data_14_a # start Validation Reply Form _vrf_PLAT410_14_a ; PROBLEM: Short Intra H...H Contact H3B ..H1D . 1.85 Ang. RESPONSE: H1D is part of a minor disorder component of one of the -CH2CH2NH- arms of the ligand. The disorder results in a relatively close contact with the neighboring arm of the ligand. ; # end Validation Reply Form _audit_creation_method 'SHELXL-2018/3' _shelx_SHELXL_version_number '2018/3' _chemical_name_systematic ? _chemical_name_common '[mCH]CuCl(ClO4)2' _chemical_melting_point ? _chemical_formula_moiety 'C33 H46 Cl Cu N5 O3, 2(Cl O4), C2 H3 N' _chemical_formula_sum 'C35 H49 Cl3 Cu N6 O11' _chemical_formula_weight 899.69 _publ_contact_author 'Subrata Kundu' _publ_contact_author_email 'skundu@iisertvm.ac.in' _publ_author_name 'Mondal, A.; Reddy, K. P.; Bertke, J. A.; Kundu, S.' _journal_name_requested 'J. Am. Chem. Soc.' loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cu' 'Cu' 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/c' _space_group_name_Hall '-P 2ybc' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 13.007(4) _cell_length_b 16.788(5) _cell_length_c 18.574(6) _cell_angle_alpha 90 _cell_angle_beta 103.666(9) _cell_angle_gamma 90 _cell_volume 3941(2) _cell_formula_units_Z 4 _cell_measurement_temperature 150(2) _cell_measurement_reflns_used 9986 _cell_measurement_theta_min 2.26 _cell_measurement_theta_max 23.44 _exptl_crystal_description 'block' _exptl_crystal_colour 'green' _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_density_diffrn 1.516 _exptl_crystal_F_000 1876 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.220 _exptl_crystal_size_mid 0.185 _exptl_crystal_size_min 0.085 _exptl_absorpt_coefficient_mu 0.824 _shelx_estimated_absorpt_T_min 0.839 _shelx_estimated_absorpt_T_max 0.933 _exptl_absorpt_correction_type 'multi-scan' _exptl_absorpt_correction_T_min 0.6478 _exptl_absorpt_correction_T_max 0.7457 _exptl_absorpt_process_details 'SADABS V2016/2 (Bruker, 2016)' _exptl_absorpt_special_details ? _diffrn_ambient_temperature 150(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_monochromator 'multilayer mirrors' _diffrn_measurement_device 'Bruker APEX ApexII CCD' _diffrn_measurement_method 'profile data from \f and \w scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 58793 _diffrn_reflns_av_unetI/netI 0.0444 _diffrn_reflns_av_R_equivalents 0.0539 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_h_max 17 _diffrn_reflns_limit_k_min -22 _diffrn_reflns_limit_k_max 22 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_limit_l_max 24 _diffrn_reflns_theta_min 2.117 _diffrn_reflns_theta_max 28.395 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.995 _diffrn_measured_fraction_theta_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.995 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.995 _diffrn_reflns_point_group_measured_fraction_full 1.000 _reflns_number_total 9841 _reflns_number_gt 6935 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'APEX3 V2016.5-0 (Bruker, 2016)' _computing_cell_refinement 'SAINT V8.37A (Bruker, 2005)' _computing_data_reduction ; SAINT V8.37A, XPREP v2014/2, SADABS V2016/2 (Bruker, 2016) ; _computing_structure_solution 'SHELX-2014-5 (Sheldrick, 2015)' _computing_structure_refinement 'SHELX-2018-3 (Sheldrick, 2015)' _computing_molecular_graphics 'SHELXLE v932 (Hubschle, 2011)' _computing_publication_material 'XCIF V2014-2 (Bruker, 2014)' _refine_special_details ; Structure was phased by intrinsic methods (Sheldrick, 2015). Systematic conditions suggested the ambiguous space group. The space group choice was confirmed by successful convergence of the full-matrix least-squares refinement on F^2^. The final map had no significant features. A final analysis of variance between observed and calculated structure factors showed little dependence on amplitude and resolution. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0542P)^2^+3.0384P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary 'intrinsic' _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 9841 _refine_ls_number_parameters 543 _refine_ls_number_restraints 173 _refine_ls_R_factor_all 0.0746 _refine_ls_R_factor_gt 0.0447 _refine_ls_wR_factor_ref 0.1219 _refine_ls_wR_factor_gt 0.1067 _refine_ls_goodness_of_fit_ref 1.019 _refine_ls_restrained_S_all 1.033 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu1 Cu 0.67400(2) 0.63327(2) 0.48046(2) 0.02450(9) Uani 1 1 d . . . . . Cl1 Cl 0.52573(6) 0.62667(4) 0.52605(4) 0.03717(17) Uani 1 1 d . . . . . O1 O 0.39730(15) 0.87505(11) 0.43097(10) 0.0331(4) Uani 1 1 d . . . . . O2 O 0.37938(15) 0.80808(13) 0.26077(12) 0.0419(5) Uani 1 1 d . . . . . O3 O 0.27627(16) 0.65897(12) 0.33649(12) 0.0433(5) Uani 1 1 d . . . . . Cl2 Cl 0.89982(5) 0.56081(4) 0.26739(4) 0.03439(16) Uani 1 1 d . U . . . O4 O 0.8344(2) 0.52935(14) 0.31215(18) 0.0737(9) Uani 1 1 d . U . . . O5 O 0.99454(18) 0.51802(14) 0.27584(15) 0.0591(7) Uani 1 1 d . U . . . O6 O 0.91828(17) 0.64372(12) 0.28142(14) 0.0471(6) Uani 1 1 d . U . . . O7 O 0.8408(2) 0.55288(16) 0.19156(15) 0.0726(8) Uani 1 1 d . U . . . Cl3 Cl 0.89431(6) 0.29710(4) -0.05530(4) 0.03703(17) Uani 1 1 d . U . . . O8 O 0.8708(2) 0.22032(16) -0.03223(16) 0.0732(8) Uani 1 1 d . U . . . O9 O 0.9362(2) 0.28908(18) -0.11863(13) 0.0676(8) Uani 1 1 d . U . . . O10 O 0.9708(2) 0.33381(15) 0.00332(13) 0.0635(7) Uani 1 1 d . U . . . O11 O 0.8016(2) 0.34455(17) -0.07317(17) 0.0723(8) Uani 1 1 d . U . . . N1 N 0.81641(19) 0.57626(14) 0.54099(13) 0.0373(6) Uani 1 1 d D . . . . N2 N 0.7237(8) 0.7227(4) 0.5605(8) 0.0429(19) Uani 0.615(7) 1 d D U P A 1 H2 H 0.667219 0.725522 0.587171 0.051 Uiso 0.615(7) 1 calc R U P A 1 C1 C 0.8188(5) 0.6047(3) 0.6190(2) 0.0394(13) Uani 0.615(7) 1 d D U P A 1 H1A H 0.756225 0.586316 0.633954 0.047 Uiso 0.615(7) 1 calc R U P A 1 H1B H 0.880662 0.583548 0.653590 0.047 Uiso 0.615(7) 1 calc R U P A 1 C2 C 0.8223(4) 0.6935(3) 0.6195(3) 0.0372(12) Uani 0.615(7) 1 d D U P A 1 H2A H 0.886702 0.712075 0.607220 0.045 Uiso 0.615(7) 1 calc R U P A 1 H2B H 0.820416 0.713715 0.668050 0.045 Uiso 0.615(7) 1 calc R U P A 1 N2B N 0.7269(13) 0.7234(6) 0.5685(12) 0.038(2) Uani 0.385(7) 1 d D U P A 2 H2C H 0.659079 0.734063 0.581007 0.046 Uiso 0.385(7) 1 calc R U P A 2 C1B C 0.8646(6) 0.6249(5) 0.6095(4) 0.0347(18) Uani 0.385(7) 1 d D U P A 2 H1C H 0.903220 0.590931 0.648881 0.042 Uiso 0.385(7) 1 calc R U P A 2 H1D H 0.912545 0.664855 0.598384 0.042 Uiso 0.385(7) 1 calc R U P A 2 C2B C 0.7740(6) 0.6629(5) 0.6310(4) 0.0350(17) Uani 0.385(7) 1 d D U P A 2 H2D H 0.797223 0.690149 0.678164 0.042 Uiso 0.385(7) 1 calc R U P A 2 H2E H 0.721543 0.623363 0.635545 0.042 Uiso 0.385(7) 1 calc R U P A 2 N3 N 0.76895(17) 0.66494(13) 0.40742(13) 0.0258(5) Uani 1 1 d . . . . . H3 H 0.766(3) 0.6290(18) 0.3775(18) 0.039 Uiso 1 1 d . U . . . N4 N 0.63696(17) 0.52108(13) 0.43229(14) 0.0309(5) Uani 1 1 d D . . . . H4 H 0.587(2) 0.5059(19) 0.4514(17) 0.046 Uiso 1 1 d D U . . . N5 N 0.21668(18) 0.81146(13) 0.33106(12) 0.0273(5) Uani 1 1 d . . . . . H5 H 0.277(3) 0.7921(19) 0.3429(17) 0.041 Uiso 1 1 d . U . . . C3 C 0.9009(2) 0.59145(18) 0.5021(2) 0.0485(9) Uani 1 1 d . . . . . H3A H 0.907171 0.545955 0.471201 0.058 Uiso 1 1 calc R U . . . H3B H 0.967767 0.597704 0.538207 0.058 Uiso 1 1 calc R U . . . C4 C 0.8789(2) 0.66598(17) 0.45399(18) 0.0360(7) Uani 1 1 d . . . . . H4A H 0.889031 0.712882 0.485368 0.043 Uiso 1 1 calc R U . . . H4B H 0.928488 0.668718 0.422374 0.043 Uiso 1 1 calc R U . . . C5 C 0.7864(3) 0.49176(18) 0.53938(18) 0.0444(8) Uani 1 1 d . . . . . H5A H 0.740879 0.482840 0.573144 0.053 Uiso 1 1 calc R U . . . H5B H 0.849251 0.459269 0.555563 0.053 Uiso 1 1 calc R U . . . C6 C 0.7289(2) 0.46770(17) 0.46167(18) 0.0382(7) Uani 1 1 d . . . . . H6A H 0.777433 0.470048 0.429328 0.046 Uiso 1 1 calc R U . . . H6B H 0.704217 0.413220 0.462172 0.046 Uiso 1 1 calc R U . . . C7 C 0.7584(2) 0.8058(2) 0.55695(17) 0.0453(8) Uani 1 1 d D . . . . H7A H 0.823815 0.806197 0.540477 0.054 Uiso 1 1 calc R U . A 1 H7B H 0.773318 0.828254 0.606468 0.054 Uiso 1 1 calc R U . A 1 C8 C 0.6796(2) 0.85811(17) 0.50644(16) 0.0351(6) Uani 1 1 d . . . . . C9 C 0.7162(3) 0.9267(2) 0.47784(19) 0.0485(9) Uani 1 1 d . . . . . H9 H 0.788454 0.936959 0.488128 0.058 Uiso 1 1 calc R U . . . C10 C 0.6470(3) 0.9791(2) 0.4348(2) 0.0538(9) Uani 1 1 d . . . . . H10 H 0.673029 1.024466 0.416456 0.065 Uiso 1 1 calc R U . . . C11 C 0.5392(3) 0.96542(17) 0.41831(17) 0.0408(7) Uani 1 1 d . . . . . H11 H 0.492617 1.001413 0.389527 0.049 Uiso 1 1 calc R U . . . C12 C 0.5016(2) 0.89704(16) 0.44544(14) 0.0304(6) Uani 1 1 d . . . . . C13 C 0.5714(2) 0.84334(16) 0.48952(14) 0.0279(6) Uani 1 1 d . . . . . H13 H 0.545459 0.797740 0.507494 0.034 Uiso 1 1 calc R U . . . C14 C 0.7471(2) 0.73787(15) 0.36021(14) 0.0277(6) Uani 1 1 d . . . . . H14A H 0.806214 0.747476 0.337826 0.033 Uiso 1 1 calc R U . . . H14B H 0.741053 0.783338 0.391168 0.033 Uiso 1 1 calc R U . . . C15 C 0.6472(2) 0.73048(14) 0.30003(14) 0.0260(5) Uani 1 1 d . . . . . C16 C 0.6443(2) 0.68453(16) 0.23678(15) 0.0345(6) Uani 1 1 d . . . . . H16 H 0.704844 0.657819 0.231653 0.041 Uiso 1 1 calc R U . . . C17 C 0.5525(3) 0.67861(17) 0.18207(15) 0.0366(7) Uani 1 1 d . . . . . H17 H 0.552116 0.647313 0.140686 0.044 Uiso 1 1 calc R U . . . C18 C 0.4607(2) 0.71797(16) 0.18688(15) 0.0314(6) Uani 1 1 d . . . . . H18 H 0.399084 0.713718 0.149554 0.038 Uiso 1 1 calc R U . . . C19 C 0.4640(2) 0.76374(16) 0.24921(15) 0.0307(6) Uani 1 1 d . . . . . C20 C 0.5558(2) 0.76961(15) 0.30537(15) 0.0287(6) Uani 1 1 d . . . . . H20 H 0.555659 0.800259 0.347055 0.034 Uiso 1 1 calc R U . . . C21 C 0.5986(2) 0.50715(18) 0.35112(16) 0.0359(6) Uani 1 1 d . . . . . H21A H 0.615628 0.452847 0.340322 0.043 Uiso 1 1 calc R U . . . H21B H 0.636835 0.542347 0.325191 0.043 Uiso 1 1 calc R U . . . C22 C 0.4821(2) 0.52008(15) 0.32119(14) 0.0268(5) Uani 1 1 d . . . . . C23 C 0.4250(2) 0.46411(18) 0.27247(17) 0.0395(7) Uani 1 1 d . . . . . H23 H 0.459500 0.420039 0.258981 0.047 Uiso 1 1 calc R U . . . C24 C 0.3178(2) 0.47332(18) 0.24399(17) 0.0402(7) Uani 1 1 d . . . . . H24 H 0.281069 0.435542 0.211161 0.048 Uiso 1 1 calc R U . . . C25 C 0.2642(2) 0.53772(16) 0.26343(15) 0.0322(6) Uani 1 1 d . . . . . H25 H 0.191696 0.543600 0.244577 0.039 Uiso 1 1 calc R U . . . C26 C 0.3211(2) 0.59306(15) 0.31160(14) 0.0282(6) Uani 1 1 d . . . . . C27 C 0.4292(2) 0.58529(15) 0.33949(15) 0.0282(6) Uani 1 1 d . . . . . H27 H 0.466244 0.624273 0.370726 0.034 Uiso 1 1 calc R U . . . C28 C 0.3204(2) 0.92760(16) 0.38811(15) 0.0350(6) Uani 1 1 d . . . . . H28A H 0.336033 0.938409 0.340498 0.042 Uiso 1 1 calc R U . . . H28B H 0.318709 0.977620 0.413932 0.042 Uiso 1 1 calc R U . . . C29 C 0.2174(2) 0.88436(16) 0.37837(16) 0.0341(6) Uani 1 1 d . . . . . H29A H 0.159745 0.919385 0.355124 0.041 Uiso 1 1 calc R U . . . H29B H 0.206906 0.868807 0.426431 0.041 Uiso 1 1 calc R U . . . C30 C 0.2770(2) 0.79088(18) 0.21421(16) 0.0368(7) Uani 1 1 d . . . . . H30A H 0.264180 0.733916 0.211615 0.044 Uiso 1 1 calc R U . . . H30B H 0.271576 0.810932 0.164471 0.044 Uiso 1 1 calc R U . . . C31 C 0.1990(2) 0.83254(17) 0.24998(14) 0.0313(6) Uani 1 1 d . . . . . H31A H 0.127664 0.817651 0.224424 0.038 Uiso 1 1 calc R U . . . H31B H 0.205916 0.889698 0.245060 0.038 Uiso 1 1 calc R U . . . C32 C 0.1649(2) 0.67031(17) 0.31168(17) 0.0353(6) Uani 1 1 d . . . . . H32A H 0.126670 0.626937 0.328012 0.042 Uiso 1 1 calc R U . . . H32B H 0.144068 0.673557 0.258056 0.042 Uiso 1 1 calc R U . . . C33 C 0.1437(2) 0.74787(16) 0.34639(17) 0.0356(6) Uani 1 1 d . . . . . H33A H 0.070887 0.763822 0.326416 0.043 Uiso 1 1 calc R U . . . H33B H 0.154157 0.740954 0.399480 0.043 Uiso 1 1 calc R U . . . N6 N 1.0730(2) 0.36719(17) 0.19121(18) 0.0513(7) Uani 1 1 d . . . . . C34 C 1.0597(2) 0.4194(2) 0.15330(18) 0.0412(7) Uani 1 1 d . . . . . C35 C 1.0405(3) 0.4901(2) 0.10460(19) 0.0544(9) Uani 1 1 d . . . . . H35A H 0.999229 0.528274 0.124125 0.082 Uiso 1 1 calc R U . . . H35B H 1.002831 0.474487 0.055769 0.082 Uiso 1 1 calc R U . . . H35C H 1.106951 0.513560 0.102272 0.082 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu1 0.01821(15) 0.02952(17) 0.02560(16) 0.00047(13) 0.00485(12) 0.00150(12) Cl1 0.0391(4) 0.0378(4) 0.0416(4) 0.0080(3) 0.0235(3) 0.0068(3) O1 0.0384(11) 0.0269(10) 0.0309(10) 0.0039(8) 0.0018(8) 0.0006(8) O2 0.0258(10) 0.0510(13) 0.0501(13) -0.0274(10) 0.0115(9) -0.0051(9) O3 0.0364(11) 0.0291(10) 0.0522(13) -0.0121(9) -0.0138(10) 0.0120(9) Cl2 0.0310(3) 0.0272(3) 0.0498(4) -0.0086(3) 0.0191(3) -0.0004(3) O4 0.094(2) 0.0378(13) 0.118(2) -0.0034(14) 0.0816(19) -0.0062(13) O5 0.0481(14) 0.0498(14) 0.0830(18) 0.0063(13) 0.0223(13) 0.0187(11) O6 0.0461(12) 0.0302(11) 0.0712(16) -0.0088(10) 0.0263(12) -0.0040(9) O7 0.0818(19) 0.0562(16) 0.0657(18) -0.0127(13) -0.0105(15) 0.0030(14) Cl3 0.0387(4) 0.0427(4) 0.0256(3) -0.0056(3) -0.0008(3) 0.0088(3) O8 0.086(2) 0.0600(17) 0.0636(17) 0.0110(14) -0.0030(15) -0.0133(14) O9 0.0587(16) 0.106(2) 0.0407(13) -0.0224(14) 0.0172(12) -0.0048(15) O10 0.0680(17) 0.0625(16) 0.0450(14) -0.0227(12) -0.0165(12) 0.0063(13) O11 0.0510(15) 0.0739(18) 0.0819(19) -0.0154(15) -0.0044(14) 0.0282(13) N1 0.0386(13) 0.0371(14) 0.0298(12) 0.0042(10) -0.0042(10) 0.0130(11) N2 0.042(3) 0.055(3) 0.023(4) -0.005(3) -0.009(2) 0.022(3) C1 0.037(3) 0.050(3) 0.027(2) 0.007(2) -0.001(2) 0.009(2) C2 0.032(2) 0.053(3) 0.023(2) 0.0000(19) -0.0030(18) 0.006(2) N2B 0.041(4) 0.051(4) 0.016(4) -0.011(3) -0.007(3) 0.017(4) C1B 0.032(4) 0.042(4) 0.025(3) 0.006(3) -0.002(3) 0.004(3) C2B 0.033(3) 0.045(3) 0.022(3) 0.006(3) -0.003(3) 0.004(3) N3 0.0266(11) 0.0228(11) 0.0300(12) -0.0008(9) 0.0110(9) -0.0032(9) N4 0.0225(11) 0.0292(12) 0.0446(14) -0.0007(10) 0.0154(10) -0.0030(9) N5 0.0253(11) 0.0293(12) 0.0261(11) 0.0014(9) 0.0036(9) 0.0102(9) C3 0.0210(14) 0.0359(17) 0.082(3) 0.0004(17) -0.0003(15) 0.0040(12) C4 0.0190(12) 0.0352(15) 0.0556(19) -0.0045(14) 0.0121(12) -0.0034(11) C5 0.0515(19) 0.0387(17) 0.0474(18) 0.0235(14) 0.0202(15) 0.0177(14) C6 0.0283(14) 0.0266(14) 0.063(2) 0.0025(14) 0.0167(14) 0.0005(11) C7 0.0272(14) 0.067(2) 0.0387(17) -0.0257(16) 0.0011(13) -0.0020(14) C8 0.0353(15) 0.0426(17) 0.0296(14) -0.0200(13) 0.0123(12) -0.0081(12) C9 0.0481(19) 0.050(2) 0.055(2) -0.0276(17) 0.0286(16) -0.0234(16) C10 0.079(3) 0.0371(18) 0.057(2) -0.0157(16) 0.040(2) -0.0253(18) C11 0.066(2) 0.0261(14) 0.0351(16) -0.0042(12) 0.0218(15) -0.0049(14) C12 0.0428(16) 0.0276(14) 0.0219(13) -0.0091(11) 0.0095(12) -0.0046(11) C13 0.0354(14) 0.0288(13) 0.0205(12) -0.0055(10) 0.0083(11) -0.0054(11) C14 0.0366(14) 0.0206(12) 0.0305(14) 0.0003(10) 0.0171(12) -0.0033(10) C15 0.0386(14) 0.0176(12) 0.0255(13) 0.0027(10) 0.0151(11) -0.0016(10) C16 0.0495(17) 0.0309(14) 0.0275(14) 0.0009(11) 0.0176(13) 0.0130(12) C17 0.0617(19) 0.0300(15) 0.0207(13) -0.0048(11) 0.0152(13) 0.0071(13) C18 0.0423(16) 0.0286(14) 0.0250(13) -0.0022(11) 0.0112(12) -0.0026(11) C19 0.0342(14) 0.0282(14) 0.0342(15) -0.0059(11) 0.0174(12) -0.0058(11) C20 0.0374(14) 0.0244(13) 0.0295(14) -0.0090(11) 0.0180(12) -0.0085(11) C21 0.0282(14) 0.0389(16) 0.0447(17) -0.0130(13) 0.0169(13) -0.0075(12) C22 0.0284(13) 0.0285(14) 0.0271(13) -0.0011(11) 0.0135(11) -0.0055(10) C23 0.0384(16) 0.0374(16) 0.0454(18) -0.0176(14) 0.0154(14) -0.0003(13) C24 0.0400(16) 0.0420(17) 0.0382(16) -0.0183(13) 0.0087(13) -0.0086(13) C25 0.0313(14) 0.0356(15) 0.0268(14) -0.0020(12) 0.0011(11) -0.0017(11) C26 0.0375(14) 0.0191(12) 0.0262(13) 0.0022(10) 0.0038(11) 0.0015(10) C27 0.0355(14) 0.0180(12) 0.0287(13) -0.0005(10) 0.0025(11) -0.0043(10) C28 0.0471(17) 0.0267(14) 0.0293(14) -0.0027(11) 0.0053(13) 0.0085(12) C29 0.0403(16) 0.0298(15) 0.0334(15) -0.0011(11) 0.0109(13) 0.0135(12) C30 0.0346(15) 0.0460(17) 0.0303(14) -0.0107(13) 0.0086(12) -0.0084(13) C31 0.0284(13) 0.0377(15) 0.0242(13) 0.0024(11) -0.0013(11) 0.0022(11) C32 0.0311(14) 0.0306(15) 0.0406(16) 0.0043(12) 0.0013(12) 0.0053(11) C33 0.0371(15) 0.0317(15) 0.0390(16) 0.0044(12) 0.0115(13) 0.0040(12) N6 0.0477(16) 0.0393(16) 0.0614(19) -0.0103(15) 0.0021(14) 0.0000(13) C34 0.0321(15) 0.050(2) 0.0396(17) -0.0118(15) 0.0037(13) -0.0038(14) C35 0.062(2) 0.059(2) 0.0426(19) -0.0008(16) 0.0115(17) -0.0101(18) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; _exptl_special_details ; One distinct cell was identified using APEX3 (Bruker, 2016). Five frame series were integrated and filtered for statistical outliers using SAINT (Bruker, 2016) then corrected for absorption by integration using SAINT/SADABS v2014/2 (Bruker, 2016) to sort, merge, and scale the combined data. No decay correction was applied. ; _publ_section_references ; Bruker (2016). APEX3, SADABS, SAINT, SHELXTL, XCIF, XPREP. Bruker AXS, Inc., Madison, Wisconsin, USA. Hubschle, C. B.; Sheldrick, G. M.; Dittrich, B. (2011), J. Appl. Cryst.,44, 1281-1284. Sheldrick, G. M. (2015). Acta Cryst. C71, 3-8. ; _publ_section_exptl_refinement ; A structural model consisting of the target complex was developed. One CH2-CH2-NH moiety of the ligand is disordered over two orientaions. The like N-C and C-C distances were restrained to be similar (esd 0.01\%A). Similar displacement amplitudes (esd 0.01) were imposed on disordered sites overlapping by less than the sum of van der Waals radii. The disordered atoms and the atoms of the anions were restrained to behave relatively isotropic. The amine/ammonium N-H hydrogen atoms were located in the difference map, except for the H atom on the disordered N2/N2B. Methyl H atom positions, R-CH~3~, were optimized by rotation about R-C bonds with idealized C-H, R--H and H--H distances. Remaining H atoms were included as riding idealized contributors. Methyl and amine H atom U's were assigned as 1.5 times U~eq~ of the carrier atom; remaining H atom U's were assigned as 1.2 times carrier U~eq~. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu1 N4 2.092(2) . ? Cu1 N2 2.104(12) . ? Cu1 N3 2.107(2) . ? Cu1 N1 2.151(2) . ? Cu1 N2B 2.215(19) . ? Cu1 Cl1 2.2847(9) . ? O1 C12 1.370(3) . ? O1 C28 1.427(3) . ? O2 C19 1.387(3) . ? O2 C30 1.435(3) . ? O3 C26 1.381(3) . ? O3 C32 1.425(3) . ? Cl2 O5 1.403(2) . ? Cl2 O4 1.424(2) . ? Cl2 O6 1.426(2) . ? Cl2 O7 1.442(3) . ? Cl3 O8 1.415(3) . ? Cl3 O9 1.415(3) . ? Cl3 O11 1.418(2) . ? Cl3 O10 1.429(2) . ? N1 C5 1.470(4) . ? N1 C3 1.474(4) . ? N1 C1B 1.517(7) . ? N1 C1 1.520(5) . ? N2 C7 1.473(6) . ? N2 C2 1.556(6) . ? N2 H2 0.9800 . ? C1 C2 1.491(6) . ? C1 H1A 0.9700 . ? C1 H1B 0.9700 . ? C2 H2A 0.9700 . ? C2 H2B 0.9700 . ? N2B C7 1.473(8) . ? N2B C2B 1.555(8) . ? N2B H2C 0.9800 . ? C1B C2B 1.476(8) . ? C1B H1C 0.9700 . ? C1B H1D 0.9700 . ? C2B H2D 0.9700 . ? C2B H2E 0.9700 . ? N3 C4 1.487(3) . ? N3 C14 1.493(3) . ? N3 H3 0.82(3) . ? N4 C21 1.490(4) . ? N4 C6 1.490(3) . ? N4 H4 0.853(18) . ? N5 C33 1.500(4) . ? N5 C29 1.506(3) . ? N5 C31 1.511(3) . ? N5 H5 0.83(3) . ? C3 C4 1.525(4) . ? C3 H3A 0.9700 . ? C3 H3B 0.9700 . ? C4 H4A 0.9700 . ? C4 H4B 0.9700 . ? C5 C6 1.515(4) . ? C5 H5A 0.9700 . ? C5 H5B 0.9700 . ? C6 H6A 0.9700 . ? C6 H6B 0.9700 . ? C7 C8 1.499(4) . ? C7 H7A 0.9700 . ? C7 H7B 0.9700 . ? C8 C13 1.389(4) . ? C8 C9 1.398(4) . ? C9 C10 1.372(5) . ? C9 H9 0.9300 . ? C10 C11 1.382(5) . ? C10 H10 0.9300 . ? C11 C12 1.388(4) . ? C11 H11 0.9300 . ? C12 C13 1.399(4) . ? C13 H13 0.9300 . ? C14 C15 1.506(4) . ? C14 H14A 0.9700 . ? C14 H14B 0.9700 . ? C15 C20 1.382(4) . ? C15 C16 1.399(4) . ? C16 C17 1.377(4) . ? C16 H16 0.9300 . ? C17 C18 1.387(4) . ? C17 H17 0.9300 . ? C18 C19 1.381(4) . ? C18 H18 0.9300 . ? C19 C20 1.391(4) . ? C20 H20 0.9300 . ? C21 C22 1.502(4) . ? C21 H21A 0.9700 . ? C21 H21B 0.9700 . ? C22 C27 1.378(4) . ? C22 C23 1.391(4) . ? C23 C24 1.378(4) . ? C23 H23 0.9300 . ? C24 C25 1.381(4) . ? C24 H24 0.9300 . ? C25 C26 1.378(4) . ? C25 H25 0.9300 . ? C26 C27 1.384(4) . ? C27 H27 0.9300 . ? C28 C29 1.497(4) . ? C28 H28A 0.9700 . ? C28 H28B 0.9700 . ? C29 H29A 0.9700 . ? C29 H29B 0.9700 . ? C30 C31 1.510(4) . ? C30 H30A 0.9700 . ? C30 H30B 0.9700 . ? C31 H31A 0.9700 . ? C31 H31B 0.9700 . ? C32 C33 1.507(4) . ? C32 H32A 0.9700 . ? C32 H32B 0.9700 . ? C33 H33A 0.9700 . ? C33 H33B 0.9700 . ? N6 C34 1.112(4) . ? C34 C35 1.478(5) . ? C35 H35A 0.9600 . ? C35 H35B 0.9600 . ? C35 H35C 0.9600 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N4 Cu1 N2 161.1(2) . . ? N4 Cu1 N3 93.59(9) . . ? N2 Cu1 N3 98.4(4) . . ? N4 Cu1 N1 84.60(9) . . ? N2 Cu1 N1 82.3(2) . . ? N3 Cu1 N1 83.43(10) . . ? N4 Cu1 N2B 158.6(3) . . ? N3 Cu1 N2B 100.1(6) . . ? N1 Cu1 N2B 80.7(3) . . ? N4 Cu1 Cl1 89.18(6) . . ? N2 Cu1 Cl1 85.3(4) . . ? N3 Cu1 Cl1 157.71(6) . . ? N1 Cu1 Cl1 118.86(8) . . ? N2B Cu1 Cl1 84.3(6) . . ? C12 O1 C28 118.3(2) . . ? C19 O2 C30 117.1(2) . . ? C26 O3 C32 118.5(2) . . ? O5 Cl2 O4 112.01(17) . . ? O5 Cl2 O6 111.96(15) . . ? O4 Cl2 O6 110.69(14) . . ? O5 Cl2 O7 108.21(17) . . ? O4 Cl2 O7 106.42(19) . . ? O6 Cl2 O7 107.25(16) . . ? O8 Cl3 O9 108.58(19) . . ? O8 Cl3 O11 110.48(19) . . ? O9 Cl3 O11 109.40(18) . . ? O8 Cl3 O10 108.89(16) . . ? O9 Cl3 O10 109.83(17) . . ? O11 Cl3 O10 109.65(16) . . ? C5 N1 C3 112.5(2) . . ? C5 N1 C1B 126.3(4) . . ? C3 N1 C1B 96.3(4) . . ? C5 N1 C1 105.5(3) . . ? C3 N1 C1 124.3(3) . . ? C5 N1 Cu1 103.10(18) . . ? C3 N1 Cu1 108.47(18) . . ? C1B N1 Cu1 109.4(3) . . ? C1 N1 Cu1 100.4(2) . . ? C7 N2 C2 96.9(4) . . ? C7 N2 Cu1 133.7(9) . . ? C2 N2 Cu1 109.7(6) . . ? C7 N2 H2 104.5 . . ? C2 N2 H2 104.5 . . ? Cu1 N2 H2 104.5 . . ? C2 C1 N1 108.2(4) . . ? C2 C1 H1A 110.1 . . ? N1 C1 H1A 110.1 . . ? C2 C1 H1B 110.1 . . ? N1 C1 H1B 110.1 . . ? H1A C1 H1B 108.4 . . ? C1 C2 N2 107.0(4) . . ? C1 C2 H2A 110.3 . . ? N2 C2 H2A 110.3 . . ? C1 C2 H2B 110.3 . . ? N2 C2 H2B 110.3 . . ? H2A C2 H2B 108.6 . . ? C7 N2B C2B 130.4(9) . . ? C7 N2B Cu1 125.6(13) . . ? C2B N2B Cu1 96.0(7) . . ? C7 N2B H2C 99.2 . . ? C2B N2B H2C 99.2 . . ? Cu1 N2B H2C 99.2 . . ? C2B C1B N1 105.2(6) . . ? C2B C1B H1C 110.7 . . ? N1 C1B H1C 110.7 . . ? C2B C1B H1D 110.7 . . ? N1 C1B H1D 110.7 . . ? H1C C1B H1D 108.8 . . ? C1B C2B N2B 106.1(10) . . ? C1B C2B H2D 110.5 . . ? N2B C2B H2D 110.5 . . ? C1B C2B H2E 110.5 . . ? N2B C2B H2E 110.5 . . ? H2D C2B H2E 108.7 . . ? C4 N3 C14 110.8(2) . . ? C4 N3 Cu1 104.96(17) . . ? C14 N3 Cu1 121.72(16) . . ? C4 N3 H3 107(2) . . ? C14 N3 H3 104(2) . . ? Cu1 N3 H3 108(2) . . ? C21 N4 C6 108.9(2) . . ? C21 N4 Cu1 124.20(18) . . ? C6 N4 Cu1 107.51(17) . . ? C21 N4 H4 106(2) . . ? C6 N4 H4 107(2) . . ? Cu1 N4 H4 102(2) . . ? C33 N5 C29 112.6(2) . . ? C33 N5 C31 113.7(2) . . ? C29 N5 C31 111.7(2) . . ? C33 N5 H5 106(2) . . ? C29 N5 H5 107(2) . . ? C31 N5 H5 106(2) . . ? N1 C3 C4 111.8(2) . . ? N1 C3 H3A 109.3 . . ? C4 C3 H3A 109.3 . . ? N1 C3 H3B 109.3 . . ? C4 C3 H3B 109.3 . . ? H3A C3 H3B 107.9 . . ? N3 C4 C3 110.7(2) . . ? N3 C4 H4A 109.5 . . ? C3 C4 H4A 109.5 . . ? N3 C4 H4B 109.5 . . ? C3 C4 H4B 109.5 . . ? H4A C4 H4B 108.1 . . ? N1 C5 C6 110.2(2) . . ? N1 C5 H5A 109.6 . . ? C6 C5 H5A 109.6 . . ? N1 C5 H5B 109.6 . . ? C6 C5 H5B 109.6 . . ? H5A C5 H5B 108.1 . . ? N4 C6 C5 111.2(2) . . ? N4 C6 H6A 109.4 . . ? C5 C6 H6A 109.4 . . ? N4 C6 H6B 109.4 . . ? C5 C6 H6B 109.4 . . ? H6A C6 H6B 108.0 . . ? N2B C7 C8 117.9(4) . . ? N2 C7 C8 114.3(3) . . ? N2 C7 H7A 108.7 . . ? C8 C7 H7A 108.7 . . ? N2 C7 H7B 108.7 . . ? C8 C7 H7B 108.7 . . ? H7A C7 H7B 107.6 . . ? C13 C8 C9 118.6(3) . . ? C13 C8 C7 122.9(3) . . ? C9 C8 C7 118.4(3) . . ? C10 C9 C8 120.9(3) . . ? C10 C9 H9 119.5 . . ? C8 C9 H9 119.5 . . ? C9 C10 C11 120.9(3) . . ? C9 C10 H10 119.5 . . ? C11 C10 H10 119.5 . . ? C10 C11 C12 118.9(3) . . ? C10 C11 H11 120.6 . . ? C12 C11 H11 120.6 . . ? O1 C12 C11 124.7(3) . . ? O1 C12 C13 114.7(2) . . ? C11 C12 C13 120.6(3) . . ? C8 C13 C12 120.0(3) . . ? C8 C13 H13 120.0 . . ? C12 C13 H13 120.0 . . ? N3 C14 C15 112.3(2) . . ? N3 C14 H14A 109.1 . . ? C15 C14 H14A 109.1 . . ? N3 C14 H14B 109.1 . . ? C15 C14 H14B 109.1 . . ? H14A C14 H14B 107.9 . . ? C20 C15 C16 118.0(3) . . ? C20 C15 C14 120.9(2) . . ? C16 C15 C14 121.0(2) . . ? C17 C16 C15 120.4(3) . . ? C17 C16 H16 119.8 . . ? C15 C16 H16 119.8 . . ? C16 C17 C18 121.9(2) . . ? C16 C17 H17 119.1 . . ? C18 C17 H17 119.1 . . ? C19 C18 C17 117.5(3) . . ? C19 C18 H18 121.3 . . ? C17 C18 H18 121.3 . . ? C18 C19 O2 124.0(3) . . ? C18 C19 C20 121.3(3) . . ? O2 C19 C20 114.7(2) . . ? C15 C20 C19 120.8(2) . . ? C15 C20 H20 119.6 . . ? C19 C20 H20 119.6 . . ? N4 C21 C22 114.8(2) . . ? N4 C21 H21A 108.6 . . ? C22 C21 H21A 108.6 . . ? N4 C21 H21B 108.6 . . ? C22 C21 H21B 108.6 . . ? H21A C21 H21B 107.6 . . ? C27 C22 C23 118.4(2) . . ? C27 C22 C21 122.9(2) . . ? C23 C22 C21 118.7(2) . . ? C24 C23 C22 120.7(3) . . ? C24 C23 H23 119.7 . . ? C22 C23 H23 119.7 . . ? C23 C24 C25 121.0(3) . . ? C23 C24 H24 119.5 . . ? C25 C24 H24 119.5 . . ? C26 C25 C24 118.0(3) . . ? C26 C25 H25 121.0 . . ? C24 C25 H25 121.0 . . ? C25 C26 O3 123.5(2) . . ? C25 C26 C27 121.5(2) . . ? O3 C26 C27 115.0(2) . . ? C22 C27 C26 120.3(2) . . ? C22 C27 H27 119.8 . . ? C26 C27 H27 119.8 . . ? O1 C28 C29 104.9(2) . . ? O1 C28 H28A 110.8 . . ? C29 C28 H28A 110.8 . . ? O1 C28 H28B 110.8 . . ? C29 C28 H28B 110.8 . . ? H28A C28 H28B 108.8 . . ? C28 C29 N5 110.3(2) . . ? C28 C29 H29A 109.6 . . ? N5 C29 H29A 109.6 . . ? C28 C29 H29B 109.6 . . ? N5 C29 H29B 109.6 . . ? H29A C29 H29B 108.1 . . ? O2 C30 C31 105.4(2) . . ? O2 C30 H30A 110.7 . . ? C31 C30 H30A 110.7 . . ? O2 C30 H30B 110.7 . . ? C31 C30 H30B 110.7 . . ? H30A C30 H30B 108.8 . . ? C30 C31 N5 111.7(2) . . ? C30 C31 H31A 109.3 . . ? N5 C31 H31A 109.3 . . ? C30 C31 H31B 109.3 . . ? N5 C31 H31B 109.3 . . ? H31A C31 H31B 107.9 . . ? O3 C32 C33 104.6(2) . . ? O3 C32 H32A 110.8 . . ? C33 C32 H32A 110.8 . . ? O3 C32 H32B 110.8 . . ? C33 C32 H32B 110.8 . . ? H32A C32 H32B 108.9 . . ? N5 C33 C32 110.2(2) . . ? N5 C33 H33A 109.6 . . ? C32 C33 H33A 109.6 . . ? N5 C33 H33B 109.6 . . ? C32 C33 H33B 109.6 . . ? H33A C33 H33B 108.1 . . ? N6 C34 C35 178.2(4) . . ? C34 C35 H35A 109.5 . . ? C34 C35 H35B 109.5 . . ? H35A C35 H35B 109.5 . . ? C34 C35 H35C 109.5 . . ? H35A C35 H35C 109.5 . . ? H35B C35 H35C 109.5 . . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A _geom_hbond_publ_flag N3 H3 O4 0.82(3) 2.36(3) 3.122(3) 155(3) . yes N4 H4 Cl1 0.853(18) 2.68(3) 3.076(2) 110(2) . yes N4 H4 Cl1 0.853(18) 2.75(2) 3.465(2) 142(3) 3_666 yes N5 H5 O1 0.83(3) 2.42(3) 2.836(3) 112(3) . yes N5 H5 O2 0.83(3) 2.27(3) 2.737(3) 116(3) . yes N5 H5 O3 0.83(3) 2.24(3) 2.670(3) 113(3) . yes _refine_diff_density_max 0.758 _refine_diff_density_min -0.516 _refine_diff_density_rms 0.073 _shelx_res_file ; TITL 14_a.res in P2(1)/c 14_a.res created by SHELXL-2018/3 at 14:10:52 on 12-Jun-2019 REM Old TITL 14 in P2(1)/c REM SHELXT solution in P2(1)/c REM R1 0.160, Rweak 0.008, Alpha 0.046, Orientation as input REM Formula found by SHELXT: C45 Cl3 Cu N5 O2 CELL 0.71073 13.0067 16.7879 18.5737 90.000 103.666 90.000 ZERR 4.000 0.0040 0.0048 0.0055 0.000 0.009 0.000 LATT 1 SYMM -X, 1/2+Y, 1/2-Z SFAC C H N O CL CU UNIT 140 196 24 44 12 4 TEMP 20.000 SIZE 0.085 0.185 0.22 L.S. 20 BOND $H ACTA HTAB HTAB N3 O4 HTAB N4 Cl1 EQIV $3 -x+1, -y+1, -z+1 HTAB N4 Cl1_$3 HTAB N5 O1 HTAB N5 O2 HTAB N5 O3 ISOR 0.01 0.01 CL2 > O11 SIMU 0.01 0.02 N2 > C2B ISOR 0.01 N2 > C2B SADI 0.01 N1 C1 N1 C1B SADI 0.01 C7 N2 C7 N2B DFIX 0.88 0.02 N4 H4 OMIT 0 1 1 OMIT 1 0 0 BUMP LIST 4 FMAP 2 PLAN 20 WGHT 0.054200 3.038400 FVAR 0.31632 0.61529 CU1 6 0.674000 0.633270 0.480456 11.00000 0.01821 0.02952 = 0.02560 0.00047 0.00485 0.00150 CL1 5 0.525731 0.626673 0.526045 11.00000 0.03908 0.03781 = 0.04162 0.00800 0.02351 0.00677 O1 4 0.397301 0.875050 0.430967 11.00000 0.03836 0.02689 = 0.03087 0.00391 0.00178 0.00063 O2 4 0.379375 0.808082 0.260770 11.00000 0.02581 0.05100 = 0.05011 -0.02738 0.01149 -0.00511 O3 4 0.276273 0.658974 0.336493 11.00000 0.03637 0.02910 = 0.05225 -0.01211 -0.01377 0.01196 CL2 5 0.899818 0.560814 0.267387 11.00000 0.03098 0.02718 = 0.04982 -0.00855 0.01913 -0.00040 O4 4 0.834411 0.529347 0.312151 11.00000 0.09366 0.03781 = 0.11805 -0.00339 0.08165 -0.00624 O5 4 0.994543 0.518019 0.275838 11.00000 0.04809 0.04975 = 0.08302 0.00630 0.02234 0.01871 O6 4 0.918278 0.643724 0.281422 11.00000 0.04607 0.03020 = 0.07120 -0.00876 0.02635 -0.00398 O7 4 0.840840 0.552876 0.191557 11.00000 0.08181 0.05624 = 0.06574 -0.01273 -0.01045 0.00296 CL3 5 0.894314 0.297101 -0.055300 11.00000 0.03870 0.04265 = 0.02556 -0.00562 -0.00078 0.00877 O8 4 0.870762 0.220317 -0.032231 11.00000 0.08575 0.05999 = 0.06357 0.01097 -0.00295 -0.01328 O9 4 0.936188 0.289076 -0.118632 11.00000 0.05870 0.10616 = 0.04065 -0.02239 0.01723 -0.00478 O10 4 0.970767 0.333814 0.003322 11.00000 0.06804 0.06248 = 0.04504 -0.02266 -0.01649 0.00632 O11 4 0.801600 0.344553 -0.073173 11.00000 0.05096 0.07391 = 0.08186 -0.01541 -0.00435 0.02825 N1 3 0.816410 0.576265 0.540994 11.00000 0.03864 0.03714 = 0.02983 0.00417 -0.00424 0.01300 PART 1 21 N2 3 0.723699 0.722684 0.560456 21.00000 0.04208 0.05477 = 0.02327 -0.00547 -0.00934 0.02180 AFIX 13 H2 2 0.667219 0.725522 0.587171 21.00000 -1.20000 AFIX 0 C1 1 0.818809 0.604691 0.619050 21.00000 0.03708 0.05024 = 0.02652 0.00726 -0.00092 0.00862 AFIX 23 H1A 2 0.756225 0.586316 0.633954 21.00000 -1.20000 H1B 2 0.880662 0.583548 0.653590 21.00000 -1.20000 AFIX 0 C2 1 0.822291 0.693485 0.619458 21.00000 0.03161 0.05267 = 0.02270 -0.00005 -0.00301 0.00640 AFIX 23 H2A 2 0.886702 0.712075 0.607220 21.00000 -1.20000 H2B 2 0.820416 0.713715 0.668050 21.00000 -1.20000 AFIX 0 PART 2 -21 SAME 0.01 N2 > C2 N2B 3 0.726877 0.723408 0.568497 -21.00000 0.04143 0.05059 = 0.01596 -0.01058 -0.00661 0.01738 AFIX 13 H2C 2 0.659079 0.734063 0.581007 -21.00000 -1.20000 AFIX 0 C1B 1 0.864591 0.624940 0.609452 -21.00000 0.03206 0.04242 = 0.02495 0.00637 -0.00245 0.00369 AFIX 23 H1C 2 0.903220 0.590931 0.648881 -21.00000 -1.20000 H1D 2 0.912545 0.664855 0.598384 -21.00000 -1.20000 AFIX 0 C2B 1 0.774003 0.662938 0.631046 -21.00000 0.03295 0.04536 = 0.02216 0.00650 -0.00259 0.00409 AFIX 23 H2D 2 0.797223 0.690149 0.678164 -21.00000 -1.20000 H2E 2 0.721543 0.623363 0.635545 -21.00000 -1.20000 AFIX 0 PART 0 N3 3 0.768949 0.664944 0.407419 11.00000 0.02656 0.02279 = 0.03005 -0.00082 0.01097 -0.00322 H3 2 0.765677 0.628966 0.377472 11.00000 -1.50000 N4 3 0.636962 0.521077 0.432287 11.00000 0.02252 0.02918 = 0.04463 -0.00069 0.01536 -0.00301 H4 2 0.586710 0.505889 0.451377 11.00000 -1.50000 N5 3 0.216685 0.811456 0.331056 11.00000 0.02532 0.02925 = 0.02615 0.00136 0.00365 0.01021 H5 2 0.277045 0.792079 0.342919 11.00000 -1.50000 C3 1 0.900950 0.591450 0.502086 11.00000 0.02097 0.03590 = 0.08248 0.00042 -0.00035 0.00399 AFIX 23 H3A 2 0.907171 0.545955 0.471201 11.00000 -1.20000 H3B 2 0.967767 0.597704 0.538207 11.00000 -1.20000 AFIX 0 C4 1 0.878942 0.665977 0.453985 11.00000 0.01896 0.03521 = 0.05560 -0.00449 0.01207 -0.00343 AFIX 23 H4A 2 0.889031 0.712882 0.485368 11.00000 -1.20000 H4B 2 0.928488 0.668718 0.422374 11.00000 -1.20000 AFIX 0 C5 1 0.786356 0.491759 0.539379 11.00000 0.05152 0.03873 = 0.04735 0.02346 0.02023 0.01775 AFIX 23 H5A 2 0.740879 0.482840 0.573144 11.00000 -1.20000 H5B 2 0.849251 0.459269 0.555563 11.00000 -1.20000 AFIX 0 C6 1 0.728864 0.467705 0.461674 11.00000 0.02831 0.02657 = 0.06277 0.00248 0.01673 0.00046 AFIX 23 H6A 2 0.777433 0.470048 0.429328 11.00000 -1.20000 H6B 2 0.704217 0.413220 0.462172 11.00000 -1.20000 AFIX 0 C7 1 0.758384 0.805840 0.556947 11.00000 0.02719 0.06651 = 0.03873 -0.02566 0.00109 -0.00202 AFIX 23 H7A 2 0.823815 0.806197 0.540477 11.00000 -1.20000 H7B 2 0.773318 0.828254 0.606468 11.00000 -1.20000 AFIX 0 C8 1 0.679555 0.858110 0.506445 11.00000 0.03531 0.04261 = 0.02958 -0.01999 0.01231 -0.00809 C9 1 0.716182 0.926706 0.477837 11.00000 0.04812 0.05015 = 0.05541 -0.02759 0.02861 -0.02345 AFIX 43 H9 2 0.788454 0.936959 0.488128 11.00000 -1.20000 AFIX 0 C10 1 0.647005 0.979107 0.434794 11.00000 0.07947 0.03710 = 0.05685 -0.01571 0.04031 -0.02530 AFIX 43 H10 2 0.673029 1.024466 0.416456 11.00000 -1.20000 AFIX 0 C11 1 0.539195 0.965421 0.418311 11.00000 0.06615 0.02611 = 0.03514 -0.00420 0.02181 -0.00495 AFIX 43 H11 2 0.492617 1.001413 0.389527 11.00000 -1.20000 AFIX 0 C12 1 0.501596 0.897042 0.445444 11.00000 0.04276 0.02758 = 0.02190 -0.00911 0.00945 -0.00460 C13 1 0.571430 0.843340 0.489519 11.00000 0.03539 0.02877 = 0.02050 -0.00547 0.00832 -0.00543 AFIX 43 H13 2 0.545459 0.797740 0.507494 11.00000 -1.20000 AFIX 0 C14 1 0.747114 0.737867 0.360215 11.00000 0.03664 0.02061 = 0.03051 0.00033 0.01712 -0.00333 AFIX 23 H14A 2 0.806214 0.747476 0.337826 11.00000 -1.20000 H14B 2 0.741053 0.783338 0.391168 11.00000 -1.20000 AFIX 0 C15 1 0.647167 0.730480 0.300027 11.00000 0.03860 0.01761 = 0.02553 0.00269 0.01506 -0.00161 C16 1 0.644340 0.684532 0.236780 11.00000 0.04946 0.03089 = 0.02750 0.00094 0.01757 0.01305 AFIX 43 H16 2 0.704844 0.657819 0.231653 11.00000 -1.20000 AFIX 0 C17 1 0.552536 0.678611 0.182069 11.00000 0.06173 0.03002 = 0.02070 -0.00485 0.01521 0.00708 AFIX 43 H17 2 0.552116 0.647313 0.140686 11.00000 -1.20000 AFIX 0 C18 1 0.460661 0.717973 0.186883 11.00000 0.04229 0.02858 = 0.02500 -0.00223 0.01123 -0.00265 AFIX 43 H18 2 0.399084 0.713718 0.149554 11.00000 -1.20000 AFIX 0 C19 1 0.464043 0.763739 0.249208 11.00000 0.03422 0.02825 = 0.03420 -0.00587 0.01744 -0.00575 C20 1 0.555794 0.769609 0.305369 11.00000 0.03735 0.02436 = 0.02953 -0.00897 0.01800 -0.00849 AFIX 43 H20 2 0.555659 0.800259 0.347055 11.00000 -1.20000 AFIX 0 C21 1 0.598646 0.507146 0.351119 11.00000 0.02820 0.03889 = 0.04466 -0.01302 0.01691 -0.00749 AFIX 23 H21A 2 0.615628 0.452847 0.340322 11.00000 -1.20000 H21B 2 0.636835 0.542347 0.325191 11.00000 -1.20000 AFIX 0 C22 1 0.482117 0.520081 0.321192 11.00000 0.02839 0.02851 = 0.02706 -0.00108 0.01346 -0.00545 C23 1 0.424985 0.464115 0.272466 11.00000 0.03839 0.03735 = 0.04542 -0.01760 0.01543 -0.00032 AFIX 43 H23 2 0.459500 0.420039 0.258981 11.00000 -1.20000 AFIX 0 C24 1 0.317835 0.473316 0.243994 11.00000 0.03996 0.04203 = 0.03822 -0.01826 0.00868 -0.00862 AFIX 43 H24 2 0.281069 0.435542 0.211161 11.00000 -1.20000 AFIX 0 C25 1 0.264167 0.537725 0.263431 11.00000 0.03133 0.03559 = 0.02678 -0.00201 0.00111 -0.00167 AFIX 43 H25 2 0.191696 0.543600 0.244577 11.00000 -1.20000 AFIX 0 C26 1 0.321150 0.593060 0.311597 11.00000 0.03751 0.01906 = 0.02621 0.00218 0.00375 0.00152 C27 1 0.429201 0.585291 0.339490 11.00000 0.03555 0.01799 = 0.02866 -0.00047 0.00254 -0.00426 AFIX 43 H27 2 0.466244 0.624273 0.370726 11.00000 -1.20000 AFIX 0 C28 1 0.320445 0.927595 0.388112 11.00000 0.04711 0.02666 = 0.02927 -0.00274 0.00535 0.00848 AFIX 23 H28A 2 0.336033 0.938409 0.340498 11.00000 -1.20000 H28B 2 0.318709 0.977620 0.413932 11.00000 -1.20000 AFIX 0 C29 1 0.217366 0.884363 0.378372 11.00000 0.04029 0.02977 = 0.03344 -0.00114 0.01089 0.01354 AFIX 23 H29A 2 0.159745 0.919385 0.355124 11.00000 -1.20000 H29B 2 0.206906 0.868807 0.426431 11.00000 -1.20000 AFIX 0 C30 1 0.277032 0.790878 0.214210 11.00000 0.03458 0.04602 = 0.03028 -0.01069 0.00859 -0.00841 AFIX 23 H30A 2 0.264180 0.733916 0.211615 11.00000 -1.20000 H30B 2 0.271576 0.810932 0.164471 11.00000 -1.20000 AFIX 0 C31 1 0.199013 0.832545 0.249981 11.00000 0.02835 0.03771 = 0.02421 0.00243 -0.00133 0.00219 AFIX 23 H31A 2 0.127664 0.817651 0.224424 11.00000 -1.20000 H31B 2 0.205916 0.889698 0.245060 11.00000 -1.20000 AFIX 0 C32 1 0.164913 0.670309 0.311680 11.00000 0.03109 0.03060 = 0.04064 0.00431 0.00128 0.00533 AFIX 23 H32A 2 0.126670 0.626937 0.328012 11.00000 -1.20000 H32B 2 0.144068 0.673557 0.258056 11.00000 -1.20000 AFIX 0 C33 1 0.143730 0.747875 0.346394 11.00000 0.03711 0.03175 = 0.03903 0.00436 0.01147 0.00404 AFIX 23 H33A 2 0.070887 0.763822 0.326416 11.00000 -1.20000 H33B 2 0.154157 0.740954 0.399480 11.00000 -1.20000 AFIX 0 N6 3 1.073015 0.367195 0.191213 11.00000 0.04774 0.03934 = 0.06142 -0.01033 0.00211 -0.00001 C34 1 1.059663 0.419411 0.153303 11.00000 0.03211 0.04952 = 0.03963 -0.01181 0.00368 -0.00383 C35 1 1.040490 0.490125 0.104603 11.00000 0.06173 0.05853 = 0.04256 -0.00077 0.01152 -0.01012 AFIX 137 H35A 2 0.999229 0.528274 0.124125 11.00000 -1.50000 H35B 2 1.002831 0.474487 0.055769 11.00000 -1.50000 H35C 2 1.106951 0.513560 0.102272 11.00000 -1.50000 REM ##### AFIX 0 HKLF 4 REM 14_a.res in P2(1)/c REM wR2 = 0.121944, GooF = S = 1.01909, Restrained GooF = 1.03300 for all data REM R1 = 0.044722 for 6935 Fo > 4sig(Fo) and 0.074600 for all 9841 data REM 543 parameters refined using 173 restraints END WGHT 0.0542 3.0336 REM Instructions for potential hydrogen bonds EQIV $1 -x+2, -y+1, -z+1 HTAB C1 O5_$1 EQIV $2 -x+2, y+1/2, -z+1/2 HTAB C2 O9_$2 HTAB N2B Cl1 HTAB C1B O5_$1 HTAB C2B Cl1 HTAB N3 O4 HTAB N4 Cl1_$3 HTAB N5 O1 HTAB N5 O2 HTAB N5 O3 HTAB C4 O6 HTAB C6 O4 EQIV $4 x, -y+3/2, z+1/2 HTAB C7 O7_$4 HTAB C13 Cl1 HTAB C14 O6 HTAB C14 N6_$2 HTAB C21 O4 HTAB C27 Cl1 EQIV $5 -x+1, y+1/2, -z+1/2 HTAB C29 O7_$5 HTAB C30 O3 EQIV $6 -x+1, -y+1, -z HTAB C31 O9_$6 HTAB C31 O4_$5 EQIV $7 x-1, y, z HTAB C32 O5_$7 HTAB C32 O6_$7 HTAB C32 O9_$6 HTAB C33 N6_$5 HTAB C33 O8_$5 HTAB C35 O10 REM Highest difference peak 0.758, deepest hole -0.516, 1-sigma level 0.073 Q1 1 0.9765 0.5404 0.3550 11.00000 0.05 0.76 Q2 1 0.9228 0.5292 0.3030 11.00000 0.05 0.63 Q3 1 0.4923 0.6159 0.4829 11.00000 0.05 0.57 Q4 1 0.7963 0.5312 0.2522 11.00000 0.05 0.51 Q5 1 1.0672 0.3722 0.1408 11.00000 0.05 0.48 Q6 1 0.7993 0.2433 -0.0382 11.00000 0.05 0.48 Q7 1 0.9501 0.5264 0.2180 11.00000 0.05 0.43 Q8 1 0.6838 0.7098 0.5673 11.00000 0.05 0.40 Q9 1 0.9208 0.2281 -0.0941 11.00000 0.05 0.40 Q10 1 0.9817 0.5433 0.0974 11.00000 0.05 0.38 Q11 1 0.6330 0.6914 0.2775 11.00000 0.05 0.37 Q12 1 0.6246 0.8603 0.5002 11.00000 0.05 0.35 Q13 1 0.9520 0.4689 0.2487 11.00000 0.05 0.34 Q14 1 0.5398 0.8638 0.4579 11.00000 0.05 0.33 Q15 1 0.5208 0.7143 0.1909 11.00000 0.05 0.33 Q16 1 0.5315 0.5112 0.3398 11.00000 0.05 0.32 Q17 1 0.5134 0.7742 0.2702 11.00000 0.05 0.32 Q18 1 0.4617 0.5020 0.2931 11.00000 0.05 0.31 Q19 1 0.9331 0.6343 0.2412 11.00000 0.05 0.30 Q20 1 0.7029 0.8289 0.5300 11.00000 0.05 0.30 ; _shelx_res_checksum 38843 _shelx_hkl_file ; 1 0 0 -0.20 0.30 1 0 0 0.50 0.60 1 0 0 0.10 0.20 1 0 0 0.40 0.60 1 0 0 0.80 0.60 -1 0 0 0.20 0.30 -1 0 0 -0.10 0.50 -1 0 0 0.10 0.50 -2 0 0 1558.74 43.20 -2 0 0 1597.44 40.90 -2 0 0 1605.84 42.30 2 0 0 1547.05 42.30 -2 0 0 1562.24 41.20 -2 0 0 1590.24 42.00 2 0 0 1584.64 42.20 3 0 0 332.77 11.90 3 0 0 337.27 10.80 -3 0 0 305.57 12.90 -3 0 0 332.07 10.20 -3 0 0 318.87 10.70 -3 0 0 330.77 11.80 3 0 0 317.47 13.00 3 0 0 321.07 10.30 3 0 0 346.47 12.40 -4 0 0 129.49 8.90 -4 0 0 148.49 6.20 4 0 0 135.09 9.00 4 0 0 153.18 6.50 4 0 0 144.89 8.40 4 0 0 142.09 6.80 -4 0 0 147.89 8.30 -4 0 0 138.19 7.80 -4 0 0 156.68 7.00 5 0 0 2133.29 63.19 5 0 0 2156.48 60.89 -5 0 0 2176.28 63.39 -5 0 0 2215.08 57.59 -5 0 0 2283.07 63.69 -5 0 0 2124.89 58.59 -5 0 0 2277.37 63.19 5 0 0 2158.38 58.79 5 0 0 2099.59 57.79 5 0 0 2140.89 61.39 -6 0 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60.19 4.60 3 -4 0 55.89 4.80 -3 -4 0 57.99 5.60 -3 -4 0 63.19 4.80 3 -4 0 53.19 5.30 -3 4 0 65.69 6.30 -3 4 0 66.19 4.90 3 4 0 55.79 5.40 3 4 0 64.49 5.00 3 4 0 60.79 5.10 3 4 0 64.39 4.30 -3 4 0 47.50 4.80 -3 4 0 77.89 6.30 -4 -4 0 -1.40 2.40 4 -4 0 0.60 2.50 4 -4 0 3.10 3.20 -4 -4 0 0.10 2.20 4 -4 0 1.90 2.70 -4 -4 0 -3.10 2.00 4 -4 0 -2.00 2.60 -4 -4 0 0.60 3.20 -4 4 0 1.50 2.50 4 4 0 -2.50 2.20 4 4 0 -3.20 1.60 4 4 0 4.00 2.80 -4 4 0 -0.60 2.10 -4 4 0 -0.20 2.50 4 4 0 0.00 2.20 -4 4 0 -2.00 2.70 -5 -4 0 500.45 20.60 -5 -4 0 483.35 18.20 5 -4 0 463.45 19.10 -5 -4 0 501.15 20.30 -5 -4 0 455.75 16.20 5 -4 0 488.55 18.30 5 -4 0 518.75 18.50 5 4 0 461.75 19.70 5 4 0 490.65 18.90 -5 4 0 494.35 20.40 5 4 0 497.35 18.40 5 4 0 502.05 16.40 -5 4 0 488.05 18.40 -6 -4 0 365.56 13.90 6 -4 0 356.26 17.20 -6 -4 0 381.36 18.80 6 -4 0 368.96 16.10 6 -4 0 365.56 15.70 6 4 0 374.36 17.00 -6 4 0 381.86 15.90 6 4 0 359.26 16.30 6 4 0 380.86 14.00 -6 4 0 377.86 18.50 7 -4 0 418.76 18.70 7 -4 0 456.55 20.60 7 -4 0 445.56 18.20 -7 -4 0 421.86 16.20 -7 -4 0 441.76 21.80 -7 -4 0 421.46 13.40 7 4 0 433.76 19.60 7 4 0 442.76 19.30 -7 4 0 427.26 18.00 -7 4 0 422.06 21.50 7 4 0 463.55 16.60 -8 -4 0 854.21 27.30 8 -4 0 808.12 30.30 8 -4 0 798.82 31.80 -8 -4 0 847.62 23.40 8 -4 0 836.22 29.40 -8 -4 0 861.21 34.50 8 4 0 797.12 31.20 8 4 0 807.72 31.10 -8 4 0 874.11 34.90 -8 4 0 876.41 29.80 9 -4 0 180.78 15.50 -9 -4 0 189.28 6.90 9 -4 0 161.28 12.00 -9 -4 0 190.08 17.10 -9 -4 0 175.88 10.80 9 -4 0 196.08 13.90 9 4 0 187.38 15.80 -9 4 0 192.08 13.50 9 4 0 166.18 14.10 -9 4 0 146.49 15.10 -10 -4 0 112.69 15.70 10 -4 0 113.69 11.10 10 -4 0 102.69 12.00 10 -4 0 106.99 13.50 -10 -4 0 77.89 8.40 10 4 0 104.19 11.90 10 4 0 104.39 12.80 -10 4 0 102.79 11.00 -10 4 0 114.09 15.50 -11 -4 0 383.56 26.10 11 -4 0 383.56 23.40 11 -4 0 338.17 20.90 11 -4 0 357.46 18.70 -11 -4 0 353.26 16.60 -11 4 0 360.76 19.20 -11 4 0 354.36 25.30 11 4 0 356.86 21.90 11 4 0 368.66 21.80 12 -4 0 163.18 17.80 -12 -4 0 129.69 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421.46 17.50 3 -8 0 427.36 15.20 -3 -8 0 410.36 14.60 3 8 0 441.46 13.90 -3 8 0 407.16 15.60 3 8 0 417.46 16.50 -3 8 0 426.36 17.90 3 8 0 438.46 17.60 -4 -8 0 159.68 9.90 4 -8 0 181.48 9.50 -4 -8 0 177.28 11.90 4 -8 0 172.28 10.30 -4 -8 0 182.98 9.90 -4 -8 0 161.18 8.20 4 -8 0 175.28 11.60 -4 -8 0 175.88 9.70 4 8 0 149.88 10.00 -4 8 0 165.68 11.20 4 8 0 155.98 8.40 -4 8 0 156.18 11.50 4 8 0 174.88 11.20 -5 -8 0 42.10 5.30 5 -8 0 47.70 6.70 -5 -8 0 38.00 5.10 5 -8 0 39.90 7.40 -5 -8 0 45.30 7.30 -5 -8 0 36.40 5.60 5 -8 0 48.60 6.10 5 8 0 37.20 5.10 5 8 0 40.80 7.00 5 8 0 34.80 6.20 -5 8 0 25.60 5.90 6 -8 0 964.90 31.40 -6 -8 0 928.71 30.20 -6 -8 0 928.71 28.60 -6 -8 0 955.10 34.50 6 -8 0 908.81 32.70 6 -8 0 994.30 34.30 6 8 0 907.21 30.60 -6 8 0 919.71 34.80 6 8 0 920.81 32.80 7 -8 0 48.30 7.30 -7 -8 0 35.80 6.10 7 -8 0 30.00 7.70 -7 -8 0 46.70 5.40 7 -8 0 32.70 7.20 -7 -8 0 55.39 9.70 -7 8 0 50.99 9.30 7 8 0 40.90 6.60 7 8 0 45.70 8.30 -8 -8 0 77.89 8.20 8 -8 0 63.19 9.70 8 -8 0 75.49 10.90 -8 -8 0 67.19 11.50 8 -8 0 77.69 9.60 -8 -8 0 73.39 6.00 -8 8 0 61.49 10.40 8 8 0 61.19 9.20 8 8 0 57.99 8.30 -9 -8 0 -8.10 7.60 9 -8 0 -9.20 5.20 9 -8 0 12.70 6.40 9 -8 0 9.90 7.40 -9 -8 0 -1.70 4.70 -9 -8 0 1.50 3.30 -9 8 0 1.20 6.20 -9 8 0 12.40 6.70 9 8 0 4.80 5.80 9 8 0 -4.40 4.70 -10 -8 0 63.49 8.10 10 -8 0 65.99 11.40 -10 -8 0 72.49 13.50 10 -8 0 68.59 10.60 10 -8 0 92.39 11.70 -10 8 0 45.40 10.50 10 8 0 59.49 10.10 10 8 0 79.29 10.70 -10 8 0 63.89 10.40 -11 -8 0 288.87 15.80 -11 -8 0 314.87 25.90 11 -8 0 333.67 20.40 11 -8 0 282.77 21.60 11 -8 0 283.47 19.00 -11 8 0 312.37 19.90 -11 8 0 262.67 24.60 11 8 0 325.07 21.20 11 8 0 313.27 19.70 12 -8 0 52.19 10.60 -12 -8 0 73.99 15.50 -12 -8 0 72.99 9.40 12 -8 0 68.69 12.90 12 -8 0 58.69 11.30 12 8 0 62.19 11.20 12 8 0 43.70 10.60 -12 8 0 52.79 13.40 -12 8 0 83.29 12.60 13 -8 0 54.59 12.30 13 -8 0 39.60 10.40 -13 -8 0 44.20 14.40 13 -8 0 48.00 10.70 -13 8 0 56.29 14.70 -13 8 0 32.40 10.20 13 8 0 29.80 9.80 13 8 0 38.90 11.50 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9 0 596.34 23.00 -3 9 0 612.24 20.40 3 9 0 606.94 22.60 3 9 0 620.84 21.80 3 9 0 588.44 17.90 4 -9 0 798.22 25.10 -4 -9 0 796.92 25.50 4 -9 0 783.52 29.10 -4 -9 0 757.42 27.70 -4 -9 0 786.62 26.30 -4 -9 0 777.72 23.30 -4 -9 0 734.03 24.20 4 9 0 760.72 23.70 -4 9 0 752.32 28.60 4 9 0 742.53 26.70 4 9 0 787.32 28.10 -5 -9 0 188.58 11.00 5 -9 0 236.78 11.90 5 -9 0 191.08 13.30 -5 -9 0 204.88 14.00 -5 -9 0 203.48 12.00 -5 -9 0 190.08 10.00 5 9 0 201.88 13.20 -5 9 0 210.18 14.20 5 9 0 209.48 10.60 5 9 0 219.58 12.90 -6 -9 0 55.59 9.50 6 -9 0 59.89 9.30 -6 -9 0 58.79 7.50 -6 -9 0 65.79 7.10 6 -9 0 80.19 8.20 6 -9 0 64.49 8.70 6 9 0 68.29 7.10 -6 9 0 69.89 9.90 6 9 0 59.89 8.20 7 -9 0 436.76 21.70 7 -9 0 437.36 19.30 -7 -9 0 408.36 18.10 7 -9 0 422.26 21.00 -7 -9 0 400.76 22.40 -7 -9 0 411.96 16.10 7 9 0 431.76 20.90 7 9 0 410.56 18.40 -7 9 0 390.86 22.00 8 -9 0 443.76 22.80 -8 -9 0 507.45 19.90 8 -9 0 452.25 22.90 8 -9 0 443.56 20.70 -8 -9 0 399.66 24.50 -8 -9 0 418.56 16.30 -8 9 0 464.85 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11 0 71.19 8.40 -1 11 0 62.09 4.70 -1 11 0 68.49 8.30 1 11 0 62.59 7.50 2 -11 0 453.45 15.70 2 -11 0 436.56 20.90 -2 -11 0 447.46 20.30 -2 -11 0 453.55 15.30 -2 -11 0 445.56 16.00 2 -11 0 450.05 15.60 2 11 0 438.06 18.80 2 11 0 449.46 20.00 2 11 0 437.36 18.20 -2 11 0 436.36 15.50 -2 11 0 448.46 19.80 3 -11 0 71.79 6.30 -3 -11 0 69.39 6.50 3 -11 0 92.19 11.10 3 -11 0 91.99 7.10 -3 -11 0 78.09 9.10 -3 -11 0 76.99 6.30 -3 -11 0 84.99 9.30 3 11 0 83.39 8.80 -3 11 0 79.39 6.90 -3 11 0 70.99 8.90 3 11 0 71.79 8.10 -4 -11 0 33.80 7.70 -4 -11 0 27.90 5.30 -4 -11 0 20.00 4.50 4 -11 0 19.00 4.90 -4 -11 0 25.90 6.70 4 -11 0 18.90 4.50 4 -11 0 29.50 7.80 -4 -11 0 27.30 3.90 4 11 0 25.50 3.50 -4 11 0 17.70 6.00 4 11 0 26.30 6.10 4 11 0 21.80 5.80 5 -11 0 158.38 14.80 -5 -11 0 134.39 12.70 -5 -11 0 136.39 8.60 5 -11 0 142.89 10.40 -5 -11 0 156.58 11.90 -5 -11 0 153.98 9.90 5 -11 0 139.69 10.20 5 11 0 145.49 8.60 5 11 0 139.29 13.00 5 11 0 164.38 13.30 -5 11 0 145.99 13.30 -6 -11 0 17.90 6.20 6 -11 0 30.60 6.20 -6 -11 0 34.80 9.10 -6 -11 0 19.90 7.10 6 -11 0 11.50 6.70 -6 -11 0 35.00 6.10 6 11 0 35.70 5.40 -6 11 0 29.80 7.40 6 11 0 24.10 7.20 7 -11 0 877.31 36.30 -7 -11 0 976.60 37.20 -7 -11 0 885.81 30.30 7 -11 0 1000.60 32.60 -7 -11 0 900.71 32.20 7 11 0 852.31 30.40 -7 11 0 916.71 37.30 7 11 0 902.41 34.70 -8 -11 0 66.29 12.00 -8 -11 0 76.29 7.90 -8 -11 0 54.29 8.30 8 -11 0 48.60 10.30 8 -11 0 68.89 9.10 8 11 0 39.00 8.60 8 11 0 63.79 8.50 -8 11 0 62.79 11.20 -9 -11 0 60.09 12.30 9 -11 0 49.00 8.60 9 -11 0 59.79 11.30 -9 -11 0 63.79 9.10 9 11 0 69.69 11.00 -9 11 0 42.90 10.90 9 11 0 41.70 7.80 10 -11 0 5.90 7.30 -10 -11 0 -2.10 5.70 10 -11 0 -0.80 6.20 -10 -11 0 5.70 9.70 10 11 0 3.10 6.60 10 11 0 1.20 5.10 -10 11 0 2.10 7.30 -10 11 0 0.00 7.20 -11 -11 0 53.59 9.20 11 -11 0 42.90 9.90 11 -11 0 57.69 12.10 -11 -11 0 46.00 13.30 11 11 0 41.80 10.60 -11 11 0 44.80 12.30 11 11 0 53.09 9.80 -11 11 0 27.90 9.80 12 -11 0 53.79 11.40 12 -11 0 37.10 10.40 -12 11 0 39.90 12.80 12 11 0 32.80 9.00 -12 11 0 37.00 11.10 12 11 0 26.40 10.20 13 -11 0 -8.10 7.00 13 -11 0 1.40 8.40 -13 11 0 12.60 10.20 -13 11 0 6.70 9.40 13 11 0 9.10 8.50 13 11 0 -6.90 6.30 14 -11 0 1.10 9.00 14 -11 0 12.80 10.00 14 11 0 6.00 8.60 14 11 0 15.90 11.20 -14 11 0 0.90 9.60 -14 11 0 8.80 11.80 0 -12 0 381.86 13.90 0 -12 0 368.36 19.40 0 -12 0 391.06 13.70 0 12 0 426.66 18.00 0 12 0 382.56 18.50 -1 -12 0 150.38 8.10 -1 -12 0 142.19 8.20 1 -12 0 148.79 13.30 1 -12 0 153.38 8.20 1 -12 0 153.78 7.90 -1 -12 0 135.49 12.70 1 12 0 152.58 11.00 1 12 0 161.78 12.20 -1 12 0 153.48 10.90 -1 12 0 157.88 12.10 -1 12 0 150.38 6.60 1 12 0 133.09 10.80 -2 -12 0 22.00 4.10 -2 -12 0 29.40 7.20 2 -12 0 22.60 4.10 2 -12 0 21.60 4.20 2 -12 0 23.00 6.60 -2 -12 0 21.40 4.30 2 12 0 18.60 5.60 -2 12 0 23.60 3.80 -2 12 0 16.50 6.00 2 12 0 16.40 5.90 2 12 0 13.40 5.10 3 -12 0 47.60 5.50 3 -12 0 45.00 5.30 3 -12 0 27.40 7.40 -3 -12 0 38.00 4.90 -3 -12 0 42.80 5.60 3 12 0 56.29 7.50 -3 12 0 35.00 7.10 -3 12 0 44.50 5.60 3 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3 -1.90 6.70 -12 9 -3 4.90 8.60 12 9 3 2.00 7.30 12 9 3 0.20 6.70 -12 9 -3 -8.60 9.30 13 -9 3 14.00 8.80 13 -9 3 4.80 8.30 13 -9 3 -6.20 9.00 13 9 3 2.60 7.00 -13 9 -3 -7.00 8.30 -13 9 -3 15.90 11.80 13 9 3 2.90 7.90 14 -9 3 2.50 9.20 14 -9 3 -8.70 9.90 14 9 3 40.20 11.80 14 9 3 -4.00 8.40 -14 9 -3 5.40 12.50 -15 -10 3 38.40 16.00 15 -10 -3 10.50 10.00 15 10 -3 6.60 9.80 -15 10 3 15.10 11.00 -15 10 3 39.60 14.50 14 -10 -3 -10.70 6.70 -14 -10 3 11.50 12.60 14 -10 -3 -3.70 8.40 -14 10 3 -0.70 9.00 -14 10 3 8.60 10.50 14 10 -3 6.90 8.70 13 -10 -3 122.39 14.10 -13 -10 3 109.99 13.10 13 -10 -3 116.49 16.10 -13 -10 3 129.09 20.20 -13 10 3 117.79 18.30 -13 10 3 130.89 16.90 13 10 -3 106.09 16.00 -12 -10 3 224.48 16.90 12 -10 -3 201.28 20.10 12 -10 -3 220.28 17.30 -12 -10 3 183.48 22.40 -12 10 3 202.38 21.00 12 10 -3 214.58 20.50 -12 10 3 232.68 21.00 -11 -10 3 10.30 7.40 -11 -10 3 23.10 11.50 11 -10 -3 16.80 8.70 -11 10 3 13.40 8.90 -11 10 3 17.30 9.30 11 10 -3 11.40 7.80 10 -10 -3 26.10 6.80 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177.48 11.20 3 12 -3 177.18 14.80 3 12 -3 171.98 13.00 -2 -12 3 28.60 7.50 2 -12 -3 -3.20 5.10 -2 -12 3 7.50 4.40 2 12 -3 8.90 5.30 2 12 -3 10.90 6.30 -2 12 3 15.40 4.10 -2 12 3 12.30 4.20 -2 12 3 12.80 3.60 -1 -12 3 290.47 16.80 -1 -12 3 280.37 13.50 1 -12 -3 245.28 16.40 1 12 -3 295.47 17.80 -1 12 3 279.07 13.60 -1 12 3 289.87 11.90 -1 12 3 267.47 12.70 0 -12 3 28.70 5.60 0 -12 3 17.50 6.60 0 -12 -3 23.60 8.10 0 12 3 17.70 4.60 0 12 3 39.00 5.50 0 12 3 38.20 4.50 0 12 3 30.60 5.30 0 12 -3 27.10 7.20 1 -12 3 5.20 5.80 -1 -12 -3 -5.50 5.40 1 -12 3 -1.90 4.10 1 12 3 5.30 2.90 1 12 3 0.30 4.30 1 12 3 -8.50 3.10 1 12 3 -2.90 3.10 -1 12 -3 3.80 5.60 -2 -12 -3 -5.60 5.30 2 -12 3 1.60 4.10 2 -12 3 -0.60 5.20 2 12 3 2.50 3.70 2 12 3 0.80 3.70 -2 12 -3 2.20 2.50 -2 12 -3 2.20 5.60 2 12 3 1.00 2.70 -3 -12 -3 119.09 11.70 3 -12 3 117.79 10.00 3 -12 3 136.99 13.60 -3 -12 -3 134.39 10.50 -3 12 -3 131.09 8.30 3 12 3 138.49 10.50 3 12 3 136.89 8.30 3 12 3 146.39 10.30 -3 12 -3 132.29 14.00 4 -12 3 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3 -14 -3 163.78 16.80 -3 -14 3 138.49 10.70 3 14 -3 148.79 13.50 -3 14 3 148.19 11.50 3 14 -3 180.08 16.70 -2 -14 3 70.59 11.70 -2 -14 3 87.89 8.50 2 -14 -3 104.09 12.90 2 14 -3 94.99 12.10 -2 14 3 74.79 8.70 1 -14 -3 12.20 8.00 -1 -14 3 1.70 6.10 -1 -14 3 19.30 5.60 -1 14 3 15.60 5.10 1 14 -3 15.80 7.40 -1 14 3 9.80 3.60 0 -14 3 3.00 4.90 0 -14 -3 11.60 7.70 0 -14 3 4.10 6.50 0 14 -3 3.00 6.10 0 14 3 9.80 4.90 0 14 3 11.10 5.10 0 14 3 5.50 3.20 1 -14 3 104.49 9.40 -1 -14 -3 110.79 13.60 1 -14 3 104.59 13.40 1 14 3 116.09 6.90 1 14 3 99.69 9.40 1 14 3 112.09 10.40 -1 14 -3 115.79 13.20 -2 -14 -3 119.99 13.70 2 -14 3 115.39 9.80 2 -14 3 99.39 13.70 2 14 3 108.49 6.90 2 14 3 90.79 9.40 -2 14 -3 91.29 12.10 2 14 3 106.39 10.70 3 -14 3 130.89 10.90 -3 -14 -3 137.09 13.80 3 -14 3 136.79 14.50 3 14 3 131.19 8.00 3 14 3 131.59 12.30 3 14 3 143.09 11.80 -3 14 -3 136.89 14.60 4 -14 3 22.00 8.70 -4 -14 -3 17.80 7.30 4 -14 3 2.20 5.10 -4 14 -3 8.70 7.40 4 14 3 14.50 5.80 4 14 3 11.00 4.10 5 -14 3 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4 78.49 13.70 -12 10 -4 68.89 16.40 13 -10 4 -18.40 7.30 13 -10 4 -13.60 8.80 -13 10 -4 -13.60 10.00 13 10 4 12.60 9.50 13 10 4 -3.20 7.30 14 -10 4 0.10 9.60 14 -10 4 -5.90 11.20 -14 10 -4 -7.30 10.90 14 10 4 9.10 8.50 14 10 4 8.50 9.50 -15 -11 4 3.60 16.10 15 -11 -4 0.10 9.50 -15 11 4 10.80 11.10 15 11 -4 -6.20 7.80 -15 11 4 7.00 9.80 14 -11 -4 21.10 11.40 -14 -11 4 26.20 14.20 -14 11 4 30.70 12.10 14 11 -4 25.60 11.00 -14 11 4 36.20 13.20 13 -11 -4 6.60 9.40 -13 -11 4 7.40 8.50 -13 -11 4 15.40 12.80 13 11 -4 -6.10 7.40 -13 11 4 6.30 9.00 -13 11 4 18.50 9.70 -12 -11 4 95.29 12.80 12 -11 -4 135.29 17.40 -12 -11 4 104.69 18.00 12 11 -4 132.19 17.80 -12 11 4 91.39 14.80 -12 11 4 133.19 18.10 -11 -11 4 24.30 11.80 11 -11 -4 18.60 7.60 11 -11 -4 19.20 9.40 -11 -11 4 10.20 7.80 -11 11 4 29.40 10.20 -11 11 4 8.70 8.70 11 11 -4 15.90 9.20 10 -11 -4 54.89 7.70 -10 -11 4 74.49 10.60 -10 -11 4 53.59 13.60 10 -11 -4 50.39 10.60 -10 11 4 57.99 11.10 -10 11 4 48.50 11.30 10 11 -4 67.19 11.80 -9 -11 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8.10 6.90 -7 15 -4 12.40 9.60 8 -15 4 56.19 10.80 8 -15 4 56.39 12.80 8 15 4 59.89 11.10 -8 15 -4 56.59 13.90 9 -15 4 6.40 7.60 9 -15 4 3.10 9.00 -9 15 -4 -10.60 8.70 9 15 4 -12.70 6.60 10 -15 4 16.90 10.40 10 -15 4 15.40 8.90 10 15 4 13.80 8.60 -10 15 -4 0.30 10.50 11 -15 4 19.00 9.90 11 -15 4 12.40 10.40 11 15 4 -0.10 8.10 -11 15 -4 -4.50 10.30 12 -16 -4 7.20 10.90 -12 -16 4 3.00 8.80 -12 16 4 3.40 9.80 12 16 -4 2.00 8.90 -12 16 4 2.80 9.10 -11 -16 4 15.20 8.90 11 -16 -4 27.10 12.20 -11 16 4 19.60 11.40 -11 16 4 16.90 9.20 11 16 -4 3.30 8.60 -10 -16 4 9.20 7.90 10 -16 -4 18.40 11.50 -10 16 4 21.20 9.40 10 16 -4 4.30 8.50 -10 16 4 19.70 10.80 9 -16 -4 0.60 9.70 -9 -16 4 28.90 8.40 -9 16 4 24.80 9.10 9 16 -4 10.40 8.20 -8 -16 4 -10.30 7.40 8 -16 -4 1.00 9.30 -8 -16 4 -5.80 6.00 8 16 -4 -4.10 6.90 -8 16 4 2.40 6.30 -7 -16 4 5.50 6.60 7 -16 -4 -0.20 7.70 -7 -16 4 0.00 8.30 -7 16 4 -3.60 5.60 7 16 -4 -8.40 6.60 6 -16 -4 31.70 10.70 -6 -16 4 58.59 12.00 -6 -16 4 38.70 8.00 6 16 -4 29.00 9.30 -6 16 4 47.80 9.20 6 16 -4 64.99 13.10 5 -16 -4 256.27 22.70 -5 -16 4 247.38 19.20 -5 -16 4 249.28 15.10 5 16 -4 232.58 19.20 5 16 -4 233.68 21.00 -5 16 4 271.37 16.80 -4 -16 4 2.80 7.70 4 -16 -4 6.50 8.70 -4 -16 4 3.40 5.30 -4 16 4 -2.50 4.60 4 16 -4 3.50 7.50 4 16 -4 4.70 6.50 -3 -16 4 -3.10 4.90 -3 -16 4 4.20 7.90 3 -16 -4 -3.30 8.00 3 16 -4 -8.40 6.60 -3 16 4 -2.30 4.30 -2 -16 4 4.40 7.80 2 -16 -4 9.00 7.80 -2 -16 4 -0.60 5.10 2 16 -4 9.00 8.10 -2 16 4 -1.30 4.30 -1 -16 4 92.29 9.30 -1 -16 4 90.19 13.10 1 -16 -4 71.09 12.70 1 16 -4 89.69 13.10 -1 16 4 93.19 9.70 0 -16 -4 61.89 12.20 0 -16 4 61.29 12.00 0 -16 4 54.69 8.10 0 16 4 66.19 8.50 0 16 -4 65.19 11.90 0 16 4 54.29 7.70 -1 -16 -4 -1.30 7.70 1 -16 4 2.30 5.20 1 -16 4 2.30 7.80 1 16 4 2.10 4.90 -1 16 -4 -0.50 7.10 1 16 4 -1.00 4.90 2 -16 4 1.10 5.20 2 -16 4 0.50 7.90 -2 -16 -4 10.00 8.40 2 16 4 3.00 5.40 2 16 4 8.70 4.80 -2 16 -4 3.20 7.40 3 -16 4 29.10 7.10 -3 -16 -4 21.00 9.00 3 -16 4 30.90 10.30 3 16 4 27.60 7.50 3 16 4 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17 -4 79.49 13.50 7 17 -4 77.19 14.80 -6 -17 4 111.59 11.30 6 -17 -4 103.29 17.20 -6 -17 4 93.89 14.20 6 17 -4 110.09 14.70 -6 17 4 95.29 12.20 6 17 -4 104.99 15.70 -5 -17 4 16.40 9.40 5 -17 -4 32.80 11.00 -5 -17 4 28.80 7.40 5 17 -4 39.90 9.80 -5 17 4 28.50 7.80 4 -17 -4 140.79 18.90 -4 -17 4 175.58 13.20 -4 -17 4 177.18 18.10 -4 17 4 205.68 14.20 4 17 -4 151.88 15.60 4 17 -4 176.58 19.40 -3 -17 4 369.26 17.80 -3 -17 4 364.96 23.90 3 -17 -4 400.96 26.50 3 17 -4 327.27 23.80 -3 17 4 338.87 18.10 2 -17 -4 37.00 11.40 -2 -17 4 41.90 7.30 -2 -17 4 34.10 10.10 -2 17 4 30.20 6.90 1 -17 -4 216.58 20.60 -1 -17 4 228.58 14.10 -1 -17 4 202.78 19.10 1 17 -4 236.28 21.30 0 -17 4 0.70 8.20 0 -17 4 1.50 5.30 0 -17 -4 -6.20 7.90 0 17 4 5.80 5.30 0 17 -4 1.30 7.30 1 -17 4 71.79 13.50 1 -17 4 91.79 9.90 -1 -17 -4 89.69 14.20 -1 17 -4 92.39 14.40 1 17 4 91.19 10.40 2 -17 4 237.08 15.00 -2 -17 -4 270.87 20.70 2 -17 4 262.37 23.00 2 17 4 232.98 15.70 -2 17 -4 279.37 22.10 -3 -17 -4 90.69 13.80 3 -17 4 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5 61.29 9.30 -7 11 -5 48.70 10.90 7 11 5 60.79 9.70 8 -11 5 5.20 6.60 8 -11 5 -0.20 7.50 8 -11 5 3.70 6.60 8 11 5 4.50 6.40 8 11 5 10.60 6.40 -8 11 -5 0.60 8.50 9 -11 5 232.78 18.20 9 -11 5 199.88 17.90 9 -11 5 218.08 19.70 9 11 5 197.58 18.30 -9 11 -5 211.88 22.00 9 11 5 205.98 17.60 10 -11 5 52.49 11.20 10 -11 5 25.30 11.00 10 -11 5 45.30 10.90 -10 11 -5 39.80 12.90 10 11 5 38.40 9.60 10 11 5 32.50 9.20 11 -11 5 16.70 8.90 11 -11 5 16.30 9.00 11 -11 5 15.20 9.90 11 11 5 19.40 8.30 -11 11 -5 1.80 10.20 -11 11 -5 13.10 9.40 11 11 5 15.00 8.20 12 -11 5 30.10 11.30 12 -11 5 45.70 13.10 12 -11 5 35.80 10.60 -12 11 -5 38.50 11.80 -12 11 -5 45.20 15.10 12 11 5 25.50 9.60 12 11 5 67.79 13.20 13 -11 5 28.60 11.70 13 -11 5 34.00 13.60 13 11 5 26.10 11.20 -13 11 -5 33.40 14.80 13 11 5 46.00 12.10 -14 -12 5 23.80 15.70 14 -12 -5 11.10 10.20 -14 -12 5 7.20 11.20 14 12 -5 40.20 11.40 -14 12 5 19.00 10.30 -14 12 5 17.70 11.20 -13 -12 5 83.79 12.80 -13 -12 5 65.09 17.20 13 12 -5 42.10 12.40 -13 12 5 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4.30 -2 12 -5 6.90 3.30 -2 12 -5 5.80 6.70 3 -12 5 76.89 10.80 -3 -12 -5 79.39 10.40 3 -12 5 88.59 9.80 3 -12 5 93.59 8.60 3 12 5 95.39 9.40 -3 12 -5 84.19 12.40 3 12 5 82.09 7.90 3 12 5 77.79 8.10 -4 -12 -5 4.00 6.00 4 -12 5 -6.30 4.90 4 -12 5 5.00 5.70 4 -12 5 4.50 5.40 4 12 5 2.10 4.10 4 12 5 8.40 4.60 -4 12 -5 1.20 6.20 5 -12 5 265.07 16.50 -5 -12 -5 264.47 15.40 5 -12 5 277.87 16.90 5 -12 5 277.37 18.50 5 12 5 266.77 14.60 -5 12 -5 274.07 20.90 5 12 5 302.07 16.00 -6 -12 -5 8.60 5.50 6 -12 5 5.70 7.10 6 -12 5 1.20 6.30 6 -12 5 7.90 6.30 -6 12 -5 7.40 7.70 6 12 5 6.70 5.00 6 12 5 12.30 6.00 7 -12 5 4.90 6.40 7 -12 5 -6.90 6.20 7 -12 5 5.30 7.20 -7 12 -5 6.80 8.20 7 12 5 -5.20 4.50 7 12 5 1.80 5.50 8 -12 5 183.88 18.10 8 -12 5 262.67 18.60 8 -12 5 206.08 17.90 -8 12 -5 196.08 20.90 8 12 5 208.68 15.70 8 12 5 224.48 18.50 9 -12 5 6.60 7.40 9 -12 5 6.10 8.70 9 -12 5 8.70 7.60 -9 12 -5 2.70 9.20 9 12 5 -1.40 6.20 9 12 5 -0.20 6.30 10 -12 5 27.40 10.10 10 -12 5 67.49 13.20 10 -12 5 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9.60 -2 -13 5 34.20 6.80 -2 -13 5 18.30 6.80 -2 13 5 21.40 4.40 2 13 -5 20.20 8.30 -2 13 5 28.90 4.50 -1 -13 5 115.49 13.10 -1 -13 5 125.39 10.40 1 -13 -5 97.59 13.30 -1 13 5 109.89 8.10 -1 13 5 110.09 8.10 1 13 -5 122.19 14.50 -1 13 5 95.19 8.30 -1 13 5 115.49 7.70 0 -13 -5 42.10 9.80 0 -13 5 27.80 6.40 0 -13 5 35.50 9.10 0 13 5 18.00 4.80 0 13 5 37.20 5.30 0 13 5 46.80 5.50 0 13 -5 31.20 9.00 0 13 5 36.80 5.40 -1 -13 -5 73.99 11.00 1 -13 5 51.79 10.20 1 -13 5 51.89 7.80 -1 13 -5 58.99 10.80 1 13 5 49.99 6.50 1 13 5 51.19 6.10 1 13 5 55.09 6.40 1 13 5 56.99 6.50 -2 -13 -5 173.28 15.30 2 -13 5 163.98 12.80 2 -13 5 144.09 15.60 2 -13 5 185.18 10.00 2 13 5 199.18 11.80 2 13 5 161.68 10.60 2 13 5 144.69 9.90 -2 13 -5 184.78 17.00 -3 -13 -5 40.70 8.90 3 -13 5 34.50 9.20 3 -13 5 31.00 7.20 3 -13 5 40.90 6.50 -3 13 -5 34.60 9.40 3 13 5 36.40 5.90 3 13 5 32.90 6.10 4 -13 5 94.29 12.40 4 -13 5 137.59 12.20 4 -13 5 106.79 9.80 -4 -13 -5 105.19 11.50 4 13 5 101.29 9.20 -4 13 -5 116.09 14.70 4 13 5 121.09 10.90 5 -13 5 31.80 7.70 5 -13 5 35.40 7.80 -5 -13 -5 29.60 7.60 5 -13 5 39.10 9.50 5 13 5 34.60 7.20 5 13 5 29.40 6.10 -5 13 -5 40.30 10.40 6 -13 5 244.68 16.90 6 -13 5 181.48 17.60 6 -13 5 217.78 16.50 6 13 5 229.08 14.40 6 13 5 227.88 15.80 -6 13 -5 211.48 20.00 7 -13 5 8.50 7.70 7 -13 5 15.00 8.10 7 -13 5 14.70 7.70 -7 13 -5 13.00 8.90 7 13 5 17.70 6.50 7 13 5 10.00 6.50 8 -13 5 62.19 12.10 8 -13 5 60.49 11.90 8 -13 5 48.70 10.30 8 13 5 40.70 9.10 -8 13 -5 18.70 10.60 8 13 5 29.20 9.00 9 -13 5 -5.00 8.40 9 -13 5 -3.00 7.80 9 -13 5 2.30 7.40 9 13 5 4.20 6.90 9 13 5 -6.20 5.90 -9 13 -5 1.40 9.70 10 -13 5 9.90 8.80 10 -13 5 6.70 8.40 10 -13 5 8.60 9.70 10 13 5 -1.70 6.80 -10 13 -5 3.60 10.30 10 13 5 -0.90 6.80 11 -13 5 -8.30 7.00 11 -13 5 3.90 8.40 11 -13 5 7.00 10.00 11 13 5 -1.30 7.20 -11 13 -5 4.70 11.70 12 -13 5 18.50 11.30 12 -13 5 6.70 9.10 12 -13 5 13.10 9.30 -12 13 -5 12.30 12.60 12 13 5 -5.60 7.80 -12 13 -5 11.90 10.60 -13 -14 5 137.59 16.90 13 -14 -5 123.49 19.50 13 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5 13 7 151.88 13.00 5 13 7 174.38 13.70 6 -13 7 34.30 8.90 6 -13 7 37.10 9.10 6 -13 7 43.50 10.20 -6 13 -7 39.90 12.20 6 13 7 40.10 8.20 6 13 7 44.40 8.20 7 -13 7 49.90 11.10 7 -13 7 60.99 11.10 7 -13 7 61.49 12.10 7 13 7 61.89 9.80 7 13 7 57.29 9.90 -7 13 -7 55.59 14.20 8 -13 7 14.10 8.60 8 -13 7 13.70 9.40 8 -13 7 13.00 8.50 -8 13 -7 6.10 10.50 8 13 7 11.80 7.20 8 13 7 15.30 7.80 9 -13 7 32.90 10.50 9 -13 7 27.00 9.70 9 -13 7 29.60 10.70 -9 13 -7 11.00 11.90 9 13 7 19.00 8.70 10 -13 7 8.70 8.80 10 -13 7 -2.90 7.70 10 -13 7 18.60 10.70 -10 13 -7 14.20 12.50 10 13 7 6.20 7.70 10 13 7 0.30 7.40 11 -13 7 4.00 11.20 11 -13 7 38.00 11.90 11 -13 7 21.00 11.20 11 13 7 21.80 9.50 -11 13 -7 33.80 14.60 -13 -14 7 27.80 10.80 13 -14 -7 10.70 11.50 13 14 -7 14.90 9.40 -13 14 7 11.00 10.60 -13 14 7 20.30 9.80 12 -14 -7 105.49 17.20 -12 -14 7 83.69 17.90 -12 -14 7 111.29 15.40 -12 14 7 84.99 16.00 12 14 -7 79.59 14.50 -12 14 7 84.29 13.90 -11 -14 7 -6.60 7.70 -11 -14 7 15.40 8.30 11 -14 -7 4.80 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5 9 19.00 7.30 6 5 9 22.20 3.00 -6 5 -9 35.00 10.70 -7 -5 -9 55.29 10.70 7 -5 9 51.79 8.70 7 -5 9 46.30 7.70 7 -5 9 65.59 11.10 7 5 9 61.89 9.00 -7 5 -9 31.00 10.90 7 5 9 45.90 9.60 -8 -5 -9 25.30 9.80 8 -5 9 32.90 9.70 8 -5 9 29.30 6.70 8 -5 9 37.60 8.70 8 5 9 33.30 9.50 -8 5 -9 25.60 11.30 8 5 9 23.50 7.30 9 -5 9 10.40 7.00 9 -5 9 10.50 8.70 -9 -5 -9 6.20 9.40 9 -5 9 11.20 5.80 9 5 9 18.90 8.40 -9 5 -9 4.60 10.20 9 5 9 14.10 6.60 10 -5 9 181.28 18.50 10 -5 9 218.78 21.50 10 5 9 207.28 20.30 -10 5 -9 215.28 24.50 10 5 9 170.78 17.50 11 -5 9 13.80 8.60 11 -5 9 6.10 10.20 11 5 9 19.80 7.70 11 5 9 19.50 10.20 -11 5 -9 -14.00 9.80 12 -5 9 0.50 10.00 12 -5 9 -8.80 6.90 12 5 9 0.90 7.10 12 5 9 6.30 9.90 -12 5 -9 12.30 13.00 13 -5 9 16.80 12.00 13 -5 9 11.80 9.40 13 5 9 -0.60 8.10 13 5 9 -3.10 9.40 -13 5 -9 -1.20 14.10 -16 -6 9 10.50 12.80 -16 -6 9 0.80 9.50 16 6 -9 -8.40 8.10 -16 6 9 -0.20 10.20 -16 6 9 -4.40 8.90 -15 -6 9 20.50 10.00 -15 -6 9 16.70 12.60 -15 6 9 26.30 10.50 15 6 -9 20.80 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26.70 -6 6 9 697.53 28.30 -6 6 9 688.73 24.10 6 6 -9 716.93 27.90 -5 -6 9 8.00 4.70 5 -6 -9 3.30 5.70 -5 -6 9 2.10 5.30 -5 6 9 5.50 2.80 -5 6 9 -4.60 3.60 5 6 -9 3.80 4.90 -5 6 9 3.10 3.00 4 -6 -9 1167.38 40.90 -4 -6 9 1179.78 37.40 -4 -6 9 1151.78 36.50 4 -6 -9 1108.49 31.40 -4 6 9 1145.89 38.20 -4 6 9 1150.18 31.90 -4 6 9 1111.09 32.10 4 6 -9 1124.09 40.60 3 -6 -9 1227.38 42.00 -3 -6 9 1225.68 38.20 -3 -6 9 1234.28 37.40 -3 -6 9 1215.58 38.60 -3 6 9 1212.88 39.50 3 6 -9 1214.08 42.50 -2 -6 9 471.85 19.00 -2 -6 9 480.05 18.70 -2 -6 9 484.25 19.20 2 6 -9 484.45 23.10 -2 6 9 506.15 19.90 -1 -6 9 420.56 17.10 -1 -6 9 394.46 16.90 -1 -6 9 403.56 17.20 -1 6 9 415.76 18.50 -1 6 9 425.26 17.20 1 6 -9 443.96 21.50 0 -6 9 298.67 13.80 0 -6 9 296.57 14.00 0 -6 9 300.67 14.50 0 6 9 286.17 9.40 0 6 9 283.67 13.10 0 6 9 309.77 15.50 0 6 -9 314.57 18.40 0 6 9 285.57 10.50 1 -6 9 90.99 8.20 -1 -6 -9 82.79 6.30 1 -6 9 90.59 8.60 1 6 9 101.99 9.70 -1 6 -9 98.79 11.60 1 6 9 98.09 5.50 1 6 9 105.79 6.60 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8 -6 9 274.67 18.90 -8 6 -9 210.68 21.80 8 6 9 244.68 20.10 8 6 9 248.98 17.00 9 -6 9 -0.80 6.50 9 -6 9 11.00 5.90 9 -6 9 18.00 9.30 9 6 9 14.60 8.30 -9 6 -9 15.00 11.70 9 6 9 6.30 6.20 10 -6 9 12.00 9.50 10 -6 9 5.60 5.70 10 -6 9 1.00 6.60 -10 6 -9 6.40 10.80 10 6 9 11.30 8.20 10 6 9 10.60 6.50 11 -6 9 37.00 12.80 11 -6 9 34.40 11.10 11 6 9 21.70 10.10 11 6 9 30.50 9.70 -11 6 -9 31.20 14.30 12 -6 9 39.80 13.80 12 -6 9 69.29 13.50 12 6 9 49.99 11.50 12 6 9 106.19 16.70 -12 6 -9 78.19 19.10 13 -6 9 -7.60 10.20 13 -6 9 5.80 9.20 13 6 9 26.40 10.30 13 6 9 22.70 11.80 -13 6 -9 8.50 15.80 -16 -7 9 128.69 16.70 -16 -7 9 127.69 22.40 -16 7 9 103.29 16.70 -16 7 9 138.49 19.10 16 7 -9 170.88 21.10 -15 -7 9 13.50 10.10 -15 -7 9 35.00 15.00 -15 7 9 13.00 10.50 15 7 -9 31.00 10.90 -15 7 9 37.80 11.60 -14 -7 9 9.30 9.50 -14 -7 9 20.10 13.00 14 7 -9 27.80 10.10 -14 7 9 1.70 9.00 -14 7 9 13.80 8.60 -13 -7 9 96.29 13.60 -13 7 9 100.89 15.50 -13 7 9 113.09 15.70 13 7 -9 77.89 13.00 12 -7 -9 4.40 5.80 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9 591.44 22.70 4 -7 -9 563.44 25.80 -4 7 9 565.24 17.30 -4 7 9 581.54 17.40 -4 7 9 571.74 23.80 4 7 -9 559.14 26.50 -3 -7 9 26.70 5.90 -3 -7 9 40.20 6.70 3 -7 -9 42.40 8.20 -3 -7 9 52.59 6.30 -3 7 9 28.60 6.30 3 7 -9 39.40 8.90 -2 -7 9 144.59 10.50 -2 -7 9 136.59 10.10 -2 -7 9 125.99 9.50 2 -7 -9 136.79 12.60 -2 7 9 159.28 10.70 2 7 -9 128.89 13.40 -1 -7 9 -0.70 3.10 -1 -7 9 -3.80 3.50 -1 -7 9 -3.80 3.60 1 -7 -9 5.80 5.50 1 7 -9 -7.70 4.70 -1 7 9 -1.20 4.40 -1 7 9 6.90 3.80 0 -7 9 67.19 7.50 0 -7 9 66.09 7.00 0 -7 9 94.09 9.10 0 7 9 56.39 6.70 0 7 -9 76.69 10.70 0 7 9 71.69 3.60 0 7 9 62.09 8.10 1 -7 9 562.54 21.70 1 -7 9 568.94 22.40 1 7 9 560.24 23.20 -1 7 -9 616.44 27.60 1 7 9 542.15 18.10 1 7 9 564.44 20.20 2 -7 9 5.60 5.10 -2 -7 -9 3.00 3.20 2 -7 9 6.30 4.70 2 7 9 5.90 3.10 2 7 9 2.30 2.40 2 7 9 6.90 4.90 -2 7 -9 2.10 6.90 2 7 9 2.10 2.80 3 -7 9 478.35 21.20 3 -7 9 480.15 21.50 3 7 9 495.55 15.60 3 7 9 466.65 19.10 3 7 9 505.05 22.00 3 7 9 481.75 16.50 -3 7 -9 461.35 25.30 3 7 9 493.85 17.70 4 -7 9 213.88 15.20 -4 -7 -9 193.88 12.70 4 -7 9 179.78 13.70 4 7 9 197.38 7.50 4 7 9 212.18 10.40 4 7 9 193.58 12.50 -4 7 -9 181.68 18.10 4 7 9 198.08 11.30 4 7 9 193.38 14.00 4 7 9 186.68 8.00 5 -7 9 548.85 24.10 -5 -7 -9 499.45 23.40 5 -7 9 549.95 24.70 5 -7 9 502.65 22.60 5 7 9 513.25 17.60 5 7 9 530.65 23.90 5 7 9 513.45 21.10 -5 7 -9 510.15 28.70 5 7 9 474.45 23.30 6 -7 9 15.30 7.80 -6 -7 -9 14.10 7.70 6 -7 9 15.20 6.60 6 -7 9 9.90 5.90 6 7 9 23.20 7.60 -6 7 -9 19.70 10.00 6 7 9 23.10 5.80 -7 -7 -9 131.39 16.30 7 -7 9 151.68 13.80 7 -7 9 157.68 14.80 7 -7 9 167.98 16.60 7 7 9 147.09 15.10 7 7 9 154.78 14.00 -7 7 -9 166.98 19.50 8 -7 9 101.39 13.90 8 -7 9 116.49 13.90 8 -7 9 88.89 11.10 8 7 9 107.89 12.60 -8 7 -9 82.49 15.00 8 7 9 113.29 13.80 9 -7 9 37.70 9.70 9 -7 9 16.20 9.70 9 -7 9 38.20 8.30 9 7 9 36.90 9.80 -9 7 -9 28.00 12.00 9 7 9 31.20 8.60 10 -7 9 131.29 17.60 10 -7 9 140.19 17.00 10 -7 9 111.69 12.60 10 7 9 133.09 16.60 -10 7 -9 96.89 18.50 10 7 9 114.39 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13.40 10.40 -9 11 9 11.00 7.70 -9 11 9 2.40 5.30 9 11 -9 -2.30 6.70 8 -11 -9 179.28 19.80 -8 -11 9 176.88 16.40 -8 -11 9 129.49 16.40 8 11 -9 154.68 15.60 -8 11 9 138.99 15.10 -8 11 9 182.78 12.70 -7 -11 9 67.59 9.90 -7 -11 9 62.49 9.20 -7 -11 9 71.59 12.20 7 -11 -9 78.29 13.90 -7 11 9 70.99 7.80 7 11 -9 51.49 9.80 -7 11 9 85.59 12.90 -6 -11 9 15.80 7.10 -6 -11 9 37.00 7.60 6 -11 -9 35.90 10.80 -6 11 9 49.99 5.80 6 11 -9 23.50 7.50 6 11 -9 44.00 11.10 -6 11 9 29.40 7.60 -5 -11 9 5.50 5.70 5 -11 -9 22.60 9.90 -5 -11 9 13.90 6.20 -5 -11 9 9.50 4.60 -5 11 9 14.00 6.80 5 11 -9 18.30 8.60 -4 -11 9 7.00 5.30 4 -11 -9 -7.20 6.20 -4 -11 9 -2.30 5.30 -4 -11 9 -0.80 3.80 -4 11 9 7.50 6.00 4 11 -9 4.30 7.20 -3 -11 9 21.40 4.50 3 -11 -9 32.00 9.80 -3 -11 9 26.70 6.80 -3 -11 9 27.70 6.80 3 11 -9 25.90 9.50 -3 11 9 30.10 7.40 -2 -11 9 7.30 5.90 -2 -11 9 5.60 3.90 2 -11 -9 21.30 9.10 -2 -11 9 3.60 5.40 -2 11 9 3.00 5.10 2 11 -9 -0.20 7.20 -1 -11 9 23.50 5.10 1 -11 -9 21.60 8.50 -1 -11 9 17.40 6.60 -1 11 9 9.90 5.50 1 11 -9 23.50 9.00 0 -11 9 164.38 13.20 0 -11 -9 178.08 16.40 0 -11 9 148.39 10.70 0 11 9 150.28 6.70 0 11 -9 167.08 17.50 0 11 9 162.18 12.40 -1 -11 -9 196.98 16.50 1 -11 9 181.48 12.30 1 -11 9 193.68 13.90 1 11 9 190.18 13.20 -1 11 -9 146.79 16.80 1 11 9 156.28 8.20 2 -11 9 10.30 5.90 2 -11 9 -1.40 6.20 2 -11 9 14.60 6.10 -2 -11 -9 20.00 7.50 2 11 9 11.90 3.70 -2 11 -9 18.50 9.50 2 11 9 10.50 5.80 2 11 9 14.90 3.80 3 -11 9 128.29 13.70 -3 -11 -9 160.08 13.50 3 -11 9 142.59 13.40 3 -11 9 137.19 12.20 3 11 9 126.19 9.30 3 11 9 129.49 12.20 -3 11 -9 122.69 15.90 4 -11 9 291.67 19.30 4 -11 9 284.97 18.30 4 -11 9 308.27 18.30 4 11 9 267.67 16.90 -4 11 -9 339.57 24.20 4 11 9 275.47 14.80 5 -11 9 3.80 6.90 5 -11 9 9.90 6.70 5 -11 9 19.20 8.20 5 11 9 8.30 6.30 5 11 9 12.30 5.10 -5 11 -9 24.50 10.40 6 -11 9 106.49 13.80 6 -11 9 86.79 12.00 6 -11 9 95.29 13.00 -6 11 -9 119.39 17.60 6 11 9 101.59 11.30 6 11 9 109.39 12.50 7 -11 9 9.20 7.60 7 -11 9 26.70 9.80 7 -11 9 11.40 7.50 -7 11 -9 24.00 12.40 7 11 9 17.60 6.70 7 11 9 14.20 7.70 8 -11 9 5.00 6.90 8 -11 9 2.50 8.90 8 -11 9 0.10 7.10 -8 11 -9 5.00 10.20 8 11 9 13.20 6.80 8 11 9 9.70 7.50 9 -11 9 59.69 11.50 9 -11 9 53.29 11.50 9 -11 9 89.09 15.00 9 11 9 68.49 11.40 -9 11 -9 88.49 18.60 9 11 9 92.19 13.60 10 -11 9 58.39 12.40 10 -11 9 51.89 11.30 10 -11 9 46.50 13.40 -10 11 -9 62.19 17.30 10 11 9 71.09 12.70 10 11 9 85.49 14.10 11 -11 9 6.60 9.50 11 -11 9 4.60 10.70 11 -11 9 18.90 10.90 11 11 9 6.20 8.80 11 11 9 5.00 8.10 -11 11 -9 16.80 13.80 14 -12 -9 84.69 17.10 -14 -12 9 56.09 16.20 -14 -12 9 98.09 15.30 -14 12 9 81.49 16.60 -14 12 9 73.89 14.10 14 12 -9 75.69 15.70 -13 -12 9 14.60 9.60 13 -12 -9 11.50 10.50 -13 -12 9 12.40 11.90 -13 12 9 25.90 9.30 13 12 -9 18.60 9.60 -13 12 9 9.10 10.30 12 -12 -9 18.30 11.30 -12 -12 9 13.50 9.70 -12 -12 9 25.90 12.20 -12 12 9 34.60 9.80 -12 12 9 41.60 12.40 12 12 -9 34.90 10.60 11 -12 -9 31.40 11.70 -11 -12 9 7.30 10.00 -11 -12 9 16.60 9.50 -11 12 9 6.00 7.00 11 12 -9 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13 -9 30.50 10.50 -3 13 9 32.30 7.30 2 -13 -9 13.80 9.20 -2 -13 9 22.80 7.00 -2 13 9 21.10 6.40 2 13 -9 30.70 9.90 1 -13 -9 31.40 10.30 -1 -13 9 18.80 6.90 -1 13 9 28.10 7.10 1 13 -9 35.30 10.40 0 -13 9 225.38 16.10 0 -13 -9 260.87 19.60 0 -13 9 283.97 18.60 0 13 9 276.77 16.10 0 13 -9 294.27 24.10 1 -13 9 -5.00 5.60 1 -13 9 4.20 6.10 1 -13 9 3.80 8.10 -1 -13 -9 16.90 7.80 1 13 9 0.00 5.00 -1 13 -9 -3.50 7.80 2 -13 9 5.70 5.40 -2 -13 -9 2.90 7.50 2 -13 9 -1.80 6.10 2 -13 9 3.70 6.30 2 13 9 -7.10 4.70 -2 13 -9 -0.40 8.00 -3 -13 -9 -0.20 6.60 3 -13 9 -1.50 6.80 3 -13 9 -9.30 5.50 3 -13 9 -2.70 5.80 -3 13 -9 0.10 8.30 3 13 9 -2.60 5.10 4 -13 9 7.20 6.60 4 -13 9 13.80 8.00 -4 -13 -9 -1.80 6.60 4 -13 9 3.00 6.70 4 13 9 6.40 6.10 -4 13 -9 5.00 8.30 5 -13 9 3.30 7.50 5 -13 9 -9.90 6.60 5 -13 9 -1.20 6.50 -5 13 -9 2.90 8.80 5 13 9 -0.80 5.50 6 -13 9 60.69 11.10 6 -13 9 56.99 11.90 6 -13 9 52.79 11.00 6 13 9 56.39 9.90 -6 13 -9 48.80 13.20 7 -13 9 29.00 9.90 7 -13 9 36.20 10.30 7 -13 9 24.60 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15 -9 29.20 10.90 -11 15 9 3.60 8.90 -11 15 9 15.10 7.80 -10 -15 9 235.28 21.10 -10 -15 9 202.98 18.30 -10 -15 9 170.88 21.70 10 -15 -9 238.98 25.40 10 15 -9 239.88 23.10 -10 15 9 210.38 16.40 -10 15 9 225.98 22.20 -9 -15 9 -4.10 7.70 -9 -15 9 -0.10 7.00 9 -15 -9 6.60 8.90 9 15 -9 5.40 7.70 -9 15 9 7.30 6.00 -9 15 9 19.20 9.50 -8 -15 9 4.80 7.40 -8 -15 9 -5.60 7.00 8 -15 -9 0.10 10.20 8 15 -9 25.60 11.70 -8 15 9 7.30 5.20 8 15 -9 9.60 8.90 -8 15 9 1.20 7.50 -7 -15 9 1.60 6.90 7 -15 -9 -6.40 9.10 -7 -15 9 -4.30 6.50 -7 15 9 -6.30 3.60 -7 15 9 -12.60 6.40 7 15 -9 5.60 10.10 7 15 -9 -6.30 6.00 6 -15 -9 -8.20 8.60 -6 -15 9 2.10 6.60 -6 -15 9 1.80 7.30 -6 15 9 3.20 6.50 6 15 -9 12.10 10.40 -5 -15 9 531.85 25.00 5 -15 -9 511.55 31.60 -5 15 9 527.75 27.90 5 15 -9 554.74 32.30 4 -15 -9 75.69 14.90 -4 -15 9 70.29 10.50 4 15 -9 49.40 12.60 -3 -15 9 5.80 6.70 -3 -15 9 -6.60 6.90 3 -15 -9 -4.90 8.30 -3 15 9 5.20 5.70 3 15 -9 16.30 9.60 -2 -15 9 42.70 8.70 2 -15 -9 33.20 11.50 -2 -15 9 42.30 10.40 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2.30 8.60 8 -4 10 -2.20 5.20 8 -4 10 5.90 4.70 8 4 10 -5.30 6.40 8 4 10 -3.30 5.00 -8 4 -10 12.10 10.30 -9 -4 -10 288.07 24.10 9 -4 10 282.47 22.90 9 -4 10 263.97 15.10 9 -4 10 223.88 19.30 9 4 10 294.87 23.70 -9 4 -10 274.47 27.20 9 4 10 264.77 19.10 10 -4 10 114.99 16.20 10 -4 10 89.49 13.30 10 4 10 136.99 15.60 -10 4 -10 100.29 17.90 10 4 10 160.08 18.40 11 -4 10 5.10 9.70 11 -4 10 25.60 9.10 11 4 10 20.20 8.50 11 4 10 13.40 9.90 -11 4 -10 10.90 12.70 12 -4 10 33.00 12.60 12 -4 10 20.40 10.20 12 4 10 23.60 9.60 12 4 10 28.60 11.70 -12 4 -10 11.20 14.20 13 -4 10 10.70 12.20 13 -4 10 19.10 9.90 13 4 10 1.70 10.10 13 4 10 -5.10 7.70 -13 4 -10 -3.30 13.90 -16 -5 10 -7.10 9.00 -16 -5 10 17.80 13.10 -16 5 10 14.70 10.80 -16 5 10 5.30 10.10 16 5 -10 19.70 10.90 -15 -5 10 76.39 13.30 -15 -5 10 77.59 17.20 -15 5 10 40.60 11.90 -15 5 10 66.29 13.90 15 5 -10 67.39 13.20 14 -5 -10 4.00 7.10 -14 -5 10 -8.30 9.70 -14 -5 10 10.30 8.50 -14 5 10 -3.20 8.20 -14 5 10 7.70 8.20 14 5 -10 -3.20 7.40 -13 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13 13 6.30 6.30 -1 -13 13 27.20 8.50 -1 13 13 33.00 9.10 1 13 -13 44.20 12.90 -1 13 13 26.10 7.60 0 -13 13 3.70 7.00 0 13 13 23.30 8.40 0 13 13 22.20 6.90 0 13 -13 15.10 11.20 1 -13 13 7.10 6.90 1 13 13 22.80 6.90 1 13 13 2.60 6.90 -1 13 -13 15.50 11.40 2 -13 13 4.50 7.00 2 -13 13 6.10 7.20 2 13 13 -2.20 6.80 -2 13 -13 4.30 11.00 3 -13 13 23.40 8.80 3 -13 13 28.80 9.90 -3 13 -13 36.10 13.60 3 13 13 27.60 9.20 4 -13 13 2.60 7.70 4 -13 13 6.60 7.90 4 13 13 22.10 8.60 -4 13 -13 14.60 11.60 5 -13 13 16.50 8.80 5 -13 13 24.60 9.70 -5 13 -13 17.10 13.00 5 13 13 20.50 8.90 6 -13 13 -2.10 7.50 6 -13 13 -2.40 7.90 -6 13 -13 -6.10 10.40 6 13 13 0.30 7.80 7 -13 13 1.40 8.40 7 -13 13 -8.30 7.20 7 13 13 -15.70 6.60 -7 13 -13 5.90 12.10 8 -13 13 10.80 9.30 8 -13 13 2.10 8.60 -8 13 -13 2.30 13.40 8 13 13 0.60 8.30 -11 -14 13 -3.20 7.80 -11 -14 13 8.70 9.80 11 14 -13 -15.40 11.40 -11 14 13 8.40 9.10 11 14 -13 15.00 9.00 10 -14 -13 12.70 12.00 -10 -14 13 11.10 9.30 -10 -14 13 1.60 7.70 -10 14 13 7.30 8.70 10 14 -13 8.20 12.60 -9 -14 13 68.49 12.10 9 -14 -13 58.49 15.80 -9 -14 13 52.89 11.80 -9 14 13 44.00 11.50 9 14 -13 49.80 15.00 8 -14 -13 72.99 16.20 -8 -14 13 102.39 14.90 -8 -14 13 73.49 11.90 8 14 -13 95.49 18.30 -8 14 13 85.39 14.60 -7 -14 13 63.39 11.20 7 -14 -13 75.69 16.30 -7 -14 13 97.79 13.70 7 14 -13 117.79 19.60 -7 14 13 62.09 13.00 -6 -14 13 46.10 10.70 6 -14 -13 49.10 13.90 -6 -14 13 20.70 8.80 -6 14 13 38.90 10.60 6 14 -13 48.40 14.20 -5 -14 13 23.20 8.40 5 -14 -13 20.00 11.60 -5 -14 13 26.40 8.50 -5 14 13 45.20 10.00 -5 14 13 18.50 8.10 5 14 -13 22.30 12.30 -4 -14 13 58.19 10.20 -4 -14 13 74.39 11.30 4 -14 -13 93.29 16.50 4 14 -13 97.29 18.00 -4 14 13 64.49 11.70 -4 14 13 62.99 10.80 -3 -14 13 66.49 10.80 3 -14 -13 73.59 15.10 -3 14 13 63.49 10.90 -3 14 13 48.50 10.00 3 14 -13 60.39 15.00 2 -14 -13 77.29 14.50 -2 -14 13 38.10 9.10 -2 14 13 36.40 9.60 2 14 -13 16.30 11.50 -2 14 13 24.60 8.00 -1 -14 13 13.90 7.60 1 14 -13 13.40 11.70 -1 14 13 6.00 7.50 -1 14 13 8.20 6.50 0 -14 13 -4.80 6.50 0 14 13 -4.30 5.20 0 14 13 -7.20 6.00 0 14 -13 7.50 11.30 1 -14 13 -1.90 6.50 1 -14 13 -1.20 7.10 1 14 13 -2.60 4.70 -1 14 -13 -1.60 10.60 1 14 13 -3.30 6.30 2 -14 13 5.20 7.90 2 -14 13 21.80 9.20 2 14 13 16.90 7.70 -2 14 -13 8.20 11.90 3 -14 13 172.38 18.70 3 -14 13 205.78 18.90 -3 14 -13 218.58 25.60 3 14 13 227.48 18.80 4 -14 13 7.40 8.30 4 -14 13 -1.60 8.10 -4 14 -13 -2.40 10.50 4 14 13 20.90 8.30 5 -14 13 -1.70 8.00 5 -14 13 -2.60 7.90 -5 14 -13 12.10 12.20 5 14 13 -4.70 6.70 6 -14 13 34.40 11.30 6 -14 13 19.50 10.30 -6 14 -13 14.70 13.60 6 14 13 35.60 10.50 7 -14 13 -0.30 8.80 7 -14 13 11.90 9.50 7 14 13 16.50 9.10 -7 14 -13 14.60 14.40 -11 -15 13 2.10 9.20 -10 -15 13 162.58 17.20 10 -15 -13 207.78 25.10 -10 -15 13 181.88 19.70 10 15 -13 127.69 21.30 -10 15 13 156.68 19.90 -9 -15 13 19.40 9.30 9 -15 -13 3.40 9.90 -9 -15 13 16.20 9.40 9 15 -13 39.00 15.10 -9 15 13 24.50 10.20 -8 -15 13 57.99 11.60 -8 -15 13 48.10 12.10 8 -15 -13 39.30 14.70 -8 15 13 24.00 10.20 8 15 -13 13.20 12.50 -7 -15 13 4.90 8.10 7 -15 -13 -8.70 10.10 -7 -15 13 1.30 7.80 -7 15 13 10.20 8.50 7 15 -13 3.20 11.80 6 -15 -13 20.10 10.90 -6 -15 13 5.00 8.30 -6 -15 13 12.70 8.10 -6 15 13 7.60 7.40 6 15 -13 12.90 11.50 -5 -15 13 261.57 21.90 -5 -15 13 269.47 19.10 5 -15 -13 258.97 25.00 -5 15 13 220.18 19.00 5 15 -13 223.18 24.10 -5 15 13 228.78 20.80 4 -15 -13 53.99 14.90 -4 -15 13 50.19 10.50 -4 15 13 65.89 11.30 -4 15 13 65.49 12.20 4 15 -13 50.29 15.20 3 -15 -13 12.40 11.20 -3 -15 13 17.50 8.40 3 15 -13 18.30 12.30 -3 15 13 -2.20 6.90 -3 15 13 20.20 8.30 -2 -15 13 -1.00 6.90 2 -15 -13 16.10 11.00 -2 15 13 16.20 7.10 -2 15 13 8.70 7.20 2 15 -13 16.90 12.20 -1 -15 13 256.87 19.40 1 -15 -13 261.17 24.00 1 15 -13 270.37 26.40 -1 15 13 272.97 18.90 -1 15 13 282.07 19.60 0 -15 13 -0.90 7.10 0 -15 13 4.90 8.20 0 15 13 7.00 7.10 0 15 -13 -2.50 10.60 0 15 13 -6.80 5.30 1 -15 13 -1.20 7.90 1 -15 13 0.90 6.80 -1 15 -13 -17.90 9.50 1 15 13 -4.00 6.70 2 -15 13 21.30 9.90 2 -15 13 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5 14 6.60 3.70 1 -5 14 298.07 16.80 1 -5 14 274.17 14.30 1 -5 14 278.07 17.90 1 5 14 281.97 12.30 1 5 14 289.97 13.50 1 5 14 256.77 18.40 -1 5 -14 294.17 23.50 2 -5 14 14.00 7.60 2 -5 14 23.60 7.00 2 5 14 23.00 3.80 -2 5 -14 39.40 10.90 2 5 14 32.40 5.80 2 5 14 27.20 8.30 3 -5 14 163.18 15.50 3 -5 14 124.39 12.50 -3 5 -14 141.99 17.70 3 5 14 156.58 15.80 3 5 14 138.79 11.20 4 -5 14 6.00 7.20 4 -5 14 -7.60 5.00 4 5 14 5.00 7.10 4 5 14 2.70 4.40 -4 5 -14 -4.80 8.50 5 -5 14 36.30 10.20 5 -5 14 32.30 8.00 5 5 14 17.80 6.30 5 5 14 24.00 8.80 -5 5 -14 23.70 11.00 6 -5 14 95.69 14.60 6 -5 14 104.79 13.00 6 5 14 110.49 14.80 -6 5 -14 67.09 14.70 6 5 14 120.79 12.60 7 -5 14 11.40 6.10 7 -5 14 -4.10 8.60 7 -5 14 7.10 7.20 7 5 14 14.50 9.20 -7 5 -14 15.90 12.40 7 5 14 9.10 6.20 8 -5 14 15.40 10.70 8 -5 14 16.10 8.30 8 5 14 20.10 10.80 -8 5 -14 7.30 13.20 8 5 14 15.50 7.50 9 -5 14 -2.40 10.50 9 -5 14 -1.50 7.30 9 5 14 -1.90 8.90 -9 5 -14 0.00 12.40 9 5 14 3.30 6.70 10 -5 14 -0.90 10.30 10 -5 14 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162.38 18.20 2 6 14 163.48 15.80 2 6 14 132.49 10.00 3 -6 14 4.90 7.60 3 -6 14 18.70 6.70 3 6 14 19.50 8.40 -3 6 -14 31.30 11.50 3 6 14 36.00 6.10 4 -6 14 13.90 6.80 4 -6 14 8.00 8.10 -4 6 -14 29.00 11.10 4 6 14 16.00 5.60 4 6 14 -1.10 7.20 5 -6 14 8.20 8.70 5 -6 14 1.80 5.60 -5 6 -14 7.60 10.00 5 6 14 1.70 7.10 5 6 14 -1.40 4.60 6 -6 14 8.10 7.20 6 -6 14 2.60 8.70 6 6 14 -7.30 6.80 6 6 14 -5.30 4.90 -6 6 -14 8.40 10.70 7 -6 14 11.40 6.70 7 -6 14 24.30 10.70 7 -6 14 9.10 7.30 -7 6 -14 5.10 12.10 7 6 14 9.00 8.80 7 6 14 10.70 6.60 8 -6 14 -7.90 9.20 8 -6 14 12.50 7.80 8 -6 14 6.10 7.00 8 6 14 2.80 8.90 -8 6 -14 -3.30 12.20 8 6 14 -4.70 5.40 9 -6 14 -1.30 10.10 9 -6 14 -17.00 6.30 9 6 14 -4.90 6.30 -9 6 -14 4.00 13.30 9 6 14 -2.60 8.60 10 -6 14 0.20 10.90 10 -6 14 -0.80 8.60 -10 6 -14 12.50 15.60 10 6 14 10.60 10.40 10 6 14 17.40 8.90 -15 -7 14 48.10 16.20 -15 -7 14 73.49 14.90 15 7 -14 56.79 13.80 -15 7 14 63.59 14.70 -15 7 14 64.19 13.50 -14 -7 14 2.50 9.20 -14 -7 14 -1.20 11.10 -14 7 14 6.90 8.40 -14 7 14 -3.80 8.50 14 7 -14 -5.00 8.20 -13 -7 14 20.90 11.40 -13 -7 14 11.30 9.50 13 7 -14 10.60 8.70 -13 7 14 7.50 8.50 -13 7 14 12.40 7.90 -12 -7 14 -14.50 6.50 -12 -7 14 2.80 9.50 12 7 -14 -2.80 7.50 -12 7 14 1.60 6.50 -12 7 14 -7.70 7.20 -11 -7 14 -0.80 6.70 -11 -7 14 -11.50 8.30 -11 7 14 -3.20 5.50 11 7 -14 0.60 7.60 -11 7 14 -2.30 6.60 -10 -7 14 104.09 13.40 -10 -7 14 112.69 16.20 10 7 -14 94.79 13.10 -10 7 14 133.69 13.10 -10 7 14 156.88 17.30 -9 -7 14 -3.40 6.30 -9 -7 14 2.60 8.10 -9 7 14 -3.80 4.60 -9 7 14 -1.70 6.20 -8 -7 14 97.19 12.20 -8 -7 14 73.79 12.80 -8 7 14 88.19 12.40 -8 7 14 97.09 9.80 8 7 -14 97.19 15.40 -7 -7 14 32.30 8.80 -7 7 14 45.80 9.40 7 7 -14 20.20 10.40 -7 7 14 29.20 5.70 -6 -7 14 219.28 15.90 -6 -7 14 208.58 15.00 6 7 -14 238.98 21.50 -6 7 14 214.78 16.30 -5 -7 14 1.00 6.60 -5 -7 14 -3.10 5.30 -5 -7 14 5.90 5.60 -5 7 14 5.10 5.50 5 7 -14 -6.00 8.30 -4 -7 14 308.87 17.80 -4 -7 14 304.27 17.00 -4 -7 14 329.97 18.60 4 7 -14 301.87 23.30 -4 7 14 290.87 17.80 -3 -7 14 166.58 13.60 -3 -7 14 138.89 12.30 -3 7 14 157.48 13.50 3 7 -14 164.48 17.90 -3 7 14 146.69 14.20 -2 -7 14 101.59 11.90 -2 -7 14 105.79 10.70 -2 -7 14 66.99 8.90 -2 7 14 84.29 11.60 -2 7 14 95.69 10.10 -2 7 14 87.89 6.40 2 7 -14 84.99 13.40 -1 -7 14 -3.20 6.10 -1 -7 14 9.90 5.90 -1 -7 14 -4.40 4.30 -1 7 14 -12.30 6.00 -1 7 14 2.90 2.80 1 7 -14 -3.40 8.00 -1 7 14 1.40 3.90 0 -7 14 215.58 15.00 0 -7 14 212.58 13.80 0 -7 14 189.38 15.30 0 7 14 215.48 10.20 0 7 14 203.28 11.90 0 7 14 204.68 17.60 0 7 -14 200.68 19.00 1 -7 14 7.40 6.10 1 -7 14 0.60 4.80 1 -7 14 5.10 7.00 1 7 14 6.30 3.60 -1 7 -14 9.60 9.40 1 7 14 16.10 4.20 1 7 14 10.50 7.30 2 -7 14 8.90 7.20 2 -7 14 3.90 5.70 -2 7 -14 -3.40 8.60 2 7 14 -4.10 2.60 2 7 14 -0.10 6.70 2 7 14 0.40 3.80 3 -7 14 55.99 9.60 3 -7 14 60.39 11.20 3 7 14 46.50 9.80 -3 7 -14 66.49 14.30 3 7 14 45.30 6.90 4 -7 14 6.00 6.20 4 -7 14 -5.10 7.30 4 7 14 0.30 4.20 -4 7 -14 22.10 11.20 4 7 14 -1.50 7.30 5 -7 14 21.60 8.00 5 -7 14 22.90 9.90 -5 7 -14 19.10 12.20 5 7 14 -1.10 7.20 5 7 14 14.60 6.10 6 -7 14 37.90 11.30 6 -7 14 34.10 9.20 6 -7 14 34.80 8.80 6 7 14 28.50 9.70 6 7 14 46.90 8.90 -6 7 -14 62.29 15.50 7 -7 14 24.20 11.30 7 -7 14 19.10 8.30 7 -7 14 11.80 7.90 -7 7 -14 17.80 12.60 7 7 14 12.70 8.90 7 7 14 23.60 7.40 8 -7 14 43.60 10.80 8 -7 14 49.60 13.80 8 -7 14 44.10 9.60 -8 7 -14 56.19 16.50 8 7 14 54.79 12.80 8 7 14 36.00 9.40 9 -7 14 7.80 8.20 9 -7 14 -2.80 10.00 -9 7 -14 -4.70 13.00 9 7 14 -2.00 9.00 9 7 14 1.10 6.90 10 -7 14 10.20 8.80 10 -7 14 -10.30 9.50 10 7 14 0.30 7.00 -10 7 -14 8.90 14.60 10 7 14 0.60 9.50 -14 -8 14 6.30 9.30 -14 -8 14 -7.00 9.50 -14 8 14 1.10 7.20 14 8 -14 10.70 9.70 -14 8 14 -14.70 7.80 -13 -8 14 -11.00 7.70 -13 -8 14 3.30 10.50 -13 8 14 -10.80 7.70 13 8 -14 -4.00 7.80 -13 8 14 7.70 6.80 -12 -8 14 6.30 9.60 -12 -8 14 -4.30 7.50 -12 8 14 -10.30 6.60 -12 8 14 1.70 5.60 12 8 -14 0.20 7.80 -11 -8 14 -4.00 7.60 -11 -8 14 -7.40 8.80 -11 8 14 -2.40 5.60 -11 8 14 -9.00 6.90 11 8 -14 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77.19 10.20 -1 8 14 62.89 10.50 -1 8 14 65.89 8.70 1 8 -14 53.49 12.60 -1 8 14 83.79 6.70 0 -8 14 15.20 6.10 0 -8 14 8.10 6.80 0 -8 14 9.50 6.10 0 8 -14 8.70 9.60 0 8 14 15.50 3.90 0 8 14 23.50 5.50 0 8 14 18.30 7.60 1 -8 14 67.89 9.90 1 -8 14 80.09 10.80 1 8 14 71.79 7.50 -1 8 -14 74.09 14.50 1 8 14 76.59 6.80 1 8 14 73.19 11.60 2 -8 14 12.50 7.40 2 -8 14 3.70 6.30 -2 8 -14 7.40 9.50 2 8 14 8.70 4.20 2 8 14 -3.20 5.60 2 8 14 1.90 3.40 3 -8 14 41.50 8.70 3 -8 14 23.30 9.10 3 8 14 25.40 5.60 3 8 14 20.00 8.40 -3 8 -14 29.30 10.80 4 -8 14 245.58 20.00 4 -8 14 242.98 18.40 -4 8 -14 297.67 27.90 4 8 14 271.37 20.10 4 8 14 269.87 15.20 5 -8 14 205.98 18.10 5 -8 14 172.08 17.40 5 8 14 192.38 18.30 5 8 14 192.08 14.30 -5 8 -14 260.67 26.50 6 -8 14 0.70 6.80 6 -8 14 7.90 9.50 6 -8 14 7.50 6.20 6 8 14 -0.70 5.10 6 8 14 -4.70 7.50 -6 8 -14 -7.80 10.90 7 -8 14 -5.40 8.20 7 -8 14 7.90 8.10 7 -8 14 12.30 7.80 -7 8 -14 -2.40 10.40 7 8 14 3.40 6.10 7 8 14 1.40 8.00 8 -8 14 16.80 8.50 8 -8 14 8.60 8.00 8 -8 14 21.60 11.20 -8 8 -14 14.50 13.10 8 8 14 10.30 8.80 8 8 14 16.40 7.70 9 -8 14 -0.30 8.40 9 -8 14 13.90 11.40 9 8 14 0.20 6.40 9 8 14 -4.80 8.90 -9 8 -14 3.40 14.10 10 -8 14 43.30 11.80 10 -8 14 40.80 15.10 10 8 14 40.30 10.90 10 8 14 56.09 14.00 -10 8 -14 31.40 16.20 -14 -9 14 16.70 10.50 -14 -9 14 -9.80 11.60 -14 9 14 14.80 9.10 -14 9 14 1.70 9.10 14 9 -14 0.00 9.00 -13 -9 14 5.70 9.00 -13 -9 14 16.30 11.70 -13 9 14 12.60 9.20 13 9 -14 4.20 8.90 -13 9 14 16.10 8.00 -12 -9 14 3.50 10.40 -12 -9 14 -2.10 7.60 -12 9 14 7.70 6.10 12 9 -14 13.20 8.20 -12 9 14 -3.00 7.90 -11 -9 14 73.59 12.20 -11 -9 14 73.89 15.50 -11 9 14 97.99 15.20 -11 9 14 75.59 11.00 11 9 -14 64.39 12.40 -10 -9 14 6.90 8.80 -10 -9 14 4.30 7.80 -10 9 14 10.80 8.80 10 9 -14 1.50 7.00 -10 9 14 -0.40 4.90 -9 -9 14 15.90 8.60 -9 -9 14 25.50 10.70 9 9 -14 17.50 11.30 -9 9 14 18.30 8.10 -9 9 14 20.40 5.90 -8 -9 14 21.10 7.70 -8 -9 14 16.50 7.20 8 9 -14 39.20 12.60 -8 9 14 16.50 8.50 -8 9 14 27.00 5.50 -7 -9 14 87.89 11.90 -7 -9 14 54.49 9.50 7 9 -14 77.39 14.20 -7 9 14 82.59 7.00 -7 9 14 77.49 12.30 -6 -9 14 327.87 19.90 -6 -9 14 328.77 18.90 -6 -9 14 304.47 18.40 6 9 -14 295.57 25.50 -6 9 14 310.87 19.90 -5 -9 14 65.59 10.50 -5 -9 14 74.19 10.20 -5 -9 14 73.89 10.00 5 9 -14 79.59 15.40 -5 9 14 87.49 12.00 -4 -9 14 -3.30 4.60 -4 -9 14 1.90 6.00 -4 -9 14 11.80 6.60 -4 9 14 9.70 6.40 4 9 -14 -4.50 8.90 -4 9 14 -0.60 6.60 -3 -9 14 291.67 17.30 -3 -9 14 306.87 18.10 -3 -9 14 290.07 17.60 -3 9 14 290.47 17.50 -3 9 14 284.37 19.50 3 9 -14 336.17 24.90 -2 -9 14 138.59 12.50 -2 -9 14 138.69 12.80 -2 -9 14 141.39 13.40 -2 9 14 124.79 12.30 -2 9 14 136.09 14.20 2 9 -14 150.98 17.90 -1 -9 14 89.69 10.70 -1 -9 14 89.39 11.00 -1 -9 14 82.99 11.10 -1 9 14 97.39 12.50 -1 9 14 93.19 10.20 1 9 -14 70.89 13.70 0 -9 14 11.00 6.40 0 -9 14 19.70 6.30 0 -9 14 5.00 6.80 0 9 14 3.10 6.90 0 9 -14 12.80 9.90 0 9 14 7.80 4.80 1 -9 14 50.49 9.10 1 -9 14 48.50 9.60 -1 9 -14 73.09 14.50 1 9 14 58.19 7.40 1 9 14 50.69 10.20 2 -9 14 82.59 11.60 2 -9 14 92.09 12.20 2 9 14 95.59 12.90 -2 9 -14 81.59 15.00 3 -9 14 160.98 15.90 3 -9 14 201.18 17.50 3 9 14 174.18 16.60 -3 9 -14 178.28 21.70 4 -9 14 0.50 6.30 4 -9 14 3.00 7.90 4 9 14 -1.00 7.20 -4 9 -14 1.80 9.00 5 -9 14 6.50 6.70 5 -9 14 7.50 9.30 5 -9 14 17.70 7.90 -5 9 -14 5.30 10.10 5 9 14 10.40 7.80 6 -9 14 154.58 16.60 6 -9 14 159.48 18.00 6 -9 14 211.08 18.60 6 9 14 166.18 18.10 -6 9 -14 208.28 24.40 7 -9 14 -11.50 6.00 7 -9 14 -3.20 9.20 7 -9 14 33.10 9.70 7 9 14 -8.50 6.90 -7 9 -14 14.60 12.40 8 -9 14 12.70 9.10 8 -9 14 15.60 11.00 8 -9 14 32.40 9.70 8 9 14 17.90 9.50 -8 9 -14 13.30 13.30 9 -9 14 4.50 11.10 9 -9 14 8.60 9.40 9 9 14 15.60 10.60 -9 9 -14 16.60 15.80 -14 -10 14 5.70 11.90 14 10 -14 6.80 9.90 -14 10 14 21.50 9.50 -13 -10 14 8.30 11.70 -13 -10 14 66.09 12.70 -13 10 14 29.30 9.10 -13 10 14 14.80 10.90 13 10 -14 45.20 12.90 -12 -10 14 9.10 9.90 -12 -10 14 12.80 11.50 -12 10 14 13.90 9.60 12 10 -14 43.40 11.90 -12 10 14 23.30 7.60 -11 -10 14 0.70 8.20 -11 -10 14 -3.30 8.70 -11 10 14 -7.70 6.60 11 10 -14 6.20 7.60 -11 10 14 6.80 5.80 -10 -10 14 15.60 10.30 -10 -10 14 5.80 7.00 -10 10 14 2.20 7.70 -10 10 14 8.10 5.60 -9 -10 14 -1.40 8.40 -9 -10 14 2.60 6.60 -9 -10 14 10.00 7.60 -9 10 14 16.60 7.80 -9 10 14 9.00 5.10 9 10 -14 -1.10 10.20 -8 -10 14 220.08 19.20 -8 -10 14 186.28 16.50 -8 10 14 260.67 22.20 8 10 -14 266.67 25.90 -8 10 14 236.28 11.90 -7 -10 14 31.50 8.40 -7 -10 14 30.40 8.60 -7 -10 14 25.90 8.10 7 10 -14 31.90 12.80 -7 10 14 44.50 9.70 -6 -10 14 8.50 6.70 -6 -10 14 14.10 7.10 -6 -10 14 30.70 8.20 6 10 -14 25.50 12.00 -6 10 14 17.40 7.70 -5 -10 14 -4.20 5.80 -5 -10 14 6.40 5.70 -5 -10 14 -7.90 5.80 5 10 -14 1.40 9.40 -5 10 14 2.90 6.10 -4 -10 14 80.89 10.80 -4 -10 14 53.49 10.00 -4 -10 14 57.69 9.00 4 10 -14 38.80 12.30 -4 10 14 54.99 10.20 -4 10 14 41.90 9.00 -3 -10 14 121.29 11.30 -3 -10 14 121.49 12.90 -3 -10 14 107.09 12.20 3 10 -14 136.69 17.70 -3 10 14 107.49 12.20 -3 10 14 125.29 13.90 -2 -10 14 19.30 7.10 -2 -10 14 26.80 7.60 -2 -10 14 11.50 6.80 2 10 -14 8.90 9.60 -2 10 14 18.20 8.10 -2 10 14 17.00 6.40 -1 -10 14 100.89 11.10 -1 -10 14 77.59 10.00 -1 -10 14 83.49 11.00 1 10 -14 67.69 13.50 -1 10 14 84.19 10.00 -1 10 14 82.49 12.00 0 -10 14 1.20 6.30 0 -10 14 6.70 6.60 0 10 14 0.80 4.60 0 10 14 13.10 7.60 0 10 -14 8.30 10.20 1 -10 14 24.90 8.50 1 -10 14 37.10 8.90 1 10 14 30.10 9.00 -1 10 -14 21.70 11.70 1 10 14 29.30 6.10 2 -10 14 5.20 7.20 2 -10 14 1.30 6.20 -2 10 -14 7.20 10.20 2 10 14 14.00 7.40 3 -10 14 110.79 13.50 3 -10 14 111.59 13.10 -3 10 -14 140.09 19.80 3 10 14 137.29 15.30 4 -10 14 20.50 9.20 4 -10 14 18.00 8.50 4 10 14 23.30 8.90 -4 10 -14 11.40 10.90 5 -10 14 69.49 12.80 5 -10 14 34.80 10.00 5 -10 14 44.70 10.10 -5 10 -14 54.69 15.50 5 10 14 54.19 11.30 6 -10 14 27.30 10.90 6 -10 14 33.50 9.90 6 -10 14 13.50 8.10 -6 10 -14 19.70 12.80 6 10 14 12.30 8.80 7 -10 14 7.10 10.20 7 -10 14 1.50 7.30 7 -10 14 2.90 7.10 7 10 14 0.60 8.30 -7 10 -14 2.80 12.00 8 -10 14 43.10 10.60 8 -10 14 22.60 9.90 8 -10 14 30.70 12.30 8 10 14 29.00 10.80 -8 10 -14 39.30 16.90 9 -10 14 2.20 8.80 9 -10 14 17.50 12.60 9 10 14 36.10 12.30 -9 10 -14 11.20 14.20 -13 -11 14 16.00 10.10 -13 -11 14 24.50 13.90 13 11 -14 8.90 9.30 -13 11 14 17.40 7.90 -13 11 14 23.80 11.30 -12 -11 14 3.60 8.70 -12 -11 14 -2.40 10.50 -12 11 14 11.10 6.60 -12 11 14 10.10 9.20 12 11 -14 23.80 10.00 -11 -11 14 12.60 11.30 -11 -11 14 2.80 8.70 -11 11 14 6.10 5.80 -11 11 14 18.60 10.00 11 11 -14 18.00 9.20 -10 -11 14 -3.50 8.80 -10 -11 14 8.60 7.50 -10 -11 14 1.90 8.20 -10 11 14 12.60 9.50 10 11 -14 0.20 10.60 -10 11 14 2.80 4.70 -9 -11 14 -6.60 6.10 -9 -11 14 8.20 8.30 -9 11 14 0.10 7.30 9 11 -14 9.50 11.60 -9 11 14 6.20 4.40 -8 -11 14 -1.00 7.00 -8 -11 14 6.00 6.80 8 11 -14 3.10 11.00 -8 11 14 -5.40 7.00 -7 -11 14 22.40 8.50 -7 -11 14 21.20 8.20 7 11 -14 14.50 11.60 -7 11 14 8.10 7.50 -6 -11 14 9.60 7.50 -6 -11 14 3.00 6.30 6 11 -14 -3.00 9.50 -6 11 14 -5.10 5.80 -5 -11 14 -3.70 5.90 -5 -11 14 -0.80 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14 31.20 9.70 5 -11 14 6.80 8.20 5 -11 14 6.40 7.50 5 -11 14 5.20 8.80 5 11 14 32.30 10.40 -5 11 -14 -15.10 9.60 6 -11 14 24.10 9.20 6 -11 14 15.60 10.80 6 -11 14 15.20 9.00 -6 11 -14 6.60 11.50 6 11 14 34.40 10.10 7 -11 14 1.10 8.00 7 -11 14 6.70 10.30 7 -11 14 4.40 8.20 -7 11 -14 -13.90 11.00 7 11 14 -6.00 7.50 8 -11 14 2.00 11.10 8 -11 14 -2.60 7.50 8 -11 14 -0.10 8.00 8 11 14 2.00 8.00 -8 11 -14 -17.70 10.10 -12 -12 14 5.20 11.90 -12 -12 14 4.00 8.50 -12 -12 14 6.50 9.10 -12 12 14 2.40 6.20 12 12 -14 4.20 8.40 -12 12 14 -6.70 7.20 -11 -12 14 9.80 8.70 -11 -12 14 26.60 12.50 -11 -12 14 17.40 9.50 -11 12 14 26.80 11.10 -11 12 14 31.00 7.60 11 12 -14 3.10 8.20 -10 -12 14 139.29 15.80 -10 -12 14 173.58 18.70 10 12 -14 114.99 19.80 -10 12 14 173.68 19.50 -9 -12 14 -7.60 6.90 -9 -12 14 10.10 8.40 9 12 -14 -1.40 10.60 -9 12 14 -0.20 7.90 -8 -12 14 -5.40 7.40 -8 -12 14 -5.60 6.10 8 12 -14 -0.20 11.00 -8 12 14 -8.50 6.60 -7 -12 14 34.00 9.60 -7 -12 14 38.70 9.30 7 12 -14 56.59 15.60 -7 12 14 37.00 9.70 -6 -12 14 -9.00 6.00 -6 -12 14 -5.60 6.20 -6 12 14 -5.70 6.10 6 12 -14 -2.00 10.40 -5 -12 14 58.99 10.60 -5 -12 14 63.69 11.20 -5 12 14 54.89 11.00 5 12 -14 41.90 13.30 -4 -12 14 13.40 8.00 -4 -12 14 7.80 7.00 4 12 -14 8.20 10.70 -4 12 14 15.10 8.00 -4 12 14 12.70 7.20 -3 -12 14 25.70 8.70 -3 -12 14 7.00 7.10 3 12 -14 15.80 11.20 -3 12 14 2.20 7.80 -3 12 14 11.20 7.10 -2 -12 14 161.78 15.60 -2 -12 14 154.48 14.70 -2 12 14 128.89 13.70 -2 12 14 115.09 14.10 2 12 -14 152.28 19.30 -1 -12 14 0.00 6.40 -1 12 14 -2.40 6.50 1 12 -14 5.90 10.20 -1 12 14 4.20 5.10 0 -12 14 2.50 7.00 0 12 -14 -11.80 9.00 0 12 14 7.70 5.00 0 12 14 -3.10 6.90 1 -12 14 1.40 7.40 1 -12 14 9.70 7.30 -1 12 -14 -2.40 10.20 1 12 14 3.10 7.30 1 12 14 -2.80 4.70 2 -12 14 30.80 8.70 2 -12 14 29.20 9.40 2 12 14 21.20 8.60 -2 12 -14 -2.40 11.10 3 -12 14 11.10 7.90 3 -12 14 33.70 9.80 -3 12 -14 16.30 12.40 3 12 14 27.90 9.10 4 -12 14 33.00 10.30 4 -12 14 32.40 9.20 4 -12 14 23.60 9.70 4 12 14 54.79 11.10 -4 12 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28.10 9.50 6 13 -14 22.40 12.30 -6 13 14 34.50 10.50 -5 -13 14 191.78 17.70 -5 -13 14 184.28 16.40 5 13 -14 252.07 25.30 -5 13 14 160.38 16.60 -5 13 14 194.28 19.00 -4 -13 14 236.68 18.70 -4 -13 14 236.68 19.30 -4 13 14 280.37 20.10 4 13 -14 193.88 21.80 -4 13 14 216.58 19.30 -3 -13 14 45.60 9.60 -3 -13 14 42.70 9.70 -3 13 14 33.30 8.80 3 13 -14 18.80 11.50 -3 13 14 32.80 9.50 -2 -13 14 70.99 11.70 -2 13 14 90.79 12.90 -2 13 14 80.69 11.60 2 13 -14 81.89 16.50 -1 -13 14 50.99 10.30 -1 13 14 32.00 8.10 1 13 -14 47.10 13.90 -1 13 14 42.60 10.30 0 -13 14 158.48 15.60 0 13 14 146.09 14.00 0 13 14 154.28 16.10 0 13 -14 176.88 22.10 1 -13 14 4.40 7.20 -1 13 -14 32.10 13.00 1 13 14 22.00 8.50 2 -13 14 3.00 7.30 2 13 14 -1.50 7.00 -2 13 -14 10.90 11.50 3 -13 14 36.60 10.30 3 -13 14 51.99 11.80 3 13 14 72.49 12.40 -3 13 -14 35.90 14.50 4 -13 14 88.99 14.20 4 -13 14 95.99 14.10 -4 13 -14 62.99 17.00 4 13 14 77.49 12.50 5 -13 14 118.29 16.30 5 -13 14 88.69 13.80 5 13 14 95.49 14.40 -5 13 -14 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15 82.29 12.30 -3 9 15 84.49 10.90 -2 -9 15 40.10 9.10 -2 -9 15 40.30 8.50 -2 -9 15 46.40 9.10 -2 9 15 35.40 7.70 -2 9 15 36.00 9.80 2 9 -15 37.30 12.50 -1 -9 15 317.87 18.60 -1 -9 15 325.07 19.10 -1 -9 15 328.27 19.70 1 9 -15 364.26 26.80 -1 9 15 308.07 20.80 -1 9 15 314.77 17.00 0 -9 15 9.10 6.20 0 -9 15 6.60 7.30 0 -9 15 18.60 7.30 0 9 15 18.50 8.40 0 9 15 14.70 5.30 0 9 -15 4.90 9.80 1 -9 15 8.90 7.30 1 -9 15 -7.00 5.50 1 9 15 9.30 7.60 -1 9 -15 -6.50 10.20 1 9 15 7.60 4.80 2 -9 15 -3.60 5.90 2 -9 15 4.80 7.40 2 9 15 -3.20 6.70 -2 9 -15 -0.90 10.20 3 -9 15 10.60 7.30 3 -9 15 5.40 7.80 -3 9 -15 -11.60 9.60 3 9 15 5.80 7.90 4 -9 15 4.30 7.10 4 -9 15 -11.20 7.60 4 9 15 -2.60 7.00 -4 9 -15 -8.10 10.20 5 -9 15 -10.80 6.00 5 -9 15 -0.30 8.60 5 9 15 -4.50 7.30 -5 9 -15 0.00 11.90 6 -9 15 -5.20 8.70 6 -9 15 0.50 7.20 6 -9 15 3.70 7.40 6 9 15 -7.80 7.20 -6 9 -15 -1.20 11.40 7 -9 15 -6.80 7.00 7 -9 15 -0.20 10.00 7 -9 15 -5.20 6.90 7 9 15 9.60 9.70 -7 9 -15 -1.70 10.80 8 -9 15 -1.70 8.20 8 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15 12.10 7.70 -8 -11 15 10.20 8.10 -8 11 15 -0.90 7.00 8 11 -15 7.30 11.20 -7 -11 15 17.40 8.10 -7 -11 15 11.50 7.30 7 11 -15 -0.30 10.90 -7 11 15 13.10 8.20 -6 -11 15 28.70 8.70 -6 -11 15 15.00 7.90 6 11 -15 27.80 12.70 -6 11 15 9.30 7.00 -5 -11 15 5.10 6.80 -5 -11 15 4.30 6.70 5 11 -15 -10.70 9.20 -5 11 15 -2.20 6.00 -5 11 15 1.80 7.70 -4 -11 15 299.47 18.80 -4 -11 15 268.77 18.90 -4 -11 15 284.97 23.50 -4 11 15 265.47 19.00 -4 11 15 280.57 21.00 4 11 -15 257.37 24.00 -3 -11 15 8.40 7.00 -3 -11 15 0.60 5.90 -3 -11 15 -4.00 6.20 -3 11 15 -10.30 6.30 -3 11 15 -5.40 5.30 3 11 -15 4.40 10.20 -2 -11 15 118.69 12.20 -2 -11 15 113.39 13.30 -2 -11 15 100.89 12.40 -2 11 15 127.39 13.10 2 11 -15 121.29 17.60 -2 11 15 118.09 14.30 -1 -11 15 191.58 15.10 -1 -11 15 168.08 15.90 -1 -11 15 196.18 17.00 1 11 -15 200.78 21.30 -1 11 15 177.08 17.00 -1 11 15 149.09 14.10 0 -11 15 143.89 14.50 0 -11 15 143.39 13.90 0 11 15 132.49 15.30 0 11 15 128.19 12.10 0 11 -15 86.39 16.30 1 -11 15 42.50 9.80 1 -11 15 38.50 9.50 -1 11 -15 31.50 13.00 1 11 15 39.10 9.90 2 -11 15 38.20 9.30 2 -11 15 30.20 9.60 -2 11 -15 39.50 13.50 2 11 15 27.70 9.20 3 -11 15 3.00 8.90 3 -11 15 5.10 7.50 3 11 15 3.50 7.70 -3 11 -15 3.40 10.60 4 -11 15 73.79 12.80 4 -11 15 98.29 14.40 4 -11 15 59.99 12.20 -4 11 -15 67.79 16.90 4 11 15 57.09 11.70 5 -11 15 44.20 11.60 5 -11 15 67.29 12.50 5 -11 15 52.29 11.80 5 11 15 29.80 9.90 -5 11 -15 18.10 12.50 6 -11 15 -7.10 8.90 6 -11 15 19.20 9.10 6 -11 15 -0.50 7.50 6 11 15 1.30 8.30 -6 11 -15 -2.40 12.80 7 -11 15 7.60 8.80 7 -11 15 -20.70 9.40 7 -11 15 17.40 8.60 7 11 15 -2.50 7.80 -7 11 -15 16.00 13.40 8 -11 15 33.10 13.80 8 -11 15 23.10 9.90 8 -11 15 59.19 14.30 -8 11 -15 39.90 15.80 8 11 15 42.00 12.60 -12 -12 15 35.90 14.70 -12 -12 15 63.99 12.50 -12 -12 15 55.49 13.00 12 12 -15 64.19 17.20 -12 12 15 57.99 14.00 -11 -12 15 4.30 8.30 -11 -12 15 -6.40 6.60 -11 12 15 -8.40 8.20 11 12 -15 2.00 12.40 -10 -12 15 -12.00 7.20 -10 -12 15 -1.50 7.70 10 12 -15 6.60 12.50 -10 12 15 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_computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 38844