data_mo_d8v19200_0m _audit_creation_method SHELXL-2013 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C33 H48 F2 N2 O2 Pd' _chemical_formula_weight 649.13 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'F' 'F' 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Pd' 'Pd' -0.9988 1.0072 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/c' _space_group_name_Hall '-P 2ybc' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 16.8572(6) _cell_length_b 12.4408(4) _cell_length_c 34.1009(13) _cell_angle_alpha 90 _cell_angle_beta 103.4980(10) _cell_angle_gamma 90 _cell_volume 6954.0(4) _cell_formula_units_Z 8 _cell_measurement_temperature 192(2) _cell_measurement_reflns_used 9700 _cell_measurement_theta_min 4.970 _cell_measurement_theta_max 54.905 _exptl_crystal_description prismatic _exptl_crystal_colour colorless _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.240 _exptl_crystal_F_000 2720 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.180 _exptl_crystal_size_mid 0.150 _exptl_crystal_size_min 0.120 _exptl_absorpt_coefficient_mu 0.573 _shelx_estimated_absorpt_T_min 0.904 _shelx_estimated_absorpt_T_max 0.934 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.6695 _exptl_absorpt_correction_T_max 0.7456 _exptl_absorpt_process_details sadabs _exptl_special_details ; ? ; _diffrn_ambient_temperature 192(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source ? _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 115656 _diffrn_reflns_av_unetI/netI 0.0277 _diffrn_reflns_av_R_equivalents 0.0495 _diffrn_reflns_limit_h_min -20 _diffrn_reflns_limit_h_max 20 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_l_min -42 _diffrn_reflns_limit_l_max 38 _diffrn_reflns_theta_min 2.241 _diffrn_reflns_theta_max 25.999 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measured_fraction_theta_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_point_group_measured_fraction_full 0.999 _reflns_number_total 13640 _reflns_number_gt 11220 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Bruker APEX2' _computing_cell_refinement 'Bruker SAINT' _computing_data_reduction 'Bruker SAINT' _computing_structure_solution 'SHELXS-97 (Sheldrick 2008)' _computing_structure_refinement 'SHELXL-2013 (Sheldrick, 2013)' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _refine_special_details ; ? ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0439P)^2^+5.4311P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method SHELXL _refine_ls_extinction_coef 0.00104(11) _refine_ls_extinction_expression 'Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^' _refine_ls_number_reflns 13640 _refine_ls_number_parameters 774 _refine_ls_number_restraints 51 _refine_ls_R_factor_all 0.0465 _refine_ls_R_factor_gt 0.0342 _refine_ls_wR_factor_ref 0.0949 _refine_ls_wR_factor_gt 0.0858 _refine_ls_goodness_of_fit_ref 1.041 _refine_ls_restrained_S_all 1.060 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Pd1 Pd 0.44435(2) 0.82303(2) 0.39005(2) 0.03168(7) Uani 1 1 d . . . . . Pd2 Pd 0.95095(2) 0.61945(2) 0.38935(2) 0.02989(7) Uani 1 1 d . . . . . F1 F 0.59711(9) 0.78530(14) 0.43573(5) 0.0471(4) Uani 1 1 d . . . . . F2 F 0.51931(11) 0.64649(14) 0.43601(6) 0.0573(5) Uani 1 1 d . . . . . F3 F 0.97511(12) 0.76488(16) 0.45488(6) 0.0621(5) Uani 1 1 d . . . . . F4 F 1.07735(9) 0.74461(14) 0.42741(6) 0.0537(4) Uani 1 1 d . . . . . N1 N 0.34072(12) 0.74879(17) 0.44559(6) 0.0306(5) Uani 1 1 d . . . . . N2 N 0.29983(12) 0.69042(17) 0.38431(6) 0.0317(5) Uani 1 1 d . . . . . N3 N 0.79737(13) 0.75078(17) 0.37508(7) 0.0355(5) Uani 1 1 d . . . . . N4 N 0.78799(13) 0.59821(17) 0.40415(7) 0.0350(5) Uani 1 1 d . . . . . O1 O 0.52818(12) 0.90115(18) 0.36221(6) 0.0497(5) Uani 1 1 d . . . . . O2 O 0.39766(13) 0.9199(2) 0.33587(7) 0.0610(6) Uani 1 1 d . . . . . O3 O 1.05926(11) 0.54564(15) 0.37987(6) 0.0436(5) Uani 1 1 d . . . . . O4 O 0.94138(12) 0.47039(17) 0.35421(7) 0.0521(5) Uani 1 1 d . . . . . C1 C 0.26459(16) 0.6911(2) 0.44611(8) 0.0381(6) Uani 1 1 d . . . . . H1A H 0.2202 0.7417 0.4477 0.046 Uiso 1 1 calc R U . . . H1B H 0.2726 0.6401 0.4690 0.046 Uiso 1 1 calc R U . . . C2 C 0.24663(17) 0.6323(2) 0.40596(8) 0.0396(6) Uani 1 1 d . . . . . H2A H 0.2616 0.5553 0.4094 0.048 Uiso 1 1 calc R U . . . H2B H 0.1884 0.6386 0.3918 0.048 Uiso 1 1 calc R U . . . C3 C 0.35517(14) 0.75120(19) 0.40849(7) 0.0284(5) Uani 1 1 d . . . . . C4 C 0.37303(15) 0.8215(2) 0.47811(8) 0.0324(6) Uani 1 1 d . . . . . C5 C 0.42027(16) 0.7779(2) 0.51412(8) 0.0359(6) Uani 1 1 d . . . . . C6 C 0.44785(19) 0.8488(3) 0.54644(9) 0.0471(7) Uani 1 1 d . . . . . H6 H 0.4798 0.8221 0.5712 0.057 Uiso 1 1 calc R U . . . C7 C 0.4291(2) 0.9571(3) 0.54260(10) 0.0551(8) Uani 1 1 d . . . . . H7 H 0.4489 1.0042 0.5646 0.066 Uiso 1 1 calc R U . . . C8 C 0.38194(19) 0.9971(3) 0.50719(10) 0.0531(8) Uani 1 1 d . . . . . H8 H 0.3696 1.0717 0.5052 0.064 Uiso 1 1 calc R U . . . C9 C 0.35173(16) 0.9308(2) 0.47404(9) 0.0400(6) Uani 1 1 d . . . . . C10 C 0.29408(18) 0.9777(2) 0.43711(10) 0.0493(7) Uani 1 1 d . . . . . H10 H 0.2820 0.9198 0.4162 0.059 Uiso 1 1 calc R U . . . C11 C 0.3318(2) 1.0718(3) 0.41895(12) 0.0707(10) Uani 1 1 d . . . . . H11A H 0.3423 1.1313 0.4383 0.106 Uiso 1 1 calc R U . . . H11B H 0.2939 1.0956 0.3941 0.106 Uiso 1 1 calc R U . . . H11C H 0.3832 1.0487 0.4128 0.106 Uiso 1 1 calc R U . . . C12 C 0.2129(2) 1.0101(4) 0.44683(13) 0.0783(12) Uani 1 1 d . . . . . H12A H 0.1905 0.9487 0.4587 0.117 Uiso 1 1 calc R U . . . H12B H 0.1742 1.0321 0.4220 0.117 Uiso 1 1 calc R U . . . H12C H 0.2220 1.0701 0.4660 0.117 Uiso 1 1 calc R U . . . C13 C 0.43982(17) 0.6592(2) 0.51967(8) 0.0402(6) Uani 1 1 d . . . . . H13 H 0.4216 0.6236 0.4928 0.048 Uiso 1 1 calc R U . . . C14 C 0.3919(2) 0.6086(3) 0.54820(10) 0.0576(9) Uani 1 1 d . . . . . H14A H 0.4098 0.6407 0.5751 0.086 Uiso 1 1 calc R U . . . H14B H 0.4020 0.5310 0.5500 0.086 Uiso 1 1 calc R U . . . H14C H 0.3335 0.6219 0.5378 0.086 Uiso 1 1 calc R U . . . C15 C 0.53100(19) 0.6373(3) 0.53512(9) 0.0512(8) Uani 1 1 d . . . . . H15A H 0.5609 0.6682 0.5164 0.077 Uiso 1 1 calc R U . . . H15B H 0.5404 0.5595 0.5371 0.077 Uiso 1 1 calc R U . . . H15C H 0.5502 0.6700 0.5618 0.077 Uiso 1 1 calc R U . . . C16 C 0.28872(16) 0.6771(2) 0.34128(8) 0.0364(6) Uani 1 1 d . . . . . C17 C 0.22973(17) 0.7409(3) 0.31606(9) 0.0452(7) Uani 1 1 d . . . . . C18 C 0.2172(2) 0.7231(3) 0.27441(9) 0.0595(9) Uani 1 1 d . . . . . H18 H 0.1780 0.7652 0.2563 0.071 Uiso 1 1 calc R U . . . C19 C 0.2601(2) 0.6466(3) 0.25937(10) 0.0637(10) Uani 1 1 d . . . . . H19 H 0.2505 0.6363 0.2310 0.076 Uiso 1 1 calc R U . . . C20 C 0.3167(2) 0.5848(3) 0.28480(9) 0.0561(8) Uani 1 1 d . . . . . H20 H 0.3457 0.5316 0.2739 0.067 Uiso 1 1 calc R U . . . C21 C 0.33270(17) 0.5984(2) 0.32665(8) 0.0422(7) Uani 1 1 d . . . . . C22 C 0.39668(18) 0.5292(3) 0.35348(9) 0.0498(8) Uani 1 1 d . . . . . H22 H 0.3978 0.5482 0.3821 0.060 Uiso 1 1 calc R U . . . C23 C 0.4814(2) 0.5532(4) 0.34631(11) 0.0774(12) Uani 1 1 d . . . . . H23A H 0.4829 0.5321 0.3188 0.116 Uiso 1 1 calc R U . . . H23B H 0.5227 0.5126 0.3657 0.116 Uiso 1 1 calc R U . . . H23C H 0.4928 0.6303 0.3499 0.116 Uiso 1 1 calc R U . . . C24 C 0.3761(3) 0.4103(3) 0.34791(12) 0.0786(12) Uani 1 1 d . . . . . H24A H 0.3232 0.3967 0.3542 0.118 Uiso 1 1 calc R U . . . H24B H 0.4184 0.3680 0.3660 0.118 Uiso 1 1 calc R U . . . H24C H 0.3736 0.3897 0.3199 0.118 Uiso 1 1 calc R U . . . C25 C 0.18005(19) 0.8254(3) 0.33187(10) 0.0558(8) Uani 1 1 d . . . . . H25 H 0.2002 0.8284 0.3619 0.067 Uiso 1 1 calc R U . . . C26 C 0.1905(2) 0.9365(3) 0.31526(15) 0.0814(12) Uani 1 1 d . . . . . H26A H 0.2487 0.9540 0.3204 0.122 Uiso 1 1 calc R U . . . H26B H 0.1628 0.9897 0.3285 0.122 Uiso 1 1 calc R U . . . H26C H 0.1668 0.9374 0.2861 0.122 Uiso 1 1 calc R U . . . C27 C 0.0896(2) 0.7939(4) 0.32255(13) 0.0747(11) Uani 1 1 d . . . . . H27A H 0.0589 0.8480 0.3338 0.112 Uiso 1 1 calc R U . . . H27B H 0.0837 0.7238 0.3347 0.112 Uiso 1 1 calc R U . . . H27C H 0.0684 0.7898 0.2933 0.112 Uiso 1 1 calc R U . . . C28 C 0.51857(15) 0.7562(2) 0.43630(8) 0.0375(6) Uani 1 1 d . . . . . H28 H 0.5055 0.7822 0.4618 0.045 Uiso 1 1 calc R U . . . C29 C 0.4710(2) 0.9392(3) 0.33546(10) 0.0609(9) Uani 1 1 d . . . . . C30 C 0.4910(4) 1.0085(6) 0.30245(18) 0.142(2) Uani 1 1 d D U . . . C31 C 0.5787(4) 1.0243(6) 0.3059(2) 0.167(3) Uani 1 1 d D U . . . H31A H 0.6037 0.9559 0.3011 0.251 Uiso 1 1 calc R U . . . H31B H 0.6043 1.0503 0.3331 0.251 Uiso 1 1 calc R U . . . H31C H 0.5867 1.0773 0.2860 0.251 Uiso 1 1 calc R U . . . C32 C 0.4707(5) 1.1312(6) 0.3164(2) 0.185(3) Uani 1 1 d D U . . . H32A H 0.4722 1.1821 0.2947 0.277 Uiso 1 1 calc R U . . . H32B H 0.5115 1.1519 0.3407 0.277 Uiso 1 1 calc R U . . . H32C H 0.4163 1.1322 0.3221 0.277 Uiso 1 1 calc R U . . . C33 C 0.4296(4) 1.0037(6) 0.26529(16) 0.163(3) Uani 1 1 d D U . . . H33A H 0.4356 0.9367 0.2511 0.245 Uiso 1 1 calc R U . . . H33B H 0.4359 1.0651 0.2483 0.245 Uiso 1 1 calc R U . . . H33C H 0.3754 1.0059 0.2711 0.245 Uiso 1 1 calc R U . . . C34 C 0.70895(16) 0.7405(2) 0.37301(10) 0.0477(7) Uani 1 1 d . . . . . H34A H 0.6781 0.7211 0.3455 0.057 Uiso 1 1 calc R U . . . H34B H 0.6862 0.8075 0.3816 0.057 Uiso 1 1 calc R U . . . C35 C 0.70864(18) 0.6504(3) 0.40243(12) 0.0567(9) Uani 1 1 d . . . . . H35A H 0.7053 0.6783 0.4292 0.068 Uiso 1 1 calc R U . . . H35B H 0.6628 0.6003 0.3925 0.068 Uiso 1 1 calc R U . . . C36 C 0.83895(15) 0.6625(2) 0.39054(7) 0.0302(5) Uani 1 1 d . . . . . C37 C 0.82877(16) 0.8376(2) 0.35525(9) 0.0412(7) Uani 1 1 d . . . . . C38 C 0.83728(19) 0.8237(3) 0.31609(10) 0.0533(8) Uani 1 1 d . . . . . C39 C 0.8695(2) 0.9108(4) 0.29856(12) 0.0724(11) Uani 1 1 d . . . . . H39 H 0.8771 0.9044 0.2719 0.087 Uiso 1 1 calc R U . . . C40 C 0.8900(2) 1.0047(3) 0.31932(16) 0.0809(13) Uani 1 1 d . . . . . H40 H 0.9124 1.0620 0.3070 0.097 Uiso 1 1 calc R U . . . C41 C 0.8789(2) 1.0176(3) 0.35760(15) 0.0725(11) Uani 1 1 d . . . . . H41 H 0.8928 1.0840 0.3712 0.087 Uiso 1 1 calc R U . . . C42 C 0.84765(18) 0.9348(2) 0.37661(11) 0.0541(8) Uani 1 1 d . . . . . C43 C 0.8342(2) 0.9512(3) 0.41838(12) 0.0683(10) Uani 1 1 d . . . . . H43 H 0.8300 0.8786 0.4303 0.082 Uiso 1 1 calc R U . . . C44 C 0.9052(3) 1.0110(3) 0.44656(15) 0.0938(14) Uani 1 1 d . . . . . H44A H 0.9567 0.9747 0.4464 0.141 Uiso 1 1 calc R U . . . H44B H 0.8968 1.0112 0.4740 0.141 Uiso 1 1 calc R U . . . H44C H 0.9072 1.0852 0.4372 0.141 Uiso 1 1 calc R U . . . C45 C 0.7539(3) 1.0105(3) 0.41696(16) 0.0926(15) Uani 1 1 d . . . . . H45A H 0.7527 1.0775 0.4017 0.139 Uiso 1 1 calc R U . . . H45B H 0.7495 1.0270 0.4445 0.139 Uiso 1 1 calc R U . . . H45C H 0.7080 0.9649 0.4038 0.139 Uiso 1 1 calc R U . . . C46 C 0.8122(2) 0.7223(3) 0.29220(10) 0.0665(10) Uani 1 1 d . . . . . H46 H 0.7936 0.6696 0.3103 0.080 Uiso 1 1 calc R U . . . C47 C 0.7390(3) 0.7461(5) 0.25643(14) 0.116(2) Uani 1 1 d . . . . . H47A H 0.6946 0.7783 0.2666 0.174 Uiso 1 1 calc R U . . . H47B H 0.7200 0.6790 0.2423 0.174 Uiso 1 1 calc R U . . . H47C H 0.7560 0.7962 0.2378 0.174 Uiso 1 1 calc R U . . . C48 C 0.8822(3) 0.6701(4) 0.27723(12) 0.0848(13) Uani 1 1 d . . . . . H48A H 0.8979 0.7171 0.2573 0.127 Uiso 1 1 calc R U . . . H48B H 0.8642 0.6006 0.2648 0.127 Uiso 1 1 calc R U . . . H48C H 0.9290 0.6594 0.3000 0.127 Uiso 1 1 calc R U . . . C49 C 0.80975(15) 0.5001(2) 0.42643(8) 0.0343(6) Uani 1 1 d . . . . . C50 C 0.83779(15) 0.5056(2) 0.46845(9) 0.0360(6) Uani 1 1 d . . . . . C51 C 0.85632(17) 0.4091(2) 0.48945(9) 0.0428(7) Uani 1 1 d . . . . . H51 H 0.8758 0.4103 0.5179 0.051 Uiso 1 1 calc R U . . . C52 C 0.84671(19) 0.3120(2) 0.46940(10) 0.0494(8) Uani 1 1 d . . . . . H52 H 0.8599 0.2469 0.4841 0.059 Uiso 1 1 calc R U . . . C53 C 0.8180(2) 0.3091(2) 0.42817(10) 0.0492(8) Uani 1 1 d . . . . . H53 H 0.8116 0.2415 0.4148 0.059 Uiso 1 1 calc R U . . . C54 C 0.79805(17) 0.4029(2) 0.40541(9) 0.0402(6) Uani 1 1 d . . . . . C55 C 0.7633(2) 0.3968(3) 0.36051(10) 0.0527(8) Uani 1 1 d . . . . . H55 H 0.7766 0.4656 0.3483 0.063 Uiso 1 1 calc R U . . . C56 C 0.6710(3) 0.3856(5) 0.35123(12) 0.1036(18) Uani 1 1 d . . . . . H56A H 0.6564 0.3206 0.3642 0.155 Uiso 1 1 calc R U . . . H56B H 0.6496 0.3804 0.3220 0.155 Uiso 1 1 calc R U . . . H56C H 0.6474 0.4486 0.3615 0.155 Uiso 1 1 calc R U . . . C57 C 0.7965(2) 0.3048(3) 0.33971(12) 0.0662(10) Uani 1 1 d . . . . . H57A H 0.8563 0.3043 0.3481 0.099 Uiso 1 1 calc R U . . . H57B H 0.7796 0.3143 0.3104 0.099 Uiso 1 1 calc R U . . . H57C H 0.7752 0.2364 0.3472 0.099 Uiso 1 1 calc R U . . . C58 C 0.84634(18) 0.6103(2) 0.49169(9) 0.0456(7) Uani 1 1 d . . . . . H58 H 0.8410 0.6708 0.4720 0.055 Uiso 1 1 calc R U . . . C59 C 0.9306(2) 0.6196(3) 0.52173(11) 0.0675(10) Uani 1 1 d . . . . . H59A H 0.9350 0.5647 0.5428 0.101 Uiso 1 1 calc R U . . . H59B H 0.9361 0.6911 0.5341 0.101 Uiso 1 1 calc R U . . . H59C H 0.9739 0.6089 0.5073 0.101 Uiso 1 1 calc R U . . . C60 C 0.7777(2) 0.6212(3) 0.51446(12) 0.0683(10) Uani 1 1 d . . . . . H60A H 0.7247 0.6120 0.4955 0.102 Uiso 1 1 calc R U . . . H60B H 0.7803 0.6925 0.5269 0.102 Uiso 1 1 calc R U . . . H60C H 0.7845 0.5659 0.5355 0.102 Uiso 1 1 calc R U . . . C61 C 0.99325(15) 0.7509(2) 0.41821(8) 0.0364(6) Uani 1 1 d . . . . . H61 H 0.9748 0.8149 0.4007 0.044 Uiso 1 1 calc R U . . . C62 C 1.01769(17) 0.4722(2) 0.35865(9) 0.0452(7) Uani 1 1 d . . . . . C63 C 1.0595(2) 0.3873(3) 0.33827(12) 0.0660(11) Uani 1 1 d . . . . . C64 C 1.1143(6) 0.4545(8) 0.3131(3) 0.080(3) Uani 0.5 1 d . U P A 1 H64A H 1.1474 0.4044 0.3015 0.121 Uiso 0.5 1 calc R U P A 1 H64B H 1.1502 0.5043 0.3313 0.121 Uiso 0.5 1 calc R U P A 1 H64C H 1.0782 0.4951 0.2915 0.121 Uiso 0.5 1 calc R U P A 1 C65 C 1.0050(9) 0.3125(9) 0.3123(4) 0.099(3) Uani 0.5 1 d . U P A 1 H65A H 0.9767 0.2686 0.3287 0.148 Uiso 0.5 1 calc R U P A 1 H65B H 1.0367 0.2658 0.2985 0.148 Uiso 0.5 1 calc R U P A 1 H65C H 0.9648 0.3528 0.2923 0.148 Uiso 0.5 1 calc R U P A 1 C66 C 1.1273(7) 0.3341(9) 0.3705(3) 0.101(2) Uani 0.5 1 d . U P A 1 H66A H 1.1032 0.2994 0.3908 0.152 Uiso 0.5 1 calc R U P A 1 H66B H 1.1664 0.3889 0.3835 0.152 Uiso 0.5 1 calc R U P A 1 H66C H 1.1554 0.2801 0.3577 0.152 Uiso 0.5 1 calc R U P A 1 C64' C 1.1430(6) 0.4109(9) 0.3382(4) 0.093(3) Uani 0.5 1 d . U P A 2 H64D H 1.1460 0.4807 0.3253 0.139 Uiso 0.5 1 calc R U P A 2 H64E H 1.1644 0.3548 0.3233 0.139 Uiso 0.5 1 calc R U P A 2 H64F H 1.1756 0.4133 0.3661 0.139 Uiso 0.5 1 calc R U P A 2 C65' C 1.0022(8) 0.3665(10) 0.2959(3) 0.089(3) Uani 0.5 1 d . U P A 2 H65D H 0.9954 0.4333 0.2802 0.133 Uiso 0.5 1 calc R U P A 2 H65E H 0.9489 0.3418 0.2991 0.133 Uiso 0.5 1 calc R U P A 2 H65F H 1.0264 0.3114 0.2817 0.133 Uiso 0.5 1 calc R U P A 2 C66' C 1.0543(6) 0.2790(7) 0.3636(3) 0.099(3) Uani 0.5 1 d . U P A 2 H66D H 1.0803 0.2198 0.3523 0.148 Uiso 0.5 1 calc R U P A 2 H66E H 0.9969 0.2612 0.3619 0.148 Uiso 0.5 1 calc R U P A 2 H66F H 1.0823 0.2902 0.3918 0.148 Uiso 0.5 1 calc R U P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Pd1 0.02775(11) 0.03942(12) 0.02928(12) 0.00326(8) 0.00949(8) -0.00242(8) Pd2 0.02591(11) 0.03300(12) 0.03285(12) 0.00018(8) 0.01110(8) 0.00098(7) F1 0.0267(8) 0.0604(10) 0.0545(10) -0.0034(8) 0.0100(7) 0.0052(7) F2 0.0606(11) 0.0409(10) 0.0623(12) 0.0084(8) -0.0022(9) 0.0033(8) F3 0.0702(12) 0.0665(12) 0.0550(11) -0.0215(10) 0.0258(10) -0.0122(10) F4 0.0308(8) 0.0521(10) 0.0744(12) -0.0106(9) 0.0044(8) -0.0014(7) N1 0.0279(10) 0.0370(12) 0.0285(11) -0.0013(9) 0.0095(9) -0.0054(9) N2 0.0272(10) 0.0427(12) 0.0253(11) 0.0014(9) 0.0063(9) -0.0043(9) N3 0.0291(11) 0.0344(12) 0.0449(13) 0.0113(10) 0.0127(10) 0.0042(9) N4 0.0291(11) 0.0323(11) 0.0486(14) 0.0096(10) 0.0193(10) 0.0058(9) O1 0.0393(11) 0.0672(14) 0.0460(12) 0.0129(11) 0.0168(10) -0.0066(10) O2 0.0453(13) 0.0886(17) 0.0498(13) 0.0285(12) 0.0126(10) 0.0045(12) O3 0.0317(10) 0.0467(11) 0.0554(12) -0.0162(10) 0.0165(9) -0.0021(8) O4 0.0348(11) 0.0555(13) 0.0681(15) -0.0229(11) 0.0165(10) -0.0054(9) C1 0.0311(13) 0.0508(17) 0.0348(15) -0.0014(12) 0.0124(11) -0.0113(12) C2 0.0356(14) 0.0500(17) 0.0347(15) 0.0016(12) 0.0111(12) -0.0110(12) C3 0.0245(12) 0.0317(13) 0.0277(13) 0.0034(10) 0.0036(10) 0.0022(10) C4 0.0279(12) 0.0396(14) 0.0318(14) -0.0047(11) 0.0114(11) -0.0034(11) C5 0.0348(14) 0.0434(15) 0.0312(14) -0.0025(12) 0.0111(11) -0.0027(12) C6 0.0476(17) 0.0606(19) 0.0303(15) -0.0081(14) 0.0035(13) -0.0022(15) C7 0.059(2) 0.056(2) 0.0465(19) -0.0220(16) 0.0062(16) -0.0038(16) C8 0.0547(19) 0.0424(17) 0.061(2) -0.0151(15) 0.0104(16) 0.0024(14) C9 0.0354(14) 0.0420(16) 0.0426(16) -0.0048(13) 0.0092(12) 0.0010(12) C10 0.0454(17) 0.0437(17) 0.0551(19) -0.0015(14) 0.0045(14) 0.0092(13) C11 0.073(2) 0.062(2) 0.071(3) 0.0152(19) 0.004(2) 0.0031(19) C12 0.052(2) 0.086(3) 0.095(3) 0.006(2) 0.012(2) 0.023(2) C13 0.0439(16) 0.0458(16) 0.0294(14) 0.0019(12) 0.0056(12) 0.0005(13) C14 0.062(2) 0.064(2) 0.0487(19) 0.0161(16) 0.0156(16) -0.0021(17) C15 0.0494(18) 0.062(2) 0.0398(17) 0.0054(15) 0.0047(14) 0.0099(15) C16 0.0307(13) 0.0510(17) 0.0254(13) 0.0002(12) 0.0022(11) -0.0076(12) C17 0.0372(15) 0.0580(19) 0.0366(16) 0.0062(14) 0.0010(12) -0.0031(13) C18 0.057(2) 0.079(2) 0.0339(17) 0.0141(17) -0.0063(15) 0.0025(18) C19 0.076(2) 0.085(3) 0.0265(16) 0.0002(17) 0.0043(16) -0.006(2) C20 0.059(2) 0.079(2) 0.0302(16) -0.0055(16) 0.0094(14) 0.0013(18) C21 0.0384(15) 0.0584(18) 0.0289(14) -0.0019(13) 0.0060(12) -0.0018(13) C22 0.0465(17) 0.069(2) 0.0315(15) -0.0082(14) 0.0034(13) 0.0138(15) C23 0.0459(19) 0.129(4) 0.058(2) -0.017(2) 0.0129(17) 0.017(2) C24 0.099(3) 0.067(2) 0.058(2) -0.0059(19) -0.005(2) 0.020(2) C25 0.0442(17) 0.069(2) 0.0491(19) 0.0086(16) -0.0004(15) 0.0110(15) C26 0.059(2) 0.066(2) 0.116(4) 0.018(2) 0.013(2) 0.0099(19) C27 0.048(2) 0.098(3) 0.078(3) 0.025(2) 0.0144(19) 0.012(2) C28 0.0297(13) 0.0437(16) 0.0400(15) 0.0000(12) 0.0103(11) 0.0027(11) C29 0.053(2) 0.083(3) 0.052(2) 0.0234(19) 0.0241(17) -0.0004(18) C30 0.110(3) 0.204(5) 0.121(3) 0.114(4) 0.047(3) 0.006(4) C31 0.127(4) 0.236(6) 0.162(5) 0.113(5) 0.083(4) -0.009(4) C32 0.173(6) 0.198(6) 0.179(6) 0.110(5) 0.032(5) -0.027(5) C33 0.196(6) 0.217(6) 0.077(3) 0.077(4) 0.031(4) -0.007(5) C34 0.0308(14) 0.0451(17) 0.070(2) 0.0161(15) 0.0180(14) 0.0072(12) C35 0.0389(16) 0.0472(17) 0.093(3) 0.0248(18) 0.0335(17) 0.0165(14) C36 0.0303(13) 0.0315(13) 0.0297(13) -0.0003(10) 0.0089(10) 0.0011(10) C37 0.0288(13) 0.0415(16) 0.0533(18) 0.0202(14) 0.0093(12) 0.0058(11) C38 0.0398(16) 0.069(2) 0.0504(19) 0.0260(16) 0.0081(14) 0.0000(15) C39 0.059(2) 0.091(3) 0.070(3) 0.041(2) 0.0217(19) 0.000(2) C40 0.064(2) 0.060(2) 0.120(4) 0.049(3) 0.024(2) -0.0027(19) C41 0.064(2) 0.0417(19) 0.115(4) 0.025(2) 0.027(2) 0.0055(16) C42 0.0410(16) 0.0350(16) 0.086(3) 0.0178(16) 0.0145(16) 0.0075(13) C43 0.084(3) 0.0378(17) 0.087(3) -0.0027(18) 0.028(2) 0.0048(17) C44 0.105(4) 0.057(2) 0.112(4) -0.022(2) 0.011(3) 0.010(2) C45 0.084(3) 0.055(2) 0.151(5) -0.020(3) 0.053(3) 0.000(2) C46 0.061(2) 0.096(3) 0.0416(19) 0.0088(19) 0.0116(16) -0.021(2) C47 0.076(3) 0.189(6) 0.067(3) 0.003(3) -0.017(2) -0.021(3) C48 0.093(3) 0.108(3) 0.059(2) -0.009(2) 0.029(2) -0.020(3) C49 0.0289(13) 0.0325(13) 0.0466(16) 0.0081(12) 0.0188(12) 0.0041(10) C50 0.0302(13) 0.0352(14) 0.0468(16) 0.0057(12) 0.0174(12) -0.0014(11) C51 0.0378(15) 0.0449(16) 0.0471(17) 0.0111(13) 0.0125(13) 0.0012(12) C52 0.0514(18) 0.0388(16) 0.060(2) 0.0171(14) 0.0159(15) 0.0072(13) C53 0.0581(19) 0.0301(14) 0.062(2) 0.0010(14) 0.0197(16) 0.0037(13) C54 0.0407(15) 0.0374(15) 0.0475(17) 0.0025(13) 0.0206(13) 0.0039(12) C55 0.067(2) 0.0483(18) 0.0480(19) -0.0005(14) 0.0232(16) 0.0043(15) C56 0.072(3) 0.182(5) 0.050(2) -0.019(3) 0.002(2) 0.041(3) C57 0.072(2) 0.061(2) 0.074(2) -0.0264(19) 0.032(2) -0.0120(18) C58 0.0490(17) 0.0417(16) 0.0496(18) -0.0003(13) 0.0186(14) -0.0050(13) C59 0.070(2) 0.066(2) 0.061(2) -0.0066(18) 0.0052(19) -0.0157(19) C60 0.081(3) 0.059(2) 0.079(3) -0.0140(19) 0.048(2) -0.0053(19) C61 0.0289(13) 0.0390(15) 0.0405(15) -0.0010(12) 0.0063(11) 0.0018(11) C62 0.0378(15) 0.0507(17) 0.0505(18) -0.0146(14) 0.0172(13) -0.0013(13) C63 0.0468(19) 0.080(3) 0.074(2) -0.041(2) 0.0203(18) 0.0031(17) C64 0.083(6) 0.097(6) 0.080(6) -0.026(5) 0.056(5) -0.002(5) C65 0.084(4) 0.094(7) 0.119(7) -0.061(5) 0.026(6) 0.005(6) C66 0.105(5) 0.095(5) 0.110(5) -0.036(4) 0.035(5) 0.040(4) C64' 0.078(5) 0.099(6) 0.113(6) -0.043(5) 0.044(5) 0.013(4) C65' 0.073(5) 0.112(8) 0.084(7) -0.053(6) 0.024(5) 0.013(6) C66' 0.100(5) 0.080(5) 0.118(6) -0.034(5) 0.029(5) 0.031(4) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Pd1 C28 1.956(3) . ? Pd1 C3 1.974(2) . ? Pd1 O1 2.1141(19) . ? Pd1 O2 2.192(2) . ? Pd1 C29 2.480(3) . ? Pd2 C61 1.955(3) . ? Pd2 C36 1.972(2) . ? Pd2 O3 2.1347(18) . ? Pd2 O4 2.193(2) . ? Pd2 C62 2.503(3) . ? F1 C28 1.377(3) . ? F2 C28 1.365(3) . ? F3 C61 1.366(3) . ? F4 C61 1.381(3) . ? N1 C3 1.343(3) . ? N1 C4 1.437(3) . ? N1 C1 1.474(3) . ? N2 C3 1.328(3) . ? N2 C16 1.445(3) . ? N2 C2 1.477(3) . ? N3 C36 1.343(3) . ? N3 C37 1.439(3) . ? N3 C34 1.481(3) . ? N4 C36 1.334(3) . ? N4 C49 1.439(3) . ? N4 C35 1.476(3) . ? O1 C29 1.255(4) . ? O2 C29 1.263(4) . ? O3 C62 1.270(3) . ? O4 C62 1.260(3) . ? C1 C2 1.519(4) . ? C1 H1A 0.9900 . ? C1 H1B 0.9900 . ? C2 H2A 0.9900 . ? C2 H2B 0.9900 . ? C4 C9 1.404(4) . ? C4 C5 1.407(4) . ? C5 C6 1.404(4) . ? C5 C13 1.515(4) . ? C6 C7 1.383(5) . ? C6 H6 0.9500 . ? C7 C8 1.375(5) . ? C7 H7 0.9500 . ? C8 C9 1.396(4) . ? C8 H8 0.9500 . ? C9 C10 1.517(4) . ? C10 C11 1.530(5) . ? C10 C12 1.536(4) . ? C10 H10 1.0000 . ? C11 H11A 0.9800 . ? C11 H11B 0.9800 . ? C11 H11C 0.9800 . ? C12 H12A 0.9800 . ? C12 H12B 0.9800 . ? C12 H12C 0.9800 . ? C13 C15 1.529(4) . ? C13 C14 1.536(4) . ? C13 H13 1.0000 . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C14 H14C 0.9800 . ? C15 H15A 0.9800 . ? C15 H15B 0.9800 . ? C15 H15C 0.9800 . ? C16 C21 1.390(4) . ? C16 C17 1.400(4) . ? C17 C18 1.404(4) . ? C17 C25 1.519(4) . ? C18 C19 1.366(5) . ? C18 H18 0.9500 . ? C19 C20 1.366(5) . ? C19 H19 0.9500 . ? C20 C21 1.399(4) . ? C20 H20 0.9500 . ? C21 C22 1.510(4) . ? C22 C24 1.521(5) . ? C22 C23 1.534(5) . ? C22 H22 1.0000 . ? C23 H23A 0.9800 . ? C23 H23B 0.9800 . ? C23 H23C 0.9800 . ? C24 H24A 0.9800 . ? C24 H24B 0.9800 . ? C24 H24C 0.9800 . ? C25 C26 1.520(5) . ? C25 C27 1.534(5) . ? C25 H25 1.0000 . ? C26 H26A 0.9800 . ? C26 H26B 0.9800 . ? C26 H26C 0.9800 . ? C27 H27A 0.9800 . ? C27 H27B 0.9800 . ? C27 H27C 0.9800 . ? C28 H28 1.0000 . ? C29 C30 1.516(5) . ? C30 C33 1.438(8) . ? C30 C31 1.469(7) . ? C30 C32 1.659(10) . ? C31 H31A 0.9800 . ? C31 H31B 0.9800 . ? C31 H31C 0.9800 . ? C32 H32A 0.9800 . ? C32 H32B 0.9800 . ? C32 H32C 0.9800 . ? C33 H33A 0.9800 . ? C33 H33B 0.9800 . ? C33 H33C 0.9800 . ? C34 C35 1.505(4) . ? C34 H34A 0.9900 . ? C34 H34B 0.9900 . ? C35 H35A 0.9900 . ? C35 H35B 0.9900 . ? C37 C38 1.387(4) . ? C37 C42 1.410(5) . ? C38 C39 1.407(5) . ? C38 C46 1.508(5) . ? C39 C40 1.368(6) . ? C39 H39 0.9500 . ? C40 C41 1.370(6) . ? C40 H40 0.9500 . ? C41 C42 1.385(5) . ? C41 H41 0.9500 . ? C42 C43 1.508(5) . ? C43 C45 1.532(5) . ? C43 C44 1.540(6) . ? C43 H43 1.0000 . ? C44 H44A 0.9800 . ? C44 H44B 0.9800 . ? C44 H44C 0.9800 . ? C45 H45A 0.9800 . ? C45 H45B 0.9800 . ? C45 H45C 0.9800 . ? C46 C48 1.534(6) . ? C46 C47 1.548(5) . ? C46 H46 1.0000 . ? C47 H47A 0.9800 . ? C47 H47B 0.9800 . ? C47 H47C 0.9800 . ? C48 H48A 0.9800 . ? C48 H48B 0.9800 . ? C48 H48C 0.9800 . ? C49 C54 1.396(4) . ? C49 C50 1.402(4) . ? C50 C51 1.396(4) . ? C50 C58 1.514(4) . ? C51 C52 1.379(4) . ? C51 H51 0.9500 . ? C52 C53 1.376(4) . ? C52 H52 0.9500 . ? C53 C54 1.398(4) . ? C53 H53 0.9500 . ? C54 C55 1.508(4) . ? C55 C56 1.521(5) . ? C55 C57 1.521(4) . ? C55 H55 1.0000 . ? C56 H56A 0.9800 . ? C56 H56B 0.9800 . ? C56 H56C 0.9800 . ? C57 H57A 0.9800 . ? C57 H57B 0.9800 . ? C57 H57C 0.9800 . ? C58 C60 1.543(4) . ? C58 C59 1.549(5) . ? C58 H58 1.0000 . ? C59 H59A 0.9800 . ? C59 H59B 0.9800 . ? C59 H59C 0.9800 . ? C60 H60A 0.9800 . ? C60 H60B 0.9800 . ? C60 H60C 0.9800 . ? C61 H61 1.0000 . ? C62 C63 1.525(4) . ? C63 C64' 1.438(10) . ? C63 C65 1.454(13) . ? C63 C66 1.537(11) . ? C63 C65' 1.561(12) . ? C63 C64 1.629(10) . ? C63 C66' 1.614(11) . ? C64 H64A 0.9800 . ? C64 H64B 0.9800 . ? C64 H64C 0.9800 . ? C65 H65A 0.9800 . ? C65 H65B 0.9800 . ? C65 H65C 0.9800 . ? C66 H66A 0.9800 . ? C66 H66B 0.9800 . ? C66 H66C 0.9800 . ? C64' H64D 0.9800 . ? C64' H64E 0.9800 . ? C64' H64F 0.9800 . ? C65' H65D 0.9800 . ? C65' H65E 0.9800 . ? C65' H65F 0.9800 . ? C66' H66D 0.9800 . ? C66' H66E 0.9800 . ? C66' H66F 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C28 Pd1 C3 86.67(10) . . ? C28 Pd1 O1 100.89(10) . . ? C3 Pd1 O1 171.87(9) . . ? C28 Pd1 O2 161.77(10) . . ? C3 Pd1 O2 111.54(9) . . ? O1 Pd1 O2 60.98(8) . . ? C28 Pd1 C29 131.26(11) . . ? C3 Pd1 C29 142.03(11) . . ? O1 Pd1 C29 30.39(9) . . ? O2 Pd1 C29 30.59(10) . . ? C61 Pd2 C36 90.06(10) . . ? C61 Pd2 O3 102.22(9) . . ? C36 Pd2 O3 167.62(9) . . ? C61 Pd2 O4 162.51(9) . . ? C36 Pd2 O4 106.98(9) . . ? O3 Pd2 O4 60.66(7) . . ? C61 Pd2 C62 132.51(10) . . ? C36 Pd2 C62 137.15(10) . . ? O3 Pd2 C62 30.47(8) . . ? O4 Pd2 C62 30.21(8) . . ? C3 N1 C4 126.4(2) . . ? C3 N1 C1 111.8(2) . . ? C4 N1 C1 118.14(19) . . ? C3 N2 C16 127.0(2) . . ? C3 N2 C2 112.9(2) . . ? C16 N2 C2 120.1(2) . . ? C36 N3 C37 125.6(2) . . ? C36 N3 C34 112.0(2) . . ? C37 N3 C34 121.3(2) . . ? C36 N4 C49 125.9(2) . . ? C36 N4 C35 111.9(2) . . ? C49 N4 C35 120.8(2) . . ? C29 O1 Pd1 91.13(18) . . ? C29 O2 Pd1 87.37(19) . . ? C62 O3 Pd2 91.03(16) . . ? C62 O4 Pd2 88.65(17) . . ? N1 C1 C2 102.4(2) . . ? N1 C1 H1A 111.3 . . ? C2 C1 H1A 111.3 . . ? N1 C1 H1B 111.3 . . ? C2 C1 H1B 111.3 . . ? H1A C1 H1B 109.2 . . ? N2 C2 C1 101.4(2) . . ? N2 C2 H2A 111.5 . . ? C1 C2 H2A 111.5 . . ? N2 C2 H2B 111.5 . . ? C1 C2 H2B 111.5 . . ? H2A C2 H2B 109.3 . . ? N2 C3 N1 108.5(2) . . ? N2 C3 Pd1 122.47(18) . . ? N1 C3 Pd1 128.99(18) . . ? C9 C4 C5 122.6(2) . . ? C9 C4 N1 119.4(2) . . ? C5 C4 N1 117.8(2) . . ? C6 C5 C4 117.3(3) . . ? C6 C5 C13 119.5(3) . . ? C4 C5 C13 123.2(2) . . ? C7 C6 C5 120.7(3) . . ? C7 C6 H6 119.6 . . ? C5 C6 H6 119.6 . . ? C8 C7 C6 120.6(3) . . ? C8 C7 H7 119.7 . . ? C6 C7 H7 119.7 . . ? C7 C8 C9 121.6(3) . . ? C7 C8 H8 119.2 . . ? C9 C8 H8 119.2 . . ? C8 C9 C4 117.1(3) . . ? C8 C9 C10 119.1(3) . . ? C4 C9 C10 123.7(3) . . ? C9 C10 C11 112.6(3) . . ? C9 C10 C12 110.7(3) . . ? C11 C10 C12 111.2(3) . . ? C9 C10 H10 107.4 . . ? C11 C10 H10 107.4 . . ? C12 C10 H10 107.4 . . ? C10 C11 H11A 109.5 . . ? C10 C11 H11B 109.5 . . ? H11A C11 H11B 109.5 . . ? C10 C11 H11C 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? C10 C12 H12A 109.5 . . ? C10 C12 H12B 109.5 . . ? H12A C12 H12B 109.5 . . ? C10 C12 H12C 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? C5 C13 C15 112.9(2) . . ? C5 C13 C14 110.3(2) . . ? C15 C13 C14 110.1(2) . . ? C5 C13 H13 107.8 . . ? C15 C13 H13 107.8 . . ? C14 C13 H13 107.8 . . ? C13 C14 H14A 109.5 . . ? C13 C14 H14B 109.5 . . ? H14A C14 H14B 109.5 . . ? C13 C14 H14C 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? C13 C15 H15A 109.5 . . ? C13 C15 H15B 109.5 . . ? H15A C15 H15B 109.5 . . ? C13 C15 H15C 109.5 . . ? H15A C15 H15C 109.5 . . ? H15B C15 H15C 109.5 . . ? C21 C16 C17 122.8(3) . . ? C21 C16 N2 119.4(2) . . ? C17 C16 N2 117.7(2) . . ? C16 C17 C18 116.7(3) . . ? C16 C17 C25 123.1(3) . . ? C18 C17 C25 120.2(3) . . ? C19 C18 C17 121.5(3) . . ? C19 C18 H18 119.2 . . ? C17 C18 H18 119.2 . . ? C18 C19 C20 120.4(3) . . ? C18 C19 H19 119.8 . . ? C20 C19 H19 119.8 . . ? C19 C20 C21 121.3(3) . . ? C19 C20 H20 119.4 . . ? C21 C20 H20 119.4 . . ? C16 C21 C20 117.3(3) . . ? C16 C21 C22 123.4(2) . . ? C20 C21 C22 119.3(3) . . ? C21 C22 C24 111.7(3) . . ? C21 C22 C23 110.6(3) . . ? C24 C22 C23 111.3(3) . . ? C21 C22 H22 107.7 . . ? C24 C22 H22 107.7 . . ? C23 C22 H22 107.7 . . ? C22 C23 H23A 109.5 . . ? C22 C23 H23B 109.5 . . ? H23A C23 H23B 109.5 . . ? C22 C23 H23C 109.5 . . ? H23A C23 H23C 109.5 . . ? H23B C23 H23C 109.5 . . ? C22 C24 H24A 109.5 . . ? C22 C24 H24B 109.5 . . ? H24A C24 H24B 109.5 . . ? C22 C24 H24C 109.5 . . ? H24A C24 H24C 109.5 . . ? H24B C24 H24C 109.5 . . ? C26 C25 C17 112.0(3) . . ? C26 C25 C27 110.6(3) . . ? C17 C25 C27 110.7(3) . . ? C26 C25 H25 107.8 . . ? C17 C25 H25 107.8 . . ? C27 C25 H25 107.8 . . ? C25 C26 H26A 109.5 . . ? C25 C26 H26B 109.5 . . ? H26A C26 H26B 109.5 . . ? C25 C26 H26C 109.5 . . ? H26A C26 H26C 109.5 . . ? H26B C26 H26C 109.5 . . ? C25 C27 H27A 109.5 . . ? C25 C27 H27B 109.5 . . ? H27A C27 H27B 109.5 . . ? C25 C27 H27C 109.5 . . ? H27A C27 H27C 109.5 . . ? H27B C27 H27C 109.5 . . ? F2 C28 F1 104.6(2) . . ? F2 C28 Pd1 115.13(19) . . ? F1 C28 Pd1 108.23(17) . . ? F2 C28 H28 109.5 . . ? F1 C28 H28 109.5 . . ? Pd1 C28 H28 109.5 . . ? O1 C29 O2 120.5(3) . . ? O1 C29 C30 119.2(3) . . ? O2 C29 C30 120.2(4) . . ? O1 C29 Pd1 58.48(15) . . ? O2 C29 Pd1 62.03(16) . . ? C30 C29 Pd1 177.6(3) . . ? C33 C30 C31 125.5(5) . . ? C33 C30 C29 113.1(5) . . ? C31 C30 C29 114.2(4) . . ? C33 C30 C32 97.9(6) . . ? C31 C30 C32 97.1(6) . . ? C29 C30 C32 102.3(5) . . ? C30 C31 H31A 109.5 . . ? C30 C31 H31B 109.5 . . ? H31A C31 H31B 109.5 . . ? C30 C31 H31C 109.5 . . ? H31A C31 H31C 109.5 . . ? H31B C31 H31C 109.5 . . ? C30 C32 H32A 109.5 . . ? C30 C32 H32B 109.5 . . ? H32A C32 H32B 109.5 . . ? C30 C32 H32C 109.5 . . ? H32A C32 H32C 109.5 . . ? H32B C32 H32C 109.5 . . ? C30 C33 H33A 109.5 . . ? C30 C33 H33B 109.5 . . ? H33A C33 H33B 109.5 . . ? C30 C33 H33C 109.5 . . ? H33A C33 H33C 109.5 . . ? H33B C33 H33C 109.5 . . ? N3 C34 C35 101.1(2) . . ? N3 C34 H34A 111.5 . . ? C35 C34 H34A 111.5 . . ? N3 C34 H34B 111.5 . . ? C35 C34 H34B 111.5 . . ? H34A C34 H34B 109.4 . . ? N4 C35 C34 102.1(2) . . ? N4 C35 H35A 111.3 . . ? C34 C35 H35A 111.3 . . ? N4 C35 H35B 111.3 . . ? C34 C35 H35B 111.3 . . ? H35A C35 H35B 109.2 . . ? N4 C36 N3 107.9(2) . . ? N4 C36 Pd2 122.82(18) . . ? N3 C36 Pd2 128.94(18) . . ? C38 C37 C42 122.9(3) . . ? C38 C37 N3 119.4(3) . . ? C42 C37 N3 117.7(3) . . ? C37 C38 C39 116.8(4) . . ? C37 C38 C46 123.1(3) . . ? C39 C38 C46 120.2(3) . . ? C40 C39 C38 120.9(4) . . ? C40 C39 H39 119.5 . . ? C38 C39 H39 119.5 . . ? C39 C40 C41 121.3(3) . . ? C39 C40 H40 119.4 . . ? C41 C40 H40 119.4 . . ? C40 C41 C42 120.6(4) . . ? C40 C41 H41 119.7 . . ? C42 C41 H41 119.7 . . ? C41 C42 C37 117.5(4) . . ? C41 C42 C43 120.0(3) . . ? C37 C42 C43 122.6(3) . . ? C42 C43 C45 111.2(3) . . ? C42 C43 C44 112.9(3) . . ? C45 C43 C44 109.8(3) . . ? C42 C43 H43 107.6 . . ? C45 C43 H43 107.6 . . ? C44 C43 H43 107.6 . . ? C43 C44 H44A 109.5 . . ? C43 C44 H44B 109.5 . . ? H44A C44 H44B 109.5 . . ? C43 C44 H44C 109.5 . . ? H44A C44 H44C 109.5 . . ? H44B C44 H44C 109.5 . . ? C43 C45 H45A 109.5 . . ? C43 C45 H45B 109.5 . . ? H45A C45 H45B 109.5 . . ? C43 C45 H45C 109.5 . . ? H45A C45 H45C 109.5 . . ? H45B C45 H45C 109.5 . . ? C38 C46 C48 113.2(3) . . ? C38 C46 C47 109.7(4) . . ? C48 C46 C47 110.6(3) . . ? C38 C46 H46 107.7 . . ? C48 C46 H46 107.7 . . ? C47 C46 H46 107.7 . . ? C46 C47 H47A 109.5 . . ? C46 C47 H47B 109.5 . . ? H47A C47 H47B 109.5 . . ? C46 C47 H47C 109.5 . . ? H47A C47 H47C 109.5 . . ? H47B C47 H47C 109.5 . . ? C46 C48 H48A 109.5 . . ? C46 C48 H48B 109.5 . . ? H48A C48 H48B 109.5 . . ? C46 C48 H48C 109.5 . . ? H48A C48 H48C 109.5 . . ? H48B C48 H48C 109.5 . . ? C54 C49 C50 122.7(2) . . ? C54 C49 N4 118.4(2) . . ? C50 C49 N4 118.8(2) . . ? C51 C50 C49 117.7(3) . . ? C51 C50 C58 119.3(3) . . ? C49 C50 C58 123.0(2) . . ? C52 C51 C50 120.9(3) . . ? C52 C51 H51 119.6 . . ? C50 C51 H51 119.6 . . ? C53 C52 C51 120.1(3) . . ? C53 C52 H52 119.9 . . ? C51 C52 H52 119.9 . . ? C52 C53 C54 121.8(3) . . ? C52 C53 H53 119.1 . . ? C54 C53 H53 119.1 . . ? C49 C54 C53 116.8(3) . . ? C49 C54 C55 122.7(3) . . ? C53 C54 C55 120.5(3) . . ? C54 C55 C56 110.6(3) . . ? C54 C55 C57 114.5(3) . . ? C56 C55 C57 107.7(3) . . ? C54 C55 H55 108.0 . . ? C56 C55 H55 108.0 . . ? C57 C55 H55 108.0 . . ? C55 C56 H56A 109.5 . . ? C55 C56 H56B 109.5 . . ? H56A C56 H56B 109.5 . . ? C55 C56 H56C 109.5 . . ? H56A C56 H56C 109.5 . . ? H56B C56 H56C 109.5 . . ? C55 C57 H57A 109.5 . . ? C55 C57 H57B 109.5 . . ? H57A C57 H57B 109.5 . . ? C55 C57 H57C 109.5 . . ? H57A C57 H57C 109.5 . . ? H57B C57 H57C 109.5 . . ? C50 C58 C60 110.4(2) . . ? C50 C58 C59 111.8(3) . . ? C60 C58 C59 109.9(3) . . ? C50 C58 H58 108.2 . . ? C60 C58 H58 108.2 . . ? C59 C58 H58 108.2 . . ? C58 C59 H59A 109.5 . . ? C58 C59 H59B 109.5 . . ? H59A C59 H59B 109.5 . . ? C58 C59 H59C 109.5 . . ? H59A C59 H59C 109.5 . . ? H59B C59 H59C 109.5 . . ? C58 C60 H60A 109.5 . . ? C58 C60 H60B 109.5 . . ? H60A C60 H60B 109.5 . . ? C58 C60 H60C 109.5 . . ? H60A C60 H60C 109.5 . . ? H60B C60 H60C 109.5 . . ? F3 C61 F4 103.7(2) . . ? F3 C61 Pd2 115.74(18) . . ? F4 C61 Pd2 107.56(17) . . ? F3 C61 H61 109.9 . . ? F4 C61 H61 109.9 . . ? Pd2 C61 H61 109.9 . . ? O4 C62 O3 119.6(3) . . ? O4 C62 C63 120.1(3) . . ? O3 C62 C63 120.4(3) . . ? O4 C62 Pd2 61.15(14) . . ? O3 C62 Pd2 58.49(13) . . ? C63 C62 Pd2 176.7(3) . . ? C64' C63 C62 114.6(5) . . ? C65 C63 C62 115.2(6) . . ? C65 C63 C66 114.7(7) . . ? C62 C63 C66 108.5(4) . . ? C64' C63 C65' 115.3(7) . . ? C62 C63 C65' 106.5(5) . . ? C65 C63 C64 111.3(7) . . ? C62 C63 C64 105.3(4) . . ? C66 C63 C64 100.3(6) . . ? C64' C63 C66' 110.3(7) . . ? C62 C63 C66' 104.2(4) . . ? C65' C63 C66' 104.9(6) . . ? C63 C64 H64A 109.5 . . ? C63 C64 H64B 109.5 . . ? H64A C64 H64B 109.5 . . ? C63 C64 H64C 109.5 . . ? H64A C64 H64C 109.5 . . ? H64B C64 H64C 109.5 . . ? C63 C65 H65A 109.5 . . ? C63 C65 H65B 109.5 . . ? H65A C65 H65B 109.5 . . ? C63 C65 H65C 109.5 . . ? H65A C65 H65C 109.5 . . ? H65B C65 H65C 109.5 . . ? C63 C66 H66A 109.5 . . ? C63 C66 H66B 109.5 . . ? H66A C66 H66B 109.5 . . ? C63 C66 H66C 109.5 . . ? H66A C66 H66C 109.5 . . ? H66B C66 H66C 109.5 . . ? C63 C64' H64D 109.5 . . ? C63 C64' H64E 109.5 . . ? H64D C64' H64E 109.5 . . ? C63 C64' H64F 109.5 . . ? H64D C64' H64F 109.5 . . ? H64E C64' H64F 109.5 . . ? C63 C65' H65D 109.5 . . ? C63 C65' H65E 109.5 . . ? H65D C65' H65E 109.5 . . ? C63 C65' H65F 109.5 . . ? H65D C65' H65F 109.5 . . ? H65E C65' H65F 109.5 . . ? C63 C66' H66D 109.5 . . ? C63 C66' H66E 109.5 . . ? H66D C66' H66E 109.5 . . ? C63 C66' H66F 109.5 . . ? H66D C66' H66F 109.5 . . ? H66E C66' H66F 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C3 N1 C1 C2 15.0(3) . . . . ? C4 N1 C1 C2 174.9(2) . . . . ? C3 N2 C2 C1 14.5(3) . . . . ? C16 N2 C2 C1 -165.9(2) . . . . ? N1 C1 C2 N2 -16.3(3) . . . . ? C16 N2 C3 N1 174.7(2) . . . . ? C2 N2 C3 N1 -5.7(3) . . . . ? C16 N2 C3 Pd1 -8.1(4) . . . . ? C2 N2 C3 Pd1 171.49(18) . . . . ? C4 N1 C3 N2 -164.4(2) . . . . ? C1 N1 C3 N2 -6.4(3) . . . . ? C4 N1 C3 Pd1 18.7(4) . . . . ? C1 N1 C3 Pd1 176.67(19) . . . . ? C3 N1 C4 C9 63.9(3) . . . . ? C1 N1 C4 C9 -92.8(3) . . . . ? C3 N1 C4 C5 -120.7(3) . . . . ? C1 N1 C4 C5 82.6(3) . . . . ? C9 C4 C5 C6 -1.5(4) . . . . ? N1 C4 C5 C6 -176.6(2) . . . . ? C9 C4 C5 C13 176.6(2) . . . . ? N1 C4 C5 C13 1.4(4) . . . . ? C4 C5 C6 C7 -0.2(4) . . . . ? C13 C5 C6 C7 -178.2(3) . . . . ? C5 C6 C7 C8 1.0(5) . . . . ? C6 C7 C8 C9 -0.2(5) . . . . ? C7 C8 C9 C4 -1.3(5) . . . . ? C7 C8 C9 C10 174.7(3) . . . . ? C5 C4 C9 C8 2.2(4) . . . . ? N1 C4 C9 C8 177.3(2) . . . . ? C5 C4 C9 C10 -173.7(3) . . . . ? N1 C4 C9 C10 1.5(4) . . . . ? C8 C9 C10 C11 58.7(4) . . . . ? C4 C9 C10 C11 -125.5(3) . . . . ? C8 C9 C10 C12 -66.5(4) . . . . ? C4 C9 C10 C12 109.3(3) . . . . ? C6 C5 C13 C15 -54.0(3) . . . . ? C4 C5 C13 C15 128.1(3) . . . . ? C6 C5 C13 C14 69.6(3) . . . . ? C4 C5 C13 C14 -108.3(3) . . . . ? C3 N2 C16 C21 87.7(3) . . . . ? C2 N2 C16 C21 -91.9(3) . . . . ? C3 N2 C16 C17 -96.1(3) . . . . ? C2 N2 C16 C17 84.4(3) . . . . ? C21 C16 C17 C18 -1.0(4) . . . . ? N2 C16 C17 C18 -177.0(3) . . . . ? C21 C16 C17 C25 178.6(3) . . . . ? N2 C16 C17 C25 2.5(4) . . . . ? C16 C17 C18 C19 0.5(5) . . . . ? C25 C17 C18 C19 -179.0(3) . . . . ? C17 C18 C19 C20 0.1(6) . . . . ? C18 C19 C20 C21 -0.4(6) . . . . ? C17 C16 C21 C20 0.7(4) . . . . ? N2 C16 C21 C20 176.7(3) . . . . ? C17 C16 C21 C22 179.8(3) . . . . ? N2 C16 C21 C22 -4.2(4) . . . . ? C19 C20 C21 C16 0.0(5) . . . . ? C19 C20 C21 C22 -179.1(3) . . . . ? C16 C21 C22 C24 121.2(3) . . . . ? C20 C21 C22 C24 -59.6(4) . . . . ? C16 C21 C22 C23 -114.2(3) . . . . ? C20 C21 C22 C23 64.9(4) . . . . ? C16 C17 C25 C26 122.1(3) . . . . ? C18 C17 C25 C26 -58.4(4) . . . . ? C16 C17 C25 C27 -114.0(3) . . . . ? C18 C17 C25 C27 65.5(4) . . . . ? Pd1 O1 C29 O2 0.6(4) . . . . ? Pd1 O1 C29 C30 -179.1(5) . . . . ? Pd1 O2 C29 O1 -0.6(4) . . . . ? Pd1 O2 C29 C30 179.1(5) . . . . ? O1 C29 C30 C33 151.6(6) . . . . ? O2 C29 C30 C33 -28.2(9) . . . . ? O1 C29 C30 C31 -0.5(9) . . . . ? O2 C29 C30 C31 179.8(6) . . . . ? O1 C29 C30 C32 -104.2(5) . . . . ? O2 C29 C30 C32 76.1(6) . . . . ? C36 N3 C34 C35 19.0(3) . . . . ? C37 N3 C34 C35 -172.2(3) . . . . ? C36 N4 C35 C34 18.6(4) . . . . ? C49 N4 C35 C34 -174.1(3) . . . . ? N3 C34 C35 N4 -20.8(3) . . . . ? C49 N4 C36 N3 -173.7(2) . . . . ? C35 N4 C36 N3 -7.2(3) . . . . ? C49 N4 C36 Pd2 12.5(4) . . . . ? C35 N4 C36 Pd2 179.0(2) . . . . ? C37 N3 C36 N4 -176.4(3) . . . . ? C34 N3 C36 N4 -8.1(3) . . . . ? C37 N3 C36 Pd2 -3.0(4) . . . . ? C34 N3 C36 Pd2 165.3(2) . . . . ? C36 N3 C37 C38 75.9(4) . . . . ? C34 N3 C37 C38 -91.3(3) . . . . ? C36 N3 C37 C42 -105.7(3) . . . . ? C34 N3 C37 C42 87.1(3) . . . . ? C42 C37 C38 C39 2.7(4) . . . . ? N3 C37 C38 C39 -179.0(3) . . . . ? C42 C37 C38 C46 -176.0(3) . . . . ? N3 C37 C38 C46 2.3(4) . . . . ? C37 C38 C39 C40 -1.0(5) . . . . ? C46 C38 C39 C40 177.8(3) . . . . ? C38 C39 C40 C41 -0.8(6) . . . . ? C39 C40 C41 C42 1.0(6) . . . . ? C40 C41 C42 C37 0.6(5) . . . . ? C40 C41 C42 C43 -178.7(3) . . . . ? C38 C37 C42 C41 -2.6(4) . . . . ? N3 C37 C42 C41 179.1(3) . . . . ? C38 C37 C42 C43 176.8(3) . . . . ? N3 C37 C42 C43 -1.6(4) . . . . ? C41 C42 C43 C45 81.2(4) . . . . ? C37 C42 C43 C45 -98.1(4) . . . . ? C41 C42 C43 C44 -42.7(4) . . . . ? C37 C42 C43 C44 138.0(3) . . . . ? C37 C38 C46 C48 -122.9(3) . . . . ? C39 C38 C46 C48 58.4(4) . . . . ? C37 C38 C46 C47 113.0(4) . . . . ? C39 C38 C46 C47 -65.7(4) . . . . ? C36 N4 C49 C54 -97.0(3) . . . . ? C35 N4 C49 C54 97.6(3) . . . . ? C36 N4 C49 C50 86.2(3) . . . . ? C35 N4 C49 C50 -79.2(3) . . . . ? C54 C49 C50 C51 1.6(4) . . . . ? N4 C49 C50 C51 178.3(2) . . . . ? C54 C49 C50 C58 -176.6(2) . . . . ? N4 C49 C50 C58 0.0(4) . . . . ? C49 C50 C51 C52 -0.4(4) . . . . ? C58 C50 C51 C52 177.9(3) . . . . ? C50 C51 C52 C53 -0.4(4) . . . . ? C51 C52 C53 C54 0.2(5) . . . . ? C50 C49 C54 C53 -1.8(4) . . . . ? N4 C49 C54 C53 -178.5(2) . . . . ? C50 C49 C54 C55 176.4(3) . . . . ? N4 C49 C54 C55 -0.2(4) . . . . ? C52 C53 C54 C49 0.9(4) . . . . ? C52 C53 C54 C55 -177.4(3) . . . . ? C49 C54 C55 C56 -90.8(4) . . . . ? C53 C54 C55 C56 87.4(4) . . . . ? C49 C54 C55 C57 147.3(3) . . . . ? C53 C54 C55 C57 -34.5(4) . . . . ? C51 C50 C58 C60 -72.3(3) . . . . ? C49 C50 C58 C60 105.9(3) . . . . ? C51 C50 C58 C59 50.3(3) . . . . ? C49 C50 C58 C59 -131.5(3) . . . . ? Pd2 O4 C62 O3 2.9(3) . . . . ? Pd2 O4 C62 C63 -176.4(3) . . . . ? Pd2 O3 C62 O4 -3.0(3) . . . . ? Pd2 O3 C62 C63 176.4(3) . . . . ? O4 C62 C63 C64' 167.1(7) . . . . ? O3 C62 C63 C64' -12.2(8) . . . . ? O4 C62 C63 C65 3.9(8) . . . . ? O3 C62 C63 C65 -175.5(7) . . . . ? O4 C62 C63 C66 -126.3(6) . . . . ? O3 C62 C63 C66 54.3(7) . . . . ? O4 C62 C63 C65' 38.4(7) . . . . ? O3 C62 C63 C65' -141.0(6) . . . . ? O4 C62 C63 C64 127.0(5) . . . . ? O3 C62 C63 C64 -52.4(6) . . . . ? O4 C62 C63 C66' -72.2(5) . . . . ? O3 C62 C63 C66' 108.4(5) . . . . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A C1 H1A F4 0.99 2.35 3.142(3) 137.0 1_455 C2 H2B O3 0.99 2.41 3.258(3) 142.8 1_455 C35 H35A F1 0.99 2.31 2.939(3) 120.5 . _refine_diff_density_max 1.199 _refine_diff_density_min -0.777 _refine_diff_density_rms 0.060 _shelxl_version_number 2013-4 _shelx_res_file ; TITL mo_d8v19200_0m_a.res in P2(1)/c CELL 0.71073 16.8572 12.4408 34.1009 90 103.498 90 ZERR 8 0.0006 0.0004 0.0013 0 0.001 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H N O F Pd UNIT 264 384 16 16 16 8 OMIT 0 1 2 OMIT 1 0 2 OMIT 1 1 0 OMIT 0 1 1 OMIT 2 2 1 OMIT 2 1 0 OMIT 1 1 1 OMIT -1 0 2 OMIT -3.00 52.00 L.S. 10 ACTA BOND $H FMAP 2 PLAN 20 LIST 4 simu 0.004 c64 c65 c66 c64' c65' c66' dfix 1.55 0.02 c30 c31 c30 c32 c30 c33 simu 0.004 c31 c32 c33 c30 size 0.18 0.15 0.12 wpdb -1 mpla c49 > c54 mpla c37 > c42 mpla c16 > c21 mpla c4 > c9 htab conf EQIV $1 x-1, y, z HTAB C1 F4_$1 HTAB C2 O3_$1 HTAB C35 F1 TEMP -80.62 WGHT 0.043900 5.431100 EXTI 0.001035 FVAR 0.25611 PD1 6 0.444347 0.823028 0.390050 11.00000 0.02775 0.03942 = 0.02928 0.00326 0.00949 -0.00242 PD2 6 0.950952 0.619452 0.389347 11.00000 0.02591 0.03300 = 0.03285 0.00018 0.01110 0.00098 F1 5 0.597108 0.785304 0.435730 11.00000 0.02666 0.06039 = 0.05446 -0.00339 0.00999 0.00516 F2 5 0.519311 0.646493 0.436014 11.00000 0.06058 0.04088 = 0.06228 0.00844 -0.00224 0.00326 F3 5 0.975111 0.764879 0.454883 11.00000 0.07020 0.06653 = 0.05497 -0.02149 0.02581 -0.01222 F4 5 1.077349 0.744611 0.427414 11.00000 0.03080 0.05208 = 0.07437 -0.01056 0.00436 -0.00140 N1 3 0.340725 0.748789 0.445586 11.00000 0.02785 0.03704 = 0.02850 -0.00127 0.00954 -0.00542 N2 3 0.299830 0.690423 0.384306 11.00000 0.02719 0.04272 = 0.02533 0.00136 0.00633 -0.00429 N3 3 0.797370 0.750780 0.375083 11.00000 0.02906 0.03443 = 0.04493 0.01127 0.01266 0.00425 N4 3 0.787988 0.598210 0.404153 11.00000 0.02909 0.03232 = 0.04857 0.00959 0.01931 0.00580 O1 4 0.528178 0.901151 0.362206 11.00000 0.03925 0.06719 = 0.04599 0.01291 0.01677 -0.00661 O2 4 0.397661 0.919875 0.335867 11.00000 0.04525 0.08858 = 0.04976 0.02854 0.01258 0.00448 O3 4 1.059258 0.545637 0.379866 11.00000 0.03169 0.04674 = 0.05541 -0.01616 0.01652 -0.00210 O4 4 0.941384 0.470388 0.354214 11.00000 0.03482 0.05555 = 0.06811 -0.02293 0.01649 -0.00543 C1 1 0.264594 0.691099 0.446106 11.00000 0.03105 0.05080 = 0.03476 -0.00145 0.01244 -0.01132 AFIX 23 H1A 2 0.220171 0.741725 0.447743 11.00000 -1.20000 H1B 2 0.272566 0.640103 0.468980 11.00000 -1.20000 AFIX 0 C2 1 0.246627 0.632258 0.405962 11.00000 0.03557 0.04996 = 0.03470 0.00155 0.01105 -0.01102 AFIX 23 H2A 2 0.261574 0.555307 0.409441 11.00000 -1.20000 H2B 2 0.188424 0.638589 0.391845 11.00000 -1.20000 AFIX 0 C3 1 0.355170 0.751204 0.408492 11.00000 0.02445 0.03174 = 0.02770 0.00341 0.00362 0.00223 C4 1 0.373028 0.821537 0.478107 11.00000 0.02795 0.03958 = 0.03180 -0.00467 0.01142 -0.00338 C5 1 0.420266 0.777903 0.514116 11.00000 0.03482 0.04342 = 0.03124 -0.00251 0.01111 -0.00270 C6 1 0.447845 0.848825 0.546441 11.00000 0.04765 0.06058 = 0.03032 -0.00807 0.00352 -0.00219 AFIX 43 H6 2 0.479773 0.822141 0.571239 11.00000 -1.20000 AFIX 0 C7 1 0.429069 0.957077 0.542598 11.00000 0.05925 0.05643 = 0.04650 -0.02195 0.00616 -0.00379 AFIX 43 H7 2 0.448914 1.004210 0.564622 11.00000 -1.20000 AFIX 0 C8 1 0.381935 0.997085 0.507185 11.00000 0.05468 0.04235 = 0.06062 -0.01511 0.01042 0.00239 AFIX 43 H8 2 0.369609 1.071685 0.505220 11.00000 -1.20000 AFIX 0 C9 1 0.351735 0.930774 0.474036 11.00000 0.03537 0.04196 = 0.04265 -0.00479 0.00918 0.00103 C10 1 0.294076 0.977728 0.437115 11.00000 0.04539 0.04370 = 0.05515 -0.00145 0.00454 0.00916 AFIX 13 H10 2 0.281961 0.919799 0.416239 11.00000 -1.20000 AFIX 0 C11 1 0.331762 1.071799 0.418954 11.00000 0.07302 0.06168 = 0.07121 0.01516 0.00424 0.00307 AFIX 137 H11A 2 0.342331 1.131342 0.438290 11.00000 -1.50000 H11B 2 0.293943 1.095574 0.394092 11.00000 -1.50000 H11C 2 0.383155 1.048743 0.412847 11.00000 -1.50000 AFIX 0 C12 1 0.212851 1.010082 0.446830 11.00000 0.05166 0.08574 = 0.09499 0.00567 0.01221 0.02305 AFIX 137 H12A 2 0.190524 0.948740 0.458742 11.00000 -1.50000 H12B 2 0.174167 1.032057 0.421974 11.00000 -1.50000 H12C 2 0.222029 1.070095 0.465974 11.00000 -1.50000 AFIX 0 C13 1 0.439815 0.659192 0.519669 11.00000 0.04390 0.04582 = 0.02939 0.00186 0.00562 0.00051 AFIX 13 H13 2 0.421619 0.623612 0.492771 11.00000 -1.20000 AFIX 0 C14 1 0.391941 0.608616 0.548198 11.00000 0.06162 0.06377 = 0.04869 0.01606 0.01556 -0.00208 AFIX 137 H14A 2 0.409777 0.640694 0.575064 11.00000 -1.50000 H14B 2 0.401997 0.530982 0.549952 11.00000 -1.50000 H14C 2 0.333511 0.621909 0.537778 11.00000 -1.50000 AFIX 0 C15 1 0.531000 0.637260 0.535116 11.00000 0.04937 0.06157 = 0.03976 0.00541 0.00468 0.00990 AFIX 137 H15A 2 0.560859 0.668221 0.516373 11.00000 -1.50000 H15B 2 0.540400 0.559505 0.537090 11.00000 -1.50000 H15C 2 0.550199 0.669993 0.561788 11.00000 -1.50000 AFIX 0 C16 1 0.288716 0.677139 0.341277 11.00000 0.03074 0.05103 = 0.02539 0.00022 0.00224 -0.00762 C17 1 0.229727 0.740920 0.316056 11.00000 0.03724 0.05802 = 0.03658 0.00615 0.00104 -0.00310 C18 1 0.217222 0.723083 0.274414 11.00000 0.05712 0.07903 = 0.03389 0.01406 -0.00629 0.00248 AFIX 43 H18 2 0.178030 0.765196 0.256285 11.00000 -1.20000 AFIX 0 C19 1 0.260104 0.646579 0.259367 11.00000 0.07596 0.08480 = 0.02654 0.00023 0.00431 -0.00580 AFIX 43 H19 2 0.250535 0.636256 0.231046 11.00000 -1.20000 AFIX 0 C20 1 0.316680 0.584803 0.284799 11.00000 0.05881 0.07867 = 0.03020 -0.00549 0.00941 0.00126 AFIX 43 H20 2 0.345719 0.531580 0.273858 11.00000 -1.20000 AFIX 0 C21 1 0.332699 0.598379 0.326650 11.00000 0.03838 0.05840 = 0.02887 -0.00187 0.00597 -0.00180 C22 1 0.396683 0.529190 0.353482 11.00000 0.04653 0.06870 = 0.03147 -0.00819 0.00336 0.01378 AFIX 13 H22 2 0.397760 0.548220 0.382092 11.00000 -1.20000 AFIX 0 C23 1 0.481423 0.553226 0.346308 11.00000 0.04594 0.12867 = 0.05805 -0.01660 0.01288 0.01736 AFIX 137 H23A 2 0.482918 0.532116 0.318803 11.00000 -1.50000 H23B 2 0.522695 0.512606 0.365655 11.00000 -1.50000 H23C 2 0.492796 0.630312 0.349883 11.00000 -1.50000 AFIX 0 C24 1 0.376141 0.410307 0.347907 11.00000 0.09946 0.06662 = 0.05816 -0.00595 -0.00519 0.02037 AFIX 137 H24A 2 0.323228 0.396665 0.354221 11.00000 -1.50000 H24B 2 0.418383 0.367959 0.366007 11.00000 -1.50000 H24C 2 0.373575 0.389688 0.319902 11.00000 -1.50000 AFIX 0 C25 1 0.180054 0.825399 0.331873 11.00000 0.04421 0.06862 = 0.04914 0.00857 -0.00035 0.01097 AFIX 13 H25 2 0.200202 0.828449 0.361855 11.00000 -1.20000 AFIX 0 C26 1 0.190518 0.936507 0.315255 11.00000 0.05883 0.06560 = 0.11598 0.01767 0.01262 0.00988 AFIX 137 H26A 2 0.248725 0.953976 0.320409 11.00000 -1.50000 H26B 2 0.162755 0.989743 0.328502 11.00000 -1.50000 H26C 2 0.166820 0.937449 0.286139 11.00000 -1.50000 AFIX 0 C27 1 0.089595 0.793893 0.322553 11.00000 0.04776 0.09802 = 0.07806 0.02487 0.01438 0.01162 AFIX 137 H27A 2 0.058900 0.848042 0.333774 11.00000 -1.50000 H27B 2 0.083730 0.723755 0.334651 11.00000 -1.50000 H27C 2 0.068371 0.789756 0.293280 11.00000 -1.50000 AFIX 0 C28 1 0.518571 0.756165 0.436304 11.00000 0.02969 0.04374 = 0.04000 -0.00001 0.01029 0.00271 AFIX 13 H28 2 0.505513 0.782217 0.461820 11.00000 -1.20000 AFIX 0 C29 1 0.471028 0.939230 0.335462 11.00000 0.05296 0.08345 = 0.05202 0.02345 0.02410 -0.00041 C30 1 0.490968 1.008471 0.302452 11.00000 0.11028 0.20427 = 0.12130 0.11435 0.04749 0.00570 C31 1 0.578695 1.024333 0.305945 11.00000 0.12748 0.23596 = 0.16190 0.11265 0.08305 -0.00857 AFIX 137 H31A 2 0.603661 0.955934 0.301134 11.00000 -1.50000 H31B 2 0.604255 1.050333 0.333081 11.00000 -1.50000 H31C 2 0.586694 1.077315 0.285952 11.00000 -1.50000 AFIX 0 C32 1 0.470674 1.131214 0.316413 11.00000 0.17346 0.19832 = 0.17876 0.10981 0.03223 -0.02745 AFIX 137 H32A 2 0.472214 1.182068 0.294656 11.00000 -1.50000 H32B 2 0.511492 1.151899 0.340718 11.00000 -1.50000 H32C 2 0.416326 1.132192 0.322113 11.00000 -1.50000 AFIX 0 C33 1 0.429577 1.003676 0.265286 11.00000 0.19628 0.21665 = 0.07674 0.07655 0.03074 -0.00748 AFIX 137 H33A 2 0.435621 0.936722 0.251124 11.00000 -1.50000 H33B 2 0.435920 1.065117 0.248294 11.00000 -1.50000 H33C 2 0.375361 1.005921 0.271116 11.00000 -1.50000 AFIX 0 C34 1 0.708954 0.740472 0.373008 11.00000 0.03077 0.04513 = 0.07018 0.01611 0.01796 0.00721 AFIX 23 H34A 2 0.678066 0.721101 0.345518 11.00000 -1.20000 H34B 2 0.686250 0.807480 0.381618 11.00000 -1.20000 AFIX 0 C35 1 0.708642 0.650433 0.402433 11.00000 0.03885 0.04716 = 0.09300 0.02476 0.03345 0.01650 AFIX 23 H35A 2 0.705268 0.678286 0.429191 11.00000 -1.20000 H35B 2 0.662780 0.600275 0.392452 11.00000 -1.20000 AFIX 0 C36 1 0.838948 0.662475 0.390538 11.00000 0.03026 0.03149 = 0.02968 -0.00026 0.00890 0.00112 C37 1 0.828772 0.837584 0.355254 11.00000 0.02878 0.04145 = 0.05331 0.02018 0.00932 0.00583 C38 1 0.837280 0.823720 0.316089 11.00000 0.03983 0.06856 = 0.05035 0.02597 0.00812 -0.00002 C39 1 0.869509 0.910822 0.298559 11.00000 0.05887 0.09149 = 0.07010 0.04122 0.02169 0.00023 AFIX 43 H39 2 0.877145 0.904358 0.271925 11.00000 -1.20000 AFIX 0 C40 1 0.890003 1.004688 0.319324 11.00000 0.06407 0.05988 = 0.12001 0.04927 0.02390 -0.00267 AFIX 43 H40 2 0.912354 1.062044 0.306976 11.00000 -1.20000 AFIX 0 C41 1 0.878929 1.017626 0.357599 11.00000 0.06354 0.04168 = 0.11543 0.02508 0.02737 0.00549 AFIX 43 H41 2 0.892841 1.084025 0.371228 11.00000 -1.20000 AFIX 0 C42 1 0.847653 0.934843 0.376606 11.00000 0.04097 0.03496 = 0.08632 0.01780 0.01451 0.00749 C43 1 0.834180 0.951219 0.418375 11.00000 0.08428 0.03782 = 0.08665 -0.00269 0.02766 0.00484 AFIX 13 H43 2 0.829971 0.878567 0.430272 11.00000 -1.20000 AFIX 0 C44 1 0.905161 1.011015 0.446559 11.00000 0.10508 0.05728 = 0.11192 -0.02211 0.01062 0.00981 AFIX 137 H44A 2 0.956652 0.974689 0.446363 11.00000 -1.50000 H44B 2 0.896770 1.011187 0.474045 11.00000 -1.50000 H44C 2 0.907228 1.085219 0.437203 11.00000 -1.50000 AFIX 0 C45 1 0.753861 1.010477 0.416959 11.00000 0.08388 0.05500 = 0.15126 -0.02042 0.05252 -0.00004 AFIX 137 H45A 2 0.752747 1.077475 0.401725 11.00000 -1.50000 H45B 2 0.749523 1.026953 0.444484 11.00000 -1.50000 H45C 2 0.707951 0.964898 0.403763 11.00000 -1.50000 AFIX 0 C46 1 0.812240 0.722297 0.292202 11.00000 0.06111 0.09650 = 0.04163 0.00877 0.01159 -0.02085 AFIX 13 H46 2 0.793619 0.669572 0.310297 11.00000 -1.20000 AFIX 0 C47 1 0.738984 0.746120 0.256434 11.00000 0.07584 0.18932 = 0.06728 0.00272 -0.01652 -0.02055 AFIX 137 H47A 2 0.694637 0.778287 0.266607 11.00000 -1.50000 H47B 2 0.719982 0.678986 0.242300 11.00000 -1.50000 H47C 2 0.755967 0.796166 0.237756 11.00000 -1.50000 AFIX 0 C48 1 0.882155 0.670131 0.277230 11.00000 0.09275 0.10795 = 0.05934 -0.00944 0.02946 -0.02008 AFIX 137 H48A 2 0.897949 0.717111 0.257269 11.00000 -1.50000 H48B 2 0.864170 0.600563 0.264810 11.00000 -1.50000 H48C 2 0.929026 0.659382 0.300043 11.00000 -1.50000 AFIX 0 C49 1 0.809751 0.500105 0.426426 11.00000 0.02891 0.03248 = 0.04658 0.00814 0.01880 0.00413 C50 1 0.837788 0.505592 0.468447 11.00000 0.03015 0.03520 = 0.04684 0.00567 0.01741 -0.00144 C51 1 0.856325 0.409059 0.489446 11.00000 0.03781 0.04492 = 0.04707 0.01112 0.01253 0.00121 AFIX 43 H51 2 0.875824 0.410271 0.517926 11.00000 -1.20000 AFIX 0 C52 1 0.846709 0.311974 0.469398 11.00000 0.05135 0.03880 = 0.05955 0.01705 0.01588 0.00725 AFIX 43 H52 2 0.859926 0.246941 0.484070 11.00000 -1.20000 AFIX 0 C53 1 0.818002 0.309080 0.428175 11.00000 0.05812 0.03011 = 0.06222 0.00105 0.01969 0.00368 AFIX 43 H53 2 0.811567 0.241522 0.414820 11.00000 -1.20000 AFIX 0 C54 1 0.798047 0.402880 0.405410 11.00000 0.04068 0.03742 = 0.04754 0.00253 0.02061 0.00387 C55 1 0.763348 0.396762 0.360514 11.00000 0.06664 0.04831 = 0.04804 -0.00052 0.02315 0.00432 AFIX 13 H55 2 0.776572 0.465604 0.348301 11.00000 -1.20000 AFIX 0 C56 1 0.670967 0.385608 0.351225 11.00000 0.07200 0.18238 = 0.05031 -0.01921 0.00203 0.04144 AFIX 137 H56A 2 0.656407 0.320594 0.364185 11.00000 -1.50000 H56B 2 0.649586 0.380441 0.321987 11.00000 -1.50000 H56C 2 0.647400 0.448604 0.361520 11.00000 -1.50000 AFIX 0 C57 1 0.796549 0.304758 0.339709 11.00000 0.07198 0.06062 = 0.07355 -0.02641 0.03236 -0.01204 AFIX 137 H57A 2 0.856253 0.304254 0.348102 11.00000 -1.50000 H57B 2 0.779619 0.314277 0.310414 11.00000 -1.50000 H57C 2 0.775175 0.236446 0.347204 11.00000 -1.50000 AFIX 0 C58 1 0.846339 0.610290 0.491689 11.00000 0.04902 0.04169 = 0.04963 -0.00028 0.01861 -0.00496 AFIX 13 H58 2 0.841031 0.670823 0.471952 11.00000 -1.20000 AFIX 0 C59 1 0.930576 0.619599 0.521729 11.00000 0.07002 0.06592 = 0.06144 -0.00661 0.00520 -0.01567 AFIX 137 H59A 2 0.935015 0.564732 0.542751 11.00000 -1.50000 H59B 2 0.936106 0.691104 0.534128 11.00000 -1.50000 H59C 2 0.973892 0.608850 0.507311 11.00000 -1.50000 AFIX 0 C60 1 0.777685 0.621170 0.514465 11.00000 0.08145 0.05924 = 0.07894 -0.01403 0.04843 -0.00529 AFIX 137 H60A 2 0.724661 0.612002 0.495499 11.00000 -1.50000 H60B 2 0.780336 0.692505 0.526895 11.00000 -1.50000 H60C 2 0.784452 0.565915 0.535468 11.00000 -1.50000 AFIX 0 C61 1 0.993248 0.750863 0.418210 11.00000 0.02887 0.03899 = 0.04048 -0.00097 0.00627 0.00176 AFIX 13 H61 2 0.974833 0.814880 0.400718 11.00000 -1.20000 AFIX 0 C62 1 1.017690 0.472214 0.358645 11.00000 0.03783 0.05073 = 0.05052 -0.01457 0.01724 -0.00127 C63 1 1.059535 0.387333 0.338266 11.00000 0.04684 0.08017 = 0.07394 -0.04139 0.02031 0.00309 PART 1 C64 1 1.114280 0.454490 0.313140 10.50000 0.08331 0.09657 = 0.07985 -0.02582 0.05614 -0.00172 AFIX 137 H64A 2 1.147361 0.404428 0.301482 10.50000 -1.50000 H64B 2 1.150172 0.504333 0.331337 10.50000 -1.50000 H64C 2 1.078247 0.495114 0.291483 10.50000 -1.50000 AFIX 0 C65 1 1.004991 0.312541 0.312322 10.50000 0.08444 0.09373 = 0.11908 -0.06115 0.02617 0.00459 AFIX 137 H65A 2 0.976723 0.268602 0.328663 10.50000 -1.50000 H65B 2 1.036656 0.265827 0.298546 10.50000 -1.50000 H65C 2 0.964833 0.352785 0.292270 10.50000 -1.50000 AFIX 0 C66 1 1.127281 0.334131 0.370485 10.50000 0.10501 0.09471 = 0.10959 -0.03625 0.03524 0.03977 AFIX 137 H66A 2 1.103220 0.299428 0.390771 10.50000 -1.50000 H66B 2 1.166444 0.388927 0.383482 10.50000 -1.50000 H66C 2 1.155362 0.280125 0.357741 10.50000 -1.50000 PART 2 AFIX 0 C64' 1 1.143041 0.410924 0.338238 10.50000 0.07818 0.09861 = 0.11276 -0.04288 0.04415 0.01346 AFIX 137 H64D 2 1.145976 0.480665 0.325289 10.50000 -1.50000 H64E 2 1.164407 0.354839 0.323332 10.50000 -1.50000 H64F 2 1.175643 0.413344 0.366073 10.50000 -1.50000 AFIX 0 C65' 1 1.002210 0.366507 0.295886 10.50000 0.07305 0.11150 = 0.08401 -0.05269 0.02361 0.01306 AFIX 137 H65D 2 0.995358 0.433260 0.280197 10.50000 -1.50000 H65E 2 0.948915 0.341773 0.299128 10.50000 -1.50000 H65F 2 1.026374 0.311417 0.281732 10.50000 -1.50000 AFIX 0 C66' 1 1.054264 0.279010 0.363562 10.50000 0.10037 0.07964 = 0.11839 -0.03411 0.02851 0.03093 AFIX 137 H66D 2 1.080327 0.219805 0.352343 10.50000 -1.50000 H66E 2 0.996922 0.261248 0.361863 10.50000 -1.50000 H66F 2 1.082342 0.290192 0.391844 10.50000 -1.50000 PART 0 AFIX 0 HKLF 4 REM mo_d8v19200_0m_a.res in P2(1)/c REM R1 = 0.0342 for 11220 Fo > 4sig(Fo) and 0.0465 for all 13640 data REM 774 parameters refined using 51 restraints END WGHT 0.0411 5.4323 REM Instructions for potential hydrogen bonds HTAB C1 F4_$1 HTAB C2 O3_$1 HTAB C35 F1 REM Highest difference peak 1.199, deepest hole -0.777, 1-sigma level 0.060 Q1 1 0.5067 0.8823 0.2686 11.00000 0.05 1.20 Q2 1 0.4920 1.0316 0.3072 11.00000 0.05 0.67 Q3 1 0.4864 0.9402 0.2923 11.00000 0.05 0.41 Q4 1 1.0878 0.2977 0.3670 11.00000 0.05 0.32 Q5 1 0.4482 0.9365 0.3899 11.00000 0.05 0.32 Q6 1 0.4498 1.1435 0.3176 11.00000 0.05 0.32 Q7 1 1.0250 0.2806 0.3369 11.00000 0.05 0.31 Q8 1 0.3760 0.9959 0.2614 11.00000 0.05 0.30 Q9 1 0.9452 0.7262 0.3908 11.00000 0.05 0.30 Q10 1 0.8124 0.5065 0.4456 11.00000 0.05 0.28 Q11 1 0.2756 0.6664 0.3926 11.00000 0.05 0.27 Q12 1 0.8796 0.6210 0.5075 11.00000 0.05 0.27 Q13 1 0.4258 0.7137 0.5152 11.00000 0.05 0.27 Q14 1 0.7184 0.3875 0.3550 11.00000 0.05 0.27 Q15 1 1.0379 0.4257 0.3530 11.00000 0.05 0.27 Q16 1 0.6672 0.6781 0.3300 11.00000 0.05 0.26 Q17 1 0.2492 0.6582 0.4300 11.00000 0.05 0.26 Q18 1 0.2046 0.7850 0.3233 11.00000 0.05 0.26 Q19 1 0.3002 0.6812 0.3631 11.00000 0.05 0.26 Q20 1 0.5319 0.6240 0.4114 11.00000 0.05 0.25 ; _shelx_res_checksum 78913 _shelx_hkl_file ; 3 0 0 3093.49 74.99 -3 0 0 3244.78 76.19 3 0 0 3172.38 69.29 3 0 0 3148.59 75.79 3 0 0 3189.58 75.89 -3 0 0 3218.48 76.19 -3 0 0 3155.28 74.89 4 0 0 322.67 14.20 4 0 0 326.47 14.80 -4 0 0 315.17 13.90 -4 0 0 307.27 14.50 -4 0 0 314.87 9.40 4 0 0 329.77 9.20 -4 0 0 329.27 14.90 -4 0 0 311.27 13.90 4 0 0 317.27 14.60 5 0 0 765.72 27.80 5 0 0 773.92 19.20 5 0 0 722.53 26.50 5 0 0 785.82 27.90 -5 0 0 758.92 27.80 -5 0 0 789.92 19.90 -5 0 0 765.12 26.70 -5 0 0 774.12 28.00 -5 0 0 763.92 26.60 -6 0 0 80.69 4.40 6 0 0 91.09 8.70 6 0 0 79.69 3.80 -6 0 0 88.89 8.10 -6 0 0 84.79 8.40 -6 0 0 80.59 7.60 6 0 0 71.29 7.70 -6 0 0 76.89 8.20 7 0 0 24.20 2.00 -7 0 0 27.30 5.80 -7 0 0 26.40 5.70 -7 0 0 25.00 5.80 7 0 0 27.10 6.00 -7 0 0 24.00 5.10 7 0 0 33.10 6.80 -7 0 0 29.60 2.90 -8 0 0 4196.08 94.09 -8 0 0 4214.68 108.19 -8 0 0 4151.78 111.09 -8 0 0 4056.69 110.79 8 0 0 4169.08 110.89 -8 0 0 4239.98 108.09 -9 0 0 237.58 17.70 -9 0 0 256.87 18.40 -9 0 0 248.48 9.80 9 0 0 242.88 18.10 -9 0 0 227.48 16.30 -9 0 0 223.38 16.10 -10 0 0 1752.22 62.39 -10 0 0 1876.11 44.90 10 0 0 1790.22 62.99 -10 0 0 1700.93 63.09 -10 0 0 1880.51 60.59 -11 0 0 45.90 9.20 -11 0 0 39.70 8.60 -11 0 0 49.40 10.00 -11 0 0 38.40 9.10 -11 0 0 46.50 4.00 11 0 0 53.29 10.80 -11 0 0 49.10 4.00 -12 0 0 621.04 31.90 -12 0 0 568.74 23.50 -12 0 0 657.43 33.30 12 0 0 599.34 34.00 -13 0 0 1.40 3.50 -13 0 0 0.80 3.10 13 0 0 6.70 5.30 -14 0 0 0.00 3.20 14 0 0 5.30 5.10 -14 0 0 1.60 4.40 15 0 0 3.40 5.40 -15 0 0 7.80 4.50 -15 0 0 3.60 5.00 16 0 0 101.79 19.60 -16 0 0 58.29 12.60 -16 0 0 64.59 21.80 -17 0 0 -6.50 4.00 -17 0 0 -0.70 4.70 -18 0 0 379.66 30.30 -18 0 0 432.36 31.40 -19 0 0 3.20 5.90 -19 0 0 7.80 5.60 -20 0 0 365.86 30.90 -20 0 0 365.46 32.50 -21 0 0 31.00 11.80 -21 0 0 8.70 8.80 0 -1 0 -0.30 0.10 0 1 0 -0.10 0.20 0 1 0 0.00 0.10 1 -1 0 -0.20 0.20 -1 1 0 0.40 0.50 -1 1 0 0.40 0.50 -2 -1 0 1864.31 43.20 -3 -1 0 11.60 1.50 -3 -1 0 6.60 1.70 3 -1 0 10.40 1.90 3 -1 0 9.80 2.40 3 -1 0 10.50 2.60 -3 -1 0 12.30 2.40 -3 -1 0 12.00 2.50 3 -1 0 11.50 2.60 -3 -1 0 9.60 1.90 -3 1 0 14.00 3.00 -3 1 0 9.00 1.90 3 1 0 10.50 2.20 -3 1 0 9.30 2.50 -3 1 0 8.50 2.20 3 1 0 12.40 1.40 3 1 0 12.80 1.50 3 1 0 13.30 2.30 -3 1 0 10.70 2.10 -4 -1 0 2174.88 55.29 4 -1 0 2174.68 58.39 4 -1 0 2077.19 51.79 -4 -1 0 2163.48 54.39 -4 -1 0 2201.18 53.99 4 -1 0 2156.08 57.79 -4 -1 0 2150.38 49.40 -4 -1 0 2194.48 56.59 -4 1 0 2158.28 52.09 -4 1 0 2185.38 58.59 4 1 0 2081.19 54.59 -4 1 0 2177.68 57.19 4 1 0 2171.58 48.70 4 1 0 2120.89 54.19 -4 1 0 2139.59 57.79 5 -1 0 44.10 5.90 -5 -1 0 40.00 9.60 5 -1 0 44.70 3.80 -5 -1 0 54.79 6.10 5 -1 0 47.80 6.00 -5 -1 0 49.10 3.10 -5 -1 0 46.10 5.10 -5 -1 0 51.79 5.10 5 1 0 50.19 5.40 5 1 0 41.30 2.40 -5 1 0 46.90 6.00 5 1 0 41.00 5.30 -5 1 0 47.10 4.00 -5 1 0 49.60 6.30 5 1 0 45.40 2.60 -5 1 0 39.00 5.20 6 -1 0 1324.97 44.20 -6 -1 0 1356.76 40.20 6 -1 0 1340.17 44.50 -6 -1 0 1340.47 40.60 -6 -1 0 1299.47 41.60 6 -1 0 1338.87 35.10 -6 -1 0 1350.76 42.90 -6 -1 0 1320.87 32.30 6 1 0 1334.77 42.30 -6 1 0 1355.06 35.60 -6 1 0 1290.47 43.70 -6 1 0 1316.17 42.60 -6 1 0 1338.37 44.80 -6 1 0 1354.16 36.20 -7 -1 0 473.45 13.90 7 -1 0 474.15 24.20 7 -1 0 477.85 24.00 -7 -1 0 489.75 21.20 -7 -1 0 451.35 22.20 -7 -1 0 480.35 21.50 -7 -1 0 448.16 22.60 7 -1 0 471.95 16.20 -7 1 0 470.85 16.80 7 1 0 488.05 23.00 -7 1 0 486.15 17.30 -7 1 0 490.75 23.40 -7 1 0 446.46 23.40 -7 1 0 476.15 24.50 -8 -1 0 1656.73 54.49 -8 -1 0 1741.83 40.40 -8 -1 0 1698.73 52.39 8 -1 0 1643.84 56.09 8 -1 0 1684.13 56.79 -8 -1 0 1680.53 51.69 -8 -1 0 1633.94 54.99 8 -1 0 1649.63 43.00 -8 1 0 1699.93 44.30 -8 1 0 1752.92 55.19 -8 1 0 1617.74 56.69 -8 1 0 1724.93 57.09 8 1 0 1692.43 54.59 -8 1 0 1741.43 45.10 -9 -1 0 427.66 22.30 -9 -1 0 454.45 23.20 -9 -1 0 449.76 13.40 9 -1 0 415.36 15.20 -9 -1 0 435.06 24.60 -9 -1 0 445.76 24.40 9 -1 0 469.35 26.30 -9 1 0 446.66 17.20 -9 1 0 428.46 16.40 -9 1 0 446.16 26.30 -9 1 0 478.65 26.60 9 1 0 440.36 24.40 -9 1 0 457.35 24.70 -9 1 0 434.66 24.40 10 -1 0 106.89 12.80 10 -1 0 91.99 5.90 -10 -1 0 108.79 11.90 -10 -1 0 88.59 12.00 -10 -1 0 83.49 9.90 -10 1 0 106.99 12.00 10 1 0 102.99 22.60 -10 1 0 105.69 12.40 -10 1 0 100.59 7.10 -10 1 0 95.19 12.30 -10 1 0 98.49 11.30 -10 1 0 90.89 6.90 -11 -1 0 813.32 39.30 -11 -1 0 834.12 39.90 -11 -1 0 893.31 37.20 11 -1 0 889.11 41.70 -11 -1 0 883.01 37.80 -11 1 0 848.32 40.90 -11 1 0 867.81 27.10 -11 1 0 851.91 41.90 -11 1 0 869.11 39.00 11 1 0 865.71 40.00 -11 1 0 863.31 27.70 -11 1 0 849.02 39.10 12 -1 0 846.92 43.20 -12 -1 0 905.11 43.10 -12 -1 0 847.82 38.60 -12 -1 0 960.30 41.20 -12 1 0 922.91 42.00 -12 1 0 995.90 29.50 -12 1 0 909.61 29.00 -12 1 0 1007.70 43.80 -13 -1 0 178.08 16.90 -13 -1 0 219.78 18.50 13 -1 0 178.38 18.80 -13 1 0 191.88 10.50 -13 1 0 206.78 19.10 -13 1 0 188.68 10.40 -13 1 0 169.08 17.10 14 -1 0 834.92 45.00 -14 -1 0 795.12 39.60 -14 -1 0 783.52 38.50 -14 1 0 772.72 25.00 -14 1 0 769.12 40.50 -14 1 0 830.02 25.60 -14 1 0 846.82 42.30 -15 -1 0 22.20 7.70 -15 -1 0 24.50 7.70 15 -1 0 11.30 6.00 -15 1 0 26.80 9.00 -15 1 0 5.20 6.00 -15 1 0 18.60 3.20 -15 1 0 18.90 3.10 -16 -1 0 318.87 25.40 16 -1 0 351.26 30.30 -16 -1 0 315.37 24.90 -16 1 0 345.77 28.10 -17 -1 0 32.40 10.20 17 -1 0 30.00 12.70 -17 1 0 29.90 9.80 -17 1 0 45.90 11.40 18 -1 0 36.70 13.90 -18 -1 0 22.10 9.80 -18 -1 0 35.40 8.30 -18 1 0 42.70 12.40 -18 1 0 34.20 10.00 -19 -1 0 35.60 10.30 -19 -1 0 0.60 5.70 -19 1 0 17.40 9.50 -19 1 0 16.30 8.30 -20 -1 0 86.49 16.60 -20 -1 0 46.10 13.40 -20 1 0 78.09 16.30 -20 1 0 57.09 15.60 -21 -1 0 4.40 9.60 -21 -1 0 11.10 8.70 -21 1 0 26.30 10.10 -21 1 0 11.40 10.10 0 -2 0 338.37 13.70 0 -2 0 317.37 10.50 0 -2 0 355.56 11.60 0 2 0 355.86 11.40 0 2 0 360.36 10.90 0 2 0 370.96 14.00 0 2 0 338.37 13.70 1 -2 0 99.49 6.70 1 -2 0 96.99 6.80 1 -2 0 103.89 6.20 -1 -2 0 97.69 6.40 -1 -2 0 97.79 6.60 -1 -2 0 101.79 4.90 1 -2 0 117.59 6.40 -1 2 0 100.49 5.90 1 2 0 102.79 4.90 -1 2 0 83.99 6.20 1 2 0 112.59 6.90 -1 2 0 95.59 5.60 -1 2 0 109.59 6.20 -1 2 0 107.69 7.00 2 -2 0 40.70 4.30 -2 -2 0 36.80 3.80 -2 -2 0 39.90 3.60 2 -2 0 42.00 4.40 -2 -2 0 35.30 3.70 2 -2 0 40.20 4.30 -2 -2 0 43.70 1.90 2 2 0 41.60 2.10 2 2 0 40.30 3.90 -2 2 0 40.30 4.30 -2 2 0 40.30 4.30 -2 2 0 34.40 4.10 2 2 0 39.10 3.30 -2 2 0 37.90 4.10 -2 2 0 32.30 3.70 -3 -2 0 14.90 2.70 -3 -2 0 18.90 1.90 -3 -2 0 15.00 2.00 -3 -2 0 18.30 2.60 3 -2 0 14.40 3.30 3 -2 0 12.70 3.20 -3 -2 0 17.10 2.80 3 -2 0 13.00 3.30 -3 2 0 25.10 4.20 -3 2 0 13.50 3.50 3 2 0 17.00 2.00 -3 2 0 9.90 2.40 3 2 0 15.50 2.70 3 2 0 17.50 4.60 -3 2 0 13.70 3.00 3 2 0 14.20 2.50 -4 -2 0 1173.18 32.40 -4 -2 0 1211.48 32.00 -4 -2 0 1138.19 31.70 4 -2 0 1210.08 38.10 -4 -2 0 1151.48 32.00 4 -2 0 1160.98 37.30 4 -2 0 1146.79 33.90 -4 -2 0 1085.49 31.60 -4 2 0 1167.48 34.20 4 2 0 1144.49 33.30 -4 2 0 1203.38 38.20 4 2 0 1151.58 31.30 -4 2 0 1158.48 36.50 -4 2 0 1160.28 36.90 4 2 0 1196.98 31.20 -4 2 0 1159.18 34.50 4 2 0 1139.19 31.20 -5 -2 0 126.59 9.50 5 -2 0 118.79 8.20 -5 -2 0 120.69 8.30 -5 -2 0 125.59 8.30 -5 -2 0 123.29 7.50 5 -2 0 131.89 10.90 5 -2 0 137.69 11.00 -5 -2 0 134.19 7.30 -5 2 0 113.39 8.30 -5 2 0 125.39 8.40 -5 2 0 112.59 10.40 5 2 0 129.79 6.70 5 2 0 122.79 8.00 -5 2 0 128.89 10.40 5 2 0 113.49 8.40 -5 2 0 130.59 10.30 5 2 0 123.49 6.70 -6 -2 0 22.10 4.50 6 -2 0 21.50 5.30 -6 -2 0 17.40 3.90 6 -2 0 19.20 5.20 -6 -2 0 27.10 3.70 -6 -2 0 22.90 5.00 -6 -2 0 29.00 3.20 6 -2 0 28.70 4.00 6 2 0 18.90 2.30 -6 2 0 21.50 5.10 -6 2 0 18.90 5.20 6 2 0 25.50 2.70 6 2 0 26.40 5.00 -6 2 0 23.40 4.20 -6 2 0 13.30 4.10 -6 2 0 22.90 5.10 -7 -2 0 356.46 13.00 -7 -2 0 344.87 17.90 7 -2 0 345.37 20.80 -7 -2 0 336.97 17.10 7 -2 0 323.27 15.20 7 -2 0 354.46 21.20 -7 -2 0 361.96 16.70 -7 -2 0 340.27 19.10 -7 2 0 354.86 15.90 7 2 0 356.66 11.50 7 2 0 337.27 11.20 -7 2 0 346.17 21.10 7 2 0 348.57 18.00 -7 2 0 353.26 20.60 -7 2 0 343.97 19.80 -7 2 0 351.96 16.30 -8 -2 0 386.66 21.70 8 -2 0 372.26 23.10 -8 -2 0 412.86 14.20 -8 -2 0 420.76 20.20 -8 -2 0 416.16 19.40 8 -2 0 388.96 16.90 8 -2 0 382.36 23.40 -8 -2 0 367.86 20.10 -8 2 0 381.16 22.80 -8 2 0 401.66 24.00 -8 2 0 419.86 23.00 -8 2 0 393.26 17.70 -8 2 0 399.86 17.40 -9 -2 0 470.35 15.10 -9 -2 0 410.96 24.10 9 -2 0 403.86 40.80 -9 -2 0 452.55 21.80 -9 -2 0 466.95 22.90 9 -2 0 437.26 18.90 -9 -2 0 433.46 23.60 -9 2 0 437.76 19.40 -9 2 0 451.55 27.30 -9 2 0 461.45 21.80 -9 2 0 487.85 27.40 -9 2 0 446.36 30.70 -10 -2 0 25.70 7.70 10 -2 0 35.20 9.00 -10 -2 0 35.10 7.00 -10 -2 0 33.30 3.10 10 -2 0 27.10 4.60 -10 -2 0 32.90 7.90 -10 2 0 36.20 5.10 -10 2 0 32.00 5.70 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0 1978.20 51.89 -2 3 0 1858.01 53.09 -2 3 0 1898.91 50.99 -2 3 0 1902.21 51.69 2 3 0 1918.31 47.70 2 3 0 1927.71 52.39 -2 3 0 1914.91 50.59 -2 3 0 2077.79 54.79 3 -3 0 908.81 31.20 3 -3 0 936.21 31.60 -3 -3 0 933.21 22.70 -3 -3 0 904.71 29.70 -3 -3 0 924.21 21.30 3 -3 0 916.21 31.10 -3 -3 0 919.11 26.50 -3 -3 0 917.51 29.60 -3 3 0 929.91 31.60 -3 3 0 895.21 30.90 -3 3 0 926.81 30.70 3 3 0 895.31 29.30 3 3 0 912.01 22.30 -3 3 0 902.01 30.20 3 3 0 916.91 29.10 -3 3 0 954.90 31.90 3 3 0 906.11 26.50 4 -3 0 245.98 14.80 -4 -3 0 257.57 11.70 -4 -3 0 248.58 12.70 -4 -3 0 253.67 9.90 4 -3 0 239.78 13.70 -4 -3 0 239.08 12.40 4 -3 0 259.17 15.20 -4 -3 0 253.37 8.70 -4 3 0 248.88 15.20 4 3 0 252.07 12.60 -4 3 0 271.47 14.60 -4 3 0 246.18 14.30 4 3 0 254.07 9.60 -4 3 0 249.97 14.30 4 3 0 246.58 12.30 -4 3 0 256.77 14.40 4 3 0 250.57 11.70 -5 -3 0 206.18 11.40 -5 -3 0 208.08 11.10 -5 -3 0 225.48 10.70 5 -3 0 214.28 14.90 -5 -3 0 224.28 9.40 5 -3 0 213.68 13.10 -5 -3 0 217.08 11.70 5 -3 0 220.88 14.90 -5 3 0 215.88 14.30 5 3 0 205.58 11.10 -5 3 0 229.28 13.60 -5 3 0 219.48 13.50 -5 3 0 210.38 14.00 5 3 0 228.88 12.00 5 3 0 219.68 11.20 -5 3 0 208.08 14.80 -6 -3 0 131.39 9.00 6 -3 0 126.59 9.70 6 -3 0 129.09 12.00 6 -3 0 127.89 12.00 -6 -3 0 125.79 8.50 -6 -3 0 126.49 7.60 -6 -3 0 127.89 8.80 -6 3 0 129.19 12.30 -6 3 0 115.09 9.60 6 3 0 128.09 9.70 -6 3 0 125.19 11.30 -6 3 0 135.49 10.50 6 3 0 125.69 8.10 -6 3 0 126.39 11.60 6 3 0 124.59 7.90 -7 -3 0 724.13 27.20 -7 -3 0 724.53 30.00 -7 -3 0 748.33 27.20 -7 -3 0 724.93 24.80 7 -3 0 726.93 27.90 7 -3 0 757.92 33.70 7 -3 0 711.63 33.10 -7 -3 0 748.13 24.80 7 3 0 732.13 23.30 7 3 0 728.03 23.50 -7 3 0 745.73 34.10 -7 3 0 727.33 28.10 -7 3 0 726.93 32.40 7 3 0 724.53 28.20 -7 3 0 721.03 33.80 -7 3 0 741.23 32.10 -8 -3 0 36.70 6.60 8 -3 0 38.50 8.40 8 -3 0 33.00 6.00 -8 -3 0 49.40 5.50 8 -3 0 46.70 9.30 -8 -3 0 48.00 5.20 -8 -3 0 46.40 6.40 -8 -3 0 50.89 8.60 -8 3 0 57.49 6.90 -8 3 0 41.80 9.00 -8 3 0 52.19 9.40 8 3 0 50.59 4.50 8 3 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473.55 27.10 -13 3 0 483.85 31.30 -13 3 0 390.16 21.90 -13 3 0 480.85 23.00 14 -3 0 -0.60 4.10 -14 -3 0 -2.10 2.50 -14 -3 0 1.70 3.30 -14 3 0 -3.00 1.70 -14 3 0 4.20 2.90 -14 3 0 -4.60 3.40 -15 -3 0 54.39 11.10 -15 -3 0 43.50 10.50 -15 3 0 30.90 10.40 -15 3 0 42.40 9.50 -15 3 0 50.59 8.10 -16 -3 0 101.29 13.20 16 -3 0 81.19 17.50 -16 -3 0 123.59 14.60 -16 3 0 85.59 15.40 -16 3 0 110.69 10.60 -16 3 0 132.29 17.00 -16 3 0 113.89 10.10 17 -3 0 117.59 21.70 -17 -3 0 146.39 16.50 -17 -3 0 94.79 13.00 -17 3 0 131.49 10.90 -17 3 0 122.19 10.80 -17 3 0 96.29 18.90 -17 3 0 121.79 17.00 -18 -3 0 20.00 8.10 18 -3 0 7.10 8.00 -18 3 0 34.30 6.40 -18 3 0 25.60 12.10 -18 3 0 30.20 5.60 -18 3 0 30.80 12.30 19 -3 0 -11.30 7.40 -19 -3 0 1.50 4.80 -19 -3 0 -10.60 6.20 -19 3 0 19.20 10.30 -19 3 0 4.80 3.00 -19 3 0 4.30 7.50 -20 -3 0 -1.40 6.70 20 -3 0 -0.80 9.30 -20 -3 0 -1.00 6.30 -20 3 0 12.90 10.80 -20 3 0 8.00 6.70 0 -4 0 479.05 21.80 0 -4 0 487.45 22.10 0 -4 0 481.35 18.10 0 4 0 488.15 16.40 0 4 0 475.05 17.30 0 4 0 483.95 22.00 0 4 0 389.36 21.60 1 -4 0 22.90 5.20 -1 -4 0 18.00 3.30 -1 -4 0 16.90 4.20 -1 -4 0 17.00 2.10 1 -4 0 19.40 3.70 1 -4 0 21.40 4.00 -1 -4 0 19.70 4.50 1 -4 0 21.80 4.90 1 4 0 20.20 2.10 -1 4 0 18.70 4.10 -1 4 0 32.40 4.10 -1 4 0 17.70 3.40 1 4 0 18.60 3.10 1 4 0 12.00 3.20 -1 4 0 14.90 4.00 -1 4 0 22.40 4.00 1 4 0 23.00 2.20 1 4 0 14.90 3.90 -2 -4 0 757.42 17.90 2 -4 0 752.72 27.50 -2 -4 0 766.22 29.00 2 -4 0 794.82 30.20 -2 -4 0 716.23 28.20 2 -4 0 776.62 27.10 2 -4 0 730.53 29.60 -2 -4 0 780.02 23.60 -2 4 0 730.43 29.20 2 4 0 793.62 29.50 -2 4 0 739.63 25.80 -2 4 0 770.12 27.10 -2 4 0 767.42 30.20 -2 4 0 760.82 26.50 2 4 0 744.93 23.40 3 -4 0 1.80 2.20 3 -4 0 0.80 1.70 3 -4 0 -1.60 1.10 -3 -4 0 0.50 1.10 -3 -4 0 3.20 2.00 3 -4 0 0.40 1.30 -3 -4 0 4.30 2.30 -3 4 0 0.70 1.30 -3 4 0 -0.10 1.80 -3 4 0 3.90 2.90 -3 4 0 2.00 1.40 3 4 0 3.50 2.20 -3 4 0 2.10 2.00 3 4 0 1.80 1.50 4 -4 0 222.38 15.00 -4 -4 0 214.68 7.80 4 -4 0 244.08 15.50 -4 -4 0 225.88 11.20 4 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2.30 7 4 0 4.50 2.20 -7 4 0 1.10 2.10 -7 4 0 7.90 3.60 -7 4 0 2.60 2.20 -7 4 0 1.70 2.90 -8 -4 0 581.84 24.00 -8 -4 0 578.54 21.10 8 -4 0 575.24 31.20 8 -4 0 576.24 26.60 -8 -4 0 602.24 23.70 -8 -4 0 556.04 24.00 -8 -4 0 575.84 27.60 8 -4 0 598.04 31.80 8 4 0 615.64 26.50 -8 4 0 560.64 27.10 -8 4 0 584.84 30.20 8 4 0 596.04 22.10 -8 4 0 565.14 26.60 8 4 0 581.44 22.40 -8 4 0 557.04 31.30 -8 4 0 612.34 30.50 -9 -4 0 262.47 16.00 -9 -4 0 266.17 14.00 9 -4 0 228.78 19.60 9 -4 0 247.18 16.40 -9 -4 0 259.17 14.30 -9 -4 0 264.47 18.90 9 -4 0 258.07 21.20 -9 -4 0 264.97 16.40 9 4 0 229.08 16.20 -9 4 0 267.67 21.50 -9 4 0 266.27 17.20 -9 4 0 258.07 17.60 -9 4 0 263.07 19.90 9 4 0 259.57 12.80 -9 4 0 261.97 20.10 -10 -4 0 1721.53 60.89 -10 -4 0 1830.22 50.19 -10 -4 0 1758.72 51.29 -10 -4 0 1785.32 55.39 -10 -4 0 1807.32 56.59 10 -4 0 1726.93 65.89 10 4 0 1683.83 57.79 -10 4 0 1770.92 63.39 10 4 0 1750.52 45.90 -10 4 0 1730.03 56.09 10 4 0 1670.73 45.60 -10 4 0 1736.73 57.59 -11 -4 0 315.97 19.80 11 -4 0 339.37 26.90 -11 -4 0 366.76 22.10 -11 -4 0 401.16 17.30 -11 -4 0 341.37 23.70 -11 -4 0 342.17 18.60 11 4 0 351.66 14.40 11 4 0 363.26 23.10 -11 4 0 380.86 26.10 -11 4 0 390.16 22.60 -11 4 0 375.96 21.50 -12 -4 0 432.46 25.40 -12 -4 0 424.46 21.90 12 -4 0 395.56 30.20 -12 -4 0 446.96 17.80 -12 -4 0 437.66 24.60 -12 4 0 347.67 22.00 -12 4 0 402.56 28.50 -12 4 0 423.46 23.40 -13 -4 0 30.30 8.30 -13 -4 0 21.70 6.90 -13 -4 0 18.40 6.10 13 -4 0 27.20 9.40 -13 4 0 22.20 6.00 -13 4 0 9.60 4.40 -13 4 0 4.10 5.20 -14 -4 0 109.19 11.40 -14 -4 0 106.89 12.50 14 -4 0 86.09 17.40 -14 -4 0 107.29 13.70 -14 4 0 86.39 10.90 -14 4 0 96.69 10.90 -14 4 0 112.49 18.40 -15 -4 0 8.20 6.20 -15 -4 0 7.40 4.90 15 -4 0 12.40 8.20 -15 4 0 14.50 6.50 -15 4 0 17.20 7.40 -15 4 0 8.10 4.40 -16 -4 0 24.90 6.80 -16 -4 0 45.80 10.70 16 -4 0 34.90 10.70 -16 4 0 35.70 11.30 -16 4 0 38.60 7.80 -16 4 0 26.80 10.40 -16 4 0 32.40 7.90 -17 -4 0 5.90 5.30 -17 -4 0 6.80 5.80 17 -4 0 -4.50 6.50 -17 4 0 0.90 3.70 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9 -22 40.80 8.50 -5 9 22 13.10 9.60 -5 9 22 43.20 14.20 -4 -9 22 27.10 10.10 4 -9 -22 21.40 11.00 -4 -9 22 26.40 6.70 4 -9 -22 14.10 7.80 4 -9 -22 11.00 7.50 -4 9 22 42.70 12.60 -4 9 22 15.90 13.30 4 9 -22 34.40 7.50 4 9 -22 23.40 8.50 -3 -9 22 147.19 20.10 3 -9 -22 183.68 28.70 3 -9 -22 153.58 17.90 3 -9 -22 155.18 18.50 -3 -9 22 140.89 13.50 3 9 -22 156.48 13.90 3 9 -22 154.08 7.20 3 9 -22 135.59 7.40 3 9 -22 172.58 20.60 -3 9 22 157.98 24.80 -3 9 22 126.69 22.50 2 -9 -22 14.50 8.30 2 -9 -22 24.80 8.90 -2 -9 22 10.20 8.20 2 -9 -22 26.40 12.10 2 9 -22 31.90 11.10 2 9 -22 14.00 3.80 2 9 -22 29.50 8.80 -2 9 22 4.10 9.70 2 9 -22 18.30 4.30 -2 9 22 30.10 10.70 -1 -9 22 25.30 8.20 1 -9 -22 31.90 9.20 1 -9 -22 29.10 8.70 1 -9 -22 15.70 8.90 1 9 -22 28.20 5.50 1 9 -22 23.90 9.00 1 9 -22 20.70 7.80 -1 9 22 13.70 13.10 1 9 -22 24.20 5.30 0 -9 22 5.80 6.50 0 -9 22 2.40 4.30 0 -9 -22 -4.70 2.70 0 -9 -22 -1.80 6.10 0 -9 -22 5.80 4.40 0 9 -22 5.40 3.50 0 9 -22 5.10 7.10 0 9 -22 5.10 5.50 0 9 -22 1.50 4.10 0 9 22 2.40 7.60 -1 -9 -22 94.29 16.10 1 -9 22 101.99 17.70 -1 -9 -22 102.99 14.20 -1 -9 -22 88.09 16.30 1 -9 22 97.39 12.20 -1 9 -22 110.59 13.60 -1 9 -22 84.99 17.50 1 9 22 115.39 21.20 -1 9 -22 99.69 11.50 -2 -9 -22 10.70 7.40 -2 -9 -22 1.00 5.30 2 -9 22 9.60 6.80 -2 -9 -22 6.70 6.10 -2 9 -22 -2.10 5.70 -2 9 -22 5.80 7.50 2 9 22 11.80 7.70 -2 9 -22 5.20 6.40 -2 9 -22 3.30 4.50 -3 -9 -22 13.10 6.70 -3 -9 -22 13.10 9.40 3 -9 22 31.00 9.40 -3 -9 -22 33.60 9.60 3 9 22 34.60 12.60 -3 9 -22 31.30 8.60 -3 9 -22 12.90 5.60 -3 9 -22 30.60 11.30 -4 -9 -22 16.70 6.30 -4 -9 -22 15.20 7.30 -4 -9 -22 -0.40 7.00 4 -9 22 14.80 8.00 4 9 22 3.50 6.80 -4 9 -22 0.50 4.40 -4 9 -22 -2.10 7.10 -4 9 -22 -8.10 4.00 -5 -9 -22 136.39 15.30 5 -9 22 153.58 18.30 -5 -9 -22 146.69 25.70 -5 -9 -22 136.29 16.50 -5 9 -22 100.49 18.70 5 9 22 121.39 21.80 -5 9 -22 134.99 14.70 -5 9 -22 143.19 16.60 6 -9 22 -5.00 7.40 -6 -9 -22 7.40 6.20 -6 -9 -22 3.80 5.50 -6 -9 -22 7.00 6.80 6 9 22 6.10 8.30 -6 9 -22 18.10 7.20 -6 9 -22 -4.60 6.80 -6 9 -22 7.20 6.20 -7 -9 -22 89.39 15.70 -7 -9 -22 102.59 21.00 -7 -9 -22 68.29 12.90 7 -9 22 87.29 17.60 7 9 22 100.39 19.00 -7 9 -22 101.09 16.50 -7 9 -22 102.99 13.80 -7 9 -22 62.69 14.90 8 -9 22 34.90 11.40 -8 -9 -22 15.10 7.10 -8 -9 -22 14.30 9.20 -8 -9 -22 9.60 7.40 8 9 22 -9.70 8.50 -8 9 -22 23.70 8.10 -8 9 -22 8.20 7.90 -8 9 -22 0.90 6.60 9 -9 22 63.19 14.10 -9 -9 -22 48.70 12.40 -9 -9 -22 55.99 16.10 -9 -9 -22 42.90 10.10 -9 9 -22 28.20 11.00 -9 9 -22 39.40 12.70 -9 9 -22 26.40 9.40 10 -9 22 -6.00 8.00 -10 -9 -22 -4.60 4.80 -10 -9 -22 -2.30 5.60 -10 -9 -22 8.20 12.00 -10 9 -22 2.00 7.40 -10 9 -22 -0.60 7.70 -10 9 -22 8.40 7.90 -11 -9 -22 6.80 7.00 11 -9 22 4.00 9.70 -11 -9 -22 5.40 7.30 -11 9 -22 -2.10 5.70 -11 9 -22 -12.50 8.70 -11 9 -22 -11.30 5.70 15 -10 -22 12.40 10.30 15 -10 -22 -4.10 9.00 -15 10 22 9.60 8.50 14 -10 -22 1.20 8.90 14 -10 -22 -0.20 8.60 13 -10 -22 -6.50 7.50 13 -10 -22 2.80 6.70 -13 -10 22 5.20 9.90 13 10 -22 10.60 5.90 -13 10 22 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11 -11 -22 50.79 16.60 11 -11 -22 64.59 16.90 -11 11 22 71.09 18.60 10 -11 -22 -11.30 7.60 10 -11 -22 -4.80 8.40 10 -11 -22 -2.30 8.20 -10 11 22 9.20 7.10 10 11 -22 8.90 5.00 9 -11 -22 0.80 8.00 9 -11 -22 40.40 11.10 9 -11 -22 4.90 8.90 9 11 -22 27.40 13.70 -9 11 22 7.00 6.90 9 11 -22 14.00 4.50 8 -11 -22 -3.70 9.50 8 -11 -22 24.10 12.60 8 -11 -22 26.30 12.70 8 11 -22 15.60 5.60 -8 11 22 28.10 12.00 7 -11 -22 -4.40 8.80 -7 -11 22 14.90 11.20 7 -11 -22 31.60 11.50 7 -11 -22 -2.00 7.20 -7 11 22 7.40 9.30 7 11 -22 4.10 7.20 7 11 -22 8.00 5.40 6 -11 -22 43.50 13.10 6 -11 -22 40.40 11.50 6 -11 -22 19.50 11.80 -6 -11 22 30.80 12.70 -6 -11 22 23.70 7.00 6 11 -22 41.50 12.80 -6 11 22 39.60 11.90 -6 11 22 43.20 14.10 6 11 -22 28.20 7.20 5 -11 -22 224.88 28.80 5 -11 -22 211.48 24.00 -5 -11 22 192.78 27.80 -5 -11 22 219.08 19.40 5 -11 -22 157.38 20.30 5 11 -22 204.18 24.80 5 11 -22 203.98 15.40 -5 11 22 136.99 23.90 -5 11 22 217.88 28.60 4 -11 -22 103.39 19.00 -4 -11 22 79.29 10.90 4 -11 -22 88.49 21.00 -4 -11 22 78.19 17.30 4 -11 -22 81.19 16.80 4 11 -22 80.69 18.10 4 11 -22 84.09 10.40 -4 11 22 70.39 17.50 -3 -11 22 280.67 30.40 -3 -11 22 254.67 18.30 3 -11 -22 197.28 27.90 3 -11 -22 211.78 22.80 3 -11 -22 193.08 23.00 -3 11 22 220.48 28.10 3 11 -22 223.38 25.80 3 11 -22 237.78 17.10 3 11 -22 216.98 10.50 3 11 -22 211.48 11.30 2 -11 -22 33.20 9.20 -2 -11 22 3.50 12.10 2 -11 -22 25.20 10.10 2 -11 -22 15.00 10.20 -2 -11 22 33.80 6.50 2 11 -22 30.40 6.00 2 11 -22 25.30 7.80 -2 11 22 9.70 9.00 2 11 -22 27.50 5.20 2 11 -22 23.90 11.00 1 -11 -22 123.79 23.60 1 -11 -22 130.49 17.60 1 -11 -22 118.99 19.90 -1 -11 22 136.29 13.30 -1 -11 22 127.39 24.00 1 11 -22 122.39 15.40 1 11 -22 120.79 10.80 1 11 -22 147.69 12.10 -1 11 22 179.18 26.20 0 -11 22 10.40 5.90 0 -11 -22 -9.10 5.80 0 -11 -22 -5.60 6.10 0 -11 -22 -0.50 6.80 0 11 -22 3.70 7.70 0 11 -22 14.10 5.70 0 11 -22 -0.20 6.70 0 11 -22 1.20 5.00 0 11 22 -1.30 9.20 -1 -11 -22 0.10 6.50 -1 -11 -22 3.80 7.10 -1 -11 -22 6.30 6.90 1 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6.40 -9 -2 28 75.19 13.10 9 -2 -28 85.19 11.40 -9 2 28 73.49 14.40 9 2 -28 86.19 15.40 9 2 -28 71.19 7.50 -9 2 28 76.19 9.20 9 2 -28 83.39 15.20 -8 -2 28 51.09 11.10 8 -2 -28 45.00 9.40 -8 -2 28 35.20 4.80 8 -2 -28 42.40 11.40 8 -2 -28 35.30 10.80 -8 2 28 50.09 10.90 -8 2 28 47.60 7.90 8 2 -28 38.70 10.80 8 2 -28 29.10 5.20 -7 -2 28 17.60 4.10 7 -2 -28 18.50 5.40 -7 -2 28 12.90 6.40 7 -2 -28 15.80 7.40 7 -2 -28 26.10 8.90 -7 2 28 13.80 7.30 7 2 -28 2.50 5.80 7 2 -28 28.80 8.40 7 2 -28 16.40 4.40 -7 2 28 14.80 5.60 -6 -2 28 0.00 2.40 6 -2 -28 -3.60 2.90 -6 -2 28 -2.00 3.80 6 -2 -28 -1.80 4.30 6 -2 -28 0.30 3.50 -6 2 28 8.80 4.80 -6 2 28 -12.60 7.60 6 2 -28 -2.70 4.60 6 2 -28 -1.80 4.20 6 2 -28 -3.90 2.00 -5 -2 28 92.19 17.80 5 -2 -28 71.79 9.60 5 -2 -28 79.39 16.50 -5 -2 28 72.59 7.70 5 -2 -28 73.59 14.00 5 2 -28 74.89 7.70 -5 2 28 75.29 13.90 5 2 -28 61.19 13.50 5 2 -28 69.49 13.40 -5 2 28 67.29 9.30 4 -2 -28 56.29 9.50 4 -2 -28 29.80 9.40 -4 -2 28 33.20 10.60 4 -2 -28 44.30 11.00 -4 -2 28 36.40 6.50 -4 2 28 39.80 10.40 4 2 -28 40.30 6.30 -4 2 28 49.50 9.10 4 2 -28 41.30 12.40 4 2 -28 39.60 9.70 -3 -2 28 268.57 24.30 3 -2 -28 241.98 17.20 -3 -2 28 247.68 15.70 3 -2 -28 231.08 24.10 3 -2 -28 243.98 21.70 3 2 -28 245.58 24.10 3 2 -28 219.98 13.50 3 2 -28 246.28 20.40 3 2 -28 233.68 16.00 -3 2 28 230.68 22.90 2 -2 -28 300.17 27.30 -2 -2 28 295.27 25.90 2 -2 -28 319.57 20.40 -2 -2 28 315.97 18.60 2 -2 -28 329.17 24.80 2 2 -28 309.27 19.60 2 2 -28 336.57 23.80 2 2 -28 331.87 28.80 2 2 -28 339.87 17.20 -2 2 28 313.07 27.70 1 -2 -28 151.18 20.00 1 -2 -28 150.18 16.60 1 -2 -28 150.38 13.80 -1 -2 28 181.68 20.20 -1 -2 28 130.69 16.00 1 2 -28 155.38 16.40 1 2 -28 148.49 12.00 1 2 -28 175.18 21.50 -1 2 28 134.09 18.20 0 -2 -28 5.60 4.70 0 -2 28 3.60 4.70 0 -2 -28 14.40 7.10 0 -2 -28 3.60 4.70 0 -2 28 12.40 4.20 0 2 -28 6.50 3.50 0 2 -28 2.60 5.00 0 2 28 11.00 8.00 0 2 -28 14.70 5.60 0 2 -28 2.60 6.20 -1 -2 -28 0.70 2.40 1 -2 28 5.90 4.90 -1 -2 -28 -1.40 3.30 -1 -2 -28 6.30 5.90 1 -2 28 -5.10 4.50 -1 2 -28 -3.30 4.60 -1 2 -28 10.20 8.30 1 2 28 -1.10 5.30 -1 2 -28 4.80 4.30 -1 2 -28 2.90 5.50 -2 -2 -28 11.70 6.10 -2 -2 -28 4.80 5.90 -2 -2 -28 13.60 6.00 -2 2 -28 14.20 5.60 -2 2 -28 12.40 9.10 -2 2 -28 13.10 7.40 -3 -2 -28 68.19 12.70 -3 -2 -28 67.69 15.50 -3 -2 -28 68.39 13.30 -3 2 -28 82.39 11.10 -3 2 -28 80.59 16.20 -3 2 -28 77.99 16.50 -4 -2 -28 12.50 7.10 -4 -2 -28 10.60 8.80 -4 -2 -28 18.90 9.40 -4 2 -28 18.00 8.60 -4 2 -28 1.80 6.80 -4 2 -28 13.10 6.20 -5 -2 -28 29.40 17.00 -5 -2 -28 23.90 10.20 -5 -2 -28 16.80 9.30 -5 2 -28 19.50 10.40 -5 2 -28 34.70 8.90 -5 2 -28 24.80 11.10 -6 -2 -28 91.09 16.90 -6 -2 -28 100.59 19.50 -6 -2 -28 87.59 15.40 -6 2 -28 94.99 19.10 -6 2 -28 104.99 13.90 -6 2 -28 100.49 17.20 -7 -2 -28 27.50 11.00 -7 -2 -28 32.50 11.50 -7 -2 -28 47.20 10.80 -7 2 -28 20.00 10.00 -7 2 -28 35.90 10.70 -7 2 -28 33.70 10.30 -8 -2 -28 32.20 11.30 -8 -2 -28 34.50 10.70 -8 -2 -28 37.10 10.10 -8 2 -28 18.60 8.20 -8 2 -28 34.90 12.00 -8 2 -28 35.10 12.30 -9 -2 -28 -5.50 6.90 -9 -2 -28 6.80 9.60 -9 -2 -28 2.20 6.60 -9 2 -28 -4.00 4.80 -9 2 -28 0.60 6.00 -9 2 -28 10.80 8.40 -10 -2 -28 6.50 9.00 -10 -2 -28 17.30 10.60 -10 -2 -28 16.20 8.90 -10 2 -28 6.90 6.40 -10 2 -28 11.80 9.40 -10 2 -28 10.00 7.80 -11 -2 -28 -3.00 7.30 -11 -2 -28 5.40 8.60 -11 -2 -28 11.00 9.40 -11 2 -28 17.90 7.50 -11 2 -28 5.70 8.50 -11 2 -28 14.40 9.00 -12 -2 -28 -8.30 6.50 -12 -2 -28 7.20 6.90 -12 -2 -28 -12.10 7.70 -12 2 -28 4.20 9.30 -12 2 -28 13.60 8.30 -13 -2 -28 5.60 9.50 -13 -2 -28 3.50 9.60 -13 -2 -28 -7.80 7.80 -13 2 -28 -3.40 8.80 -13 2 -28 3.80 7.40 -13 2 -28 -0.10 7.00 19 -3 -28 60.19 15.30 19 -3 -28 61.29 18.70 -19 -3 28 81.99 10.70 -19 3 28 57.39 12.20 -19 3 28 59.19 12.60 19 3 -28 76.19 19.30 18 -3 -28 9.40 8.40 -18 -3 28 26.80 7.00 18 -3 -28 17.90 12.50 -18 3 28 37.00 9.80 18 3 -28 24.20 13.00 -18 3 28 6.80 8.50 -17 -3 28 105.69 13.30 17 -3 -28 89.09 20.90 -17 -3 28 96.09 9.50 17 -3 -28 90.49 17.70 -17 3 28 106.99 15.60 -17 3 28 116.99 17.00 17 3 -28 83.79 18.20 16 -3 -28 39.40 12.80 -16 -3 28 53.19 10.90 16 -3 -28 20.50 10.90 16 -3 -28 48.30 14.90 -16 -3 28 63.69 7.00 -16 3 28 41.20 10.70 16 3 -28 43.60 13.20 -16 3 28 40.90 12.30 15 -3 -28 72.79 14.30 15 -3 -28 79.29 15.40 15 -3 -28 83.59 20.20 -15 -3 28 92.59 6.80 -15 -3 28 109.19 19.60 -15 -3 28 96.09 7.20 -15 3 28 109.09 17.50 15 3 -28 88.19 17.10 15 3 -28 108.19 20.40 -15 3 28 86.29 15.00 14 -3 -28 0.60 6.60 14 -3 -28 1.10 6.30 14 -3 -28 4.80 6.10 -14 -3 28 1.60 4.20 -14 -3 28 0.30 1.90 14 3 -28 3.80 9.60 -14 3 28 11.80 6.00 13 -3 -28 -1.30 5.40 -13 -3 28 4.70 1.80 13 -3 -28 -5.10 5.50 13 -3 -28 -1.20 6.90 -13 -3 28 -0.30 4.70 -13 3 28 4.10 5.60 13 3 -28 -10.50 5.00 13 3 -28 -2.20 5.40 12 -3 -28 -2.60 5.00 -12 -3 28 4.90 4.00 12 -3 -28 7.80 7.50 12 3 -28 10.10 5.90 -12 3 28 3.10 6.60 11 -3 -28 81.09 14.40 11 -3 -28 114.59 20.50 -11 -3 28 47.00 10.80 11 -3 -28 78.19 14.00 11 3 -28 58.29 12.00 11 3 -28 52.79 13.70 -11 3 28 61.49 12.50 -10 -3 28 1.30 4.20 10 -3 -28 0.80 4.40 10 -3 -28 6.30 6.00 10 -3 -28 1.30 5.30 10 3 -28 4.70 5.20 10 3 -28 3.40 6.20 -10 3 28 7.50 5.60 9 -3 -28 282.27 21.90 9 -3 -28 301.07 34.50 -9 -3 28 310.27 25.40 9 -3 -28 285.57 25.80 -9 3 28 277.87 26.10 9 3 -28 301.87 25.70 9 3 -28 272.97 24.10 8 -3 -28 172.78 16.40 -8 -3 28 172.88 7.30 8 -3 -28 222.88 22.10 8 -3 -28 192.78 21.00 -8 -3 28 158.88 17.60 8 3 -28 164.98 7.50 8 3 -28 177.78 7.50 8 3 -28 156.58 18.20 -8 3 28 164.78 20.50 -7 -3 28 290.97 11.60 -7 -3 28 314.57 26.30 7 -3 -28 289.37 26.20 7 -3 -28 273.77 20.70 7 -3 -28 288.67 26.20 7 3 -28 284.07 23.40 7 3 -28 261.97 24.50 7 3 -28 285.87 12.10 7 3 -28 278.97 12.00 -7 3 28 293.47 26.50 6 -3 -28 78.49 15.50 -6 -3 28 71.69 8.80 6 -3 -28 97.99 11.80 -6 -3 28 89.19 15.30 6 -3 -28 102.39 17.90 6 3 -28 89.79 6.50 6 3 -28 87.49 14.80 -6 3 28 70.69 14.40 6 3 -28 75.39 16.10 -5 -3 28 319.47 15.00 5 -3 -28 261.77 25.80 5 -3 -28 299.07 25.10 5 -3 -28 318.77 21.70 -5 -3 28 352.56 28.70 5 3 -28 295.07 13.70 5 3 -28 326.77 24.20 -5 3 28 315.47 27.90 5 3 -28 301.27 15.40 5 3 -28 250.87 24.90 -4 -3 28 11.80 3.90 -4 -3 28 12.40 5.80 4 -3 -28 12.40 6.40 4 -3 -28 24.50 9.90 4 -3 -28 1.90 3.60 4 3 -28 4.70 2.90 4 3 -28 -0.50 5.60 4 3 -28 20.10 4.40 4 3 -28 14.60 6.00 -4 3 28 9.10 8.70 3 -3 -28 100.99 18.10 -3 -3 28 110.59 10.00 -3 -3 28 117.99 16.30 3 -3 -28 120.99 15.30 3 -3 -28 115.89 13.00 -3 3 28 103.59 17.10 3 3 -28 101.69 8.50 3 3 -28 91.19 10.40 3 3 -28 89.19 17.90 3 3 -28 144.59 15.20 -2 -3 28 6.60 4.90 2 -3 -28 11.80 7.20 2 -3 -28 14.60 7.10 -2 -3 28 13.70 4.80 2 -3 -28 17.30 5.70 2 3 -28 12.00 7.60 2 3 -28 14.10 5.80 2 3 -28 17.50 5.50 2 3 -28 10.80 4.10 -2 3 28 3.80 5.50 -1 -3 28 101.09 17.20 1 -3 -28 100.49 13.70 1 -3 -28 75.19 16.20 1 -3 -28 76.19 10.50 1 3 -28 77.79 13.80 1 3 -28 88.29 17.50 1 3 -28 86.19 9.60 -1 3 28 98.89 17.70 1 3 -28 64.89 10.70 0 -3 28 8.90 6.20 0 -3 -28 8.40 5.10 0 -3 -28 2.90 4.40 0 -3 -28 7.50 6.80 0 3 -28 3.10 7.30 0 3 -28 5.40 6.10 0 3 28 1.80 5.10 0 3 -28 7.30 4.90 0 3 -28 25.40 6.10 -1 -3 -28 106.29 12.70 1 -3 28 111.69 19.60 -1 -3 -28 103.49 13.70 -1 -3 -28 78.19 15.80 -1 3 -28 122.99 13.70 -1 3 -28 144.69 17.80 -1 3 -28 143.39 13.00 -1 3 -28 147.99 20.00 -2 -3 -28 155.68 16.10 -2 -3 -28 137.79 19.70 -2 -3 -28 147.49 14.60 -2 3 -28 156.28 20.90 -2 3 -28 135.69 17.20 -2 3 -28 157.78 14.40 -3 -3 -28 105.89 16.60 -3 -3 -28 100.99 18.90 -3 -3 -28 130.99 14.20 -3 3 -28 104.79 17.60 -3 3 -28 100.09 29.90 -3 3 -28 121.59 12.50 -4 -3 -28 15.70 8.20 -4 -3 -28 1.30 5.50 -4 -3 -28 6.40 5.90 -4 3 -28 -6.40 5.40 -4 3 -28 2.30 3.70 -4 3 -28 6.90 6.60 -5 -3 -28 177.28 19.20 -5 -3 -28 176.28 18.20 -5 -3 -28 179.68 23.40 -5 3 -28 177.28 16.90 -5 3 -28 185.98 21.00 -5 3 -28 162.78 21.50 -6 -3 -28 7.30 5.30 -6 -3 -28 -0.70 5.90 -6 3 -28 13.30 8.70 -6 3 -28 -4.30 6.20 -6 3 -28 6.10 5.10 -7 -3 -28 1.10 7.10 -7 -3 -28 20.10 8.20 -7 -3 -28 13.20 8.00 -7 3 -28 25.40 9.80 -7 3 -28 3.40 4.80 -7 3 -28 7.10 6.90 -8 -3 -28 -5.80 4.40 -8 -3 -28 13.80 8.80 -8 -3 -28 3.10 6.00 -8 3 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23.40 4 5 -28 240.08 9.60 4 5 -28 249.78 20.80 3 -5 -28 8.30 6.60 3 -5 -28 -1.10 4.00 -3 -5 28 12.50 8.30 3 -5 -28 3.70 5.80 3 5 -28 1.40 4.20 3 5 -28 14.30 9.40 3 5 -28 5.40 3.00 -3 5 28 12.50 7.40 3 5 -28 2.80 2.50 2 -5 -28 57.79 12.20 2 -5 -28 72.99 14.70 2 -5 -28 73.89 16.10 -2 -5 28 32.70 10.40 2 5 -28 74.29 13.60 2 5 -28 91.39 18.00 2 5 -28 59.19 8.90 2 5 -28 66.19 7.20 -2 5 28 56.09 12.60 1 -5 -28 64.49 12.90 1 -5 -28 54.39 10.50 1 -5 -28 26.30 10.80 -1 -5 28 48.20 13.80 1 5 -28 54.09 12.10 1 5 -28 70.09 16.20 1 5 -28 60.89 7.70 -1 5 28 54.59 13.40 1 5 -28 56.19 9.40 0 -5 28 75.39 16.60 0 -5 -28 60.29 11.40 0 -5 -28 56.99 13.10 0 -5 -28 81.99 17.70 0 5 -28 56.49 13.20 0 5 -28 60.19 8.10 0 5 -28 54.49 26.50 0 5 -28 50.49 9.40 1 -5 28 4.00 6.60 -1 -5 -28 2.70 3.80 -1 -5 -28 1.60 3.60 -1 -5 -28 2.50 5.60 -1 5 -28 -3.30 6.40 -1 5 -28 -2.70 2.70 -1 5 -28 4.00 8.10 -1 5 -28 -1.60 5.00 -2 -5 -28 270.17 22.80 -2 -5 -28 331.47 31.30 -2 -5 -28 272.77 23.90 -2 5 -28 318.97 19.80 -2 5 -28 286.97 30.80 -2 5 -28 299.87 29.00 -3 -5 -28 12.40 5.40 -3 -5 -28 6.10 4.90 -3 -5 -28 2.10 4.90 -3 5 -28 4.70 5.90 -3 5 -28 10.20 8.20 -3 5 -28 1.40 4.00 -4 -5 -28 35.50 10.10 -4 -5 -28 39.20 11.80 -4 -5 -28 29.70 9.30 -4 5 -28 30.90 8.00 -4 5 -28 33.30 10.90 -4 5 -28 44.10 14.20 -5 -5 -28 4.60 4.80 -5 -5 -28 0.30 3.80 -5 5 -28 21.00 8.90 -5 5 -28 0.60 7.10 -5 5 -28 -7.10 3.10 -6 -5 -28 33.90 9.90 -6 -5 -28 34.80 9.90 -6 -5 -28 28.70 12.20 -6 5 -28 11.00 8.10 -6 5 -28 45.80 10.20 -6 5 -28 15.30 11.50 -7 -5 -28 -3.20 4.50 -7 -5 -28 0.50 6.30 -7 -5 -28 3.60 7.60 -7 5 -28 8.90 8.70 -7 5 -28 5.30 7.20 -7 5 -28 6.30 4.80 -8 -5 -28 -5.60 5.60 -8 -5 -28 -0.80 5.60 -8 -5 -28 10.10 7.00 -8 5 -28 4.70 7.40 -8 5 -28 -3.20 4.80 -8 5 -28 -5.40 7.30 -9 -5 -28 0.10 6.30 -9 -5 -28 -2.80 5.80 -9 -5 -28 0.50 5.90 -9 5 -28 9.40 6.40 -9 5 -28 -12.00 5.80 -9 5 -28 -2.30 6.40 -10 -5 -28 39.10 13.60 -10 -5 -28 50.99 13.50 -10 -5 -28 52.89 17.30 -10 5 -28 67.69 13.10 -10 5 -28 49.70 17.10 -10 5 -28 31.10 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255.37 24.40 -11 6 28 291.77 29.00 -11 6 28 301.57 28.40 11 6 -28 228.88 23.10 10 -6 -28 177.58 23.70 -10 -6 28 192.88 20.00 10 -6 -28 133.49 21.60 10 -6 -28 167.48 20.90 10 6 -28 151.58 17.70 -10 6 28 160.38 21.90 10 6 -28 122.09 17.80 -10 6 28 166.08 21.40 9 -6 -28 49.00 12.50 9 -6 -28 82.89 16.60 -9 -6 28 55.39 12.10 9 -6 -28 46.90 15.00 9 6 -28 57.59 13.40 9 6 -28 58.49 12.40 -9 6 28 51.59 12.90 -8 -6 28 194.38 21.00 8 -6 -28 209.28 25.00 8 -6 -28 206.58 23.70 8 -6 -28 179.58 20.00 -8 6 28 242.78 25.60 8 6 -28 230.48 20.80 7 -6 -28 6.60 5.40 7 -6 -28 -1.90 4.70 -7 -6 28 -4.20 3.70 7 6 -28 -0.90 5.20 7 6 -28 -1.10 4.40 -7 6 28 -9.00 6.70 -6 -6 28 24.70 9.40 6 -6 -28 32.80 10.90 6 -6 -28 29.70 9.40 6 -6 -28 46.60 11.50 6 6 -28 44.10 10.30 -6 6 28 23.50 9.70 6 6 -28 39.50 11.20 -5 -6 28 1.30 5.60 5 -6 -28 3.50 5.30 5 -6 -28 4.60 7.90 5 -6 -28 9.00 8.50 5 6 -28 4.70 6.00 -5 6 28 12.60 7.10 5 6 -28 3.70 4.70 -4 -6 28 66.29 13.80 4 -6 -28 17.20 9.00 4 -6 -28 32.90 9.50 4 -6 -28 32.70 10.40 -4 6 28 10.20 9.00 4 6 -28 32.90 11.50 4 6 -28 36.80 9.60 3 -6 -28 357.56 29.60 3 -6 -28 401.96 35.30 3 -6 -28 397.96 27.60 -3 -6 28 383.16 32.60 3 6 -28 377.16 13.90 -3 6 28 397.56 35.00 3 6 -28 416.66 33.90 3 6 -28 435.06 26.70 2 -6 -28 96.39 15.60 2 -6 -28 88.99 16.40 2 -6 -28 116.99 21.40 -2 -6 28 120.49 19.90 -2 6 28 123.69 20.70 2 6 -28 144.69 19.80 2 6 -28 118.59 10.20 2 6 -28 94.59 8.00 2 6 -28 93.29 13.00 1 -6 -28 91.09 15.90 1 -6 -28 78.49 23.20 1 -6 -28 60.89 15.30 1 6 -28 74.19 8.00 1 6 -28 76.19 14.30 1 6 -28 96.09 10.20 1 6 -28 84.89 17.40 0 -6 28 174.38 21.80 0 -6 -28 155.28 18.10 0 -6 -28 181.58 18.00 0 -6 -28 116.39 20.70 0 6 -28 189.38 19.70 0 6 -28 201.78 24.20 0 6 -28 185.18 15.60 0 6 -28 167.08 12.70 -1 -6 -28 103.89 14.20 -1 -6 -28 106.49 14.10 -1 -6 -28 131.99 23.00 -1 6 -28 100.19 17.80 -1 6 -28 119.99 11.40 -1 6 -28 95.99 19.20 -1 6 -28 121.89 14.10 -2 -6 -28 8.40 6.60 -2 -6 -28 8.20 6.60 -2 -6 -28 2.60 4.50 -2 6 -28 -5.50 5.90 -2 6 -28 -11.90 5.60 -2 6 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