data_20190605d _audit_creation_date 2019-06-12 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _shelx_SHELXL_version_number '2014/7' _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_name '' _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C15 H14 Cl N3 O6' _chemical_formula_sum 'C15 H14 Cl N3 O6' _chemical_formula_weight 367.74 _chemical_absolute_configuration ad _chemical_melting_point ? _chemical_oxdiff_formula c1h1n1o1Cl1 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'orthorhombic' _space_group_IT_number 19 _space_group_name_H-M_alt 'P 21 21 21' _space_group_name_Hall 'P 2ac 2ab' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' _cell_length_a 8.35980(10) _cell_length_b 11.94590(10) _cell_length_c 32.5899(4) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 3254.60(6) _cell_formula_units_Z 8 _cell_measurement_reflns_used 13545 _cell_measurement_temperature 100.00(10) _cell_measurement_theta_max 74.9850 _cell_measurement_theta_min 3.9550 _shelx_estimated_absorpt_T_max 0.792 _shelx_estimated_absorpt_T_min 0.641 _exptl_absorpt_coefficient_mu 2.443 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.84993 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.35a (Rigaku Oxford Diffraction, 2018) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.501 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description block _exptl_crystal_F_000 1520 _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.15 _exptl_crystal_size_min 0.1 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0365 _diffrn_reflns_av_unetI/netI 0.0370 _diffrn_reflns_Laue_measured_fraction_full 0.993 _diffrn_reflns_Laue_measured_fraction_max 0.972 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 38 _diffrn_reflns_limit_l_min -40 _diffrn_reflns_number 15719 _diffrn_reflns_point_group_measured_fraction_full 0.978 _diffrn_reflns_point_group_measured_fraction_max 0.943 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 75.343 _diffrn_reflns_theta_min 2.712 _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100.00(10) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 0.993 _diffrn_measured_fraction_theta_max 0.972 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -114.00 -31.00 0.10 0.10 -- -47.70 -65.00 92.00 830 2 \w -172.00-142.00 0.10 0.10 -- -102.00 -56.00-102.00 300 3 \w -106.00 -29.00 0.10 0.10 -- -102.00 65.00-131.00 770 4 \w 45.00 95.00 0.10 0.10 -- 104.75-121.00 24.00 500 5 \w -116.00 -88.00 0.10 0.10 -- -47.70-125.00 30.00 280 6 \w -108.00 -82.00 0.10 0.10 -- -47.70-125.00-150.00 260 7 \w -5.00 31.00 0.10 0.10 -- 47.70 -19.00 -90.00 360 8 \w -175.00-143.00 0.10 0.10 -- -102.00 -30.00-150.00 320 9 \w -144.00 -96.00 0.10 0.10 -- -102.00 -30.00 120.00 480 10 \w -166.00 -88.00 0.10 0.10 -- -102.00 -15.00 -30.00 780 11 \w -126.00 -89.00 0.10 0.10 -- -102.00 -30.00-150.00 370 12 \w -175.00-150.00 0.10 0.10 -- -102.00 -30.00 120.00 250 13 \w 34.00 59.00 0.10 0.10 -- 104.75 -94.00 60.00 250 14 \w 101.00 176.00 0.10 0.10 -- 104.75 45.00-180.00 750 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy R, DW system, HyPix' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0739892000 _diffrn_orient_matrix_UB_12 -0.0926543000 _diffrn_orient_matrix_UB_13 0.0268433000 _diffrn_orient_matrix_UB_21 -0.1673624000 _diffrn_orient_matrix_UB_22 0.0300203000 _diffrn_orient_matrix_UB_23 -0.0164413000 _diffrn_orient_matrix_UB_31 0.0216898000 _diffrn_orient_matrix_UB_32 -0.0845207000 _diffrn_orient_matrix_UB_33 -0.0352726000 _diffrn_oxdiff_digest_frames ; 015b991b5d2fc8fdb5c6048012c73b013106500fe10 ; _diffrn_oxdiff_digest_hkl ; 01f51b41985444fba5ae4c242160387901605f ; _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_source 'Rotating-anode X-ray tube' _diffrn_source_type 'Rigaku (Cu) X-ray Source' _reflns_Friedel_coverage 0.710 _reflns_Friedel_fraction_full 0.957 _reflns_Friedel_fraction_max 0.905 _reflns_number_gt 6070 _reflns_number_total 6356 _reflns_odcompleteness_completeness 99.37 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 66.97 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'CrysAlisPro 1.171.40.35a (Rigaku OD, 2018)' _computing_data_collection 'CrysAlisPro 1.171.40.35a (Rigaku OD, 2018)' _computing_data_reduction 'CrysAlisPro 1.171.40.35a (Rigaku OD, 2018)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _refine_diff_density_max 0.299 _refine_diff_density_min -0.301 _refine_diff_density_rms 0.053 _refine_ls_abs_structure_details ; Flack x determined using 2394 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.005(5) _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.099 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 455 _refine_ls_number_reflns 6356 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0367 _refine_ls_R_factor_gt 0.0315 _refine_ls_restrained_S_all 1.099 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0340P)^2^+1.5656P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0770 _refine_ls_wR_factor_ref 0.0834 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C13(H13), C28(H28) 2.b Aromatic/amide H refined with riding coordinates: C2(H2), C5(H5), C6(H6), C7(H7), C14(H14), C17(H17), C20(H20), C21(H21), C22(H22), C29(H29) 2.c X=CH2 refined with riding coordinates: C15(H15A,H15B), C30(H30A,H30B) 2.d Idealised Me refined as rotating group: C10(H10A,H10B,H10C), C12(H12A,H12B,H12C), C25(H25A,H25B,H25C), C27(H27A,H27B, H27C) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cl1 Cl -0.08249(9) 0.17060(6) 0.42638(2) 0.02930(16) Uani 1 1 d . . . . . O1 O 0.4147(3) 0.55585(17) 0.31396(6) 0.0293(5) Uani 1 1 d . . . . . O2 O 0.5549(2) 0.68354(17) 0.34467(6) 0.0295(5) Uani 1 1 d . . . . . O3 O 0.3078(2) 0.81282(16) 0.37604(6) 0.0258(4) Uani 1 1 d . . . . . O4 O 0.4356(3) 0.84811(17) 0.43585(6) 0.0282(4) Uani 1 1 d . . . . . O5 O 0.5542(2) 0.52827(17) 0.49755(6) 0.0229(4) Uani 1 1 d . . . . . O6 O 0.6668(2) 0.57991(17) 0.43712(6) 0.0244(4) Uani 1 1 d . . . . . N1 N 0.4487(3) 0.61264(19) 0.34422(7) 0.0226(5) Uani 1 1 d . . . . . N2 N 0.3893(3) 0.66851(19) 0.41384(6) 0.0200(5) Uani 1 1 d . . . . . N3 N 0.4076(3) 0.62457(19) 0.45272(7) 0.0195(5) Uani 1 1 d . . . . . C1 C 0.0221(3) 0.2915(2) 0.43972(8) 0.0229(5) Uani 1 1 d . . . . . C2 C 0.1018(3) 0.3506(2) 0.40965(8) 0.0214(5) Uani 1 1 d . . . . . H2 H 0.1013 0.3245 0.3828 0.026 Uiso 1 1 calc R . . . . C3 C 0.1840(3) 0.4500(2) 0.41932(8) 0.0194(5) Uani 1 1 d . . . . . C4 C 0.1823(3) 0.4886(2) 0.46020(8) 0.0203(5) Uani 1 1 d . . . . . C5 C 0.1035(3) 0.4246(2) 0.48987(9) 0.0227(6) Uani 1 1 d . . . . . H5 H 0.1047 0.4487 0.5170 0.027 Uiso 1 1 calc R . . . . C6 C 0.0240(4) 0.3268(2) 0.48025(9) 0.0247(6) Uani 1 1 d . . . . . H6 H -0.0272 0.2854 0.5005 0.030 Uiso 1 1 calc R . . . . C7 C 0.2722(3) 0.4986(2) 0.38489(8) 0.0197(5) Uani 1 1 d . . . . . H7 H 0.2695 0.4566 0.3609 0.024 Uiso 1 1 calc R . . . . C8 C 0.3558(3) 0.5936(2) 0.38239(8) 0.0189(5) Uani 1 1 d . . . . . C9 C 0.3828(3) 0.7856(2) 0.41065(8) 0.0219(6) Uani 1 1 d . . . . . C10 C 0.2970(4) 0.9316(3) 0.36783(11) 0.0344(7) Uani 1 1 d . . . . . H10A H 0.2383 0.9435 0.3429 0.052 Uiso 1 1 calc GR . . . . H10B H 0.4026 0.9622 0.3650 0.052 Uiso 1 1 calc GR . . . . H10C H 0.2429 0.9680 0.3901 0.052 Uiso 1 1 calc GR . . . . C11 C 0.5546(3) 0.5757(2) 0.46060(8) 0.0196(5) Uani 1 1 d . . . . . C12 C 0.7024(4) 0.4725(3) 0.50806(10) 0.0292(6) Uani 1 1 d . . . . . H12A H 0.7228 0.4136 0.4887 0.044 Uiso 1 1 calc GR . . . . H12B H 0.6940 0.4413 0.5351 0.044 Uiso 1 1 calc GR . . . . H12C H 0.7887 0.5255 0.5073 0.044 Uiso 1 1 calc GR . . . . C13 C 0.2588(3) 0.5969(2) 0.47474(8) 0.0208(6) Uani 1 1 d . . . . . H13 H 0.2873 0.5862 0.5036 0.025 Uiso 1 1 calc R . . . . C14 C 0.1501(3) 0.6969(2) 0.47280(9) 0.0251(6) Uani 1 1 d . . . . . H14 H 0.1827 0.7608 0.4867 0.030 Uiso 1 1 calc R . . . . C15 C 0.0125(4) 0.7020(3) 0.45307(9) 0.0289(6) Uani 1 1 d . . . . . H15A H -0.0248 0.6400 0.4387 0.035 Uiso 1 1 calc R . . . . H15B H -0.0473 0.7677 0.4535 0.035 Uiso 1 1 calc R . . . . Cl2 Cl 1.03702(9) 0.69977(5) 0.32416(2) 0.02721(16) Uani 1 1 d . . . . . O7 O 0.5008(2) 0.33261(16) 0.43641(5) 0.0227(4) Uani 1 1 d . . . . . O8 O 0.4384(3) 0.16856(17) 0.41237(6) 0.0282(4) Uani 1 1 d . . . . . O9 O 0.7016(2) 0.02246(16) 0.36254(6) 0.0253(4) Uani 1 1 d . . . . . O10 O 0.8968(3) 0.03601(18) 0.31478(7) 0.0301(5) Uani 1 1 d . . . . . O11 O 0.4126(3) 0.11469(17) 0.29502(6) 0.0267(4) Uani 1 1 d . . . . . O12 O 0.3068(2) 0.25322(18) 0.33371(6) 0.0277(4) Uani 1 1 d . . . . . N4 N 0.5031(3) 0.26048(19) 0.40945(6) 0.0198(5) Uani 1 1 d . . . . . N5 N 0.5688(3) 0.20698(19) 0.34008(7) 0.0203(5) Uani 1 1 d . . . . . N6 N 0.7049(3) 0.17012(19) 0.31995(7) 0.0223(5) Uani 1 1 d . . . . . C16 C 0.9693(3) 0.5634(2) 0.31719(8) 0.0207(5) Uani 1 1 d . . . . . C17 C 0.8605(3) 0.5189(2) 0.34451(8) 0.0205(5) Uani 1 1 d . . . . . H17 H 0.8302 0.5599 0.3675 0.025 Uiso 1 1 calc R . . . . C18 C 0.7951(3) 0.4117(2) 0.33791(8) 0.0191(5) Uani 1 1 d . . . . . C19 C 0.8416(3) 0.3514(2) 0.30281(8) 0.0194(5) Uani 1 1 d . . . . . C20 C 0.9599(4) 0.3972(2) 0.27742(8) 0.0229(6) Uani 1 1 d . . . . . H20 H 0.9961 0.3556 0.2551 0.028 Uiso 1 1 calc R . . . . C21 C 1.0246(4) 0.5014(2) 0.28423(8) 0.0242(6) Uani 1 1 d . . . . . H21 H 1.1039 0.5295 0.2671 0.029 Uiso 1 1 calc R . . . . C22 C 0.6880(3) 0.3738(2) 0.37067(8) 0.0195(5) Uani 1 1 d . . . . . H22 H 0.6888 0.4168 0.3945 0.023 Uiso 1 1 calc R . . . . C23 C 0.5899(3) 0.2863(2) 0.37094(7) 0.0191(5) Uani 1 1 d . . . . . C24 C 0.4159(4) 0.1958(2) 0.32283(8) 0.0229(5) Uani 1 1 d . . . . . C25 C 0.2665(4) 0.1135(3) 0.27088(11) 0.0354(7) Uani 1 1 d . . . . . H25A H 0.2745 0.0573 0.2499 0.053 Uiso 1 1 calc GR . . . . H25B H 0.2513 0.1855 0.2584 0.053 Uiso 1 1 calc GR . . . . H25C H 0.1773 0.0970 0.2884 0.053 Uiso 1 1 calc GR . . . . C26 C 0.7781(3) 0.0717(2) 0.33133(9) 0.0236(6) Uani 1 1 d . . . . . C27 C 0.7722(4) -0.0817(3) 0.37638(11) 0.0357(7) Uani 1 1 d . . . . . H27A H 0.7697 -0.1354 0.3545 0.053 Uiso 1 1 calc GR . . . . H27B H 0.7127 -0.1100 0.3993 0.053 Uiso 1 1 calc GR . . . . H27C H 0.8811 -0.0688 0.3845 0.053 Uiso 1 1 calc GR . . . . C28 C 0.7705(3) 0.2418(2) 0.28762(8) 0.0221(6) Uani 1 1 d . . . . . H28 H 0.8581 0.1999 0.2748 0.027 Uiso 1 1 calc R . . . . C29 C 0.6455(4) 0.2598(3) 0.25466(8) 0.0274(6) Uani 1 1 d . . . . . H29 H 0.6306 0.2024 0.2358 0.033 Uiso 1 1 calc R . . . . C30 C 0.5557(4) 0.3499(3) 0.25042(10) 0.0341(7) Uani 1 1 d . . . . . H30A H 0.5666 0.4093 0.2686 0.041 Uiso 1 1 calc R . . . . H30B H 0.4815 0.3540 0.2292 0.041 Uiso 1 1 calc R . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cl1 0.0315(3) 0.0219(3) 0.0345(4) 0.0040(3) -0.0037(3) -0.0064(3) O1 0.0455(13) 0.0249(10) 0.0174(9) 0.0000(8) 0.0043(9) -0.0005(9) O2 0.0293(11) 0.0309(11) 0.0283(10) 0.0040(9) 0.0056(9) -0.0067(9) O3 0.0325(11) 0.0177(10) 0.0271(10) 0.0022(8) -0.0059(8) -0.0021(8) O4 0.0352(12) 0.0233(10) 0.0261(10) -0.0058(8) -0.0009(9) -0.0047(9) O5 0.0212(10) 0.0258(10) 0.0217(9) 0.0002(7) -0.0015(8) 0.0005(8) O6 0.0203(10) 0.0265(10) 0.0265(10) -0.0052(8) 0.0035(8) -0.0028(8) N1 0.0298(13) 0.0179(11) 0.0200(11) 0.0029(9) 0.0042(10) 0.0046(10) N2 0.0256(12) 0.0195(11) 0.0148(10) -0.0004(9) -0.0001(9) -0.0017(10) N3 0.0201(11) 0.0224(11) 0.0162(10) 0.0007(9) 0.0014(9) 0.0002(9) C1 0.0202(12) 0.0218(13) 0.0268(13) 0.0026(11) -0.0018(11) 0.0009(11) C2 0.0220(13) 0.0203(13) 0.0218(12) 0.0004(10) -0.0017(11) 0.0031(11) C3 0.0209(12) 0.0165(13) 0.0206(13) 0.0014(10) -0.0010(11) 0.0020(10) C4 0.0192(12) 0.0228(13) 0.0190(12) 0.0000(10) 0.0006(10) 0.0023(11) C5 0.0226(13) 0.0245(14) 0.0211(13) 0.0000(11) -0.0001(11) 0.0027(11) C6 0.0241(13) 0.0249(14) 0.0252(13) 0.0067(11) 0.0014(11) 0.0009(12) C7 0.0237(14) 0.0196(13) 0.0159(12) -0.0001(10) 0.0002(10) 0.0039(11) C8 0.0224(13) 0.0185(13) 0.0160(12) -0.0001(10) 0.0033(10) 0.0016(10) C9 0.0246(14) 0.0184(13) 0.0228(13) -0.0014(11) 0.0027(11) -0.0024(11) C10 0.0409(18) 0.0188(15) 0.0435(18) 0.0067(13) -0.0047(15) -0.0036(13) C11 0.0204(13) 0.0178(12) 0.0205(12) -0.0056(10) 0.0000(11) -0.0025(10) C12 0.0267(15) 0.0278(15) 0.0332(16) 0.0008(12) -0.0081(13) 0.0036(13) C13 0.0215(13) 0.0262(14) 0.0147(12) -0.0029(10) 0.0006(10) -0.0013(11) C14 0.0262(14) 0.0211(14) 0.0281(14) -0.0068(11) 0.0065(11) -0.0017(12) C15 0.0258(14) 0.0263(14) 0.0345(15) -0.0033(12) 0.0035(12) 0.0034(12) Cl2 0.0311(3) 0.0193(3) 0.0313(3) 0.0003(3) 0.0004(3) -0.0061(3) O7 0.0294(10) 0.0227(9) 0.0159(8) -0.0034(7) 0.0012(7) -0.0001(8) O8 0.0369(12) 0.0206(10) 0.0269(10) -0.0003(8) 0.0058(9) -0.0072(9) O9 0.0280(10) 0.0192(10) 0.0286(10) 0.0035(8) 0.0054(9) -0.0009(8) O10 0.0296(11) 0.0272(11) 0.0336(11) -0.0002(9) 0.0087(9) 0.0049(9) O11 0.0302(11) 0.0238(10) 0.0261(10) -0.0091(8) -0.0005(9) -0.0040(9) O12 0.0243(10) 0.0303(11) 0.0286(10) -0.0061(9) 0.0001(8) 0.0028(9) N4 0.0224(11) 0.0188(11) 0.0182(10) 0.0004(8) 0.0004(9) 0.0008(9) N5 0.0216(11) 0.0194(10) 0.0198(10) -0.0044(8) 0.0036(9) -0.0012(9) N6 0.0279(12) 0.0164(11) 0.0227(11) -0.0021(9) 0.0082(9) 0.0010(9) C16 0.0217(12) 0.0199(13) 0.0206(12) 0.0032(10) -0.0038(11) -0.0007(11) C17 0.0215(12) 0.0205(13) 0.0194(12) -0.0016(10) -0.0008(10) 0.0009(10) C18 0.0202(12) 0.0183(13) 0.0187(12) 0.0026(10) -0.0012(10) 0.0003(10) C19 0.0223(13) 0.0170(13) 0.0188(12) 0.0002(10) 0.0004(10) 0.0005(10) C20 0.0276(14) 0.0219(13) 0.0193(12) -0.0017(10) 0.0019(11) 0.0019(12) C21 0.0272(14) 0.0251(14) 0.0204(13) 0.0055(10) 0.0022(11) -0.0019(12) C22 0.0232(13) 0.0207(13) 0.0147(12) -0.0031(10) 0.0000(10) 0.0011(11) C23 0.0250(13) 0.0179(12) 0.0143(11) 0.0002(9) 0.0026(10) 0.0014(11) C24 0.0302(14) 0.0202(13) 0.0183(12) -0.0011(10) 0.0008(11) -0.0069(11) C25 0.0298(17) 0.0382(18) 0.0383(17) -0.0128(15) -0.0082(14) -0.0021(14) C26 0.0257(14) 0.0203(13) 0.0247(14) -0.0024(11) 0.0018(11) -0.0027(11) C27 0.0379(18) 0.0238(16) 0.0452(19) 0.0087(14) 0.0054(15) 0.0035(14) C28 0.0278(14) 0.0196(13) 0.0189(12) -0.0019(10) 0.0052(11) -0.0013(11) C29 0.0371(16) 0.0294(15) 0.0157(12) -0.0050(11) 0.0027(12) -0.0120(13) C30 0.0409(18) 0.0339(16) 0.0275(15) 0.0033(12) -0.0055(14) -0.0084(15) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cl1 C1 1.743(3) . ? O1 N1 1.230(3) . ? O2 N1 1.227(3) . ? O3 C9 1.331(3) . ? O3 C10 1.447(4) . ? O4 C9 1.194(3) . ? O5 C11 1.331(3) . ? O5 C12 1.448(4) . ? O6 C11 1.212(3) . ? N1 C8 1.484(3) . ? N2 N3 1.380(3) . ? N2 C8 1.389(3) . ? N2 C9 1.403(4) . ? N3 C11 1.384(4) . ? N3 C13 1.474(4) . ? C1 C2 1.379(4) . ? C1 C6 1.386(4) . ? C2 H2 0.9300 . ? C2 C3 1.408(4) . ? C3 C4 1.410(4) . ? C3 C7 1.463(4) . ? C4 C5 1.397(4) . ? C4 C13 1.519(4) . ? C5 H5 0.9300 . ? C5 C6 1.381(4) . ? C6 H6 0.9300 . ? C7 H7 0.9300 . ? C7 C8 1.335(4) . ? C10 H10A 0.9600 . ? C10 H10B 0.9600 . ? C10 H10C 0.9600 . ? C12 H12A 0.9600 . ? C12 H12B 0.9600 . ? C12 H12C 0.9600 . ? C13 H13 0.9800 . ? C13 C14 1.502(4) . ? C14 H14 0.9300 . ? C14 C15 1.319(4) . ? C15 H15A 0.9300 . ? C15 H15B 0.9300 . ? Cl2 C16 1.739(3) . ? O7 N4 1.231(3) . ? O8 N4 1.228(3) . ? O9 C26 1.338(4) . ? O9 C27 1.450(4) . ? O10 C26 1.207(4) . ? O11 C24 1.327(3) . ? O11 C25 1.453(4) . ? O12 C24 1.195(4) . ? N4 C23 1.482(3) . ? N5 N6 1.385(3) . ? N5 C23 1.393(3) . ? N5 C24 1.403(4) . ? N6 C26 1.376(4) . ? N6 C28 1.464(3) . ? C16 C17 1.379(4) . ? C16 C21 1.385(4) . ? C17 H17 0.9300 . ? C17 C18 1.408(4) . ? C18 C19 1.406(4) . ? C18 C22 1.465(4) . ? C19 C20 1.401(4) . ? C19 C28 1.521(4) . ? C20 H20 0.9300 . ? C20 C21 1.375(4) . ? C21 H21 0.9300 . ? C22 H22 0.9300 . ? C22 C23 1.329(4) . ? C25 H25A 0.9600 . ? C25 H25B 0.9600 . ? C25 H25C 0.9600 . ? C27 H27A 0.9600 . ? C27 H27B 0.9600 . ? C27 H27C 0.9600 . ? C28 H28 0.9800 . ? C28 C29 1.514(4) . ? C29 H29 0.9300 . ? C29 C30 1.320(5) . ? C30 H30A 0.9300 . ? C30 H30B 0.9300 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C9 O3 C10 115.2(2) . . ? C11 O5 C12 114.1(2) . . ? O1 N1 C8 117.8(2) . . ? O2 N1 O1 123.9(2) . . ? O2 N1 C8 118.3(2) . . ? N3 N2 C8 117.0(2) . . ? N3 N2 C9 116.8(2) . . ? C8 N2 C9 125.4(2) . . ? N2 N3 C11 115.4(2) . . ? N2 N3 C13 116.0(2) . . ? C11 N3 C13 124.4(2) . . ? C2 C1 Cl1 119.3(2) . . ? C2 C1 C6 121.0(3) . . ? C6 C1 Cl1 119.7(2) . . ? C1 C2 H2 119.7 . . ? C1 C2 C3 120.6(3) . . ? C3 C2 H2 119.7 . . ? C2 C3 C4 118.9(2) . . ? C2 C3 C7 114.2(2) . . ? C4 C3 C7 126.8(2) . . ? C3 C4 C13 124.7(2) . . ? C5 C4 C3 118.6(3) . . ? C5 C4 C13 116.6(2) . . ? C4 C5 H5 118.9 . . ? C6 C5 C4 122.2(3) . . ? C6 C5 H5 118.9 . . ? C1 C6 H6 120.7 . . ? C5 C6 C1 118.6(3) . . ? C5 C6 H6 120.7 . . ? C3 C7 H7 114.8 . . ? C8 C7 C3 130.4(2) . . ? C8 C7 H7 114.8 . . ? N2 C8 N1 114.5(2) . . ? C7 C8 N1 117.1(2) . . ? C7 C8 N2 127.4(2) . . ? O3 C9 N2 108.9(2) . . ? O4 C9 O3 127.1(3) . . ? O4 C9 N2 123.9(3) . . ? O3 C10 H10A 109.5 . . ? O3 C10 H10B 109.5 . . ? O3 C10 H10C 109.5 . . ? H10A C10 H10B 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? O5 C11 N3 110.2(2) . . ? O6 C11 O5 126.2(3) . . ? O6 C11 N3 123.5(2) . . ? O5 C12 H12A 109.5 . . ? O5 C12 H12B 109.5 . . ? O5 C12 H12C 109.5 . . ? H12A C12 H12B 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? N3 C13 C4 113.2(2) . . ? N3 C13 H13 106.9 . . ? N3 C13 C14 108.2(2) . . ? C4 C13 H13 106.9 . . ? C14 C13 C4 114.2(2) . . ? C14 C13 H13 106.9 . . ? C13 C14 H14 117.1 . . ? C15 C14 C13 125.8(3) . . ? C15 C14 H14 117.1 . . ? C14 C15 H15A 120.0 . . ? C14 C15 H15B 120.0 . . ? H15A C15 H15B 120.0 . . ? C26 O9 C27 114.8(2) . . ? C24 O11 C25 113.2(2) . . ? O7 N4 C23 117.8(2) . . ? O8 N4 O7 124.3(2) . . ? O8 N4 C23 117.9(2) . . ? N6 N5 C23 117.0(2) . . ? N6 N5 C24 121.9(2) . . ? C23 N5 C24 118.0(2) . . ? N5 N6 C28 117.5(2) . . ? C26 N6 N5 120.6(2) . . ? C26 N6 C28 121.8(2) . . ? C17 C16 Cl2 119.5(2) . . ? C17 C16 C21 120.9(3) . . ? C21 C16 Cl2 119.6(2) . . ? C16 C17 H17 119.7 . . ? C16 C17 C18 120.5(3) . . ? C18 C17 H17 119.7 . . ? C17 C18 C22 114.0(2) . . ? C19 C18 C17 118.9(2) . . ? C19 C18 C22 127.1(2) . . ? C18 C19 C28 126.7(2) . . ? C20 C19 C18 118.4(2) . . ? C20 C19 C28 114.8(2) . . ? C19 C20 H20 118.8 . . ? C21 C20 C19 122.4(3) . . ? C21 C20 H20 118.8 . . ? C16 C21 H21 120.7 . . ? C20 C21 C16 118.6(3) . . ? C20 C21 H21 120.7 . . ? C18 C22 H22 115.7 . . ? C23 C22 C18 128.7(2) . . ? C23 C22 H22 115.7 . . ? N5 C23 N4 114.1(2) . . ? C22 C23 N4 118.1(2) . . ? C22 C23 N5 127.5(2) . . ? O11 C24 N5 111.2(2) . . ? O12 C24 O11 127.3(3) . . ? O12 C24 N5 121.4(2) . . ? O11 C25 H25A 109.5 . . ? O11 C25 H25B 109.5 . . ? O11 C25 H25C 109.5 . . ? H25A C25 H25B 109.5 . . ? H25A C25 H25C 109.5 . . ? H25B C25 H25C 109.5 . . ? O9 C26 N6 111.6(2) . . ? O10 C26 O9 125.3(3) . . ? O10 C26 N6 123.1(3) . . ? O9 C27 H27A 109.5 . . ? O9 C27 H27B 109.5 . . ? O9 C27 H27C 109.5 . . ? H27A C27 H27B 109.5 . . ? H27A C27 H27C 109.5 . . ? H27B C27 H27C 109.5 . . ? N6 C28 C19 114.6(2) . . ? N6 C28 H28 106.7 . . ? N6 C28 C29 109.6(2) . . ? C19 C28 H28 106.7 . . ? C29 C28 C19 112.2(2) . . ? C29 C28 H28 106.7 . . ? C28 C29 H29 117.2 . . ? C30 C29 C28 125.6(3) . . ? C30 C29 H29 117.2 . . ? C29 C30 H30A 120.0 . . ? C29 C30 H30B 120.0 . . ? H30A C30 H30B 120.0 . . ? _shelx_res_file ; 20190605d.res created by SHELXL-2014/7 TITL 20190605d_a.res in P2(1)2(1)2(1) REM Old TITL 20190605d in P2(1)2(1)2(1) REM SHELXT solution in P2(1)2(1)2(1) REM R1 0.157, Rweak 0.032, Alpha 0.001, Orientation as input REM Flack x = 0.009 ( 0.030 ) from Parsons' quotients REM Formula found by SHELXT: C31 N3 O14 Cl2 CELL 1.54184 8.3598 11.9459 32.5899 90 90 90 ZERR 8 0.0001 0.0001 0.0004 0 0 0 LATT -1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H Cl N O UNIT 120 112 8 24 48 L.S. 8 PLAN 8 SIZE 0.1 0.15 0.2 BOND $H LIST 6 fmap 2 acta OMIT -9 4 3 OMIT 1 11 23 OMIT 1 11 22 OMIT 4 12 7 OMIT 5 12 5 OMIT -3 11 22 OMIT -7 7 20 OMIT -3 8 29 OMIT -3 11 21 OMIT 4 12 4 OMIT -1 11 25 OMIT 1 6 34 OMIT 5 12 7 OMIT -2 11 24 OMIT 7 4 26 OMIT 2 5 34 OMIT -2 11 23 OMIT 0 2 0 OMIT -4 8 28 OMIT 1 5 33 OMIT 7 4 25 OMIT 5 12 4 OMIT 4 12 5 OMIT 5 4 32 OMIT 0 6 33 OMIT 1 13 19 OMIT 1 5 34 OMIT 8 4 20 REM REM REM WGHT 0.034000 1.565600 FVAR 4.88605 CL1 3 -0.082495 0.170598 0.426382 11.00000 0.03148 0.02193 = 0.03450 0.00397 -0.00366 -0.00643 O1 5 0.414714 0.555853 0.313956 11.00000 0.04548 0.02493 = 0.01737 -0.00005 0.00432 -0.00047 O2 5 0.554880 0.683540 0.344671 11.00000 0.02929 0.03087 = 0.02834 0.00399 0.00561 -0.00673 O3 5 0.307779 0.812816 0.376043 11.00000 0.03252 0.01770 = 0.02711 0.00218 -0.00594 -0.00208 O4 5 0.435591 0.848112 0.435846 11.00000 0.03524 0.02331 = 0.02612 -0.00577 -0.00087 -0.00467 O5 5 0.554194 0.528275 0.497553 11.00000 0.02121 0.02583 = 0.02166 0.00017 -0.00154 0.00049 O6 5 0.666775 0.579914 0.437118 11.00000 0.02027 0.02651 = 0.02647 -0.00517 0.00355 -0.00276 N1 4 0.448704 0.612644 0.344221 11.00000 0.02976 0.01792 = 0.01999 0.00290 0.00422 0.00456 N2 4 0.389265 0.668509 0.413839 11.00000 0.02562 0.01950 = 0.01476 -0.00039 -0.00013 -0.00166 N3 4 0.407633 0.624570 0.452720 11.00000 0.02006 0.02236 = 0.01616 0.00072 0.00136 0.00020 C1 1 0.022138 0.291472 0.439722 11.00000 0.02020 0.02181 = 0.02683 0.00259 -0.00178 0.00086 C2 1 0.101822 0.350556 0.409651 11.00000 0.02201 0.02030 = 0.02182 0.00042 -0.00173 0.00306 AFIX 43 H2 2 0.101255 0.324496 0.382761 11.00000 -1.20000 AFIX 0 C3 1 0.183996 0.449966 0.419318 11.00000 0.02090 0.01654 = 0.02062 0.00137 -0.00104 0.00195 C4 1 0.182281 0.488627 0.460204 11.00000 0.01921 0.02280 = 0.01901 -0.00002 0.00057 0.00229 C5 1 0.103540 0.424616 0.489870 11.00000 0.02260 0.02450 = 0.02109 -0.00001 -0.00010 0.00273 AFIX 43 H5 2 0.104721 0.448732 0.517001 11.00000 -1.20000 AFIX 0 C6 1 0.024046 0.326763 0.480249 11.00000 0.02413 0.02491 = 0.02519 0.00669 0.00140 0.00093 AFIX 43 H6 2 -0.027168 0.285373 0.500536 11.00000 -1.20000 AFIX 0 C7 1 0.272165 0.498618 0.384893 11.00000 0.02375 0.01958 = 0.01590 -0.00012 0.00017 0.00385 AFIX 43 H7 2 0.269513 0.456633 0.360872 11.00000 -1.20000 AFIX 0 C8 1 0.355824 0.593563 0.382394 11.00000 0.02235 0.01851 = 0.01597 -0.00009 0.00335 0.00162 C9 1 0.382817 0.785587 0.410651 11.00000 0.02461 0.01835 = 0.02275 -0.00140 0.00266 -0.00244 C10 1 0.297003 0.931638 0.367830 11.00000 0.04095 0.01885 = 0.04349 0.00672 -0.00472 -0.00360 AFIX 137 H10A 2 0.238319 0.943512 0.342887 11.00000 -1.50000 H10B 2 0.402646 0.962200 0.365027 11.00000 -1.50000 H10C 2 0.242896 0.968018 0.390129 11.00000 -1.50000 AFIX 0 C11 1 0.554571 0.575718 0.460600 11.00000 0.02041 0.01785 = 0.02046 -0.00565 -0.00003 -0.00252 C12 1 0.702426 0.472476 0.508061 11.00000 0.02669 0.02782 = 0.03319 0.00080 -0.00809 0.00362 AFIX 137 H12A 2 0.722808 0.413643 0.488688 11.00000 -1.50000 H12B 2 0.694046 0.441310 0.535127 11.00000 -1.50000 H12C 2 0.788689 0.525485 0.507333 11.00000 -1.50000 AFIX 0 C13 1 0.258757 0.596919 0.474744 11.00000 0.02151 0.02616 = 0.01471 -0.00295 0.00062 -0.00133 AFIX 13 H13 2 0.287317 0.586231 0.503645 11.00000 -1.20000 AFIX 0 C14 1 0.150102 0.696873 0.472804 11.00000 0.02624 0.02105 = 0.02811 -0.00683 0.00650 -0.00175 AFIX 43 H14 2 0.182712 0.760847 0.486749 11.00000 -1.20000 AFIX 0 C15 1 0.012481 0.702008 0.453075 11.00000 0.02577 0.02634 = 0.03454 -0.00335 0.00346 0.00342 AFIX 93 H15A 2 -0.024755 0.639977 0.438718 11.00000 -1.20000 H15B 2 -0.047287 0.767657 0.453525 11.00000 -1.20000 AFIX 0 CL2 3 1.037020 0.699773 0.324156 11.00000 0.03107 0.01926 = 0.03131 0.00030 0.00039 -0.00606 O7 5 0.500785 0.332614 0.436414 11.00000 0.02941 0.02267 = 0.01594 -0.00338 0.00116 -0.00014 O8 5 0.438377 0.168562 0.412369 11.00000 0.03693 0.02061 = 0.02694 -0.00026 0.00582 -0.00720 O9 5 0.701562 0.022463 0.362538 11.00000 0.02804 0.01916 = 0.02859 0.00354 0.00538 -0.00093 O10 5 0.896793 0.036010 0.314778 11.00000 0.02963 0.02722 = 0.03356 -0.00021 0.00873 0.00486 O11 5 0.412631 0.114694 0.295023 11.00000 0.03020 0.02384 = 0.02608 -0.00914 -0.00046 -0.00399 O12 5 0.306755 0.253219 0.333709 11.00000 0.02432 0.03032 = 0.02859 -0.00606 0.00010 0.00281 N4 4 0.503141 0.260482 0.409453 11.00000 0.02245 0.01879 = 0.01818 0.00043 0.00035 0.00083 N5 4 0.568770 0.206985 0.340079 11.00000 0.02164 0.01935 = 0.01980 -0.00440 0.00356 -0.00124 N6 4 0.704902 0.170120 0.319955 11.00000 0.02792 0.01645 = 0.02267 -0.00215 0.00819 0.00105 C16 1 0.969260 0.563435 0.317188 11.00000 0.02173 0.01988 = 0.02062 0.00316 -0.00377 -0.00073 C17 1 0.860535 0.518862 0.344513 11.00000 0.02153 0.02050 = 0.01938 -0.00164 -0.00082 0.00087 AFIX 43 H17 2 0.830177 0.559887 0.367481 11.00000 -1.20000 AFIX 0 C18 1 0.795145 0.411741 0.337907 11.00000 0.02023 0.01834 = 0.01869 0.00258 -0.00124 0.00025 C19 1 0.841577 0.351437 0.302813 11.00000 0.02228 0.01697 = 0.01881 0.00024 0.00040 0.00050 C20 1 0.959945 0.397196 0.277419 11.00000 0.02759 0.02188 = 0.01932 -0.00168 0.00189 0.00192 AFIX 43 H20 2 0.996073 0.355600 0.255149 11.00000 -1.20000 AFIX 0 C21 1 1.024621 0.501357 0.284230 11.00000 0.02720 0.02505 = 0.02036 0.00549 0.00218 -0.00192 AFIX 43 H21 2 1.103865 0.529533 0.267071 11.00000 -1.20000 AFIX 0 C22 1 0.688042 0.373820 0.370672 11.00000 0.02324 0.02068 = 0.01466 -0.00306 -0.00003 0.00109 AFIX 43 H22 2 0.688846 0.416760 0.394474 11.00000 -1.20000 AFIX 0 C23 1 0.589887 0.286279 0.370940 11.00000 0.02503 0.01790 = 0.01431 0.00019 0.00257 0.00145 C24 1 0.415851 0.195778 0.322826 11.00000 0.03019 0.02024 = 0.01825 -0.00112 0.00080 -0.00693 C25 1 0.266528 0.113515 0.270879 11.00000 0.02980 0.03824 = 0.03827 -0.01282 -0.00818 -0.00207 AFIX 137 H25A 2 0.274520 0.057286 0.249934 11.00000 -1.50000 H25B 2 0.251263 0.185462 0.258354 11.00000 -1.50000 H25C 2 0.177267 0.097019 0.288398 11.00000 -1.50000 AFIX 0 C26 1 0.778089 0.071686 0.331326 11.00000 0.02565 0.02034 = 0.02467 -0.00242 0.00185 -0.00274 C27 1 0.772246 -0.081730 0.376380 11.00000 0.03789 0.02383 = 0.04524 0.00866 0.00536 0.00345 AFIX 137 H27A 2 0.769708 -0.135432 0.354475 11.00000 -1.50000 H27B 2 0.712749 -0.109990 0.399347 11.00000 -1.50000 H27C 2 0.881085 -0.068761 0.384483 11.00000 -1.50000 AFIX 0 C28 1 0.770535 0.241809 0.287623 11.00000 0.02779 0.01961 = 0.01893 -0.00195 0.00520 -0.00131 AFIX 13 H28 2 0.858112 0.199876 0.274843 11.00000 -1.20000 AFIX 0 C29 1 0.645459 0.259783 0.254658 11.00000 0.03711 0.02942 = 0.01571 -0.00499 0.00265 -0.01201 AFIX 43 H29 2 0.630637 0.202353 0.235770 11.00000 -1.20000 AFIX 0 C30 1 0.555699 0.349909 0.250424 11.00000 0.04089 0.03385 = 0.02754 0.00332 -0.00546 -0.00835 AFIX 93 H30A 2 0.566641 0.409325 0.268648 11.00000 -1.20000 H30B 2 0.481496 0.354011 0.229217 11.00000 -1.20000 AFIX 0 HKLF 4 REM 20190605d_a.res in P2(1)2(1)2(1) REM R1 = 0.0315 for 6070 Fo > 4sig(Fo) and 0.0367 for all 6356 data REM 455 parameters refined using 0 restraints END WGHT 0.0340 1.5656 REM Highest difference peak 0.299, deepest hole -0.301, 1-sigma level 0.053 Q1 1 0.4786 0.0608 0.3020 11.00000 0.05 0.30 Q2 1 -0.0450 0.1253 0.3954 11.00000 0.05 0.20 Q3 1 -0.0180 0.1069 0.4542 11.00000 0.05 0.20 Q4 1 0.1864 0.1767 0.3173 11.00000 0.05 0.20 Q5 1 -0.0223 0.8037 0.4912 11.00000 0.05 0.19 Q6 1 0.7026 0.2543 0.2742 11.00000 0.05 0.19 Q7 1 0.9536 0.3744 0.2418 11.00000 0.05 0.19 Q8 1 0.4934 0.4172 0.2806 11.00000 0.05 0.19 ; _shelx_res_checksum 70452 _shelx_hkl_file ; 0 0 -2 14429.0 389.724 5 0 0 -3 7.96289 33.1601 5 0 0 -4 314852. 7752.09 5 0 0 -5 144.513 63.3936 5 0 0 -6 175616. 4391.69 5 0 0 -7 73.0311 76.9434 5 0 0 -8 378235. 9369.35 5 0 0 -9 85.7936 91.0931 5 0 0 9 6.15917 41.2075 7 0 0 10 32931.3 887.552 7 0 0 -10 33810.3 990.234 5 0 0 -11 54.6403 104.325 5 0 0 11 12.4548 43.1755 7 0 0 12 363681. 8982.44 7 0 0 -12 367105. 9129.02 5 0 0 -13 74.5509 121.262 5 0 0 13 39.5249 45.0348 7 0 0 -14 7293.31 389.460 5 0 0 14 7903.72 280.457 7 0 0 15 40.9307 45.0715 7 0 0 -15 53.1567 119.170 5 0 0 -16 111283. 3365.87 5 0 0 16 130761. 3179.35 7 0 0 -17-10.4397 134.327 5 0 0 -18 6506.00 416.227 5 0 0 -19 86.7639 139.315 5 0 0 -20 156899. 4212.50 3 0 0 -21 23.8959 118.878 3 0 0 -22 6199.86 419.144 3 0 0 -23 54.4161 139.950 3 0 0 -24 107511. 3098.62 3 0 0 -25 15.1727 137.333 3 0 0 -26 6449.52 468.399 3 0 0 -27 330.005 179.244 3 0 0 -28 339.870 180.552 3 0 0 -29 52.1656 157.394 3 0 0 -30 10479.7 638.469 3 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633.456 3 0 1 -20 14533.3 639.778 3 0 -1 -21 26037.5 960.879 3 0 1 -21 25283.7 948.212 3 0 1 -22 1853.11 267.971 5 0 1 -22 2085.73 252.962 3 0 -1 -22 1766.52 250.193 3 0 -1 -23 1219.51 221.026 3 0 1 -23 1000.64 204.888 3 0 1 -23 1282.66 251.183 5 0 -1 -24 4507.20 371.513 3 0 1 -24 3762.38 350.021 3 0 -1 -25 2135.62 281.456 3 0 1 -25 2018.68 281.531 3 0 1 -26 94.6212 147.152 3 0 1 -27 17987.1 848.958 3 0 1 -28 40371.1 1473.61 3 0 1 -29 11105.6 656.068 3 0 1 -30 14922.4 787.654 3 0 -1 31 6419.56 518.341 1 0 1 -31 7263.33 519.539 3 0 1 31 6967.64 534.510 1 0 1 -32 7961.52 539.137 3 0 1 -33 19957.2 914.210 3 0 1 -34 11051.8 619.267 3 0 1 -35 6224.14 444.674 3 0 1 -36 183.910 163.776 3 0 1 -37 4054.41 327.072 3 0 1 -38 4102.29 313.251 3 0 1 -39 6715.08 368.329 3 0 -1 -39 6421.72 362.966 3 0 -1 -40 82.4940 79.3250 3 0 1 -40-6.89605 81.5882 3 0 -2 0 69714.5 1803.62 6 0 -2 -1 310322. 7066.74 7 0 -2 -1 260762. 7072.49 6 0 -2 2 14980.4 448.750 7 0 -2 -2 13595.4 460.135 6 0 -2 -2 14198.5 415.946 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22395.7 929.673 3 0 2 -24 22266.3 916.773 3 0 2 -24 19080.8 938.015 5 0 -2 -25 25963.1 1053.97 3 0 2 -25 27756.8 1063.34 3 0 -2 -26 101654. 2922.26 3 0 2 -26 100934. 2907.82 3 0 -2 -27 98.8647 166.766 3 0 2 -27 112.643 153.072 3 0 2 -28 13477.2 722.141 3 0 -2 -28 13884.8 732.738 3 0 -2 -29 71429.7 2273.34 3 0 2 -29 71099.9 2266.31 3 0 -2 -30 51.7214 165.517 3 0 2 30-19.3359 131.264 1 0 -2 30 56.5152 141.384 1 0 2 -30 84.3769 164.985 3 0 2 -31 1067.35 247.075 3 0 -2 -31 1360.14 268.878 3 0 -2 31 982.813 227.637 1 0 2 31 1171.88 243.507 1 0 2 -32 259.538 179.919 3 0 -2 -32 231.205 185.696 3 0 2 -33 33576.9 1276.76 3 0 -2 -33 35112.3 1295.46 3 0 -2 -34 11699.1 635.702 3 0 2 -34 11752.3 634.811 3 0 2 -35 5284.50 398.922 3 0 -2 -35 5075.16 390.515 3 0 -2 -36 3497.47 316.386 3 0 2 -36 3639.09 319.671 3 0 -2 36 2649.26 245.918 9 0 -2 -37 28259.7 1016.14 3 0 2 -37 28535.9 1017.09 3 0 2 -38 3860.98 291.042 3 0 -2 -38 4186.57 299.655 3 0 -2 -39 163.081 104.569 3 0 2 -39 241.542 109.271 3 0 2 -40 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1 0 3 -30 17870.2 826.707 3 0 3 -31 6639.82 479.157 3 0 -3 -31 6709.22 485.813 3 0 3 -32 1770.70 269.808 3 0 -3 -32 2354.92 309.574 3 0 -3 -33 37968.9 1365.26 3 0 3 -33 38780.3 1365.40 3 0 -3 -34 11596.9 609.850 3 0 3 -34 11672.1 608.642 3 0 -3 -35 15585.7 706.391 3 0 3 -35 15764.3 703.294 3 0 3 -36 1066.98 190.423 3 0 -3 -36 1236.11 201.329 3 0 -3 36 1066.59 178.258 9 0 3 -37 4322.84 308.585 3 0 -3 -37 4035.27 303.692 3 0 -3 37 3836.00 264.703 9 0 3 -38 198.777 107.555 3 0 -3 -38 189.982 106.580 3 0 -3 -39 963.150 134.475 3 0 3 -39 965.898 133.324 3 0 -4 0 15814.0 558.116 7 0 -4 0 16632.1 572.969 6 0 -4 -1 2848.08 187.481 7 0 -4 1 2711.01 196.679 6 0 -4 -1 2991.23 196.386 6 0 -4 1 2815.71 191.869 7 0 -4 2 6567.80 358.051 6 0 -4 -2 9509.59 354.174 7 0 -4 -3 6216.44 277.633 7 0 4 4 1284.45 68.5588 1 0 -4 -4 1253.38 118.427 7 0 -4 5 69309.2 1949.86 7 0 4 5 71551.7 1803.53 1 0 -4 6 238639. 6062.59 7 0 -4 7 1517.21 164.597 7 0 -4 8 62579.3 1781.47 7 0 -4 9 39093.5 1202.91 7 0 -4 10 13167.5 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408.922 164.140 10 -2 -11 10 24914.0 993.788 14 2 -11 -10 26452.6 1120.56 4 -2 11 -10 24972.9 1028.26 10 -2 -11 11 2183.94 326.553 8 -2 -11 11 1689.13 248.044 14 -2 11 -11 2011.18 269.635 10 2 -11 -11 1699.72 308.510 4 -2 -11 12 3501.91 397.584 8 2 -11 -12 3343.64 367.956 4 -2 11 -12 3530.31 345.843 10 -2 -11 12 2782.71 302.522 14 -2 -11 13 8408.74 517.699 14 2 -11 -13 9160.33 593.023 4 -2 11 -13 9757.62 562.803 10 -2 -11 14 17494.8 779.891 14 2 -11 -14 18433.0 872.447 4 -2 11 -14 17004.7 799.625 10 -2 -11 15 3113.47 314.418 14 -2 -11 15 3879.66 396.483 8 2 -11 -15 3384.90 363.899 4 -2 11 -15 3676.63 347.900 10 -2 -11 16 8792.17 516.574 14 -2 -11 16 10453.6 631.086 8 2 -11 -16 10752.1 614.995 4 -2 11 -16 10130.6 572.136 10 -2 -11 17 1499.75 229.464 14 2 -11 -17 1654.12 273.979 4 -2 11 -17 1799.56 257.334 10 -2 -11 17 2159.70 302.782 8 -2 -11 18 2218.55 262.565 14 -2 11 -18 2697.46 289.551 10 -2 -11 18 2346.25 308.317 8 2 -11 -18 2301.12 305.470 4 -2 -11 19 5460.67 381.518 14 -2 11 -19 5856.77 415.904 10 2 -11 -19 6747.80 452.037 4 -2 -11 19 6500.85 455.921 8 -2 -11 20 999.529 186.477 14 -2 11 -20 1072.66 203.733 10 -2 -11 20 985.143 207.872 8 -2 11 -21 5415.37 370.315 10 -2 -11 21 5230.33 347.694 14 -2 -11 21 6013.50 406.140 8 -2 -11 22 9636.97 462.464 14 -2 11 -22 10207.7 510.455 10 -2 -11 23 4965.50 307.741 14 -2 11 -23 6111.99 361.700 10 -2 -11 24 6834.46 345.132 14 -2 11 -24 8314.91 413.911 10 -2 11 -25 2322.19 206.647 10 -2 11 -26 8693.89 385.721 10 2 12 -23 5741.06 290.445 10 2 12 -22 59.2309 85.9853 10 2 12 -21 27469.2 926.955 10 2 12 -20 1490.20 195.944 10 2 12 -19 6650.71 398.863 10 2 12 -18 33468.8 1155.64 10 -2 -12 -17 5211.24 371.711 4 2 12 -17 5965.60 394.583 10 -2 -12 -16 3979.42 338.176 4 2 12 -16 3444.57 320.054 10 2 12 -15 3002.25 309.310 10 -2 -12 -15 3282.14 326.797 4 -2 -12 -14 38464.9 1321.47 4 2 12 -14 35039.6 1290.44 10 2 12 -13 16165.2 777.752 10 -2 -12 -13 19421.2 828.014 4 2 12 -12 2696.55 314.191 10 -2 -12 -12 3741.29 358.199 4 2 12 -11 16257.0 777.838 10 -2 -12 -11 17556.1 802.646 4 2 12 -10 4196.35 382.843 10 -2 -12 -10 5668.87 430.055 4 2 12 -9 2648.05 308.095 10 -2 -12 -9 3530.56 362.011 4 2 12 -8 3470.55 348.250 10 -2 -12 -8 4354.17 387.252 4 -2 -12 -7 1263.80 253.680 4 2 12 -7 991.941 217.291 10 2 12 -6 68353.8 2163.94 10 -2 -12 -6 72937.5 2249.70 4 -2 -12 -5 24457.7 1031.55 4 2 -12 5 24236.7 1036.13 4 2 12 -5 23652.4 970.408 10 2 12 -4 6527.92 447.938 10 -2 -12 -4 7884.69 531.784 4 2 -12 4 7687.66 525.728 4 2 -12 3 5084.24 433.875 4 2 12 -3 4411.50 365.022 10 -2 -12 -3 5660.67 449.126 4 -2 -12 -2 21730.6 961.502 4 2 -12 2 21154.5 962.369 4 -2 -12 -1 17265.6 833.732 4 2 -12 1 16733.3 832.540 4 -2 -12 0 17439.4 847.397 4 2 -12 0 17889.2 853.632 4 2 -12 -1 16471.5 821.148 4 -2 -12 1 17498.3 837.675 4 2 -12 -2 20129.9 928.871 4 -2 -12 2 21322.1 953.843 4 -2 -12 3 5449.72 455.423 4 2 -12 -3 5551.43 445.311 4 -2 -12 3 4941.30 413.583 8 -2 -12 4 8526.15 563.577 4 2 -12 -4 9232.41 577.621 4 -2 -12 4 8977.41 559.026 8 -2 -12 5 23979.4 1010.95 8 2 -12 -5 23574.9 1016.80 4 -2 -12 5 23628.4 1023.70 4 -2 -12 6 70572.7 2253.85 4 -2 -12 6 71943.4 2253.08 8 2 -12 -6 70634.3 2244.52 4 -2 -12 7 446.822 199.652 8 2 -12 -7 483.494 194.451 4 -2 -12 8 3059.20 352.878 8 2 -12 -8 3607.56 362.151 4 -2 -12 9 4185.76 391.994 8 2 -12 -9 4038.38 379.276 4 -2 -12 10 4719.06 410.072 8 -2 12 -10 3899.05 316.390 10 2 -12 -10 4680.81 405.285 4 -2 12 -11 12200.5 585.585 10 -2 -12 11 13500.6 706.153 8 2 -12 -11 13776.5 692.203 4 -2 -12 12 3164.90 343.615 8 2 -12 -12 2928.12 321.488 4 -2 12 -12 2545.93 258.386 10 -2 12 -13 14847.2 663.148 10 2 -12 -13 15330.7 745.157 4 2 -12 -14 37711.1 1323.29 4 -2 12 -14 36453.9 1229.04 10 2 -12 -15 3306.89 318.837 4 -2 12 -15 3248.58 279.843 10 -2 12 -16 3048.40 268.590 10 2 -12 -16 2760.07 300.178 4 -2 -12 16 3385.08 321.632 8 -2 12 -17 5051.15 332.446 10 2 -12 -17 4976.63 362.737 4 -2 12 -18 29751.7 1010.32 10 -2 12 -19 7288.64 386.874 10 -2 12 -20 1428.33 176.073 10 -2 12 -21 24118.1 810.629 10 -2 12 -22 435.137 99.8349 10 2 13 -18 2084.07 173.218 10 2 -13 17 579.776 114.297 4 2 13 -17 943.319 136.210 10 2 13 -16 6841.90 330.378 10 2 -13 16 3646.12 259.258 4 2 13 -15 2825.35 231.072 10 2 -13 15 2204.63 210.553 4 -2 -13 -14 13324.9 551.262 4 2 13 -14 13163.6 537.008 10 -2 -13 -13 2916.80 263.053 4 2 13 -13 3047.40 250.383 10 2 -13 13 2894.92 255.456 4 -2 -13 -12 6410.80 394.015 4 2 13 -12 6246.52 365.744 10 2 -13 12 6091.84 379.740 4 2 13 -11 12650.9 572.258 10 -2 -13 -11 14769.8 635.565 4 2 -13 11 13331.2 606.485 4 -2 -13 -10 3578.29 307.838 4 2 13 -10 2863.83 262.064 10 2 -13 10 3490.61 297.726 4 2 13 -9 6707.11 400.386 10 -2 -13 -9 7292.72 441.312 4 2 -13 9 7919.97 455.885 4 2 -13 8 13063.0 615.196 4 2 13 -8 11717.5 545.766 10 -2 -13 -8 12826.4 615.081 4 -2 -13 -7 23146.0 876.714 4 2 -13 7 21096.2 847.459 4 -2 -13 -6 10430.3 559.106 4 2 -13 6 10450.8 554.926 4 -2 -13 -5 19109.4 818.507 4 2 -13 5 19901.7 827.758 4 -2 -13 -4 1881.53 253.118 4 2 -13 4 1791.00 248.593 4 -2 -13 -3 6755.15 442.783 4 2 -13 3 7027.08 451.168 4 -2 -13 -2 6379.36 430.166 4 2 -13 2 6650.65 438.094 4 -2 -13 -1 9289.99 532.164 4 2 -13 1 9086.88 524.092 4 -2 -13 0 12668.4 639.936 4 2 -13 0 12905.4 640.521 4 2 -13 -1 8840.62 518.732 4 -2 -13 1 10120.5 548.919 4 -2 -13 2 7342.33 463.558 4 2 -13 -2 6841.12 451.120 4 2 -13 -3 5369.28 401.603 4 -2 -13 3 5893.65 413.337 4 2 -13 -4 2945.09 293.878 4 -2 -13 4 2896.48 299.405 4 2 -13 -5 20496.9 841.404 4 -2 -13 5 19323.4 821.751 4 2 -13 -6 8651.77 500.382 4 -2 -13 6 8931.01 501.589 4 2 -13 -7 21572.1 853.600 4 -2 -13 7 19136.9 814.587 4 2 -13 -8 12559.7 608.344 4 -2 -13 8 11699.3 583.735 4 2 -13 -9 5946.44 393.270 4 -2 -13 9 4817.83 357.341 4 -2 -13 10 2258.28 256.529 4 2 -13 -10 2765.47 276.873 4 2 -13 -11 12565.7 574.018 4 -2 -13 11 9256.59 502.035 4 2 -13 -12 8216.38 443.761 4 -2 -13 12 5934.26 377.146 4 2 -13 -13 2326.47 242.653 4 -2 -13 13 1243.57 187.396 4 -2 -13 14 7403.16 418.417 4 2 -13 -14 13200.3 528.897 4 2 -13 -15 2874.58 238.338 4 -2 -13 15 1090.47 164.890 4 -2 -13 16 2235.89 197.163 4 2 -14 10 263.527 88.0656 4 -2 -14 -9 1163.88 149.397 4 2 -14 9 848.656 128.465 4 -2 -14 -8 486.211 121.494 4 2 -14 8 622.194 117.036 4 -2 -14 -7 13907.9 544.850 4 2 -14 7 13098.4 529.659 4 -2 -14 -6 2544.66 218.167 4 2 -14 6 2377.15 209.928 4 2 -14 5 6328.43 344.719 4 -2 -14 -5 5812.53 335.959 4 -2 -14 -4 6388.12 349.583 4 2 -14 4 6084.86 343.766 4 2 -14 3 544.671 133.131 4 -2 -14 -3 523.830 134.995 4 -2 -14 -2 4717.41 297.285 4 2 -14 2 4671.01 301.181 4 2 -14 1 30420.4 998.722 4 -2 -14 -1 29154.5 979.665 4 2 -14 0 367.980 112.614 4 -2 -14 0 472.144 115.974 4 2 -14 -1 31064.7 1009.68 4 -2 -14 1 29223.5 985.885 4 2 -14 -2 4143.79 280.837 4 -2 -14 2 3579.34 263.324 4 -2 -14 3 406.404 115.276 4 2 -14 -3 395.682 117.732 4 2 -14 -4 6789.56 360.135 4 -2 -14 4 5225.16 316.334 4 2 -14 -5 5845.69 327.863 4 -2 -14 5 4516.08 290.316 4 2 -14 -6 3245.67 245.121 4 -2 -14 6 2341.70 204.617 4 2 -14 -7 14080.6 526.794 4 -2 -14 7 9553.20 443.433 4 -2 -14 8 337.158 102.574 4 2 -14 -8 617.898 129.846 4 2 -14 -9 1165.49 151.997 4 2 -14 -10 745.457 126.352 4 3 0 0 16.4515 68.7191 1 3 0 -1 115576. 3123.93 1 3 0 1 125019. 3135.43 1 3 0 2 74622.7 2001.42 1 3 0 -2 72553.9 1994.24 1 3 0 3 2406.12 185.356 1 3 0 -3 2303.97 187.644 1 3 0 -4 18384.7 668.568 1 3 0 4 19457.5 661.119 1 3 0 5 28318.7 901.401 1 3 0 6 33929.8 1047.66 1 3 0 7 18299.7 659.626 1 3 0 8 21091.9 740.999 1 3 0 9 14223.5 569.298 1 3 0 10 91073.2 2503.92 1 3 0 11 7874.18 412.391 1 3 0 12 78080.0 2217.25 1 3 0 13 18419.7 729.576 1 3 0 14 5371.10 355.684 1 3 0 15 199461. 5257.46 1 -3 0 -16 2201.95 247.078 3 3 0 16 2395.67 252.718 1 -3 0 -17 18872.5 793.671 3 3 0 17 19153.0 805.010 1 3 0 18 16630.8 757.906 1 -3 0 -18 18285.2 777.465 10 -3 0 -18 17063.6 758.886 3 3 0 19 91139.1 2682.01 9 3 0 19 93615.6 2755.64 1 -3 0 -19 96115.9 2750.85 10 -3 0 -19 95413.8 2749.85 3 3 0 -19 95822.5 2752.52 3 -3 0 -20 5460.05 411.457 3 3 0 20 5515.93 413.263 1 -3 0 -20 5018.75 392.573 10 3 0 20 4821.81 368.855 9 3 0 -20 5563.89 412.928 3 -3 0 -21 68716.2 2148.89 3 3 0 21 71682.2 2191.20 1 -3 0 -21 68936.0 2132.93 10 3 0 21 66477.3 2079.05 9 3 0 -21 69498.4 2151.53 3 3 0 -22 61.5492 147.725 3 3 0 22 16.4930 123.781 1 -3 0 -22 125.748 159.068 3 3 0 22-26.0893 109.125 9 3 0 23 18882.4 891.560 1 3 0 23 19574.9 827.080 9 3 0 -23 18411.4 866.270 3 -3 0 -23 19265.5 880.671 3 -3 0 -24 166453. 4550.59 3 3 0 24 161504. 4561.83 1 3 0 -24 160509. 4516.06 3 -3 0 -25 25492.6 1098.90 3 3 0 25 27673.8 1149.48 1 3 0 -25 26528.0 1100.18 3 -3 0 -26 12412.2 701.525 3 3 0 26 11680.3 689.305 1 3 0 -26 10880.0 652.173 3 3 0 -27 53586.9 1834.84 3 -3 0 -27 56464.2 1871.72 3 3 0 27 50450.5 1846.46 1 3 0 -28 27643.9 1133.48 3 -3 0 -28 27226.6 1141.95 3 3 0 28 25118.9 1132.16 1 -3 0 -29 3499.56 376.755 3 3 0 -29 2754.36 340.900 3 3 0 29 3018.62 359.056 1 -3 0 -30 637.886 235.325 3 3 0 -30 489.238 209.528 3 3 0 -31 2025.04 299.857 3 -3 0 -31 2512.48 321.295 3 3 0 -32 59133.7 1936.02 3 -3 0 -32 60426.0 1967.96 3 3 0 -33 18111.1 826.815 3 -3 0 -33 19199.9 863.511 3 3 0 -34 91.8995 150.522 3 3 0 -35 743.756 182.741 3 3 0 -36 21642.5 826.411 3 3 0 -37 1858.44 207.849 3 3 0 -38 1008.14 150.187 3 3 0 -39 4940.97 258.425 3 3 1 -39 4906.44 249.554 3 3 1 -38 2705.44 213.562 3 3 1 -37 546.862 138.140 3 3 1 -36 23866.9 878.379 3 3 1 -35 9635.11 513.956 3 3 1 -34 14598.6 683.941 3 3 1 -33 8372.91 513.861 3 3 1 -32 4916.04 398.565 3 3 1 -31 7259.54 511.602 3 3 1 -30 9356.74 580.501 3 3 -1 30 8421.28 501.069 9 3 1 -29 3289.54 359.958 3 3 -1 29 2848.11 348.900 1 3 -1 29 2566.12 293.870 9 3 -1 28 4497.15 422.532 1 3 -1 28 3910.97 355.687 9 3 1 -28 3844.36 394.878 3 3 -1 27 757.556 214.977 1 3 1 -27 593.356 219.371 3 3 -1 27 761.543 191.923 9 3 -1 26 11206.6 669.775 1 3 -1 26 11558.2 626.646 9 3 1 -26 10613.4 639.480 3 3 -1 25 34893.0 1371.49 1 3 -1 25 37847.1 1339.81 9 3 1 -25 35030.2 1350.09 3 3 -1 24 29564.4 1211.67 1 3 -1 24 29928.4 1160.95 9 3 1 -24 31222.3 1204.10 3 3 1 -23 5959.64 457.905 3 3 -1 23 6039.99 460.761 1 3 -1 23 6077.11 441.817 9 3 -1 22 11383.1 613.052 9 3 1 -22 11165.5 627.027 3 3 -1 21 27446.9 1071.59 9 3 1 -21 28336.0 1097.16 3 3 -1 20 13218.1 661.179 9 3 1 -20 14286.3 691.126 3 -3 -1 -19 11967.0 625.287 3 3 -1 19 12377.3 617.723 9 3 1 -19 12406.4 629.503 3 -3 -1 -18 493.560 169.291 3 3 -1 18 520.486 150.652 9 -3 -1 -17 74648.2 2239.35 3 3 1 -17 78507.0 2219.60 5 3 -1 17 73050.7 2216.72 9 -3 -1 -16 4339.77 339.098 3 3 1 -16 4949.83 327.515 5 3 1 -15 12167.3 541.706 5 3 1 -14 15589.2 624.293 5 3 1 -13 20707.5 742.416 5 3 1 -12 40019.5 1213.36 5 3 1 -11 225297. 5725.96 5 3 1 -10 90777.9 2420.83 5 3 1 -9 15152.8 532.993 5 3 1 -8 151167. 3851.50 5 3 1 -7 74494.5 1959.85 5 3 -1 6 514.348 56.3696 6 3 1 -6 1712.34 121.102 5 3 1 -5 48455.9 536.715 5 3 -1 5 5718.73 238.047 6 3 1 -4 26067.6 705.247 5 3 1 -4 24283.5 827.569 1 3 1 -3 31048.5 983.452 1 3 1 -3 32422.7 843.889 5 3 1 -2 128408. 3191.49 5 3 1 -2 135158. 3369.15 1 3 1 -1 72763.9 1971.30 1 3 1 0 923.454 124.617 1 -3 -1 1 10325.1 310.454 6 3 1 1 76752.4 920.755 1 3 1 2 129902. 3373.79 1 3 1 3 30194.1 935.463 1 3 1 4 27868.4 884.247 1 -3 1 -5 46394.2 1217.47 5 3 1 5 50276.5 1384.14 1 -3 1 -6 2047.25 119.101 5 3 1 6 2066.64 180.757 1 -3 1 -7 77963.0 2029.90 5 3 1 7 80971.2 2174.88 1 -3 1 -8 130034. 3333.08 5 3 1 8 134120. 3470.86 1 -3 1 -9 21920.5 670.178 5 3 1 9 20945.6 759.188 1 -3 1 -10 91807.5 2348.82 5 3 1 10 84469.1 2446.51 1 3 1 11 217123. 5838.51 1 -3 1 -11 233880. 5747.63 5 -3 1 -12 38872.5 1149.20 5 3 1 12 37673.7 1231.29 1 -3 1 -13 22501.4 758.850 5 3 1 13 21630.2 823.671 1 -3 1 -14 16640.1 637.996 5 3 1 14 15851.0 679.669 1 -3 1 -15 13875.6 590.166 5 3 1 15 13332.8 618.519 1 -3 1 -16 2883.65 275.083 3 3 1 16 3429.27 295.170 1 3 1 17 72425.9 2150.83 1 -3 1 -17 70871.9 2164.39 10 -3 1 -17 70296.5 2124.16 3 3 1 18 297.726 136.017 1 -3 1 -18 394.348 146.032 3 -3 1 -18 246.010 149.584 10 -3 1 -19 12258.6 624.610 3 -3 1 -19 12023.1 633.951 10 3 -1 -19 11893.6 619.748 3 3 1 19 11725.2 621.902 1 -3 1 -20 11920.9 627.604 3 3 1 20 11605.3 633.617 1 -3 1 -20 12291.9 646.824 10 3 -1 -20 12030.4 629.626 3 -3 1 -21 24883.0 1013.77 3 3 1 21 24903.2 1031.42 1 -3 1 -21 24650.1 1022.89 10 3 -1 -21 24766.2 1008.78 3 -3 1 -22 9367.68 574.029 10 -3 1 -22 9809.22 586.423 3 3 1 22 11214.3 628.849 1 3 -1 -22 9275.82 566.167 3 -3 1 -23 5961.32 457.021 3 3 1 23 6433.74 477.781 1 -3 1 -23 6391.37 474.694 10 3 -1 -23 6064.87 461.997 3 3 1 24 27880.3 1162.91 1 3 -1 -24 27380.7 1124.33 3 -3 1 -24 27937.9 1123.67 10 -3 1 -24 28938.1 1158.26 3 3 1 25 37779.8 1410.59 1 -3 1 -25 35317.4 1367.92 3 -3 1 -25 34927.2 1326.82 10 -3 1 -26 10707.5 649.563 3 3 1 26 9642.29 630.066 1 -3 1 -27 359.776 191.274 3 3 1 27 599.485 204.014 1 -3 1 -28 4282.45 410.518 3 3 1 28 4336.95 424.730 1 -3 1 -29 4899.76 445.656 3 3 1 29 4941.58 456.726 1 -3 1 -30 7200.45 533.207 3 -3 1 -31 9300.74 596.065 3 -3 1 -32 3533.77 362.085 3 3 -1 -36 22727.5 849.048 3 3 -1 -37 344.233 127.971 3 3 -1 -38 2014.73 184.738 3 3 -1 -39 4068.16 225.306 3 3 2 -38 5023.62 272.699 3 3 2 -37 1057.90 164.232 3 3 2 -36 24632.2 878.259 3 3 2 -35 9606.56 497.191 3 3 2 -34 10236.0 542.801 3 3 2 -33 1132.81 217.228 3 3 -2 33 1186.70 181.423 9 3 -2 32 35712.6 1227.41 9 3 2 -32 36263.7 1305.50 3 3 2 -31 29699.2 1143.96 3 -3 -2 -31 29191.8 1168.10 3 3 -2 31 27968.0 1070.14 9 3 2 -30 2577.20 315.473 3 -3 -2 -30 3129.46 345.942 3 3 -2 30 2720.83 309.791 9 -3 -2 -29 8803.25 575.727 3 3 2 -29 8886.39 568.984 3 3 -2 29 8868.20 544.942 9 3 2 -28 6387.87 489.210 3 -3 -2 -28 7561.97 534.886 3 3 -2 28 7026.05 520.918 1 3 -2 28 6756.38 479.370 9 3 2 -27 19982.9 921.291 3 -3 -2 -27 19762.6 936.488 3 3 -2 27 18701.3 921.926 1 3 -2 27 20192.5 908.663 9 -3 -2 -26 7255.87 531.471 3 3 -2 26 6609.00 504.031 1 3 -2 26 6767.20 492.241 9 3 2 -26 7209.47 513.007 3 -3 -2 -25 21482.2 959.456 3 3 -2 25 19264.0 919.423 1 3 -2 25 18878.6 897.679 9 3 2 -25 20534.2 920.342 3 -3 -2 -24 41177.0 1506.25 3 3 -2 24 41606.6 1508.83 1 3 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2148.93 13 -3 -2 -16 74437.5 2184.17 3 3 2 -16 74487.2 2149.29 5 3 -2 16 74799.9 2175.44 1 3 -2 16 72869.0 2188.35 9 3 -2 15 57036.7 1722.44 1 3 2 -15 54793.5 1685.02 5 3 -2 14 10595.0 518.414 1 3 2 -14 10437.5 492.887 5 3 2 -13 215452. 5476.55 5 3 -2 13 208434. 5520.80 1 3 2 -12 135078. 3508.49 5 3 -2 12 129029. 3541.08 1 3 2 -11 30775.7 977.642 5 3 -2 11 29641.0 1004.73 1 3 2 -10 4778.89 276.190 5 3 -2 10 4123.60 280.040 1 3 2 -9 8786.62 380.298 5 3 -2 9 7313.88 383.317 1 3 -2 8 251726. 6400.76 1 3 -2 7 123709. 3258.60 1 3 -2 6 122027. 2965.71 1 3 -2 6 106546. 2831.43 6 3 -2 5 22251.9 688.910 6 3 -2 5 29180.3 825.668 1 3 -2 4 14174.6 466.089 1 3 -2 4 8157.62 316.038 6 3 -2 3 212169. 5330.29 1 3 2 -3 207382. 5342.93 1 3 -2 2 3198.22 207.706 1 3 2 -2 3577.87 223.781 1 3 2 -1 74897.3 1982.01 1 3 -2 1 71365.5 1964.96 1 3 -2 0 58280.3 775.336 1 3 2 0 60199.3 801.333 1 3 -2 -1 71725.3 1302.14 1 3 2 1 67722.4 1291.82 1 3 2 2 3099.21 208.851 1 3 -2 -2 3201.41 210.859 1 3 -2 -3 222226. 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790.207 213.858 11 -7 -5 -1 32111.6 1272.46 14 7 -5 1 30831.2 1236.48 12 -7 -5 -1 32738.1 1270.31 11 7 -5 0 58072.6 1962.12 12 -7 -5 0 63026.6 2030.29 14 -7 -5 0 59893.2 2008.71 11 -7 -5 1 28928.5 1209.99 14 7 -5 -1 30548.8 1200.73 12 -7 -5 1 31167.7 1246.32 11 -7 -5 2 247.434 194.596 14 7 -5 -2 82.5490 147.919 12 -7 -5 2 187.786 185.260 11 -7 -5 3 5504.59 451.803 14 7 -5 -3 5124.65 429.980 12 -7 -5 3 4968.94 456.135 11 -7 -5 4 35951.1 1379.48 14 7 -5 -4 35200.4 1334.52 12 -7 -5 4 37473.6 1438.47 11 -7 -5 5 470.683 202.782 14 7 -5 -5 401.983 182.318 12 -7 -5 5 665.510 231.875 11 -7 -5 6 14759.7 786.136 14 7 -5 -6 15208.1 763.700 12 -7 -5 6 16244.2 844.427 11 -7 -5 7 8630.31 566.372 14 7 -5 -7 8186.37 528.657 12 -7 -5 7 8384.98 594.474 11 -7 -5 8 11146.6 646.252 14 -7 -5 8 10302.6 670.890 11 -7 -5 9 12486.4 698.232 14 -7 -5 10 8266.51 553.771 14 -7 -5 11 1757.90 272.576 14 -7 -5 11 1405.94 278.327 11 -7 -5 12 36889.8 1370.88 14 -7 -5 12 37509.9 1447.14 11 -7 -5 12 36973.2 1384.73 2 -7 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5540.46 394.446 9 -7 -6 -16 168.913 148.775 13 7 -6 16 208.005 141.569 9 -7 -6 -15 22.7034 86.8271 2 -7 -6 -15 10249.5 492.663 13 -7 -6 -14 1718.29 251.647 2 -7 -6 -14 1830.06 263.004 13 -7 -6 -13 6432.61 441.442 13 -7 -6 -13 5382.17 418.976 2 -7 -6 -12 4285.31 374.165 13 -7 -6 -12 3819.52 376.521 2 -7 -6 -11 14518.0 711.591 13 -7 -6 -11 13073.7 708.946 2 -7 -6 -10 497.977 213.256 2 -7 -6 -10 609.751 206.448 13 -7 -6 -9 10432.7 643.369 2 -7 -6 -8 1971.03 311.100 2 -7 -6 -8 1508.24 292.854 14 -7 -6 -7 8387.36 574.537 14 -7 -6 -7 8451.99 588.370 2 -7 -6 -6 37777.3 1408.89 14 -7 -6 -6 35768.2 1435.24 2 -7 -6 -5 22669.0 1001.92 14 7 -6 5 21522.4 939.640 12 -7 -6 -5 23469.1 1054.46 2 -7 -6 -4 9375.63 598.793 14 7 -6 4 8093.04 530.955 12 -7 -6 -4 7718.55 497.538 11 -7 -6 -3 390.780 209.015 14 7 -6 3 332.951 161.984 12 -7 -6 -3 306.782 162.152 11 -7 -6 -2 1456.70 269.895 14 7 -6 2 788.473 200.349 12 -7 -6 -2 1137.68 240.733 11 -7 -6 -1 19130.7 893.832 14 7 -6 1 18108.1 839.606 12 -7 -6 -1 17130.2 830.020 11 -7 -6 0 8859.15 577.633 14 7 -6 0 7043.05 494.086 12 -7 -6 0 7867.05 535.713 11 -7 -6 1 20450.5 944.084 14 7 -6 -1 19330.3 880.817 12 -7 -6 1 19627.4 913.195 11 -7 -6 2 1307.10 275.587 14 7 -6 -2 1608.38 248.028 12 -7 -6 2 1668.53 283.498 11 -7 -6 3 1392.32 268.588 14 7 -6 -3 1362.38 245.754 12 -7 -6 3 1326.67 259.765 11 -7 -6 4 8720.32 576.613 14 7 -6 -4 8476.51 525.614 12 -7 -6 4 8655.43 582.471 11 -7 -6 5 23202.8 1007.53 14 7 -6 -5 21378.7 920.851 12 -7 -6 5 21363.7 1007.85 11 -7 -6 5 22723.6 1044.50 2 -7 -6 6 36294.7 1366.21 14 7 -6 -6 33369.6 1260.93 12 -7 -6 6 36210.6 1390.63 11 -7 -6 6 36008.8 1408.51 2 -7 -6 7 9088.16 573.932 14 -7 -6 7 8234.43 578.991 11 -7 -6 7 8150.50 587.339 2 -7 -6 8 1679.79 292.207 2 -7 -6 8 1926.12 293.136 14 -7 -6 8 1385.91 287.154 11 -7 -6 9 10200.1 614.224 14 -7 -6 9 9833.85 635.389 11 -7 -6 9 9406.42 619.337 2 -7 -6 10 952.786 234.316 2 -7 -6 10 981.514 238.191 14 -7 -6 11 12170.9 665.693 14 -7 -6 11 11955.5 667.099 2 -7 -6 12 3923.57 375.699 14 -7 -6 12 3966.18 402.795 11 -7 -6 12 3896.01 375.311 2 -7 -6 13 6549.21 466.662 14 -7 -6 13 6817.03 503.394 11 -7 -6 13 6061.07 439.737 2 -7 -6 14 1874.19 261.913 14 -7 -6 14 2067.75 265.350 2 -7 -6 15 9064.26 533.556 14 -7 -6 16 132.351 155.652 14 -7 -6 17 4390.06 352.160 14 -7 -6 18 10209.9 530.032 14 -7 -6 19 353.505 147.033 14 -7 -6 20 2119.39 230.220 14 -7 -6 21 3518.32 268.367 14 -7 -6 22 149.659 101.190 14 -7 -6 23 76.5907 92.8225 8 -7 -6 23 111.168 83.8838 14 -7 -6 24 134.806 78.1578 8 7 7 -20 6.73891 50.5754 10 7 7 -19 2511.48 225.561 10 7 7 -18 8308.47 437.383 10 -7 -7 -17 4762.87 330.854 13 7 7 -17 4214.57 323.485 10 -7 -7 -16 5784.99 380.599 13 7 7 -16 5620.59 386.567 10 -7 -7 -15 21300.5 666.539 13 7 7 -15 17742.3 642.134 10 -7 -7 -14-65.3475 91.1285 2 -7 -7 -14 8880.79 454.130 13 -7 -7 -13 7172.34 448.051 13 -7 -7 -13 5021.63 389.575 2 -7 -7 -12 20715.5 856.574 13 -7 -7 -12 18449.3 827.130 2 -7 -7 -11 1569.21 257.999 2 -7 -7 -11 1704.22 263.686 13 -7 -7 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6537.55 507.579 2 -7 -7 6 6031.56 467.370 14 -7 -7 6 5751.40 484.714 2 -7 -7 7 4534.79 409.514 14 -7 -7 7 5690.54 467.972 2 -7 -7 8 3433.31 353.320 14 -7 -7 8 3371.88 367.126 2 -7 -7 9 4387.18 388.088 14 -7 -7 9 4246.65 394.860 2 -7 -7 10 1078.55 240.001 2 -7 -7 10 1362.73 253.172 14 -7 -7 11 1260.72 240.186 2 -7 -7 11 1415.28 245.264 14 -7 -7 12 20601.4 882.010 14 -7 -7 12 20046.3 853.115 2 -7 -7 13 4721.53 381.591 14 -7 -7 13 4299.18 352.828 2 -7 -7 14 8658.28 510.707 14 -7 -7 14 7948.64 454.471 2 -7 -7 15 17732.1 768.849 14 -7 -7 16 4913.99 361.013 14 -7 -7 17 4186.53 322.284 14 -7 -7 18 10299.4 506.764 14 -7 -7 19 2951.32 260.299 14 -7 -7 20 9710.62 451.623 14 -7 -7 20 9986.25 486.670 8 -7 -7 21 1289.58 170.616 8 -7 -7 21 1274.72 159.124 14 -7 -7 22 1948.15 174.381 14 -7 -7 22 2241.38 193.814 8 7 -8 21 2313.71 164.174 12 7 -8 20 992.677 123.673 12 7 8 -19 4951.56 274.350 10 7 8 -18 13235.6 536.879 10 7 8 -17-35.6732 95.3735 10 -7 -8 -16 1954.33 224.819 13 7 8 -16 1546.95 207.187 10 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818.351 240.869 2 7 -8 1 524.996 149.910 12 7 -8 0 7153.03 420.639 12 -7 -8 0 7183.26 532.668 2 -7 -8 1 639.788 233.676 2 7 -8 -1 475.879 134.385 12 7 -8 -2 1523.64 189.138 12 -7 -8 2 8586.91 540.002 2 -7 -8 3 1307.53 266.589 2 7 -8 -3-28.4593 64.3988 12 -7 -8 4 6955.77 479.399 14 -7 -8 4 6487.14 496.930 2 -7 -8 5 3045.79 324.648 14 -7 -8 5 2626.62 333.663 2 -7 -8 6 1306.60 242.870 14 -7 -8 6 1624.28 286.068 2 -7 -8 7 3208.70 330.282 14 -7 -8 7 3166.26 345.346 2 -7 -8 8 4254.18 367.047 14 -7 -8 8 4006.05 367.728 2 -7 -8 9 2516.43 288.991 14 -7 -8 9 2167.60 284.047 2 -7 -8 10 644.015 195.704 14 -7 -8 10 528.151 183.918 2 -7 -8 11 8862.24 516.231 14 -7 -8 11 9018.44 504.510 2 -7 -8 12 3450.00 302.270 2 -7 -8 12 4148.01 339.249 14 -7 -8 13 7841.38 431.867 2 -7 -8 13 8679.01 480.927 14 -7 -8 14 3427.63 299.418 14 -7 -8 15 5633.15 365.091 14 -7 -8 16 2067.41 224.759 14 -7 -8 16 2217.19 245.395 8 -7 -8 17 134.934 117.457 8 -7 -8 17 54.2492 113.936 14 -7 -8 18 15624.3 612.925 14 -7 -8 18 16035.6 648.118 8 -7 -8 19 8108.97 384.877 14 -7 -8 19 8568.04 413.200 8 -7 -8 20 641.904 123.719 8 -7 -8 20 562.094 113.915 14 7 9 -17 2414.57 187.328 10 7 -9 16 389.765 84.9860 12 7 9 -16 277.025 101.141 10 7 -9 15 4502.36 250.331 12 7 9 -15 4414.40 288.680 10 -7 -9 -14 503.663 143.023 13 7 -9 14 427.505 100.147 12 7 9 -14 266.238 122.105 10 7 -9 13 6755.29 351.223 12 7 9 -13 7961.20 431.194 10 -7 -9 -12 4141.57 301.777 13 7 -9 12 3091.82 225.855 12 -7 -9 -11 3169.97 273.898 13 7 -9 11 2457.96 208.825 12 -7 -9 -10 2738.30 266.787 13 7 -9 10 2088.50 196.537 12 -7 -9 -9 147.839 133.747 2 -7 -9 -9 120.531 138.823 13 7 -9 9 109.387 90.7760 12 -7 -9 -8 19059.5 784.823 2 -7 -9 -8 21021.7 794.689 13 -7 -9 -7 13982.9 650.923 2 -7 -9 -7 15340.4 649.183 13 -7 -9 -6-11.6513 131.827 14 -7 -9 -6 190.076 159.639 2 -7 -9 -6 132.222 152.255 13 7 -9 6 7.93748 61.3547 12 -7 -9 -5 9903.99 515.397 2 -7 -9 -5 9590.68 462.615 14 -7 -9 -5 10641.6 488.798 13 -7 -9 -4 2833.36 280.627 14 -7 -9 -4 3362.17 326.845 2 -7 -9 -3 4489.62 332.457 14 7 -9 3 7.46420 42.5472 12 -7 -9 -2 1255.82 212.420 14 7 -9 2 7.14559 30.9690 12 -7 -9 -1 2033.80 259.549 14 -7 -9 -1 2362.98 302.818 2 -7 -9 0 44863.8 1457.85 14 -7 -9 0 42108.4 1504.19 2 -7 -9 1 3563.17 304.416 14 -7 -9 1 3585.68 345.226 2 -7 -9 2 984.422 207.960 14 -7 -9 2 1048.60 238.933 2 -7 -9 3 3677.85 324.905 14 -7 -9 3 3731.92 350.390 2 -7 -9 4 2490.23 268.230 8 -7 -9 4 4254.34 371.973 2 -7 -9 5 12068.2 623.839 2 -7 -9 5 11066.5 552.228 8 -7 -9 6 57.4679 127.449 8 -7 -9 6 242.489 168.839 2 -7 -9 7 12418.1 612.969 2 -7 -9 7 11668.4 572.234 8 -7 -9 8 17853.4 753.400 2 -7 -9 8 17309.2 735.897 8 -7 -9 9 171.928 133.994 8 -7 -9 9 156.968 140.554 2 -7 -9 10 2197.53 244.545 14 -7 -9 10 2114.33 244.888 8 -7 -9 11 3389.97 283.732 14 -7 -9 11 3350.54 292.112 8 -7 -9 12 3946.62 293.852 14 -7 -9 12 3514.93 293.983 8 -7 -9 13 8912.14 448.250 14 -7 -9 13 9385.33 470.895 8 -7 -9 14 386.242 127.214 14 -7 -9 15 3748.05 261.717 14 -7 -9 16 327.743 108.845 14 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1 5 6137.15 464.854 12 8 1 6 15789.1 776.353 12 8 1 7 3955.83 368.808 12 -8 -1 7 3975.00 407.924 11 8 1 8 1454.02 246.154 12 -8 -1 8 1219.86 264.930 11 8 1 9 4356.16 375.852 12 -8 -1 9 4531.08 440.956 11 8 1 10 1087.16 219.107 12 -8 -1 10 1109.11 255.443 11 8 1 11 4641.24 380.035 12 -8 -1 11 5510.63 462.404 11 8 1 12 1106.54 208.672 12 -8 -1 12 1385.37 258.002 11 8 1 13 266.561 139.948 12 -8 -1 13 257.238 172.211 11 8 1 14 11732.2 578.890 12 -8 -1 14 13548.3 705.653 11 -8 -1 15 3878.48 368.501 11 -8 -1 16 8538.74 533.548 11 -8 -1 17 7683.79 489.774 11 -8 -1 18 3437.87 314.932 11 -8 -1 19 4232.06 328.544 11 8 -1 -19 4003.57 329.863 3 -8 -1 20 3362.17 282.835 11 8 -1 -20 3802.62 308.718 3 -8 -1 21 1198.14 171.097 11 8 -1 -21 1268.98 192.830 3 8 -1 -22 28026.4 964.982 3 8 -1 -23 5441.03 323.969 3 8 -1 -24 880.596 144.130 3 8 -1 -25 6645.49 321.927 3 8 -1 -26 1376.37 132.467 3 8 2 -25 1940.39 163.822 3 8 2 -24 1492.03 160.954 3 8 2 -23 1073.27 158.269 3 8 -2 22 14984.4 560.181 12 8 2 -22 16480.1 638.440 3 8 -2 21 2082.72 197.949 12 8 2 -21 2292.17 234.775 3 8 -2 20 8608.98 433.052 12 8 2 -20 9138.71 478.343 3 8 -2 19 1467.46 194.229 12 -8 2 19 1359.87 179.026 11 8 2 -19 1716.63 223.204 3 8 -2 18 5640.87 367.515 12 -8 2 18 5442.08 357.875 11 8 2 -18 5362.62 383.741 3 8 -2 17 70.6653 124.067 12 -8 2 17 91.9576 123.850 11 8 -2 16 730.157 178.584 12 -8 2 16 558.747 172.321 11 8 -2 15 5029.18 379.627 12 -8 2 15 4543.45 376.361 11 8 -2 14 2680.05 292.367 12 -8 2 14 3176.90 325.562 11 8 -2 13 9228.62 550.061 12 -8 2 13 9693.19 577.818 11 8 -2 12 1054.75 227.136 12 -8 2 12 1333.07 251.468 11 8 -2 11 12417.7 666.989 12 8 -2 10 12853.6 690.316 12 8 -2 9 18606.2 866.964 12 -8 -2 -9 18262.7 783.116 11 8 -2 8 3904.82 370.262 12 -8 -2 -8 3535.29 337.204 11 8 -2 7 9091.35 580.550 12 -8 -2 -7 9790.86 564.667 11 8 -2 6 54272.5 1827.89 12 -8 -2 -6 53517.5 1783.86 11 8 -2 5 1016.84 235.476 12 -8 -2 -5 1150.02 241.786 11 -8 -2 -4 13564.2 688.816 14 8 -2 4 11898.7 689.812 12 -8 -2 -4 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257.972 12 8 -6 18 13554.1 539.309 12 8 -6 17 2202.46 203.430 12 8 -6 16 7891.03 358.305 12 8 6 -16 49.3492 57.8150 10 8 -6 15 314.951 122.397 12 8 6 -15 300.691 115.210 10 -8 -6 -14 21.6477 32.6807 2 -8 -6 -14 553.257 132.477 13 -8 -6 -13 2509.58 223.489 13 -8 6 13 2026.37 195.435 11 -8 -6 -12 8800.04 427.692 13 -8 -6 -12 6862.06 418.420 2 -8 -6 -11 1576.46 225.294 2 -8 -6 -11 1589.22 212.081 13 -8 -6 -10 16696.2 673.706 13 8 -6 10 14710.4 680.697 12 -8 -6 -10 15469.0 702.501 2 -8 -6 -9 2819.59 265.965 13 8 -6 9 2586.45 270.042 12 -8 -6 -9 2423.86 283.214 2 -8 -6 -8 9195.74 493.662 13 8 -6 8 8957.41 506.190 12 -8 -6 -8 9277.97 551.341 2 -8 -6 -7 888.657 223.524 2 -8 -6 -7 807.039 186.164 13 8 -6 7 786.747 186.425 12 -8 -6 -6 1391.24 256.074 2 -8 -6 -6 1575.46 254.394 14 -8 -6 -6 1486.64 230.238 13 8 -6 6 1555.63 228.310 12 -8 -6 -5 981.800 236.080 2 -8 -6 -5 937.695 220.040 14 8 -6 5 792.144 181.630 12 -8 -6 -4 8318.87 515.500 14 8 -6 4 7815.61 478.843 12 -8 -6 -4 7915.97 534.770 2 -8 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10541.9 584.969 11 -8 -6 8 10494.6 587.815 2 -8 -6 9 2079.80 255.719 14 -8 -6 9 1710.23 250.638 2 -8 -6 9 2461.82 289.923 11 -8 -6 10 13168.0 627.952 14 -8 -6 10 14303.3 656.861 2 -8 -6 11 1594.62 224.412 2 -8 -6 11 1285.93 199.912 14 -8 -6 12 7669.98 429.495 14 -8 -6 12 7750.47 434.436 2 -8 -6 13 3476.50 275.051 14 -8 -6 13 3027.46 259.152 2 -8 -6 14 406.029 137.320 14 -8 -6 15 304.939 125.786 14 -8 -6 16 6850.91 351.050 14 -8 -6 17 1852.05 177.998 14 -8 -6 18 10371.2 407.179 14 -8 -6 20 861.949 119.242 8 8 -7 15 1025.85 140.537 12 8 7 -15 558.214 112.240 10 8 -7 14 3937.69 256.742 12 8 7 -14 2877.09 239.378 10 -8 -7 -13 7694.99 324.577 13 8 -7 13 7555.27 340.919 12 -8 -7 -12 866.870 155.157 13 8 -7 12 786.796 143.420 12 -8 -7 -11 13570.2 544.432 13 8 -7 11 12368.5 542.430 12 -8 -7 -10 14149.6 578.187 13 8 -7 10 12355.5 560.536 12 -8 -7 -10 12741.7 583.730 2 -8 -7 -9 6735.62 389.197 13 8 -7 9 6212.90 373.234 12 -8 -7 -9 6214.35 404.405 2 -8 -7 -8 8992.87 457.269 13 8 -7 8 7556.93 426.726 12 -8 -7 -8 8212.05 477.215 2 -8 -7 -7 24205.0 881.454 13 8 -7 7 22343.4 861.880 12 -8 -7 -7 24250.8 938.615 2 -8 -7 -6 10371.3 521.192 13 8 -7 6 10693.3 518.359 12 -8 -7 -6 10196.2 566.348 2 -8 -7 -5 8572.13 492.634 14 -8 -7 -5 8150.21 459.819 13 8 -7 5 7786.99 437.678 12 -8 -7 -5 7831.19 498.442 2 -8 -7 -4 1950.91 259.861 14 8 -7 4 1922.57 220.835 12 -8 -7 -4 2047.91 270.196 2 -8 -7 -3 1007.09 213.507 14 8 -7 3 632.883 156.405 12 -8 -7 -2 20270.6 822.663 14 8 -7 2 17360.1 731.150 12 -8 -7 -1 838.586 225.692 2 -8 -7 -1 915.894 210.132 14 8 -7 1 789.003 162.337 12 -8 -7 0 3216.93 310.263 14 8 -7 0 2530.43 249.759 12 -8 -7 0 2867.62 328.339 2 -8 -7 1 478.742 204.453 2 -8 -7 1 614.679 190.440 14 8 -7 -1 489.683 139.976 12 -8 -7 2 18747.4 802.891 14 -8 -7 2 19097.2 850.115 2 -8 -7 3 670.568 196.764 2 -8 -7 3 676.059 185.776 14 -8 -7 4 1860.56 244.177 14 -8 -7 4 2168.53 283.759 2 -8 -7 5 6780.24 433.488 14 -8 -7 5 7474.65 479.314 2 -8 -7 6 11107.3 566.173 14 -8 -7 6 11994.9 607.167 2 -8 -7 7 23288.5 904.937 14 -8 -7 7 24604.6 946.808 2 -8 -7 8 7891.52 448.509 14 -8 -7 8 7529.85 455.830 2 -8 -7 9 6180.15 383.131 14 -8 -7 9 6321.92 401.884 2 -8 -7 10 13010.8 583.146 14 -8 -7 10 12789.2 581.155 2 -8 -7 11 12659.7 552.097 14 -8 -7 11 11211.3 520.793 2 -8 -7 12 820.489 158.129 14 -8 -7 12 646.261 135.239 2 -8 -7 13 7116.13 374.337 14 -8 -7 14 3050.15 234.734 14 -8 -7 15 733.074 131.238 14 -8 -7 16 1199.82 139.953 14 -8 -7 17 10388.0 447.086 8 -8 -7 18 634.054 109.296 8 8 -8 13 1741.53 147.633 12 8 8 -13 1306.60 153.433 10 -8 -8 -12 2388.15 190.617 13 8 -8 12 2310.33 177.559 12 8 8 -12 1996.41 195.975 10 8 -8 11 7500.88 353.449 12 8 8 -11 7510.26 392.359 10 -8 -8 -10 6112.93 341.684 2 8 -8 10 6639.21 330.331 12 8 8 -10 6510.25 370.401 10 -8 -8 -9 14210.0 599.597 2 8 -8 9 14698.0 571.736 12 -8 -8 -8 9477.25 468.659 2 8 -8 8 8667.92 411.179 12 -8 -8 -7 304.002 131.919 2 -8 -8 -7 310.219 132.922 13 8 -8 7 281.462 93.1369 12 -8 -8 -6 3276.60 262.826 13 8 -8 6 2516.85 210.366 12 -8 -8 -6 2941.84 279.848 2 -8 -8 -5 756.769 175.387 2 -8 -8 -5 611.960 150.265 13 8 -8 5 690.287 127.635 12 -8 -8 -4 7850.29 413.015 13 -8 -8 -4 7153.94 433.086 2 -8 -8 -3 3097.68 266.358 13 8 -8 3 2161.79 195.128 12 8 -8 2-21.1975 59.1103 12 -8 -8 -1 11439.6 547.448 14 -8 -8 -1 10431.6 556.286 2 -8 -8 0 6336.96 390.924 14 -8 -8 0 6137.46 411.064 2 -8 -8 1 11170.3 469.303 14 -8 -8 1 12456.8 528.513 2 -8 -8 2 2006.76 230.228 14 -8 -8 2 2527.25 273.603 2 -8 -8 3 2596.52 253.010 14 -8 -8 3 2639.48 273.987 2 -8 -8 4 8962.25 470.656 14 -8 -8 4 9125.22 495.569 2 -8 -8 5 630.274 159.694 14 -8 -8 5 583.831 166.611 2 -8 -8 6 3092.40 264.849 14 -8 -8 6 2941.23 277.976 2 -8 -8 7 319.696 134.780 14 -8 -8 7 301.196 136.521 2 -8 -8 8 9674.32 478.414 2 -8 -8 8 11061.4 494.440 14 -8 -8 9 14940.0 614.391 2 -8 -8 9 17747.7 655.164 14 -8 -8 10 6736.29 353.660 14 -8 -8 10 5391.68 313.703 2 -8 -8 11 6414.32 336.112 14 -8 -8 11 6154.96 346.579 8 -8 -8 12 2711.92 213.113 14 -8 -8 12 2540.65 219.067 8 -8 -8 13 1336.19 150.521 14 -8 -8 13 1382.35 161.563 8 -8 -8 14 338.353 89.7212 14 -8 -9 -8 1252.76 141.874 13 -8 -9 -7 4790.40 258.525 13 8 9 -7 3396.45 249.604 10 -8 -9 -6 2441.37 193.449 13 8 9 -6 1841.01 189.542 10 -8 -9 -5 910.498 140.988 13 -8 -9 -4 3868.24 278.184 2 -8 -9 -4 4695.49 272.917 13 -8 -9 -3 6374.25 366.730 2 -8 -9 -3 7186.43 353.325 13 -8 -9 -2 7102.84 358.435 13 -8 -9 -1 928.066 155.879 14 -8 -9 -1 968.319 166.950 2 -8 -9 -1 722.435 141.288 13 -8 -9 0 4068.02 296.121 2 -8 -9 0 4409.73 276.924 13 -8 -9 1 810.279 154.148 2 -8 -9 1 954.846 151.685 13 -8 -9 2 5783.03 346.206 2 -8 -9 3 6228.45 355.492 2 -8 -9 4 3117.14 250.178 2 -8 -9 5 676.335 128.882 14 -8 -9 6 2254.31 194.905 14 -8 -9 7 4004.55 251.257 14 -8 -9 8 1503.47 154.603 14 -8 -9 9 2444.15 184.580 14 -9 0 0 124.269 161.106 11 -9 0 -1 213.935 162.336 11 -9 0 1 377.325 184.988 11 -9 0 -2 7941.34 512.357 11 -9 0 2 9299.29 557.775 11 -9 0 -3 14.4866 140.359 11 -9 0 3 31.6772 144.846 11 -9 0 -4 1881.75 257.756 11 -9 0 -5 439.243 161.617 11 -9 0 -6 577.995 173.516 11 -9 0 6 571.372 195.062 11 -9 0 -7 2295.66 259.047 11 -9 0 7 2982.50 322.910 11 9 0 8 2486.76 274.232 12 -9 0 -8 1951.27 230.026 11 -9 0 8 2946.85 314.192 11 9 0 9 8508.68 422.871 12 -9 0 9 8208.23 472.016 11 9 0 10 667.991 155.491 12 -9 0 10 606.569 180.119 11 9 0 11 7437.36 417.788 12 -9 0 11 7610.44 471.869 11 -9 0 12 714.244 179.428 11 -9 0 13 709.008 182.177 11 -9 0 14 482.350 152.024 11 -9 0 15 159.811 113.075 11 -9 0 16 415.566 129.016 11 9 0 -16 401.689 134.250 3 -9 0 17 865.535 143.124 11 9 0 -17 890.683 152.424 3 -9 0 18 12404.8 492.404 11 9 0 -18 13807.5 536.747 3 9 0 -19 854.629 135.415 3 9 0 -20 986.830 129.057 3 9 0 -21 15034.7 515.017 3 9 1 -20 850.307 115.880 3 9 1 -19 4464.45 260.684 3 -9 1 18 2121.86 169.647 11 9 1 -18 2806.42 215.902 3 -9 1 17 8284.37 391.252 11 9 1 -17 9795.85 441.623 3 9 -1 16 12.8613 73.7237 12 -9 1 16 65.9140 97.4753 11 9 1 -16 8.95955 106.641 3 9 -1 15 383.398 111.178 12 -9 1 15 506.709 139.631 11 9 -1 14 8984.32 439.966 12 -9 1 14 10237.8 497.944 11 9 -1 13 28237.6 989.239 12 -9 1 13 30623.3 1057.80 11 9 -1 12 14371.7 626.405 12 -9 1 12 15121.5 673.832 11 9 -1 11 4141.06 317.090 12 -9 1 11 4464.19 353.325 11 9 -1 10 2306.27 253.996 12 -9 1 10 2264.73 272.849 11 9 -1 9 1377.82 214.719 12 -9 1 9 1907.38 254.223 11 9 -1 8 12919.0 538.406 12 -9 1 8 12460.6 569.786 11 9 -1 7 8217.48 487.869 12 -9 1 7 8646.95 526.451 11 -9 -1 -7 7212.36 428.938 11 9 -1 6 2461.54 280.272 12 -9 1 6 2227.12 282.570 11 -9 -1 -6 1926.27 238.254 11 9 -1 5 864.810 197.511 12 -9 1 5 993.230 214.583 11 -9 -1 -5 713.480 175.791 11 9 -1 4 925.547 200.586 12 -9 -1 -4 1139.80 210.712 11 9 -1 3 17194.3 796.118 12 -9 -1 -3 18230.3 796.809 11 -9 -1 -2 43.1449 143.095 11 -9 -1 -1 769.447 198.034 11 -9 -1 0 272.238 153.197 11 -9 -1 1 752.963 214.194 11 -9 -1 2 15.5087 140.375 11 -9 -1 3 19685.9 879.475 11 -9 -1 4 715.408 211.872 11 -9 1 -8 10862.1 545.414 11 -9 -1 8 10805.7 603.724 11 -9 1 -9 1327.06 196.166 11 -9 -1 9 1341.23 240.920 11 -9 -1 10 2709.66 295.697 11 -9 1 -10 36.6882 61.1989 11 -9 -1 11 4188.01 339.679 11 -9 1 -11 38.8500 38.0419 11 -9 -1 12 15959.1 718.778 11 -9 -1 13 27821.3 1024.59 11 -9 -1 14 8264.90 457.193 11 -9 -1 15 886.853 168.453 11 -9 -1 16 9.08131 99.9755 11 9 -1 -16 87.1636 110.410 3 -9 -1 17 9294.59 440.452 11 9 -1 -17 10083.7 449.152 3 -9 -1 18 2008.35 186.266 11 9 -1 -18 2399.56 203.733 3 9 -1 -19 4353.96 255.357 3 9 -1 -20 717.582 108.889 3 9 2 -19 6985.80 321.721 3 9 2 -18 5449.87 292.559 3 9 -2 17 1752.20 159.091 12 -9 2 17 1453.14 146.133 11 9 2 -17 1935.61 182.485 3 9 -2 16 1402.04 159.826 12 -9 2 16 899.414 135.775 11 9 2 -16 1317.30 175.646 3 9 -2 15 206.726 97.5065 12 -9 2 15 124.872 101.503 11 9 2 -15 88.7737 105.719 3 9 -2 14 3077.33 247.292 12 -9 2 14 3064.39 259.961 11 9 -2 13 10864.9 434.335 12 -9 2 13 10371.4 440.398 11 9 -2 12 727.178 157.659 12 -9 2 12 761.235 168.370 11 9 -2 11 228.773 120.954 12 -9 2 11 348.682 148.343 11 9 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8798.54 507.359 11 -9 -3 0 8454.25 496.454 11 -9 -3 1 8944.27 526.775 11 -9 -3 2 2287.71 282.242 11 -9 -3 3 2352.53 244.409 14 -9 -3 3 2164.87 277.532 11 -9 -3 4 2680.48 248.833 14 -9 -3 4 2834.89 310.366 11 -9 -3 5 7104.17 387.433 14 -9 -3 5 7480.30 481.604 11 -9 -3 6 27468.5 1062.34 11 -9 -3 7 8426.24 507.328 11 -9 -3 10 1692.59 240.926 11 -9 -3 11 9003.94 491.307 11 -9 -3 11 7662.93 427.209 2 -9 -3 12 8455.34 459.491 11 -9 -3 12 6496.87 373.005 2 -9 -3 13 7076.14 417.922 11 -9 -3 14 11682.2 536.053 11 9 -3 -14 10998.7 472.585 3 -9 -3 15 10630.4 487.469 11 9 -3 -15 9641.44 421.825 3 9 -3 -16 564.974 111.552 3 9 -3 -17 1069.91 121.717 3 9 -4 17 2790.39 186.009 12 9 -4 16 1896.53 167.746 12 9 -4 15 449.502 108.473 12 9 4 -15 256.984 82.6057 3 -9 4 14 9502.14 393.825 11 9 4 -14 8479.57 381.683 3 9 -4 13 2489.67 216.647 12 -9 4 13 2200.40 192.128 11 9 -4 12 1576.93 187.789 12 -9 4 12 1577.77 176.911 11 9 4 -12 1117.86 155.300 3 9 -4 11 12826.4 556.026 12 -9 4 11 12489.0 539.718 11 -9 -4 -11 11098.2 507.246 2 -9 -4 -10 537.860 141.842 2 9 -4 10 521.671 140.987 12 -9 4 10 327.818 130.254 11 9 -4 9 17556.6 713.196 12 -9 4 9 16537.3 701.781 11 -9 -4 -9 17655.4 712.559 2 9 -4 8 6729.63 406.627 12 -9 -4 -8 6845.02 419.875 2 9 -4 7 4888.26 345.352 12 -9 -4 -7 4788.72 363.693 2 9 -4 6 2022.38 236.307 12 9 -4 5 4957.97 362.785 12 -9 -4 -4-8.22470 46.8373 11 -9 -4 -3 9.19086 63.5373 11 -9 -4 -2 79.9179 111.525 11 -9 -4 -1 2981.24 273.394 11 -9 -4 0 4341.82 330.933 11 -9 -4 1 3813.28 302.686 14 -9 -4 1 3788.88 315.683 11 -9 -4 2 80.3336 121.676 14 -9 -4 2 83.6623 123.951 11 -9 -4 3 19816.5 771.298 14 -9 -4 3 21492.7 846.195 11 -9 -4 4 1396.04 191.709 14 -9 -4 4 1109.08 199.553 11 -9 -4 5 4950.79 329.636 14 -9 -4 5 6024.92 396.437 11 -9 -4 6 1169.63 174.383 14 -9 -4 6 1258.81 217.700 11 -9 -4 7 5427.27 326.998 14 -9 -4 7 6240.49 404.820 11 -9 -4 7 6312.60 410.140 2 -9 -4 8 5023.29 302.773 14 -9 -4 8 6271.36 399.295 11 -9 -4 8 5681.60 378.877 2 -9 -4 9 14822.0 570.923 14 -9 -4 9 17239.8 685.341 2 -9 -4 10 334.262 139.735 2 -9 -4 11 10004.4 420.519 2 9 -4 -11 4492.50 277.747 3 -9 -4 12 2353.98 232.088 11 -9 -4 12 1673.36 172.615 2 -9 -4 13 3034.89 250.178 11 9 -4 -13 27.1159 43.7620 3 9 -5 15 930.513 118.683 12 9 -5 14 5471.20 289.099 12 9 -5 13 169.796 85.3153 12 9 -5 12 886.788 138.812 12 -9 5 12 801.651 119.198 11 9 -5 11 3097.88 221.970 12 -9 5 11 2371.74 190.151 11 9 -5 10 1914.05 198.865 12 -9 5 10 2163.12 200.603 11 -9 -5 -10 1633.32 186.399 2 -9 -5 -9 1054.09 166.983 2 9 -5 9 1262.09 172.288 12 -9 5 9 1241.98 171.504 11 -9 -5 -8 2555.00 246.905 2 -9 -5 -7 444.213 147.928 2 -9 -5 -6 3728.25 312.037 2 -9 -5 -5 14329.7 651.911 2 9 -5 4 20797.9 805.426 12 -9 -5 -4 21406.1 855.063 2 9 -5 3 7732.87 430.016 12 -9 -5 -2 306.994 114.035 13 9 -5 2 469.848 143.994 12 -9 -5 -1 3009.36 236.606 13 -9 -5 -1 5289.11 372.670 2 -9 -5 0 1007.11 211.941 2 -9 -5 0 839.135 170.386 14 -9 -5 0 402.174 129.389 11 -9 -5 1 6139.04 368.405 14 -9 -5 1 5158.03 346.490 11 -9 -5 1 6481.68 425.521 2 -9 -5 2 596.254 184.322 2 -9 -5 2 613.691 159.050 14 -9 -5 2 494.931 146.947 11 -9 -5 3 8864.09 437.847 14 -9 -5 3 7683.59 431.069 11 -9 -5 3 7716.95 470.614 2 -9 -5 4 21646.3 792.751 14 -9 -5 4 21237.6 820.898 11 -9 -5 4 22320.5 869.105 2 -9 -5 5 12673.7 544.235 14 -9 -5 5 12305.9 571.484 11 -9 -5 5 13175.1 609.794 2 -9 -5 6 5096.73 311.283 14 -9 -5 6 4972.63 343.927 11 -9 -5 6 5148.72 359.431 2 -9 -5 7 294.888 153.373 2 -9 -5 7 199.723 108.311 14 -9 -5 7 427.677 142.447 11 -9 -5 8 2351.34 203.288 14 -9 -5 8 2576.06 248.959 11 -9 -5 8 2250.64 238.068 2 -9 -5 9 1491.42 163.703 14 -9 -5 9 1384.89 189.136 2 -9 -5 10 1590.03 162.140 14 -9 -5 10 1668.93 185.671 2 -9 -5 11 2209.29 192.525 2 9 -6 9 3847.64 246.912 12 -9 6 9 3577.95 225.326 11 -9 -6 -9 3099.87 228.490 2 9 -6 8 1593.49 167.939 12 -9 6 8 1292.65 152.259 11 -9 -6 -8 1355.26 168.513 2 9 -6 7 5845.83 322.328 12 -9 -6 -7 5351.78 328.188 2 9 -6 6 6907.40 357.088 12 -9 -6 -6 6648.98 376.080 2 -9 -6 -5 251.923 131.003 2 -9 -6 -5 120.890 79.6157 13 9 -6 5 184.443 95.5321 12 -9 -6 -4 597.031 156.645 2 -9 -6 -4 246.149 90.7784 13 9 -6 4 365.863 112.720 12 -9 -6 -3 1225.40 147.612 13 -9 -6 -2 4641.22 265.056 13 -9 -6 -1 3216.92 230.984 13 -9 -6 -1 5269.04 348.915 2 -9 -6 0 7336.88 368.867 13 -9 -6 0 12446.8 536.658 2 -9 -6 1 5560.94 333.871 14 -9 -6 1 5264.94 359.647 2 -9 -6 2 8834.78 427.014 14 -9 -6 2 8087.07 452.309 2 -9 -6 3 3029.70 243.213 14 -9 -6 3 3040.04 274.255 2 -9 -6 4 614.041 155.801 2 -9 -6 4 638.836 140.414 14 -9 -6 5 463.258 137.293 2 -9 -6 5 336.097 115.477 14 -9 -6 6 6821.38 345.549 14 -9 -6 6 6426.09 371.574 2 -9 -6 7 5701.95 302.877 14 -9 -6 7 5414.27 329.124 2 -9 -6 8 1295.68 148.470 14 -9 -6 8 1468.76 173.142 2 -9 -6 9 3128.88 206.745 14 -9 -6 9 3252.55 226.084 2 -9 -7 -6 535.115 108.961 2 -9 -7 -5 471.827 113.436 2 -9 -7 -4 1891.03 193.529 2 -9 -7 -3 7777.58 390.210 2 -9 -7 0 6592.19 315.285 13 -9 -7 0 10255.2 435.698 2 -9 -7 1 5173.76 270.643 13 -9 -7 1 7988.90 378.823 2 -9 -7 2 1318.72 142.069 13 -9 -7 2 2506.25 218.201 2 -9 -7 3 3391.53 216.113 13 -9 -7 3 5828.60 314.134 2 -9 -7 4 2040.26 179.946 14 -9 -7 4 2280.56 204.272 2 -9 -7 5 717.607 118.848 14 -9 -7 5 817.406 129.677 2 -9 -7 6 754.674 116.377 14 -9 -7 6 744.887 123.406 2 -10 0 0 4159.12 284.289 11 -10 0 1 87.0073 102.317 11 -10 0 -1 57.0045 90.2913 11 -10 0 2 5462.50 326.985 11 -10 0 -2 4926.85 297.858 11 -10 0 3 854.642 148.530 11 -10 0 -3 824.653 137.290 11 -10 0 4 9675.60 448.031 11 -10 0 -4 8167.88 377.842 11 -10 0 -5-33.8739 43.0153 11 -10 0 7 6699.90 358.051 11 -10 0 8 2277.08 205.924 11 -10 0 9 5296.99 300.179 11 -10 0 10 1488.57 158.399 11 -10 0 11 4812.41 263.216 11 10 0 -12 35.9855 63.0091 3 -10 1 11 5436.59 268.178 11 10 1 -11 4227.02 240.990 3 -10 1 10 2621.82 198.751 11 -10 1 9 9131.68 410.512 11 -10 1 8 3919.12 260.057 11 -10 1 7 1822.77 188.811 11 -10 1 6 6698.57 363.500 11 -10 1 3 13167.8 467.945 11 -10 -1 -3 2862.27 216.865 11 -10 1 2 13166.1 540.104 11 -10 -1 -2 11100.6 477.324 11 -10 1 1 19167.7 698.726 11 -10 -1 -1 17241.3 652.579 11 -10 1 0 1336.01 173.625 11 -10 -1 0 1237.25 161.552 11 -10 1 -1 18633.5 686.666 11 -10 -1 1 17900.4 680.296 11 -10 1 -2 12546.9 518.591 11 -10 -1 2 12274.9 527.035 11 -10 1 -3 13024.6 528.688 11 -10 -1 3 13915.3 565.323 11 -10 1 -4 6232.78 324.937 11 -10 -1 4 6659.34 361.861 11 -10 1 -5 1841.72 165.068 11 -10 -1 5 2059.73 206.471 11 -10 -1 9 8878.68 403.255 11 -10 -1 10 3319.19 225.324 11 -10 -1 11 5380.88 278.958 11 10 -1 -11 4852.99 253.510 3 -10 2 10 1746.22 152.579 11 10 2 -10 1273.03 133.080 3 -10 2 9 14748.3 544.985 11 -10 2 8 1692.69 167.871 11 -10 -2 -7 268.061 93.9223 2 -10 2 7 530.223 113.387 11 -10 2 6 5844.80 321.785 11 -10 2 5 4407.10 281.590 11 -10 2 2 4941.24 282.184 11 -10 -2 -2 50.7750 47.3961 11 -10 2 1 16340.6 609.550 11 -10 -2 -1 13681.7 532.831 11 -10 2 0 272.807 109.751 11 -10 -2 0 197.819 90.1746 11 -10 2 -1 16233.4 613.345 11 -10 -2 1 15122.9 584.315 11 -10 2 -2 5553.68 312.970 11 -10 -2 2 5301.06 307.069 11 -10 2 -3 7965.25 380.276 11 -10 -2 3 7978.73 386.413 11 -10 2 -4 1255.56 149.499 11 -10 -2 4 1417.90 169.153 11 -10 2 -5 4213.96 247.790 11 -10 -2 5 4433.63 278.094 11 -10 -2 6 4800.93 287.567 11 -10 -2 7 282.957 96.7351 2 -10 -2 7 368.960 106.335 11 -10 -2 8 1110.59 136.128 2 -10 -2 10 1246.06 143.283 11 -10 -2 11 993.773 121.829 11 -10 3 8 384.477 88.2490 11 -10 3 7 5611.92 288.332 11 -10 3 6 3969.97 243.037 11 -10 -3 -6 3695.85 239.314 2 -10 -3 -5 882.853 135.601 2 -10 3 5 713.207 124.583 11 -10 3 4 7419.92 359.257 11 -10 -3 -4 7063.03 362.556 2 -10 3 3 1697.80 175.812 11 -10 -3 -3 1580.04 178.810 2 -10 -3 0 681.741 139.336 2 -10 3 0 477.469 111.956 11 -10 3 -1 4579.42 267.321 11 -10 -3 1 4181.93 276.786 2 -10 -3 2-56.8132 98.9025 2 -10 3 -2 42.1466 81.0507 11 -10 -3 2 48.4035 69.8130 11 -10 -3 3 904.318 146.535 2 -10 3 -3 957.784 128.657 11 -10 -3 3 813.920 124.441 11 -10 3 -4 6254.70 311.154 11 -10 -3 4 6125.53 316.260 11 -10 -3 5 266.675 101.962 2 -10 3 -5 351.185 86.8057 11 -10 -3 5 298.560 91.2447 11 -10 -3 6 4094.82 245.835 11 -10 -3 6 3576.96 232.824 2 -10 -3 7 5676.70 293.407 11 -10 -3 8 390.836 92.1037 11 -10 4 5 4353.23 238.865 11 -10 -4 -4 217.604 83.4702 2 -10 4 4 343.647 89.5224 11 -10 -4 -3 657.591 118.509 2 -10 4 3 887.357 120.065 11 -10 4 2 2967.39 203.965 11 -10 -4 0 945.419 136.058 2 -10 4 -1 1306.61 139.637 11 -10 -4 1 1352.19 153.191 2 -10 4 -2 2765.29 191.641 11 -10 -4 2 2416.69 199.758 2 -10 -4 3 859.433 127.612 2 -10 4 -3 901.855 115.623 11 -10 -4 4 169.383 82.9923 2 0 0 0 0.00 0.00 0 TITL 20190605d in P2(1)2(1)2(1) REM P2(1)2(1)2(1) (#19 in standard setting) CELL 1.54184 8.359846 11.945903 32.589926 90.0000 90.0000 90.0000 ZERR 46.00 0.000095 0.000128 0.000367 0.0000 0.0000 0.0000 LATT -1 SYMM -x+1/2,-y, z+1/2 SYMM -x, y+1/2,-z+1/2 SYMM x+1/2,-y+1/2,-z SFAC C H N O Cl UNIT 46.00 46.00 46.00 46.00 46.00 TREF HKLF 4 END ; _shelx_hkl_checksum 76284 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.280 _oxdiff_exptl_absorpt_empirical_full_min 0.864