data_4tritylArOH_0m_a _audit_creation_method 'SHELXL-2018/3' _shelx_SHELXL_version_number '2018/3' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C33 H36 O' _chemical_formula_sum 'C33 H36 O' _chemical_formula_weight 448.62 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.6158(9) _cell_length_b 10.5411(10) _cell_length_c 13.8499(14) _cell_angle_alpha 99.752(3) _cell_angle_beta 106.021(4) _cell_angle_gamma 98.980(4) _cell_volume 1299.0(2) _cell_formula_units_Z 2 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 11245 _cell_measurement_theta_min 2.815 _cell_measurement_theta_max 28.2715 _exptl_crystal_description block _exptl_crystal_colour colorless _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.147 _exptl_crystal_F_000 484 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.2 _exptl_absorpt_coefficient_mu 0.067 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type ? _exptl_absorpt_correction_T_min ? _exptl_absorpt_correction_T_max ? _exptl_absorpt_process_details ? _exptl_absorpt_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source ? _diffrn_measurement_device_type 'Bruker AXS Area Detector' _diffrn_measurement_method ? _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 28364 _diffrn_reflns_av_unetI/netI 0.0615 _diffrn_reflns_av_R_equivalents 0.0676 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_theta_min 2.007 _diffrn_reflns_theta_max 28.325 _diffrn_reflns_theta_full 25.000 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measured_fraction_theta_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.996 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.996 _diffrn_reflns_point_group_measured_fraction_full 0.999 _reflns_number_total 6449 _reflns_number_gt 5149 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0577P)^2^+0.6500P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 6449 _refine_ls_number_parameters 314 _refine_ls_number_restraints 2 _refine_ls_R_factor_all 0.0666 _refine_ls_R_factor_gt 0.0521 _refine_ls_wR_factor_ref 0.1433 _refine_ls_wR_factor_gt 0.1320 _refine_ls_goodness_of_fit_ref 1.031 _refine_ls_restrained_S_all 1.041 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 0.80417(14) 0.79585(13) 0.77891(10) 0.0163(3) Uani 1 1 d . . . . . C2 C 0.71254(14) 0.75275(13) 0.83595(10) 0.0164(3) Uani 1 1 d . . . . . C3 C 0.65702(14) 0.61732(13) 0.81721(10) 0.0165(3) Uani 1 1 d . . . . . H3 H 0.600244 0.585752 0.857875 0.020 Uiso 1 1 calc R U . . . C4 C 0.68144(14) 0.52677(13) 0.74144(10) 0.0150(3) Uani 1 1 d . . . . . C5 C 0.77203(14) 0.57405(13) 0.68669(10) 0.0155(3) Uani 1 1 d . . . . . H5 H 0.790019 0.513022 0.635047 0.019 Uiso 1 1 calc R U . . . C6 C 0.83753(14) 0.70708(13) 0.70434(10) 0.0155(3) Uani 1 1 d . . . . . C7 C 0.66861(16) 0.84874(14) 0.91385(11) 0.0195(3) Uani 1 1 d . . . . . C8 C 0.57302(19) 0.93326(16) 0.85614(13) 0.0299(3) Uani 1 1 d . . . . . H8A H 0.627105 0.978709 0.816961 0.045 Uiso 1 1 calc DR U . . . H8B H 0.550740 0.998434 0.905928 0.045 Uiso 1 1 calc R U . . . H8C H 0.480364 0.876465 0.808780 0.045 Uiso 1 1 calc R U . . . C9 C 0.80282(18) 0.93794(15) 1.00116(12) 0.0265(3) Uani 1 1 d . . . . . H9A H 0.780207 0.947407 1.066473 0.040 Uiso 1 1 calc R U . . . H9B H 0.823959 1.024881 0.985604 0.040 Uiso 1 1 calc DR U . . . H9C H 0.889447 0.898132 1.006774 0.040 Uiso 1 1 calc R U . . . C10 C 0.57452(19) 0.77386(16) 0.96839(13) 0.0292(3) Uani 1 1 d . . . . . H10A H 0.485284 0.717038 0.916929 0.044 Uiso 1 1 calc R U . . . H10B H 0.546014 0.837120 1.015873 0.044 Uiso 1 1 calc R U . . . H10C H 0.632361 0.719724 1.007094 0.044 Uiso 1 1 calc R U . . . C11 C 0.62663(14) 0.37773(13) 0.73053(10) 0.0152(3) Uani 1 1 d . . . . . C12 C 0.46335(14) 0.33820(13) 0.72796(10) 0.0164(3) Uani 1 1 d . . . . . C13 C 0.36253(15) 0.42007(14) 0.71411(11) 0.0205(3) Uani 1 1 d . . . . . H13 H 0.394380 0.507886 0.708866 0.025 Uiso 1 1 calc R U . . . C14 C 0.21502(16) 0.37483(16) 0.70782(12) 0.0256(3) Uani 1 1 d . . . . . H14 H 0.148448 0.432878 0.700018 0.031 Uiso 1 1 calc R U . . . C15 C 0.16492(17) 0.24675(16) 0.71281(12) 0.0268(3) Uani 1 1 d . . . . . H15 H 0.064566 0.216465 0.708539 0.032 Uiso 1 1 calc R U . . . C16 C 0.26315(17) 0.16298(15) 0.72415(13) 0.0271(3) Uani 1 1 d . . . . . H16 H 0.229968 0.074396 0.727087 0.033 Uiso 1 1 calc R U . . . C17 C 0.40993(16) 0.20832(14) 0.73121(12) 0.0222(3) Uani 1 1 d . . . . . H17 H 0.475754 0.149579 0.738437 0.027 Uiso 1 1 calc R U . . . C18 C 0.73440(15) 0.34859(13) 0.82583(10) 0.0169(3) Uani 1 1 d . . . . . C19 C 0.69444(16) 0.33070(15) 0.91268(11) 0.0225(3) Uani 1 1 d . . . . . H19 H 0.595110 0.328791 0.912103 0.027 Uiso 1 1 calc R U . . . C20 C 0.79805(18) 0.31556(17) 1.00040(12) 0.0283(3) Uani 1 1 d . . . . . H20 H 0.768310 0.302839 1.058640 0.034 Uiso 1 1 calc R U . . . C21 C 0.94337(17) 0.31882(16) 1.00370(12) 0.0279(3) Uani 1 1 d . . . . . H21 H 1.013346 0.307504 1.063422 0.033 Uiso 1 1 calc R U . . . C22 C 0.98576(17) 0.33886(15) 0.91855(12) 0.0262(3) Uani 1 1 d . . . . . H22 H 1.085615 0.341887 0.920062 0.031 Uiso 1 1 calc R U . . . C23 C 0.88306(16) 0.35452(14) 0.83117(11) 0.0216(3) Uani 1 1 d . . . . . H23 H 0.914095 0.369536 0.773874 0.026 Uiso 1 1 calc R U . . . C24 C 0.62823(14) 0.29636(13) 0.62692(10) 0.0165(3) Uani 1 1 d . . . . . C25 C 0.68912(16) 0.18501(14) 0.61849(12) 0.0223(3) Uani 1 1 d . . . . . H25 H 0.738741 0.159051 0.678995 0.027 Uiso 1 1 calc R U . . . C26 C 0.67779(18) 0.11111(15) 0.52165(12) 0.0276(3) Uani 1 1 d . . . . . H26 H 0.720596 0.035830 0.517051 0.033 Uiso 1 1 calc R U . . . C27 C 0.60524(17) 0.14629(15) 0.43287(12) 0.0244(3) Uani 1 1 d . . . . . H27 H 0.598893 0.096073 0.367417 0.029 Uiso 1 1 calc R U . . . C28 C 0.54123(16) 0.25593(14) 0.43965(11) 0.0219(3) Uani 1 1 d . . . . . H28 H 0.490475 0.280662 0.378851 0.026 Uiso 1 1 calc R U . . . C29 C 0.55212(15) 0.32888(13) 0.53590(11) 0.0190(3) Uani 1 1 d . . . . . H29 H 0.506771 0.402642 0.540024 0.023 Uiso 1 1 calc R U . . . C30 C 0.94632(15) 0.75215(13) 0.64722(10) 0.0177(3) Uani 1 1 d . . . . . C31 C 0.89739(19) 0.85682(15) 0.58789(12) 0.0259(3) Uani 1 1 d . . . . . H31A H 0.967311 0.880720 0.550831 0.039 Uiso 1 1 calc R U . . . H31B H 0.895548 0.935243 0.636557 0.039 Uiso 1 1 calc R U . . . H31C H 0.798149 0.821132 0.538506 0.039 Uiso 1 1 calc R U . . . C32 C 1.10153(16) 0.80574(16) 0.72611(12) 0.0255(3) Uani 1 1 d . . . . . H32A H 1.172485 0.831722 0.690327 0.038 Uiso 1 1 calc R U . . . H32B H 1.131565 0.737149 0.761961 0.038 Uiso 1 1 calc R U . . . H32C H 1.099393 0.882488 0.776283 0.038 Uiso 1 1 calc R U . . . C33 C 0.95874(17) 0.63724(14) 0.56776(11) 0.0228(3) Uani 1 1 d . . . . . H33A H 0.861005 0.598400 0.517226 0.034 Uiso 1 1 calc R U . . . H33B H 0.995496 0.570225 0.602907 0.034 Uiso 1 1 calc R U . . . H33C H 1.027626 0.669779 0.532450 0.034 Uiso 1 1 calc R U . . . O1 O 0.86704(12) 0.92748(9) 0.79333(8) 0.0239(2) Uani 1 1 d . . . . . H1 H 0.849730 0.971391 0.843603 0.036 Uiso 1 1 calc DR U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.0163(6) 0.0133(6) 0.0177(6) 0.0021(5) 0.0038(5) 0.0028(5) C2 0.0159(6) 0.0163(6) 0.0162(6) 0.0017(5) 0.0040(5) 0.0051(5) C3 0.0147(6) 0.0176(6) 0.0175(6) 0.0040(5) 0.0053(5) 0.0036(5) C4 0.0134(6) 0.0144(6) 0.0169(6) 0.0038(5) 0.0035(5) 0.0036(5) C5 0.0154(6) 0.0151(6) 0.0163(6) 0.0024(5) 0.0054(5) 0.0045(5) C6 0.0149(6) 0.0164(6) 0.0155(6) 0.0037(5) 0.0044(5) 0.0043(5) C7 0.0206(7) 0.0179(6) 0.0196(6) -0.0003(5) 0.0078(5) 0.0052(5) C8 0.0312(8) 0.0291(8) 0.0318(8) 0.0029(6) 0.0101(7) 0.0169(7) C9 0.0297(8) 0.0237(7) 0.0215(7) -0.0039(6) 0.0076(6) 0.0027(6) C10 0.0351(9) 0.0242(7) 0.0312(8) -0.0021(6) 0.0216(7) 0.0036(6) C11 0.0141(6) 0.0144(6) 0.0182(6) 0.0042(5) 0.0056(5) 0.0041(5) C12 0.0149(6) 0.0173(6) 0.0158(6) 0.0029(5) 0.0043(5) 0.0024(5) C13 0.0184(7) 0.0201(7) 0.0237(7) 0.0068(5) 0.0064(5) 0.0044(5) C14 0.0182(7) 0.0285(8) 0.0309(8) 0.0057(6) 0.0078(6) 0.0082(6) C15 0.0173(7) 0.0313(8) 0.0300(8) 0.0034(6) 0.0094(6) 0.0002(6) C16 0.0239(7) 0.0218(7) 0.0345(8) 0.0065(6) 0.0107(6) -0.0018(6) C17 0.0200(7) 0.0188(7) 0.0276(7) 0.0052(6) 0.0077(6) 0.0030(5) C18 0.0170(6) 0.0143(6) 0.0191(6) 0.0040(5) 0.0045(5) 0.0042(5) C19 0.0189(7) 0.0278(7) 0.0233(7) 0.0100(6) 0.0074(6) 0.0066(6) C20 0.0282(8) 0.0377(9) 0.0228(7) 0.0140(6) 0.0085(6) 0.0097(7) C21 0.0244(8) 0.0317(8) 0.0259(8) 0.0106(6) 0.0006(6) 0.0099(6) C22 0.0171(7) 0.0285(8) 0.0325(8) 0.0081(6) 0.0047(6) 0.0070(6) C23 0.0182(7) 0.0242(7) 0.0241(7) 0.0063(6) 0.0081(5) 0.0057(5) C24 0.0149(6) 0.0142(6) 0.0196(6) 0.0026(5) 0.0059(5) 0.0014(5) C25 0.0255(7) 0.0193(7) 0.0234(7) 0.0056(5) 0.0069(6) 0.0089(5) C26 0.0340(8) 0.0212(7) 0.0292(8) 0.0019(6) 0.0114(7) 0.0121(6) C27 0.0281(8) 0.0213(7) 0.0215(7) -0.0020(6) 0.0088(6) 0.0042(6) C28 0.0211(7) 0.0234(7) 0.0189(7) 0.0041(5) 0.0041(5) 0.0024(5) C29 0.0183(6) 0.0171(6) 0.0211(7) 0.0037(5) 0.0052(5) 0.0043(5) C30 0.0199(7) 0.0161(6) 0.0183(6) 0.0040(5) 0.0086(5) 0.0023(5) C31 0.0359(8) 0.0217(7) 0.0253(7) 0.0101(6) 0.0140(6) 0.0082(6) C32 0.0207(7) 0.0283(8) 0.0252(7) 0.0038(6) 0.0086(6) -0.0013(6) C33 0.0278(7) 0.0198(7) 0.0242(7) 0.0034(6) 0.0149(6) 0.0037(6) O1 0.0320(6) 0.0121(5) 0.0279(5) -0.0006(4) 0.0152(5) 0.0005(4) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 O1 1.3813(16) . ? C1 C2 1.4099(19) . ? C1 C6 1.4122(18) . ? C2 C3 1.3967(19) . ? C2 C7 1.5432(18) . ? C3 C4 1.3907(18) . ? C3 H3 0.9500 . ? C4 C5 1.3925(18) . ? C4 C11 1.5447(18) . ? C5 C6 1.3950(18) . ? C5 H5 0.9500 . ? C6 C30 1.5410(18) . ? C7 C10 1.539(2) . ? C7 C8 1.539(2) . ? C7 C9 1.545(2) . ? C8 H8A 0.9800 . ? C8 H8B 0.9800 . ? C8 H8C 0.9800 . ? C9 H9A 0.9800 . ? C9 H9B 0.9800 . ? C9 H9C 0.9800 . ? C10 H10A 0.9800 . ? C10 H10B 0.9800 . ? C10 H10C 0.9800 . ? C11 C18 1.5467(18) . ? C11 C24 1.5474(18) . ? C11 C12 1.5492(18) . ? C12 C13 1.3915(18) . ? C12 C17 1.3979(19) . ? C13 C14 1.398(2) . ? C13 H13 0.9500 . ? C14 C15 1.381(2) . ? C14 H14 0.9500 . ? C15 C16 1.386(2) . ? C15 H15 0.9500 . ? C16 C17 1.388(2) . ? C16 H16 0.9500 . ? C17 H17 0.9500 . ? C18 C19 1.393(2) . ? C18 C23 1.4017(19) . ? C19 C20 1.393(2) . ? C19 H19 0.9500 . ? C20 C21 1.380(2) . ? C20 H20 0.9500 . ? C21 C22 1.387(2) . ? C21 H21 0.9500 . ? C22 C23 1.388(2) . ? C22 H22 0.9500 . ? C23 H23 0.9500 . ? C24 C25 1.3928(18) . ? C24 C29 1.3992(19) . ? C25 C26 1.399(2) . ? C25 H25 0.9500 . ? C26 C27 1.378(2) . ? C26 H26 0.9500 . ? C27 C28 1.393(2) . ? C27 H27 0.9500 . ? C28 C29 1.389(2) . ? C28 H28 0.9500 . ? C29 H29 0.9500 . ? C30 C33 1.5357(19) . ? C30 C32 1.539(2) . ? C30 C31 1.5395(19) . ? C31 H31A 0.9800 . ? C31 H31B 0.9800 . ? C31 H31C 0.9800 . ? C32 H32A 0.9800 . ? C32 H32B 0.9800 . ? C32 H32C 0.9800 . ? C33 H33A 0.9800 . ? C33 H33B 0.9800 . ? C33 H33C 0.9800 . ? O1 H1 0.8400 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 C1 C2 121.76(12) . . ? O1 C1 C6 116.26(12) . . ? C2 C1 C6 121.99(12) . . ? C3 C2 C1 117.33(12) . . ? C3 C2 C7 119.91(12) . . ? C1 C2 C7 122.73(12) . . ? C4 C3 C2 122.69(12) . . ? C4 C3 H3 118.7 . . ? C2 C3 H3 118.7 . . ? C3 C4 C5 117.81(12) . . ? C3 C4 C11 119.78(11) . . ? C5 C4 C11 121.88(11) . . ? C4 C5 C6 122.90(12) . . ? C4 C5 H5 118.6 . . ? C6 C5 H5 118.6 . . ? C5 C6 C1 117.15(12) . . ? C5 C6 C30 120.50(11) . . ? C1 C6 C30 122.30(12) . . ? C10 C7 C8 106.98(13) . . ? C10 C7 C2 111.27(11) . . ? C8 C7 C2 109.32(12) . . ? C10 C7 C9 105.38(12) . . ? C8 C7 C9 110.26(12) . . ? C2 C7 C9 113.39(11) . . ? C7 C8 H8A 109.5 . . ? C7 C8 H8B 109.5 . . ? H8A C8 H8B 109.5 . . ? C7 C8 H8C 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C7 C9 H9A 109.5 . . ? C7 C9 H9B 109.5 . . ? H9A C9 H9B 109.5 . . ? C7 C9 H9C 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? C7 C10 H10A 109.5 . . ? C7 C10 H10B 109.5 . . ? H10A C10 H10B 109.5 . . ? C7 C10 H10C 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C4 C11 C18 103.17(10) . . ? C4 C11 C24 111.54(10) . . ? C18 C11 C24 113.47(10) . . ? C4 C11 C12 114.11(10) . . ? C18 C11 C12 111.56(11) . . ? C24 C11 C12 103.34(10) . . ? C13 C12 C17 117.44(13) . . ? C13 C12 C11 124.37(12) . . ? C17 C12 C11 117.98(12) . . ? C12 C13 C14 120.87(13) . . ? C12 C13 H13 119.6 . . ? C14 C13 H13 119.6 . . ? C15 C14 C13 120.78(14) . . ? C15 C14 H14 119.6 . . ? C13 C14 H14 119.6 . . ? C14 C15 C16 119.05(14) . . ? C14 C15 H15 120.5 . . ? C16 C15 H15 120.5 . . ? C15 C16 C17 120.12(14) . . ? C15 C16 H16 119.9 . . ? C17 C16 H16 119.9 . . ? C16 C17 C12 121.69(14) . . ? C16 C17 H17 119.2 . . ? C12 C17 H17 119.2 . . ? C19 C18 C23 117.57(13) . . ? C19 C18 C11 122.59(12) . . ? C23 C18 C11 119.46(12) . . ? C18 C19 C20 120.94(14) . . ? C18 C19 H19 119.5 . . ? C20 C19 H19 119.5 . . ? C21 C20 C19 120.80(14) . . ? C21 C20 H20 119.6 . . ? C19 C20 H20 119.6 . . ? C20 C21 C22 119.04(14) . . ? C20 C21 H21 120.5 . . ? C22 C21 H21 120.5 . . ? C21 C22 C23 120.34(14) . . ? C21 C22 H22 119.8 . . ? C23 C22 H22 119.8 . . ? C22 C23 C18 121.27(14) . . ? C22 C23 H23 119.4 . . ? C18 C23 H23 119.4 . . ? C25 C24 C29 117.93(13) . . ? C25 C24 C11 123.66(12) . . ? C29 C24 C11 118.12(11) . . ? C24 C25 C26 120.53(14) . . ? C24 C25 H25 119.7 . . ? C26 C25 H25 119.7 . . ? C27 C26 C25 120.73(14) . . ? C27 C26 H26 119.6 . . ? C25 C26 H26 119.6 . . ? C26 C27 C28 119.60(14) . . ? C26 C27 H27 120.2 . . ? C28 C27 H27 120.2 . . ? C29 C28 C27 119.57(13) . . ? C29 C28 H28 120.2 . . ? C27 C28 H28 120.2 . . ? C28 C29 C24 121.61(13) . . ? C28 C29 H29 119.2 . . ? C24 C29 H29 119.2 . . ? C33 C30 C32 106.98(12) . . ? C33 C30 C31 106.63(11) . . ? C32 C30 C31 110.70(12) . . ? C33 C30 C6 111.80(11) . . ? C32 C30 C6 108.71(11) . . ? C31 C30 C6 111.91(11) . . ? C30 C31 H31A 109.5 . . ? C30 C31 H31B 109.5 . . ? H31A C31 H31B 109.5 . . ? C30 C31 H31C 109.5 . . ? H31A C31 H31C 109.5 . . ? H31B C31 H31C 109.5 . . ? C30 C32 H32A 109.5 . . ? C30 C32 H32B 109.5 . . ? H32A C32 H32B 109.5 . . ? C30 C32 H32C 109.5 . . ? H32A C32 H32C 109.5 . . ? H32B C32 H32C 109.5 . . ? C30 C33 H33A 109.5 . . ? C30 C33 H33B 109.5 . . ? H33A C33 H33B 109.5 . . ? C30 C33 H33C 109.5 . . ? H33A C33 H33C 109.5 . . ? H33B C33 H33C 109.5 . . ? C1 O1 H1 109.5 . . ? _refine_diff_density_max 0.525 _refine_diff_density_min -0.521 _refine_diff_density_rms 0.055 _shelx_res_file ; TITL 4tritylArOH_0m_a.res in P-1 4tritylArOH_0m_a.res created by SHELXL-2018/3 at 10:27:56 on 08-Dec-2019 CELL 0.71073 9.6158 10.5411 13.8499 99.752 106.021 98.980 ZERR 2.00 0.0009 0.0010 0.0014 0.003 0.004 0.004 LATT 1 SFAC C H O UNIT 66 72 2 LIST 6 ! automatically inserted. Change 6 to 4 for CHECKCIF!! MERG 2 DFIX 2.1 0.005 H1 H8A H1 H9B FMAP 2 PLAN 50 ACTA 50.00 BOND $H L.S. 10 TEMP -173.15 WGHT 0.057700 0.650000 FVAR 0.68541 C1 1 0.804173 0.795853 0.778909 11.00000 0.01628 0.01334 = 0.01770 0.00215 0.00379 0.00284 C2 1 0.712540 0.752755 0.835954 11.00000 0.01588 0.01628 = 0.01618 0.00171 0.00401 0.00511 C3 1 0.657018 0.617315 0.817207 11.00000 0.01472 0.01759 = 0.01752 0.00401 0.00533 0.00365 AFIX 43 H3 2 0.600244 0.585752 0.857875 11.00000 -1.20000 AFIX 0 C4 1 0.681444 0.526767 0.741437 11.00000 0.01337 0.01436 = 0.01685 0.00382 0.00352 0.00363 C5 1 0.772033 0.574049 0.686692 11.00000 0.01545 0.01506 = 0.01635 0.00239 0.00539 0.00450 AFIX 43 H5 2 0.790019 0.513022 0.635047 11.00000 -1.20000 AFIX 0 C6 1 0.837533 0.707076 0.704343 11.00000 0.01488 0.01638 = 0.01551 0.00369 0.00436 0.00435 C7 1 0.668608 0.848740 0.913851 11.00000 0.02065 0.01786 = 0.01957 -0.00031 0.00785 0.00516 C8 1 0.573023 0.933264 0.856139 11.00000 0.03119 0.02909 = 0.03177 0.00293 0.01013 0.01690 AFIX 137 H8A 2 0.627105 0.978709 0.816961 11.00000 -1.50000 H8B 2 0.550740 0.998434 0.905928 11.00000 -1.50000 H8C 2 0.480364 0.876465 0.808780 11.00000 -1.50000 AFIX 0 C9 1 0.802823 0.937944 1.001156 11.00000 0.02974 0.02373 = 0.02154 -0.00385 0.00762 0.00266 AFIX 137 H9A 2 0.780207 0.947407 1.066473 11.00000 -1.50000 H9B 2 0.823959 1.024881 0.985604 11.00000 -1.50000 H9C 2 0.889447 0.898132 1.006774 11.00000 -1.50000 AFIX 0 C10 1 0.574524 0.773856 0.968389 11.00000 0.03514 0.02421 = 0.03124 -0.00207 0.02156 0.00358 AFIX 137 H10A 2 0.485284 0.717038 0.916929 11.00000 -1.50000 H10B 2 0.546014 0.837120 1.015873 11.00000 -1.50000 H10C 2 0.632361 0.719724 1.007094 11.00000 -1.50000 AFIX 0 C11 1 0.626629 0.377726 0.730527 11.00000 0.01410 0.01443 = 0.01816 0.00417 0.00565 0.00413 C12 1 0.463350 0.338195 0.727961 11.00000 0.01494 0.01732 = 0.01580 0.00285 0.00431 0.00236 C13 1 0.362530 0.420071 0.714113 11.00000 0.01836 0.02008 = 0.02373 0.00677 0.00639 0.00435 AFIX 43 H13 2 0.394380 0.507886 0.708866 11.00000 -1.20000 AFIX 0 C14 1 0.215025 0.374826 0.707821 11.00000 0.01821 0.02849 = 0.03088 0.00568 0.00779 0.00819 AFIX 43 H14 2 0.148448 0.432878 0.700018 11.00000 -1.20000 AFIX 0 C15 1 0.164918 0.246751 0.712812 11.00000 0.01726 0.03130 = 0.03000 0.00344 0.00940 0.00020 AFIX 43 H15 2 0.064566 0.216465 0.708539 11.00000 -1.20000 AFIX 0 C16 1 0.263154 0.162983 0.724147 11.00000 0.02386 0.02176 = 0.03454 0.00648 0.01069 -0.00184 AFIX 43 H16 2 0.229968 0.074396 0.727087 11.00000 -1.20000 AFIX 0 C17 1 0.409928 0.208323 0.731210 11.00000 0.01998 0.01880 = 0.02756 0.00521 0.00771 0.00304 AFIX 43 H17 2 0.475754 0.149579 0.738437 11.00000 -1.20000 AFIX 0 C18 1 0.734404 0.348591 0.825834 11.00000 0.01698 0.01429 = 0.01910 0.00405 0.00446 0.00425 C19 1 0.694440 0.330700 0.912678 11.00000 0.01894 0.02779 = 0.02330 0.01001 0.00740 0.00657 AFIX 43 H19 2 0.595110 0.328791 0.912103 11.00000 -1.20000 AFIX 0 C20 1 0.798047 0.315561 1.000395 11.00000 0.02825 0.03774 = 0.02281 0.01399 0.00847 0.00972 AFIX 43 H20 2 0.768310 0.302839 1.058640 11.00000 -1.20000 AFIX 0 C21 1 0.943367 0.318821 1.003699 11.00000 0.02440 0.03172 = 0.02591 0.01065 0.00062 0.00991 AFIX 43 H21 2 1.013346 0.307504 1.063422 11.00000 -1.20000 AFIX 0 C22 1 0.985762 0.338863 0.918551 11.00000 0.01706 0.02855 = 0.03248 0.00810 0.00471 0.00702 AFIX 43 H22 2 1.085615 0.341887 0.920062 11.00000 -1.20000 AFIX 0 C23 1 0.883057 0.354516 0.831174 11.00000 0.01816 0.02415 = 0.02409 0.00635 0.00806 0.00573 AFIX 43 H23 2 0.914095 0.369536 0.773874 11.00000 -1.20000 AFIX 0 C24 1 0.628231 0.296360 0.626920 11.00000 0.01489 0.01422 = 0.01959 0.00261 0.00591 0.00137 C25 1 0.689120 0.185012 0.618491 11.00000 0.02551 0.01926 = 0.02343 0.00560 0.00689 0.00890 AFIX 43 H25 2 0.738741 0.159051 0.678995 11.00000 -1.20000 AFIX 0 C26 1 0.677789 0.111109 0.521651 11.00000 0.03402 0.02120 = 0.02923 0.00191 0.01142 0.01211 AFIX 43 H26 2 0.720596 0.035830 0.517051 11.00000 -1.20000 AFIX 0 C27 1 0.605239 0.146286 0.432871 11.00000 0.02813 0.02129 = 0.02149 -0.00197 0.00876 0.00415 AFIX 43 H27 2 0.598893 0.096073 0.367417 11.00000 -1.20000 AFIX 0 C28 1 0.541234 0.255934 0.439652 11.00000 0.02115 0.02337 = 0.01893 0.00413 0.00409 0.00245 AFIX 43 H28 2 0.490475 0.280662 0.378851 11.00000 -1.20000 AFIX 0 C29 1 0.552116 0.328879 0.535902 11.00000 0.01833 0.01707 = 0.02109 0.00367 0.00520 0.00426 AFIX 43 H29 2 0.506771 0.402642 0.540024 11.00000 -1.20000 AFIX 0 C30 1 0.946321 0.752145 0.647222 11.00000 0.01987 0.01612 = 0.01831 0.00398 0.00855 0.00233 C31 1 0.897386 0.856820 0.587888 11.00000 0.03589 0.02170 = 0.02534 0.01010 0.01401 0.00818 AFIX 137 H31A 2 0.967311 0.880720 0.550831 11.00000 -1.50000 H31B 2 0.895548 0.935243 0.636557 11.00000 -1.50000 H31C 2 0.798149 0.821132 0.538506 11.00000 -1.50000 AFIX 0 C32 1 1.101532 0.805742 0.726111 11.00000 0.02072 0.02832 = 0.02520 0.00381 0.00860 -0.00128 AFIX 137 H32A 2 1.172485 0.831722 0.690327 11.00000 -1.50000 H32B 2 1.131565 0.737149 0.761961 11.00000 -1.50000 H32C 2 1.099393 0.882488 0.776283 11.00000 -1.50000 AFIX 0 C33 1 0.958735 0.637242 0.567763 11.00000 0.02779 0.01978 = 0.02417 0.00335 0.01492 0.00372 AFIX 137 H33A 2 0.861005 0.598400 0.517226 11.00000 -1.50000 H33B 2 0.995496 0.570225 0.602907 11.00000 -1.50000 H33C 2 1.027626 0.669779 0.532450 11.00000 -1.50000 AFIX 0 O1 3 0.867037 0.927479 0.793329 11.00000 0.03198 0.01208 = 0.02789 -0.00056 0.01525 0.00046 AFIX 147 H1 2 0.849730 0.971391 0.843603 11.00000 -1.50000 AFIX 0 HKLF 4 REM 4tritylArOH_0m_a.res in P-1 REM wR2 = 0.143250, GooF = S = 1.03131, Restrained GooF = 1.04124 for all data REM R1 = 0.052069 for 5149 Fo > 4sig(Fo) and 0.066600 for all 6449 data REM 314 parameters refined using 2 restraints END WGHT 0.0577 0.6500 REM Highest difference peak 0.525, deepest hole -0.521, 1-sigma level 0.055 Q1 1 0.8660 0.8802 1.0438 11.00000 0.05 0.53 Q2 1 0.8780 0.9993 0.9765 11.00000 0.05 0.45 Q3 1 0.7641 1.0008 1.0460 11.00000 0.05 0.44 Q4 1 1.0224 0.7904 0.6847 11.00000 0.05 0.37 Q5 1 0.6904 0.8030 0.8769 11.00000 0.05 0.37 Q6 1 0.6334 0.3367 0.6796 11.00000 0.05 0.36 Q7 1 0.8136 0.7531 0.7334 11.00000 0.05 0.35 Q8 1 0.9557 0.6981 0.6107 11.00000 0.05 0.34 Q9 1 0.7300 0.8890 0.9515 11.00000 0.05 0.31 Q10 1 0.5410 0.3596 0.7260 11.00000 0.05 0.30 Q11 1 0.5563 0.2958 0.4906 11.00000 0.05 0.29 Q12 1 0.7309 0.7813 0.7978 11.00000 0.05 0.29 Q13 1 0.6768 0.3558 0.7755 11.00000 0.05 0.29 Q14 1 0.6570 0.4583 0.7360 11.00000 0.05 0.28 Q15 1 0.4444 0.2787 0.7484 11.00000 0.05 0.28 Q16 1 0.6500 0.2396 0.6164 11.00000 0.05 0.28 Q17 1 0.2835 0.3814 0.7054 11.00000 0.05 0.27 Q18 1 0.6500 0.5681 0.7632 11.00000 0.05 0.26 Q19 1 0.9170 0.8015 0.6222 11.00000 0.05 0.26 Q20 1 0.4109 0.3773 0.7244 11.00000 0.05 0.26 Q21 1 0.7574 0.3103 0.9532 11.00000 0.05 0.26 Q22 1 0.8940 0.7257 0.6816 11.00000 0.05 0.26 Q23 1 0.6248 0.8865 0.8849 11.00000 0.05 0.26 Q24 1 0.7017 0.6850 0.8411 11.00000 0.05 0.26 Q25 1 0.6262 0.8119 0.9354 11.00000 0.05 0.25 Q26 1 0.6975 0.5511 0.7013 11.00000 0.05 0.24 Q27 1 0.1893 0.2989 0.6812 11.00000 0.05 0.24 Q28 1 0.6161 0.3272 0.5830 11.00000 0.05 0.24 Q29 1 0.6845 0.1385 0.5711 11.00000 0.05 0.24 Q30 1 0.8608 0.2972 0.9888 11.00000 0.05 0.22 Q31 1 0.2003 0.3242 0.7454 11.00000 0.05 0.20 Q32 1 0.7857 0.6564 0.6835 11.00000 0.05 0.20 Q33 1 0.9234 0.3204 0.8728 11.00000 0.05 0.20 Q34 1 0.8258 0.6400 0.7148 11.00000 0.05 0.20 Q35 1 0.5960 0.2194 0.4526 11.00000 0.05 0.20 Q36 1 0.5616 0.1956 0.4417 11.00000 0.05 0.19 Q37 1 0.7100 0.3007 0.8616 11.00000 0.05 0.19 Q38 1 0.6737 0.1596 0.4831 11.00000 0.05 0.19 Q39 1 0.3431 0.2039 0.7428 11.00000 0.05 0.18 Q40 1 0.8038 0.3056 0.8253 11.00000 0.05 0.18 Q41 1 0.8171 0.3822 0.8423 11.00000 0.05 0.18 Q42 1 0.9265 0.3741 0.8917 11.00000 0.05 0.17 Q43 1 1.0869 0.4453 1.0625 11.00000 0.05 0.17 Q44 1 0.2337 0.2178 0.7515 11.00000 0.05 0.16 Q45 1 0.8306 0.9046 0.6126 11.00000 0.05 0.16 Q46 1 0.2024 0.1967 0.6950 11.00000 0.05 0.16 Q47 1 0.3663 0.5225 0.7364 11.00000 0.05 0.16 Q48 1 0.7190 0.3541 0.8716 11.00000 0.05 0.15 Q49 1 0.6865 0.0830 0.5164 11.00000 0.05 0.15 Q50 1 0.7979 0.9739 0.7941 11.00000 0.05 0.15 ; _shelx_res_checksum 77716 _shelx_hkl_file ; 1 0 0 147.99 11.90 -2 0 0 342.17 27.20 -3 0 0 25.00 2.50 -3 0 0 24.40 2.10 3 0 0 19.50 2.10 3 0 0 19.60 2.40 3 0 0 21.20 2.10 -4 0 0 244.38 19.00 -4 0 0 234.48 19.00 -4 0 0 243.08 19.40 4 0 0 247.78 19.50 4 0 0 221.08 19.10 4 0 0 229.38 19.00 -5 0 0 12.40 1.80 -5 0 0 10.50 2.20 -5 0 0 12.90 2.30 5 0 0 15.30 1.70 5 0 0 12.30 2.30 -6 0 0 4.90 1.20 -6 0 0 4.30 1.70 -6 0 0 6.80 1.90 6 0 0 3.40 1.40 6 0 0 4.30 1.00 -7 0 0 0.60 1.00 -7 0 0 1.60 2.00 -7 0 0 1.60 1.50 7 0 0 0.90 0.80 7 0 0 1.10 1.30 -8 0 0 52.89 5.90 -8 0 0 55.49 6.10 -8 0 0 57.49 6.10 -8 0 0 49.90 4.80 8 0 0 47.30 4.90 -9 0 0 23.30 2.50 -9 0 0 24.70 4.10 -9 0 0 22.40 4.10 -9 0 0 23.40 4.20 9 0 0 21.60 2.70 9 0 0 13.20 3.50 -10 0 0 2.20 2.40 -10 0 0 -0.20 2.10 -10 0 0 -1.80 2.50 10 0 0 0.80 0.80 -11 0 0 3.40 2.50 -11 0 0 -0.40 3.10 11 0 0 0.30 1.00 -12 0 0 33.90 6.20 12 0 0 25.30 3.10 -12 1 0 14.70 4.10 -12 1 0 10.40 4.30 11 -1 0 80.29 7.70 -11 1 0 104.69 9.90 -11 1 0 91.99 9.60 10 -1 0 24.50 2.90 10 -1 0 21.80 4.30 -10 1 0 26.30 4.60 -10 1 0 28.00 4.80 -10 1 0 39.20 5.40 9 -1 0 12.70 1.90 9 -1 0 8.60 2.60 -9 1 0 6.40 2.90 -9 1 0 11.70 3.00 -9 1 0 8.90 1.40 -9 1 0 9.00 2.90 8 -1 0 2.20 0.90 8 -1 0 0.20 1.60 -8 1 0 4.00 1.20 -8 1 0 2.30 2.00 -8 1 0 3.20 2.20 7 -1 0 206.88 16.90 7 -1 0 185.48 17.60 -7 1 0 194.38 16.70 -7 1 0 233.48 17.80 -7 1 0 211.38 17.50 6 -1 0 0.10 0.50 6 -1 0 0.40 1.00 -6 1 0 -2.50 1.30 -6 1 0 0.50 1.10 -6 1 0 -0.10 0.50 5 -1 0 33.60 3.40 5 -1 0 32.00 3.90 -5 1 0 36.40 3.90 -5 1 0 42.20 3.40 -5 1 0 41.80 4.10 -5 1 0 35.70 3.40 4 -1 0 669.23 53.09 3 -1 0 515.95 40.20 -3 1 0 489.25 40.00 2 -1 0 330.57 24.00 2 -1 0 285.17 24.10 -2 1 0 275.67 24.10 -2 1 0 315.77 24.00 0 1 0 173.68 12.90 0 1 0 148.19 12.80 -1 -1 0 347.57 33.50 1 1 0 323.77 32.80 -2 -1 0 386.46 30.90 -3 -1 0 159.88 14.00 -3 -1 0 173.88 13.80 -3 -1 0 177.98 14.10 3 1 0 161.28 14.00 3 1 0 168.28 13.80 3 1 0 177.58 13.80 -4 -1 0 19.70 2.40 -4 -1 0 12.80 2.40 -4 -1 0 11.00 1.80 4 1 0 14.30 2.30 4 1 0 14.60 1.80 -5 -1 0 25.10 3.00 -5 -1 0 21.90 2.40 -5 -1 0 21.50 2.90 5 1 0 15.60 2.20 5 1 0 11.40 2.50 5 1 0 17.80 2.40 -6 -1 0 87.59 8.10 -6 -1 0 89.79 8.00 -6 -1 0 91.39 8.10 -6 -1 0 86.29 7.40 6 1 0 80.79 7.50 6 1 0 77.29 7.30 -7 -1 0 7.20 2.30 -7 -1 0 6.70 2.30 -7 -1 0 6.30 2.20 -7 -1 0 5.00 1.40 7 1 0 2.70 1.70 7 1 0 4.10 1.30 -8 -1 0 47.20 5.40 -8 -1 0 47.50 5.50 -8 -1 0 42.00 4.20 -8 -1 0 43.40 5.40 8 1 0 33.00 4.20 -9 -1 0 -3.00 1.70 -9 -1 0 0.20 0.90 -9 -1 0 1.10 2.00 9 1 0 0.20 1.00 9 1 0 1.20 1.70 -10 -1 0 12.90 3.90 -10 -1 0 9.80 3.10 -11 -1 0 41.60 5.60 -11 -1 0 42.10 6.40 11 1 0 26.10 3.70 -12 2 0 85.59 10.10 -12 2 0 93.29 10.00 -11 2 0 9.50 3.30 -11 2 0 9.50 3.60 10 -2 0 1.60 0.80 10 -2 0 0.70 1.50 -10 2 0 1.70 2.30 -10 2 0 2.50 2.90 9 -2 0 27.60 4.50 9 -2 0 36.10 3.50 -9 2 0 35.90 3.40 -9 2 0 37.70 5.00 -9 2 0 42.20 5.40 8 -2 0 190.38 15.30 8 -2 0 172.18 16.30 -8 2 0 177.08 15.20 -8 2 0 188.68 16.20 -8 2 0 205.48 16.50 7 -2 0 133.49 11.10 -7 2 0 139.29 11.90 -7 2 0 133.79 11.10 -7 2 0 130.39 11.00 -7 2 0 129.49 11.70 6 -2 0 14.50 2.60 6 -2 0 16.00 1.80 -6 2 0 13.20 2.00 -6 2 0 16.50 1.80 -6 2 0 17.90 2.60 5 -2 0 51.49 4.40 5 -2 0 38.70 4.80 -5 2 0 50.69 4.40 -5 2 0 52.99 4.40 -5 2 0 50.29 4.80 -5 2 0 53.49 5.00 4 -2 0 114.39 9.50 4 -2 0 108.89 9.80 -4 2 0 117.79 9.90 -4 2 0 117.09 9.80 -4 2 0 118.69 9.50 3 -2 0 129.79 12.50 -3 2 0 152.48 12.50 -3 2 0 169.68 12.40 -3 2 0 156.28 12.40 -2 2 0 0.60 0.60 -2 2 0 0.40 0.50 1 -2 0 391.36 31.50 -1 2 0 401.46 31.60 0 2 0 4700.13 377.46 -1 -2 0 378.06 26.80 -1 -2 0 287.37 26.60 1 2 0 306.67 26.60 1 2 0 359.66 26.80 -2 -2 0 582.14 47.70 2 2 0 612.14 47.70 -3 -2 0 37.30 4.10 -3 -2 0 35.60 4.00 3 2 0 44.50 3.90 3 2 0 40.80 4.00 3 2 0 46.30 4.20 -4 -2 0 1.90 1.40 -4 -2 0 2.10 1.40 -4 -2 0 -1.10 1.60 4 2 0 1.50 1.40 4 2 0 0.30 0.80 4 2 0 -1.70 1.10 -5 -2 0 24.10 3.00 -5 -2 0 29.20 3.20 -5 -2 0 30.80 3.60 5 2 0 26.70 2.90 5 2 0 18.50 3.00 5 2 0 25.40 3.20 -6 -2 0 76.09 7.00 -6 -2 0 74.49 6.60 -6 -2 0 76.99 7.30 -6 -2 0 77.69 7.10 6 2 0 68.59 6.60 6 2 0 56.99 6.80 6 2 0 68.09 6.50 -7 -2 0 1.10 2.00 -7 -2 0 1.00 1.90 -7 -2 0 3.10 1.90 -7 -2 0 2.10 1.30 7 2 0 0.60 1.00 7 2 0 1.00 1.50 7 2 0 0.40 1.40 -8 -2 0 2.30 1.30 -8 -2 0 0.80 2.30 -8 -2 0 3.50 2.30 -8 -2 0 0.50 1.80 8 2 0 2.40 1.30 8 2 0 1.50 1.70 8 2 0 1.90 1.40 -9 -2 0 49.70 6.30 -9 -2 0 46.00 4.70 -9 -2 0 55.19 6.10 -9 -2 0 48.50 6.00 9 2 0 39.60 4.90 -10 -2 0 2.20 2.30 -10 -2 0 1.70 3.20 10 2 0 2.60 1.40 -11 -2 0 35.90 5.70 -11 -2 0 34.30 6.10 11 2 0 34.40 4.30 -12 3 0 64.19 8.20 -12 3 0 60.79 7.90 -11 3 0 46.10 6.70 -11 3 0 50.89 6.50 10 -3 0 2.10 1.80 -10 3 0 -3.00 2.40 -10 3 0 1.00 0.70 -10 3 0 0.90 0.80 -10 3 0 3.50 2.30 9 -3 0 14.50 3.20 -9 3 0 23.80 3.80 -9 3 0 16.90 3.40 -9 3 0 12.50 2.00 -8 3 0 157.88 13.90 -8 3 0 152.18 12.80 -8 3 0 157.98 13.80 -8 3 0 158.78 13.00 7 -3 0 1.80 1.30 -7 3 0 5.80 2.10 -7 3 0 4.50 1.60 -7 3 0 0.20 1.00 -7 3 0 2.50 0.80 6 -3 0 16.00 2.60 -6 3 0 24.70 2.90 -6 3 0 19.50 2.10 -6 3 0 20.30 3.00 5 -3 0 67.49 7.50 -5 3 0 98.09 7.60 -5 3 0 89.29 7.70 -5 3 0 83.89 7.20 -4 3 0 53.69 5.20 -4 3 0 58.19 5.00 -4 3 0 59.89 5.20 -3 3 0 40.10 4.10 -3 3 0 54.89 4.20 -3 3 0 43.60 4.10 -2 3 0 499.45 39.90 1 -3 0 809.22 71.19 -1 3 0 812.52 70.49 0 -3 0 607.94 49.90 0 3 0 647.14 50.09 -1 -3 0 13.30 2.00 -1 -3 0 12.20 2.00 -1 -3 0 13.80 1.60 1 3 0 15.60 2.20 1 3 0 11.60 1.70 1 3 0 11.70 1.50 -2 -3 0 104.89 9.40 -2 -3 0 109.19 9.40 2 3 0 105.19 9.40 2 3 0 113.69 9.50 2 3 0 108.79 9.20 -3 -3 0 76.99 7.40 -3 -3 0 70.09 7.30 -3 -3 0 97.99 7.40 3 3 0 80.09 7.30 3 3 0 83.89 7.60 3 3 0 73.99 7.30 3 3 0 83.49 7.10 -4 -3 0 115.49 9.80 -4 -3 0 108.29 10.00 -4 -3 0 117.09 9.90 4 3 0 99.99 9.80 4 3 0 125.29 9.70 4 3 0 103.79 9.80 -5 -3 0 93.69 7.50 -5 -3 0 81.29 7.50 -5 -3 0 76.09 7.10 5 3 0 76.69 6.90 5 3 0 66.99 7.20 5 3 0 68.19 7.10 -6 -3 0 6.10 2.50 -6 -3 0 11.20 2.60 -6 -3 0 9.90 2.10 -6 -3 0 7.40 2.40 6 3 0 4.80 2.10 6 3 0 8.20 1.80 6 3 0 8.40 2.20 -7 -3 0 -0.90 1.60 -7 -3 0 -0.90 2.00 -7 -3 0 0.70 1.20 -7 -3 0 2.00 2.00 7 3 0 -0.30 1.70 7 3 0 -0.80 1.30 7 3 0 -0.80 1.00 -8 -3 0 255.87 20.70 -8 -3 0 261.17 20.90 -8 -3 0 228.38 19.90 -8 -3 0 226.18 20.90 8 3 0 226.28 19.80 -9 -3 0 41.20 5.30 -9 -3 0 41.60 5.80 9 3 0 30.20 4.20 9 3 0 34.20 4.30 -10 -3 0 145.79 13.40 -10 -3 0 172.08 13.90 10 3 0 112.09 12.20 -11 -3 0 7.90 3.90 -11 -3 0 10.60 3.40 11 3 0 5.90 2.20 -12 4 0 -3.20 2.70 -12 4 0 0.20 2.30 -11 4 0 -0.50 1.90 -11 4 0 -0.80 2.40 10 -4 0 1.50 1.50 -10 4 0 -0.20 1.00 -10 4 0 2.70 2.80 -10 4 0 4.50 2.50 -10 4 0 1.90 0.90 9 -4 0 60.09 7.70 -9 4 0 79.79 6.60 -9 4 0 93.69 8.20 -9 4 0 75.89 6.90 -9 4 0 78.09 7.00 -9 4 0 79.09 8.00 8 -4 0 36.10 4.70 -8 4 0 44.40 3.90 -8 4 0 51.29 5.30 -8 4 0 44.40 4.90 -8 4 0 31.20 4.10 -7 4 0 49.90 4.50 -7 4 0 43.30 5.10 -7 4 0 49.80 5.30 -6 4 0 112.99 9.10 -6 4 0 103.89 9.50 -6 4 0 101.09 9.30 -5 4 0 18.40 2.60 -5 4 0 20.90 2.20 -5 4 0 18.10 2.40 -4 4 0 16.90 2.20 -4 4 0 18.70 2.10 -4 4 0 17.40 2.10 -4 4 0 15.30 2.10 -3 4 0 84.49 7.90 -3 4 0 93.99 8.00 -3 4 0 99.79 7.80 2 -4 0 594.54 47.90 -2 4 0 591.04 47.90 -2 4 0 613.74 48.10 1 -4 0 663.03 52.39 -1 4 0 655.13 52.59 -1 4 0 652.93 52.39 0 -4 0 716.23 55.99 0 -4 0 704.13 56.49 0 4 0 699.03 56.79 0 4 0 716.33 56.49 -1 -4 0 388.96 33.40 -1 -4 0 434.96 33.10 -1 -4 0 353.76 33.40 1 4 0 444.36 33.20 1 4 0 470.15 33.80 1 4 0 390.66 33.40 -2 -4 0 285.57 22.10 -2 -4 0 304.17 21.70 -2 -4 0 246.48 21.80 2 4 0 242.38 21.80 2 4 0 233.68 21.90 2 4 0 276.67 21.70 -3 -4 0 365.56 26.90 -3 -4 0 303.17 27.00 -3 -4 0 336.97 27.20 3 4 0 312.27 27.00 3 4 0 327.87 27.10 -4 -4 0 68.49 6.10 -4 -4 0 56.89 6.10 -4 -4 0 62.59 6.40 4 4 0 62.09 6.30 4 4 0 60.99 6.10 4 4 0 62.69 6.30 4 4 0 64.99 5.90 -5 -4 0 90.59 8.90 -5 -4 0 101.29 8.70 -5 -4 0 98.79 8.60 5 4 0 85.59 8.60 5 4 0 93.39 8.60 5 4 0 83.79 8.20 -6 -4 0 85.99 7.80 -6 -4 0 80.49 7.60 -6 -4 0 71.19 8.00 -6 -4 0 82.59 7.60 6 4 0 72.29 7.30 6 4 0 73.99 7.60 -7 -4 0 40.40 4.80 -7 -4 0 38.40 5.40 -7 -4 0 38.60 4.40 -7 -4 0 46.40 5.00 7 4 0 34.40 4.70 7 4 0 28.20 4.10 7 4 0 27.80 4.50 -8 -4 0 124.49 10.80 -8 -4 0 114.39 11.00 -8 -4 0 107.89 10.50 8 4 0 102.19 10.00 8 4 0 99.49 10.00 -9 -4 0 48.80 6.10 -9 -4 0 46.20 6.30 9 4 0 44.20 5.30 -10 -4 0 5.70 2.80 -10 -4 0 7.30 3.60 10 4 0 2.90 1.80 10 4 0 0.10 1.60 -12 5 0 1.00 3.10 -12 5 0 1.70 2.30 -11 5 0 2.50 2.90 -11 5 0 5.20 2.40 -11 5 0 4.30 1.30 -10 5 0 22.10 2.30 -10 5 0 22.90 4.20 -10 5 0 25.30 2.90 -10 5 0 18.10 2.90 -10 5 0 23.60 4.10 -9 5 0 14.50 3.20 -9 5 0 11.40 2.80 -9 5 0 13.30 2.40 -9 5 0 12.70 2.10 -9 5 0 14.70 1.80 -8 5 0 255.57 21.70 -8 5 0 257.37 21.20 -8 5 0 282.97 22.10 -8 5 0 243.68 21.40 -7 5 0 78.09 6.60 -7 5 0 68.99 7.00 -7 5 0 68.99 6.90 -6 5 0 40.20 4.20 -6 5 0 41.50 4.10 -6 5 0 40.80 4.30 -6 5 0 39.10 4.30 -5 5 0 2.90 1.10 -5 5 0 3.70 1.20 -5 5 0 3.10 0.90 -5 5 0 2.80 1.30 -4 5 0 13.00 1.70 -4 5 0 6.90 1.50 -4 5 0 6.00 1.90 -4 5 0 9.50 1.60 -3 5 0 111.09 9.80 -3 5 0 107.99 9.00 -3 5 0 109.49 9.50 2 -5 0 39.20 4.40 -2 5 0 41.50 3.60 -2 5 0 36.90 4.50 -2 5 0 47.50 4.20 1 -5 0 892.61 68.19 -1 5 0 770.72 67.49 -1 5 0 899.11 68.19 -1 5 0 864.21 68.49 0 -5 0 3.60 1.50 0 5 0 0.50 1.70 -1 -5 0 1068.89 83.19 1 5 0 1103.29 83.29 1 5 0 959.90 83.39 -2 -5 0 54.09 4.90 -2 -5 0 54.99 5.40 -2 -5 0 55.49 5.50 2 5 0 60.59 5.80 2 5 0 48.90 5.40 2 5 0 39.60 4.70 -3 -5 0 -1.40 1.20 -3 -5 0 0.50 1.00 -3 -5 0 0.50 1.40 3 5 0 0.60 1.00 3 5 0 0.60 1.30 3 5 0 4.10 2.00 -4 -5 0 2.50 1.90 -4 -5 0 0.20 1.50 -4 -5 0 2.00 1.60 4 5 0 1.50 1.80 4 5 0 -1.00 1.10 4 5 0 2.00 1.30 4 5 0 2.00 2.00 -5 -5 0 48.40 5.00 -5 -5 0 45.70 5.70 -5 -5 0 46.60 5.40 -5 -5 0 52.19 5.30 5 5 0 43.40 5.20 5 5 0 38.50 5.50 5 5 0 49.80 5.00 -6 -5 0 54.09 5.80 -6 -5 0 52.29 5.40 -6 -5 0 34.90 4.90 -6 -5 0 43.50 5.00 6 5 0 33.20 4.90 6 5 0 42.20 5.40 6 5 0 45.20 4.90 -7 -5 0 14.00 3.30 -7 -5 0 13.00 3.10 -7 -5 0 11.40 2.90 7 5 0 6.60 2.80 7 5 0 8.50 2.30 -8 -5 0 46.20 5.80 -8 -5 0 43.70 5.40 8 5 0 33.30 4.60 8 5 0 36.70 5.20 -9 -5 0 46.60 6.00 -9 -5 0 42.20 6.10 9 5 0 32.90 5.20 -10 -5 0 4.30 3.20 -10 -5 0 4.70 3.00 10 5 0 -1.60 1.70 10 5 0 0.60 1.80 -12 6 0 0.30 2.00 -11 6 0 3.80 1.60 -11 6 0 3.70 2.40 -11 6 0 5.70 1.60 -11 6 0 5.20 2.90 -10 6 0 44.90 5.00 -10 6 0 48.10 4.50 -10 6 0 50.29 5.20 -10 6 0 50.29 6.00 -10 6 0 57.79 6.10 -9 6 0 1.20 0.90 -9 6 0 1.90 1.10 -9 6 0 1.50 1.40 -9 6 0 -0.70 1.80 -8 6 0 0.30 1.20 -8 6 0 -0.20 0.70 -8 6 0 0.20 1.10 -8 6 0 0.90 0.80 -8 6 0 1.10 1.60 -7 6 0 40.60 4.50 -7 6 0 40.80 4.20 -7 6 0 40.60 4.50 -7 6 0 41.20 4.50 -7 6 0 36.00 4.40 -6 6 0 142.79 12.30 -6 6 0 154.48 12.40 -6 6 0 148.29 12.50 -6 6 0 137.39 12.60 -6 6 0 138.49 12.60 -5 6 0 0.30 0.80 -5 6 0 -0.40 1.10 -5 6 0 0.10 0.70 -5 6 0 0.10 0.70 -4 6 0 38.80 3.80 -4 6 0 42.20 4.00 -4 6 0 30.30 4.30 -4 6 0 44.40 4.20 3 -6 0 286.37 23.50 -3 6 0 274.57 23.50 -3 6 0 283.17 22.90 -3 6 0 301.97 23.90 2 -6 0 46.50 4.60 -2 6 0 46.60 4.60 -2 6 0 50.09 5.20 -2 6 0 41.40 3.90 1 -6 0 79.89 6.80 1 -6 0 85.59 7.70 -1 6 0 86.79 8.20 -1 6 0 86.29 7.10 -1 6 0 85.89 7.70 0 -6 0 85.99 7.00 0 -6 0 91.39 8.00 0 6 0 89.89 7.40 0 6 0 81.89 8.30 0 6 0 83.89 7.90 -1 -6 0 50.59 4.40 -1 -6 0 43.30 4.80 -1 -6 0 39.90 4.00 1 6 0 48.70 4.90 1 6 0 49.20 4.40 1 6 0 39.60 5.20 -2 -6 0 62.29 5.50 -2 -6 0 52.79 5.90 -2 -6 0 44.70 5.90 2 6 0 57.49 6.30 2 6 0 63.79 5.60 2 6 0 61.79 6.00 -3 -6 0 15.50 3.20 -3 -6 0 20.20 2.80 -3 -6 0 18.90 3.50 3 6 0 18.00 2.70 3 6 0 20.90 3.40 3 6 0 15.50 3.40 -4 -6 0 358.16 26.60 -4 -6 0 289.87 26.80 -4 -6 0 366.16 27.00 4 6 0 310.47 26.90 4 6 0 300.47 26.80 4 6 0 294.97 26.40 -5 -6 0 127.99 10.80 -5 -6 0 109.89 11.00 -5 -6 0 121.39 10.90 -5 -6 0 122.89 10.40 5 6 0 103.49 10.60 5 6 0 110.69 10.50 5 6 0 112.99 10.90 -6 -6 0 129.69 11.60 -6 -6 0 129.29 10.60 6 6 0 104.59 10.80 6 6 0 110.39 11.00 6 6 0 107.99 10.50 -7 -6 0 6.60 2.70 -7 -6 0 5.70 2.60 -7 -6 0 5.70 2.80 7 6 0 4.40 2.00 7 6 0 5.60 2.80 7 6 0 4.10 2.10 -8 -6 0 2.00 2.40 -8 -6 0 -2.10 2.30 8 6 0 -0.60 2.40 8 6 0 -2.60 1.20 -9 -6 0 38.70 5.50 -9 -6 0 35.50 5.30 9 6 0 27.50 4.80 9 6 0 23.20 4.30 -11 7 0 -1.70 1.60 -11 7 0 -1.70 2.00 -11 7 0 -0.70 1.20 -11 7 0 -2.30 1.30 -11 7 0 -0.60 1.40 -10 7 0 23.10 3.80 -10 7 0 27.00 3.40 -10 7 0 22.20 3.90 -10 7 0 26.40 4.10 -10 7 0 21.10 2.70 -9 7 0 4.70 1.80 -9 7 0 6.90 2.10 -9 7 0 7.20 2.20 -9 7 0 2.90 1.10 -9 7 0 2.80 1.50 -8 7 0 1.10 1.30 -8 7 0 1.30 1.00 -8 7 0 0.10 1.50 -8 7 0 2.80 1.50 -8 7 0 1.50 1.40 -7 7 0 95.59 8.30 -7 7 0 89.19 8.10 -7 7 0 85.39 8.30 -7 7 0 88.59 8.60 -7 7 0 89.89 8.50 -6 7 0 0.00 0.80 -6 7 0 0.00 1.30 -6 7 0 0.10 0.70 -6 7 0 -0.20 1.10 -6 7 0 1.40 1.10 -5 7 0 34.60 3.70 -5 7 0 34.00 4.10 -5 7 0 36.50 4.00 -5 7 0 40.90 4.00 -5 7 0 31.40 4.40 -4 7 0 88.69 7.80 -4 7 0 88.59 8.40 -4 7 0 86.49 8.80 -4 7 0 100.99 8.20 3 -7 0 5.10 1.70 -3 7 0 5.50 2.20 -3 7 0 8.20 1.80 -3 7 0 6.20 1.20 2 -7 0 91.79 8.50 -2 7 0 96.29 8.50 -2 7 0 85.59 7.60 -2 7 0 90.09 9.00 -2 7 0 101.39 7.80 1 -7 0 215.58 18.40 -1 7 0 223.78 19.00 -1 7 0 227.48 17.80 -1 7 0 207.98 18.40 0 -7 0 222.78 17.10 0 -7 0 208.38 18.20 0 7 0 221.78 18.80 0 7 0 212.48 17.70 0 7 0 211.48 18.20 -1 -7 0 18.20 2.00 -1 -7 0 13.20 2.80 1 7 0 11.90 2.70 1 7 0 15.10 3.40 1 7 0 13.80 2.10 -2 -7 0 3.00 1.30 -2 -7 0 6.10 2.10 2 7 0 3.70 1.40 2 7 0 0.50 1.60 2 7 0 2.80 2.20 -3 -7 0 44.70 5.70 -3 -7 0 58.39 5.30 3 7 0 46.60 5.20 3 7 0 42.10 5.70 3 7 0 48.60 6.20 -4 -7 0 19.60 3.20 -4 -7 0 19.70 2.80 -4 -7 0 19.30 3.90 4 7 0 19.30 3.70 4 7 0 18.60 3.80 4 7 0 15.50 3.00 -5 -7 0 1.00 1.60 -5 -7 0 3.60 2.30 -5 -7 0 5.70 2.20 5 7 0 0.30 1.50 5 7 0 4.00 1.90 5 7 0 0.90 2.50 -6 -7 0 22.90 4.60 -6 -7 0 26.30 3.80 -6 -7 0 28.80 4.20 6 7 0 23.80 4.60 6 7 0 24.10 3.90 6 7 0 19.80 4.00 -7 -7 0 30.50 4.30 -7 -7 0 32.30 4.60 7 7 0 21.60 4.00 7 7 0 20.00 4.30 -8 -7 0 53.69 6.40 -8 -7 0 55.99 6.70 8 7 0 44.20 6.70 -9 -7 0 13.60 4.00 -9 -7 0 26.90 4.80 9 7 0 14.50 3.70 -11 8 0 8.10 2.60 -11 8 0 7.10 2.50 -11 8 0 6.40 1.30 -11 8 0 3.40 2.30 -11 8 0 5.90 2.10 -11 8 0 7.10 2.40 -10 8 0 2.80 2.00 -10 8 0 1.90 1.40 -10 8 0 1.50 1.00 -10 8 0 0.60 1.60 -10 8 0 4.00 1.70 -9 8 0 1.80 1.30 -9 8 0 1.00 1.00 -9 8 0 0.00 1.70 -9 8 0 0.30 1.30 -9 8 0 -0.40 1.00 -8 8 0 -0.70 0.70 -8 8 0 1.10 1.50 -8 8 0 0.70 1.20 -8 8 0 0.20 1.20 -8 8 0 -1.00 0.90 -7 8 0 7.40 1.90 -7 8 0 8.90 2.10 -7 8 0 10.40 2.10 -7 8 0 11.00 2.40 -7 8 0 8.70 2.30 -6 8 0 4.10 1.50 -6 8 0 3.00 1.30 -6 8 0 2.10 1.20 -6 8 0 4.20 1.60 -6 8 0 3.40 1.80 -5 8 0 60.89 6.40 -5 8 0 62.79 5.80 -5 8 0 69.29 7.00 -4 8 0 83.49 7.20 -4 8 0 81.49 7.50 -4 8 0 88.99 7.90 -4 8 0 80.99 8.50 3 -8 0 4.60 1.90 -3 8 0 6.40 2.70 -3 8 0 3.90 1.70 2 -8 0 56.79 6.10 -2 8 0 63.59 5.30 -2 8 0 55.89 6.70 -2 8 0 57.99 6.00 1 -8 0 19.60 3.30 -1 8 0 13.70 3.70 -1 8 0 19.70 2.30 -1 8 0 18.10 3.10 0 -8 0 17.60 3.40 0 8 0 19.80 3.80 0 8 0 18.90 2.50 0 8 0 17.30 3.20 -1 -8 0 45.90 4.30 -1 -8 0 52.49 4.40 -1 -8 0 50.89 5.90 1 8 0 55.89 6.60 1 8 0 59.79 5.30 1 8 0 56.19 6.00 -2 -8 0 0.50 1.80 -2 -8 0 -0.80 1.10 -2 -8 0 -0.30 0.90 -2 -8 0 -1.70 1.00 2 8 0 -1.10 1.10 2 8 0 -0.50 2.00 2 8 0 -0.90 2.20 -3 -8 0 149.88 13.20 -3 -8 0 164.18 14.60 -3 -8 0 178.38 13.90 3 8 0 157.78 14.50 3 8 0 146.49 13.80 3 8 0 166.08 14.90 -4 -8 0 53.09 6.60 -4 -8 0 59.19 5.90 -4 -8 0 52.59 5.30 4 8 0 57.29 6.60 4 8 0 48.50 5.90 4 8 0 52.89 6.00 4 8 0 61.29 7.20 -5 -8 0 5.60 2.70 -5 -8 0 5.50 2.20 -5 -8 0 8.20 2.10 5 8 0 7.40 2.40 5 8 0 4.70 3.20 5 8 0 5.20 3.00 5 8 0 5.20 2.20 -6 -8 0 19.00 3.20 -6 -8 0 19.60 3.70 6 8 0 11.00 3.00 6 8 0 13.00 3.30 6 8 0 10.90 3.80 -7 -8 0 0.00 2.00 -7 -8 0 -0.40 2.00 7 8 0 -1.00 2.60 -8 -8 0 3.80 2.50 -8 -8 0 6.40 2.80 8 8 0 1.80 3.20 -10 9 0 6.10 2.30 -10 9 0 4.00 1.90 -10 9 0 7.30 1.70 -10 9 0 6.90 2.30 -10 9 0 8.50 2.40 -9 9 0 7.00 1.90 -9 9 0 5.50 1.80 -9 9 0 12.40 2.50 -9 9 0 9.50 2.40 -9 9 0 8.70 2.50 -8 9 0 40.60 4.90 -8 9 0 45.70 5.30 -8 9 0 35.60 4.40 -8 9 0 38.50 4.60 -8 9 0 41.20 4.50 -7 9 0 193.18 16.30 -7 9 0 176.88 15.70 -7 9 0 183.78 15.50 -7 9 0 187.98 16.60 -7 9 0 184.28 16.00 -6 9 0 10.50 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4 3.10 2.10 7 9 -4 0.00 3.30 -7 -9 4 3.10 1.90 -7 -9 4 5.50 2.40 6 9 -4 30.50 5.80 -6 -9 4 28.30 3.90 -6 -9 4 46.60 6.10 5 9 -4 12.80 3.10 5 9 -4 20.00 4.80 -5 -9 4 21.00 4.20 -5 -9 4 21.80 2.80 -5 -9 4 23.20 4.50 4 9 -4 0.30 1.50 4 9 -4 2.10 3.40 -4 -9 4 2.20 1.10 -4 -9 4 4.00 2.60 -4 -9 4 0.90 2.20 3 9 -4 3.00 1.70 3 9 -4 0.40 2.90 3 9 -4 6.20 2.40 -3 -9 4 5.70 2.80 -3 -9 4 5.20 0.90 -3 -9 4 3.70 2.30 2 9 -4 2.10 1.80 2 9 -4 6.50 3.20 2 9 -4 2.10 1.40 -2 -9 4 1.80 1.90 -2 -9 4 1.10 1.80 1 9 -4 5.30 2.90 1 9 -4 3.00 1.70 1 9 -4 5.30 1.70 -1 -9 4 5.50 2.00 -1 -9 4 3.50 2.40 0 9 -4 -0.20 2.70 0 9 -4 3.60 1.60 0 9 -4 0.10 1.00 0 -9 4 1.80 2.40 0 -9 4 -0.10 1.30 -1 9 -4 128.79 11.30 -1 9 -4 122.69 12.50 -1 9 -4 136.09 11.40 1 -9 4 135.89 12.60 1 -9 4 130.69 11.50 -2 9 -4 33.00 3.60 -2 9 -4 34.40 5.20 2 -9 4 29.60 3.60 -3 9 -4 7.50 1.20 -3 9 -4 9.40 2.90 -3 9 -4 6.80 2.10 -3 9 -4 8.30 1.20 -3 9 -4 8.90 1.80 -4 9 -4 110.39 9.30 -4 9 -4 118.49 9.80 -4 9 -4 112.19 10.80 -4 9 -4 104.09 10.50 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3.00 -11 -5 5 10.40 3.10 -11 -5 5 5.80 3.20 10 5 -5 46.30 6.50 10 5 -5 34.90 5.00 -10 -5 5 67.59 7.40 -10 -5 5 53.89 6.40 -10 -5 5 54.79 6.20 9 5 -5 110.69 10.90 9 5 -5 92.49 9.60 -9 -5 5 114.19 10.40 -9 -5 5 106.29 11.00 -9 -5 5 118.29 10.70 8 5 -5 56.19 6.40 8 5 -5 52.39 5.50 8 5 -5 54.09 6.80 -8 -5 5 54.99 6.20 -8 -5 5 46.10 6.70 -8 -5 5 60.99 6.80 -8 -5 5 53.59 6.10 7 5 -5 67.99 8.20 7 5 -5 84.29 9.00 -7 -5 5 97.09 8.50 -7 -5 5 89.69 9.10 -7 -5 5 89.69 8.10 -7 -5 5 82.09 8.70 6 5 -5 509.55 42.50 6 5 -5 501.95 42.80 -6 -5 5 517.95 42.80 -6 -5 5 509.05 43.00 -6 -5 5 551.74 42.50 -6 -5 5 533.25 42.00 5 5 -5 50.89 5.00 5 5 -5 44.20 5.70 -5 -5 5 39.60 5.70 -5 -5 5 50.89 5.40 -5 -5 5 40.70 4.70 -5 -5 5 37.70 4.50 3 5 -5 81.69 7.40 3 5 -5 96.99 8.80 3 5 -5 83.49 7.80 -3 -5 5 86.39 7.50 -3 -5 5 95.59 8.70 -3 -5 5 89.49 8.00 2 5 -5 8.80 1.60 -2 -5 5 7.80 2.30 -2 -5 5 7.50 1.50 -2 -5 5 10.80 1.80 1 5 -5 970.10 76.89 1 5 -5 992.30 76.89 1 5 -5 988.90 75.99 -1 -5 5 896.01 75.99 -1 -5 5 963.80 76.99 -1 -5 5 952.20 76.19 0 5 -5 185.08 14.80 0 5 -5 179.58 15.60 0 5 -5 175.88 15.50 0 -5 5 190.58 15.80 0 -5 5 180.38 14.80 -1 5 -5 42.20 4.60 -1 5 -5 41.70 3.60 -1 5 -5 45.90 4.90 -1 5 -5 41.60 4.20 1 -5 5 42.50 3.60 1 -5 5 47.70 5.00 -2 5 -5 20.00 1.90 -2 5 -5 21.70 3.00 -2 5 -5 30.00 3.30 2 -5 5 21.90 3.10 -3 5 -5 32.30 3.90 -3 5 -5 34.90 3.00 -3 5 -5 35.20 3.90 3 -5 5 31.20 3.80 -4 5 -5 109.79 12.20 -4 5 -5 131.79 12.00 -4 5 -5 142.49 11.20 -4 5 -5 147.49 11.60 4 -5 5 142.09 12.10 -5 5 -5 10.30 1.80 -5 5 -5 9.60 2.20 -5 5 -5 9.90 3.00 5 -5 5 11.00 2.20 -6 5 -5 64.49 5.30 -6 5 -5 52.59 6.80 -6 5 -5 53.69 6.20 6 -5 5 62.19 6.20 -7 5 -5 50.29 6.30 -7 5 -5 54.69 5.50 -7 5 -5 39.10 4.80 7 -5 5 49.70 5.30 -8 5 -5 74.89 7.70 -8 5 -5 71.59 7.30 -8 5 -5 82.69 8.90 8 -5 5 77.19 7.60 -9 5 -5 2.70 2.80 -9 5 -5 1.90 1.90 -9 5 -5 2.80 1.80 -9 5 -5 9.40 3.10 -10 5 -5 2.90 3.10 -10 5 -5 4.30 2.00 -10 5 -5 5.70 3.10 -10 5 -5 2.40 1.90 11 4 -5 -2.10 1.00 -11 -4 5 -0.70 2.40 -11 -4 5 -1.70 1.80 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30.80 5.80 -4 12 6 33.50 6.30 -3 12 6 -1.30 2.20 -3 12 6 0.60 2.30 2 -12 -6 8.20 1.80 -2 12 6 9.70 3.20 -2 12 6 10.30 3.90 2 13 -7 -1.30 3.50 2 13 -7 1.10 2.00 -2 -13 7 2.50 2.20 1 13 -7 0.30 1.60 1 13 -7 0.30 3.90 -1 -13 7 -0.90 1.60 0 13 -7 0.00 1.60 0 13 -7 -0.50 3.80 0 -13 7 1.70 1.60 -1 13 -7 72.89 8.20 -1 13 -7 70.39 9.20 1 -13 7 59.09 6.40 -2 13 -7 43.90 7.60 -2 13 -7 54.99 5.20 -2 13 -7 42.70 6.30 -3 13 -7 23.90 2.90 -3 13 -7 18.00 3.80 -3 13 -7 13.90 4.90 -4 13 -7 49.80 4.90 -4 13 -7 54.99 7.80 -4 13 -7 45.20 6.40 4 12 -7 0.80 3.50 3 12 -7 14.50 5.10 -3 -12 7 20.20 4.00 2 12 -7 1.10 3.60 -2 -12 7 2.00 2.10 1 12 -7 13.00 4.80 1 12 -7 8.60 2.80 1 12 -7 16.40 4.10 -1 -12 7 10.00 2.60 0 12 -7 5.40 1.70 0 12 -7 0.30 1.50 0 12 -7 1.60 3.60 0 -12 7 1.00 1.60 -1 12 -7 65.59 6.10 -1 12 -7 67.59 7.60 -1 12 -7 56.19 6.30 -1 12 -7 57.09 8.30 1 -12 7 58.09 6.00 -2 12 -7 8.00 3.90 -2 12 -7 8.70 2.30 -2 12 -7 13.60 2.20 -2 12 -7 12.10 3.20 -3 12 -7 0.00 3.10 -3 12 -7 0.10 0.90 -3 12 -7 -2.60 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1.20 0.60 -2 10 -7 2.90 3.00 2 -10 7 3.10 2.50 -3 10 -7 5.80 1.60 -3 10 -7 10.10 3.30 -3 10 -7 10.20 1.50 -3 10 -7 9.50 1.40 -4 10 -7 20.10 2.40 -4 10 -7 17.10 3.60 -4 10 -7 14.70 1.80 -4 10 -7 14.60 2.40 -4 10 -7 15.60 3.80 -5 10 -7 -0.80 0.40 -5 10 -7 -0.20 1.10 -5 10 -7 -1.00 2.00 -5 10 -7 0.30 1.30 -5 10 -7 0.10 1.40 -5 10 -7 0.00 1.30 -6 10 -7 36.40 3.60 -6 10 -7 42.30 5.50 -6 10 -7 42.60 5.50 -6 10 -7 32.70 5.20 -6 10 -7 45.30 4.40 -7 10 -7 35.00 4.00 -7 10 -7 28.80 3.10 -7 10 -7 30.60 4.60 -7 10 -7 33.20 4.80 -7 10 -7 27.60 5.20 -8 10 -7 0.30 1.70 -8 10 -7 -1.90 0.70 -8 10 -7 3.70 1.90 -8 10 -7 -3.40 1.40 -8 10 -7 1.20 1.70 8 9 -7 -0.30 3.40 -8 -9 7 2.00 2.10 7 9 -7 11.00 4.20 -7 -9 7 12.40 2.70 6 9 -7 0.90 3.40 -6 -9 7 1.30 1.70 -6 -9 7 -1.10 2.10 5 9 -7 6.60 3.70 5 9 -7 2.40 1.80 -5 -9 7 0.10 1.50 -5 -9 7 3.00 2.60 -5 -9 7 -0.90 1.70 4 9 -7 20.10 4.70 4 9 -7 21.90 3.40 -4 -9 7 21.20 2.90 -4 -9 7 25.10 4.90 -4 -9 7 22.50 3.80 3 9 -7 34.30 4.20 3 9 -7 24.90 5.30 -3 -9 7 30.70 4.40 -3 -9 7 33.60 5.50 2 9 -7 95.39 8.40 2 9 -7 92.19 9.80 2 9 -7 81.39 8.90 -2 -9 7 82.49 9.50 -2 -9 7 84.39 8.30 1 9 -7 4.00 3.10 1 9 -7 3.70 1.50 1 9 -7 1.00 1.60 -1 -9 7 1.80 1.40 -1 -9 7 0.70 2.50 0 9 -7 97.09 9.90 0 9 -7 85.19 8.50 0 9 -7 86.59 9.20 0 -9 7 97.49 9.90 0 -9 7 96.99 8.20 -1 9 -7 37.30 5.60 -1 9 -7 34.50 3.20 -1 9 -7 42.60 5.10 1 -9 7 36.30 5.50 1 -9 7 33.90 3.50 -2 9 -7 713.93 58.99 -2 9 -7 813.02 60.89 -2 9 -7 715.13 58.99 -2 9 -7 745.83 60.49 2 -9 7 738.53 60.59 -3 9 -7 91.89 8.20 -3 9 -7 69.39 6.00 -3 9 -7 64.59 6.50 -3 9 -7 71.29 7.80 3 -9 7 78.59 8.10 -4 9 -7 13.70 1.50 -4 9 -7 13.40 2.50 -4 9 -7 14.30 3.20 -4 9 -7 15.20 3.40 -5 9 -7 7.90 2.60 -5 9 -7 4.90 2.10 -5 9 -7 6.70 1.00 -5 9 -7 5.90 2.40 -6 9 -7 -0.30 1.50 -6 9 -7 -0.80 0.60 -6 9 -7 -0.70 1.70 -6 9 -7 2.10 1.50 -6 9 -7 -0.90 1.30 -7 9 -7 0.30 1.70 -7 9 -7 -0.30 1.50 -7 9 -7 1.60 1.70 -7 9 -7 1.50 1.50 -8 9 -7 -2.10 0.80 -8 9 -7 -0.50 1.50 -8 9 -7 0.90 2.00 -8 9 -7 2.40 1.80 -8 9 -7 0.70 1.20 9 8 -7 15.00 4.70 9 8 -7 10.40 3.60 -9 -8 7 18.90 3.60 8 8 -7 75.29 9.60 -8 -8 7 77.79 7.80 7 8 -7 114.79 12.40 -7 -8 7 120.09 11.90 -7 -8 7 123.19 10.90 6 8 -7 4.10 3.40 6 8 -7 4.30 2.00 -6 -8 7 4.70 2.50 -6 -8 7 4.30 3.30 -6 -8 7 7.40 2.10 5 8 -7 5.20 2.00 5 8 -7 8.10 3.60 -5 -8 7 9.40 2.80 -5 -8 7 4.60 1.80 -5 -8 7 3.90 3.30 4 8 -7 53.29 7.20 4 8 -7 60.79 6.00 -4 -8 7 60.39 7.50 -4 -8 7 47.30 5.30 -4 -8 7 61.39 6.40 3 8 -7 0.70 1.30 -3 -8 7 1.40 2.80 -3 -8 7 2.70 1.80 -3 -8 7 0.00 1.20 2 8 -7 404.96 34.20 2 8 -7 453.15 35.20 2 8 -7 456.55 36.20 2 8 -7 405.26 35.70 -2 -8 7 423.36 36.30 -2 -8 7 446.16 35.10 1 8 -7 8.00 2.00 1 8 -7 10.00 1.40 1 8 -7 9.70 3.60 1 8 -7 9.10 2.40 -1 -8 7 12.10 3.70 -1 -8 7 11.00 2.00 0 8 -7 44.90 6.20 0 8 -7 46.30 4.10 0 8 -7 46.20 5.50 0 -8 7 45.10 6.30 0 -8 7 47.20 4.50 -1 8 -7 0.10 1.00 -1 8 -7 -0.80 1.20 -1 8 -7 2.70 2.80 1 -8 7 -1.10 2.10 1 -8 7 1.40 0.80 -2 8 -7 13.60 3.00 -2 8 -7 14.10 2.30 -2 8 -7 21.50 3.70 2 -8 7 12.60 3.50 -3 8 -7 5.30 2.30 -3 8 -7 2.90 1.70 3 -8 7 2.30 2.00 -4 8 -7 133.79 12.20 -4 8 -7 128.89 10.60 -4 8 -7 143.69 12.70 -5 8 -7 12.60 2.60 -5 8 -7 8.40 1.10 -5 8 -7 7.60 2.40 -5 8 -7 5.90 2.70 -6 8 -7 31.80 3.20 -6 8 -7 30.80 3.20 -6 8 -7 38.30 4.40 -6 8 -7 36.60 5.40 -6 8 -7 37.50 4.80 -7 8 -7 27.90 3.10 -7 8 -7 24.50 4.90 -7 8 -7 23.60 4.30 -7 8 -7 26.00 2.90 -7 8 -7 29.70 3.50 -8 8 -7 1.40 1.00 -8 8 -7 8.40 2.30 -8 8 -7 2.40 2.60 -8 8 -7 4.30 1.30 -8 8 -7 -0.30 1.00 -8 8 -7 1.70 1.60 -9 8 -7 19.50 4.90 -9 8 -7 16.50 2.60 -9 8 -7 17.90 3.30 -9 8 -7 9.60 3.00 9 7 -7 54.89 6.70 9 7 -7 61.59 8.20 -9 -7 7 65.49 7.40 -9 -7 7 81.89 7.50 8 7 -7 12.30 4.10 -8 -7 7 11.20 2.80 -8 -7 7 7.00 3.70 7 7 -7 21.30 4.80 7 7 -7 23.60 4.50 -7 -7 7 22.40 5.00 -7 -7 7 23.20 4.30 -7 -7 7 24.30 3.70 6 7 -7 154.08 15.50 6 7 -7 165.68 14.70 -6 -7 7 175.98 14.20 -6 -7 7 165.68 15.00 -6 -7 7 155.38 15.70 5 7 -7 11.50 2.60 5 7 -7 14.50 3.80 -5 -7 7 10.90 3.70 -5 -7 7 12.50 2.50 -5 -7 7 20.30 3.60 4 7 -7 3.00 1.60 4 7 -7 7.40 3.00 -4 -7 7 8.20 2.40 -4 -7 7 6.60 1.80 -4 -7 7 8.90 3.30 3 7 -7 242.48 20.70 3 7 -7 243.28 19.90 3 7 -7 220.78 19.10 3 7 -7 245.18 20.40 -3 -7 7 237.38 19.90 -3 -7 7 228.68 19.40 -3 -7 7 247.48 21.00 2 7 -7 16.40 3.30 2 7 -7 24.20 2.50 2 7 -7 25.50 4.50 2 7 -7 22.00 3.10 -2 -7 7 27.60 4.70 -2 -7 7 23.20 3.00 -2 -7 7 26.00 3.20 1 7 -7 55.39 5.80 1 7 -7 66.49 7.10 1 7 -7 59.69 5.20 1 7 -7 60.99 6.40 -1 -7 7 55.79 5.50 -1 -7 7 62.69 7.10 0 7 -7 10.80 1.70 0 7 -7 11.20 2.70 0 7 -7 10.90 3.00 0 -7 7 11.40 3.30 0 -7 7 11.00 1.60 -1 7 -7 114.29 10.70 -1 7 -7 105.39 9.50 -1 7 -7 118.89 10.60 1 -7 7 113.29 10.80 -2 7 -7 198.88 16.60 -2 7 -7 191.28 16.80 -2 7 -7 177.98 15.80 2 -7 7 194.28 16.70 -3 7 -7 60.89 7.00 -3 7 -7 81.69 7.60 -3 7 -7 77.79 7.70 3 -7 7 80.99 7.70 -4 7 -7 -0.30 1.20 -4 7 -7 2.00 1.70 4 -7 7 -0.30 1.60 -5 7 -7 8.10 2.40 -5 7 -7 6.50 2.80 -5 7 -7 8.10 1.20 -5 7 -7 8.00 1.10 -6 7 -7 17.30 3.30 -6 7 -7 16.90 2.10 -6 7 -7 17.90 4.00 -6 7 -7 12.40 1.70 -6 7 -7 12.30 2.30 -7 7 -7 -0.40 0.80 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6.60 -3 -6 7 74.19 7.70 -3 -6 7 78.59 6.90 2 6 -7 188.78 16.50 2 6 -7 191.18 15.20 2 6 -7 187.98 15.80 2 6 -7 196.68 16.30 -2 -6 7 172.78 15.40 -2 -6 7 186.78 15.50 -2 -6 7 183.08 16.60 1 6 -7 3.60 1.60 1 6 -7 4.70 1.30 -1 -6 7 1.60 2.20 -1 -6 7 1.50 1.10 0 6 -7 62.79 6.00 0 6 -7 75.49 7.00 0 6 -7 74.59 7.30 0 -6 7 66.09 5.60 0 -6 7 61.19 7.10 -1 6 -7 43.30 4.50 -1 6 -7 47.60 5.40 -1 6 -7 44.50 5.00 1 -6 7 36.60 5.20 -2 6 -7 1.80 1.80 -2 6 -7 0.40 1.50 -2 6 -7 0.20 1.30 2 -6 7 -0.70 1.50 -3 6 -7 3.00 1.80 -3 6 -7 -0.80 1.10 3 -6 7 -1.50 1.40 -4 6 -7 0.70 0.40 -4 6 -7 0.60 1.50 -4 6 -7 1.20 2.10 -4 6 -7 2.00 1.50 -4 6 -7 0.00 0.30 4 -6 7 3.00 1.90 -5 6 -7 8.90 2.20 -5 6 -7 5.00 1.00 -5 6 -7 7.10 2.70 -5 6 -7 7.30 1.70 -5 6 -7 5.60 1.10 -6 6 -7 8.30 1.50 -6 6 -7 9.70 2.60 -6 6 -7 10.90 3.40 -6 6 -7 14.50 1.90 -6 6 -7 9.60 1.70 -7 6 -7 10.10 2.60 -7 6 -7 11.60 2.00 -7 6 -7 10.70 3.60 -8 6 -7 1.50 2.40 -8 6 -7 0.70 1.60 -9 6 -7 54.59 8.00 -9 6 -7 60.39 6.80 -9 6 -7 58.09 6.00 11 5 -7 -2.60 1.10 11 5 -7 1.10 1.20 11 5 -7 3.00 3.30 -11 -5 7 3.00 2.20 -11 -5 7 5.00 2.90 10 5 -7 20.00 4.30 10 5 -7 11.90 2.40 10 5 -7 14.90 2.60 -10 -5 7 10.30 4.00 -10 -5 7 18.10 3.80 -10 -5 7 24.10 4.10 9 5 -7 52.79 5.80 9 5 -7 51.59 5.70 9 5 -7 60.09 7.50 -9 -5 7 64.49 6.80 -9 -5 7 54.09 7.30 -9 -5 7 66.79 6.70 8 5 -7 72.39 8.20 8 5 -7 65.09 7.30 8 5 -7 67.39 6.70 -8 -5 7 68.39 8.20 -8 -5 7 67.39 7.20 -8 -5 7 67.89 7.10 -8 -5 7 70.09 7.70 7 5 -7 10.50 3.60 7 5 -7 12.10 2.70 -7 -5 7 10.20 2.70 -7 -5 7 11.50 3.50 -7 -5 7 8.80 2.70 -7 -5 7 10.80 2.50 6 5 -7 209.38 19.00 6 5 -7 195.48 17.90 6 5 -7 233.88 18.60 6 5 -7 216.28 18.40 -6 -5 7 211.88 18.60 -6 -5 7 217.08 19.20 -6 -5 7 227.78 18.20 5 5 -7 54.39 5.70 5 5 -7 56.29 6.70 5 5 -7 53.69 5.40 5 5 -7 60.19 5.80 -5 -5 7 53.39 5.90 -5 -5 7 56.89 6.90 -5 -5 7 55.99 5.70 4 5 -7 0.50 1.10 4 5 -7 0.20 1.00 4 5 -7 0.30 2.00 4 5 -7 0.80 1.20 -4 -5 7 1.10 1.40 -4 -5 7 2.20 2.20 -4 -5 7 1.60 1.60 3 5 -7 29.40 3.60 3 5 -7 25.90 3.20 3 5 -7 29.70 4.60 3 5 -7 28.30 3.40 -3 -5 7 31.80 4.40 -3 -5 7 31.00 3.60 -3 -5 7 35.70 3.70 2 5 -7 22.80 2.80 2 5 -7 23.90 3.80 2 5 -7 24.90 2.70 2 5 -7 19.30 3.00 -2 -5 7 22.10 2.60 -2 -5 7 20.40 3.00 -2 -5 7 21.40 3.80 1 5 -7 18.60 2.90 -1 -5 7 21.70 2.30 -1 -5 7 21.40 3.00 -1 -5 7 22.90 3.70 0 5 -7 197.38 17.30 0 5 -7 184.68 17.30 0 -5 7 222.08 16.10 0 -5 7 195.88 17.40 -1 5 -7 -1.20 0.90 -1 5 -7 0.30 1.70 -1 5 -7 2.40 1.70 1 -5 7 0.90 1.70 -2 5 -7 33.70 4.10 -2 5 -7 32.40 4.00 -2 5 -7 28.20 4.00 2 -5 7 29.90 4.20 2 -5 7 27.60 3.70 -3 5 -7 7.00 1.80 -3 5 -7 2.80 1.50 3 -5 7 4.00 1.70 3 -5 7 6.10 1.90 -4 5 -7 110.19 12.50 -4 5 -7 146.19 12.40 -4 5 -7 131.49 10.90 -4 5 -7 152.28 10.90 -4 5 -7 136.69 11.50 4 -5 7 134.09 12.20 4 -5 7 122.39 11.50 -5 5 -7 124.79 13.90 -5 5 -7 159.48 12.40 -5 5 -7 139.29 13.50 -5 5 -7 161.38 12.60 5 -5 7 158.18 13.60 -6 5 -7 55.49 6.00 -6 5 -7 55.39 6.80 -6 5 -7 47.90 4.80 6 -5 7 50.19 5.80 -7 5 -7 5.10 2.10 -7 5 -7 5.70 1.60 -7 5 -7 6.30 3.00 7 -5 7 7.30 2.20 -8 5 -7 154.08 15.00 -8 5 -7 148.19 13.00 8 -5 7 147.89 13.80 -9 5 -7 2.80 1.80 -9 5 -7 1.80 2.00 -9 5 -7 1.10 2.90 9 -5 7 1.10 1.70 -10 5 -7 13.00 4.50 11 4 -7 -0.30 0.80 -11 -4 7 -2.60 2.50 -11 -4 7 0.50 1.90 -11 -4 7 -2.80 2.20 10 4 -7 5.90 3.30 10 4 -7 8.40 1.60 10 4 -7 5.20 1.50 -10 -4 7 4.50 3.20 -10 -4 7 6.60 3.00 -10 -4 7 10.60 2.90 9 4 -7 3.60 2.80 9 4 -7 0.40 1.70 9 4 -7 1.60 1.00 9 4 -7 -0.80 1.00 -9 -4 7 2.00 2.40 -9 -4 7 -4.30 2.30 -9 -4 7 1.50 1.90 -9 -4 7 -3.10 2.00 8 4 -7 5.50 1.50 8 4 -7 0.60 2.80 8 4 -7 2.70 2.00 -8 -4 7 6.80 3.20 -8 -4 7 5.10 2.50 -8 -4 7 2.70 2.00 -8 -4 7 5.80 2.60 7 4 -7 0.30 1.40 7 4 -7 1.30 1.00 7 4 -7 1.90 2.50 -7 -4 7 4.00 2.10 -7 -4 7 0.50 2.00 -7 -4 7 1.80 1.50 -7 -4 7 3.50 2.70 6 4 -7 287.27 23.90 6 4 -7 302.67 24.40 6 4 -7 259.17 23.40 6 4 -7 267.17 23.60 -6 -4 7 298.87 24.10 -6 -4 7 284.97 23.60 -6 -4 7 312.07 24.70 5 4 -7 68.69 7.60 5 4 -7 81.39 6.90 5 4 -7 65.59 6.40 5 4 -7 71.99 6.70 -5 -4 7 54.59 6.70 -5 -4 7 73.49 6.80 -5 -4 7 73.79 7.80 4 4 -7 9.10 3.00 4 4 -7 13.40 2.20 4 4 -7 10.50 2.00 4 4 -7 10.30 2.10 -4 -4 7 11.80 2.30 3 4 -7 11.10 2.10 3 4 -7 12.90 3.10 3 4 -7 12.10 2.00 3 4 -7 15.50 2.20 -3 -4 7 13.20 3.00 2 4 -7 44.20 4.10 2 4 -7 37.40 4.30 2 4 -7 40.00 5.10 -2 -4 7 49.60 5.40 -2 -4 7 38.40 4.40 -2 -4 7 37.10 3.80 1 4 -7 -2.50 1.90 1 4 -7 0.70 1.20 1 4 -7 2.30 1.20 -1 -4 7 6.60 2.30 -1 -4 7 0.80 1.70 -1 -4 7 0.30 0.60 0 4 -7 50.99 5.20 0 4 -7 51.49 5.50 0 4 -7 68.79 6.00 0 -4 7 53.39 5.50 0 -4 7 46.40 5.60 -1 4 -7 60.39 6.20 -1 4 -7 64.29 6.40 -1 4 -7 66.09 6.50 1 -4 7 75.19 6.70 1 -4 7 65.09 6.50 -2 4 -7 27.40 4.10 -2 4 -7 37.10 4.20 -2 4 -7 41.60 4.20 2 -4 7 38.70 4.20 2 -4 7 31.50 4.00 -3 4 -7 3.50 1.40 -3 4 -7 -0.50 1.80 -3 4 -7 1.30 1.30 -3 4 -7 1.10 0.40 3 -4 7 1.20 1.10 3 -4 7 1.10 1.30 -4 4 -7 85.49 6.90 -4 4 -7 86.39 8.70 -4 4 -7 83.99 7.10 -4 4 -7 73.19 7.90 4 -4 7 83.29 8.00 4 -4 7 75.19 7.20 -5 4 -7 60.59 6.90 -5 4 -7 65.69 6.00 -5 4 -7 75.89 8.00 5 -4 7 71.19 7.00 -6 4 -7 120.89 11.90 -6 4 -7 108.49 11.00 6 -4 7 124.29 11.10 -7 4 -7 181.88 14.70 -7 4 -7 163.08 15.40 -7 4 -7 174.68 16.30 7 -4 7 165.68 15.30 -8 4 -7 77.09 7.60 -8 4 -7 72.69 8.70 -8 4 -7 63.39 6.80 8 -4 7 64.59 7.30 -9 4 -7 6.60 2.20 -9 4 -7 4.30 3.40 -9 4 -7 4.90 2.30 9 -4 7 6.30 2.20 -10 4 -7 5.50 2.40 -10 4 -7 7.40 2.60 -10 4 -7 9.40 3.80 10 -4 7 3.00 2.00 11 3 -7 17.90 2.00 11 3 -7 15.90 2.00 -11 -3 7 16.00 4.40 -11 -3 7 21.20 4.20 -11 -3 7 23.10 4.20 10 3 -7 43.70 4.60 10 3 -7 51.79 4.80 -10 -3 7 57.59 6.40 -10 -3 7 59.69 6.20 -10 -3 7 48.00 6.90 9 3 -7 33.20 3.50 9 3 -7 31.30 5.30 9 3 -7 34.20 4.70 9 3 -7 29.60 3.50 -9 -3 7 36.00 5.50 -9 -3 7 39.00 5.00 -9 -3 7 30.80 5.10 -9 -3 7 40.70 4.80 8 3 -7 0.30 0.80 8 3 -7 -1.30 1.40 8 3 -7 0.90 2.30 -8 -3 7 -0.80 2.00 -8 -3 7 0.70 1.50 -8 -3 7 1.00 2.70 7 3 -7 198.38 17.20 7 3 -7 180.18 16.80 7 3 -7 210.88 17.90 7 3 -7 209.48 17.50 -7 -3 7 214.88 17.40 -7 -3 7 203.18 18.10 -7 -3 7 208.58 17.40 6 3 -7 96.49 8.70 6 3 -7 85.69 8.30 6 3 -7 87.89 8.50 6 3 -7 97.99 9.40 -6 -3 7 96.79 8.70 -6 -3 7 91.19 8.70 -6 -3 7 104.19 9.70 5 3 -7 85.79 7.80 5 3 -7 84.29 8.60 5 3 -7 79.69 7.60 5 3 -7 80.09 7.70 -5 -3 7 91.49 7.90 -5 -3 7 84.69 8.70 4 3 -7 38.50 5.10 4 3 -7 40.90 4.00 4 3 -7 36.70 4.00 4 3 -7 31.50 3.90 -4 -3 7 43.70 4.40 -4 -3 7 44.00 5.20 3 3 -7 163.98 14.10 3 3 -7 151.38 14.20 3 3 -7 171.98 14.70 3 3 -7 171.98 14.00 -3 -3 7 182.88 14.20 2 3 -7 15.90 2.80 2 3 -7 9.30 2.00 2 3 -7 12.40 2.10 -2 -3 7 12.70 2.40 -2 -3 7 12.80 2.90 1 3 -7 201.38 16.30 1 3 -7 204.28 16.70 1 3 -7 193.78 16.60 -1 -3 7 196.18 16.70 -1 -3 7 220.68 16.80 -1 -3 7 167.58 16.30 0 3 -7 22.60 3.30 0 3 -7 27.30 3.40 0 3 -7 21.90 3.00 0 -3 7 21.40 2.00 0 -3 7 25.30 3.60 0 -3 7 24.00 2.90 -1 3 -7 5.10 1.60 -1 3 -7 7.60 2.10 -1 3 -7 5.80 1.80 1 -3 7 7.90 2.10 1 -3 7 8.40 1.80 -2 3 -7 19.20 1.80 -2 3 -7 22.20 3.40 -2 3 -7 20.00 2.90 2 -3 7 19.00 2.80 2 -3 7 20.00 2.90 -3 3 -7 141.59 13.60 -3 3 -7 152.58 12.50 -3 3 -7 153.18 13.30 -3 3 -7 151.88 12.20 3 -3 7 152.38 12.60 3 -3 7 144.79 13.20 -4 3 -7 4.20 1.20 -4 3 -7 5.90 1.90 -4 3 -7 2.30 1.90 4 -3 7 3.10 1.10 4 -3 7 4.40 1.60 -5 3 -7 373.86 30.90 -5 3 -7 356.46 31.60 -5 3 -7 424.26 32.50 5 -3 7 376.66 31.70 -6 3 -7 335.47 26.50 -6 3 -7 329.57 27.90 6 -3 7 302.67 27.10 -7 3 -7 109.99 9.90 -7 3 -7 111.49 11.40 -7 3 -7 107.19 10.40 7 -3 7 105.09 10.40 -8 3 -7 61.79 6.80 -8 3 -7 69.29 7.30 -8 3 -7 69.59 8.40 8 -3 7 62.09 7.10 -9 3 -7 3.40 2.20 -9 3 -7 2.70 2.80 -9 3 -7 3.10 2.10 9 -3 7 2.80 1.90 -10 3 -7 18.70 5.10 -10 3 -7 11.10 3.10 -10 3 -7 11.90 3.30 10 -3 7 13.80 2.90 -12 -2 7 53.69 6.20 -12 -2 7 33.30 6.10 -12 -2 7 44.70 6.40 -11 -2 7 10.70 2.90 -11 -2 7 8.80 3.30 -11 -2 7 6.60 3.30 10 2 -7 16.60 3.30 10 2 -7 13.90 1.40 10 2 -7 12.20 1.30 -10 -2 7 14.20 3.70 -10 -2 7 20.00 3.50 -10 -2 7 22.90 4.00 9 2 -7 43.40 4.10 9 2 -7 44.40 5.40 9 2 -7 44.10 4.00 -9 -2 7 49.70 5.80 -9 -2 7 43.10 5.20 -9 -2 7 46.30 6.20 8 2 -7 18.30 2.30 8 2 -7 19.90 3.40 8 2 -7 24.30 3.50 8 2 -7 22.30 4.10 -8 -2 7 22.70 3.80 -8 -2 7 21.80 4.20 -8 -2 7 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4.50 4 7 -9 14.60 2.40 4 7 -9 14.30 3.90 4 7 -9 13.70 2.70 4 7 -9 13.70 3.00 -4 -7 9 14.80 2.80 -4 -7 9 11.50 3.90 -4 -7 9 17.20 2.90 3 7 -9 175.48 15.40 3 7 -9 174.28 13.80 3 7 -9 174.28 14.50 3 7 -9 137.59 14.60 -3 -7 9 169.68 14.20 -3 -7 9 155.48 14.10 -3 -7 9 173.18 15.60 2 7 -9 12.10 3.30 2 7 -9 7.40 1.70 2 7 -9 6.70 2.00 2 7 -9 8.00 2.30 -2 -7 9 5.40 3.20 -2 -7 9 9.30 1.80 1 7 -9 115.79 10.70 1 7 -9 101.29 9.10 1 7 -9 99.69 10.10 -1 -7 9 106.69 8.80 -1 -7 9 109.19 10.90 0 7 -9 17.10 2.60 0 7 -9 12.70 3.00 0 -7 9 21.60 4.20 -1 7 -9 0.80 1.70 -1 7 -9 1.20 1.60 -1 7 -9 -0.50 2.10 1 -7 9 0.60 2.20 -2 7 -9 2.30 1.70 -2 7 -9 0.30 1.90 -2 7 -9 -1.20 1.80 2 -7 9 1.40 2.20 -3 7 -9 12.40 2.70 -3 7 -9 8.40 2.40 -3 7 -9 7.20 2.40 3 -7 9 5.80 2.60 -4 7 -9 7.70 2.60 -4 7 -9 8.90 2.90 -4 7 -9 5.60 2.70 -4 7 -9 13.10 2.50 4 -7 9 10.30 2.70 -5 7 -9 66.19 7.00 -5 7 -9 59.19 6.10 -5 7 -9 53.49 7.40 -6 7 -9 40.40 5.70 -6 7 -9 37.90 6.40 -6 7 -9 53.29 4.70 -7 7 -9 8.80 3.60 -7 7 -9 10.50 1.40 -7 7 -9 11.20 3.00 -7 7 -9 10.50 1.30 -8 7 -9 -0.40 1.70 -8 7 -9 -2.90 2.30 -8 7 -9 1.30 1.00 -8 7 -9 1.70 0.90 10 6 -9 17.60 3.10 10 6 -9 22.60 5.10 10 6 -9 19.40 3.30 -10 -6 9 27.50 4.60 9 6 -9 5.10 3.70 9 6 -9 2.00 1.40 -9 -6 9 2.60 2.60 8 6 -9 37.30 6.20 8 6 -9 35.40 4.60 -8 -6 9 44.50 5.40 -8 -6 9 40.50 5.60 -8 -6 9 31.50 6.20 7 6 -9 54.79 7.10 7 6 -9 37.30 5.30 7 6 -9 47.00 5.30 -7 -6 9 47.00 5.50 -7 -6 9 48.50 5.90 -7 -6 9 46.50 6.90 6 6 -9 -0.40 1.40 6 6 -9 -2.50 2.70 6 6 -9 0.20 1.20 6 6 -9 -0.80 1.50 -6 -6 9 0.20 2.10 -6 -6 9 0.10 1.90 -6 -6 9 2.40 2.80 5 6 -9 36.20 5.60 5 6 -9 39.30 4.20 5 6 -9 39.00 4.50 5 6 -9 31.30 4.40 -5 -6 9 37.30 4.80 -5 -6 9 42.00 6.10 -5 -6 9 36.20 4.70 4 6 -9 143.69 14.10 4 6 -9 149.59 13.50 4 6 -9 151.98 12.70 4 6 -9 147.49 13.20 -4 -6 9 153.88 14.30 -4 -6 9 147.89 13.10 -4 -6 9 154.68 13.10 3 6 -9 21.60 4.30 3 6 -9 22.60 3.00 3 6 -9 24.80 3.40 3 6 -9 21.80 3.60 -3 -6 9 21.90 3.10 -3 -6 9 24.80 4.60 -3 -6 9 22.90 3.50 2 6 -9 52.49 6.60 2 6 -9 62.09 6.10 2 6 -9 50.79 5.10 -2 -6 9 48.80 5.50 -2 -6 9 48.90 4.90 -2 -6 9 50.29 6.60 1 6 -9 163.08 13.60 1 6 -9 154.98 14.50 1 6 -9 171.98 14.60 -1 -6 9 157.78 14.70 -1 -6 9 158.28 13.10 0 6 -9 8.90 2.20 0 6 -9 7.70 2.80 0 6 -9 7.50 2.20 0 -6 9 11.50 3.20 -1 6 -9 124.59 11.60 -1 6 -9 137.59 11.90 -1 6 -9 118.39 11.10 1 -6 9 120.79 11.70 -2 6 -9 34.50 4.40 -2 6 -9 18.50 3.50 -2 6 -9 21.20 3.70 2 -6 9 21.50 3.90 -3 6 -9 29.60 4.30 -3 6 -9 38.90 4.30 -3 6 -9 23.70 4.20 3 -6 9 27.00 4.20 3 -6 9 28.90 4.10 -4 6 -9 3.30 2.30 -4 6 -9 7.90 2.00 -4 6 -9 5.40 2.60 -4 6 -9 3.50 1.90 4 -6 9 4.90 1.80 4 -6 9 5.50 2.00 -5 6 -9 46.70 7.30 -5 6 -9 67.19 7.20 5 -6 9 75.39 7.20 -6 6 -9 1.70 0.70 -6 6 -9 0.80 0.60 -6 6 -9 2.30 2.50 -6 6 -9 2.30 1.70 6 -6 9 0.40 1.30 -7 6 -9 8.50 1.60 -7 6 -9 11.10 3.80 -7 6 -9 7.30 2.70 7 -6 9 9.30 2.70 -8 6 -9 0.20 2.20 -8 6 -9 0.60 1.90 -8 6 -9 1.90 1.20 10 5 -9 48.00 7.20 10 5 -9 50.69 5.10 10 5 -9 37.70 4.70 -10 -5 9 56.19 6.40 9 5 -9 2.20 1.40 9 5 -9 0.40 2.90 -9 -5 9 -1.30 3.10 -9 -5 9 -0.80 2.40 8 5 -9 -0.60 1.00 8 5 -9 -1.70 1.40 8 5 -9 -1.30 3.00 -8 -5 9 5.30 2.70 -8 -5 9 0.30 3.00 -8 -5 9 -1.90 1.80 7 5 -9 -1.20 1.40 7 5 -9 0.80 1.20 7 5 -9 0.10 1.60 7 5 -9 -1.40 2.90 -7 -5 9 1.30 2.30 -7 -5 9 0.90 2.10 -7 -5 9 3.90 3.00 6 5 -9 15.50 2.90 6 5 -9 17.50 3.10 6 5 -9 13.20 3.90 6 5 -9 13.80 2.70 -6 -5 9 17.40 3.40 -6 -5 9 21.00 3.40 -6 -5 9 20.80 4.40 5 5 -9 36.80 4.50 5 5 -9 35.00 4.60 5 5 -9 44.50 4.70 5 5 -9 42.90 6.00 -5 -5 9 37.30 4.80 -5 -5 9 39.60 5.00 -5 -5 9 48.10 6.20 4 5 -9 -0.60 1.00 4 5 -9 2.10 1.50 4 5 -9 -0.10 1.40 4 5 -9 0.40 2.50 -4 -5 9 -1.30 2.50 -4 -5 9 4.20 2.10 -4 -5 9 -0.30 1.40 3 5 -9 7.10 1.90 3 5 -9 13.00 3.70 3 5 -9 6.20 1.90 3 5 -9 7.80 2.00 -3 -5 9 23.70 4.80 -3 -5 9 10.40 2.60 -3 -5 9 6.40 1.80 2 5 -9 109.39 10.50 2 5 -9 113.69 9.80 2 5 -9 122.69 11.00 -2 -5 9 119.19 11.10 -2 -5 9 112.69 9.60 -2 -5 9 108.09 10.20 1 5 -9 26.10 3.50 1 5 -9 29.90 4.30 1 5 -9 18.60 3.40 -1 -5 9 25.90 2.40 -1 -5 9 24.90 2.40 -1 -5 9 27.50 4.40 0 5 -9 6.50 2.50 0 5 -9 3.50 1.80 0 5 -9 4.30 1.70 0 -5 9 1.50 1.30 0 -5 9 0.50 2.10 -1 5 -9 54.79 5.80 -1 5 -9 48.80 5.80 -1 5 -9 57.19 6.00 1 -5 9 47.90 5.70 1 -5 9 60.29 6.50 -2 5 -9 3.90 1.70 -2 5 -9 4.20 2.30 -2 5 -9 4.90 2.10 2 -5 9 2.50 1.50 2 -5 9 1.90 2.20 -3 5 -9 1.00 2.20 -3 5 -9 1.10 1.60 -3 5 -9 -0.40 1.30 3 -5 9 -2.00 1.70 3 -5 9 -1.10 0.80 -4 5 -9 19.20 3.70 -4 5 -9 27.90 3.30 -4 5 -9 18.90 4.20 4 -5 9 23.80 3.50 4 -5 9 22.70 3.90 -5 5 -9 6.00 3.00 -5 5 -9 9.00 2.70 -5 5 -9 12.20 1.40 5 -5 9 10.20 2.50 -6 5 -9 71.59 8.50 -6 5 -9 68.19 6.10 -6 5 -9 65.79 7.50 6 -5 9 68.99 7.50 -7 5 -9 0.40 1.70 -7 5 -9 3.10 2.50 -7 5 -9 0.10 1.00 7 -5 9 1.10 1.60 -8 5 -9 113.99 12.70 -8 5 -9 127.29 10.60 -8 5 -9 109.09 11.70 11 4 -9 -0.70 0.80 -11 -4 9 1.90 2.70 -11 -4 9 1.30 1.70 10 4 -9 16.30 2.60 10 4 -9 22.80 2.80 10 4 -9 27.60 5.00 -10 -4 9 34.30 8.80 -10 -4 9 22.90 4.30 9 4 -9 9.30 3.70 9 4 -9 7.50 1.80 -9 -4 9 8.50 3.10 -9 -4 9 9.80 3.30 -9 -4 9 8.30 3.80 8 4 -9 4.00 1.90 8 4 -9 6.10 2.20 8 4 -9 5.40 1.50 8 4 -9 4.10 3.30 -8 -4 9 4.30 2.70 -8 -4 9 4.30 2.50 -8 -4 9 7.40 3.20 7 4 -9 63.69 7.60 7 4 -9 62.89 6.50 7 4 -9 61.09 6.20 7 4 -9 58.79 6.30 -7 -4 9 64.79 6.70 -7 -4 9 67.59 7.90 6 4 -9 50.49 5.70 6 4 -9 55.09 5.70 6 4 -9 58.99 5.90 6 4 -9 57.09 7.10 -6 -4 9 57.49 7.10 -6 -4 9 57.09 6.30 5 4 -9 33.10 4.00 5 4 -9 34.60 4.10 5 4 -9 28.40 3.90 5 4 -9 38.10 5.50 -5 -4 9 31.90 4.40 -5 -4 9 42.80 5.80 4 4 -9 225.18 18.70 4 4 -9 191.18 18.00 4 4 -9 225.08 18.00 4 4 -9 212.88 17.70 -4 -4 9 211.28 18.00 -4 -4 9 215.98 18.90 3 4 -9 68.39 6.20 3 4 -9 60.79 7.20 3 4 -9 63.49 6.20 3 4 -9 71.59 6.70 -3 -4 9 60.49 6.70 -3 -4 9 64.39 7.20 2 4 -9 42.70 4.40 2 4 -9 34.50 5.20 2 4 -9 37.90 4.50 -2 -4 9 41.30 5.50 -2 -4 9 34.80 4.60 1 4 -9 11.20 2.40 1 4 -9 9.20 2.20 -1 -4 9 9.50 2.20 -1 -4 9 12.30 3.10 -1 -4 9 9.00 1.30 0 4 -9 23.30 3.50 0 4 -9 16.90 3.40 0 4 -9 26.70 3.40 0 -4 9 18.50 3.20 0 -4 9 20.30 3.60 -1 4 -9 71.89 6.70 -1 4 -9 63.69 6.80 -1 4 -9 52.79 6.60 1 -4 9 67.29 6.90 1 -4 9 75.39 7.00 -2 4 -9 58.89 6.80 -2 4 -9 68.09 6.60 -2 4 -9 63.99 7.00 2 -4 9 63.09 6.70 2 -4 9 75.19 7.00 -3 4 -9 -0.60 2.30 -3 4 -9 0.10 1.70 3 -4 9 2.40 1.80 3 -4 9 0.90 1.20 -4 4 -9 0.00 1.20 -4 4 -9 -0.80 1.70 -4 4 -9 0.90 0.70 4 -4 9 1.70 1.40 4 -4 9 -0.30 1.20 -5 4 -9 29.40 4.40 -5 4 -9 29.60 5.20 -5 4 -9 28.30 3.10 5 -4 9 34.30 4.40 -6 4 -9 0.30 1.20 -6 4 -9 5.10 2.50 -6 4 -9 0.10 1.60 6 -4 9 2.60 1.70 -7 4 -9 218.08 18.70 -7 4 -9 184.38 16.20 7 -4 9 180.48 17.30 -8 4 -9 41.00 4.80 -8 4 -9 40.90 5.80 -8 4 -9 42.60 6.80 -9 4 -9 58.99 7.60 -9 4 -9 64.29 6.70 -9 4 -9 67.69 9.00 -11 -3 9 0.30 2.70 -11 -3 9 0.30 1.80 10 3 -9 6.80 1.30 10 3 -9 6.50 1.30 -10 -3 9 7.10 2.40 -10 -3 9 10.50 3.80 -10 -3 9 10.60 3.50 9 3 -9 3.70 2.20 9 3 -9 0.80 1.80 9 3 -9 0.20 0.80 -9 -3 9 4.70 2.60 -9 -3 9 0.20 3.00 8 3 -9 341.27 28.80 8 3 -9 317.87 28.40 8 3 -9 355.06 29.70 8 3 -9 368.26 29.20 -8 -3 9 377.66 29.10 -8 -3 9 334.87 29.80 7 3 -9 61.99 6.80 7 3 -9 49.40 5.40 7 3 -9 47.60 5.40 7 3 -9 46.30 5.00 -7 -3 9 52.99 6.80 -7 -3 9 48.70 5.90 6 3 -9 7.80 3.20 6 3 -9 15.90 2.60 6 3 -9 8.80 1.90 6 3 -9 9.20 2.50 -6 -3 9 8.50 3.10 -6 -3 9 10.10 2.90 5 3 -9 5.60 1.50 5 3 -9 6.80 3.00 5 3 -9 3.80 1.60 5 3 -9 5.50 2.10 -5 -3 9 3.60 2.90 -5 -3 9 3.20 2.20 4 3 -9 15.00 2.60 4 3 -9 21.20 3.80 4 3 -9 13.80 2.50 -4 -3 9 17.00 3.70 -4 -3 9 20.00 3.20 3 3 -9 32.60 4.20 3 3 -9 31.10 5.00 3 3 -9 49.60 4.60 -3 -3 9 34.80 4.70 -3 -3 9 37.80 4.20 -3 -3 9 39.40 5.40 2 3 -9 2.20 1.30 2 3 -9 3.70 1.80 2 3 -9 6.40 2.40 -2 -3 9 1.40 1.10 -2 -3 9 3.70 2.30 -2 -3 9 2.90 0.90 -2 -3 9 2.20 2.10 1 3 -9 99.69 8.90 1 3 -9 109.59 9.30 1 3 -9 86.19 9.10 -1 -3 9 90.59 9.10 -1 -3 9 105.39 8.30 -1 -3 9 109.09 9.60 -1 -3 9 90.29 9.20 0 3 -9 33.40 4.50 0 3 -9 35.20 4.40 0 3 -9 39.70 4.70 0 -3 9 40.50 4.50 0 -3 9 36.20 3.30 0 -3 9 41.80 4.90 -1 3 -9 77.19 7.10 -1 3 -9 73.39 7.40 -1 3 -9 68.19 7.40 1 -3 9 65.89 7.20 1 -3 9 79.19 7.30 -2 3 -9 17.10 1.80 -2 3 -9 23.00 3.80 -2 3 -9 19.00 3.30 2 -3 9 25.50 3.50 2 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106.39 9.90 -2 9 -10 104.99 11.20 2 -9 10 119.89 11.50 -3 9 -10 23.70 4.10 -3 9 -10 13.50 3.50 -3 9 -10 17.10 3.20 3 -9 10 15.80 3.90 -4 9 -10 11.90 3.00 -4 9 -10 7.10 2.50 -4 9 -10 11.30 3.10 4 -9 10 16.90 3.50 -5 9 -10 14.00 4.10 -5 9 -10 19.70 4.00 -5 9 -10 19.10 3.40 -5 9 -10 21.60 3.60 -6 9 -10 89.19 7.90 -6 9 -10 69.19 9.10 -6 9 -10 79.09 8.10 -6 9 -10 69.89 8.50 -7 9 -10 0.40 1.60 -7 9 -10 2.80 2.70 -7 9 -10 1.90 1.40 8 8 -10 103.99 9.90 8 8 -10 105.69 11.30 -8 -8 10 87.89 9.50 7 8 -10 4.10 2.10 7 8 -10 4.80 3.50 -7 -8 10 9.70 2.80 -7 -8 10 6.40 2.80 6 8 -10 18.00 3.60 6 8 -10 19.00 4.80 -6 -8 10 22.00 3.70 -6 -8 10 19.20 3.80 5 8 -10 6.50 1.80 5 8 -10 9.90 3.80 5 8 -10 7.10 2.30 5 8 -10 5.50 3.60 -5 -8 10 6.60 2.50 -5 -8 10 6.10 2.50 -5 -8 10 5.40 3.30 4 8 -10 41.90 4.60 4 8 -10 45.90 5.20 4 8 -10 50.59 5.80 4 8 -10 42.90 6.60 -4 -8 10 42.40 5.10 -4 -8 10 52.49 7.20 -4 -8 10 43.80 5.20 3 8 -10 -0.40 1.20 3 8 -10 1.20 1.30 3 8 -10 -0.30 3.00 3 8 -10 -0.10 1.20 -3 -8 10 0.20 1.30 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1.50 -8 5 -10 -3.00 1.70 -8 5 -10 -0.30 1.30 -8 5 -10 -2.70 2.80 11 4 -10 10.60 1.70 11 4 -10 7.30 1.50 -11 -4 10 14.50 3.90 -10 -4 10 -3.30 2.40 9 4 -10 13.30 4.10 9 4 -10 11.40 2.20 9 4 -10 19.40 3.20 -9 -4 10 13.60 4.20 -9 -4 10 19.40 3.90 -9 -4 10 15.20 4.50 8 4 -10 7.20 2.50 8 4 -10 12.30 3.80 8 4 -10 7.30 2.30 8 4 -10 5.00 1.60 -8 -4 10 6.10 3.60 -8 -4 10 8.40 3.10 7 4 -10 3.20 1.40 7 4 -10 5.10 2.00 7 4 -10 7.80 2.40 7 4 -10 7.90 3.50 -7 -4 10 6.60 3.30 -7 -4 10 3.50 2.60 6 4 -10 85.99 7.90 6 4 -10 86.99 9.10 6 4 -10 80.39 7.90 6 4 -10 73.79 7.80 -6 -4 10 84.29 8.30 -6 -4 10 90.29 9.40 5 4 -10 38.00 4.50 5 4 -10 42.70 6.00 5 4 -10 38.00 4.50 5 4 -10 40.40 4.50 -5 -4 10 41.00 6.10 -5 -4 10 36.50 5.20 4 4 -10 -1.90 1.50 4 4 -10 -0.80 1.10 4 4 -10 0.50 1.20 4 4 -10 -0.70 2.20 -4 -4 10 1.00 2.10 -4 -4 10 1.40 2.60 3 4 -10 -2.40 2.30 3 4 -10 0.80 1.70 3 4 -10 2.10 1.40 3 4 -10 0.40 1.20 -3 -4 10 -0.20 2.20 -3 -4 10 -0.30 2.10 2 4 -10 0.20 1.10 2 4 -10 -2.00 1.50 2 4 -10 0.30 2.20 -2 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4.60 -11 -3 10 49.99 6.70 10 3 -10 8.70 1.50 -10 -3 10 17.20 3.90 9 3 -10 19.40 3.50 9 3 -10 13.40 3.10 9 3 -10 18.20 2.40 -9 -3 10 11.10 4.30 -9 -3 10 18.60 3.90 8 3 -10 17.40 4.20 8 3 -10 12.50 2.20 8 3 -10 14.20 3.00 8 3 -10 18.20 3.20 -8 -3 10 15.70 3.70 -8 -3 10 11.50 4.00 7 3 -10 109.19 10.90 7 3 -10 88.69 9.40 7 3 -10 99.59 9.80 7 3 -10 123.19 10.00 -7 -3 10 112.99 10.30 -7 -3 10 107.79 11.10 6 3 -10 24.30 3.60 6 3 -10 20.70 4.40 6 3 -10 20.40 3.20 -6 -3 10 23.50 4.00 -6 -3 10 24.20 4.50 5 3 -10 -0.50 1.20 5 3 -10 0.30 2.60 5 3 -10 9.50 2.10 5 3 -10 -0.40 0.90 -5 -3 10 -0.50 2.10 -5 -3 10 2.90 2.80 4 3 -10 3.20 1.90 4 3 -10 0.50 1.10 4 3 -10 0.40 2.20 4 3 -10 -1.00 1.10 -4 -3 10 -0.40 2.00 -4 -3 10 1.50 2.40 3 3 -10 -1.30 1.60 3 3 -10 0.00 1.00 3 3 -10 -1.40 1.50 -3 -3 10 -1.50 2.00 -3 -3 10 1.00 1.10 -3 -3 10 -0.90 2.30 -3 -3 10 -0.50 0.90 2 3 -10 174.28 14.30 2 3 -10 160.08 13.80 2 3 -10 168.08 14.40 -2 -3 10 155.58 14.10 -2 -3 10 147.99 13.30 -2 -3 10 165.28 14.20 -2 -3 10 155.98 14.50 1 3 -10 92.09 8.50 1 3 -10 104.69 8.90 1 3 -10 89.49 8.70 -1 -3 10 93.19 9.00 -1 -3 10 77.99 7.50 0 3 -10 104.29 9.70 0 3 -10 110.99 9.90 0 3 -10 103.69 9.60 0 -3 10 106.89 9.90 0 -3 10 99.59 8.50 0 -3 10 98.59 9.70 -1 3 -10 461.55 37.90 -1 3 -10 395.56 37.90 1 -3 10 430.56 38.10 1 -3 10 503.55 36.70 1 -3 10 510.35 37.90 -2 3 -10 1.20 2.40 -2 3 -10 0.40 2.00 -2 3 -10 2.30 1.70 -2 3 -10 1.80 0.70 2 -3 10 2.10 1.50 2 -3 10 2.40 2.10 -3 3 -10 8.60 1.40 -3 3 -10 9.90 3.20 -3 3 -10 6.30 2.60 -3 3 -10 8.20 2.60 3 -3 10 10.60 2.70 3 -3 10 11.40 2.40 -4 3 -10 14.80 2.10 -4 3 -10 15.90 3.80 -4 3 -10 10.60 2.90 -4 3 -10 17.90 3.90 4 -3 10 15.60 2.40 4 -3 10 12.50 3.00 -5 3 -10 3.10 1.30 -5 3 -10 1.80 2.40 -5 3 -10 1.50 1.70 5 -3 10 1.20 1.50 -6 3 -10 22.30 4.10 -6 3 -10 21.70 4.80 -6 3 -10 17.50 2.80 6 -3 10 17.60 3.80 -7 3 -10 99.99 10.40 -7 3 -10 92.09 11.00 -7 3 -10 103.49 9.30 -8 3 -10 -3.70 1.60 -8 3 -10 -2.60 1.30 -8 3 -10 -3.60 2.10 -11 -2 10 18.40 4.20 10 2 -10 0.30 0.40 10 2 -10 -0.40 1.80 10 2 -10 0.50 0.30 -10 -2 10 -6.40 2.80 -10 -2 10 -0.50 2.60 9 2 -10 31.70 4.60 9 2 -10 34.00 3.40 9 2 -10 40.70 4.80 -9 -2 10 38.70 5.50 -9 -2 10 33.40 5.90 8 2 -10 8.50 2.70 8 2 -10 5.40 1.40 8 2 -10 10.50 2.40 -8 -2 10 9.60 3.70 -8 -2 10 8.30 3.10 7 2 -10 3.40 1.60 7 2 -10 2.40 1.10 7 2 -10 2.30 2.10 -7 -2 10 4.10 2.70 -7 -2 10 1.30 2.80 6 2 -10 26.90 3.90 6 2 -10 29.90 3.60 6 2 -10 25.70 3.30 -6 -2 10 25.50 4.70 5 2 -10 1.30 1.20 5 2 -10 0.60 1.00 5 2 -10 2.00 1.80 -5 -2 10 2.90 2.60 -5 -2 10 1.50 2.50 4 2 -10 8.20 2.80 4 2 -10 7.00 1.70 4 2 -10 5.90 1.70 4 2 -10 9.40 2.40 -4 -2 10 9.50 2.80 -4 -2 10 6.10 1.70 -4 -2 10 7.60 3.00 3 2 -10 32.70 3.90 3 2 -10 30.90 3.60 -3 -2 10 24.70 3.20 -3 -2 10 26.70 4.30 -3 -2 10 17.10 3.90 -3 -2 10 29.20 3.50 2 2 -10 140.69 12.10 2 2 -10 128.09 12.20 -2 -2 10 137.19 12.30 -2 -2 10 145.39 12.70 -2 -2 10 138.89 11.60 -2 -2 10 133.79 12.40 1 2 -10 6.30 1.80 1 2 -10 2.70 2.30 -1 -2 10 7.70 2.60 -1 -2 10 4.00 1.50 -1 -2 10 2.40 1.10 0 2 -10 33.80 4.40 0 2 -10 33.80 4.90 0 -2 10 36.30 4.90 0 -2 10 34.30 3.50 0 -2 10 40.80 4.60 -1 2 -10 32.80 4.80 -1 2 -10 24.80 3.90 -1 2 -10 28.90 3.00 1 -2 10 28.70 3.10 1 -2 10 34.40 4.20 1 -2 10 29.40 4.40 -2 2 -10 79.39 7.70 -2 2 -10 85.79 9.00 -2 2 -10 86.19 9.10 -2 2 -10 89.09 8.90 2 -2 10 93.39 8.50 2 -2 10 92.39 7.80 2 -2 10 104.59 9.10 -3 2 -10 -0.70 1.80 -3 2 -10 1.80 2.80 -3 2 -10 0.50 1.50 -3 2 -10 -0.70 0.90 3 -2 10 0.40 1.20 3 -2 10 2.10 1.70 -4 2 -10 1.40 1.20 -4 2 -10 0.60 2.70 -4 2 -10 1.60 1.70 -4 2 -10 0.00 1.90 4 -2 10 1.60 1.30 4 -2 10 1.10 1.40 -5 2 -10 1.00 1.30 -5 2 -10 2.00 2.20 -5 2 -10 0.40 1.70 5 -2 10 -1.70 1.30 -6 2 -10 5.80 2.80 -6 2 -10 5.70 2.00 -6 2 -10 4.20 2.40 6 -2 10 5.60 2.40 -7 2 -10 9.00 3.00 -7 2 -10 9.50 2.40 -7 2 -10 6.80 3.60 -8 2 -10 -3.40 1.80 -8 2 -10 -1.00 1.80 -8 2 -10 0.80 2.90 -12 -1 10 11.00 3.70 -11 -1 10 4.60 3.30 10 1 -10 0.80 1.60 -10 -1 10 1.00 3.20 -10 -1 10 1.40 2.80 9 1 -10 15.50 3.00 9 1 -10 17.50 1.80 9 1 -10 19.10 3.60 -9 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7 -11 8.30 2.60 -4 7 -11 7.40 2.80 -4 7 -11 3.40 2.50 4 -7 11 9.80 2.80 -5 7 -11 0.60 1.80 -5 7 -11 2.80 1.70 -5 7 -11 7.70 2.90 -5 7 -11 1.60 2.30 -6 7 -11 2.00 2.10 -6 7 -11 -0.80 2.30 -7 7 -11 15.40 3.70 -7 7 -11 10.80 3.80 10 6 -11 6.40 4.20 10 6 -11 8.70 2.20 -10 -6 11 14.80 3.80 9 6 -11 25.40 4.10 9 6 -11 24.60 5.40 -9 -6 11 27.90 4.80 8 6 -11 30.80 5.70 8 6 -11 23.10 3.90 8 6 -11 31.60 3.80 -8 -6 11 24.30 4.80 -8 -6 11 23.70 4.50 7 6 -11 28.40 5.50 7 6 -11 22.40 3.80 7 6 -11 24.10 3.80 -7 -6 11 26.60 4.40 -7 -6 11 30.60 4.60 6 6 -11 12.20 2.90 6 6 -11 18.50 4.20 6 6 -11 17.00 3.00 6 6 -11 13.40 2.90 -6 -6 11 16.90 3.20 -6 -6 11 11.20 4.20 -6 -6 11 15.50 3.60 5 6 -11 28.10 3.90 5 6 -11 30.30 3.90 5 6 -11 21.50 3.90 5 6 -11 26.00 5.30 -5 -6 11 32.40 4.60 -5 -6 11 32.90 4.20 -5 -6 11 25.60 5.30 4 6 -11 2.40 2.70 4 6 -11 1.50 1.40 4 6 -11 1.90 1.60 4 6 -11 1.50 1.60 -4 -6 11 0.90 2.40 -4 -6 11 0.50 2.60 -4 -6 11 1.00 1.50 3 6 -11 8.20 3.30 3 6 -11 7.50 2.20 3 6 -11 11.50 2.70 3 6 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5 -11 4.00 2.20 8 5 -11 -0.30 1.10 -8 -5 11 2.20 2.30 -8 -5 11 1.90 2.60 7 5 -11 1.40 1.30 7 5 -11 2.20 1.80 7 5 -11 4.10 2.30 7 5 -11 3.10 3.00 -7 -5 11 3.00 2.70 -7 -5 11 1.90 2.10 -7 -5 11 3.30 3.30 6 5 -11 51.69 7.50 6 5 -11 55.29 6.10 6 5 -11 59.89 6.30 6 5 -11 60.59 6.30 -6 -5 11 59.39 6.50 -6 -5 11 54.89 7.80 -6 -5 11 63.39 6.90 5 5 -11 36.10 4.50 5 5 -11 32.00 5.50 5 5 -11 35.50 4.30 5 5 -11 34.70 4.40 -5 -5 11 41.10 5.10 -5 -5 11 30.00 5.60 4 5 -11 154.38 13.40 4 5 -11 136.79 13.60 4 5 -11 161.58 14.40 4 5 -11 149.49 13.20 -4 -5 11 153.08 13.60 -4 -5 11 164.08 14.60 3 5 -11 8.00 2.20 3 5 -11 4.50 1.70 3 5 -11 5.50 3.20 3 5 -11 7.30 2.20 -3 -5 11 6.40 3.10 -3 -5 11 6.40 1.70 -3 -5 11 6.90 2.90 2 5 -11 39.80 4.60 2 5 -11 44.40 5.90 2 5 -11 48.80 5.20 -2 -5 11 36.80 5.30 -2 -5 11 39.90 6.00 -2 -5 11 40.70 3.80 -2 -5 11 34.50 3.70 1 5 -11 111.59 10.00 1 5 -11 108.19 10.50 -1 -5 11 100.89 8.70 -1 -5 11 113.29 8.70 -1 -5 11 110.99 10.50 -1 -5 11 113.29 11.00 0 5 -11 27.60 4.40 0 5 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6.10 -5 -6 12 50.39 7.60 4 6 -12 21.80 3.40 4 6 -12 23.10 3.40 4 6 -12 19.20 4.70 4 6 -12 20.20 3.70 -4 -6 12 23.30 4.20 -4 -6 12 20.10 3.20 -4 -6 12 20.00 4.80 3 6 -12 4.40 1.80 3 6 -12 7.10 3.00 3 6 -12 2.40 1.70 3 6 -12 0.80 1.80 -3 -6 12 1.10 2.50 -3 -6 12 3.40 1.40 -3 -6 12 5.50 3.20 2 6 -12 4.10 2.10 2 6 -12 2.60 1.90 2 6 -12 3.30 2.90 -2 -6 12 2.80 1.00 -2 -6 12 5.20 1.00 -2 -6 12 5.30 3.40 1 6 -12 218.58 19.10 1 6 -12 252.67 20.30 1 6 -12 218.68 19.90 -1 -6 12 219.68 20.20 0 6 -12 76.99 7.70 0 6 -12 60.89 7.40 0 6 -12 60.49 6.80 0 -6 12 69.99 8.00 -1 6 -12 39.30 5.40 -1 6 -12 44.10 5.40 -1 6 -12 39.90 5.50 1 -6 12 31.30 4.80 1 -6 12 37.70 5.70 -2 6 -12 24.70 4.00 -2 6 -12 25.70 4.40 -2 6 -12 20.50 4.10 2 -6 12 25.10 4.50 2 -6 12 20.40 4.00 -3 6 -12 23.70 3.70 -3 6 -12 17.90 4.00 -3 6 -12 19.30 4.10 -3 6 -12 20.00 4.00 3 -6 12 18.50 3.90 3 -6 12 17.80 3.70 -4 6 -12 2.70 2.50 -4 6 -12 6.80 2.80 -4 6 -12 6.80 2.70 4 -6 12 8.80 2.60 -5 6 -12 4.30 2.90 -5 6 -12 -0.10 1.80 -6 6 -12 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2.10 -5 -6 14 8.60 3.40 4 6 -14 23.10 3.70 4 6 -14 21.70 4.00 4 6 -14 23.50 4.90 -4 -6 14 28.30 4.90 -4 -6 14 20.40 3.10 -4 -6 14 18.30 2.90 3 6 -14 77.29 8.90 3 6 -14 96.19 7.90 3 6 -14 73.99 8.20 -3 -6 14 76.79 9.40 -3 -6 14 73.29 6.60 -3 -6 14 63.49 6.60 2 6 -14 11.10 3.00 2 6 -14 8.70 2.60 2 6 -14 6.70 3.40 -2 -6 14 3.40 3.50 1 6 -14 8.40 2.90 1 6 -14 5.50 3.20 -1 -6 14 5.70 3.40 0 6 -14 3.30 3.00 0 6 -14 8.20 2.90 0 6 -14 8.30 2.60 0 -6 14 1.30 3.00 -1 6 -14 1.60 2.60 -1 6 -14 -1.60 2.40 -1 6 -14 -0.40 1.40 1 -6 14 -2.30 2.80 -2 6 -14 25.20 5.10 -2 6 -14 39.90 5.70 2 -6 14 37.10 5.70 -3 6 -14 1.10 2.10 -3 6 -14 0.40 2.20 3 -6 14 0.70 2.90 -4 6 -14 2.30 2.20 -4 6 -14 3.20 2.50 4 -6 14 7.80 2.30 -5 6 -14 73.59 9.40 -5 6 -14 61.19 9.50 5 -6 14 99.49 7.60 9 5 -14 1.40 1.50 -9 -5 14 2.90 3.30 8 5 -14 6.90 2.20 8 5 -14 9.00 4.20 -8 -5 14 4.00 3.60 -8 -5 14 6.30 3.10 7 5 -14 -1.10 2.00 7 5 -14 -1.10 1.20 7 5 -14 0.00 3.20 -7 -5 14 -0.60 2.90 6 5 -14 178.58 14.80 6 5 -14 138.99 14.80 6 5 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2.80 1.90 2 1 -18 -1.20 1.90 -2 -1 18 0.10 1.70 5 0 -18 18.80 4.30 5 0 -18 26.40 4.60 -5 0 18 30.50 6.00 -5 0 18 26.50 4.60 4 0 -18 -1.40 1.80 -4 0 18 -1.40 1.80 3 0 -18 2.20 1.80 3 0 -18 2.50 2.50 -3 0 18 3.00 2.20 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 95088