . ? C13 C12 C11 120.35(14) . . ? C14 C13 C12 119.84(16) . . ? C14 C13 H13 120.1 . . ? C12 C13 H13 120.1 . . ? C15 C14 C13 120.37(17) . . ? C15 C14 H14 119.8 . . ? C13 C14 H14 119.8 . . ? C16 C15 C14 120.00(16) . . ? C16 C15 H15 120.0 . . ? C14 C15 H15 120.0 . . ? C15 C16 C17 120.30(17) . . ? C15 C16 H16 119.9 . . ? C17 C16 H16 119.9 . . ? C16 C17 C12 120.10(16) . . ? C16 C17 H17 119.9 . . ? C12 C17 H17 119.9 . . ? C23 C18 C19 121.60(13) . . ? C23 C18 N3 118.97(13) . . ? C19 C18 N3 119.34(13) . . ? C20 C19 C18 117.82(14) . . ? C20 C19 C27 120.80(14) . . ? C18 C19 C27 121.37(13) . . ? C21 C20 C19 121.41(15) . . ? C21 C20 H20 119.3 . . ? C19 C20 H20 119.3 . . ? C20 C21 C22 119.87(15) . . ? C20 C21 H21 120.1 . . ? C22 C21 H21 120.1 . . ? C21 C22 C23 121.16(15) . . ? C21 C22 H22 119.4 . . ? C23 C22 H22 119.4 . . ? C22 C23 C18 117.98(15) . . ? C22 C23 C24 119.95(15) . . ? C18 C23 C24 122.04(14) . . ? C23 C24 C25 112.18(16) . . ? C23 C24 C26 109.79(15) . . ? C25 C24 C26 111.71(17) . . ? C23 C24 H24 107.7 . . ? C25 C24 H24 107.7 . . ? C26 C24 H24 107.7 . . ? C24 C25 H25A 109.5 . . ? C24 C25 H25B 109.5 . . ? H25A C25 H25B 109.5 . . ? C24 C25 H25C 109.5 . . ? H25A C25 H25C 109.5 . . ? H25B C25 H25C 109.5 . . ? C24 C26 H26A 109.5 . . ? C24 C26 H26B 109.5 . . ? H26A C26 H26B 109.5 . . ? C24 C26 H26C 109.5 . . ? H26A C26 H26C 109.5 . . ? H26B C26 H26C 109.5 . . ? C19 C27 C28 110.60(14) . . ? C19 C27 C29 113.01(14) . . ? C28 C27 C29 109.57(15) . . ? C19 C27 H27 107.8 . . ? C28 C27 H27 107.8 . . ? C29 C27 H27 107.8 . . ? C27 C28 H28A 109.5 . . ? C27 C28 H28B 109.5 . . ? H28A C28 H28B 109.5 . . ? C27 C28 H28C 109.5 . . ? H28A C28 H28C 109.5 . . ? H28B C28 H28C 109.5 . . ? C27 C29 H29A 109.5 . . ? C27 C29 H29B 109.5 . . ? H29A C29 H29B 109.5 . . ? C27 C29 H29C 109.5 . . ? H29A C29 H29C 109.5 . . ? H29B C29 H29C 109.5 . . ? C35 C30 C31 120.95(14) . . ? C35 C30 N4 121.68(14) . . ? C31 C30 N4 117.02(14) . . ? C32 C31 C30 118.17(16) . . ? C32 C31 C39 120.61(16) . . ? C30 C31 C39 121.22(14) . . ? C33 C32 C31 121.32(17) . . ? C33 C32 H32 119.3 . . ? C31 C32 H32 119.3 . . ? C34 C33 C32 119.84(16) . . ? C34 C33 H33 120.1 . . ? C32 C33 H33 120.1 . . ? C33 C34 C35 121.86(17) . . ? C33 C34 H34 119.1 . . ? C35 C34 H34 119.1 . . ? C34 C35 C30 117.86(16) . . ? C34 C35 C36 119.61(16) . . ? C30 C35 C36 122.50(15) . . ? C35 C36 C38 111.78(18) . . ? C35 C36 C37 110.15(17) . . ? C38 C36 C37 112.0(2) . . ? C35 C36 H36 107.6 . . ? C38 C36 H36 107.6 . . ? C37 C36 H36 107.6 . . ? C36 C37 H37A 109.5 . . ? C36 C37 H37B 109.5 . . ? H37A C37 H37B 109.5 . . ? C36 C37 H37C 109.5 . . ? H37A C37 H37C 109.5 . . ? H37B C37 H37C 109.5 . . ? C36 C38 H38A 109.5 . . ? C36 C38 H38B 109.5 . . ? H38A C38 H38B 109.5 . . ? C36 C38 H38C 109.5 . . ? H38A C38 H38C 109.5 . . ? H38B C38 H38C 109.5 . . ? C31 C39 C40 111.07(17) . . ? C31 C39 C41 112.97(16) . . ? C40 C39 C41 110.70(17) . . ? C31 C39 H39 107.3 . . ? C40 C39 H39 107.3 . . ? C41 C39 H39 107.3 . . ? C39 C40 H40A 109.5 . . ? C39 C40 H40B 109.5 . . ? H40A C40 H40B 109.5 . . ? C39 C40 H40C 109.5 . . ? H40A C40 H40C 109.5 . . ? H40B C40 H40C 109.5 . . ? C39 C41 H41A 109.5 . . ? C39 C41 H41B 109.5 . . ? H41A C41 H41B 109.5 . . ? C39 C41 H41C 109.5 . . ? H41A C41 H41C 109.5 . . ? H41B C41 H41C 109.5 . . ? C44 C42 C43 123.7(15) 3_566 . ? C44 C42 H42 118.1 3_566 . ? C43 C42 H42 118.1 . . ? C42 C43 C44 117.9(12) . . ? C42 C43 H43 121.1 . . ? C44 C43 H43 121.1 . . ? C42 C44 C43 118.4(14) 3_566 . ? C42 C44 H44 120.8 3_566 . ? C43 C44 H44 120.8 . . ? C47 C45 C46 117.3(14) 3_566 . ? C47 C45 H45 121.3 3_566 . ? C46 C45 H45 121.3 . . ? C45 C46 C47 120.3(13) . . ? C45 C46 H46 119.8 . . ? C47 C46 H46 119.9 . . ? C45 C47 C46 122.3(12) 3_566 . ? C45 C47 H47 118.8 3_566 . ? C46 C47 H47 118.8 . . ? C49 C48 C53 120.0 . . ? C49 C48 H48 120.0 . . ? C53 C48 H48 120.0 . . ? C50 C49 C48 120.0 . . ? C50 C49 H49 120.0 . . ? C48 C49 H49 120.0 . . ? C49 C50 C51 120.0 . . ? C49 C50 H50 120.0 . . ? C51 C50 H50 120.0 . . ? C52 C51 C50 120.0 . . ? C52 C51 H51 120.0 . . ? C50 C51 H51 120.0 . . ? C51 C52 C53 120.0 . . ? C51 C52 H52 120.0 . . ? C53 C52 H52 120.0 . . ? C52 C53 C48 120.0 . . ? C52 C53 H53 120.0 . . ? C48 C53 H53 120.0 . . ? C55 C54 C59 120.0 . . ? C55 C54 H54 120.0 . . ? C59 C54 H54 120.0 . . ? C54 C55 C56 120.0 . . ? C54 C55 H55 120.0 . . ? C56 C55 H55 120.0 . . ? C57 C56 C55 120.0 . . ? C57 C56 H56 120.0 . . ? C55 C56 H56 120.0 . . ? C58 C57 C56 120.0 . . ? C58 C57 H57 120.0 . . ? C56 C57 H57 120.0 . . ? C57 C58 C59 120.0 . . ? C57 C58 H58 120.0 . . ? C59 C58 H58 120.0 . . ? C58 C59 C54 120.0 . . ? C58 C59 H59 120.0 . . ? C54 C59 H59 120.0 . . ? C61 C60 C62 117.1(8) . 3_756 ? C61 C60 H60 121.4 . . ? C62 C60 H60 121.4 3_756 . ? C60 C61 C62 119.2(10) . . ? C60 C61 H61 120.4 . . ? C62 C61 H61 120.4 . . ? C61 C62 C60 123.6(8) . 3_756 ? C61 C62 H62 118.2 . . ? C60 C62 H62 118.2 3_756 . ? C64 C63 C65 129.1(12) . 3_756 ? C64 C63 H63 115.4 . . ? C65 C63 H63 115.4 3_756 . ? C63 C64 C65 113.3(12) . . ? C63 C64 H64 123.3 . . ? C65 C64 H64 123.3 . . ? C64 C65 H65 121.2 . . ? C63 C65 H65 121.2 3_756 . ? _refine_diff_density_max 0.369 _refine_diff_density_min -0.343 _refine_diff_density_rms 0.045 _shelx_res_file ; TITL gn248 in P2(1)/n shelx.res created by SHELXL-2018/3 at 12:51:46 on 19-Jan-2020 CELL 0.71073 13.9768 14.7308 22.7506 90.000 91.163 90.000 ZERR 4.00 0.0002 0.0003 0.0004 0.000 0.001 0.000 LATT 1 SYMM 1/2 - X, 1/2 + Y, 1/2 - Z SFAC C H GE N UNIT 212 232 4 16 MERG 2 EADP Ge1 Ge2 RIGU C48 C49 C50 C51 C52 C53 RIGU C54 C55 C56 C57 C58 C59 EADP C48 C54 EADP C49 C55 EADP C50 C56 EADP C51 C57 EADP C52 C58 EADP C53 C59 RIGU C60 C61 C62 RIGU C63 C64 C65 EADP C60 C61 C62 C63 C64 C65 SADI C42 C43 C43 C44 C45 C46 C46 C47 DFIX 1.395 0.01 C42 C43 C43 C44 DFIX 1.395 0.015 C45 C46 C46 C47 SADI 0.04 C42 C44 C45 C47 SADI C60 C61 C61 C62 C63 C64 C64 C65 SADI 0.04 C60 C62 C63 C65 FMAP 2 PLAN 20 SIZE 0.236 0.443 0.600 ACTA BOND $H LIST 4 L.S. 40 TEMP -73.15 WGHT 0.039600 1.756800 FVAR 0.33344 0.95468 0.54272 0.61584 0.56231 PART 1 GE1 3 0.329368 0.303578 0.734542 21.00000 0.02578 0.02597 = 0.03614 -0.00712 0.00230 -0.00608 PART 2 GE2 3 0.389425 0.290745 0.730081 -21.00000 0.02578 0.02597 = 0.03614 -0.00712 0.00230 -0.00608 PART 0 N1 4 0.397370 0.148380 0.656716 11.00000 0.02025 0.02743 = 0.03065 -0.00469 0.00056 0.00035 N2 4 0.245915 0.150285 0.682208 11.00000 0.01946 0.02299 = 0.03077 -0.00431 -0.00111 -0.00080 N3 4 0.191500 0.265799 0.734677 11.00000 0.02259 0.02191 = 0.02957 -0.00265 0.00206 -0.00089 N4 4 0.513278 0.236644 0.695811 11.00000 0.02295 0.03113 = 0.03035 -0.00357 0.00203 -0.00094 C1 1 0.331646 0.196799 0.689280 11.00000 0.02022 0.02494 = 0.02896 -0.00165 0.00098 -0.00085 C2 1 0.351339 0.073652 0.631014 11.00000 0.02598 0.02809 = 0.03346 -0.00804 -0.00141 0.00198 AFIX 43 H2 2 0.380709 0.029383 0.606955 11.00000 -1.20000 AFIX 0 C3 1 0.259567 0.074567 0.645731 11.00000 0.02601 0.02454 = 0.03534 -0.00794 -0.00072 -0.00157 AFIX 43 H3 2 0.212082 0.031887 0.633769 11.00000 -1.20000 AFIX 0 C4 1 0.168449 0.186989 0.708430 11.00000 0.02085 0.02361 = 0.02747 -0.00031 0.00021 0.00083 C5 1 0.076679 0.138376 0.710077 11.00000 0.02338 0.02617 = 0.02863 -0.00478 0.00052 -0.00217 C6 1 -0.010015 0.183266 0.700533 11.00000 0.02558 0.02699 = 0.05113 -0.00740 -0.00251 0.00063 AFIX 43 H6 2 -0.010204 0.246006 0.690868 11.00000 -1.20000 AFIX 0 C7 1 -0.095746 0.137222 0.705018 11.00000 0.02106 0.04405 = 0.07104 -0.01410 -0.00136 -0.00041 AFIX 43 H7 2 -0.154377 0.168656 0.698586 11.00000 -1.20000 AFIX 0 C8 1 -0.096882 0.045964 0.718764 11.00000 0.03013 0.04637 = 0.05874 -0.01051 0.00767 -0.01485 AFIX 43 H8 2 -0.156003 0.014717 0.721986 11.00000 -1.20000 AFIX 0 C9 1 -0.011744 0.000523 0.727776 11.00000 0.04104 0.03114 = 0.04366 0.00087 0.00366 -0.01101 AFIX 43 H9 2 -0.012210 -0.062427 0.736840 11.00000 -1.20000 AFIX 0 C10 1 0.074344 0.045943 0.723711 11.00000 0.02921 0.02947 = 0.03642 0.00184 -0.00201 -0.00177 AFIX 43 H10 2 0.132612 0.013961 0.730262 11.00000 -1.20000 AFIX 0 C11 1 0.493561 0.172777 0.659106 11.00000 0.02103 0.02778 = 0.02652 0.00144 0.00042 0.00073 C12 1 0.558890 0.126599 0.617979 11.00000 0.02357 0.02478 = 0.03247 -0.00144 0.00381 -0.00332 C13 1 0.647629 0.094464 0.637858 11.00000 0.02480 0.03219 = 0.04030 -0.00499 0.00057 -0.00114 AFIX 43 H13 2 0.665619 0.099852 0.678200 11.00000 -1.20000 AFIX 0 C14 1 0.709465 0.054681 0.598655 11.00000 0.02782 0.04277 = 0.06077 -0.01130 0.00541 0.00439 AFIX 43 H14 2 0.769730 0.032401 0.612265 11.00000 -1.20000 AFIX 0 C15 1 0.684084 0.047223 0.540006 11.00000 0.04384 0.04729 = 0.05483 -0.01583 0.02068 0.00128 AFIX 43 H15 2 0.726937 0.020140 0.513276 11.00000 -1.20000 AFIX 0 C16 1 0.596633 0.079019 0.520156 11.00000 0.05179 0.04607 = 0.03501 -0.00907 0.01045 -0.00391 AFIX 43 H16 2 0.579196 0.073615 0.479730 11.00000 -1.20000 AFIX 0 C17 1 0.533963 0.118845 0.558847 11.00000 0.03407 0.03623 = 0.03456 -0.00238 0.00282 0.00017 AFIX 43 H17 2 0.473807 0.140893 0.544883 11.00000 -1.20000 AFIX 0 C18 1 0.125059 0.309294 0.772487 11.00000 0.01924 0.02232 = 0.02960 -0.00533 0.00116 -0.00304 C19 1 0.075639 0.386897 0.752469 11.00000 0.02332 0.02379 = 0.03041 -0.00361 -0.00182 -0.00330 C20 1 0.011908 0.427592 0.790383 11.00000 0.02822 0.02567 = 0.03987 -0.00593 -0.00029 0.00278 AFIX 43 H20 2 -0.022177 0.480156 0.777833 11.00000 -1.20000 AFIX 0 C21 1 -0.002987 0.393289 0.845944 11.00000 0.03227 0.03392 = 0.03916 -0.01051 0.00972 0.00070 AFIX 43 H21 2 -0.048773 0.420726 0.870615 11.00000 -1.20000 AFIX 0 C22 1 0.048834 0.318986 0.865581 11.00000 0.03978 0.03516 = 0.02882 -0.00244 0.00807 -0.00258 AFIX 43 H22 2 0.039281 0.296608 0.904183 11.00000 -1.20000 AFIX 0 C23 1 0.114798 0.276335 0.829796 11.00000 0.03012 0.02691 = 0.03155 -0.00114 0.00054 -0.00226 C24 1 0.174899 0.198544 0.853798 11.00000 0.04748 0.03588 = 0.03519 0.00583 0.00251 0.00828 AFIX 13 H24 2 0.211463 0.172603 0.820408 11.00000 -1.20000 AFIX 0 C25 1 0.113875 0.122938 0.878766 11.00000 0.08094 0.03841 = 0.05441 0.01250 0.00551 0.00082 AFIX 33 H25A 2 0.155434 0.074225 0.893742 11.00000 -1.50000 H25B 2 0.075612 0.146919 0.910878 11.00000 -1.50000 H25C 2 0.071232 0.098923 0.847776 11.00000 -1.50000 AFIX 0 C26 1 0.247494 0.234313 0.899235 11.00000 0.05469 0.06988 = 0.05454 0.00926 -0.01195 0.01023 AFIX 33 H26A 2 0.286145 0.183789 0.914608 11.00000 -1.50000 H26B 2 0.289293 0.278883 0.880689 11.00000 -1.50000 H26C 2 0.213621 0.263216 0.931561 11.00000 -1.50000 AFIX 0 C27 1 0.092093 0.426028 0.691781 11.00000 0.03281 0.02837 = 0.03382 0.00013 0.00111 0.00164 AFIX 13 H27 2 0.128365 0.380047 0.668797 11.00000 -1.20000 AFIX 0 C28 1 0.152807 0.511603 0.696002 11.00000 0.06408 0.05649 = 0.05503 0.01528 -0.00637 -0.02759 AFIX 33 H28A 2 0.162685 0.535891 0.656485 11.00000 -1.50000 H28B 2 0.119966 0.557002 0.719770 11.00000 -1.50000 H28C 2 0.214875 0.497033 0.714472 11.00000 -1.50000 AFIX 0 C29 1 -0.000705 0.446585 0.658006 11.00000 0.04641 0.05443 = 0.04199 0.01007 -0.00695 0.00060 AFIX 33 H29A 2 0.014171 0.471575 0.619330 11.00000 -1.50000 H29B 2 -0.037749 0.390534 0.652999 11.00000 -1.50000 H29C 2 -0.038193 0.490860 0.679977 11.00000 -1.50000 AFIX 0 C30 1 0.606076 0.274280 0.704263 11.00000 0.02176 0.02690 = 0.03434 -0.00853 0.00282 -0.00020 C31 1 0.652613 0.257365 0.758607 11.00000 0.02903 0.03199 = 0.03853 -0.00657 0.00035 -0.00187 C32 1 0.738383 0.302210 0.770812 11.00000 0.03150 0.04399 = 0.04867 -0.00665 -0.00910 -0.00496 AFIX 43 H32 2 0.770499 0.292064 0.807425 11.00000 -1.20000 AFIX 0 C33 1 0.777486 0.360786 0.731019 11.00000 0.02948 0.04560 = 0.06603 -0.00866 -0.00101 -0.01380 AFIX 43 H33 2 0.835929 0.391009 0.740241 11.00000 -1.20000 AFIX 0 C34 1 0.732054 0.375578 0.677968 11.00000 0.03596 0.03657 = 0.05464 -0.00259 0.01051 -0.00983 AFIX 43 H34 2 0.760340 0.415538 0.650529 11.00000 -1.20000 AFIX 0 C35 1 0.645713 0.333758 0.663145 11.00000 0.03198 0.02894 = 0.03946 -0.00599 0.00714 -0.00138 C36 1 0.596628 0.355551 0.604964 11.00000 0.04894 0.03949 = 0.03803 0.00345 0.00406 -0.00626 AFIX 13 H36 2 0.539194 0.315362 0.601022 11.00000 -1.20000 AFIX 0 C37 1 0.561533 0.453272 0.604723 11.00000 0.12495 0.05278 = 0.07623 0.00649 -0.02928 0.02025 AFIX 33 H37A 2 0.529888 0.466651 0.566876 11.00000 -1.50000 H37B 2 0.516027 0.461837 0.636459 11.00000 -1.50000 H37C 2 0.616068 0.494298 0.610679 11.00000 -1.50000 AFIX 0 C38 1 0.660767 0.335708 0.553344 11.00000 0.08904 0.10840 = 0.04558 -0.00173 0.01778 -0.01485 AFIX 33 H38A 2 0.626693 0.350595 0.516525 11.00000 -1.50000 H38B 2 0.719007 0.372529 0.556808 11.00000 -1.50000 H38C 2 0.677949 0.271209 0.553423 11.00000 -1.50000 AFIX 0 C39 1 0.610207 0.193368 0.803183 11.00000 0.03922 0.04776 = 0.03775 0.00443 -0.00723 -0.01095 AFIX 13 H39 2 0.564434 0.152700 0.781440 11.00000 -1.20000 AFIX 0 C40 1 0.553417 0.244920 0.848312 11.00000 0.06321 0.09329 = 0.05188 0.01872 0.01489 0.01517 AFIX 33 H40A 2 0.526786 0.202077 0.876588 11.00000 -1.50000 H40B 2 0.595515 0.288005 0.869054 11.00000 -1.50000 H40C 2 0.501205 0.278037 0.828496 11.00000 -1.50000 AFIX 0 C41 1 0.684985 0.132809 0.833210 11.00000 0.05935 0.04655 = 0.06191 0.00863 -0.01024 -0.00284 AFIX 33 H41A 2 0.653701 0.092973 0.861474 11.00000 -1.50000 H41B 2 0.716805 0.095856 0.803590 11.00000 -1.50000 H41C 2 0.732499 0.170683 0.853863 11.00000 -1.50000 AFIX 0 PART 1 C42 1 0.026947 0.413646 0.494073 31.00000 0.08498 0.10313 = 0.06110 -0.01063 0.00392 0.02374 AFIX 43 H42 2 0.046346 0.352281 0.489528 31.00000 -1.20000 AFIX 0 C43 1 0.096547 0.479622 0.495290 31.00000 0.07078 0.16308 = 0.05255 -0.02588 -0.01230 0.02984 AFIX 43 H43 2 0.162300 0.464336 0.492292 31.00000 -1.20000 AFIX 0 C44 1 0.067788 0.568844 0.501012 31.00000 0.06249 0.13530 = 0.05266 -0.01570 -0.00091 -0.00803 AFIX 43 H44 2 0.113280 0.616768 0.501491 31.00000 -1.20000 AFIX 0 PART 2 C45 1 0.063379 0.428698 0.489590 -31.00000 0.06750 0.09263 = 0.04103 0.00280 -0.00711 0.01485 AFIX 43 H45 2 0.106141 0.380276 0.481708 -31.00000 -1.20000 AFIX 0 C46 1 0.096319 0.514468 0.501683 -31.00000 0.05691 0.10378 = 0.05011 0.00339 0.00039 0.00499 AFIX 43 H46 2 0.163221 0.525732 0.503867 -31.00000 -1.20000 AFIX 0 C47 1 0.032931 0.584317 0.510670 -31.00000 0.07521 0.06839 = 0.04475 0.00235 0.00070 -0.01269 AFIX 43 H47 2 0.057310 0.643723 0.517290 -31.00000 -1.20000 PART 1 AFIX 66 C48 1 0.364621 0.337672 0.500949 41.00000 0.07750 0.15755 = 0.06190 0.00688 -0.01069 0.00093 AFIX 43 H48 2 0.412322 0.383197 0.497500 41.00000 -1.20000 AFIX 65 C49 1 0.309622 0.333464 0.551098 41.00000 0.11850 0.08556 = 0.04940 0.01998 -0.00516 0.00034 AFIX 43 H49 2 0.319734 0.376113 0.581925 41.00000 -1.20000 AFIX 65 C50 1 0.239828 0.266855 0.556144 41.00000 0.12049 0.05315 = 0.05314 0.01271 -0.00125 0.01337 AFIX 43 H50 2 0.202239 0.263980 0.590419 41.00000 -1.20000 AFIX 65 C51 1 0.225032 0.204454 0.511040 41.00000 0.13830 0.07015 = 0.05181 0.00659 0.00096 0.03072 AFIX 43 H51 2 0.177330 0.158930 0.514489 41.00000 -1.20000 AFIX 65 C52 1 0.280030 0.208661 0.460890 41.00000 0.10125 0.10230 = 0.06277 0.00544 -0.00517 0.04602 AFIX 43 H52 2 0.269917 0.166012 0.430064 41.00000 -1.20000 AFIX 65 C53 1 0.349825 0.275269 0.455844 41.00000 0.06808 0.14915 = 0.06770 -0.00395 -0.01278 0.03944 AFIX 43 H53 2 0.387413 0.278145 0.421569 41.00000 -1.20000 PART 2 AFIX 66 C54 1 0.333106 0.337184 0.530484 -41.00000 0.07750 0.15755 = 0.06190 0.00688 -0.01069 0.00093 AFIX 43 H54 2 0.367373 0.387992 0.545691 -41.00000 -1.20000 AFIX 65 C55 1 0.254192 0.304095 0.559904 -41.00000 0.11850 0.08556 = 0.04940 0.01998 -0.00516 0.00034 AFIX 43 H55 2 0.234524 0.332288 0.595218 -41.00000 -1.20000 AFIX 65 C56 1 0.204055 0.229757 0.537653 -41.00000 0.12049 0.05315 = 0.05314 0.01271 -0.00125 0.01337 AFIX 43 H56 2 0.150120 0.207142 0.557761 -41.00000 -1.20000 AFIX 65 C57 1 0.232832 0.188506 0.485983 -41.00000 0.13830 0.07015 = 0.05181 0.00659 0.00096 0.03072 AFIX 43 H57 2 0.198565 0.137698 0.470777 -41.00000 -1.20000 AFIX 65 C58 1 0.311746 0.221593 0.456563 -41.00000 0.10125 0.10230 = 0.06277 0.00544 -0.00517 0.04602 AFIX 43 H58 2 0.331413 0.193400 0.421248 -41.00000 -1.20000 AFIX 65 C59 1 0.361884 0.295932 0.478812 -41.00000 0.06808 0.14915 = 0.06770 -0.00395 -0.01278 0.03944 AFIX 43 H59 2 0.415818 0.318546 0.458704 -41.00000 -1.20000 AFIX 0 PART 1 C60 1 1.032369 -0.048981 0.549867 51.00000 0.10397 0.18148 = 0.06302 -0.02680 0.01797 -0.02917 AFIX 43 H60 2 1.053655 -0.084142 0.582604 51.00000 -1.20000 AFIX 0 C61 1 0.990944 0.032699 0.556988 51.00000 0.10397 0.18148 = 0.06302 -0.02680 0.01797 -0.02917 AFIX 43 H61 2 0.984757 0.057869 0.595168 51.00000 -1.20000 AFIX 0 C62 1 0.957299 0.079802 0.507729 51.00000 0.10397 0.18148 = 0.06302 -0.02680 0.01797 -0.02917 AFIX 43 H62 2 0.925559 0.136006 0.513596 51.00000 -1.20000 AFIX 0 PART 2 C63 1 0.997630 -0.006078 0.556998 -51.00000 0.10397 0.18148 = 0.06302 -0.02680 0.01797 -0.02917 AFIX 43 H63 2 0.995865 -0.013741 0.598424 -51.00000 -1.20000 AFIX 0 C64 1 0.962939 0.074026 0.536443 -51.00000 0.10397 0.18148 = 0.06302 -0.02680 0.01797 -0.02917 AFIX 43 H64 2 0.940484 0.121006 0.561225 -51.00000 -1.20000 AFIX 0 C65 1 0.963485 0.080681 0.474867 -51.00000 0.10397 0.18148 = 0.06302 -0.02680 0.01797 -0.02917 AFIX 43 H65 2 0.938936 0.132796 0.455128 -51.00000 -1.20000 AFIX 0 HKLF 4 REM gn248 in P2(1)/n REM wR2 = 0.0900, GooF = S = 1.018, Restrained GooF = 1.018 for all data REM R1 = 0.0347 for 8466 Fo > 4sig(Fo) and 0.0547 for all 11015 data REM 548 parameters refined using 108 restraints END WGHT 0.0395 1.7687 REM Highest difference peak 0.369, deepest hole -0.343, 1-sigma level 0.045 Q1 1 0.3265 0.2425 0.7002 11.00000 0.05 0.37 Q2 1 0.0131 0.3021 0.7973 11.00000 0.05 0.35 Q3 1 0.3365 0.2207 0.7231 11.00000 0.05 0.33 Q4 1 0.3219 0.2990 0.5451 11.00000 0.05 0.33 Q5 1 0.9372 0.1204 0.4802 11.00000 0.05 0.30 Q6 1 0.6669 0.4001 0.5499 11.00000 0.05 0.29 Q7 1 0.2507 0.2976 0.7410 11.00000 0.05 0.27 Q8 1 0.0381 0.1618 0.7158 11.00000 0.05 0.26 Q9 1 0.5964 0.1048 0.6261 11.00000 0.05 0.26 Q10 1 0.3205 0.3002 0.6841 11.00000 0.05 0.24 Q11 1 0.6200 0.2774 0.7394 11.00000 0.05 0.24 Q12 1 1.0332 -0.0542 0.5679 11.00000 0.05 0.24 Q13 1 0.3862 0.3025 0.7704 11.00000 0.05 0.24 Q14 1 0.0784 0.4050 0.7196 11.00000 0.05 0.23 Q15 1 0.5332 0.1411 0.6384 11.00000 0.05 0.23 Q16 1 0.2562 0.1957 0.5087 11.00000 0.05 0.23 Q17 1 0.0725 0.2792 0.8388 11.00000 0.05 0.22 Q18 1 0.3107 0.2085 0.4716 11.00000 0.05 0.22 Q19 1 0.2430 0.1168 0.6645 11.00000 0.05 0.22 Q20 1 0.3394 0.3648 0.5176 11.00000 0.05 0.22 ; _shelx_res_checksum 70876 _shelx_hkl_file ; -1 0 0 -0.20 0.20 1 0 0 -0.10 0.20 1 0 0 -0.10 0.20 -1 0 0 0.20 0.10 2 0 0 35.00 1.00 -2 0 0 34.20 0.90 -2 0 0 32.70 1.10 2 0 0 33.20 1.00 -3 0 0 -0.10 0.50 3 0 0 1.60 0.70 3 0 0 0.80 0.60 -3 0 0 1.30 0.70 4 0 0 29.50 1.30 -4 0 0 22.80 1.20 -4 0 0 27.10 1.50 4 0 0 24.40 1.40 -5 0 0 -0.50 0.70 5 0 0 0.50 0.90 -5 0 0 -0.40 0.90 5 0 0 1.50 0.80 6 0 0 892.01 16.80 6 0 0 891.41 16.70 -6 0 0 883.51 16.70 -6 0 0 874.61 17.00 7 0 0 -1.10 1.10 -7 0 0 -2.10 1.30 -7 0 0 -1.30 0.90 7 0 0 0.90 1.00 8 0 0 32.10 2.00 -8 0 0 30.00 2.10 8 0 0 28.00 2.30 -8 0 0 30.10 1.90 9 0 0 -0.20 1.30 -9 0 0 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2.50 1.90 9 -6 0 2.00 1.90 -9 6 0 1.70 1.90 -9 6 0 3.70 1.80 10 -6 0 -2.90 2.00 10 -6 0 0.10 2.10 -10 -6 0 -2.30 2.00 -10 6 0 -0.90 1.90 -10 6 0 1.20 2.10 11 -6 0 26.30 3.00 -11 -6 0 23.40 2.80 11 -6 0 25.90 2.90 -11 6 0 23.80 2.70 -11 6 0 19.90 2.80 12 -6 0 41.70 3.60 -12 -6 0 43.90 3.50 12 -6 0 46.00 4.30 -12 6 0 48.10 4.10 -12 6 0 38.40 3.40 13 -6 0 114.09 5.30 -13 -6 0 130.99 6.00 13 -6 0 108.79 6.10 -13 6 0 134.19 5.70 -13 6 0 133.89 5.80 14 -6 0 40.20 4.10 -14 -6 0 37.40 3.90 -14 6 0 40.10 3.90 -14 6 0 43.90 3.70 -15 -6 0 7.40 3.50 15 -6 0 5.90 3.20 -15 6 0 10.40 3.10 -15 6 0 10.40 3.50 -16 -6 0 3.00 3.70 16 -6 0 5.40 3.60 -16 6 0 7.00 3.60 -17 -6 0 8.00 4.00 -17 6 0 1.30 4.30 0 -7 0 -0.20 1.10 0 7 0 -0.30 0.70 1 -7 0 146.19 4.30 -1 -7 0 146.79 4.20 1 -7 0 156.78 3.10 -1 7 0 149.09 3.70 1 7 0 155.78 3.30 -2 -7 0 690.53 13.70 2 -7 0 688.23 13.90 -2 -7 0 682.33 12.70 -2 7 0 678.53 13.30 3 -7 0 201.08 4.80 -3 -7 0 204.28 5.10 -3 -7 0 210.28 4.30 3 -7 0 212.58 5.50 -3 7 0 204.78 5.00 4 -7 0 108.99 3.40 4 -7 0 104.89 3.90 -4 -7 0 105.89 2.80 -4 -7 0 108.49 3.40 -4 7 0 107.09 3.50 -4 7 0 107.69 4.50 -4 7 0 105.69 2.90 -5 -7 0 68.99 2.40 -5 -7 0 69.49 2.80 5 -7 0 76.09 3.50 5 -7 0 67.19 2.90 -5 7 0 66.39 3.00 5 7 0 70.89 3.90 -5 7 0 69.59 2.50 -5 7 0 71.29 3.90 -6 -7 0 12.90 1.50 6 -7 0 11.90 1.70 6 -7 0 12.70 2.10 -6 -7 0 11.00 1.40 6 7 0 9.80 2.00 -6 7 0 13.30 1.50 -6 7 0 11.50 1.80 -6 7 0 12.30 2.00 -7 -7 0 -0.80 1.40 -7 -7 0 2.50 1.40 7 -7 0 1.10 1.70 7 -7 0 -0.20 1.80 -7 7 0 0.70 1.60 7 7 0 1.40 1.80 -7 7 0 0.20 1.60 -7 7 0 2.30 1.40 -8 -7 0 116.49 4.00 8 -7 0 109.69 4.60 8 -7 0 120.19 4.70 -8 -7 0 119.79 3.90 8 7 0 110.49 5.10 -8 7 0 115.39 4.90 -8 7 0 112.99 4.30 -8 7 0 113.69 4.00 -9 -7 0 375.06 8.60 9 -7 0 382.96 9.30 9 -7 0 369.96 9.10 -9 7 0 360.96 9.00 9 7 0 383.06 12.00 -9 7 0 377.26 8.70 10 -7 0 76.99 4.30 10 -7 0 69.09 4.50 -10 -7 0 78.89 4.10 -10 7 0 81.89 4.20 -10 7 0 78.29 4.60 -11 -7 0 12.40 2.60 11 -7 0 9.00 2.60 11 -7 0 12.10 2.60 -11 7 0 14.20 2.70 -11 7 0 14.10 2.50 12 -7 0 55.69 4.70 -12 -7 0 55.89 4.60 12 -7 0 49.00 3.80 -12 7 0 54.29 4.40 -12 7 0 58.09 4.70 13 -7 0 0.60 2.70 13 -7 0 2.50 2.80 -13 -7 0 2.50 3.00 -13 7 0 1.80 2.70 -13 7 0 9.10 2.90 14 -7 0 63.79 5.90 14 -7 0 47.90 4.30 -14 -7 0 58.69 4.40 -14 7 0 68.29 5.30 -14 7 0 69.29 5.60 15 -7 0 49.00 4.60 -15 -7 0 73.79 6.00 -15 7 0 69.79 5.50 -15 7 0 64.99 4.80 -16 -7 0 8.30 3.80 -16 7 0 8.60 3.30 -16 7 0 1.70 3.60 -17 -7 0 22.80 4.40 0 -8 0 955.80 18.80 0 8 0 959.80 18.10 1 -8 0 353.46 8.10 -1 -8 0 358.86 8.00 -1 8 0 344.27 7.30 1 8 0 355.96 7.00 2 -8 0 208.78 5.50 -2 -8 0 209.48 5.50 -2 8 0 201.18 4.90 2 8 0 211.48 4.30 3 -8 0 405.16 9.00 -3 -8 0 392.76 7.60 -3 -8 0 392.46 8.60 -3 8 0 385.36 8.40 -3 8 0 388.46 10.00 -4 -8 0 80.29 3.20 4 -8 0 85.39 3.80 4 -8 0 82.89 3.10 -4 -8 0 80.59 2.40 -4 8 0 88.59 4.50 -4 8 0 83.89 3.20 5 -8 0 35.00 2.60 -5 -8 0 37.10 2.00 5 -8 0 35.70 3.20 -5 -8 0 37.20 2.60 -5 8 0 31.20 2.10 -5 8 0 32.00 3.60 5 8 0 38.30 3.80 -5 8 0 34.50 2.80 -6 -8 0 719.43 14.20 -6 -8 0 714.13 14.60 6 -8 0 736.03 14.80 6 -8 0 727.73 15.20 -6 8 0 760.22 15.00 -6 8 0 729.53 16.10 -6 8 0 713.63 14.30 6 8 0 742.43 16.20 7 -8 0 7.80 2.20 -7 -8 0 1.00 1.50 -7 -8 0 5.20 1.70 7 -8 0 1.20 1.90 -7 8 0 -0.30 1.50 -7 8 0 5.70 1.90 -7 8 0 -2.70 1.90 8 -8 0 71.39 4.20 -8 -8 0 72.19 3.40 8 -8 0 75.69 3.90 -8 -8 0 68.59 3.30 -8 8 0 71.99 3.40 -8 8 0 66.69 4.50 -8 8 0 68.99 4.00 8 8 0 71.89 4.70 -9 -8 0 4.30 2.00 9 -8 0 1.40 2.10 9 -8 0 -0.30 2.20 9 8 0 3.20 2.30 -9 8 0 1.70 1.80 -9 8 0 -0.40 2.10 -10 -8 0 14.20 2.40 10 -8 0 14.00 2.70 10 -8 0 10.80 2.60 -10 8 0 13.60 2.70 -10 8 0 9.90 2.20 11 -8 0 18.90 2.90 11 -8 0 18.40 3.00 -11 -8 0 18.20 2.70 -11 8 0 17.00 2.70 -11 8 0 22.90 3.00 12 -8 0 137.89 5.90 12 -8 0 119.79 6.20 -12 -8 0 135.99 5.60 -12 8 0 140.69 6.10 -12 8 0 134.89 5.80 13 -8 0 6.30 3.20 -13 -8 0 16.00 3.20 13 -8 0 20.40 3.40 -13 8 0 20.10 3.30 -13 8 0 18.50 3.20 14 -8 0 64.59 5.60 -14 -8 0 68.29 4.90 14 -8 0 47.20 4.50 -14 8 0 64.99 5.40 -14 8 0 70.39 5.50 15 -8 0 11.30 3.60 -15 8 0 7.80 3.50 -15 8 0 14.90 3.50 -16 8 0 5.10 3.30 -16 8 0 3.20 3.60 0 -9 0 -0.90 1.40 0 9 0 0.00 0.90 1 -9 0 49.50 3.20 -1 -9 0 41.60 2.90 -1 9 0 42.60 2.10 1 9 0 43.70 1.80 2 -9 0 340.97 6.80 -2 -9 0 328.57 7.80 2 -9 0 340.37 8.10 -2 9 0 347.97 9.50 -2 9 0 319.37 7.30 2 9 0 331.17 6.70 -3 -9 0 -0.30 1.50 3 -9 0 0.40 1.80 3 9 0 0.90 1.90 -3 9 0 -0.80 1.90 -3 9 0 -0.40 1.30 4 -9 0 426.16 9.80 -4 -9 0 416.16 9.30 -4 9 0 425.96 11.00 4 9 0 427.76 11.10 -4 9 0 415.16 9.20 -5 -9 0 0.70 1.60 5 -9 0 -3.50 1.30 5 -9 0 1.00 2.00 -5 9 0 -1.20 1.90 -5 9 0 0.00 1.60 5 9 0 -1.40 2.00 6 -9 0 171.68 5.10 6 -9 0 173.38 5.60 -6 -9 0 172.18 5.00 6 9 0 168.48 6.70 -6 9 0 177.28 5.40 -6 9 0 176.38 4.60 -6 9 0 175.68 6.60 7 -9 0 3.30 2.30 -7 -9 0 5.50 1.80 7 -9 0 6.60 2.00 -7 9 0 2.60 1.90 -7 9 0 5.80 1.60 -7 9 0 5.40 2.20 7 9 0 4.10 2.40 8 -9 0 267.57 7.70 8 -9 0 267.27 7.30 8 9 0 274.77 8.70 -8 9 0 263.87 8.30 -8 9 0 279.97 6.70 -8 9 0 273.97 7.40 9 -9 0 51.59 4.40 9 -9 0 52.09 3.50 -9 9 0 58.29 4.20 9 9 0 40.80 5.00 -9 9 0 53.99 3.40 10 -9 0 280.67 8.20 10 -9 0 271.47 8.00 -10 9 0 289.87 8.10 -10 9 0 272.47 7.30 11 -9 0 2.70 2.70 11 -9 0 -3.10 2.40 -11 9 0 2.90 2.70 -11 9 0 -3.80 2.10 12 -9 0 6.30 2.90 12 -9 0 0.00 2.90 -12 9 0 0.10 2.50 -12 9 0 1.30 2.80 13 -9 0 -0.80 2.90 13 -9 0 -2.20 2.90 -13 9 0 1.60 3.00 -13 9 0 2.80 2.90 14 -9 0 16.90 3.60 14 -9 0 21.20 3.80 -14 9 0 21.10 3.50 -14 9 0 20.90 3.50 -15 9 0 5.40 3.50 -15 9 0 7.70 3.50 -16 9 0 22.20 4.10 0 -10 0 151.58 5.00 0 10 0 144.79 6.30 0 10 0 147.99 3.90 1 -10 0 9.60 2.00 -1 -10 0 13.00 2.10 -1 10 0 10.70 1.40 1 10 0 6.10 2.40 -1 10 0 6.90 2.30 1 10 0 10.50 1.20 -2 -10 0 130.59 4.50 2 -10 0 124.09 4.50 2 10 0 128.79 6.20 2 10 0 117.89 3.10 -2 10 0 120.29 3.80 -2 10 0 126.19 5.90 3 -10 0 10.60 2.20 -3 -10 0 11.30 2.00 -3 10 0 12.50 1.70 3 10 0 12.10 2.60 -3 10 0 11.90 2.50 4 -10 0 77.49 3.90 -4 -10 0 79.29 3.60 -4 10 0 74.39 5.20 -4 10 0 74.69 3.50 4 10 0 78.69 5.40 -5 -10 0 1.40 1.90 5 -10 0 0.20 2.10 -5 10 0 -0.60 2.20 5 10 0 -3.70 2.30 -5 10 0 0.80 1.80 6 -10 0 770.42 16.60 -6 -10 0 754.62 15.70 -6 10 0 778.12 17.80 -6 10 0 772.42 16.00 6 10 0 768.02 17.80 -7 -10 0 33.10 2.60 7 -10 0 36.50 3.30 7 -10 0 35.20 2.70 -7 10 0 36.80 2.90 -7 10 0 37.20 2.70 7 10 0 24.70 3.50 -7 10 0 28.00 3.30 8 -10 0 34.90 2.90 8 -10 0 35.50 3.50 8 10 0 28.20 3.40 -8 10 0 34.00 3.10 -8 10 0 33.40 3.40 -8 10 0 35.10 2.50 9 -10 0 8.50 2.40 9 -10 0 9.60 2.90 -9 10 0 13.10 2.20 9 10 0 7.50 2.90 -9 10 0 8.70 2.60 10 -10 0 67.09 4.80 10 -10 0 68.09 5.10 -10 10 0 72.49 5.00 -10 10 0 65.59 4.00 11 -10 0 6.60 3.00 11 -10 0 8.10 2.90 -11 10 0 7.90 2.50 -11 10 0 12.90 3.10 12 -10 0 94.29 6.20 12 -10 0 80.09 5.80 -12 10 0 97.19 5.90 -12 10 0 88.59 5.20 13 -10 0 1.60 3.00 13 -10 0 8.30 3.40 -13 10 0 3.20 3.00 -13 10 0 5.60 3.10 14 -10 0 43.50 4.40 14 -10 0 48.60 4.60 -14 10 0 51.19 4.30 -14 10 0 54.79 4.60 -15 10 0 -0.80 3.30 -16 10 0 -2.40 4.20 0 -11 0 2.90 2.00 0 11 0 -0.30 2.30 0 11 0 0.20 1.20 1 -11 0 9.20 2.40 -1 -11 0 10.10 2.00 -1 11 0 7.90 1.50 -1 11 0 3.40 2.40 1 11 0 10.20 1.30 1 11 0 6.50 2.50 2 -11 0 139.99 5.30 -2 -11 0 135.99 5.00 -2 11 0 144.79 6.70 -2 11 0 136.59 4.20 2 11 0 139.09 6.80 -3 -11 0 97.29 4.30 3 -11 0 111.19 4.90 -3 11 0 105.49 6.30 -3 11 0 103.49 3.90 3 11 0 98.09 6.20 4 -11 0 238.98 7.10 -4 -11 0 245.08 6.80 -4 11 0 247.68 8.70 4 11 0 257.47 8.90 -4 11 0 248.48 6.50 -5 -11 0 646.64 13.80 5 -11 0 649.34 14.50 -5 11 0 647.74 15.90 -5 11 0 641.14 13.80 5 11 0 650.93 16.20 6 -11 0 0.50 2.50 -6 -11 0 0.80 2.10 -6 11 0 -0.50 2.40 6 11 0 -0.80 2.70 -6 11 0 2.70 2.10 -7 -11 0 13.60 2.30 7 -11 0 7.50 2.70 -7 11 0 9.80 2.40 7 11 0 9.20 3.00 -7 11 0 10.60 2.80 8 -11 0 158.78 6.50 -8 11 0 171.18 7.50 -8 11 0 161.58 6.00 8 11 0 159.88 7.80 9 -11 0 62.09 4.30 9 -11 0 60.39 5.20 -9 11 0 61.69 4.80 9 11 0 57.49 5.90 10 -11 0 120.09 6.20 10 -11 0 111.79 5.40 -10 11 0 122.59 5.90 11 -11 0 42.00 3.70 11 -11 0 34.40 3.80 -11 11 0 40.70 3.90 12 -11 0 10.20 3.50 12 -11 0 11.30 3.10 -12 11 0 9.30 3.30 13 -11 0 15.40 3.40 13 -11 0 17.20 3.90 -13 11 0 18.90 3.60 14 -11 0 35.70 4.40 0 -12 0 170.88 6.00 0 12 0 177.38 7.80 0 12 0 181.78 4.80 -1 -12 0 182.88 6.10 1 -12 0 186.78 6.30 -1 12 0 179.78 8.10 1 12 0 184.38 7.90 -1 12 0 180.18 5.00 2 -12 0 67.09 4.50 -2 -12 0 61.79 4.10 2 12 0 78.19 6.00 -2 12 0 61.79 6.00 -2 12 0 72.49 3.30 -3 -12 0 20.90 2.80 3 -12 0 19.90 2.70 3 12 0 18.10 3.30 -3 12 0 23.80 2.30 -3 12 0 21.00 3.30 -4 -12 0 51.69 3.80 4 -12 0 53.69 4.50 4 12 0 54.39 6.00 -4 12 0 54.29 5.90 -4 12 0 41.00 3.40 -5 -12 0 14.90 2.60 5 -12 0 12.40 3.00 -5 12 0 7.20 3.00 -5 12 0 10.50 2.20 5 12 0 8.60 3.20 -6 -12 0 5.40 2.30 6 -12 0 10.20 3.00 -6 12 0 5.40 2.30 6 12 0 5.00 3.20 -6 12 0 7.40 2.90 7 -12 0 3.60 2.90 -7 12 0 4.70 2.40 7 12 0 -3.70 2.90 -7 12 0 -2.70 2.60 8 -12 0 139.39 6.50 -8 12 0 136.39 7.50 -8 12 0 153.48 6.00 8 12 0 137.29 7.60 9 -12 0 1.20 3.10 -9 12 0 1.70 2.60 9 12 0 -1.60 3.00 10 -12 0 2.20 3.30 -10 12 0 0.40 2.90 11 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13 0 91.89 6.20 12 -13 0 12.60 4.00 13 -13 0 8.40 4.10 0 -14 0 12.10 2.90 0 14 0 13.10 3.70 1 -14 0 143.49 6.20 -1 -14 0 145.19 6.20 -1 14 0 140.09 8.10 1 14 0 148.89 8.60 -2 -14 0 21.30 3.10 2 -14 0 22.30 3.20 -2 14 0 19.20 3.90 -2 14 0 23.10 2.40 2 14 0 16.00 3.90 -3 -14 0 11.40 2.90 3 -14 0 14.50 3.20 -3 14 0 12.00 3.60 3 14 0 7.40 3.50 -3 14 0 10.70 2.20 4 -14 0 5.80 2.80 -4 -14 0 5.80 2.80 -4 14 0 5.10 3.30 4 14 0 6.10 3.50 -4 14 0 3.40 2.20 -5 -14 0 95.59 5.40 5 -14 0 108.19 6.10 -5 14 0 100.59 5.00 5 14 0 91.89 7.40 -5 14 0 92.39 7.20 -6 -14 0 100.59 8.00 6 -14 0 92.89 6.10 6 14 0 87.99 7.70 -6 14 0 90.69 7.30 -6 14 0 92.69 5.10 7 -14 0 40.80 4.20 7 14 0 36.30 4.70 -7 14 0 52.69 3.90 -7 14 0 40.50 4.50 8 -14 0 15.70 3.70 -8 14 0 13.00 3.80 -8 14 0 18.90 3.20 8 14 0 19.00 4.10 9 -14 0 1.40 3.50 9 14 0 1.80 3.70 -9 14 0 -2.50 2.80 10 -14 0 -1.20 3.60 -10 14 0 2.10 3.20 11 -14 0 8.10 3.80 12 -14 0 -0.90 3.80 0 -15 0 -0.90 2.80 0 15 0 -2.10 3.40 1 -15 0 35.60 4.00 -1 -15 0 33.20 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79.69 2.50 -4 9 3 82.89 5.00 -4 9 3 89.39 3.40 -3 -9 3 279.37 7.00 -3 -9 3 283.07 5.90 3 -9 -3 295.27 7.40 -3 9 3 293.17 8.60 -3 9 3 274.87 6.60 -3 9 3 273.37 5.70 -2 -9 3 4.90 1.80 2 -9 -3 2.90 1.80 -2 9 3 1.50 1.20 -2 9 3 -0.90 1.90 -1 -9 3 520.05 10.20 -1 -9 3 531.45 11.50 1 -9 -3 531.55 11.50 -1 9 3 536.15 10.70 -1 9 3 548.15 13.00 1 9 -3 532.75 10.50 0 -9 -3 78.19 3.50 0 -9 3 84.39 2.40 0 -9 3 86.99 3.60 0 9 3 84.09 2.60 0 9 -3 83.39 2.70 0 9 3 84.89 4.70 1 -9 3 44.70 3.20 1 -9 3 41.30 1.80 -1 -9 -3 41.10 2.80 1 9 3 39.40 3.90 -1 9 -3 40.10 2.20 1 9 3 39.40 1.80 2 -9 3 306.97 6.30 2 -9 3 307.37 7.60 2 -9 3 303.57 6.50 -2 -9 -3 300.67 7.30 2 9 3 299.57 8.90 2 9 3 310.97 6.20 -2 9 -3 300.77 6.90 3 -9 3 563.74 12.00 3 -9 3 545.95 11.00 -3 -9 -3 534.65 11.40 -3 9 -3 539.45 11.30 3 9 3 536.55 13.10 3 9 3 536.65 10.30 4 -9 3 15.40 1.70 4 -9 3 14.10 2.10 -4 -9 -3 17.60 1.90 4 9 3 14.60 2.60 -4 9 -3 12.90 1.80 5 -9 3 177.98 4.90 5 -9 3 171.38 5.60 -5 -9 -3 170.18 4.80 -5 9 -3 184.38 5.30 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-4 258.47 6.00 7 -8 4 247.98 6.60 7 -8 4 251.37 7.00 -7 8 -4 254.27 6.90 7 8 4 260.37 7.90 -8 -8 -4 133.09 4.30 8 -8 4 133.19 5.20 8 -8 4 132.69 4.80 8 8 4 128.29 5.80 -8 8 -4 125.89 4.90 -9 -8 -4 7.40 2.10 9 -8 4 6.00 2.50 9 -8 4 5.80 2.30 9 8 4 5.30 3.80 -9 8 -4 7.60 2.40 -10 -8 -4 2.60 2.60 10 -8 4 2.20 2.30 10 -8 4 7.50 2.60 -10 8 -4 1.40 2.40 11 -8 4 22.10 3.00 11 -8 4 21.00 3.00 -11 8 -4 16.60 2.70 -11 8 -4 16.90 3.00 12 -8 4 22.10 3.20 12 -8 4 19.00 3.20 -12 8 -4 24.10 3.30 -12 8 -4 25.10 3.20 13 -8 4 -0.20 3.00 -13 8 -4 -2.60 2.90 -13 8 -4 4.40 3.00 14 -8 4 208.68 8.00 -14 8 -4 226.78 7.90 -14 8 -4 220.08 7.90 -15 8 -4 7.50 3.40 -15 8 -4 3.40 3.50 -16 8 -4 15.80 4.40 -16 8 -4 16.30 4.20 16 -9 -4 10.80 4.40 -16 9 4 0.90 3.60 15 -9 -4 3.00 3.60 -15 9 4 7.70 3.60 -15 9 4 5.00 3.30 14 -9 -4 27.80 4.00 -14 9 4 27.70 3.70 -14 9 4 26.40 3.70 13 -9 -4 1.00 3.20 -13 9 4 2.50 3.00 -13 9 4 3.70 2.80 12 -9 -4 1.90 3.10 -12 -9 4 -4.90 4.30 -12 9 4 -2.00 2.70 -12 9 4 -0.30 2.40 11 -9 -4 28.30 3.50 -11 -9 4 23.60 3.00 -11 9 4 23.90 3.20 -11 9 4 22.20 2.70 -10 -9 4 123.79 5.00 10 -9 -4 127.39 6.00 -10 9 4 126.09 4.80 -10 9 4 139.39 5.70 -9 -9 4 1.20 2.30 9 -9 -4 0.80 2.60 -9 -9 4 1.00 2.10 -9 9 4 0.30 2.20 -9 9 4 0.60 1.80 8 -9 -4 705.33 15.90 -8 -9 4 714.83 14.70 -8 -9 4 733.73 15.30 -8 9 4 727.63 15.30 -8 9 4 723.53 14.60 -8 9 4 739.13 16.60 -7 -9 4 193.08 6.00 -7 -9 4 192.08 5.30 7 -9 -4 180.78 6.30 -7 9 4 187.88 5.00 -7 9 4 197.68 5.90 -7 9 4 195.78 7.10 6 -9 -4 273.37 7.60 -6 -9 4 267.17 6.30 -6 -9 4 259.07 7.10 -6 9 4 267.57 6.10 -6 9 4 274.37 7.00 -6 9 4 271.97 8.40 5 -9 -4 42.20 3.60 -5 -9 4 37.10 3.10 -5 -9 4 40.80 2.50 -5 9 4 37.30 2.10 -5 9 4 39.10 3.10 -5 9 4 38.40 4.20 -4 -9 4 191.28 5.50 -4 -9 4 185.98 4.50 4 -9 -4 196.58 5.90 -4 9 4 188.28 6.80 -4 9 4 181.98 4.20 -4 9 4 183.58 5.10 -3 -9 4 28.70 2.40 3 -9 -4 36.80 3.20 -3 -9 4 27.80 2.00 -3 9 4 21.80 2.60 -3 9 4 28.10 1.70 -3 9 4 27.80 2.00 2 -9 -4 348.47 8.30 -2 -9 4 347.37 8.20 -2 -9 4 337.07 7.00 -2 9 4 357.36 9.70 -2 9 4 336.47 7.50 -1 -9 4 19.30 1.30 -1 -9 4 14.90 2.10 1 -9 -4 16.90 2.10 -1 9 4 15.10 1.50 -1 9 4 14.50 2.50 0 -9 -4 7.80 1.80 0 -9 4 8.80 2.00 0 -9 4 9.70 1.10 0 9 -4 9.60 1.30 0 9 4 8.40 2.10 0 9 4 9.90 1.20 -1 -9 -4 26.90 2.30 -1 9 -4 40.80 2.20 1 9 4 27.40 1.70 1 9 4 33.90 3.80 2 -9 4 43.90 2.10 -2 -9 -4 44.30 2.90 2 -9 4 44.00 3.30 2 -9 4 43.80 2.10 2 9 4 49.20 4.20 -2 9 -4 38.70 2.50 2 9 4 46.60 1.80 -3 -9 -4 23.40 2.10 3 -9 4 25.00 2.00 3 -9 4 24.90 2.10 3 -9 4 26.70 2.50 3 9 4 27.30 1.40 3 9 4 22.60 2.70 -3 9 -4 27.70 2.10 4 -9 4 724.33 15.10 4 -9 4 706.73 14.30 -4 -9 -4 698.83 14.30 -4 9 -4 731.33 14.60 4 9 4 710.23 16.30 5 -9 4 3.90 2.20 5 -9 4 3.20 1.60 -5 -9 -4 3.90 1.60 -5 9 -4 4.80 1.80 5 9 4 1.30 2.10 6 -9 4 472.75 11.10 6 -9 4 480.25 10.50 -6 9 -4 476.25 10.70 6 9 4 488.25 12.20 7 -9 4 5.10 2.30 7 -9 4 3.00 1.90 -7 9 -4 1.50 2.10 7 9 4 1.80 2.30 8 -9 4 23.50 3.00 8 -9 4 29.50 2.80 8 9 4 22.10 3.00 -8 9 -4 24.40 2.80 9 -9 4 37.90 3.40 9 -9 4 33.60 3.10 9 9 4 23.90 3.60 -9 9 -4 31.80 3.10 10 -9 4 475.85 11.60 10 -9 4 478.35 11.50 -10 9 -4 493.95 11.70 11 -9 4 1.00 2.70 11 -9 4 5.10 2.70 -11 9 -4 1.80 2.70 12 -9 4 78.29 5.50 12 -9 4 67.39 5.30 -12 9 -4 81.69 5.60 13 -9 4 1.00 3.00 -13 9 -4 4.50 3.20 14 -9 4 6.60 3.40 -14 9 -4 8.50 3.40 -15 9 -4 18.50 3.90 16 -10 -4 1.10 5.30 15 -10 -4 4.60 3.70 14 -10 -4 28.30 4.20 -14 10 4 32.10 4.10 13 -10 -4 0.80 3.30 -13 10 4 0.70 3.00 12 -10 -4 73.49 5.70 -12 10 4 75.79 5.40 11 -10 -4 7.70 2.80 -11 10 4 12.50 3.00 10 -10 -4 19.30 3.30 -10 10 4 20.10 3.10 9 -10 -4 26.40 3.40 -9 -10 4 24.80 2.90 -9 10 4 23.60 3.00 -8 -10 4 10.70 2.50 8 -10 -4 6.60 2.80 -8 10 4 8.50 2.70 -8 10 4 7.70 2.40 7 -10 -4 8.70 2.70 -7 -10 4 11.30 2.50 -7 10 4 9.10 2.30 -7 10 4 8.30 2.60 6 -10 -4 121.19 5.30 -6 -10 4 127.39 5.00 -6 10 4 122.29 6.20 -6 10 4 124.49 4.70 -5 -10 4 124.99 4.80 5 -10 -4 130.39 5.30 -5 10 4 122.79 6.20 -5 10 4 125.59 4.60 4 -10 -4 60.99 4.10 -4 -10 4 56.39 3.70 -4 10 4 63.89 3.30 -4 10 4 60.19 5.00 3 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4.10 7 10 4 53.89 5.40 8 -10 4 81.59 4.90 8 -10 4 83.29 4.40 -8 10 -4 75.99 4.70 8 10 4 77.89 5.60 9 -10 4 -3.10 2.60 9 -10 4 -0.40 2.20 9 10 4 -1.10 2.70 -9 10 -4 2.50 2.50 10 -10 4 2.80 2.80 10 -10 4 -1.20 2.40 -10 10 -4 -0.20 2.60 11 -10 4 0.90 2.80 11 -10 4 -2.90 2.50 -11 10 -4 0.20 2.70 12 -10 4 65.19 5.70 12 -10 4 64.29 5.40 -12 10 -4 63.39 5.40 13 -10 4 0.10 3.00 13 -10 4 -0.40 3.20 -13 10 -4 2.20 3.20 -14 10 -4 104.29 6.60 15 -11 -4 17.40 4.80 14 -11 -4 34.90 4.60 13 -11 -4 15.00 3.90 -13 11 4 8.80 3.40 12 -11 -4 0.50 3.20 -12 11 4 4.30 3.00 11 -11 -4 -1.50 3.00 -11 11 4 3.30 2.80 10 -11 -4 54.59 4.70 -10 11 4 64.39 5.10 -9 -11 4 66.59 5.10 9 -11 -4 59.89 5.30 -9 11 4 64.29 4.80 -8 -11 4 360.46 9.30 8 -11 -4 376.86 10.20 -8 11 4 363.36 11.00 -8 11 4 379.86 9.50 -7 -11 4 22.90 2.80 7 -11 -4 18.70 3.10 -7 11 4 17.80 3.20 -7 11 4 21.50 2.80 6 -11 -4 59.39 4.70 -6 -11 4 49.80 4.20 -6 11 4 56.59 4.00 -6 11 4 60.69 5.60 -5 -11 4 350.16 8.90 5 -11 -4 345.67 9.30 -5 11 4 355.86 10.60 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6 11 4 50.89 5.50 7 -11 4 11.70 2.20 7 -11 4 9.10 2.90 7 11 4 8.50 2.90 -7 11 -4 6.30 2.40 8 -11 4 6.00 2.80 8 -11 4 7.70 2.30 -8 11 -4 2.70 2.50 8 11 4 0.20 2.90 9 -11 4 12.80 2.70 9 -11 4 18.40 3.20 -9 11 -4 14.90 2.90 9 11 4 7.50 3.10 10 -11 4 119.69 6.10 10 -11 4 106.39 5.60 -10 11 -4 114.79 6.10 11 -11 4 25.70 3.80 11 -11 4 26.20 3.40 -11 11 -4 23.00 3.60 12 -11 4 12.90 3.50 12 -11 4 15.50 3.30 -12 11 -4 15.50 3.40 13 -11 4 0.90 3.00 13 -11 4 0.60 3.40 -13 11 -4 -2.50 3.20 14 -12 -4 0.90 4.20 13 -12 -4 6.10 3.80 12 -12 -4 93.39 6.60 -12 12 4 92.29 6.40 11 -12 -4 31.20 4.20 -11 12 4 29.10 3.60 10 -12 -4 97.19 6.20 -10 12 4 99.09 5.60 9 -12 -4 10.10 3.40 9 12 -4 2.50 3.10 -9 12 4 7.20 2.80 -8 -12 4 4.50 2.80 8 -12 -4 2.40 3.00 -8 12 4 3.00 2.90 -8 12 4 0.30 2.50 -7 -12 4 16.60 3.00 7 -12 -4 14.10 3.20 -7 12 4 15.50 3.30 -7 12 4 22.90 2.90 -6 -12 4 4.90 2.50 6 -12 -4 5.50 2.90 -6 12 4 5.10 2.90 -6 12 4 3.60 2.30 -5 -12 4 203.18 6.60 5 -12 -4 194.68 7.10 -5 12 4 210.68 8.40 -5 12 4 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16.40 3.50 8 12 4 14.30 3.50 -8 12 -4 16.60 2.90 -8 12 -4 15.60 3.30 9 -12 4 36.10 4.00 9 -12 4 32.70 3.20 9 12 4 36.80 4.70 -9 12 -4 47.00 3.90 10 -12 4 4.10 2.60 10 -12 4 6.50 3.50 -10 12 -4 6.10 3.10 11 -12 4 0.90 2.70 11 -12 4 -1.60 3.20 -11 12 -4 1.60 3.00 12 -12 4 33.10 4.30 12 -12 4 23.70 3.60 -12 12 -4 29.40 4.00 13 -12 4 1.10 3.60 12 -13 -4 -0.50 3.60 11 -13 -4 32.60 4.30 -11 13 4 42.40 4.20 10 -13 -4 2.60 3.50 -10 13 4 3.50 2.90 9 -13 -4 62.99 5.20 -9 13 4 66.89 5.40 9 13 -4 66.39 6.90 8 -13 -4 -0.30 3.10 -8 -13 4 2.80 3.00 -8 13 4 3.60 2.70 8 13 -4 3.10 3.30 -8 13 4 -3.00 3.00 7 -13 -4 14.80 3.10 -7 -13 4 16.40 3.10 -7 13 4 14.80 3.50 -7 13 4 16.30 2.80 6 -13 -4 37.30 3.90 -6 -13 4 37.30 3.50 -6 13 4 24.50 3.80 -6 13 4 36.30 3.20 -5 -13 4 141.79 5.80 5 -13 -4 134.19 5.80 -5 13 4 119.99 7.60 -5 13 4 131.89 5.30 4 -13 -4 5.20 2.90 -4 -13 4 4.50 2.80 -4 13 4 5.10 2.10 -4 13 4 2.50 3.00 -3 -13 4 110.79 5.40 3 -13 -4 112.69 5.70 -3 13 4 115.29 4.40 -3 13 4 108.49 7.00 2 -13 -4 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5 111.49 5.70 -1 10 5 110.99 3.50 1 10 -5 108.29 3.30 0 -10 5 29.80 2.80 0 -10 -5 22.80 2.30 0 10 5 26.10 2.00 0 10 -5 25.30 2.20 0 10 5 18.00 2.70 1 -10 5 635.04 12.90 -1 -10 -5 622.44 13.40 1 -10 5 642.44 13.70 1 10 5 633.44 12.40 -1 10 -5 635.04 12.90 1 10 5 634.04 15.30 2 -10 5 18.20 1.60 -2 -10 -5 15.50 2.00 2 -10 5 16.30 1.60 2 -10 5 19.50 2.60 2 10 5 17.70 2.80 2 10 5 16.80 1.40 -2 10 -5 15.70 1.90 3 -10 5 130.79 3.90 3 -10 5 131.89 3.90 3 -10 5 144.59 5.30 -3 -10 -5 128.39 4.50 3 10 5 144.49 6.30 -3 10 -5 135.69 4.50 -4 -10 -5 69.79 3.40 4 -10 5 74.19 4.30 4 -10 5 70.39 3.20 4 10 5 71.29 5.10 -4 10 -5 71.89 3.70 -5 -10 -5 375.36 8.50 5 -10 5 377.46 9.50 5 -10 5 373.86 8.60 -5 10 -5 384.26 9.00 5 10 5 366.46 10.70 6 -10 5 5.80 1.90 6 -10 5 4.60 2.40 6 10 5 4.00 2.60 -6 10 -5 5.20 2.20 7 -10 5 2.50 2.50 7 -10 5 0.20 1.90 7 10 5 0.60 2.50 -7 10 -5 -0.40 2.20 8 -10 5 12.00 2.80 8 -10 5 20.50 2.60 -8 10 -5 14.60 2.70 8 10 5 12.60 2.90 9 -10 5 48.60 3.80 9 -10 5 52.19 4.30 -9 10 -5 52.19 4.50 9 10 5 40.50 4.50 10 -10 5 11.00 2.80 10 -10 5 10.90 3.00 -10 10 -5 5.60 2.80 11 -10 5 0.90 2.70 11 -10 5 2.30 2.80 -11 10 -5 7.80 3.00 12 -10 5 2.20 2.90 12 -10 5 3.00 3.10 -12 10 -5 6.10 3.20 13 -10 5 75.99 5.70 -13 10 -5 82.69 6.00 -14 10 -5 4.90 3.90 14 -11 -5 14.30 4.00 13 -11 -5 27.20 4.20 -13 11 5 23.60 3.90 12 -11 -5 1.60 3.40 -12 11 5 7.50 3.20 11 -11 -5 5.50 3.40 -11 11 5 14.20 3.20 10 -11 -5 39.30 4.20 -10 11 5 32.10 3.50 -9 -11 5 24.00 3.10 9 -11 -5 24.90 3.50 -9 11 5 26.90 3.20 8 -11 -5 95.79 5.60 -8 -11 5 87.79 4.90 -8 11 5 86.49 6.50 -8 11 5 103.59 5.00 -7 -11 5 285.77 8.10 7 -11 -5 309.07 8.90 -7 11 5 312.37 8.10 -7 11 5 290.17 9.80 6 -11 -5 91.19 5.20 -6 -11 5 91.69 4.70 -6 11 5 90.89 6.20 -6 11 5 93.79 4.60 5 -11 -5 10.50 2.50 -5 -11 5 12.80 2.50 -5 11 5 14.60 2.30 -5 11 5 14.10 3.00 -4 -11 5 0.10 2.20 4 -11 -5 3.40 2.40 -4 11 5 6.20 2.60 -4 11 5 6.60 1.90 -3 -11 5 95.99 4.60 3 -11 -5 101.19 4.90 -3 11 5 89.69 3.80 -3 11 5 96.39 6.20 2 -11 -5 15.80 2.60 -2 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3.30 -7 14 5 6.30 2.80 -7 14 5 2.60 3.40 6 -14 -5 55.69 4.60 -6 -14 5 54.49 5.10 -6 14 5 39.30 4.70 -6 14 5 55.89 4.60 5 -14 -5 1.50 2.80 -5 -14 5 6.00 3.00 -5 14 5 -1.20 3.20 -5 14 5 2.90 2.40 4 -14 -5 182.68 7.20 -4 -14 5 177.08 6.90 -4 14 5 174.98 6.00 -4 14 5 181.18 9.10 3 -14 -5 2.50 2.80 -3 -14 5 3.60 3.00 -3 14 5 2.20 2.10 -3 14 5 4.60 3.30 -2 -14 5 1.70 2.90 2 -14 -5 0.90 2.80 -2 14 5 4.00 3.20 -2 14 5 2.80 2.00 -1 -14 5 26.50 3.60 1 -14 -5 18.00 3.20 -1 14 5 16.90 3.80 0 -14 -5 85.19 5.40 0 -14 5 82.79 5.50 0 14 5 76.39 7.20 1 -14 5 28.30 3.30 -1 -14 -5 29.40 3.30 -1 14 -5 32.00 2.60 1 14 5 22.20 3.90 -2 -14 -5 131.09 5.70 2 -14 5 139.49 6.00 -2 14 -5 126.19 4.90 2 14 5 142.09 8.10 -3 -14 -5 3.80 2.50 3 -14 5 3.00 3.20 -3 14 -5 5.00 2.20 3 14 5 3.90 3.30 4 -14 5 6.50 3.30 -4 14 -5 9.20 2.50 4 14 5 6.50 3.40 5 -14 5 2.10 3.20 5 14 5 -2.90 3.20 -5 14 -5 1.80 2.40 6 -14 5 79.19 6.00 -6 14 -5 78.99 5.00 6 14 5 69.89 7.40 7 -14 5 51.59 4.60 -7 14 -5 55.09 6.70 7 14 5 45.00 4.90 -7 14 -5 60.09 5.00 8 -14 5 71.79 6.00 -8 14 -5 76.49 5.50 -8 14 -5 75.09 7.10 8 14 5 77.29 7.40 9 -14 5 5.10 3.60 -9 14 -5 -0.40 2.90 10 -14 5 4.40 3.70 -10 14 -5 6.50 3.50 11 -14 5 -4.00 3.70 11 -14 5 -3.00 3.00 12 -14 5 15.60 4.40 10 -15 -5 19.60 5.00 9 -15 -5 16.50 4.20 -9 15 5 18.20 3.60 9 15 -5 11.70 4.40 8 -15 -5 45.20 4.60 -8 15 5 47.30 4.20 8 15 -5 47.70 5.40 -8 15 5 41.50 5.10 7 -15 -5 64.39 5.30 -7 -15 5 46.70 4.40 -7 15 5 60.99 5.20 7 15 -5 68.89 7.80 -7 15 5 55.59 5.50 -6 -15 5 2.10 3.20 6 -15 -5 -1.40 3.20 -6 15 5 -2.80 3.50 -6 15 5 3.10 2.60 5 -15 -5 7.10 3.50 -5 -15 5 3.80 3.20 -5 15 5 1.50 3.70 -5 15 5 5.40 2.70 -4 -15 5 109.19 6.20 4 -15 -5 112.09 6.50 -4 15 5 107.09 8.40 -4 15 5 117.09 5.30 3 -15 -5 -0.10 3.10 -3 -15 5 1.90 3.20 -3 15 5 4.40 2.30 -3 15 5 -0.70 3.50 2 -15 -5 136.79 6.60 -2 -15 5 139.49 6.60 -2 15 5 146.19 9.10 1 -15 -5 47.40 4.10 -1 -15 5 44.00 4.20 -1 15 5 38.90 4.80 0 -15 5 13.90 3.40 0 -15 -5 11.80 3.20 0 15 5 11.80 3.80 -1 -15 -5 6.20 3.00 1 -15 5 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3.20 1.80 -7 -3 9 4.10 1.10 7 -3 -9 5.60 1.90 -7 3 9 3.50 1.60 -7 3 9 3.00 1.70 -6 -3 9 38.70 2.00 -6 -3 9 35.30 2.80 6 -3 -9 39.00 3.10 -6 3 9 41.60 2.60 -6 3 9 39.30 2.60 5 -3 -9 25.50 2.20 -5 -3 9 25.20 2.00 -5 -3 9 29.60 1.80 -5 3 9 26.30 1.80 -5 3 9 30.70 2.30 -4 -3 9 410.56 8.30 -4 -3 9 417.46 8.70 4 -3 -9 412.76 9.00 -4 3 9 393.16 8.50 -4 3 9 405.96 8.60 -3 -3 9 54.19 2.10 -3 -3 9 46.40 2.50 3 -3 -9 67.19 2.90 -3 -3 9 52.39 2.80 -2 -3 9 3.00 1.20 -2 -3 9 3.40 1.00 -2 -3 9 4.10 1.30 2 -3 -9 5.50 1.40 -2 3 9 3.10 1.10 -2 3 9 2.10 1.00 -1 -3 9 77.99 2.80 1 -3 -9 83.29 2.90 -1 -3 9 81.99 2.60 -1 -3 9 80.39 3.00 -1 3 9 81.19 2.50 -1 3 9 79.59 2.60 0 -3 -9 259.17 5.70 0 -3 9 249.08 5.70 0 -3 9 253.97 5.60 0 -3 9 254.87 5.90 0 3 9 252.77 5.50 0 3 9 249.48 5.50 -1 -3 -9 872.61 16.70 1 -3 9 882.71 16.90 1 -3 9 886.21 16.90 1 -3 9 864.11 17.00 1 3 9 903.71 16.70 1 3 9 870.21 16.80 2 -3 9 91.19 3.00 2 -3 9 86.49 2.80 2 -3 9 86.59 3.00 -2 -3 -9 88.29 2.50 2 3 9 89.89 2.70 2 3 9 88.99 2.80 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-9 10.10 3.70 -15 -4 9 8.50 3.90 -15 4 9 13.70 3.80 14 -4 -9 4.30 3.30 -14 -4 9 2.00 3.50 -14 4 9 0.80 2.70 14 4 -9 -2.20 2.80 -14 4 9 4.40 3.30 13 -4 -9 3.80 2.90 -13 -4 9 5.50 3.30 -13 4 9 1.40 3.00 -13 4 9 5.70 2.60 -12 -4 9 197.98 7.00 12 -4 -9 199.98 7.20 -12 4 9 190.38 6.30 -12 4 9 201.98 6.90 11 -4 -9 17.60 3.10 -11 -4 9 23.10 3.20 -11 4 9 18.70 2.60 -11 4 9 17.10 2.90 -10 -4 9 374.76 9.20 10 -4 -9 358.76 9.50 -10 4 9 375.36 9.00 -10 4 9 354.66 8.80 -9 -4 9 12.30 2.50 9 -4 -9 11.80 2.60 -9 4 9 6.40 2.00 -9 4 9 10.00 2.30 -8 -4 9 111.59 4.40 8 -4 -9 109.59 4.50 -8 4 9 108.09 4.20 -8 4 9 108.39 4.10 -7 -4 9 3.70 1.90 -7 -4 9 1.40 1.20 7 -4 -9 3.60 2.00 6 -4 -9 153.88 5.00 -6 -4 9 150.38 3.60 -6 -4 9 147.49 4.60 -6 4 9 150.08 4.40 -6 4 9 144.29 4.30 -5 -4 9 60.39 2.20 5 -4 -9 60.79 3.30 -5 -4 9 59.19 3.00 -5 4 9 54.39 2.80 -5 4 9 58.49 2.70 4 -4 -9 1200.68 23.10 -4 -4 9 1195.58 23.20 -4 -4 9 1204.18 22.30 -4 -4 9 1206.08 22.80 -4 4 9 1146.39 22.50 -4 4 9 1200.28 22.80 3 -4 -9 260.27 6.30 -3 -4 9 262.27 5.60 -3 -4 9 254.67 6.20 -3 -4 9 257.27 6.00 -3 4 9 267.37 6.00 -3 4 9 260.37 5.70 -2 -4 9 320.77 7.30 -2 -4 9 313.37 6.90 2 -4 -9 306.77 7.10 -2 -4 9 320.67 6.60 -2 4 9 316.37 6.90 -2 4 9 315.77 6.60 -1 -4 9 28.70 1.80 1 -4 -9 30.00 2.20 -1 -4 9 28.90 2.30 -1 -4 9 27.60 2.10 -1 4 9 26.50 1.80 -1 4 9 32.80 1.80 0 -4 9 2562.74 48.30 0 -4 9 2613.34 48.10 0 -4 9 2572.34 48.10 0 -4 -9 2678.03 48.20 0 4 9 2547.25 48.00 0 4 9 2681.13 47.80 1 -4 9 18.80 1.60 1 -4 9 23.80 1.90 -1 -4 -9 21.40 1.80 1 4 9 18.60 1.40 1 4 9 19.10 1.60 2 -4 9 1803.52 33.10 2 -4 9 1732.63 33.10 -2 -4 -9 1795.22 32.80 2 -4 9 1789.12 33.20 2 4 9 1768.12 32.80 2 4 9 1742.83 32.80 3 -4 9 38.00 2.40 3 -4 9 37.90 2.50 -3 -4 -9 42.00 1.90 -3 -4 -9 38.40 1.70 3 -4 9 43.70 2.50 -3 4 -9 40.70 2.50 3 4 9 42.80 1.90 -4 -4 -9 224.88 4.80 4 -4 9 236.58 5.70 4 -4 9 225.98 5.50 -4 -4 -9 240.98 5.00 4 4 9 238.38 5.20 -4 4 -9 237.38 5.80 -5 -4 -9 48.70 1.90 5 -4 9 45.80 2.50 5 -4 9 46.90 2.80 5 4 9 47.20 2.10 -5 4 -9 45.90 2.90 6 -4 9 179.18 5.10 6 -4 9 172.08 4.70 6 4 9 182.38 4.50 -6 4 -9 178.48 5.10 7 -4 9 34.40 2.50 7 -4 9 35.20 2.50 -7 4 -9 29.80 2.50 7 4 9 36.40 2.30 8 -4 9 449.56 9.70 8 -4 9 458.65 10.30 8 4 9 472.05 9.70 -8 4 -9 450.95 10.20 9 -4 9 -3.00 1.90 -9 4 -9 0.30 2.10 9 4 9 3.20 1.70 10 -4 9 12.80 2.50 10 4 9 13.00 2.00 -10 4 -9 11.60 2.50 11 -4 9 -0.60 2.40 11 4 9 1.50 2.00 -11 4 -9 -3.40 2.30 12 -4 9 141.69 5.90 -12 4 -9 122.09 5.60 13 -4 9 20.60 3.40 -13 4 -9 21.60 3.10 14 -4 9 132.19 6.60 15 -4 9 12.40 3.50 16 -5 -9 28.30 4.40 -16 -5 9 29.60 4.60 -16 5 9 24.70 4.20 15 -5 -9 12.70 3.80 -15 -5 9 21.10 4.20 -15 5 9 12.10 3.20 -15 5 9 13.00 3.80 -14 -5 9 107.29 6.40 14 -5 -9 107.89 6.30 -14 5 9 102.39 5.60 -14 5 9 104.39 6.10 13 -5 -9 2.00 3.00 -13 -5 9 5.40 3.40 -13 5 9 8.10 3.10 -13 5 9 9.10 2.80 -12 -5 9 48.80 4.00 12 -5 -9 49.80 4.20 -12 5 9 47.10 3.70 -12 5 9 57.19 4.40 11 -5 -9 1.80 2.80 -11 -5 9 2.20 2.70 -11 5 9 1.20 2.30 -11 5 9 3.40 2.50 10 -5 -9 271.17 8.00 -10 -5 9 276.67 7.70 -10 5 9 262.27 7.40 -10 5 9 267.17 7.40 9 -5 -9 40.80 3.50 -9 -5 9 42.60 3.20 -9 5 9 41.90 2.90 -9 5 9 39.10 2.90 8 -5 -9 515.85 11.70 -8 -5 9 499.95 11.10 -8 5 9 507.25 10.90 -8 5 9 487.35 11.00 7 -5 -9 13.30 2.40 -7 -5 9 9.50 2.10 -7 5 9 11.90 1.90 -7 5 9 15.80 2.00 -6 -5 9 25.00 2.20 6 -5 -9 20.70 2.20 -6 5 9 26.50 2.10 -6 5 9 26.30 1.90 5 -5 -9 39.10 3.20 -5 -5 9 45.20 2.90 -5 -5 9 44.70 1.80 -5 -5 9 36.20 3.10 -5 5 9 40.80 2.40 -5 5 9 43.20 2.70 4 -5 -9 68.69 3.40 -4 -5 9 67.39 3.30 -4 -5 9 61.09 2.10 -4 -5 9 63.39 2.90 -4 5 9 66.59 2.90 -4 5 9 57.79 2.50 -3 -5 9 15.40 1.70 3 -5 -9 11.80 1.80 -3 -5 9 13.60 1.90 -3 -5 9 14.00 1.20 -3 5 9 13.30 1.60 -3 5 9 11.50 1.30 2 -5 -9 355.36 7.90 -2 -5 9 344.37 7.60 -2 -5 9 361.86 7.30 -2 -5 9 356.96 8.00 -2 5 9 350.96 7.20 -2 5 9 350.36 7.60 -1 -5 9 0.10 1.20 1 -5 -9 2.40 1.30 -1 -5 9 0.10 0.90 -1 -5 9 1.20 1.40 -1 5 9 0.50 1.70 -1 5 9 1.30 1.00 -1 5 9 1.50 0.90 0 -5 9 142.79 4.10 0 -5 -9 138.09 3.80 0 -5 9 137.39 3.60 0 -5 9 125.49 3.70 0 5 9 135.09 5.10 0 5 9 133.09 3.60 0 5 9 136.19 3.30 -1 -5 -9 11.90 1.40 1 -5 9 11.10 1.50 1 -5 9 9.90 1.40 1 -5 9 14.30 1.40 1 5 9 12.10 1.20 1 5 9 11.50 1.10 1 5 9 6.40 1.80 2 -5 9 0.70 1.30 2 -5 9 3.80 1.20 -2 -5 -9 1.60 1.10 2 -5 9 3.40 1.30 2 5 9 3.90 1.10 2 5 9 3.50 1.60 2 5 9 2.80 1.00 3 -5 9 57.09 2.80 -3 -5 -9 62.29 2.00 3 -5 9 56.39 2.70 -3 -5 -9 58.69 2.20 3 -5 9 57.09 2.80 -3 5 -9 63.59 3.00 3 5 9 56.89 2.20 3 5 9 59.69 2.40 -4 -5 -9 1170.68 22.60 4 -5 9 1217.68 23.50 4 -5 9 1222.48 23.40 -4 -5 -9 1222.78 22.50 -4 5 -9 1237.08 23.60 4 5 9 1255.97 22.90 5 -5 9 32.10 2.70 5 -5 9 31.40 2.60 5 5 9 33.30 1.90 -5 5 -9 29.90 2.30 6 -5 9 254.57 6.60 6 -5 9 258.27 6.30 6 5 9 267.47 5.80 -6 5 -9 263.47 6.70 7 -5 9 7.90 1.80 7 -5 9 7.90 1.90 -7 5 -9 7.80 2.10 7 5 9 12.40 1.50 8 -5 9 9.80 1.90 8 -5 9 5.70 2.00 -8 5 -9 7.40 2.20 8 5 9 8.60 1.60 9 -5 9 1.60 2.10 9 -5 9 0.70 1.90 9 5 9 1.70 1.70 -9 5 -9 1.70 2.20 10 -5 9 96.49 4.90 -10 5 -9 96.89 4.70 11 -5 9 88.79 5.10 -11 5 -9 89.19 5.00 12 -5 9 100.29 5.60 -12 5 -9 91.39 5.20 13 -5 9 6.20 3.00 -13 5 -9 9.50 3.00 14 -5 9 -0.30 3.10 -14 5 -9 -1.60 2.90 15 -5 9 -1.60 3.30 17 -6 -9 43.30 5.60 -16 -6 9 29.00 4.70 16 -6 -9 28.10 4.50 -16 6 9 29.10 4.40 -15 -6 9 -1.20 3.70 15 -6 -9 1.50 3.40 -15 6 9 4.50 3.50 -15 6 9 1.70 3.10 -14 -6 9 3.80 3.60 14 -6 -9 1.20 3.20 -14 6 9 1.50 3.30 -14 6 9 7.70 3.10 -13 -6 9 62.89 4.60 13 -6 -9 65.69 5.60 -13 6 9 61.49 5.00 -13 6 9 63.19 5.10 12 -6 -9 40.80 4.00 -12 -6 9 37.80 3.80 -12 6 9 40.60 3.70 -12 6 9 33.80 3.40 11 -6 -9 -1.70 2.80 -11 -6 9 2.50 2.80 -11 6 9 -1.10 2.40 -11 6 9 2.00 2.50 -10 -6 9 100.19 4.90 10 -6 -9 100.29 5.40 -10 6 9 92.79 4.60 -10 6 9 98.69 4.90 -9 -6 9 29.80 3.00 9 -6 -9 29.40 3.20 -9 6 9 29.20 2.80 -9 6 9 28.10 2.50 8 -6 -9 87.59 4.70 -8 -6 9 98.59 4.50 -8 6 9 93.19 4.00 -8 6 9 88.19 4.20 7 -6 -9 53.69 3.90 -7 -6 9 35.20 2.70 -7 6 9 51.19 3.40 6 -6 -9 386.56 9.30 -6 -6 9 393.56 8.80 -6 -6 9 389.76 9.20 -6 6 9 381.26 8.40 -6 6 9 380.46 8.80 -5 -6 9 51.39 3.40 -5 -6 9 46.00 3.00 5 -6 -9 47.30 3.10 -5 6 9 45.20 2.50 -5 6 9 47.70 2.90 -4 -6 9 332.97 6.60 -4 -6 9 342.97 7.50 -4 -6 9 339.47 8.00 4 -6 -9 325.07 8.00 -4 6 9 338.77 7.60 -4 6 9 317.67 7.00 -4 6 9 324.47 9.00 3 -6 -9 525.15 11.20 -3 -6 9 525.25 10.10 -3 -6 9 524.65 11.20 -3 -6 9 512.45 10.70 -3 6 9 515.85 12.30 -3 6 9 500.45 10.20 -3 6 9 515.45 10.70 2 -6 -9 6.40 1.60 -2 -6 9 6.20 1.50 -2 -6 9 4.70 1.70 -2 -6 9 7.70 1.10 -2 6 9 7.00 1.10 -2 6 9 5.60 1.90 -2 6 9 6.50 1.30 1 -6 -9 37.70 2.50 -1 -6 9 39.40 2.80 -1 -6 9 39.80 2.40 -1 -6 9 41.20 2.00 -1 6 9 39.70 1.90 -1 6 9 39.10 3.80 -1 6 9 41.10 2.20 0 -6 9 210.58 5.10 0 -6 9 211.78 4.90 0 -6 9 214.88 5.60 0 -6 -9 208.78 5.30 0 6 9 212.68 4.60 0 6 9 206.38 4.90 0 6 9 210.68 6.80 1 -6 9 12.30 1.40 1 -6 9 11.70 1.60 1 -6 9 11.80 1.70 -1 -6 -9 14.50 1.60 1 6 9 14.40 1.30 1 6 9 12.20 2.10 1 6 9 18.90 1.20 2 -6 9 379.36 8.40 2 -6 9 368.76 8.00 -2 -6 -9 370.26 7.80 2 -6 9 364.46 8.00 2 6 9 365.76 7.60 2 6 9 364.46 9.60 2 6 9 375.26 7.50 3 -6 9 56.79 2.80 -3 -6 -9 54.09 2.30 3 -6 9 54.99 3.00 3 -6 9 55.09 2.80 3 6 9 57.79 2.20 3 6 9 54.69 2.20 -3 6 -9 57.79 3.00 3 6 9 50.69 3.90 4 -6 9 71.19 3.20 4 -6 9 69.89 3.30 -4 -6 -9 65.19 2.30 4 6 9 76.89 2.40 -4 6 -9 73.19 3.30 4 6 9 71.89 4.50 5 -6 9 24.80 2.20 5 -6 9 27.30 2.20 5 6 9 27.70 1.80 -5 6 -9 25.00 2.20 5 6 9 20.90 2.60 6 -6 9 277.47 6.90 6 -6 9 267.77 6.90 6 6 9 278.87 6.00 -6 6 -9 269.77 7.00 7 -6 9 10.00 2.00 7 -6 9 3.60 1.90 7 6 9 9.40 1.40 -7 6 -9 3.10 2.10 8 -6 9 240.38 6.80 8 -6 9 250.47 6.60 -8 6 -9 242.68 7.00 9 -6 9 125.39 4.70 9 -6 9 123.69 5.10 -9 6 -9 127.29 5.30 10 -6 9 10.10 2.60 -10 6 -9 12.90 2.70 11 -6 9 3.50 2.70 -11 6 -9 1.50 2.70 12 -6 9 6.90 2.90 -12 6 -9 3.50 2.90 13 -6 9 5.20 3.10 -13 6 -9 5.70 3.00 14 -6 9 98.29 6.00 -14 6 -9 111.49 5.90 -15 6 -9 2.30 4.30 -16 -7 9 26.90 4.70 16 -7 -9 27.10 4.50 -16 7 9 29.00 4.30 15 -7 -9 26.80 4.40 -15 -7 9 23.80 4.30 -15 7 9 23.30 3.70 -15 7 9 19.80 4.00 -14 -7 9 59.99 4.80 14 -7 -9 51.19 4.80 -14 7 9 50.39 4.20 -14 7 9 50.59 4.20 -13 -7 9 70.39 5.80 13 -7 -9 72.09 5.80 -13 7 9 69.19 5.50 -13 7 9 69.19 5.30 12 -7 -9 5.60 3.10 -12 -7 9 3.80 3.00 -12 7 9 6.30 2.80 -12 7 9 2.70 2.80 -11 -7 9 4.60 2.80 11 -7 -9 0.20 2.80 -11 7 9 -1.10 2.40 -11 7 9 -2.40 2.50 -10 -7 9 33.60 3.20 10 -7 -9 31.70 3.60 -10 7 9 28.80 3.10 -10 7 9 29.80 2.90 -9 -7 9 11.00 2.60 9 -7 -9 12.30 2.90 -9 7 9 12.20 2.50 -9 7 9 11.00 2.20 -8 -7 9 252.17 6.90 8 -7 -9 246.88 7.20 -8 7 9 254.27 6.50 -8 7 9 234.28 6.90 -7 -7 9 154.28 5.60 -7 -7 9 159.58 5.10 7 -7 -9 156.88 5.70 -7 7 9 145.39 4.50 -7 7 9 151.68 5.20 6 -7 -9 177.08 5.80 -6 -7 9 177.38 5.80 -6 -7 9 171.48 5.20 -6 7 9 171.38 4.70 -6 7 9 175.18 6.70 -6 7 9 165.88 5.20 -5 -7 9 14.50 2.00 5 -7 -9 14.00 2.30 -5 -7 9 11.90 2.30 -5 7 9 11.90 1.90 -5 7 9 11.80 1.50 -5 7 9 8.90 2.40 -4 -7 9 22.00 2.00 4 -7 -9 20.90 2.30 -4 -7 9 15.40 2.10 -4 7 9 20.30 2.60 -4 7 9 20.80 1.50 3 -7 -9 9.60 1.80 -3 -7 9 6.40 1.60 -3 -7 9 9.40 1.00 -3 -7 9 9.50 2.00 -3 7 9 8.20 2.20 -3 7 9 8.90 1.60 -3 7 9 11.00 1.20 2 -7 -9 348.17 8.30 -2 -7 9 354.46 7.80 -2 -7 9 363.76 7.20 -2 -7 9 357.96 8.40 -2 7 9 349.87 7.80 -2 7 9 351.16 7.20 -2 7 9 368.66 9.70 -1 -7 9 433.16 8.70 -1 -7 9 433.26 9.10 1 -7 -9 438.36 9.60 -1 -7 9 423.76 9.60 -1 7 9 440.86 8.50 -1 7 9 421.66 9.00 -1 7 9 445.56 11.10 0 -7 9 57.19 2.70 0 -7 9 61.69 2.40 0 -7 -9 61.19 2.90 0 -7 9 64.29 3.40 0 7 9 63.39 4.30 0 7 9 62.29 2.50 0 7 9 59.19 2.00 1 -7 9 67.19 3.40 1 -7 9 64.89 2.60 1 -7 9 65.89 2.80 -1 -7 -9 64.99 2.90 1 7 9 61.89 2.40 1 7 9 70.69 4.40 1 7 9 65.49 2.10 2 -7 9 60.49 3.30 2 -7 9 50.99 2.60 -2 -7 -9 49.10 2.60 2 -7 9 55.49 2.80 2 7 9 55.39 2.30 2 7 9 54.59 4.20 2 7 9 55.89 2.10 -2 7 -9 56.79 3.00 3 -7 9 1.80 1.50 -3 -7 -9 4.80 1.30 3 -7 9 3.20 1.40 3 -7 9 4.00 1.80 3 7 9 3.90 1.10 -3 7 -9 4.90 1.70 3 7 9 5.20 2.00 3 7 9 3.20 1.10 4 -7 9 87.89 3.60 4 -7 9 81.99 3.90 4 -7 9 82.09 3.40 -4 -7 -9 79.69 2.80 -4 7 -9 91.69 3.80 4 7 9 89.89 5.10 4 7 9 89.79 2.70 5 -7 9 520.95 11.60 5 -7 9 528.15 11.40 -5 7 -9 548.65 11.60 5 7 9 531.45 12.90 5 7 9 542.35 10.60 6 -7 9 175.88 5.40 6 -7 9 164.98 5.40 -6 7 -9 172.68 5.60 6 7 9 182.18 6.80 6 7 9 183.58 4.30 7 -7 9 51.59 3.70 7 -7 9 58.49 3.80 7 7 9 48.10 4.70 -7 7 -9 52.99 3.80 8 -7 9 83.69 4.30 8 -7 9 81.49 4.30 -8 7 -9 86.09 4.50 9 -7 9 6.80 2.30 9 -7 9 7.80 2.40 -9 7 -9 10.60 2.60 10 -7 9 190.08 6.50 10 -7 9 184.28 6.80 -10 7 -9 178.28 6.60 11 -7 9 415.86 10.60 -11 7 -9 421.76 10.70 12 -7 9 94.89 5.70 -12 7 -9 92.99 5.70 13 -7 9 16.00 3.40 -13 7 -9 14.20 3.40 14 -7 9 4.10 3.30 -14 7 -9 1.80 3.20 -15 7 -9 5.10 3.40 -16 -8 9 5.80 4.60 -16 8 9 5.40 3.90 15 -8 -9 -0.20 3.80 -15 -8 9 7.10 4.10 -15 8 9 7.30 4.00 -15 8 9 4.70 3.60 14 -8 -9 7.80 3.80 -14 -8 9 6.60 3.80 -14 8 9 6.10 3.20 -14 8 9 6.00 3.30 13 -8 -9 0.10 3.50 -13 -8 9 -3.10 3.30 -13 8 9 2.80 3.00 -13 8 9 2.40 3.00 12 -8 -9 25.50 3.90 -12 -8 9 20.50 3.40 -12 8 9 21.10 3.40 -12 8 9 23.40 3.20 -11 -8 9 134.09 5.90 11 -8 -9 139.39 6.60 -11 8 9 137.99 5.60 -11 8 9 144.69 6.00 10 -8 -9 2.90 2.90 -10 -8 9 5.90 2.80 -10 8 9 7.00 2.70 -10 8 9 6.60 2.30 -9 -8 9 52.89 4.20 9 -8 -9 47.20 4.00 -9 8 9 49.80 3.60 -9 8 9 50.69 4.30 -8 -8 9 15.50 2.50 -8 -8 9 11.80 2.70 8 -8 -9 12.30 2.90 -8 8 9 19.30 2.30 -8 8 9 16.80 2.50 7 -8 -9 2.40 2.50 -7 -8 9 7.70 2.60 -7 -8 9 7.90 2.20 -7 8 9 13.40 1.80 -7 8 9 6.80 2.60 -7 8 9 10.00 2.20 -6 -8 9 127.79 4.60 -6 -8 9 131.69 5.20 6 -8 -9 134.49 5.40 -6 8 9 126.39 4.70 -6 8 9 127.09 3.90 -6 8 9 130.99 6.30 5 -8 -9 312.07 8.30 -5 -8 9 318.47 8.20 -5 -8 9 310.37 7.40 -5 8 9 323.37 9.50 -5 8 9 311.17 6.90 -5 8 9 321.17 7.70 -4 -8 9 3.30 2.10 4 -8 -9 5.50 2.00 -4 -8 9 7.00 1.80 -4 8 9 7.80 1.30 -4 8 9 4.00 2.20 -4 8 9 7.40 1.80 3 -8 -9 42.10 3.40 -3 -8 9 47.30 2.80 -3 -8 9 44.70 3.40 -3 8 9 47.50 4.60 -3 8 9 43.20 2.00 -3 8 9 42.30 2.80 -2 -8 9 -0.60 1.60 -2 -8 9 -0.60 1.40 -1 -8 9 4.50 1.90 1 -8 -9 4.30 1.80 -1 -8 9 6.80 1.50 -1 -8 9 5.50 1.10 -1 8 9 5.40 2.20 -1 8 9 7.10 1.00 -1 8 9 7.00 1.40 0 -8 9 2.80 1.40 0 -8 -9 0.80 1.70 0 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5.80 2.90 -11 8 -9 6.20 3.00 12 -8 9 5.20 3.00 -12 8 -9 9.30 3.20 13 -8 9 -1.70 3.00 -13 8 -9 3.00 3.10 14 -8 9 23.00 4.60 -14 8 -9 30.00 3.90 -15 8 -9 34.10 4.50 15 -9 -9 45.00 5.00 -15 -9 9 44.90 6.10 -14 -9 9 3.90 3.70 14 -9 -9 -0.80 3.70 -14 9 9 1.30 3.30 -13 -9 9 188.88 7.20 13 -9 -9 192.28 8.10 -13 9 9 174.38 7.20 -12 -9 9 6.60 3.20 12 -9 -9 6.30 3.60 -12 9 9 12.90 3.20 -12 9 9 13.10 4.40 11 -9 -9 -4.90 3.00 -11 -9 9 1.70 3.00 -11 9 9 1.80 3.00 -11 9 9 4.60 2.90 10 -9 -9 1.30 3.10 -10 -9 9 2.70 2.70 -10 9 9 -1.00 2.80 -10 9 9 0.20 2.60 -9 -9 9 53.19 4.20 9 -9 -9 34.50 3.70 -9 9 9 43.20 3.50 -9 9 9 48.60 4.60 -8 -9 9 0.30 2.30 8 -9 -9 2.90 2.60 -8 -9 9 2.00 2.70 -8 9 9 0.40 2.30 -8 9 9 -0.90 2.60 7 -9 -9 192.28 6.70 -7 -9 9 189.58 6.50 -7 -9 9 191.08 5.80 -7 9 9 177.18 7.60 -7 9 9 190.38 6.10 6 -9 -9 55.09 4.40 -6 -9 9 66.49 3.70 -6 -9 9 64.19 4.40 -6 9 9 56.89 5.40 -6 9 9 61.09 3.90 -5 -9 9 9.40 2.60 -5 -9 9 6.90 2.00 5 -9 -9 6.80 2.50 -5 9 9 5.30 2.60 -5 9 9 5.50 1.90 -4 -9 9 1.80 2.30 -4 -9 9 2.50 1.80 4 -9 -9 5.00 2.20 -4 9 9 4.10 1.70 -4 9 9 3.80 2.40 -3 -9 9 132.39 4.20 -3 -9 9 138.39 5.20 3 -9 -9 140.89 5.10 -3 9 9 125.99 4.30 -3 9 9 137.19 6.40 -2 -9 9 33.10 3.00 2 -9 -9 41.30 3.50 -2 -9 9 38.50 2.70 -2 9 9 46.70 4.90 -2 9 9 43.00 2.80 -1 -9 9 797.42 15.70 -1 -9 9 805.22 16.70 1 -9 -9 801.42 16.50 -1 9 9 775.92 15.70 -1 9 9 809.12 18.30 0 -9 9 79.69 2.70 0 -9 9 71.29 3.20 0 -9 9 73.99 4.10 0 -9 -9 70.59 3.60 0 9 9 76.19 5.20 0 9 9 75.09 3.00 1 -9 9 151.38 4.40 1 -9 9 146.09 4.10 1 -9 9 160.48 5.40 -1 -9 -9 147.69 4.90 -1 9 -9 152.08 4.60 1 9 9 162.18 4.20 1 9 9 154.38 6.60 2 -9 9 36.10 2.50 2 -9 9 33.70 2.90 -2 -9 -9 37.00 2.90 2 -9 9 38.90 3.60 -2 9 -9 35.30 3.00 2 9 9 35.70 2.20 2 9 9 25.70 3.10 3 -9 9 36.00 3.10 -3 -9 -9 39.10 2.90 3 -9 9 41.90 2.90 3 -9 9 38.70 2.70 3 9 9 39.30 4.90 -3 9 -9 35.20 2.60 3 9 9 40.30 2.20 4 -9 9 161.48 4.80 4 -9 9 158.18 5.60 4 -9 9 158.28 4.80 -4 9 -9 155.88 5.20 4 9 9 156.88 7.00 5 -9 9 398.26 9.10 5 -9 9 404.86 9.80 5 -9 9 409.26 9.20 5 9 9 390.66 11.10 -5 9 -9 405.66 9.50 6 -9 9 6.00 2.50 6 -9 9 5.30 2.00 6 9 9 2.30 2.50 -6 9 -9 3.20 2.10 7 -9 9 2.90 2.10 7 -9 9 -1.10 2.20 -7 9 -9 1.20 2.40 7 9 9 -1.60 2.40 8 -9 9 11.10 2.60 8 -9 9 11.20 2.50 -8 9 -9 9.30 2.70 8 9 9 7.10 2.80 9 -9 9 -1.40 2.30 9 -9 9 1.90 2.50 -9 9 -9 0.70 2.60 10 -9 9 19.10 3.10 10 -9 9 28.40 3.30 -10 9 -9 27.20 3.50 11 -9 9 142.69 6.30 -11 9 -9 148.29 6.60 12 -9 9 14.80 3.30 -12 9 -9 18.10 3.60 13 -9 9 14.70 3.50 -13 9 -9 16.60 3.70 -14 9 -9 3.00 3.60 14 -10 -9 2.50 4.00 13 -10 -9 11.30 3.90 -13 10 9 12.80 3.70 12 -10 -9 4.70 3.50 -12 10 9 4.50 3.20 11 -10 -9 130.79 6.40 -11 10 9 130.99 6.30 10 -10 -9 2.50 3.30 -10 10 9 0.80 2.80 -9 -10 9 81.99 5.40 -9 -10 9 80.29 5.50 9 -10 -9 71.49 5.50 -9 10 9 72.89 5.10 -8 -10 9 1.60 2.80 8 -10 -9 0.20 2.80 -8 -10 9 0.00 2.40 -8 10 9 -3.30 2.70 -8 10 9 2.40 2.50 -7 -10 9 32.20 3.40 7 -10 -9 33.40 3.60 -7 -10 9 32.30 2.80 -7 10 9 26.20 3.60 -7 10 9 34.00 3.10 6 -10 -9 2.40 2.60 -6 -10 9 5.70 2.10 -6 -10 9 4.20 2.60 -6 10 9 5.80 2.20 -6 10 9 5.30 2.80 -5 -10 9 -0.50 1.90 -5 -10 9 2.40 2.40 5 -10 -9 2.40 2.40 -5 10 9 0.90 2.60 -5 10 9 3.10 2.00 -4 -10 9 17.60 2.20 -4 -10 9 12.80 2.40 4 -10 -9 17.30 2.80 -4 10 9 13.40 3.00 -4 10 9 20.80 2.30 3 -10 -9 347.27 8.90 -3 -10 9 348.17 7.80 -3 -10 9 335.57 8.90 -3 10 9 332.07 8.10 -3 10 9 359.36 10.60 2 -10 -9 74.29 4.20 -2 -10 9 48.20 4.10 -2 -10 9 51.49 3.20 -2 10 9 65.29 3.20 -1 -10 9 20.20 2.00 -1 -10 9 17.80 2.70 1 -10 -9 17.00 2.50 -1 10 9 21.10 1.90 -1 10 9 13.20 2.90 0 -10 9 17.50 2.50 0 -10 9 23.80 2.10 0 -10 -9 19.90 2.40 0 10 9 20.20 3.20 0 10 9 20.30 1.80 -1 -10 -9 220.88 6.40 1 -10 9 227.98 6.90 1 -10 9 230.18 5.80 1 10 9 231.98 5.50 1 10 9 229.68 8.30 -1 10 -9 212.28 6.00 2 -10 9 170.78 6.00 2 -10 9 172.08 4.70 2 -10 9 168.68 4.90 -2 -10 -9 162.78 5.20 2 10 9 173.38 7.60 -2 10 -9 171.78 5.30 2 10 9 169.38 4.50 3 -10 9 400.46 9.00 3 -10 9 409.26 10.10 3 -10 9 409.16 9.00 -3 -10 -9 401.76 9.20 3 10 9 418.46 11.80 -3 10 -9 400.56 9.40 4 -10 9 0.80 1.80 4 -10 9 3.40 1.80 4 -10 9 1.60 2.50 -4 10 -9 3.90 2.00 4 10 9 2.70 2.70 5 -10 9 49.40 3.50 5 -10 9 51.59 3.50 5 -10 9 52.99 4.30 -5 10 -9 53.29 3.90 5 10 9 47.50 5.60 6 -10 9 20.90 2.40 6 -10 9 14.50 2.80 6 10 9 11.40 3.10 -6 10 -9 18.50 2.70 7 -10 9 68.29 4.60 7 -10 9 59.69 4.10 7 10 9 57.99 6.00 -7 10 -9 51.79 4.60 8 -10 9 17.30 2.70 8 -10 9 23.80 3.10 -8 10 -9 16.40 3.00 8 10 9 19.70 3.40 9 -10 9 106.99 5.30 9 -10 9 113.89 5.80 -9 10 -9 119.29 5.90 10 -10 9 -0.90 2.80 10 -10 9 -0.40 2.60 -10 10 -9 3.40 3.00 11 -10 9 -1.30 2.80 -11 10 -9 2.80 3.10 12 -10 9 95.09 6.00 -12 10 -9 98.89 6.40 13 -10 9 19.00 4.10 -13 10 -9 10.20 3.80 13 -11 -9 47.20 5.00 12 -11 -9 17.10 4.00 -12 11 9 23.40 3.80 11 -11 -9 0.40 3.60 -11 11 9 -0.80 2.90 10 -11 -9 12.70 3.50 -10 11 9 12.40 3.20 9 -11 -9 46.40 4.30 -9 -11 9 42.40 4.10 -9 11 9 49.70 3.90 -8 -11 9 192.28 7.00 8 -11 -9 188.88 7.40 -8 11 9 176.78 8.30 -8 11 9 182.98 6.60 -7 -11 9 41.30 3.80 7 -11 -9 37.70 3.80 -7 11 9 28.60 3.80 -7 11 9 42.70 3.40 6 -11 -9 5.70 2.90 -6 -11 9 8.30 3.00 -6 11 9 8.60 2.40 -6 11 9 6.70 3.00 5 -11 -9 68.29 5.00 -5 -11 9 60.89 4.30 -5 11 9 65.59 6.20 -5 11 9 61.49 4.10 4 -11 -9 74.89 4.90 -4 -11 9 86.19 5.10 -4 11 9 74.29 6.10 -4 11 9 81.09 4.20 -3 -11 9 42.50 3.80 3 -11 -9 43.80 3.80 -3 11 9 49.90 5.60 -3 11 9 46.10 3.40 -2 -11 9 6.30 2.40 2 -11 -9 5.60 2.50 -2 11 9 3.90 2.80 -2 11 9 5.40 1.80 -1 -11 9 29.00 3.20 1 -11 -9 32.10 3.00 -1 11 9 29.80 2.20 -1 11 9 23.40 3.40 0 -11 -9 2.30 2.20 0 -11 9 0.40 2.20 0 11 9 0.40 2.70 0 11 -9 1.50 1.70 0 11 9 0.50 1.50 1 -11 9 293.47 8.20 -1 -11 -9 308.47 7.90 1 11 9 301.37 6.90 -1 11 -9 301.07 7.50 1 11 9 299.17 10.10 2 -11 9 12.00 2.80 -2 -11 -9 11.60 2.20 2 11 9 8.40 3.00 -2 11 -9 11.20 2.10 3 -11 9 -3.60 2.50 3 -11 9 0.90 1.60 -3 11 -9 2.90 2.00 3 11 9 3.40 2.90 4 -11 9 22.50 3.10 4 -11 9 25.10 2.30 4 -11 9 27.50 3.80 4 11 9 21.70 3.50 -4 11 -9 24.80 2.70 5 -11 9 44.30 3.50 5 -11 9 55.29 4.00 5 -11 9 55.49 4.70 -5 11 -9 51.49 4.30 5 11 9 50.19 6.00 6 -11 9 34.20 2.90 6 -11 9 34.30 3.60 6 -11 9 34.10 3.20 -6 11 -9 34.80 3.30 6 11 9 32.20 4.00 7 -11 9 0.50 2.80 7 -11 9 6.80 2.30 -7 11 -9 6.00 2.60 7 11 9 -1.00 2.90 8 -11 9 3.80 2.50 8 -11 9 5.80 3.00 8 11 9 1.40 3.10 -8 11 -9 6.30 2.80 9 -11 9 39.90 3.90 9 -11 9 43.10 3.70 -9 11 -9 40.80 3.80 10 -11 9 32.40 3.50 10 -11 9 30.60 3.70 -10 11 -9 32.40 3.90 11 -11 9 19.90 3.40 11 -11 9 22.40 3.60 -11 11 -9 22.00 3.70 12 -11 9 52.69 4.50 -12 11 -9 54.89 4.60 12 -12 -9 58.49 5.20 11 -12 -9 24.70 4.40 -11 12 9 28.40 4.00 10 -12 -9 42.00 4.70 -10 -12 9 31.10 4.30 -10 12 9 42.20 4.00 9 -12 -9 3.10 3.40 -9 -12 9 7.00 3.40 -9 12 9 10.70 3.10 8 -12 -9 5.40 3.40 -8 -12 9 6.40 3.30 -8 12 9 -0.30 3.10 -8 12 9 4.70 2.70 7 -12 -9 36.40 4.00 -7 -12 9 33.70 3.80 -7 12 9 45.10 3.60 -7 12 9 23.00 3.90 6 -12 -9 11.60 3.20 -6 -12 9 3.30 3.10 -6 12 9 10.00 3.20 -6 12 9 10.20 2.60 -5 -12 9 152.88 6.40 5 -12 -9 147.39 6.60 -5 12 9 152.18 8.10 -5 12 9 155.38 5.80 -4 -12 9 297.27 8.80 4 -12 -9 300.67 8.90 -4 12 9 304.17 7.90 -4 12 9 303.97 10.80 -3 -12 9 102.09 5.50 3 -12 -9 92.49 5.30 -3 12 9 93.59 7.00 -3 12 9 91.29 4.30 -2 -12 9 145.89 6.20 2 -12 -9 145.89 5.90 -2 12 9 148.69 7.80 -2 12 9 157.38 5.00 1 -12 -9 5.90 2.60 -1 -12 9 8.60 3.00 1 12 -9 8.60 1.90 -1 12 9 7.30 1.90 -1 12 9 8.50 3.20 0 -12 9 173.78 6.60 0 -12 -9 170.58 6.00 0 12 -9 173.48 5.30 0 12 9 171.78 8.30 0 12 9 168.48 5.00 1 -12 9 248.28 7.70 -1 -12 -9 237.58 7.10 -1 12 -9 233.68 6.60 1 12 9 232.08 9.50 2 -12 9 129.49 5.90 -2 -12 -9 122.99 4.90 2 12 9 124.89 7.40 -2 12 -9 129.79 5.00 3 -12 9 2.70 2.50 3 12 9 1.60 3.00 -3 12 -9 1.70 2.00 4 -12 9 24.90 3.40 4 12 9 21.00 3.70 -4 12 -9 28.50 2.90 5 -12 9 -3.10 2.80 5 -12 9 -1.30 1.90 -5 12 -9 -0.90 2.30 5 12 9 -4.80 3.00 6 -12 9 52.29 4.30 6 -12 9 46.70 3.80 6 12 9 43.50 4.60 -6 12 -9 46.70 3.80 7 -12 9 83.29 4.70 7 -12 9 93.99 5.80 -7 12 -9 87.79 5.40 7 12 9 85.69 7.40 8 -12 9 57.69 4.50 8 -12 9 66.69 5.50 -8 12 -9 65.29 5.40 8 12 9 60.89 6.70 9 -12 9 53.79 4.00 9 -12 9 56.19 4.60 -9 12 -9 48.70 4.20 10 -12 9 24.20 3.40 10 -12 9 27.90 4.00 -10 12 -9 29.80 3.80 11 -12 9 5.20 3.50 11 -12 9 2.70 3.00 -11 12 -9 0.00 3.30 12 -12 9 3.00 3.90 11 -13 -9 -0.20 3.80 -10 -13 9 0.80 3.70 10 -13 -9 -1.90 3.60 -10 13 9 4.80 3.20 9 -13 -9 0.70 3.10 -9 -13 9 4.40 3.40 -9 13 9 1.50 2.90 -8 -13 9 182.48 7.50 8 -13 -9 170.18 7.60 -8 13 9 169.18 9.00 -8 13 9 179.98 7.00 7 -13 -9 -1.30 3.10 -7 -13 9 1.90 3.30 -7 13 9 -1.90 3.30 -7 13 9 4.00 2.70 6 -13 -9 144.19 6.40 -6 -13 9 150.68 6.80 -6 13 9 153.68 6.10 -6 13 9 151.78 8.70 5 -13 -9 -3.40 3.00 -5 -13 9 3.40 3.10 -5 13 9 1.50 2.40 -5 13 9 -3.50 3.20 -4 -13 9 129.19 6.30 4 -13 -9 126.29 6.30 -4 13 9 126.59 7.80 -4 13 9 126.49 5.30 -3 -13 9 0.10 3.00 3 -13 -9 4.70 2.70 -3 13 9 3.00 2.10 -3 13 9 4.50 3.30 2 -13 -9 24.80 3.40 -2 -13 9 18.80 3.40 -2 13 9 30.20 2.70 -2 13 9 21.20 3.90 1 -13 -9 -0.40 2.60 -1 -13 9 0.70 2.80 -1 13 9 1.50 1.90 -1 13 9 0.50 3.10 0 -13 9 8.50 3.20 0 -13 -9 6.70 2.60 0 13 9 7.90 3.40 0 13 -9 8.00 2.10 1 -13 9 12.40 3.20 -1 -13 -9 13.70 2.80 1 13 9 11.70 3.60 -1 13 -9 12.10 2.30 -2 -13 -9 30.00 3.20 2 -13 9 38.10 3.90 -2 13 -9 34.20 3.00 2 13 9 31.50 4.30 3 -13 9 2.70 3.00 -3 13 -9 3.50 2.20 3 13 9 0.50 3.20 4 -13 9 190.68 7.30 4 13 9 185.68 9.20 -4 13 -9 179.08 6.40 5 -13 9 0.00 3.10 5 13 9 5.50 3.50 -5 13 -9 8.30 2.70 6 -13 9 406.56 11.00 6 13 9 376.76 12.90 -6 13 -9 402.86 10.40 7 -13 9 3.00 3.50 -7 13 -9 3.50 2.90 7 13 9 1.20 3.60 8 -13 9 16.40 3.70 8 -13 9 7.50 2.70 -8 13 -9 10.40 3.30 8 13 9 7.00 3.80 9 -13 9 22.20 4.00 9 -13 9 21.30 3.30 -9 13 -9 22.30 3.60 10 -13 9 32.00 3.80 10 -13 9 41.10 4.50 -10 13 -9 45.80 4.50 11 -13 9 9.10 3.20 11 -13 9 17.80 4.00 10 -14 -9 33.50 4.90 9 -14 -9 6.80 3.70 -9 -14 9 2.20 3.70 -9 14 9 6.80 3.30 -8 -14 9 3.20 3.70 8 -14 -9 -0.80 3.30 -8 14 9 1.60 2.90 -8 14 9 -5.30 3.40 7 -14 -9 15.90 3.90 -7 -14 9 11.90 3.70 -7 14 9 19.60 3.30 -7 14 9 12.60 4.00 -6 -14 9 74.49 5.80 6 -14 -9 82.99 6.10 -6 14 9 69.49 7.80 -6 14 9 74.79 5.20 -5 -14 9 92.29 6.00 5 -14 -9 82.89 6.00 -5 14 9 90.09 5.20 -5 14 9 83.19 8.10 -4 -14 9 283.87 9.10 4 -14 -9 287.17 9.20 -4 14 9 272.17 11.30 -4 14 9 280.57 8.00 -3 -14 9 10.40 3.30 3 -14 -9 14.30 3.40 -3 14 9 10.70 2.50 -3 14 9 5.40 3.70 2 -14 -9 83.99 5.50 -2 -14 9 76.89 5.30 -2 14 9 90.69 8.10 -2 14 9 85.69 4.30 -1 -14 9 2.90 3.20 1 -14 -9 -0.20 2.70 -1 14 9 0.70 3.40 0 -14 -9 99.19 5.40 0 -14 9 100.59 5.60 0 14 9 111.99 7.90 1 -14 9 11.20 3.40 -1 -14 -9 14.50 3.00 1 14 9 16.70 3.90 -1 14 -9 13.70 2.50 2 -14 9 154.68 7.00 -2 14 -9 142.29 5.60 2 14 9 153.68 9.10 3 -14 9 5.50 3.00 3 14 9 4.40 3.70 -3 14 -9 4.40 2.50 4 -14 9 18.10 3.80 4 14 9 18.20 4.20 -4 14 -9 22.00 3.10 5 -14 9 16.10 3.60 5 14 9 11.70 4.10 -5 14 -9 14.90 3.00 6 -14 9 2.00 3.30 -6 14 -9 4.70 3.00 6 14 9 2.30 3.80 7 -14 9 13.50 3.90 7 14 9 9.10 4.20 -7 14 -9 14.00 3.30 8 -14 9 26.10 4.30 -8 14 -9 26.50 3.70 8 14 9 21.30 4.50 9 -14 9 6.40 3.90 -9 14 -9 3.80 3.50 10 -14 9 51.99 5.10 11 -14 9 1.90 3.90 9 -15 -9 21.60 6.20 -9 -15 9 28.50 4.50 -8 -15 9 103.09 6.80 8 -15 -9 86.49 6.30 -8 15 9 101.29 6.10 -8 15 9 86.69 8.80 -7 -15 9 24.30 4.20 7 -15 -9 25.70 4.40 -7 15 9 34.40 3.80 -7 15 9 19.30 4.50 -6 -15 9 4.30 3.60 6 -15 -9 0.90 3.50 -6 15 9 3.10 2.80 -6 15 9 -1.40 3.70 -5 -15 9 12.70 3.90 5 -15 -9 8.90 3.50 -5 15 9 9.20 4.20 -5 15 9 14.70 3.00 -4 -15 9 5.90 3.40 4 -15 -9 0.40 3.20 -4 15 9 4.40 2.60 -4 15 9 -0.40 3.70 3 -15 -9 27.20 4.00 -3 -15 9 22.10 3.80 -3 15 9 26.60 3.10 -3 15 9 22.20 4.60 -2 -15 9 176.18 7.60 2 -15 -9 163.28 7.10 -2 15 9 173.48 10.00 1 -15 -9 2.30 3.00 -1 -15 9 -0.60 3.40 -1 15 9 2.70 3.80 0 -15 -9 5.20 3.00 0 -15 9 -1.90 3.40 0 15 9 0.00 3.70 -1 -15 -9 76.59 5.30 1 -15 9 101.29 6.40 1 15 9 85.09 8.00 2 -15 9 5.00 3.60 2 15 9 -2.70 3.70 -2 15 -9 3.60 2.40 3 -15 9 -0.20 3.50 3 15 9 -2.30 3.80 -3 15 -9 1.70 2.50 4 -15 9 155.18 7.50 -4 15 -9 158.58 6.40 4 15 9 155.18 9.80 5 -15 9 24.50 4.20 -5 15 -9 26.50 3.40 5 15 9 14.60 4.60 6 -15 9 68.69 6.20 6 15 9 49.99 5.60 -6 15 -9 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3 -10 19.40 1.80 5 -3 10 544.85 11.20 -5 -3 -10 571.84 11.00 5 -3 10 548.55 11.60 5 3 10 556.74 11.20 -5 3 -10 560.74 11.60 6 -3 10 3.70 1.60 6 -3 10 6.70 1.40 -6 -3 -10 7.00 1.30 6 3 10 6.90 1.40 -6 3 -10 4.00 1.70 7 -3 10 8.20 1.90 -7 -3 -10 5.40 1.50 7 -3 10 5.80 1.40 -7 3 -10 5.70 1.90 7 3 10 5.60 1.60 8 -3 10 10.90 2.10 8 -3 10 12.70 2.10 8 3 10 9.50 1.80 -8 3 -10 13.10 2.20 9 -3 10 228.68 6.60 9 3 10 239.48 6.20 -9 3 -10 247.78 6.70 10 -3 10 -2.80 2.20 -10 3 -10 1.10 2.10 10 3 10 1.40 1.90 11 -3 10 125.69 5.60 -11 3 -10 131.39 5.20 11 3 10 130.89 5.00 12 -3 10 27.10 3.30 -12 3 -10 20.40 2.90 12 3 10 23.70 2.90 13 -3 10 118.49 6.00 13 3 10 117.29 6.40 14 -3 10 31.10 3.80 15 -3 10 3.60 3.20 17 -4 -10 94.29 8.80 16 -4 -10 7.10 3.90 -16 -4 10 4.10 4.20 -16 4 10 4.60 4.00 15 -4 -10 6.20 3.60 -15 -4 10 2.80 3.90 -15 4 10 6.70 3.70 14 -4 -10 -3.10 3.30 -14 -4 10 -0.10 3.50 -14 4 10 1.70 2.80 -14 4 10 1.30 3.30 14 4 -10 -6.90 2.80 -13 -4 10 49.50 4.30 13 -4 -10 53.49 4.50 -13 4 10 57.59 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12 -11 -10 68.49 5.60 -12 11 10 76.79 5.80 11 -11 -10 2.30 3.60 -11 11 10 6.50 3.40 10 -11 -10 3.30 3.60 -10 11 10 7.80 3.10 -9 -11 10 10.00 3.40 9 -11 -10 5.80 3.40 -9 11 10 10.80 3.00 8 -11 -10 102.49 5.70 -8 -11 10 104.49 5.90 -8 11 10 109.89 5.70 -8 11 10 102.29 7.40 7 -11 -10 0.10 2.60 -7 -11 10 3.60 3.20 -7 11 10 -1.60 2.90 -7 11 10 5.70 2.50 -6 -11 10 114.09 5.80 6 -11 -10 112.99 6.00 -6 11 10 108.29 5.10 -6 11 10 109.59 7.20 -5 -11 10 63.69 5.00 5 -11 -10 60.29 5.00 -5 11 10 68.09 4.30 -5 11 10 55.89 6.40 4 -11 -10 32.40 3.40 -4 -11 10 34.40 3.40 -4 11 10 30.90 3.80 -4 11 10 43.00 3.00 3 -11 -10 133.89 5.70 -3 -11 10 136.59 5.50 -3 11 10 129.19 4.80 -3 11 10 129.89 7.10 2 -11 -10 10.70 2.70 -2 -11 10 15.50 3.00 -2 11 10 12.40 2.00 -2 11 10 11.50 3.10 -1 -11 10 62.49 4.60 1 -11 -10 59.09 4.20 -1 11 10 56.89 6.10 -1 11 10 65.19 3.30 0 -11 -10 99.49 4.60 0 -11 10 96.69 5.20 0 11 -10 99.89 4.10 0 11 10 96.99 3.70 0 11 10 94.49 6.50 -1 -11 -10 31.30 2.80 1 -11 10 22.80 2.90 1 11 10 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3.80 1.60 6 -4 -14 7.20 2.50 -6 4 14 4.70 2.00 -6 4 14 6.00 2.00 -5 -4 14 392.66 9.10 -5 -4 14 381.96 8.40 5 -4 -14 392.36 9.50 -5 4 14 371.56 8.70 -5 4 14 379.96 8.90 -4 -4 14 12.90 1.70 -4 -4 14 11.00 2.20 4 -4 -14 14.80 2.50 -4 4 14 12.60 2.00 -4 4 14 12.00 2.00 3 -4 -14 476.85 10.80 -3 -4 14 482.85 10.20 -3 -4 14 486.85 10.60 -3 4 14 478.55 10.30 -3 4 14 489.65 10.50 2 -4 -14 30.10 2.50 -2 -4 14 34.00 2.60 -2 -4 14 34.50 2.70 -2 -4 14 29.30 2.50 -2 4 14 32.40 2.70 -2 4 14 34.10 2.40 -1 -4 14 4.90 2.00 -1 -4 14 6.10 1.90 -1 -4 14 4.30 1.50 1 -4 -14 2.10 1.80 -1 4 14 7.60 1.60 -1 4 14 3.90 1.60 0 -4 -14 7.60 1.70 0 -4 14 7.30 1.90 0 -4 14 4.20 1.80 0 -4 14 4.00 1.60 0 4 14 6.50 1.60 0 4 14 8.70 1.60 -1 -4 -14 13.40 1.80 1 -4 14 14.20 2.10 1 -4 14 16.50 2.10 1 -4 14 13.90 1.80 1 4 14 14.40 1.80 1 4 14 14.60 1.80 2 -4 14 30.60 2.50 2 -4 14 35.50 2.80 2 -4 14 32.90 2.80 -2 -4 -14 36.20 2.50 2 4 14 39.20 2.70 2 4 14 36.20 2.70 3 -4 14 178.08 5.20 3 -4 14 181.48 5.30 3 -4 14 184.18 5.50 3 4 14 175.78 4.90 3 4 14 176.18 5.00 -4 -4 -14 1.00 1.50 4 -4 14 2.60 1.60 4 -4 14 1.90 2.00 4 -4 14 -0.60 1.70 4 4 14 1.40 1.70 4 4 14 2.40 1.60 -4 4 -14 1.60 1.90 5 -4 14 0.90 1.60 5 -4 14 2.10 1.90 5 -4 14 0.20 2.10 -5 -4 -14 2.40 1.60 5 4 14 1.10 1.90 -5 4 -14 0.20 2.00 5 4 14 -0.20 1.60 6 -4 14 256.77 6.30 6 -4 14 238.58 6.90 -6 4 -14 244.68 7.00 6 4 14 250.97 6.50 7 -4 14 222.08 6.70 7 4 14 227.68 6.20 -7 4 -14 225.08 6.80 8 -4 14 22.70 2.90 -8 4 -14 24.10 3.00 8 4 14 24.10 2.60 9 -4 14 200.48 6.60 -9 4 -14 198.28 6.80 9 4 14 209.08 6.20 10 -4 14 7.20 2.80 10 4 14 10.60 2.50 -10 4 -14 12.10 3.00 11 -4 14 28.00 3.50 11 4 14 25.90 3.00 -11 4 -14 30.60 3.50 12 -4 14 -0.10 3.00 -12 4 -14 6.80 3.10 13 -4 14 7.90 3.30 14 -4 14 10.40 3.70 15 -5 -14 12.90 4.40 -15 -5 14 15.80 4.70 15 5 -14 11.80 4.00 -15 5 14 20.20 4.30 14 -5 -14 -8.90 3.60 -14 -5 14 -1.40 3.90 -14 5 14 4.40 3.60 -14 5 14 1.60 3.00 -13 -5 14 111.59 6.70 13 -5 -14 91.49 6.70 -13 5 14 97.99 5.70 -13 5 14 102.89 6.20 -12 -5 14 1.60 3.50 12 -5 -14 -0.70 3.40 -12 5 14 0.80 2.70 -12 5 14 3.30 3.10 11 -5 -14 78.79 5.90 -11 -5 14 79.39 5.70 -11 5 14 73.99 5.40 -11 5 14 77.79 5.10 -10 -5 14 -3.30 2.90 10 -5 -14 -3.70 3.00 -10 5 14 3.50 2.60 -10 5 14 1.80 2.70 9 -5 -14 127.39 6.20 -9 -5 14 123.29 5.70 -9 5 14 125.89 5.30 -9 5 14 134.89 5.40 8 -5 -14 17.10 3.20 -8 -5 14 16.10 2.90 -8 5 14 12.90 2.50 -8 5 14 13.70 2.50 7 -5 -14 97.39 5.20 -7 -5 14 88.59 4.90 -7 5 14 101.89 4.40 -7 5 14 101.59 4.60 -6 -5 14 3.50 2.30 6 -5 -14 5.70 2.60 -6 5 14 -1.00 1.80 -6 5 14 2.30 2.00 5 -5 -14 293.97 7.90 -5 -5 14 304.67 7.60 -5 -5 14 288.77 6.80 -5 5 14 291.67 7.20 -5 5 14 300.87 7.50 -4 -5 14 -0.10 1.40 -4 -5 14 -4.50 2.00 4 -5 -14 1.20 2.20 -4 -5 14 3.90 2.20 -4 5 14 -1.90 1.60 -4 5 14 -0.70 1.60 -3 -5 14 0.20 1.40 -3 -5 14 -0.20 1.90 3 -5 -14 -0.60 1.90 -3 -5 14 2.70 2.10 -3 5 14 0.40 1.60 -3 5 14 -1.90 1.40 2 -5 -14 -0.60 1.80 -2 -5 14 0.90 2.00 -2 -5 14 0.30 1.40 -2 -5 14 0.00 1.80 -2 5 14 -0.10 1.50 -2 5 14 0.70 1.50 1 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3.70 -8 5 -14 58.69 4.50 9 -5 14 2.80 2.50 9 5 14 3.40 2.10 -9 5 -14 2.20 2.70 10 -5 14 3.70 2.70 -10 5 -14 6.30 3.00 11 -5 14 109.39 6.00 -11 5 -14 112.39 5.80 12 -5 14 2.40 3.10 -12 5 -14 6.40 3.10 13 -5 14 129.39 6.80 -13 5 -14 144.49 6.80 -15 6 14 26.50 4.30 -14 -6 14 5.60 4.10 14 -6 -14 -4.80 3.70 -14 6 14 -1.30 3.50 -14 6 14 -1.70 3.10 -13 -6 14 4.00 3.80 13 -6 -14 3.60 3.70 -13 6 14 4.60 3.10 -13 6 14 2.10 3.40 12 -6 -14 22.50 4.20 -12 -6 14 24.30 4.00 -12 6 14 22.10 3.50 -12 6 14 24.10 3.70 11 -6 -14 43.50 4.40 -11 -6 14 48.80 4.30 -11 6 14 47.60 3.80 -11 6 14 53.09 4.00 10 -6 -14 82.19 6.00 -10 -6 14 95.79 5.90 -10 6 14 98.09 5.20 -10 6 14 98.89 5.40 -9 -6 14 162.78 6.30 9 -6 -14 156.58 6.80 -9 6 14 158.88 5.80 -9 6 14 150.68 6.00 8 -6 -14 31.10 3.30 -8 -6 14 36.00 3.40 -8 6 14 35.80 3.20 -8 6 14 32.50 2.80 -7 -6 14 2.80 2.60 7 -6 -14 1.10 2.30 -7 6 14 -0.20 2.10 -7 6 14 0.90 2.00 -6 -6 14 1.00 2.30 6 -6 -14 0.90 2.50 -6 6 14 2.20 1.90 -6 6 14 0.30 2.00 5 -6 -14 33.40 3.20 -5 -6 14 30.40 3.20 -5 -6 14 37.50 3.00 -5 6 14 31.20 2.70 -5 6 14 32.00 2.40 -4 -6 14 67.99 4.40 -4 -6 14 66.09 3.00 -4 -6 14 67.99 4.00 4 -6 -14 67.29 4.30 -4 6 14 66.29 3.30 -4 6 14 67.79 3.60 -3 -6 14 186.58 5.00 -3 -6 14 180.28 6.10 -3 -6 14 181.58 5.60 3 -6 -14 184.98 5.90 -3 6 14 189.68 5.50 -3 6 14 186.08 5.00 -2 -6 14 39.40 3.10 2 -6 -14 35.60 2.90 -2 -6 14 35.40 2.60 -2 -6 14 32.60 2.70 -2 6 14 35.10 2.70 -2 6 14 36.40 3.00 -1 -6 14 29.70 2.70 -1 -6 14 32.90 2.70 1 -6 -14 34.40 3.20 -1 -6 14 32.40 2.60 -1 6 14 36.60 2.60 -1 6 14 32.20 2.40 0 -6 14 -1.10 1.80 0 -6 14 1.10 1.80 0 -6 14 -0.10 1.50 0 -6 -14 -0.50 1.70 0 6 14 1.10 1.50 0 6 14 -1.10 1.50 1 -6 14 175.18 5.40 -1 -6 -14 183.48 5.20 1 -6 14 177.48 5.60 1 -6 14 174.48 5.20 1 6 14 183.18 4.80 1 6 14 181.58 5.10 2 -6 14 59.19 3.70 2 -6 14 52.39 3.70 -2 -6 -14 55.19 3.10 2 -6 14 58.59 3.40 2 6 14 60.29 3.10 2 6 14 62.99 3.10 3 -6 14 548.55 11.90 3 -6 14 556.34 12.10 3 -6 14 545.55 12.00 3 6 14 555.64 11.40 -3 6 -14 548.95 12.00 3 6 14 544.15 11.50 4 -6 14 264.87 7.00 4 -6 14 251.17 6.90 4 -6 14 259.27 7.00 -4 6 -14 256.97 7.00 4 6 14 260.17 6.40 4 6 14 253.87 6.40 5 -6 14 39.50 3.10 5 -6 14 38.30 3.30 5 -6 14 45.00 3.10 5 6 14 41.10 3.30 -5 6 -14 42.00 3.20 5 6 14 38.00 2.90 6 -6 14 4.10 2.10 6 -6 14 8.80 2.50 6 -6 14 11.40 2.40 6 6 14 5.50 2.10 -6 6 -14 7.20 2.50 6 6 14 8.60 1.90 7 -6 14 10.00 2.50 7 -6 14 6.40 2.20 7 6 14 6.00 2.00 -7 6 -14 10.00 2.70 8 -6 14 0.00 2.30 8 6 14 1.90 1.90 -8 6 -14 3.00 2.70 9 -6 14 81.89 5.10 -9 6 -14 89.29 5.20 10 -6 14 3.20 2.80 -10 6 -14 2.30 3.00 11 -6 14 24.80 3.50 -11 6 -14 24.80 3.60 12 -6 14 -0.70 2.90 -12 6 -14 7.90 3.30 13 -6 14 30.90 4.10 -13 6 -14 40.90 4.20 -14 6 -14 3.60 3.50 -15 7 14 0.80 3.80 14 -7 -14 2.40 4.00 -14 -7 14 1.60 4.00 -14 7 14 2.80 3.90 -14 7 14 7.50 3.60 13 -7 -14 116.39 7.40 -13 -7 14 116.29 7.20 -13 7 14 121.29 6.50 -13 7 14 130.09 6.60 12 -7 -14 76.09 6.40 -12 -7 14 75.79 6.30 -12 7 14 74.69 5.70 -12 7 14 84.29 5.50 -11 -7 14 32.30 4.00 11 -7 -14 30.70 4.40 -11 7 14 36.60 3.60 -11 7 14 33.20 3.70 10 -7 -14 0.20 3.10 -10 -7 14 5.40 3.20 -10 7 14 -1.60 2.50 -10 7 14 -1.70 2.70 9 -7 -14 91.69 6.00 -9 -7 14 92.39 5.40 -9 7 14 97.49 5.20 -9 7 14 92.89 4.80 8 -7 -14 20.10 3.50 -8 -7 14 21.50 3.20 -8 7 14 19.80 3.00 -8 7 14 18.60 2.50 7 -7 -14 173.18 6.70 -7 -7 14 172.78 6.10 -7 7 14 168.38 5.90 -7 7 14 163.18 5.40 -6 -7 14 54.99 4.20 6 -7 -14 50.09 4.70 -6 -7 14 65.89 4.90 -6 7 14 57.49 4.00 -6 7 14 61.39 3.50 5 -7 -14 82.09 4.50 -5 -7 14 75.49 4.50 -5 -7 14 94.39 5.10 -5 7 14 89.49 3.70 -5 7 14 88.79 4.40 4 -7 -14 1.10 2.30 -4 -7 14 3.50 2.40 -4 -7 14 2.00 2.20 -4 7 14 0.90 1.90 -4 7 14 4.40 1.60 -3 -7 14 45.40 4.10 -3 -7 14 50.19 2.90 3 -7 -14 44.70 3.90 -3 -7 14 50.79 3.70 -3 7 14 50.29 3.50 -3 7 14 51.89 2.90 -2 -7 14 1.00 1.50 -2 -7 14 0.40 2.30 -2 -7 14 3.80 2.10 2 -7 -14 0.80 2.00 -2 7 14 3.40 1.90 -2 7 14 3.60 1.50 1 -7 -14 576.24 12.50 -1 -7 14 559.84 11.80 -1 -7 14 580.14 12.30 -1 -7 14 560.14 12.80 -1 7 14 584.44 11.60 -1 7 14 561.34 12.00 0 -7 14 447.36 9.80 0 -7 -14 444.96 10.10 0 -7 14 457.55 10.70 0 -7 14 445.66 10.10 0 7 14 467.45 9.50 0 7 14 447.06 9.90 1 -7 14 272.47 7.40 -1 -7 -14 273.87 6.90 1 -7 14 270.97 6.80 1 -7 14 271.37 7.10 1 7 14 261.77 6.30 1 7 14 270.27 6.70 2 -7 14 101.79 4.60 2 -7 14 91.89 4.50 2 -7 14 99.19 4.10 -2 -7 -14 108.99 4.50 2 7 14 102.79 3.60 2 7 14 96.19 3.80 3 -7 14 -2.40 2.10 3 -7 14 -0.60 1.80 3 -7 14 -1.30 2.10 -3 7 -14 0.10 2.10 3 7 14 -0.20 1.60 3 7 14 1.30 1.60 4 -7 14 21.40 2.70 4 -7 14 21.60 2.40 4 -7 14 17.60 2.50 -4 7 -14 18.90 2.60 4 7 14 19.80 2.10 4 7 14 18.80 2.00 5 -7 14 288.57 7.90 5 -7 14 310.07 8.10 5 -7 14 299.57 7.90 -5 7 -14 302.17 8.10 5 7 14 304.77 7.30 5 7 14 301.77 7.20 6 -7 14 116.09 5.10 6 -7 14 127.79 5.20 6 -7 14 120.99 5.30 6 7 14 127.59 4.30 6 7 14 125.09 4.60 -6 7 -14 127.89 5.40 7 -7 14 17.90 3.00 7 -7 14 16.10 2.50 7 -7 14 15.10 2.60 -7 7 -14 17.20 2.90 8 -7 14 4.20 2.50 -8 7 -14 3.70 2.80 9 -7 14 6.60 2.80 -9 7 -14 6.70 3.10 10 -7 14 34.60 3.60 -10 7 -14 30.00 3.70 11 -7 14 10.30 3.30 -11 7 -14 7.40 3.30 12 -7 14 24.50 3.80 -12 7 -14 30.70 4.00 -13 7 -14 4.80 3.50 -14 7 -14 1.90 3.70 -14 -8 14 6.90 4.20 -13 -8 14 -3.60 3.80 13 -8 -14 -4.70 3.60 -13 8 14 -1.80 3.30 -13 8 14 -2.40 4.20 -12 -8 14 12.30 3.80 12 -8 -14 9.10 3.90 -12 8 14 11.70 3.50 -12 8 14 13.80 3.70 11 -8 -14 8.20 3.80 -11 -8 14 13.60 3.50 -11 8 14 6.30 3.10 -11 8 14 10.70 3.20 -10 -8 14 34.30 3.90 10 -8 -14 32.20 4.20 -10 8 14 35.90 3.60 -10 8 14 31.60 3.30 9 -8 -14 -2.90 3.00 -9 -8 14 0.70 3.00 -9 8 14 2.40 2.30 -9 8 14 2.70 2.70 8 -8 -14 -0.20 3.10 -8 -8 14 0.60 2.80 -8 8 14 2.30 2.20 -8 8 14 -3.30 2.50 -7 -8 14 120.79 5.40 7 -8 -14 112.69 6.00 -7 8 14 126.09 5.40 -7 8 14 120.69 4.90 6 -8 -14 1.40 2.80 -6 -8 14 1.10 2.50 -6 -8 14 -0.60 2.80 -6 8 14 1.50 2.10 -6 8 14 -0.20 2.20 -5 -8 14 17.30 2.60 5 -8 -14 15.90 3.00 -5 -8 14 16.60 3.20 -5 8 14 13.10 2.50 -5 8 14 21.70 3.20 -4 -8 14 318.77 8.20 -4 -8 14 320.17 8.80 4 -8 -14 324.27 8.80 -4 8 14 310.47 8.10 3 -8 -14 19.60 2.80 -3 -8 14 17.10 2.60 -3 -8 14 20.30 2.90 -3 8 14 21.10 2.50 -2 -8 14 42.80 3.00 2 -8 -14 41.10 3.80 -2 -8 14 42.10 3.40 -2 8 14 41.20 3.30 -1 -8 14 30.40 3.10 -1 -8 14 26.00 2.50 1 -8 -14 25.40 2.70 -1 -8 14 23.90 2.00 -1 8 14 24.40 2.40 0 -8 14 62.79 3.90 0 -8 14 65.49 3.30 0 -8 14 60.69 4.40 0 -8 -14 69.29 4.00 0 8 14 65.69 3.50 1 -8 14 204.18 6.60 1 -8 14 198.98 6.10 -1 -8 -14 204.88 5.90 1 -8 14 203.08 5.60 1 8 14 204.58 5.60 2 -8 14 12.00 2.40 2 -8 14 10.10 2.00 2 -8 14 6.40 2.30 2 8 14 10.50 1.80 3 -8 14 -1.20 2.20 3 -8 14 0.60 2.30 3 -8 14 -0.90 1.80 3 8 14 1.50 1.60 -3 8 -14 -1.90 2.10 4 -8 14 145.59 5.40 4 -8 14 153.58 5.70 4 -8 14 146.69 5.20 -4 8 -14 153.98 5.70 4 8 14 146.69 4.60 5 -8 14 39.00 3.10 5 -8 14 39.40 3.20 5 -8 14 41.50 3.30 -5 8 -14 38.40 3.30 5 8 14 39.80 3.00 6 -8 14 15.70 2.70 6 -8 14 10.10 2.70 6 -8 14 16.20 2.60 -6 8 -14 14.90 2.90 7 -8 14 9.70 2.60 7 -8 14 12.20 2.60 7 -8 14 5.80 2.70 -7 8 -14 8.70 2.80 8 -8 14 32.00 3.30 8 -8 14 38.30 4.40 -8 8 -14 34.70 3.60 9 -8 14 0.10 2.60 -9 8 -14 4.50 2.90 10 -8 14 151.08 6.60 -10 8 -14 152.98 6.70 11 -8 14 0.80 2.90 -11 8 -14 1.00 3.20 12 -8 14 26.60 3.90 -12 8 -14 34.40 4.10 -13 8 -14 48.20 4.90 -14 -9 14 56.49 5.40 -13 -9 14 5.60 4.10 13 -9 -14 11.20 5.10 -12 -9 14 23.40 4.20 12 -9 -14 17.90 4.30 -12 9 14 20.30 3.80 -11 -9 14 -0.40 3.40 11 -9 -14 1.90 3.80 -11 9 14 2.80 3.10 10 -9 -14 -3.00 3.40 -10 -9 14 1.90 3.30 -10 9 14 0.70 3.00 9 -9 -14 4.50 3.30 -9 -9 14 2.70 3.10 -9 9 14 7.90 2.90 -8 -9 14 151.18 6.00 8 -9 -14 152.78 7.00 -8 9 14 153.88 6.30 -7 -9 14 2.60 3.20 -7 -9 14 3.90 2.70 7 -9 -14 2.30 3.00 -7 9 14 -1.80 2.40 -6 -9 14 81.79 5.60 6 -9 -14 90.29 5.10 -6 -9 14 85.99 4.90 -6 9 14 79.19 4.70 -5 -9 14 -2.10 2.40 5 -9 -14 -1.10 2.60 -5 -9 14 2.70 2.80 -5 9 14 2.40 2.30 -4 -9 14 40.00 3.70 -4 -9 14 55.89 4.10 4 -9 -14 48.20 4.50 -4 9 14 45.00 3.20 3 -9 -14 10.00 2.70 -3 -9 14 11.90 3.00 -3 -9 14 11.80 2.50 -3 9 14 13.50 2.30 -2 -9 14 162.68 5.60 -2 -9 14 171.58 6.50 2 -9 -14 176.28 6.00 -2 9 14 164.48 5.40 -1 -9 14 4.60 2.20 1 -9 -14 3.60 2.30 -1 -9 14 2.10 2.60 -1 9 14 3.90 1.90 0 -9 -14 158.88 5.40 0 -9 14 156.08 5.40 0 -9 14 143.19 4.70 0 -9 14 145.69 6.00 0 9 14 159.58 5.00 1 -9 14 13.10 2.00 1 -9 14 8.10 2.70 -1 -9 -14 8.50 2.30 1 -9 14 14.70 2.50 1 9 14 11.90 2.00 2 -9 14 48.80 4.00 2 -9 14 47.00 3.40 2 -9 14 48.70 4.50 2 9 14 53.59 3.20 -2 9 -14 52.99 4.10 3 -9 14 16.20 2.90 3 -9 14 18.20 2.40 3 -9 14 16.20 2.60 3 9 14 19.70 2.10 -3 9 -14 17.20 2.60 4 -9 14 69.29 4.50 4 -9 14 71.09 4.70 4 -9 14 72.89 4.10 -4 9 -14 74.79 4.80 4 9 14 76.19 3.40 5 -9 14 35.30 3.00 5 -9 14 37.00 3.40 5 -9 14 35.10 3.20 -5 9 -14 36.80 3.30 6 -9 14 88.39 5.00 6 -9 14 87.79 4.90 6 -9 14 94.39 4.80 -6 9 -14 89.89 5.10 7 -9 14 12.90 2.70 7 -9 14 6.60 2.80 7 -9 14 10.40 2.80 -7 9 -14 5.90 2.90 8 -9 14 20.50 3.20 8 -9 14 21.10 3.10 8 -9 14 17.70 3.30 -8 9 -14 14.50 3.20 9 -9 14 -1.20 2.60 -9 9 -14 0.50 3.10 10 -9 14 19.40 3.40 -10 9 -14 17.20 3.60 11 -9 14 2.10 3.10 -11 9 -14 0.30 3.30 -12 9 -14 63.99 5.10 12 -10 -14 2.40 4.20 -12 -10 14 1.80 3.90 11 -10 -14 4.80 4.00 -11 -10 14 2.10 3.60 -11 10 14 4.90 3.30 10 -10 -14 55.59 5.20 -10 -10 14 57.09 4.50 -10 10 14 46.80 4.10 -9 -10 14 36.20 3.90 9 -10 -14 25.90 3.80 -9 10 14 35.10 3.70 -8 -10 14 16.70 3.30 8 -10 -14 9.60 3.50 -8 -10 14 10.80 3.70 -8 10 14 14.40 3.10 7 -10 -14 7.10 3.30 -7 -10 14 5.10 3.40 -7 -10 14 2.20 2.80 -7 10 14 4.80 2.70 -6 -10 14 -0.90 2.60 -6 -10 14 -4.90 3.00 6 -10 -14 0.10 2.90 -6 10 14 -3.70 2.40 5 -10 -14 6.80 3.10 -5 -10 14 7.40 3.30 -5 -10 14 8.00 2.70 -5 10 14 2.90 2.40 4 -10 -14 310.37 9.00 -4 -10 14 306.57 8.10 -4 -10 14 315.97 9.20 -4 10 14 311.87 8.30 3 -10 -14 24.10 3.20 -3 -10 14 18.10 3.40 -3 -10 14 26.40 2.90 -3 10 14 24.40 2.70 -2 -10 14 187.88 7.00 2 -10 -14 191.68 6.70 -2 -10 14 193.38 6.00 -2 10 14 186.38 5.90 1 -10 -14 43.10 4.00 -1 -10 14 39.20 3.00 -1 -10 14 37.80 3.60 -1 10 14 43.00 3.50 0 -10 14 15.30 3.10 0 -10 -14 8.70 2.50 0 -10 14 13.30 2.60 0 10 14 16.10 2.20 1 -10 14 19.40 3.10 1 -10 14 9.90 2.40 1 10 14 11.80 2.10 2 -10 14 46.60 3.90 2 -10 14 46.70 3.20 2 -10 14 50.39 3.40 2 10 14 45.50 3.20 -2 10 -14 52.69 4.20 3 -10 14 272.67 7.30 3 -10 14 277.77 7.60 3 -10 14 275.77 8.30 3 10 14 285.77 7.40 -3 10 -14 272.87 7.90 4 -10 14 59.29 4.00 4 -10 14 59.69 4.40 4 -10 14 61.49 4.90 -4 10 -14 65.49 4.60 5 -10 14 4.40 2.80 5 -10 14 3.50 2.60 5 -10 14 0.00 2.20 -5 10 -14 4.90 2.70 6 -10 14 0.40 2.60 6 -10 14 6.30 3.00 6 -10 14 6.30 2.40 -6 10 -14 2.10 2.70 7 -10 14 10.40 3.00 7 -10 14 8.00 2.60 7 -10 14 15.10 3.10 -7 10 -14 16.30 3.20 8 -10 14 140.09 6.40 8 -10 14 141.89 6.20 8 -10 14 158.28 6.70 -8 10 -14 152.98 6.80 9 -10 14 11.00 3.30 9 -10 14 6.70 2.80 -9 10 -14 8.20 3.40 10 -10 14 97.09 6.00 -10 10 -14 98.69 6.50 11 -10 14 0.00 3.20 -11 10 -14 1.60 3.60 11 -11 -14 3.40 4.00 10 -11 -14 5.30 3.80 -10 11 14 10.50 3.40 9 -11 -14 -1.60 3.10 -9 11 14 2.30 2.90 -8 -11 14 54.69 4.90 8 -11 -14 49.00 4.70 -8 11 14 62.69 5.40 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13.50 4.40 7 -14 -14 19.50 4.40 -7 14 14 17.60 3.50 6 -14 -14 0.20 3.50 -6 -14 14 -5.50 4.00 -6 14 14 5.50 3.00 -6 14 14 -5.20 4.20 5 -14 -14 20.50 4.00 -5 -14 14 16.20 4.40 -5 14 14 25.80 3.50 -5 14 14 8.90 4.60 -4 -14 14 4.00 3.50 4 -14 -14 4.20 3.40 -4 14 14 -4.10 3.90 -4 14 14 4.10 2.80 -3 -14 14 98.99 6.90 3 -14 -14 95.69 6.20 -3 14 14 83.49 9.00 -3 14 14 96.69 5.40 -2 -14 14 0.00 3.70 2 -14 -14 0.60 3.20 -2 14 14 -4.00 3.90 -2 14 14 1.30 2.60 -1 -14 14 4.20 3.70 1 -14 -14 4.20 3.30 -1 14 14 0.60 4.00 0 -14 14 3.20 3.40 0 14 -14 2.10 2.70 0 14 14 -1.60 3.90 1 -14 14 111.69 6.90 -1 14 -14 109.79 5.70 1 14 14 90.69 9.00 2 -14 14 5.70 3.70 -2 14 -14 1.80 2.80 2 14 14 2.60 4.00 3 -14 14 191.48 8.10 -3 14 -14 186.78 7.10 3 14 14 184.18 10.60 4 -14 14 16.80 4.00 -4 14 -14 16.20 3.30 4 14 14 11.50 4.50 5 -14 14 6.80 3.70 -5 14 -14 4.30 3.00 5 14 14 -3.50 4.10 6 -14 14 3.20 3.80 6 14 14 -2.60 4.40 -6 14 -14 6.10 3.20 7 -14 14 27.30 4.50 8 -14 14 4.80 3.80 9 -14 14 85.19 6.70 -7 -15 14 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29.60 4.10 8 6 21 27.20 3.40 9 -6 21 30.60 4.60 9 -6 21 27.10 3.90 -9 6 -21 27.40 4.10 9 6 21 27.10 4.60 10 -6 21 44.00 5.00 -10 6 -21 37.20 4.40 10 -7 -21 -1.80 4.10 -10 -7 21 -1.60 4.00 9 -7 -21 19.20 4.60 -9 -7 21 23.10 4.40 -9 7 21 18.50 3.70 -8 -7 21 -0.10 3.70 8 -7 -21 -3.50 3.70 -8 7 21 1.70 3.20 7 -7 -21 -4.60 3.60 -7 -7 21 -1.10 3.50 -7 7 21 0.90 3.00 -6 -7 21 83.99 6.10 6 -7 -21 81.69 6.30 -6 7 21 80.09 5.60 5 -7 -21 104.29 6.50 -5 -7 21 105.29 6.20 -5 7 21 104.09 5.80 -4 -7 21 31.60 3.90 4 -7 -21 25.20 4.00 -4 7 21 30.40 3.50 -3 -7 21 5.50 3.40 3 -7 -21 2.60 3.20 -3 7 21 3.70 2.70 -2 -7 21 25.00 3.60 2 -7 -21 21.40 3.50 -2 7 21 18.60 3.10 -1 -7 21 8.00 3.30 -1 -7 21 7.70 2.40 -1 -7 21 9.60 3.50 -1 7 21 15.30 2.90 0 -7 21 69.69 5.40 0 -7 21 67.09 4.50 0 -7 21 67.79 4.60 0 7 21 75.59 4.90 1 -7 21 6.50 3.30 1 -7 21 4.90 3.00 1 -7 21 6.30 2.50 1 7 21 6.00 2.60 2 -7 21 0.80 3.00 2 -7 21 -1.10 3.20 2 -7 21 -0.10 2.50 2 7 21 -0.30 2.50 3 -7 21 25.50 3.40 3 -7 21 28.30 3.30 3 -7 21 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5.60 1 -7 27 9.20 3.20 6 0 -28 52.09 6.40 -5 0 28 -0.20 4.20 5 0 -28 -4.60 4.00 -4 0 28 6.30 4.20 4 0 -28 2.90 4.20 3 0 -28 -5.40 4.00 -3 0 28 -6.20 3.80 -2 0 28 -2.70 3.90 -1 0 28 2.10 4.00 0 0 28 121.09 7.60 1 0 28 -2.80 4.00 2 0 28 1.70 4.10 3 0 28 -4.40 4.00 4 0 28 6.00 4.30 -4 0 -28 12.00 3.90 -5 0 -28 -2.30 4.10 6 -1 -28 15.60 5.50 6 1 -28 18.40 8.00 5 -1 -28 3.30 4.10 -5 1 28 8.30 4.10 5 1 -28 -1.80 4.30 4 -1 -28 27.00 4.80 -4 -1 28 35.90 4.90 -4 1 28 43.90 4.90 -3 -1 28 -6.50 3.90 -3 -1 28 0.30 3.90 -3 1 28 0.10 4.00 -2 -1 28 -1.30 3.90 -2 -1 28 1.10 3.70 -2 1 28 1.80 4.00 -1 -1 28 4.60 4.10 -1 -1 28 -3.00 5.00 -1 1 28 2.40 4.00 0 -1 28 13.50 4.30 0 1 28 10.60 4.20 1 -1 28 -2.70 3.90 1 1 28 1.60 3.90 2 -1 28 21.20 4.60 2 1 28 29.70 4.60 3 -1 28 10.00 4.40 3 1 28 10.10 4.40 -4 -1 -28 8.80 5.50 4 -1 28 5.10 4.80 4 1 28 4.70 4.20 5 1 28 -2.50 4.60 6 -2 -28 10.80 5.20 -5 -2 28 3.50 3.60 5 -2 -28 -4.60 4.00 -5 2 28 3.30 4.00 4 -2 -28 -6.10 3.70 -4 -2 28 -6.40 3.10 -4 -2 28 2.00 5.20 -4 2 28 -1.10 3.90 -3 -2 28 6.20 4.20 -3 -2 28 3.20 3.20 -3 2 28 7.90 3.90 -2 -2 28 5.60 4.10 -2 -2 28 2.90 3.30 -2 2 28 4.60 3.90 -1 -2 28 54.99 5.40 -1 -2 28 68.39 5.50 -1 2 28 66.19 5.20 0 -2 28 54.99 5.20 0 2 28 61.29 5.20 1 -2 28 3.70 4.10 1 2 28 0.60 4.00 2 -2 28 5.60 4.30 2 2 28 7.10 4.00 3 -2 28 7.40 4.60 3 2 28 1.40 4.00 4 2 28 5.80 4.10 5 2 28 -0.80 4.20 6 -3 -28 0.10 7.10 -6 3 28 4.00 5.30 5 -3 -28 7.80 4.40 -5 3 28 18.20 4.40 4 -3 -28 -7.80 3.90 -4 -3 28 2.20 3.20 -4 3 28 -3.70 3.70 -3 -3 28 6.90 3.30 -3 -3 28 2.90 4.80 -3 3 28 5.80 3.80 -2 -3 28 -1.00 3.30 -2 -3 28 -5.50 4.10 -2 3 28 3.70 3.90 -1 -3 28 -0.20 3.30 -1 -3 28 9.60 4.30 -1 3 28 3.70 3.70 0 -3 28 0.20 4.20 0 3 28 0.30 3.80 1 -3 28 5.60 4.30 1 3 28 -3.40 3.80 2 -3 28 8.70 4.60 2 3 28 5.70 4.00 3 3 28 45.60 5.00 4 3 28 6.70 4.10 5 3 28 3.00 4.00 -6 4 28 1.10 4.40 5 -4 -28 5.00 4.30 -5 4 28 19.90 4.40 -4 4 28 8.00 3.80 -3 -4 28 7.30 3.30 -3 4 28 8.80 4.10 -2 -4 28 6.60 3.20 -2 4 28 7.90 3.80 -1 -4 28 139.89 9.90 -1 -4 28 123.59 7.40 -1 4 28 144.89 7.50 0 -4 28 0.50 4.90 0 4 28 11.80 4.10 1 4 28 -3.10 3.80 2 4 28 -4.50 3.80 3 4 28 15.00 4.20 4 4 28 0.00 4.00 5 4 28 32.90 4.70 6 4 28 -1.10 6.20 -6 5 28 6.70 5.90 5 -5 -28 4.90 4.40 -5 5 28 14.60 5.20 -4 5 28 -3.00 5.00 -3 5 28 7.50 6.40 -2 -5 28 6.20 3.20 -1 -5 28 2.00 3.30 4 0 -29 -3.40 4.20 -2 0 29 1.30 6.20 -1 0 29 14.20 4.50 0 0 29 6.70 4.30 1 0 29 10.40 4.40 2 0 29 4.60 6.30 5 -1 -29 22.50 5.90 4 -1 -29 -6.00 4.00 4 1 -29 -6.70 4.40 -3 1 29 17.70 6.70 -2 1 29 1.00 4.10 -1 1 29 19.70 4.50 0 1 29 -1.60 4.10 1 1 29 22.10 4.70 2 1 29 -2.40 4.10 5 -2 -29 9.00 7.00 -3 2 29 2.40 4.10 -2 2 29 46.20 4.90 -1 2 29 5.80 4.10 0 2 29 22.80 4.50 1 2 29 24.60 4.50 2 2 29 -1.20 4.10 3 2 29 -1.40 4.60 -3 3 29 -3.10 4.00 -2 3 29 3.30 4.00 -1 3 29 2.70 4.00 0 3 29 3.20 4.00 1 3 29 2.40 4.00 2 3 29 13.10 4.30 3 3 29 1.10 4.20 -4 4 29 1.50 4.50 -3 4 29 1.50 3.90 -2 4 29 55.59 5.00 -1 4 29 51.89 4.90 0 4 29 58.59 5.20 1 4 29 -8.90 3.90 2 4 29 -1.40 3.90 3 4 29 -4.80 4.10 4 4 29 21.70 7.00 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 86133