data_6PF6
_audit_creation_date               2019-12-18
_audit_creation_method
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number       '2018/3'
_audit_contact_author_address      ?
_audit_contact_author_email        ?
_audit_contact_author_name         ''
_audit_contact_author_phone        ?
_publ_contact_author_id_orcid      ?
_publ_section_references
;
Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H.
 (2009), J. Appl. Cryst. 42, 339-341.

Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8.
;
_chemical_name_common              ?
_chemical_name_systematic          ?
_chemical_formula_moiety           'C40 H40 N12, 3(F6 P)'
_chemical_formula_sum              'C40 H40 F18 N12 P3'
_chemical_formula_weight           1123.75
_chemical_melting_point            ?
loop_
  _atom_type_symbol
  _atom_type_description
  _atom_type_scat_dispersion_real
  _atom_type_scat_dispersion_imag
  _atom_type_scat_source
 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'F' 'F' 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'N' 'N' 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'P' 'P' 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system        'monoclinic'
_space_group_IT_number             15
_space_group_name_H-M_alt          'C 1 2/c 1'
_space_group_name_Hall             '-C 2yc'
loop_
  _space_group_symop_operation_xyz
 'x, y, z'
 '-x, y, -z+1/2'
 'x+1/2, y+1/2, z'
 '-x+1/2, y+1/2, -z+1/2'
 '-x, -y, -z'
 'x, -y, z-1/2'
 '-x+1/2, -y+1/2, -z'
 'x+1/2, -y+1/2, z-1/2'

_cell_length_a                     16.1323(5)
_cell_length_b                     11.4829(4)
_cell_length_c                     30.2137(9)
_cell_angle_alpha                  90
_cell_angle_beta                   101.490(2)
_cell_angle_gamma                  90
_cell_volume                       5484.8(3)
_cell_formula_units_Z              4
_cell_measurement_reflns_used      9877
_cell_measurement_temperature      100(2)
_cell_measurement_theta_max        68.04
_cell_measurement_theta_min        4.76
_shelx_estimated_absorpt_T_max     ?
_shelx_estimated_absorpt_T_min     ?
_exptl_absorpt_coefficient_mu      1.918
_exptl_absorpt_correction_T_max    ?
_exptl_absorpt_correction_T_min    ?
_exptl_absorpt_correction_type     'multi-scan'
_exptl_absorpt_process_details     ?
_exptl_absorpt_special_details     ?
_exptl_crystal_colour              'red'
_exptl_crystal_density_diffrn      1.361
_exptl_crystal_density_meas        .
_exptl_crystal_density_method      ?
_exptl_crystal_description         block
_exptl_crystal_F_000               2284
_exptl_crystal_size_max            0.288
_exptl_crystal_size_mid            0.124
_exptl_crystal_size_min            0.114
_exptl_transmission_factor_max     0.7530
_exptl_transmission_factor_min     0.6523
_diffrn_reflns_av_R_equivalents    0.0269
_diffrn_reflns_av_unetI/netI       0.0201
_diffrn_reflns_Laue_measured_fraction_full  0.996
_diffrn_reflns_Laue_measured_fraction_max  0.992
_diffrn_reflns_limit_h_max         19
_diffrn_reflns_limit_h_min         -18
_diffrn_reflns_limit_k_max         13
_diffrn_reflns_limit_k_min         -13
_diffrn_reflns_limit_l_max         35
_diffrn_reflns_limit_l_min         -35
_diffrn_reflns_number              26936
_diffrn_reflns_point_group_measured_fraction_full  0.996
_diffrn_reflns_point_group_measured_fraction_max  0.992
_diffrn_reflns_theta_full          67.679
_diffrn_reflns_theta_max           68.196
_diffrn_reflns_theta_min           4.760
_diffrn_ambient_temperature        100.04
_diffrn_detector_area_resol_mean   8
_diffrn_measured_fraction_theta_full  0.996
_diffrn_measured_fraction_theta_max  0.992
_diffrn_measurement_device_type    'Bruker Kappa APEX CCD area detector'
_diffrn_measurement_method         'ω and φ scans'
_diffrn_radiation_monochromator    'MX optics'
_diffrn_radiation_type             CuK\a
_diffrn_radiation_wavelength       1.54178
_diffrn_source                     microsource
_reflns_Friedel_coverage           0.000
_reflns_Friedel_fraction_full      .
_reflns_Friedel_fraction_max       .
_reflns_number_gt                  4478
_reflns_number_total               4970
_reflns_special_details
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression       'I > 2σ(I)'
_computing_cell_refinement         'SAINT V8.34A (Bruker, 2017)'
_computing_data_collection         'APEX2 V2017.3 (Bruker, 2017)'
_computing_data_reduction          'Bruker SAINT'
_computing_molecular_graphics      'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material    'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement    'ShelXL (Sheldrick, 2015)'
_computing_structure_solution      'SHELXT 2014/5 (Sheldrick, 2014)'
_refine_diff_density_max           0.313
_refine_diff_density_min           -0.248
_refine_diff_density_rms           0.044
_refine_ls_extinction_coef         .
_refine_ls_extinction_method       none
_refine_ls_goodness_of_fit_ref     1.059
_refine_ls_hydrogen_treatment      constr
_refine_ls_matrix_type             full
_refine_ls_number_parameters       339
_refine_ls_number_reflns           4970
_refine_ls_number_restraints       0
_refine_ls_R_factor_all            0.0444
_refine_ls_R_factor_gt             0.0405
_refine_ls_restrained_S_all        1.059
_refine_ls_shift/su_max            0.001
_refine_ls_shift/su_mean           0.000
_refine_ls_structure_factor_coef   Fsqd
_refine_ls_weighting_details      
 'w=1/[σ²(Fo²)+(0.0476P)²+6.2647P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme        calc
_refine_ls_wR_factor_gt            0.1060
_refine_ls_wR_factor_ref           0.1091
_refine_special_details            ?
_olex2_refinement_description
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups, All N(H,H) groups
2. Others
 Fixed Sof: F9(0.5) F10(0.5)
3.a Secondary CH2 refined with riding coordinates:
 C6(H6A,H6B), C13(H13A,H13B)
3.b Aromatic/amide H refined with riding coordinates:
 C2(H2), C3(H3), C4(H4), C5(H5), C8(H8), C9(H9), C11(H11), C12(H12), C14(H14),
 C15(H15), C17(H17), C18(H18)
3.c X=CH2 refined with riding coordinates:
 N3(H3A,H3B), N6(H6C,H6D)
;
_atom_sites_solution_hydrogens     geom
_atom_sites_solution_primary       ?
_atom_sites_solution_secondary     ?
loop_
  _atom_site_label
  _atom_site_type_symbol
  _atom_site_fract_x
  _atom_site_fract_y
  _atom_site_fract_z
  _atom_site_U_iso_or_equiv
  _atom_site_adp_type
  _atom_site_occupancy
  _atom_site_site_symmetry_order
  _atom_site_calc_flag
  _atom_site_refinement_flags_posn
  _atom_site_refinement_flags_adp
  _atom_site_refinement_flags_occupancy
  _atom_site_disorder_assembly
  _atom_site_disorder_group
 N1 N 0.69310(10) 0.51862(13) 0.70960(5) 0.0375(3) Uani 1 1 d . . . . .
 N2 N 0.55672(11) 0.98504(14) 0.60464(5) 0.0430(4) Uani 1 1 d . . . . .
 N3 N 0.31699(11) 0.84786(16) 0.48117(6) 0.0504(4) Uani 1 1 d . . . . .
 H3A H 0.285765 0.817618 0.456648 0.060 Uiso 1 1 calc R . . . .
 H3B H 0.292769 0.884403 0.500836 0.060 Uiso 1 1 calc R . . . .
 N4 N 0.44438(10) 0.78616(14) 0.46184(5) 0.0402(4) Uani 1 1 d . . . . .
 N5 N 0.39292(10) 0.73376(14) 0.42486(5) 0.0424(4) Uani 1 1 d . . . . .
 N6 N 0.52104(13) 0.6959(2) 0.40325(8) 0.0863(8) Uani 1 1 d . . . . .
 H6C H 0.550263 0.735482 0.426059 0.104 Uiso 1 1 calc R . . . .
 H6D H 0.547118 0.661946 0.383758 0.104 Uiso 1 1 calc R . . . .
 C1 C 0.60956(12) 0.38029(16) 0.64090(6) 0.0400(4) Uani 1 1 d . . . . .
 C2 C 0.69613(14) 0.3982(2) 0.64681(8) 0.0568(6) Uani 1 1 d . . . . .
 H2 H 0.727340 0.362432 0.626941 0.068 Uiso 1 1 calc R . . . .
 C3 C 0.73650(13) 0.4675(2) 0.68138(7) 0.0544(6) Uani 1 1 d . . . . .
 H3 H 0.795792 0.479507 0.685392 0.065 Uiso 1 1 calc R . . . .
 C4 C 0.61094(13) 0.49769(19) 0.70576(7) 0.0487(5) Uani 1 1 d . . . . .
 H4 H 0.581583 0.530779 0.727022 0.058 Uiso 1 1 calc R . . . .
 C5 C 0.56821(14) 0.42979(18) 0.67195(7) 0.0484(5) Uani 1 1 d . . . . .
 H5 H 0.509410 0.416362 0.669709 0.058 Uiso 1 1 calc R . . . .
 C6 C 0.73334(13) 0.60989(17) 0.74228(6) 0.0421(4) Uani 1 1 d . . . . .
 H6A H 0.795663 0.601767 0.748110 0.051 Uiso 1 1 calc R . . . .
 H6B H 0.714329 0.601121 0.771305 0.051 Uiso 1 1 calc R . . . .
 C7 C 0.70779(12) 0.72736(17) 0.72205(6) 0.0381(4) Uani 1 1 d . . . . .
 C8 C 0.75399(13) 0.77858(19) 0.69323(7) 0.0468(5) Uani 1 1 d . . . . .
 H8 H 0.805393 0.743870 0.689135 0.056 Uiso 1 1 calc R . . . .
 C9 C 0.72574(13) 0.88015(19) 0.67030(7) 0.0483(5) Uani 1 1 d . . . . .
 H9 H 0.758368 0.915775 0.651104 0.058 Uiso 1 1 calc R . . . .
 C10 C 0.65011(13) 0.92954(17) 0.67539(6) 0.0423(5) Uani 1 1 d . . . . .
 C11 C 0.60558(13) 0.88150(16) 0.70555(6) 0.0412(4) Uani 1 1 d . . . . .
 H11 H 0.554842 0.917272 0.710102 0.049 Uiso 1 1 calc R . . . .
 C12 C 0.63473(13) 0.78139(16) 0.72913(6) 0.0398(4) Uani 1 1 d . . . . .
 H12 H 0.604507 0.749591 0.750255 0.048 Uiso 1 1 calc R . . . .
 C13 C 0.61386(14) 1.03087(18) 0.64606(7) 0.0493(5) Uani 1 1 d . . . . .
 H13A H 0.581731 1.082342 0.662845 0.059 Uiso 1 1 calc R . . . .
 H13B H 0.660140 1.076863 0.637499 0.059 Uiso 1 1 calc R . . . .
 C14 C 0.47324(14) 0.9927(2) 0.59974(7) 0.0522(5) Uani 1 1 d . . . . .
 H14 H 0.449624 1.030816 0.622245 0.063 Uiso 1 1 calc R . . . .
 C15 C 0.42060(14) 0.9462(2) 0.56263(7) 0.0529(5) Uani 1 1 d . . . . .
 H15 H 0.361017 0.952786 0.559544 0.064 Uiso 1 1 calc R . . . .
 C16 C 0.45391(13) 0.89025(16) 0.52988(6) 0.0410(4) Uani 1 1 d . . . . .
 C17 C 0.54149(14) 0.88254(19) 0.53618(7) 0.0502(5) Uani 1 1 d . . . . .
 H17 H 0.566895 0.843857 0.514472 0.060 Uiso 1 1 calc R . . . .
 C18 C 0.59078(14) 0.9307(2) 0.57361(7) 0.0532(5) Uani 1 1 d . . . . .
 H18 H 0.650583 0.925386 0.577651 0.064 Uiso 1 1 calc R . . . .
 C19 C 0.40121(12) 0.83830(17) 0.48853(6) 0.0406(4) Uani 1 1 d . . . . .
 C20 C 0.43677(13) 0.68729(17) 0.39819(7) 0.0443(5) Uani 1 1 d . . . . .
 P1 P 0.38802(3) 0.66997(5) 0.64102(2) 0.04170(15) Uani 1 1 d . . . . .
 F1 F 0.39474(7) 0.80103(10) 0.65946(4) 0.0494(3) Uani 1 1 d . . . . .
 F2 F 0.43420(8) 0.62357(11) 0.68998(4) 0.0511(3) Uani 1 1 d . . . . .
 F3 F 0.29886(7) 0.65666(11) 0.65620(4) 0.0557(3) Uani 1 1 d . . . . .
 F4 F 0.33973(8) 0.71566(12) 0.59256(4) 0.0583(3) Uani 1 1 d . . . . .
 F5 F 0.47596(8) 0.68289(12) 0.62624(4) 0.0578(3) Uani 1 1 d . . . . .
 F6 F 0.37993(9) 0.53793(11) 0.62313(4) 0.0625(4) Uani 1 1 d . . . . .
 P2 P 0.500000 1.19236(7) 0.750000 0.0521(2) Uani 1 2 d S T P . .
 F7 F 0.45268(8) 1.09486(13) 0.71726(5) 0.0679(4) Uani 1 1 d . . . . .
 F8 F 0.57609(8) 1.19240(12) 0.72335(5) 0.0642(4) Uani 1 1 d . . . . .
 F9 F 0.4489(3) 1.2768(4) 0.70639(12) 0.0606(10) Uani 0.5 1 d . . . A 1
 F10 F 0.4570(3) 1.3019(4) 0.72821(12) 0.0553(9) Uani 0.5 1 d . . . A 2


_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
  _geom_bond_atom_site_label_1
  _geom_bond_atom_site_label_2
  _geom_bond_distance
  _geom_bond_site_symmetry_2
  _geom_bond_publ_flag
 N1 C3 1.342(3) . ?
 N1 C4 1.329(3) . ?
 N1 C6 1.496(2) . ?
 N2 C13 1.494(2) . ?
 N2 C14 1.328(3) . ?
 N2 C18 1.333(3) . ?
 N3 H3A 0.8800 . ?
 N3 H3B 0.8800 . ?
 N3 C19 1.337(3) . ?
 N4 N5 1.389(2) . ?
 N4 C19 1.311(3) . ?
 N5 C20 1.289(3) . ?
 N6 H6C 0.8800 . ?
 N6 H6D 0.8800 . ?
 N6 C20 1.341(3) . ?
 C1 C2 1.388(3) . ?
 C1 C5 1.377(3) . ?
 C1 C20 1.485(3) 5_666 ?
 C2 H2 0.9500 . ?
 C2 C3 1.370(3) . ?
 C3 H3 0.9500 . ?
 C4 H4 0.9500 . ?
 C4 C5 1.359(3) . ?
 C5 H5 0.9500 . ?
 C6 H6A 0.9900 . ?
 C6 H6B 0.9900 . ?
 C6 C7 1.504(3) . ?
 C7 C8 1.385(3) . ?
 C7 C12 1.386(3) . ?
 C8 H8 0.9500 . ?
 C8 C9 1.386(3) . ?
 C9 H9 0.9500 . ?
 C9 C10 1.382(3) . ?
 C10 C11 1.383(3) . ?
 C10 C13 1.508(3) . ?
 C11 H11 0.9500 . ?
 C11 C12 1.384(3) . ?
 C12 H12 0.9500 . ?
 C13 H13A 0.9900 . ?
 C13 H13B 0.9900 . ?
 C14 H14 0.9500 . ?
 C14 C15 1.372(3) . ?
 C15 H15 0.9500 . ?
 C15 C16 1.376(3) . ?
 C16 C17 1.390(3) . ?
 C16 C19 1.489(3) . ?
 C17 H17 0.9500 . ?
 C17 C18 1.363(3) . ?
 C18 H18 0.9500 . ?
 P1 F1 1.6009(13) . ?
 P1 F2 1.6088(12) . ?
 P1 F3 1.6019(13) . ?
 P1 F4 1.6036(12) . ?
 P1 F5 1.5768(13) . ?
 P1 F6 1.6062(14) . ?
 P2 F7 1.5854(14) 2_656 ?
 P2 F7 1.5854(14) . ?
 P2 F8 1.5965(14) . ?
 P2 F8 1.5964(14) 2_656 ?
 P2 F9 1.710(4) 2_656 ?
 P2 F9 1.710(4) . ?
 P2 F10 1.521(4) 2_656 ?
 P2 F10 1.521(4) . ?
 F10 F10 1.713(8) 2_656 ?

loop_
  _geom_angle_atom_site_label_1
  _geom_angle_atom_site_label_2
  _geom_angle_atom_site_label_3
  _geom_angle
  _geom_angle_site_symmetry_1
  _geom_angle_site_symmetry_3
  _geom_angle_publ_flag
 C3 N1 C6 120.87(17) . . ?
 C4 N1 C3 120.20(18) . . ?
 C4 N1 C6 118.57(16) . . ?
 C14 N2 C13 120.85(18) . . ?
 C14 N2 C18 120.24(18) . . ?
 C18 N2 C13 118.82(19) . . ?
 H3A N3 H3B 120.0 . . ?
 C19 N3 H3A 120.0 . . ?
 C19 N3 H3B 120.0 . . ?
 C19 N4 N5 112.77(16) . . ?
 C20 N5 N4 111.57(16) . . ?
 H6C N6 H6D 120.0 . . ?
 C20 N6 H6C 120.0 . . ?
 C20 N6 H6D 120.0 . . ?
 C2 C1 C20 120.92(18) . 5_666 ?
 C5 C1 C2 117.58(19) . . ?
 C5 C1 C20 121.48(18) . 5_666 ?
 C1 C2 H2 120.1 . . ?
 C3 C2 C1 119.8(2) . . ?
 C3 C2 H2 120.1 . . ?
 N1 C3 C2 120.7(2) . . ?
 N1 C3 H3 119.7 . . ?
 C2 C3 H3 119.7 . . ?
 N1 C4 H4 119.4 . . ?
 N1 C4 C5 121.14(19) . . ?
 C5 C4 H4 119.4 . . ?
 C1 C5 H5 119.8 . . ?
 C4 C5 C1 120.5(2) . . ?
 C4 C5 H5 119.8 . . ?
 N1 C6 H6A 110.1 . . ?
 N1 C6 H6B 110.1 . . ?
 N1 C6 C7 108.19(14) . . ?
 H6A C6 H6B 108.4 . . ?
 C7 C6 H6A 110.1 . . ?
 C7 C6 H6B 110.1 . . ?
 C8 C7 C6 119.88(18) . . ?
 C8 C7 C12 119.19(18) . . ?
 C12 C7 C6 120.75(17) . . ?
 C7 C8 H8 119.8 . . ?
 C7 C8 C9 120.5(2) . . ?
 C9 C8 H8 119.8 . . ?
 C8 C9 H9 120.0 . . ?
 C10 C9 C8 119.97(19) . . ?
 C10 C9 H9 120.0 . . ?
 C9 C10 C11 119.73(18) . . ?
 C9 C10 C13 119.93(19) . . ?
 C11 C10 C13 120.2(2) . . ?
 C10 C11 H11 119.9 . . ?
 C10 C11 C12 120.18(19) . . ?
 C12 C11 H11 119.9 . . ?
 C7 C12 H12 119.9 . . ?
 C11 C12 C7 120.30(18) . . ?
 C11 C12 H12 119.9 . . ?
 N2 C13 C10 108.83(15) . . ?
 N2 C13 H13A 109.9 . . ?
 N2 C13 H13B 109.9 . . ?
 C10 C13 H13A 109.9 . . ?
 C10 C13 H13B 109.9 . . ?
 H13A C13 H13B 108.3 . . ?
 N2 C14 H14 119.5 . . ?
 N2 C14 C15 120.9(2) . . ?
 C15 C14 H14 119.5 . . ?
 C14 C15 H15 119.9 . . ?
 C14 C15 C16 120.2(2) . . ?
 C16 C15 H15 119.9 . . ?
 C15 C16 C17 117.58(19) . . ?
 C15 C16 C19 123.45(19) . . ?
 C17 C16 C19 118.97(18) . . ?
 C16 C17 H17 120.1 . . ?
 C18 C17 C16 119.8(2) . . ?
 C18 C17 H17 120.1 . . ?
 N2 C18 C17 121.3(2) . . ?
 N2 C18 H18 119.4 . . ?
 C17 C18 H18 119.4 . . ?
 N3 C19 C16 119.89(18) . . ?
 N4 C19 N3 125.61(18) . . ?
 N4 C19 C16 114.50(17) . . ?
 N5 C20 N6 124.6(2) . . ?
 N5 C20 C1 117.50(18) . 5_666 ?
 N6 C20 C1 117.86(18) . 5_666 ?
 F1 P1 F2 90.26(7) . . ?
 F1 P1 F3 89.57(7) . . ?
 F1 P1 F4 89.83(7) . . ?
 F1 P1 F6 178.87(8) . . ?
 F3 P1 F2 89.02(7) . . ?
 F3 P1 F4 89.55(7) . . ?
 F3 P1 F6 89.36(8) . . ?
 F4 P1 F2 178.56(7) . . ?
 F4 P1 F6 90.54(7) . . ?
 F5 P1 F1 90.44(7) . . ?
 F5 P1 F2 90.78(7) . . ?
 F5 P1 F3 179.79(8) . . ?
 F5 P1 F4 90.66(7) . . ?
 F5 P1 F6 90.63(8) . . ?
 F6 P1 F2 89.34(7) . . ?
 F7 P2 F7 90.16(12) 2_656 . ?
 F7 P2 F8 89.53(8) . 2_656 ?
 F7 P2 F8 90.50(8) . . ?
 F7 P2 F8 89.53(7) 2_656 . ?
 F7 P2 F8 90.50(8) 2_656 2_656 ?
 F7 P2 F9 168.41(16) 2_656 . ?
 F7 P2 F9 79.73(16) . . ?
 F7 P2 F9 79.73(16) 2_656 2_656 ?
 F7 P2 F9 168.41(16) . 2_656 ?
 F8 P2 F8 179.96(11) 2_656 . ?
 F8 P2 F9 84.95(15) . . ?
 F8 P2 F9 95.03(15) 2_656 . ?
 F8 P2 F9 84.95(15) 2_656 2_656 ?
 F8 P2 F9 95.03(15) . 2_656 ?
 F9 P2 F9 110.9(3) . 2_656 ?
 F10 P2 F7 167.19(15) 2_656 . ?
 F10 P2 F7 101.07(16) . . ?
 F10 P2 F8 83.54(16) 2_656 . ?
 F10 P2 F8 96.43(16) . . ?
 F10 P2 F10 68.5(3) 2_656 . ?
 P2 F10 F10 55.74(16) . 2_656 ?

_olex2_submission_special_instructions  'No special instructions were received'
