data_shelx _audit_creation_method 'SHELXL-2018/1' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C24 H27 N O5' _chemical_formula_sum 'C24 H27 N O5' _chemical_formula_weight 409.46 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/n' _space_group_name_Hall '-P 2yn' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 14.2282(14) _cell_length_b 9.0871(9) _cell_length_c 16.8947(16) _cell_angle_alpha 90 _cell_angle_beta 94.998(3) _cell_angle_gamma 90 _cell_volume 2176.1(4) _cell_formula_units_Z 4 _cell_measurement_temperature 296(2) _cell_measurement_reflns_used 9253 _cell_measurement_theta_min 2.98 _cell_measurement_theta_max 27.50 _exptl_crystal_description TABULAR _exptl_crystal_colour colourless _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_density_diffrn 1.250 _exptl_crystal_F_000 872 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.429 _exptl_crystal_size_mid 0.165 _exptl_crystal_size_min 0.065 _exptl_absorpt_coefficient_mu 0.087 _shelx_estimated_absorpt_T_min 0.964 _shelx_estimated_absorpt_T_max 0.994 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.6516 _exptl_absorpt_correction_T_max 0.7214 _exptl_absorpt_process_details 'SADABS-2016/2' _diffrn_ambient_temperature 296(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'sealed X-ray tube' _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 46902 _diffrn_reflns_av_unetI/netI 0.0937 _diffrn_reflns_av_R_equivalents 0.1524 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_l_min -22 _diffrn_reflns_limit_l_max 22 _diffrn_reflns_theta_min 2.873 _diffrn_reflns_theta_max 27.803 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.993 _diffrn_measured_fraction_theta_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.993 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.993 _diffrn_reflns_point_group_measured_fraction_full 0.999 _reflns_number_total 5120 _reflns_number_gt 2248 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Bruker APEX2' _computing_cell_refinement 'Bruker SAINT' _computing_data_reduction 'Bruker SAINT' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2018/1 (Sheldrick, 2018)' _computing_molecular_graphics 'Ortep for Windows (Farrugia, 2012)' _computing_publication_material 'WinGX publication routines (Farrugia, 2012)' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0662P)^2^+1.7987P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 5120 _refine_ls_number_parameters 277 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.1987 _refine_ls_R_factor_gt 0.0801 _refine_ls_wR_factor_ref 0.2108 _refine_ls_wR_factor_gt 0.1603 _refine_ls_goodness_of_fit_ref 1.010 _refine_ls_restrained_S_all 1.010 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 0.4540(2) 0.3003(3) 0.3876(2) 0.0474(8) Uani 1 1 d . . . . . C2 C 0.3885(2) 0.2250(3) 0.44268(18) 0.0428(8) Uani 1 1 d . . . . . C3 C 0.4463(2) 0.2320(3) 0.52175(19) 0.0454(8) Uani 1 1 d . . . . . C4 C 0.4271(3) 0.1867(4) 0.5960(2) 0.0601(10) Uani 1 1 d . . . . . H4 H 0.370433 0.140197 0.603767 0.072 Uiso 1 1 calc R U . . . C5 C 0.4943(3) 0.2118(4) 0.6595(2) 0.0703(11) Uani 1 1 d . . . . . H5 H 0.482571 0.181682 0.710304 0.084 Uiso 1 1 calc R U . . . C6 C 0.5771(3) 0.2803(4) 0.6476(3) 0.0741(12) Uani 1 1 d . . . . . H6 H 0.620475 0.297041 0.691137 0.089 Uiso 1 1 calc R U . . . C7 C 0.5990(2) 0.3254(4) 0.5740(2) 0.0621(10) Uani 1 1 d . . . . . H7 H 0.656066 0.370878 0.566522 0.074 Uiso 1 1 calc R U . . . C8 C 0.5315(2) 0.2996(3) 0.5114(2) 0.0464(8) Uani 1 1 d . . . . . C9 C 0.6121(2) 0.4170(4) 0.3986(2) 0.0630(10) Uani 1 1 d . . . . . H9A H 0.635865 0.489924 0.437268 0.076 Uiso 1 1 calc R U . . . H9B H 0.587248 0.469131 0.351258 0.076 Uiso 1 1 calc R U . . . C10 C 0.6928(2) 0.3223(4) 0.3780(2) 0.0578(9) Uani 1 1 d . . . . . C11 C 0.7830(3) 0.3650(5) 0.3993(3) 0.0927(15) Uani 1 1 d . . . . . H11 H 0.794091 0.449615 0.429693 0.111 Uiso 1 1 calc R U . . . C12 C 0.8577(4) 0.2854(8) 0.3768(4) 0.128(2) Uani 1 1 d . . . . . H12 H 0.918869 0.317879 0.390895 0.153 Uiso 1 1 calc R U . . . C13 C 0.8442(5) 0.1615(8) 0.3347(4) 0.123(2) Uani 1 1 d . . . . . H13 H 0.895478 0.108381 0.319415 0.148 Uiso 1 1 calc R U . . . C14 C 0.7542(5) 0.1135(6) 0.3142(3) 0.1084(17) Uani 1 1 d . . . . . H14 H 0.744182 0.026120 0.286076 0.130 Uiso 1 1 calc R U . . . C15 C 0.6789(3) 0.1943(5) 0.3352(3) 0.0825(12) Uani 1 1 d . . . . . H15 H 0.617783 0.162242 0.320379 0.099 Uiso 1 1 calc R U . . . C16 C 0.3549(2) 0.0733(3) 0.4118(2) 0.0530(9) Uani 1 1 d . . . . . H16A H 0.380393 0.051455 0.361707 0.064 Uiso 1 1 calc R U . . . H16B H 0.374909 -0.002889 0.449826 0.064 Uiso 1 1 calc R U . . . C17 C 0.2471(2) 0.0827(3) 0.40087(18) 0.0447(8) Uani 1 1 d . . . . . C18 C 0.2102(2) -0.0045(4) 0.3281(2) 0.0580(9) Uani 1 1 d . . . . . H18A H 0.240006 0.029724 0.282033 0.070 Uiso 1 1 calc R U . . . H18B H 0.225303 -0.107845 0.335966 0.070 Uiso 1 1 calc R U . . . C19 C 0.2021(3) 0.0294(4) 0.47426(19) 0.0620(10) Uani 1 1 d . . . . . H19A H 0.220230 0.093372 0.518197 0.093 Uiso 1 1 calc R U . . . H19B H 0.223010 -0.068875 0.486951 0.093 Uiso 1 1 calc R U . . . H19C H 0.134674 0.030261 0.463901 0.093 Uiso 1 1 calc R U . . . C20 C 0.2354(2) 0.2493(3) 0.38790(19) 0.0441(8) Uani 1 1 d . . . . . H20 H 0.251011 0.273979 0.334127 0.053 Uiso 1 1 calc R U . . . C21 C 0.1415(2) 0.3162(4) 0.4016(2) 0.0530(9) Uani 1 1 d . . . . . H21A H 0.092233 0.261645 0.370971 0.064 Uiso 1 1 calc R U . . . H21B H 0.131100 0.305596 0.457303 0.064 Uiso 1 1 calc R U . . . C22 C 0.1329(2) 0.4743(4) 0.3797(2) 0.0590(10) Uani 1 1 d . . . . . C23 C 0.0411(4) 0.6893(5) 0.3827(5) 0.180(4) Uani 1 1 d . . . . . H23A H 0.074372 0.750092 0.423191 0.216 Uiso 1 1 calc R U . . . H23B H 0.066343 0.710841 0.332458 0.216 Uiso 1 1 calc R U . . . C24 C -0.0492(4) 0.7230(7) 0.3775(4) 0.153(3) Uani 1 1 d . . . . . H24A H -0.082226 0.664458 0.336735 0.229 Uiso 1 1 calc R U . . . H24B H -0.056974 0.825356 0.364506 0.229 Uiso 1 1 calc R U . . . H24C H -0.074199 0.703707 0.427430 0.229 Uiso 1 1 calc R U . . . N1 N 0.53570(17) 0.3373(3) 0.43056(17) 0.0493(7) Uani 1 1 d . . . . . O1 O 0.43621(16) 0.3231(3) 0.31693(14) 0.0647(7) Uani 1 1 d . . . . . O2 O 0.30501(13) 0.3129(2) 0.44461(12) 0.0472(6) Uani 1 1 d . . . . . O3 O 0.11083(19) 0.0133(3) 0.31505(17) 0.0674(8) Uani 1 1 d . . . . . O4 O 0.1889(2) 0.5459(3) 0.3472(2) 0.1018(11) Uani 1 1 d . . . . . O5 O 0.0578(2) 0.5349(3) 0.4023(3) 0.1211(14) Uani 1 1 d . . . . . H3O H 0.096(3) -0.033(5) 0.276(3) 0.111(19) Uiso 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.048(2) 0.0378(18) 0.055(2) -0.0009(16) 0.0008(17) 0.0080(15) C2 0.0402(17) 0.0346(17) 0.0521(19) -0.0059(14) -0.0050(15) 0.0068(14) C3 0.0498(19) 0.0345(17) 0.050(2) -0.0036(15) -0.0042(16) 0.0068(15) C4 0.069(2) 0.054(2) 0.056(2) -0.0006(18) -0.0023(19) 0.0101(18) C5 0.092(3) 0.068(3) 0.049(2) -0.0055(19) -0.007(2) 0.026(2) C6 0.088(3) 0.063(3) 0.065(3) -0.020(2) -0.028(2) 0.022(2) C7 0.056(2) 0.041(2) 0.085(3) -0.020(2) -0.019(2) 0.0060(16) C8 0.050(2) 0.0276(16) 0.060(2) -0.0058(15) -0.0057(17) 0.0085(14) C9 0.057(2) 0.045(2) 0.088(3) 0.0091(19) 0.005(2) -0.0032(18) C10 0.050(2) 0.052(2) 0.071(2) 0.0130(19) 0.0064(18) -0.0005(17) C11 0.053(3) 0.090(3) 0.137(4) 0.010(3) 0.014(3) -0.010(2) C12 0.062(3) 0.129(5) 0.197(7) 0.041(5) 0.039(4) 0.010(4) C13 0.107(5) 0.118(5) 0.157(6) 0.053(4) 0.080(4) 0.047(4) C14 0.128(5) 0.093(4) 0.109(4) -0.001(3) 0.044(4) 0.025(4) C15 0.077(3) 0.077(3) 0.095(3) -0.010(3) 0.011(2) 0.011(2) C16 0.052(2) 0.0395(18) 0.065(2) -0.0083(16) -0.0064(17) 0.0045(15) C17 0.0502(19) 0.0374(17) 0.0451(18) -0.0020(14) -0.0040(15) -0.0036(15) C18 0.063(2) 0.050(2) 0.060(2) -0.0065(17) -0.0032(18) -0.0029(17) C19 0.077(3) 0.052(2) 0.055(2) 0.0055(17) 0.0005(19) -0.0054(19) C20 0.0421(18) 0.0411(17) 0.0479(19) 0.0005(15) -0.0038(15) -0.0011(14) C21 0.0463(19) 0.047(2) 0.065(2) 0.0037(17) 0.0021(16) 0.0008(16) C22 0.039(2) 0.058(2) 0.080(3) 0.012(2) 0.0054(18) 0.0048(18) C23 0.106(4) 0.051(3) 0.392(12) 0.045(5) 0.075(6) 0.035(3) C24 0.157(6) 0.106(5) 0.202(7) 0.063(5) 0.052(5) 0.045(4) N1 0.0427(16) 0.0368(14) 0.0680(19) 0.0005(14) 0.0013(14) 0.0006(12) O1 0.0671(16) 0.0741(17) 0.0520(15) 0.0086(13) -0.0005(12) 0.0095(13) O2 0.0407(12) 0.0376(12) 0.0612(14) -0.0094(10) -0.0066(10) 0.0046(10) O3 0.0667(18) 0.0660(17) 0.0657(18) -0.0088(14) -0.0165(14) -0.0075(13) O4 0.096(2) 0.074(2) 0.140(3) 0.037(2) 0.041(2) 0.0171(17) O5 0.077(2) 0.0573(18) 0.239(4) 0.026(2) 0.071(2) 0.0180(15) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 O1 1.217(4) . ? C1 N1 1.358(4) . ? C1 C2 1.534(4) . ? C2 O2 1.433(3) . ? C2 C3 1.508(4) . ? C2 C16 1.535(4) . ? C3 C4 1.370(5) . ? C3 C8 1.384(4) . ? C4 C5 1.392(5) . ? C4 H4 0.9300 . ? C5 C6 1.363(6) . ? C5 H5 0.9300 . ? C6 C7 1.371(6) . ? C6 H6 0.9300 . ? C7 C8 1.385(4) . ? C7 H7 0.9300 . ? C8 N1 1.414(4) . ? C9 N1 1.449(4) . ? C9 C10 1.500(5) . ? C9 H9A 0.9700 . ? C9 H9B 0.9700 . ? C10 C11 1.360(5) . ? C10 C15 1.374(5) . ? C11 C12 1.367(7) . ? C11 H11 0.9300 . ? C12 C13 1.336(8) . ? C12 H12 0.9300 . ? C13 C14 1.368(8) . ? C13 H13 0.9300 . ? C14 C15 1.372(6) . ? C14 H14 0.9300 . ? C15 H15 0.9300 . ? C16 C17 1.532(4) . ? C16 H16A 0.9700 . ? C16 H16B 0.9700 . ? C17 C18 1.517(4) . ? C17 C19 1.523(4) . ? C17 C20 1.537(4) . ? C18 O3 1.421(4) . ? C18 H18A 0.9700 . ? C18 H18B 0.9700 . ? C19 H19A 0.9600 . ? C19 H19B 0.9600 . ? C19 H19C 0.9600 . ? C20 O2 1.438(3) . ? C20 C21 1.504(4) . ? C20 H20 0.9800 . ? C21 C22 1.486(5) . ? C21 H21A 0.9700 . ? C21 H21B 0.9700 . ? C22 O4 1.198(4) . ? C22 O5 1.289(4) . ? C23 C24 1.316(7) . ? C23 O5 1.456(5) . ? C23 H23A 0.9700 . ? C23 H23B 0.9700 . ? C24 H24A 0.9600 . ? C24 H24B 0.9600 . ? C24 H24C 0.9600 . ? O3 H3O 0.79(5) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 C1 N1 125.3(3) . . ? O1 C1 C2 125.8(3) . . ? N1 C1 C2 108.9(3) . . ? O2 C2 C3 110.2(2) . . ? O2 C2 C16 105.9(2) . . ? C3 C2 C16 117.9(3) . . ? O2 C2 C1 108.3(2) . . ? C3 C2 C1 101.8(2) . . ? C16 C2 C1 112.4(3) . . ? C4 C3 C8 119.7(3) . . ? C4 C3 C2 131.4(3) . . ? C8 C3 C2 108.9(3) . . ? C3 C4 C5 118.6(4) . . ? C3 C4 H4 120.7 . . ? C5 C4 H4 120.7 . . ? C6 C5 C4 120.4(4) . . ? C6 C5 H5 119.8 . . ? C4 C5 H5 119.8 . . ? C5 C6 C7 122.5(4) . . ? C5 C6 H6 118.8 . . ? C7 C6 H6 118.8 . . ? C6 C7 C8 116.5(4) . . ? C6 C7 H7 121.8 . . ? C8 C7 H7 121.8 . . ? C3 C8 C7 122.3(3) . . ? C3 C8 N1 109.9(3) . . ? C7 C8 N1 127.8(3) . . ? N1 C9 C10 114.4(3) . . ? N1 C9 H9A 108.7 . . ? C10 C9 H9A 108.7 . . ? N1 C9 H9B 108.7 . . ? C10 C9 H9B 108.7 . . ? H9A C9 H9B 107.6 . . ? C11 C10 C15 118.1(4) . . ? C11 C10 C9 119.9(4) . . ? C15 C10 C9 122.0(3) . . ? C10 C11 C12 120.9(5) . . ? C10 C11 H11 119.5 . . ? C12 C11 H11 119.5 . . ? C13 C12 C11 121.0(6) . . ? C13 C12 H12 119.5 . . ? C11 C12 H12 119.5 . . ? C12 C13 C14 119.4(5) . . ? C12 C13 H13 120.3 . . ? C14 C13 H13 120.3 . . ? C13 C14 C15 120.0(5) . . ? C13 C14 H14 120.0 . . ? C15 C14 H14 120.0 . . ? C14 C15 C10 120.6(5) . . ? C14 C15 H15 119.7 . . ? C10 C15 H15 119.7 . . ? C17 C16 C2 105.6(2) . . ? C17 C16 H16A 110.6 . . ? C2 C16 H16A 110.6 . . ? C17 C16 H16B 110.6 . . ? C2 C16 H16B 110.6 . . ? H16A C16 H16B 108.7 . . ? C18 C17 C19 110.7(3) . . ? C18 C17 C16 110.0(3) . . ? C19 C17 C16 111.8(3) . . ? C18 C17 C20 111.9(3) . . ? C19 C17 C20 112.4(3) . . ? C16 C17 C20 99.6(2) . . ? O3 C18 C17 109.6(3) . . ? O3 C18 H18A 109.7 . . ? C17 C18 H18A 109.7 . . ? O3 C18 H18B 109.7 . . ? C17 C18 H18B 109.7 . . ? H18A C18 H18B 108.2 . . ? C17 C19 H19A 109.5 . . ? C17 C19 H19B 109.5 . . ? H19A C19 H19B 109.5 . . ? C17 C19 H19C 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? O2 C20 C21 107.8(2) . . ? O2 C20 C17 103.9(2) . . ? C21 C20 C17 117.6(3) . . ? O2 C20 H20 109.1 . . ? C21 C20 H20 109.1 . . ? C17 C20 H20 109.1 . . ? C22 C21 C20 114.0(3) . . ? C22 C21 H21A 108.7 . . ? C20 C21 H21A 108.7 . . ? C22 C21 H21B 108.7 . . ? C20 C21 H21B 108.7 . . ? H21A C21 H21B 107.6 . . ? O4 C22 O5 120.4(4) . . ? O4 C22 C21 126.5(3) . . ? O5 C22 C21 113.1(3) . . ? C24 C23 O5 112.2(5) . . ? C24 C23 H23A 109.2 . . ? O5 C23 H23A 109.2 . . ? C24 C23 H23B 109.2 . . ? O5 C23 H23B 109.2 . . ? H23A C23 H23B 107.9 . . ? C23 C24 H24A 109.5 . . ? C23 C24 H24B 109.5 . . ? H24A C24 H24B 109.5 . . ? C23 C24 H24C 109.5 . . ? H24A C24 H24C 109.5 . . ? H24B C24 H24C 109.5 . . ? C1 N1 C8 110.5(3) . . ? C1 N1 C9 124.1(3) . . ? C8 N1 C9 125.2(3) . . ? C2 O2 C20 106.6(2) . . ? C18 O3 H3O 105(4) . . ? C22 O5 C23 117.8(4) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1 C1 C2 O2 -62.3(4) . . . . ? N1 C1 C2 O2 117.9(3) . . . . ? O1 C1 C2 C3 -178.5(3) . . . . ? N1 C1 C2 C3 1.8(3) . . . . ? O1 C1 C2 C16 54.4(4) . . . . ? N1 C1 C2 C16 -125.4(3) . . . . ? O2 C2 C3 C4 63.6(4) . . . . ? C16 C2 C3 C4 -58.2(5) . . . . ? C1 C2 C3 C4 178.3(3) . . . . ? O2 C2 C3 C8 -115.4(3) . . . . ? C16 C2 C3 C8 122.9(3) . . . . ? C1 C2 C3 C8 -0.6(3) . . . . ? C8 C3 C4 C5 0.7(5) . . . . ? C2 C3 C4 C5 -178.2(3) . . . . ? C3 C4 C5 C6 0.1(5) . . . . ? C4 C5 C6 C7 -0.9(6) . . . . ? C5 C6 C7 C8 0.8(5) . . . . ? C4 C3 C8 C7 -0.8(5) . . . . ? C2 C3 C8 C7 178.3(3) . . . . ? C4 C3 C8 N1 -179.7(3) . . . . ? C2 C3 C8 N1 -0.7(3) . . . . ? C6 C7 C8 C3 0.0(5) . . . . ? C6 C7 C8 N1 178.8(3) . . . . ? N1 C9 C10 C11 -135.2(4) . . . . ? N1 C9 C10 C15 47.2(5) . . . . ? C15 C10 C11 C12 2.0(7) . . . . ? C9 C10 C11 C12 -175.8(4) . . . . ? C10 C11 C12 C13 -1.6(9) . . . . ? C11 C12 C13 C14 -0.3(9) . . . . ? C12 C13 C14 C15 1.6(9) . . . . ? C13 C14 C15 C10 -1.1(7) . . . . ? C11 C10 C15 C14 -0.6(6) . . . . ? C9 C10 C15 C14 177.1(4) . . . . ? O2 C2 C16 C17 -2.6(3) . . . . ? C3 C2 C16 C17 121.3(3) . . . . ? C1 C2 C16 C17 -120.7(3) . . . . ? C2 C16 C17 C18 143.5(3) . . . . ? C2 C16 C17 C19 -93.1(3) . . . . ? C2 C16 C17 C20 25.8(3) . . . . ? C19 C17 C18 O3 60.1(4) . . . . ? C16 C17 C18 O3 -175.8(3) . . . . ? C20 C17 C18 O3 -66.1(4) . . . . ? C18 C17 C20 O2 -157.1(2) . . . . ? C19 C17 C20 O2 77.6(3) . . . . ? C16 C17 C20 O2 -40.9(3) . . . . ? C18 C17 C20 C21 83.9(4) . . . . ? C19 C17 C20 C21 -41.3(4) . . . . ? C16 C17 C20 C21 -159.9(3) . . . . ? O2 C20 C21 C22 69.1(4) . . . . ? C17 C20 C21 C22 -174.0(3) . . . . ? C20 C21 C22 O4 6.6(6) . . . . ? C20 C21 C22 O5 -170.6(3) . . . . ? O1 C1 N1 C8 177.9(3) . . . . ? C2 C1 N1 C8 -2.3(3) . . . . ? O1 C1 N1 C9 3.5(5) . . . . ? C2 C1 N1 C9 -176.8(3) . . . . ? C3 C8 N1 C1 1.9(3) . . . . ? C7 C8 N1 C1 -177.0(3) . . . . ? C3 C8 N1 C9 176.3(3) . . . . ? C7 C8 N1 C9 -2.6(5) . . . . ? C10 C9 N1 C1 -100.6(4) . . . . ? C10 C9 N1 C8 85.7(4) . . . . ? C3 C2 O2 C20 -152.8(2) . . . . ? C16 C2 O2 C20 -24.2(3) . . . . ? C1 C2 O2 C20 96.7(3) . . . . ? C21 C20 O2 C2 167.2(2) . . . . ? C17 C20 O2 C2 41.8(3) . . . . ? O4 C22 O5 C23 3.7(7) . . . . ? C21 C22 O5 C23 -178.9(5) . . . . ? C24 C23 O5 C22 153.5(6) . . . . ? _refine_diff_density_max 0.423 _refine_diff_density_min -0.288 _refine_diff_density_rms 0.044 _shelx_res_file ; TITL jothi1_0ma_a.res in P2(1)/n shelx.res created by SHELXL-2018/1 at 16:12:10 on 26-Feb-2019 CELL 0.71073 14.2282 9.0871 16.8947 90.000 94.998 90.000 ZERR 4.00 0.0014 0.0009 0.0016 0.000 0.003 0.000 LATT 1 SYMM 1/2 - X, 1/2 + Y, 1/2 - Z SFAC C H N O UNIT 96 108 4 20 MERG 2 SIZE 0.065 0.165 0.429 ACTA BOND $H HTAB CONF L.S. 10 TEMP 23.00 WGHT 0.066200 1.798700 FVAR 0.38811 C1 1 0.453995 0.300300 0.387635 11.00000 0.04842 0.03777 = 0.05549 -0.00091 0.00085 0.00798 C2 1 0.388457 0.225003 0.442679 11.00000 0.04017 0.03464 = 0.05214 -0.00586 -0.00502 0.00680 C3 1 0.446307 0.232023 0.521753 11.00000 0.04977 0.03454 = 0.05030 -0.00363 -0.00425 0.00682 C4 1 0.427111 0.186717 0.595969 11.00000 0.06855 0.05403 = 0.05632 -0.00056 -0.00233 0.01012 AFIX 43 H4 2 0.370433 0.140197 0.603767 11.00000 -1.20000 AFIX 0 C5 1 0.494292 0.211816 0.659485 11.00000 0.09189 0.06785 = 0.04899 -0.00555 -0.00694 0.02556 AFIX 43 H5 2 0.482571 0.181682 0.710304 11.00000 -1.20000 AFIX 0 C6 1 0.577127 0.280284 0.647629 11.00000 0.08809 0.06269 = 0.06538 -0.01980 -0.02775 0.02198 AFIX 43 H6 2 0.620475 0.297041 0.691137 11.00000 -1.20000 AFIX 0 C7 1 0.598969 0.325378 0.574019 11.00000 0.05581 0.04095 = 0.08504 -0.01977 -0.01867 0.00599 AFIX 43 H7 2 0.656066 0.370878 0.566522 11.00000 -1.20000 AFIX 0 C8 1 0.531533 0.299620 0.511387 11.00000 0.05017 0.02757 = 0.05969 -0.00581 -0.00567 0.00847 C9 1 0.612112 0.417001 0.398635 11.00000 0.05660 0.04468 = 0.08769 0.00906 0.00550 -0.00317 AFIX 23 H9A 2 0.635865 0.489924 0.437268 11.00000 -1.20000 H9B 2 0.587248 0.469131 0.351258 11.00000 -1.20000 AFIX 0 C10 1 0.692773 0.322258 0.377986 11.00000 0.05023 0.05231 = 0.07118 0.01304 0.00641 -0.00054 C11 1 0.783024 0.365019 0.399324 11.00000 0.05263 0.08981 = 0.13679 0.00986 0.01409 -0.01035 AFIX 43 H11 2 0.794091 0.449615 0.429693 11.00000 -1.20000 AFIX 0 C12 1 0.857729 0.285370 0.376752 11.00000 0.06249 0.12856 = 0.19651 0.04086 0.03904 0.00962 AFIX 43 H12 2 0.918869 0.317879 0.390895 11.00000 -1.20000 AFIX 0 C13 1 0.844176 0.161496 0.334665 11.00000 0.10695 0.11783 = 0.15727 0.05337 0.08032 0.04734 AFIX 43 H13 2 0.895478 0.108381 0.319415 11.00000 -1.20000 AFIX 0 C14 1 0.754238 0.113493 0.314208 11.00000 0.12842 0.09328 = 0.10930 -0.00062 0.04401 0.02452 AFIX 43 H14 2 0.744182 0.026120 0.286076 11.00000 -1.20000 AFIX 0 C15 1 0.678852 0.194328 0.335218 11.00000 0.07701 0.07652 = 0.09462 -0.00957 0.01058 0.01104 AFIX 43 H15 2 0.617783 0.162242 0.320379 11.00000 -1.20000 AFIX 0 C16 1 0.354949 0.073336 0.411823 11.00000 0.05201 0.03945 = 0.06548 -0.00827 -0.00640 0.00448 AFIX 23 H16A 2 0.380393 0.051455 0.361707 11.00000 -1.20000 H16B 2 0.374909 -0.002889 0.449826 11.00000 -1.20000 AFIX 0 C17 1 0.247099 0.082707 0.400871 11.00000 0.05023 0.03743 = 0.04512 -0.00196 -0.00405 -0.00358 C18 1 0.210161 -0.004502 0.328120 11.00000 0.06271 0.04980 = 0.06010 -0.00655 -0.00320 -0.00294 AFIX 23 H18A 2 0.240006 0.029724 0.282033 11.00000 -1.20000 H18B 2 0.225303 -0.107845 0.335966 11.00000 -1.20000 AFIX 0 C19 1 0.202093 0.029443 0.474264 11.00000 0.07729 0.05244 = 0.05527 0.00554 0.00054 -0.00536 AFIX 137 H19A 2 0.220230 0.093372 0.518197 11.00000 -1.50000 H19B 2 0.223010 -0.068875 0.486951 11.00000 -1.50000 H19C 2 0.134674 0.030261 0.463901 11.00000 -1.50000 AFIX 0 C20 1 0.235364 0.249316 0.387901 11.00000 0.04212 0.04109 = 0.04785 0.00052 -0.00377 -0.00114 AFIX 13 H20 2 0.251011 0.273979 0.334127 11.00000 -1.20000 AFIX 0 C21 1 0.141462 0.316193 0.401598 11.00000 0.04627 0.04714 = 0.06510 0.00372 0.00209 0.00078 AFIX 23 H21A 2 0.092233 0.261645 0.370971 11.00000 -1.20000 H21B 2 0.131100 0.305596 0.457303 11.00000 -1.20000 AFIX 0 C22 1 0.132861 0.474349 0.379697 11.00000 0.03910 0.05761 = 0.08033 0.01206 0.00535 0.00476 C23 1 0.041097 0.689299 0.382697 11.00000 0.10575 0.05065 = 0.39170 0.04519 0.07488 0.03485 AFIX 23 H23A 2 0.074372 0.750092 0.423191 11.00000 -1.20000 H23B 2 0.066343 0.710841 0.332458 11.00000 -1.20000 AFIX 0 C24 1 -0.049180 0.722983 0.377490 11.00000 0.15680 0.10600 = 0.20178 0.06333 0.05228 0.04502 AFIX 137 H24A 2 -0.082226 0.664458 0.336735 11.00000 -1.50000 H24B 2 -0.056974 0.825356 0.364506 11.00000 -1.50000 H24C 2 -0.074199 0.703707 0.427430 11.00000 -1.50000 AFIX 0 N1 3 0.535696 0.337254 0.430565 11.00000 0.04267 0.03678 = 0.06800 0.00050 0.00133 0.00060 O1 4 0.436213 0.323062 0.316927 11.00000 0.06708 0.07406 = 0.05205 0.00855 -0.00053 0.00948 O2 4 0.305005 0.312850 0.444610 11.00000 0.04071 0.03759 = 0.06123 -0.00937 -0.00655 0.00455 O3 4 0.110835 0.013329 0.315048 11.00000 0.06666 0.06604 = 0.06570 -0.00885 -0.01655 -0.00747 O4 4 0.188888 0.545887 0.347246 11.00000 0.09636 0.07428 = 0.14024 0.03669 0.04072 0.01712 O5 4 0.057759 0.534946 0.402319 11.00000 0.07749 0.05727 = 0.23863 0.02595 0.07089 0.01799 H3O 2 0.096290 -0.033341 0.276167 11.00000 0.11126 HKLF 4 1.0 1.00 0.00 0.00 0.00 1.00 0.00 0.00 0.00 1.00 REM jothi1_0ma_a.res in P2(1)/n REM R1 = 0.0801 for 2248 Fo > 4sig(Fo) and 0.1987 for all 5120 data REM 277 parameters refined using 0 restraints END WGHT 0.0651 1.8188 REM Instructions for potential hydrogen bonds EQIV $1 -x+1, -y+1, -z+1 HTAB C7 O4_$1 EQIV $2 -x+1/2, y-1/2, -z+1/2 HTAB C18 O4_$2 HTAB C21 O3 HTAB O3 O1_$2 REM Highest difference peak 0.423, deepest hole -0.288, 1-sigma level 0.044 Q1 1 0.1288 0.4969 0.3005 11.00000 0.05 0.42 Q2 1 0.0680 0.4948 0.4558 11.00000 0.05 0.25 Q3 1 0.0226 0.7340 0.4806 11.00000 0.05 0.20 Q4 1 0.0385 0.6984 0.4420 11.00000 0.05 0.19 Q5 1 0.5001 0.3624 0.2961 11.00000 0.05 0.17 Q6 1 -0.0192 0.6552 0.3296 11.00000 0.05 0.16 Q7 1 -0.1030 0.6569 0.3864 11.00000 0.05 0.16 Q8 1 0.0485 0.7119 0.3631 11.00000 0.05 0.15 Q9 1 0.4455 0.1804 0.7235 11.00000 0.05 0.15 Q10 1 0.6822 0.4192 0.5528 11.00000 0.05 0.15 Q11 1 0.7199 0.4332 0.5583 11.00000 0.05 0.14 Q12 1 0.5376 0.3053 0.4705 11.00000 0.05 0.14 Q13 1 0.1226 0.7444 0.3999 11.00000 0.05 0.14 Q14 1 0.6621 0.3219 0.6907 11.00000 0.05 0.14 Q15 1 0.4573 0.1554 0.3183 11.00000 0.05 0.14 Q16 1 0.5786 0.3723 0.4302 11.00000 0.05 0.13 Q17 1 0.7951 0.2030 0.2955 11.00000 0.05 0.13 Q18 1 -0.0996 0.8199 0.3259 11.00000 0.05 0.13 Q19 1 0.0467 0.5087 0.3756 11.00000 0.05 0.13 Q20 1 0.0471 0.6551 0.2768 11.00000 0.05 0.13 ; _shelx_res_checksum 95798 _shelx_hkl_file ; 0 2 0 2080.39 193.08 0 2 0 2105.89 193.08 0 2 0 2623.34 192.98 0 -2 0 2536.85 193.18 0 -2 0 2187.68 192.98 0 -2 0 2243.58 193.08 0 3 0 -0.50 1.00 0 3 0 0.90 0.80 0 -3 0 2.50 1.70 0 -3 0 -1.30 1.00 0 -3 0 3.30 1.50 0 4 0 898.51 73.89 0 4 0 864.71 73.69 0 4 0 777.62 74.39 0 -4 0 790.92 74.09 0 -4 0 1002.30 73.79 0 -4 0 892.81 74.19 0 -4 0 883.71 73.89 0 5 0 1.60 2.80 0 5 0 -0.80 1.40 0 5 0 1.00 2.60 0 -5 0 -2.00 2.70 0 -5 0 -4.00 2.40 0 -5 0 -2.20 1.90 0 -5 0 0.80 1.40 0 6 0 257.97 22.40 0 6 0 260.87 22.50 0 6 0 223.78 21.30 0 -6 0 261.47 21.70 0 -6 0 230.88 21.30 0 7 0 -0.60 3.90 0 7 0 0.80 2.40 0 7 0 1.20 3.90 0 -7 0 -1.40 2.00 0 -7 0 -0.10 2.70 0 8 0 136.49 13.90 0 8 0 117.09 13.70 0 -8 0 97.09 11.20 0 -8 0 132.89 12.60 0 9 0 -1.80 6.00 0 9 0 -1.30 6.00 0 -9 0 -0.20 4.20 0 -9 0 -5.30 3.10 0 10 0 15.50 9.20 0 -10 0 18.30 4.60 0 11 0 1.30 8.50 0 -11 0 12.90 6.90 1 -11 0 3.10 6.80 -1 11 0 6.30 8.10 -1 11 0 3.60 9.80 1 -10 0 -6.40 3.90 1 -10 0 -4.70 5.20 1 -9 0 6.60 3.10 1 -9 0 10.90 4.70 -1 9 0 2.20 7.00 -1 9 0 1.70 6.10 1 -8 0 0.50 3.40 1 -8 0 -1.40 2.50 -1 8 0 1.40 5.00 1 -7 0 32.10 5.40 -1 7 0 31.70 5.90 -1 7 0 32.00 5.90 -1 7 0 30.30 4.30 1 -6 0 36.10 4.90 1 -6 0 35.90 4.10 -1 6 0 38.40 6.50 -1 6 0 36.10 6.20 -1 6 0 31.00 4.10 1 -5 0 -0.70 1.90 1 -5 0 -0.50 2.60 1 -5 0 -0.70 2.70 1 -5 0 1.50 1.40 1 -5 0 0.00 0.80 1 -5 0 0.00 0.80 -1 5 0 -1.60 1.80 -1 5 0 -0.10 1.40 -1 5 0 -4.00 2.60 -1 5 0 2.40 3.00 1 -4 0 394.16 33.60 1 -4 0 370.36 34.00 1 -4 0 395.56 33.20 1 -4 0 399.46 34.00 -1 4 0 388.26 33.60 -1 4 0 412.66 33.40 1 -3 0 120.19 10.30 1 -3 0 104.19 10.90 1 -3 0 134.59 11.10 1 -3 0 118.69 10.60 1 -3 0 130.39 10.50 -1 3 0 121.39 10.90 -1 3 0 125.39 11.00 -1 3 0 132.39 10.40 -1 3 0 101.89 10.50 1 -2 0 294.67 29.20 1 -2 0 393.56 29.60 1 -2 0 348.67 29.50 1 -2 0 298.37 29.30 -1 2 0 400.86 29.20 -1 2 0 345.17 29.50 1 2 0 400.66 30.40 1 2 0 324.07 30.30 1 2 0 356.46 30.60 -1 -2 0 383.96 30.60 -1 -2 0 397.56 30.40 -1 -2 0 350.36 30.50 -1 -2 0 297.57 30.30 1 3 0 108.79 11.20 1 3 0 111.59 11.00 1 3 0 142.49 11.40 1 3 0 108.89 10.90 -1 -3 0 147.19 11.40 -1 -3 0 120.39 11.30 -1 -3 0 140.39 11.10 -1 -3 0 129.09 10.90 1 4 0 394.66 33.80 1 4 0 391.46 33.70 1 4 0 398.66 34.30 -1 -4 0 388.66 34.20 -1 -4 0 432.06 33.70 -1 -4 0 346.57 34.60 -1 -4 0 415.26 34.20 1 5 0 -1.20 1.40 1 5 0 -0.80 2.80 1 5 0 -1.40 1.90 -1 -5 0 -3.10 2.60 -1 -5 0 -0.80 2.80 -1 -5 0 0.30 1.40 -1 -5 0 1.30 2.20 1 6 0 37.00 4.60 1 6 0 35.90 6.30 1 6 0 44.20 6.30 -1 -6 0 37.70 5.20 1 7 0 36.60 4.90 1 7 0 43.00 6.70 1 7 0 40.80 7.50 -1 -7 0 35.40 5.70 1 8 0 6.30 5.00 1 8 0 1.80 5.20 -1 -8 0 0.50 3.00 -1 -8 0 5.60 3.90 1 9 0 -0.40 6.60 1 9 0 8.80 7.00 -1 -9 0 5.90 4.60 -1 -9 0 10.60 3.60 1 10 0 -5.70 8.70 1 10 0 0.00 8.90 -1 -10 0 6.00 4.20 1 11 0 9.20 10.20 1 11 0 24.90 9.00 -1 -11 0 5.60 5.40 -1 -11 0 1.30 6.70 2 -11 0 -6.20 6.50 -2 11 0 -7.90 9.20 -2 11 0 -14.20 7.60 2 -10 0 1.50 5.30 2 -10 0 3.60 3.80 -2 10 0 -9.20 8.80 -2 10 0 -1.70 7.50 2 -9 0 -2.30 4.20 2 -9 0 -1.00 2.80 -2 9 0 -9.00 5.30 -2 9 0 -5.30 6.30 2 -8 0 9.70 4.00 2 -8 0 10.70 3.10 2 -8 0 13.70 3.30 -2 8 0 4.40 4.50 -2 8 0 9.70 5.50 2 -7 0 -3.60 2.60 2 -7 0 1.30 3.30 2 -7 0 1.20 1.10 2 -7 0 0.00 1.20 2 -7 0 3.60 2.40 -2 7 0 -0.90 3.80 -2 7 0 -5.40 3.10 2 -6 0 23.10 3.00 2 -6 0 26.10 3.50 2 -6 0 33.30 4.30 -2 6 0 34.20 5.10 -2 6 0 31.30 5.60 -2 6 0 23.60 3.50 2 -5 0 14.00 2.30 2 -5 0 9.30 3.30 2 -5 0 12.70 2.60 2 -5 0 17.10 4.30 -2 5 0 11.10 3.20 -2 5 0 11.70 2.00 -2 5 0 8.10 2.50 -2 5 0 10.20 3.20 -2 5 0 15.50 2.00 2 -4 0 81.59 7.70 2 -4 0 88.99 8.40 2 -4 0 90.59 7.50 2 -4 0 82.09 7.50 2 -4 0 76.39 8.40 -2 4 0 78.99 7.40 -2 4 0 85.19 7.70 2 -3 0 3.60 1.30 2 -3 0 6.90 1.10 2 -3 0 6.00 1.20 2 -3 0 5.10 1.90 2 -3 0 6.10 1.40 2 -3 0 4.10 2.00 -2 3 0 5.50 1.80 -2 3 0 7.40 1.30 -2 3 0 6.20 1.30 -2 3 0 6.80 1.80 2 -2 0 2129.29 171.58 2 -2 0 2008.90 171.38 2 -2 0 1941.21 171.48 2 -2 0 1970.60 171.28 2 -2 0 2155.18 171.58 -2 2 0 1906.31 171.38 -2 2 0 2120.69 171.58 -2 2 0 2066.29 171.38 -2 2 0 2056.99 171.58 2 -1 0 102.49 9.20 2 -1 0 93.69 9.00 2 -1 0 112.09 9.20 2 -1 0 113.39 9.20 -2 1 0 103.19 9.10 -2 1 0 106.29 9.20 -2 1 0 107.89 9.10 -2 1 0 109.79 9.10 -2 0 0 1.40 0.90 -2 0 0 0.50 0.60 -2 0 0 1.30 0.50 2 1 0 105.29 10.20 2 1 0 145.29 10.20 2 1 0 113.99 10.10 -2 -1 0 123.29 10.30 -2 -1 0 113.89 10.20 -2 -1 0 107.29 10.10 2 2 0 1884.11 162.78 2 2 0 1892.41 162.58 2 2 0 2088.39 162.98 2 2 0 1684.23 162.88 -2 -2 0 2062.19 162.68 -2 -2 0 2088.69 162.88 -2 -2 0 1728.73 162.78 -2 -2 0 2117.29 162.98 -2 -2 0 1880.91 162.88 2 3 0 5.40 1.70 2 3 0 5.80 0.90 2 3 0 5.20 1.70 2 3 0 4.20 1.40 2 3 0 5.30 1.30 -2 -3 0 5.40 1.60 -2 -3 0 6.20 0.90 -2 -3 0 5.90 1.70 -2 -3 0 4.50 1.80 -2 -3 0 7.10 1.40 2 4 0 78.09 7.70 2 4 0 87.49 7.60 2 4 0 71.99 8.30 -2 -4 0 82.19 8.20 -2 -4 0 85.79 8.10 -2 -4 0 85.19 7.60 2 5 0 16.30 3.60 2 5 0 13.80 2.70 2 5 0 17.30 3.80 -2 -5 0 12.00 3.50 -2 -5 0 16.40 3.30 -2 -5 0 15.80 2.80 -2 -5 0 11.80 3.40 2 6 0 23.00 4.00 2 6 0 32.70 5.70 2 6 0 36.60 5.90 -2 -6 0 28.20 4.30 -2 -6 0 37.40 4.90 2 7 0 10.60 4.30 2 7 0 -4.10 4.00 2 7 0 6.10 2.90 -2 -7 0 1.40 3.10 -2 -7 0 2.00 2.50 2 8 0 8.70 5.50 2 8 0 3.10 4.90 -2 -8 0 17.10 3.60 -2 -8 0 7.40 4.40 2 9 0 6.10 7.10 2 9 0 -12.10 6.00 -2 -9 0 -1.30 4.70 -2 -9 0 -7.30 3.50 2 10 0 17.80 7.60 2 10 0 9.10 10.00 -2 -10 0 1.10 4.40 -2 -10 0 -3.60 5.40 2 11 0 12.40 9.00 2 11 0 -10.50 9.30 -2 -11 0 -2.30 5.20 3 -11 0 -7.40 6.00 -3 11 0 -11.70 8.20 -3 11 0 -8.40 9.60 3 -10 0 1.80 3.70 3 -10 0 -1.30 5.40 -3 10 0 -8.90 5.80 -3 10 0 -7.60 7.50 3 -9 0 3.40 4.30 3 -9 0 -2.40 3.00 -3 9 0 -7.40 6.50 -3 9 0 -6.40 5.70 3 -8 0 7.10 2.90 3 -8 0 4.60 3.60 3 -8 0 6.80 1.90 3 -8 0 6.00 2.60 -3 8 0 -2.00 4.30 -3 8 0 6.40 5.30 3 -7 0 12.10 2.40 3 -7 0 13.10 2.90 3 -7 0 13.80 3.00 3 -7 0 16.70 3.80 3 -7 0 15.00 2.40 -3 7 0 14.30 5.00 -3 7 0 11.60 4.70 3 -6 0 70.39 6.50 3 -6 0 75.09 7.30 3 -6 0 62.99 6.80 3 -6 0 75.89 6.80 -3 6 0 70.49 8.30 -3 6 0 57.79 8.20 3 -5 0 11.80 2.10 3 -5 0 13.70 2.20 3 -5 0 13.80 2.50 3 -5 0 17.90 3.00 -3 5 0 10.10 3.20 -3 5 0 12.80 3.30 -3 5 0 10.10 2.60 -3 5 0 16.10 2.30 3 -4 0 82.09 7.50 3 -4 0 90.89 7.50 3 -4 0 80.69 7.60 3 -4 0 86.49 8.60 3 -4 0 74.29 8.40 3 -4 0 80.59 7.60 3 -4 0 77.19 7.50 -3 4 0 78.39 7.40 -3 4 0 93.29 7.70 3 -3 0 34.30 3.50 3 -3 0 40.30 4.50 3 -3 0 39.70 3.70 3 -3 0 36.60 4.40 3 -3 0 34.90 3.60 3 -3 0 40.20 3.60 3 -3 0 31.60 3.60 -3 3 0 32.40 3.60 -3 3 0 41.70 4.30 -3 3 0 39.60 4.20 3 -2 0 228.38 23.50 3 -2 0 308.37 23.80 3 -2 0 289.57 23.50 3 -2 0 233.18 23.40 3 -2 0 298.77 23.60 3 -2 0 298.57 23.70 -3 2 0 240.68 23.50 -3 2 0 296.97 23.40 -3 2 0 294.37 23.70 3 -1 0 6.10 1.30 3 -1 0 9.70 1.50 3 -1 0 7.90 1.30 3 -1 0 9.70 1.50 3 -1 0 7.70 1.10 -3 1 0 7.30 1.10 -3 1 0 7.00 1.40 -3 1 0 7.10 1.10 -3 1 0 7.80 1.50 3 0 0 0.30 0.80 3 0 0 -1.50 1.00 3 0 0 -0.20 0.70 3 0 0 -0.50 0.50 3 0 0 0.50 0.80 -3 0 0 -0.60 0.70 -3 0 0 0.50 0.80 -3 0 0 -0.10 0.80 -3 0 0 -0.60 0.90 3 1 0 9.50 1.50 3 1 0 7.70 1.90 3 1 0 4.80 1.00 3 1 0 6.50 1.20 -3 -1 0 6.20 1.20 -3 -1 0 4.60 1.10 -3 -1 0 7.50 1.30 -3 -1 0 8.60 1.30 -3 -1 0 6.10 1.30 3 2 0 254.77 23.00 3 2 0 263.37 22.90 3 2 0 227.28 23.00 3 2 0 292.47 23.20 -3 -2 0 292.47 23.10 -3 -2 0 274.67 22.90 -3 -2 0 254.27 23.00 -3 -2 0 297.67 23.20 3 3 0 34.80 3.30 3 3 0 43.30 3.90 3 3 0 35.80 3.80 3 3 0 36.10 4.30 3 3 0 30.90 4.00 -3 -3 0 38.20 4.00 -3 -3 0 30.50 3.70 -3 -3 0 33.80 4.10 -3 -3 0 34.30 4.10 -3 -3 0 37.40 3.40 3 4 0 80.79 7.70 3 4 0 85.29 7.20 3 4 0 80.29 7.80 3 4 0 76.99 9.00 -3 -4 0 80.09 7.80 -3 -4 0 77.99 8.30 -3 -4 0 84.89 7.20 -3 -4 0 89.69 8.20 3 5 0 13.50 3.90 3 5 0 11.60 3.20 3 5 0 15.60 2.50 -3 -5 0 13.40 3.10 -3 -5 0 17.00 3.40 -3 -5 0 16.50 4.00 -3 -5 0 10.70 3.10 3 6 0 64.59 8.40 3 6 0 65.69 7.10 3 6 0 80.79 8.80 -3 -6 0 74.89 7.20 -3 -6 0 55.79 7.40 3 7 0 12.10 4.80 3 7 0 11.90 5.00 -3 -7 0 6.50 3.50 -3 -7 0 13.60 3.40 3 8 0 4.60 5.10 3 8 0 3.80 5.70 -3 -8 0 8.50 4.30 -3 -8 0 7.60 3.60 3 9 0 1.30 6.00 3 9 0 -3.20 5.90 -3 -9 0 4.10 3.90 -3 -9 0 -2.20 4.70 3 10 0 14.70 8.40 3 10 0 -8.00 7.60 -3 -10 0 2.50 6.20 -3 -10 0 -4.30 4.00 3 11 0 11.00 10.40 3 11 0 8.20 9.20 -3 -11 0 -5.70 7.30 4 -11 0 2.20 6.70 -4 11 0 2.00 7.50 -4 11 0 -1.50 9.90 4 -10 0 0.70 5.00 4 -10 0 -8.10 4.40 -4 10 0 16.40 8.20 -4 10 0 0.30 5.80 4 -9 0 -2.60 3.60 4 -9 0 -4.40 4.20 4 -9 0 -1.80 3.10 -4 9 0 -4.80 6.50 -4 9 0 -6.70 5.30 4 -8 0 4.10 2.30 4 -8 0 6.10 2.50 4 -8 0 3.90 2.80 4 -8 0 8.40 3.20 4 -8 0 5.10 3.90 -4 8 0 1.50 4.40 -4 8 0 0.20 5.20 4 -7 0 4.00 2.20 4 -7 0 1.60 2.40 4 -7 0 3.20 2.50 4 -7 0 6.00 3.20 4 -7 0 3.80 2.60 -4 7 0 0.10 3.70 -4 7 0 2.40 4.20 4 -6 0 16.50 3.50 4 -6 0 14.20 2.70 4 -6 0 18.20 2.80 4 -6 0 20.70 3.10 -4 6 0 11.10 3.90 -4 6 0 18.40 2.90 -4 6 0 14.30 3.70 4 -5 0 8.40 2.40 4 -5 0 14.40 2.10 4 -5 0 9.30 2.30 4 -5 0 9.10 2.00 4 -5 0 9.70 2.40 -4 5 0 9.10 3.20 -4 5 0 7.90 2.10 -4 5 0 8.90 3.00 4 -4 0 26.00 4.50 4 -4 0 28.90 3.50 4 -4 0 29.50 3.30 4 -4 0 28.10 3.20 4 -4 0 33.40 3.30 4 -4 0 21.40 4.40 4 -4 0 25.30 3.40 -4 4 0 31.50 4.40 -4 4 0 30.50 4.30 -4 4 0 24.00 3.30 4 -3 0 116.29 10.30 4 -3 0 116.29 9.90 4 -3 0 118.09 10.50 4 -3 0 114.49 10.50 4 -3 0 109.99 9.90 4 -3 0 107.79 10.00 -4 3 0 108.19 9.90 4 -2 0 149.59 11.90 4 -2 0 120.49 11.60 4 -2 0 123.49 11.70 4 -2 0 158.88 12.10 4 -2 0 143.99 12.10 4 -2 0 125.19 11.90 -4 2 0 130.39 11.70 -4 2 0 121.49 11.90 -4 2 0 137.39 11.70 -4 2 0 149.59 12.10 4 -1 0 26.70 2.40 4 -1 0 24.70 2.70 4 -1 0 26.10 2.60 4 -1 0 26.10 3.00 4 -1 0 22.20 2.80 4 -1 0 22.90 2.70 -4 1 0 27.30 2.40 -4 1 0 23.80 2.60 -4 1 0 19.40 2.70 -4 1 0 27.10 2.90 -4 1 0 28.70 2.90 4 0 0 71.89 6.10 4 0 0 72.69 6.30 4 0 0 60.09 6.10 4 0 0 56.39 5.90 -4 0 0 71.09 6.10 -4 0 0 70.49 6.20 -4 0 0 64.09 6.20 -4 0 0 76.89 6.20 4 1 0 24.50 2.60 4 1 0 25.80 2.60 4 1 0 24.30 2.70 4 1 0 24.80 2.60 4 1 0 22.10 2.50 -4 -1 0 27.70 2.70 -4 -1 0 17.50 2.40 -4 -1 0 19.40 2.50 -4 -1 0 22.50 2.60 4 2 0 120.79 11.60 4 2 0 153.58 11.70 4 2 0 141.09 11.90 4 2 0 114.19 11.60 4 2 0 139.79 11.50 -4 -2 0 114.39 11.70 -4 -2 0 137.49 11.60 -4 -2 0 112.79 11.60 -4 -2 0 141.19 11.70 -4 -2 0 148.49 11.60 4 3 0 115.69 10.70 4 3 0 114.59 10.90 4 3 0 121.29 10.70 4 3 0 118.09 10.40 -4 -3 0 110.99 10.70 -4 -3 0 115.49 10.80 -4 -3 0 120.69 11.00 -4 -3 0 133.29 10.50 -4 -3 0 129.79 11.80 4 4 0 21.80 4.10 4 4 0 25.70 2.80 4 4 0 25.60 3.60 4 4 0 22.20 3.50 -4 -4 0 25.60 3.90 -4 -4 0 25.40 3.00 -4 -4 0 30.70 4.20 4 5 0 6.90 3.10 4 5 0 10.30 3.30 4 5 0 13.60 2.60 4 5 0 9.30 1.70 -4 -5 0 13.40 3.20 -4 -5 0 8.30 1.70 -4 -5 0 11.80 2.90 -4 -5 0 10.00 2.60 4 6 0 13.30 4.60 4 6 0 19.30 4.60 -4 -6 0 10.10 3.40 4 7 0 4.90 5.00 4 7 0 10.40 4.70 -4 -7 0 4.50 3.30 -4 -7 0 8.00 4.00 4 8 0 3.60 5.00 4 8 0 7.00 5.50 -4 -8 0 1.40 3.40 -4 -8 0 5.30 4.30 4 9 0 4.20 6.80 4 9 0 -4.60 6.30 -4 -9 0 2.70 4.90 4 10 0 -11.30 7.30 4 10 0 1.80 8.60 -4 -10 0 -5.50 4.60 -4 -10 0 -2.50 6.10 4 11 0 -20.30 10.00 4 11 0 19.30 9.60 -4 -11 0 8.90 7.70 5 -11 0 -4.80 8.20 5 -11 0 13.10 7.30 -5 11 0 12.00 8.00 5 -10 0 -2.30 5.40 5 -10 0 -9.40 6.00 -5 10 0 -3.60 7.50 -5 10 0 11.50 7.00 5 -9 0 1.90 2.90 5 -9 0 6.60 3.30 5 -9 0 -8.10 4.10 -5 9 0 2.70 5.70 -5 9 0 0.70 6.70 5 -8 0 3.50 3.00 5 -8 0 7.30 4.10 5 -8 0 6.90 3.00 5 -8 0 10.50 3.10 5 -8 0 8.60 2.90 -5 8 0 5.40 5.50 -5 8 0 3.00 5.20 5 -7 0 2.90 2.40 5 -7 0 1.80 3.00 -5 7 0 -0.20 3.90 -5 7 0 9.20 5.00 5 -6 0 29.60 3.90 5 -6 0 26.80 4.10 5 -6 0 31.00 4.90 5 -6 0 29.30 4.30 -5 6 0 29.80 4.80 -5 6 0 22.90 4.80 -5 6 0 45.40 6.40 5 -5 0 49.90 5.10 5 -5 0 56.59 5.50 5 -5 0 46.50 5.40 5 -5 0 54.99 6.30 5 -5 0 45.80 5.20 5 -5 0 44.40 5.10 -5 5 0 47.40 5.30 -5 5 0 57.59 6.40 5 -4 0 85.09 8.30 5 -4 0 97.29 9.10 5 -4 0 78.89 8.00 5 -4 0 96.89 8.90 5 -4 0 88.19 8.20 5 -4 0 85.69 8.20 5 -4 0 90.59 9.20 -5 4 0 81.19 8.00 -5 4 0 98.29 8.90 -5 4 0 96.79 8.40 5 -3 0 37.20 4.00 5 -3 0 39.80 5.70 5 -3 0 36.30 5.00 5 -3 0 49.99 4.20 5 -3 0 40.50 4.30 5 -3 0 36.10 4.00 5 -3 0 39.40 5.00 -5 3 0 41.80 4.10 5 -2 0 122.69 10.90 5 -2 0 108.79 10.80 5 -2 0 123.89 11.00 5 -2 0 134.89 11.10 5 -2 0 123.99 10.60 5 -2 0 117.19 10.80 5 -2 0 120.69 10.50 -5 2 0 122.59 10.90 -5 2 0 114.19 10.50 -5 2 0 126.99 10.70 5 -1 0 0.10 1.10 5 -1 0 0.10 1.30 5 -1 0 1.10 1.20 5 -1 0 -1.00 0.90 -5 1 0 -0.20 1.10 -5 1 0 0.40 0.80 -5 1 0 -0.20 1.00 -5 1 0 0.50 1.20 -5 1 0 -0.90 1.30 5 0 0 1.00 1.00 5 0 0 1.10 1.30 5 0 0 -1.10 0.90 5 0 0 -1.20 0.70 5 0 0 -0.40 1.00 -5 0 0 0.00 1.00 -5 0 0 -0.50 1.00 -5 0 0 -0.30 0.80 -5 0 0 0.20 1.00 -5 0 0 0.10 1.40 5 1 0 -0.20 1.10 5 1 0 -0.60 0.90 5 1 0 0.30 0.90 5 1 0 -1.50 1.10 5 1 0 -1.60 1.20 -5 -1 0 -1.60 0.90 -5 -1 0 -1.40 0.90 -5 -1 0 -0.50 1.00 -5 -1 0 -1.10 1.10 -5 -1 0 0.10 1.10 5 2 0 139.29 11.00 5 2 0 114.29 10.90 5 2 0 122.39 11.70 5 2 0 122.69 11.00 5 2 0 134.49 11.00 -5 -2 0 137.49 11.00 -5 -2 0 125.89 10.90 -5 -2 0 102.89 11.00 -5 -2 0 127.79 11.00 -5 -2 0 106.79 11.10 5 3 0 40.30 4.10 5 3 0 36.30 6.60 5 3 0 38.50 4.70 5 3 0 47.10 4.50 5 3 0 41.10 4.60 -5 -3 0 34.10 4.70 -5 -3 0 46.30 4.20 -5 -3 0 37.20 4.80 5 4 0 95.29 8.30 5 4 0 76.49 8.60 5 4 0 89.19 7.80 5 4 0 94.59 8.20 5 4 0 74.89 8.70 -5 -4 0 81.39 8.30 -5 -4 0 80.59 7.80 -5 -4 0 97.79 8.70 -5 -4 0 89.09 8.70 -5 -4 0 77.19 8.40 5 5 0 59.39 6.30 5 5 0 48.60 6.70 5 5 0 52.29 4.70 -5 -5 0 42.40 5.40 -5 -5 0 40.10 4.70 -5 -5 0 50.09 6.00 5 6 0 33.80 5.40 5 6 0 38.70 6.30 -5 -6 0 21.00 4.10 -5 -6 0 27.80 4.90 5 7 0 1.50 5.10 5 7 0 0.20 4.80 -5 -7 0 -2.40 3.60 -5 -7 0 -1.80 2.90 5 8 0 10.00 6.20 5 8 0 22.20 6.60 -5 -8 0 4.60 4.20 -5 -8 0 7.50 4.70 5 9 0 -9.30 6.20 5 9 0 -0.90 6.90 -5 -9 0 -6.50 4.00 -5 -9 0 -4.40 5.50 5 10 0 -10.40 8.60 5 10 0 -4.30 7.80 -5 -10 0 -3.80 5.00 -5 -10 0 0.10 6.00 5 11 0 -13.00 9.30 5 11 0 -19.70 10.70 -5 -11 0 1.60 7.60 -5 -11 0 -2.60 6.20 6 -11 0 7.10 7.20 6 -11 0 -6.40 8.20 -6 11 0 -5.00 8.20 6 -10 0 -4.00 5.20 6 -10 0 -1.10 6.60 -6 10 0 -6.20 6.60 6 -9 0 0.60 4.10 6 -9 0 1.20 3.40 6 -9 0 0.50 4.30 -6 9 0 -4.90 4.80 6 -8 0 10.70 4.00 6 -8 0 4.60 2.90 6 -8 0 9.20 3.60 6 -8 0 6.30 5.20 -6 8 0 12.90 5.50 6 -7 0 44.30 5.60 6 -7 0 48.10 5.30 6 -7 0 36.50 6.60 6 -7 0 38.00 5.90 6 -7 0 40.40 6.40 -6 7 0 47.70 6.10 -6 7 0 36.80 6.90 6 -6 0 32.30 4.30 6 -6 0 31.30 4.80 6 -6 0 31.50 5.10 6 -6 0 28.50 5.20 -6 6 0 33.70 5.70 -6 6 0 36.70 4.90 6 -5 0 -1.40 2.00 6 -5 0 -4.10 2.60 6 -5 0 -1.10 2.30 6 -5 0 1.70 1.70 6 -5 0 -3.30 1.90 -6 5 0 0.70 2.90 -6 5 0 -2.00 2.40 6 -4 0 18.20 3.30 6 -4 0 18.20 3.30 6 -4 0 18.50 4.50 6 -4 0 12.50 2.40 6 -4 0 12.80 2.30 6 -4 0 26.00 4.40 6 -4 0 13.70 2.50 -6 4 0 15.30 3.60 -6 4 0 20.00 3.50 -6 4 0 15.20 2.40 6 -3 0 74.59 7.10 6 -3 0 73.39 8.00 6 -3 0 74.89 8.10 6 -3 0 83.59 7.60 6 -3 0 74.09 7.80 6 -3 0 85.99 7.30 6 -3 0 78.49 7.90 6 -3 0 70.19 7.20 -6 3 0 88.09 7.40 -6 3 0 85.79 7.90 6 -2 0 -0.50 1.00 6 -2 0 -0.80 1.20 6 -2 0 -1.90 1.60 6 -2 0 -0.30 1.50 6 -2 0 -0.40 1.80 6 -2 0 0.60 1.70 -6 2 0 0.70 1.70 -6 2 0 0.90 1.10 -6 2 0 -1.60 1.50 6 -1 0 75.49 6.50 6 -1 0 77.59 7.00 6 -1 0 71.59 6.70 6 -1 0 74.89 7.10 6 -1 0 84.29 7.00 -6 1 0 68.99 6.80 -6 1 0 80.29 7.10 -6 1 0 66.99 6.90 -6 1 0 64.19 6.50 6 0 0 237.48 19.90 6 0 0 214.58 19.80 6 0 0 225.08 19.90 6 0 0 209.38 19.90 -6 0 0 239.88 19.60 -6 0 0 245.88 19.80 -6 0 0 229.88 19.80 -6 0 0 245.28 20.00 -6 0 0 217.88 19.90 6 1 0 76.09 6.90 6 1 0 64.29 6.60 6 1 0 76.79 6.90 6 1 0 84.39 6.80 6 1 0 62.79 7.10 -6 -1 0 71.39 6.70 -6 -1 0 74.79 7.00 -6 -1 0 71.49 6.90 -6 -1 0 67.19 6.90 6 2 0 -2.10 1.60 6 2 0 -2.40 1.50 -6 -2 0 1.90 1.50 -6 -2 0 -0.50 1.60 6 3 0 76.59 7.20 6 3 0 67.99 7.50 6 3 0 83.99 7.60 6 3 0 70.99 7.30 6 3 0 73.19 7.90 -6 -3 0 73.09 7.40 -6 -3 0 74.09 7.70 -6 -3 0 87.09 7.30 -6 -3 0 85.29 7.60 6 4 0 11.70 3.70 6 4 0 14.60 2.50 6 4 0 14.00 3.30 6 4 0 12.90 3.10 6 4 0 19.50 3.40 -6 -4 0 21.30 3.60 -6 -4 0 13.60 2.60 -6 -4 0 16.90 3.50 -6 -4 0 11.30 2.70 6 5 0 1.10 3.00 6 5 0 -2.20 3.00 6 5 0 2.10 1.70 -6 -5 0 -0.70 1.80 -6 -5 0 -1.80 2.40 -6 -5 0 -3.60 2.50 6 6 0 36.40 6.10 6 6 0 29.60 3.80 6 6 0 36.00 6.40 -6 -6 0 24.90 4.90 -6 -6 0 25.60 3.80 -6 -6 0 35.90 5.40 6 7 0 45.80 7.90 6 7 0 43.20 7.70 6 7 0 48.50 4.60 -6 -7 0 40.10 7.40 -6 -7 0 37.50 6.90 6 8 0 9.90 6.60 6 8 0 8.80 6.40 -6 -8 0 6.30 4.80 -6 -8 0 6.80 4.20 6 9 0 20.20 8.20 -6 -9 0 -5.40 4.70 6 10 0 -7.30 8.50 6 10 0 7.60 9.80 -6 -10 0 -6.40 5.10 -6 -10 0 -3.20 6.50 6 11 0 -1.60 9.70 6 11 0 -6.00 10.90 -6 -11 0 -3.30 6.60 -6 -11 0 -0.60 9.10 7 -11 0 -1.70 11.80 7 -10 0 -3.70 5.90 7 -10 0 -10.20 6.90 -7 10 0 13.20 7.40 7 -9 0 6.00 3.80 7 -9 0 -11.70 5.70 7 -9 0 -3.30 4.60 7 -9 0 3.00 4.60 7 -8 0 14.50 4.70 7 -8 0 16.00 5.70 7 -8 0 14.10 3.60 -7 8 0 22.80 4.80 -7 8 0 17.90 5.60 7 -7 0 -3.40 4.20 7 -7 0 1.50 2.70 7 -7 0 3.70 3.00 7 -7 0 4.30 3.40 -7 7 0 0.90 3.80 -7 7 0 -1.90 4.20 7 -6 0 2.30 4.30 7 -6 0 1.90 2.30 7 -6 0 -1.40 2.70 7 -6 0 0.10 2.60 -7 6 0 2.60 3.30 -7 6 0 1.20 3.40 7 -5 0 88.99 8.50 7 -5 0 78.29 7.80 7 -5 0 71.79 7.20 7 -5 0 72.69 7.40 7 -5 0 67.09 7.40 -7 5 0 62.99 8.30 -7 5 0 78.09 8.00 7 -4 0 8.50 2.10 7 -4 0 6.90 1.90 7 -4 0 8.40 2.20 7 -4 0 12.50 3.00 7 -4 0 8.50 2.80 -7 4 0 10.20 3.00 -7 4 0 10.10 3.10 7 -3 0 37.60 5.30 7 -3 0 32.10 4.90 7 -3 0 42.20 5.40 7 -3 0 38.30 4.30 7 -3 0 43.80 5.20 7 -3 0 44.80 4.20 -7 3 0 35.80 4.90 -7 3 0 46.10 4.80 -7 3 0 36.10 4.20 7 -2 0 4.60 2.30 7 -2 0 5.00 1.80 7 -2 0 7.30 2.50 7 -2 0 7.40 1.40 7 -2 0 7.10 2.40 -7 2 0 9.90 2.10 -7 2 0 7.80 1.50 -7 2 0 9.00 2.30 -7 2 0 6.10 2.40 7 -1 0 102.59 9.10 7 -1 0 95.39 8.90 7 -1 0 103.49 9.40 7 -1 0 101.59 9.60 7 -1 0 105.79 9.30 -7 1 0 88.39 8.80 -7 1 0 113.89 9.30 -7 1 0 101.19 9.50 -7 1 0 93.09 9.40 7 0 0 -2.20 1.60 7 0 0 0.50 1.80 7 0 0 -1.30 1.70 7 0 0 -2.50 1.70 7 0 0 3.80 1.90 -7 0 0 -0.80 1.50 -7 0 0 2.30 1.60 -7 0 0 -0.30 2.30 7 1 0 109.09 9.90 7 1 0 88.69 9.50 7 1 0 104.79 9.40 7 1 0 102.89 9.60 7 1 0 116.69 9.60 -7 -1 0 101.29 9.60 -7 -1 0 84.49 9.50 -7 -1 0 123.39 9.60 -7 -1 0 101.99 9.70 -7 -1 0 101.89 9.60 7 2 0 6.80 1.90 7 2 0 6.80 2.30 7 2 0 1.60 2.10 7 2 0 4.90 1.90 7 2 0 10.60 2.80 -7 -2 0 2.50 3.20 -7 -2 0 4.40 1.70 -7 -2 0 8.10 2.20 -7 -2 0 6.80 2.40 -7 -2 0 5.70 2.20 7 3 0 36.90 5.30 7 3 0 37.80 4.70 7 3 0 40.60 4.40 -7 -3 0 30.50 4.90 -7 -3 0 39.70 4.90 -7 -3 0 43.70 4.60 7 4 0 9.00 2.80 7 4 0 3.90 2.90 7 4 0 9.00 2.40 -7 -4 0 3.90 2.60 -7 -4 0 7.60 3.10 -7 -4 0 10.10 2.60 7 5 0 77.29 9.30 7 5 0 72.29 7.60 7 5 0 99.79 9.40 -7 -5 0 84.49 7.70 -7 -5 0 61.49 8.50 -7 -5 0 82.39 8.30 7 6 0 0.50 2.20 7 6 0 2.80 4.10 7 6 0 -1.50 4.20 -7 -6 0 -0.10 3.20 -7 -6 0 5.70 4.00 -7 -6 0 -3.30 2.50 7 7 0 1.30 2.40 7 7 0 17.10 5.60 7 7 0 2.20 2.40 7 7 0 3.70 4.80 -7 -7 0 1.70 4.50 -7 -7 0 2.40 4.00 7 8 0 31.30 8.20 7 8 0 19.40 8.10 -7 -8 0 14.90 4.70 -7 -8 0 6.30 5.10 7 9 0 10.60 7.70 7 9 0 0.10 7.60 -7 -9 0 8.10 5.00 -7 -9 0 -9.50 6.00 7 10 0 -5.70 7.90 7 10 0 5.60 9.40 -7 -10 0 -8.10 5.70 -7 -10 0 -6.30 7.60 -7 -11 0 -12.70 8.10 8 -10 0 -5.20 6.10 8 -10 0 0.60 9.80 -8 10 0 12.80 7.70 8 -9 0 -3.60 4.50 8 -9 0 0.90 4.90 8 -9 0 -6.80 4.40 8 -9 0 2.70 7.70 -8 9 0 -1.30 6.50 8 -8 0 12.80 4.90 8 -8 0 23.20 7.10 -8 8 0 26.50 6.60 8 -7 0 -2.00 4.90 8 -7 0 1.30 3.70 8 -7 0 3.20 3.50 8 -7 0 3.90 3.10 -8 7 0 -2.60 4.20 -8 7 0 3.60 4.80 8 -6 0 55.79 7.10 8 -6 0 71.29 6.60 8 -6 0 48.70 6.90 8 -6 0 70.49 8.70 -8 6 0 70.79 7.30 -8 6 0 51.59 8.20 8 -5 0 27.10 4.50 8 -5 0 32.80 6.20 8 -5 0 26.90 4.10 8 -5 0 27.30 4.40 -8 5 0 35.30 6.10 -8 5 0 36.90 5.80 -8 5 0 40.90 4.90 8 -4 0 1.90 2.80 8 -4 0 3.70 2.10 8 -4 0 0.80 1.90 8 -4 0 -1.70 2.40 8 -4 0 2.50 1.90 -8 4 0 1.40 2.90 -8 4 0 3.80 2.40 8 -3 0 4.10 2.80 8 -3 0 1.00 2.60 8 -3 0 2.30 1.50 8 -3 0 5.00 2.50 8 -3 0 1.80 1.80 -8 3 0 0.30 1.40 -8 3 0 2.10 2.30 -8 3 0 -1.20 3.00 8 -2 0 86.59 8.80 8 -2 0 104.99 9.50 8 -2 0 91.69 8.50 8 -2 0 99.69 9.20 -8 2 0 102.09 9.10 -8 2 0 87.79 8.50 -8 2 0 89.49 9.00 -8 2 0 107.09 9.40 8 -1 0 1.80 1.30 8 -1 0 1.10 1.80 8 -1 0 0.80 2.00 8 -1 0 -0.70 2.30 8 -1 0 2.00 2.10 -8 1 0 1.50 2.10 -8 1 0 1.60 1.90 -8 1 0 -0.70 1.90 -8 1 0 0.70 2.60 -8 1 0 -0.60 1.10 8 0 0 50.59 5.50 8 0 0 56.99 5.60 8 0 0 40.20 5.20 8 0 0 51.19 5.60 8 0 0 59.39 5.90 -8 0 0 42.50 5.00 -8 0 0 57.99 5.80 -8 0 0 63.59 5.70 -8 0 0 44.40 5.60 -8 0 0 50.09 5.60 8 1 0 1.20 2.30 8 1 0 -0.90 2.10 8 1 0 0.60 1.40 -8 -1 0 4.00 2.10 -8 -1 0 4.90 1.90 -8 -1 0 2.10 2.20 -8 -1 0 2.80 2.70 8 2 0 80.29 8.40 8 2 0 106.79 9.10 8 2 0 85.69 8.30 -8 -2 0 97.19 8.60 -8 -2 0 75.89 8.50 -8 -2 0 90.99 8.50 -8 -2 0 79.69 9.60 8 3 0 -1.00 2.40 8 3 0 1.10 2.50 8 3 0 3.50 2.40 8 3 0 0.60 2.10 -8 -3 0 -0.40 2.10 -8 -3 0 3.50 2.40 -8 -3 0 1.70 2.60 -8 -3 0 0.30 1.90 8 4 0 -1.50 2.90 8 4 0 0.80 3.20 8 4 0 2.40 2.40 -8 -4 0 -1.60 2.50 -8 -4 0 -3.30 2.60 -8 -4 0 5.80 2.80 -8 -4 0 3.40 2.30 8 5 0 27.00 5.10 8 5 0 23.20 4.10 -8 -5 0 28.80 5.50 -8 -5 0 27.10 4.60 8 6 0 59.89 8.90 8 6 0 45.50 5.70 8 6 0 53.99 8.60 -8 -6 0 61.59 7.10 -8 -6 0 39.20 7.30 8 7 0 1.10 5.70 8 7 0 0.50 5.80 -8 -7 0 0.60 4.10 -8 -7 0 -3.30 4.70 8 8 0 10.70 7.40 8 8 0 18.10 6.80 -8 -8 0 13.30 4.80 8 9 0 -4.70 6.50 8 9 0 3.70 8.30 -8 -9 0 -6.20 5.10 8 10 0 11.70 9.50 8 10 0 -2.50 10.30 -8 -10 0 -11.30 8.00 9 -10 0 -2.10 10.70 9 -10 0 -2.80 6.50 -9 10 0 -1.50 8.40 9 -9 0 -9.30 4.90 9 -9 0 -8.20 8.20 9 -9 0 0.90 5.60 -9 9 0 -1.30 7.00 9 -8 0 5.90 4.10 9 -8 0 1.50 4.50 9 -8 0 13.30 8.10 -9 8 0 7.60 5.60 9 -7 0 3.40 3.80 9 -7 0 -3.10 3.10 9 -7 0 5.90 5.70 -9 7 0 -2.20 4.60 -9 7 0 10.30 5.80 9 -6 0 1.80 4.70 9 -6 0 1.50 3.20 9 -6 0 1.00 4.80 9 -6 0 2.00 3.10 -9 6 0 0.20 4.30 -9 6 0 3.00 4.00 9 -5 0 5.80 2.60 9 -5 0 1.10 2.90 9 -5 0 5.40 2.90 9 -5 0 2.90 3.80 9 -5 0 1.30 3.90 -9 5 0 4.70 3.10 -9 5 0 1.70 4.00 9 -4 0 10.80 2.30 9 -4 0 11.70 2.80 9 -4 0 10.60 3.80 9 -4 0 9.70 2.70 9 -4 0 9.70 3.80 -9 4 0 8.60 3.60 -9 4 0 10.60 3.10 9 -3 0 122.69 10.70 9 -3 0 134.79 11.40 9 -3 0 120.99 11.30 9 -3 0 110.39 10.20 -9 3 0 98.59 10.20 -9 3 0 114.09 11.20 -9 3 0 104.19 10.60 9 -2 0 2.70 2.50 9 -2 0 6.70 2.80 9 -2 0 0.20 2.30 9 -2 0 4.40 1.60 -9 2 0 2.30 2.30 -9 2 0 0.30 3.00 -9 2 0 1.80 1.30 -9 2 0 5.80 2.80 9 -1 0 63.79 6.70 9 -1 0 81.79 7.80 9 -1 0 73.89 7.60 -9 1 0 69.99 7.30 -9 1 0 83.09 7.50 -9 1 0 56.49 7.30 -9 1 0 74.49 6.60 9 0 0 0.70 2.30 9 0 0 0.70 1.60 -9 0 0 0.70 2.00 -9 0 0 -3.50 2.70 -9 0 0 -2.40 2.20 -9 0 0 -1.10 1.30 9 1 0 74.79 7.70 9 1 0 84.19 8.70 -9 -1 0 89.49 8.20 -9 -1 0 88.29 8.20 -9 -1 0 75.39 8.10 -9 -1 0 76.39 8.10 9 2 0 7.10 3.10 9 2 0 2.00 2.10 9 2 0 3.80 2.50 -9 -2 0 4.10 2.60 -9 -2 0 0.20 2.30 -9 -2 0 1.10 2.70 -9 -2 0 0.20 2.20 9 3 0 105.69 11.00 9 3 0 106.99 11.40 -9 -3 0 102.39 10.80 -9 -3 0 123.99 11.00 -9 -3 0 121.19 10.90 9 4 0 8.60 4.10 9 4 0 16.10 4.00 -9 -4 0 18.20 3.90 -9 -4 0 12.30 4.00 -9 -4 0 9.70 3.30 9 5 0 5.30 4.10 9 5 0 7.50 4.50 9 5 0 -0.40 4.40 -9 -5 0 1.30 3.10 -9 -5 0 7.40 3.50 -9 -5 0 2.10 3.40 9 6 0 4.20 5.10 9 6 0 -2.40 5.00 -9 -6 0 1.90 3.70 -9 -6 0 -6.10 4.20 -9 -6 0 0.80 3.60 9 7 0 0.80 5.80 9 7 0 -1.10 5.80 -9 -7 0 -7.20 5.50 -9 -7 0 -0.10 4.20 -9 -7 0 -1.10 3.60 9 8 0 -2.90 7.60 9 8 0 16.70 7.60 -9 -8 0 6.20 5.40 -9 -8 0 11.50 9.90 9 9 0 -2.40 7.50 9 9 0 0.00 9.80 -9 -9 0 -7.60 9.10 -9 -9 0 -13.20 7.50 9 10 0 17.00 9.90 9 10 0 12.50 12.30 -9 -10 0 -4.10 9.20 -9 -10 0 2.60 7.60 10 -10 0 23.40 12.70 10 -9 0 13.80 10.80 10 -9 0 7.70 6.40 -10 9 0 19.40 8.50 10 -8 0 -0.50 4.10 10 -8 0 -0.80 9.70 10 -8 0 3.80 4.70 10 -8 0 -11.60 8.10 -10 8 0 15.90 6.00 -10 8 0 11.60 7.10 10 -7 0 10.50 6.40 10 -7 0 -1.20 3.70 10 -7 0 13.50 4.10 10 -7 0 2.60 6.20 -10 7 0 4.00 5.30 10 -6 0 10.00 3.40 10 -6 0 7.80 5.50 10 -6 0 12.30 5.10 -10 6 0 14.80 5.10 -10 6 0 7.50 3.80 10 -5 0 6.00 2.70 10 -5 0 7.70 4.30 10 -5 0 8.60 4.70 10 -5 0 2.30 2.90 -10 5 0 3.00 4.60 -10 5 0 6.40 3.30 10 -4 0 -3.40 3.60 10 -4 0 0.30 3.80 10 -4 0 -0.60 2.00 -10 4 0 0.20 3.30 -10 4 0 5.40 3.70 10 -3 0 0.90 3.20 10 -3 0 1.90 1.90 10 -3 0 4.50 3.50 -10 3 0 3.20 2.90 -10 3 0 2.50 1.90 -10 3 0 5.80 3.70 10 -2 0 34.60 5.40 10 -2 0 22.90 3.80 10 -2 0 36.70 5.10 -10 2 0 31.10 5.10 -10 2 0 32.00 4.50 -10 2 0 25.40 3.50 10 -1 0 24.10 4.30 10 -1 0 17.70 3.70 10 -1 0 15.80 2.90 -10 1 0 17.60 2.80 -10 1 0 15.80 3.50 -10 1 0 12.00 4.00 -10 1 0 22.10 3.60 10 0 0 18.70 3.80 10 0 0 24.00 3.80 10 0 0 21.00 3.90 -10 0 0 19.10 3.50 -10 0 0 22.90 3.20 -10 0 0 15.00 3.80 -10 0 0 17.20 3.50 10 1 0 18.30 3.40 10 1 0 26.20 4.60 10 1 0 17.30 3.50 -10 -1 0 23.70 4.30 -10 -1 0 16.00 3.60 -10 -1 0 13.40 3.40 10 2 0 39.30 5.90 10 2 0 34.50 4.70 10 2 0 33.90 5.40 -10 -2 0 27.80 5.40 -10 -2 0 29.90 5.10 -10 -2 0 34.10 5.40 -10 -2 0 36.20 5.20 10 3 0 2.90 3.20 10 3 0 2.20 3.40 -10 -3 0 9.60 3.90 -10 -3 0 3.80 3.50 -10 -3 0 0.20 2.80 -10 -3 0 5.20 3.60 10 4 0 -2.80 3.40 10 4 0 2.90 3.60 -10 -4 0 1.60 3.30 -10 -4 0 3.70 3.90 -10 -4 0 -1.90 3.70 10 5 0 3.50 4.40 10 5 0 3.30 4.50 -10 -5 0 2.00 4.10 -10 -5 0 5.60 3.70 -10 -5 0 0.10 4.20 10 6 0 16.70 6.10 10 6 0 18.10 5.90 -10 -6 0 7.90 4.40 -10 -6 0 12.30 4.40 -10 -6 0 13.10 5.60 10 7 0 8.70 6.40 10 7 0 4.90 6.90 -10 -7 0 7.30 5.70 -10 -7 0 10.30 4.60 -10 -7 0 7.70 4.80 10 8 0 -4.10 6.40 10 8 0 -6.60 8.10 -10 -8 0 -4.30 5.30 -10 -8 0 -0.50 6.30 10 9 0 -14.10 8.00 -10 -9 0 -11.40 7.10 -10 -9 0 1.60 6.30 -10 -10 0 -2.40 8.80 11 -9 0 -8.40 6.10 11 -9 0 4.40 10.80 11 -9 0 -7.90 9.50 -11 9 0 -7.50 8.40 11 -8 0 -0.70 4.90 11 -8 0 1.40 8.30 11 -8 0 6.10 7.90 11 -8 0 -0.40 5.00 -11 8 0 10.60 6.90 11 -7 0 -3.30 7.20 11 -7 0 -1.40 6.00 11 -7 0 3.30 4.00 11 -7 0 6.90 4.20 -11 7 0 -4.10 5.90 11 -6 0 -3.60 3.30 11 -6 0 1.30 5.80 11 -6 0 -3.30 4.90 -11 6 0 1.90 4.00 -11 6 0 -1.50 5.00 11 -5 0 3.80 5.40 11 -5 0 -1.80 4.00 11 -5 0 6.30 3.10 11 -5 0 4.20 2.90 -11 5 0 1.70 3.50 -11 5 0 -0.40 4.60 11 -4 0 22.60 5.60 11 -4 0 16.20 5.20 11 -4 0 13.40 2.90 11 -4 0 15.00 5.90 -11 4 0 23.60 4.40 -11 4 0 16.10 4.70 11 -3 0 4.50 2.30 11 -3 0 -1.80 3.20 11 -3 0 -1.00 3.60 -11 3 0 -3.30 2.90 -11 3 0 -1.10 3.60 11 -2 0 31.90 5.30 11 -2 0 30.90 5.30 11 -2 0 26.10 4.10 -11 2 0 29.40 4.90 -11 2 0 30.00 4.90 11 -1 0 18.20 3.90 11 -1 0 13.40 3.10 11 -1 0 12.20 3.70 -11 1 0 17.80 2.90 -11 1 0 10.10 3.60 -11 1 0 7.50 3.40 11 0 0 2.10 2.60 11 0 0 -0.10 2.80 11 0 0 6.20 2.50 -11 0 0 -1.80 2.90 -11 0 0 -2.50 3.10 -11 0 0 -0.80 3.70 11 1 0 21.90 4.80 11 1 0 17.00 3.70 11 1 0 17.80 3.70 -11 -1 0 23.40 4.30 -11 -1 0 21.10 3.70 -11 -1 0 23.50 4.40 11 2 0 33.40 6.30 11 2 0 31.00 5.50 -11 -2 0 26.40 5.20 -11 -2 0 30.80 4.70 -11 -2 0 23.90 5.00 -11 -2 0 31.60 6.10 11 3 0 1.90 3.30 11 3 0 -0.60 3.70 -11 -3 0 -1.60 3.40 -11 -3 0 3.50 4.10 -11 -3 0 -0.20 3.30 11 4 0 17.30 5.00 11 4 0 12.20 4.60 -11 -4 0 13.40 4.30 -11 -4 0 18.30 4.80 -11 -4 0 23.00 5.00 11 5 0 2.20 4.70 -11 -5 0 5.30 4.20 -11 -5 0 -0.60 4.60 -11 -5 0 0.00 5.20 11 6 0 3.50 6.10 11 6 0 -1.60 5.00 -11 -6 0 -4.40 5.30 -11 -6 0 0.60 4.80 -11 -6 0 0.90 4.20 11 7 0 -7.90 7.10 11 7 0 -10.20 5.50 -11 -7 0 -3.00 5.10 -11 -7 0 2.60 6.30 -11 -7 0 8.50 5.60 11 8 0 2.20 8.30 11 8 0 0.50 8.10 -11 -8 0 -10.50 6.00 -11 -8 0 20.40 8.70 11 9 0 -3.80 10.90 11 9 0 8.50 10.60 -11 -9 0 25.00 10.00 -11 -9 0 -1.60 6.80 12 -9 0 21.00 12.10 12 -9 0 13.30 10.40 -12 9 0 -8.70 12.30 12 -8 0 35.80 10.30 12 -8 0 10.50 8.90 12 -8 0 -0.20 6.80 -12 8 0 10.90 7.80 12 -7 0 27.60 12.90 12 -7 0 6.90 5.00 12 -7 0 12.10 4.70 12 -7 0 4.70 7.30 -12 7 0 0.60 6.90 12 -6 0 17.00 7.30 12 -6 0 14.00 4.40 12 -6 0 3.50 6.10 -12 6 0 24.00 6.20 12 -5 0 7.30 3.50 12 -5 0 4.10 5.70 12 -5 0 1.10 4.80 -12 5 0 -0.30 4.70 -12 5 0 6.00 4.10 12 -4 0 12.80 4.50 12 -4 0 8.20 5.30 12 -4 0 7.90 2.70 12 -4 0 9.60 3.00 -12 4 0 8.40 4.30 -12 4 0 11.90 4.50 12 -3 0 0.70 2.50 12 -3 0 -1.50 4.30 12 -3 0 9.00 4.40 -12 3 0 3.20 3.40 -12 3 0 0.60 3.50 12 -2 0 -2.80 2.50 12 -2 0 -0.70 3.70 12 -2 0 6.70 3.70 -12 2 0 -0.20 3.50 -12 2 0 -4.80 3.70 12 -1 0 23.80 5.10 12 -1 0 25.20 4.60 12 -1 0 22.90 4.70 -12 1 0 25.70 4.70 -12 1 0 12.20 4.30 12 0 0 136.49 11.80 12 0 0 92.69 11.60 12 0 0 99.19 10.70 -12 0 0 107.89 11.30 -12 0 0 125.19 10.60 12 1 0 31.30 5.00 12 1 0 30.50 5.50 12 1 0 24.40 4.30 -12 -1 0 24.20 5.10 -12 -1 0 15.90 4.60 -12 -1 0 31.30 4.50 12 2 0 3.40 4.20 12 2 0 1.10 3.60 -12 -2 0 -5.50 3.50 -12 -2 0 1.50 3.80 -12 -2 0 2.60 4.10 12 3 0 13.10 4.80 12 3 0 5.10 4.50 -12 -3 0 6.60 3.80 -12 -3 0 9.70 5.10 -12 -3 0 14.10 4.20 12 4 0 7.10 5.60 12 4 0 6.90 5.30 -12 -4 0 10.50 5.20 -12 -4 0 10.90 5.10 -12 -4 0 15.80 4.90 12 5 0 3.50 5.10 12 5 0 9.00 5.50 -12 -5 0 -0.30 4.50 -12 -5 0 0.50 4.50 -12 -5 0 8.00 5.50 12 6 0 19.70 7.20 -12 -6 0 17.70 6.60 -12 -6 0 15.60 5.70 -12 -6 0 11.00 6.00 12 7 0 -0.80 7.90 12 7 0 -2.40 7.40 -12 -7 0 8.50 6.50 -12 -7 0 9.40 6.00 12 8 0 6.20 9.30 12 8 0 7.50 8.50 -12 -8 0 0.00 6.70 -12 -8 0 9.50 8.20 12 9 0 11.80 9.80 -12 -9 0 4.30 9.80 -12 -9 0 -10.80 7.30 13 -8 0 -16.60 9.80 13 -8 0 -17.50 8.80 -13 8 0 10.00 8.50 13 -7 0 -12.30 6.90 13 -7 0 5.30 5.60 13 -7 0 -14.40 8.40 -13 7 0 -1.30 9.30 13 -6 0 0.90 4.10 13 -6 0 -1.40 7.50 13 -6 0 -2.40 6.30 -13 6 0 13.70 6.70 -13 6 0 20.40 5.10 13 -5 0 6.30 5.50 13 -5 0 22.00 6.90 13 -5 0 12.90 4.00 -13 5 0 0.00 5.00 -13 5 0 16.10 5.20 13 -4 0 12.70 5.50 13 -4 0 -0.20 3.10 13 -4 0 -1.80 5.40 -13 4 0 4.30 4.20 -13 4 0 7.40 4.40 13 -3 0 11.40 5.50 13 -3 0 12.10 5.10 -13 3 0 7.30 3.30 -13 3 0 16.50 4.50 13 -2 0 10.30 5.20 13 -2 0 3.20 3.90 13 -2 0 -0.80 2.70 -13 2 0 1.60 4.30 -13 2 0 2.50 3.50 13 -1 0 21.60 4.80 13 -1 0 21.60 5.40 13 -1 0 15.90 3.80 -13 1 0 22.00 4.00 -13 1 0 18.20 4.80 13 0 0 -3.80 3.00 13 0 0 -3.40 3.80 13 0 0 1.90 4.40 -13 0 0 -2.50 2.50 -13 0 0 1.10 3.70 -13 0 0 2.00 4.40 13 1 0 29.60 5.90 13 1 0 22.00 4.80 -13 -1 0 14.00 4.70 -13 -1 0 6.40 3.40 -13 -1 0 15.20 4.00 13 2 0 6.50 4.60 13 2 0 8.60 4.60 -13 -2 0 11.30 4.40 -13 -2 0 4.00 4.60 -13 -2 0 5.80 4.20 13 3 0 15.40 5.50 13 3 0 19.20 5.90 -13 -3 0 6.80 4.90 -13 -3 0 14.20 4.70 -13 -3 0 13.90 5.50 13 4 0 1.40 4.80 13 4 0 2.10 5.60 -13 -4 0 10.50 5.10 -13 -4 0 7.10 5.40 -13 -4 0 5.60 4.60 13 5 0 14.60 6.60 -13 -5 0 10.80 7.50 -13 -5 0 15.70 6.50 -13 -5 0 7.80 6.30 13 6 0 17.70 7.50 13 6 0 -2.80 6.00 -13 -6 0 4.40 6.50 -13 -6 0 0.30 5.80 -13 -6 0 -5.90 5.80 13 7 0 -3.60 8.80 13 7 0 2.60 8.70 -13 -7 0 10.20 7.60 -13 -7 0 -5.00 6.90 -13 -7 0 5.90 6.40 13 8 0 12.30 8.90 -13 -8 0 10.00 7.90 -13 -8 0 17.10 9.80 14 -7 0 3.30 6.80 14 -7 0 7.50 10.90 14 -7 0 -6.00 8.90 -14 7 0 -5.00 8.30 14 -6 0 11.90 7.80 -14 6 0 1.50 6.70 -14 6 0 16.40 5.90 14 -5 0 2.10 7.80 14 -5 0 9.80 7.00 -14 5 0 -1.90 5.00 -14 5 0 -1.00 5.20 14 -4 0 -2.50 3.40 14 -4 0 1.40 5.60 14 -4 0 -10.50 7.10 -14 4 0 4.00 4.80 -14 4 0 -2.30 4.80 14 -3 0 15.40 6.20 14 -3 0 16.90 5.80 -14 3 0 17.50 5.40 -14 3 0 9.60 4.80 14 -2 0 1.00 4.70 14 -2 0 -6.80 5.10 -14 2 0 2.40 4.80 -14 2 0 4.70 4.00 14 -1 0 28.10 5.90 14 -1 0 23.60 6.30 -14 1 0 33.60 5.10 -14 1 0 21.60 5.70 -14 1 0 38.20 6.40 14 0 0 -3.30 4.10 14 0 0 -4.70 4.60 -14 0 0 1.20 4.30 -14 0 0 -2.80 3.00 -14 0 0 -5.10 4.50 14 1 0 36.40 7.00 14 1 0 23.10 5.80 -14 -1 0 34.50 6.70 -14 -1 0 30.30 5.60 14 2 0 8.40 4.90 14 2 0 0.60 5.60 -14 -2 0 -0.70 4.20 -14 -2 0 8.80 5.00 -14 -2 0 2.30 3.90 14 3 0 17.50 6.00 14 3 0 10.00 6.00 -14 -3 0 16.00 5.60 -14 -3 0 9.30 5.10 -14 -3 0 9.20 5.40 14 4 0 3.30 6.70 14 4 0 -9.80 7.90 -14 -4 0 -5.70 6.00 -14 -4 0 -0.40 5.20 -14 -4 0 0.00 6.60 14 5 0 7.60 6.80 14 5 0 4.90 6.90 -14 -5 0 7.80 5.80 -14 -5 0 23.00 7.60 -14 -5 0 3.50 6.10 14 6 0 2.00 7.80 14 6 0 -0.80 8.60 -14 -6 0 -3.90 7.00 -14 -6 0 -2.80 5.70 14 7 0 8.90 8.90 14 7 0 -7.10 9.80 -14 -7 0 7.30 8.50 -14 -7 0 6.20 6.80 -14 -7 0 20.40 9.60 -15 7 0 10.50 9.90 15 -6 0 26.40 8.90 15 -6 0 -14.00 10.20 -15 6 0 8.10 6.80 -15 6 0 -3.60 6.40 15 -5 0 0.70 7.10 -15 5 0 6.30 6.00 -15 5 0 0.90 4.70 15 -4 0 11.80 7.70 15 -4 0 7.80 6.70 -15 4 0 2.50 5.40 -15 4 0 5.70 5.90 15 -3 0 1.30 6.70 15 -3 0 7.80 6.80 -15 3 0 7.10 5.80 -15 3 0 -9.40 5.00 15 -2 0 2.00 6.10 15 -2 0 10.00 6.40 -15 2 0 -4.00 5.00 15 -1 0 5.50 5.10 15 -1 0 7.10 5.50 -15 1 0 4.50 6.20 -15 1 0 11.60 5.70 15 0 0 0.10 5.60 15 0 0 0.80 4.70 -15 0 0 -1.60 4.90 -15 0 0 0.60 4.50 -15 0 0 0.80 3.30 15 1 0 3.80 5.00 15 1 0 14.10 6.80 -15 -1 0 3.90 3.90 -15 -1 0 11.20 4.80 15 2 0 5.50 5.40 -15 -2 0 0.70 4.10 -15 -2 0 5.70 4.10 -15 -2 0 3.20 8.70 15 3 0 3.60 5.90 15 3 0 -3.40 6.20 -15 -3 0 11.60 5.80 -15 -3 0 -3.00 4.90 -15 -3 0 5.90 5.10 15 4 0 -4.00 7.10 15 4 0 -0.20 6.20 -15 -4 0 -8.00 5.90 -15 -4 0 9.80 6.30 15 5 0 -0.40 7.80 15 5 0 3.20 8.10 -15 -5 0 11.60 6.90 -15 -5 0 -8.80 6.50 -15 -5 0 16.60 8.60 15 6 0 24.60 9.80 15 6 0 6.50 8.90 -15 -6 0 1.50 8.00 -15 -6 0 0.80 7.10 -15 -6 0 -0.40 8.60 -16 6 0 -10.70 6.10 16 -5 0 -6.50 8.30 16 -5 0 3.50 11.90 -16 5 0 -4.80 7.60 -16 5 0 0.70 7.50 16 -4 0 -2.00 9.20 16 -4 0 3.40 8.10 -16 4 0 8.20 6.40 -16 4 0 4.80 6.80 16 -3 0 -2.20 6.10 16 -3 0 -0.90 8.00 -16 3 0 -4.70 6.90 -16 3 0 -1.10 4.80 16 -2 0 -11.90 6.40 16 -2 0 -1.90 5.80 -16 2 0 9.20 5.00 16 -1 0 -6.00 5.90 16 -1 0 -8.90 5.50 -16 1 0 -1.70 10.70 -16 1 0 0.80 4.90 16 0 0 2.20 5.50 16 0 0 3.20 6.40 -16 0 0 4.60 3.80 -16 0 0 3.20 5.20 -16 0 0 2.20 5.90 16 1 0 2.00 6.90 16 1 0 2.90 6.20 -16 -1 0 -2.90 5.80 -16 -1 0 3.90 5.40 16 2 0 3.80 6.70 16 2 0 -3.20 7.00 -16 -2 0 3.10 4.90 -16 -2 0 3.20 6.30 -16 -2 0 -5.60 5.60 16 3 0 -4.50 6.40 -16 -3 0 1.40 5.90 -16 -3 0 -4.20 5.30 -16 -3 0 11.30 6.40 16 4 0 7.60 8.50 16 4 0 -0.90 7.10 -16 -4 0 0.30 7.20 -16 -4 0 6.40 7.40 -16 -4 0 -1.00 6.20 16 5 0 14.60 9.30 16 5 0 -1.40 9.10 -16 -5 0 4.10 7.70 -16 -5 0 -12.30 7.70 -16 -6 0 13.40 10.80 17 -4 0 9.00 8.40 -17 4 0 3.10 6.80 -17 4 0 3.60 7.80 17 -3 0 -12.40 9.10 17 -3 0 9.40 8.20 -17 3 0 -3.30 5.70 -17 3 0 -7.60 7.60 17 -2 0 -11.80 6.80 17 -2 0 9.40 8.40 -17 2 0 1.40 6.70 -17 2 0 -10.60 5.30 17 -1 0 0.40 7.50 -17 1 0 -9.80 6.10 -17 1 0 -3.50 5.80 17 0 0 1.90 6.70 17 0 0 -1.20 6.80 -17 0 0 8.80 6.70 -17 0 0 -0.20 5.90 17 1 0 12.30 7.70 17 1 0 6.80 7.20 -17 -1 0 -6.30 7.10 -17 -1 0 -4.70 5.30 17 2 0 9.90 7.80 17 2 0 14.50 8.30 -17 -2 0 4.00 6.30 -17 -2 0 10.40 7.30 -17 -3 0 1.30 5.80 -17 -3 0 2.50 5.80 -17 -3 0 0.40 7.30 17 4 0 -12.00 8.30 17 4 0 -5.40 10.10 -17 -4 0 3.10 9.20 -17 -4 0 10.50 7.80 18 -2 0 -1.60 8.50 18 -2 0 11.60 9.80 -18 2 0 2.70 5.60 -18 2 0 7.40 8.10 18 -1 0 3.70 8.50 18 -1 0 -14.30 7.90 -18 1 0 -5.60 6.10 -18 1 0 -4.10 7.80 18 0 0 -12.30 7.70 18 0 0 19.90 9.20 -18 0 0 5.30 7.90 18 1 0 6.20 8.10 18 1 0 -10.20 9.30 -18 -1 0 10.90 6.50 -18 -1 0 -2.30 6.90 18 2 0 19.40 8.80 -18 -2 0 -0.80 7.10 -18 -2 0 9.10 8.00 -18 -3 1 -0.70 6.20 -18 -2 1 0.60 7.50 -18 -2 1 12.90 8.30 18 2 -1 11.10 10.20 18 2 -1 3.30 8.50 -18 -1 1 1.90 6.30 -18 -1 1 11.90 8.10 18 1 -1 2.50 9.00 18 1 -1 -2.50 8.90 -18 0 1 24.20 8.00 -18 0 1 4.80 6.30 18 0 -1 -2.10 8.20 18 0 -1 11.30 8.50 -18 1 1 7.70 6.70 -18 1 1 -15.20 7.50 18 -1 -1 5.60 8.80 18 -1 -1 -14.40 7.80 -18 2 1 -2.70 8.30 -18 2 1 5.40 6.30 18 -2 -1 12.00 11.10 -18 3 1 1.10 6.50 -17 -4 1 0.60 7.10 -17 -4 1 20.10 8.20 -17 -4 1 -5.00 8.60 17 4 -1 12.00 10.30 17 4 -1 -12.90 7.70 -17 -3 1 -1.10 5.50 -17 -3 1 14.30 6.70 17 3 -1 1.30 8.30 17 3 -1 -9.60 9.00 -17 -2 1 -5.20 6.00 -17 -2 1 -4.80 7.10 17 2 -1 3.50 7.40 17 2 -1 0.70 8.70 -17 -1 1 3.70 5.50 -17 -1 1 -2.10 6.50 17 1 -1 2.10 7.10 17 1 -1 7.90 7.40 -17 0 1 -0.30 5.50 -17 0 1 -3.00 6.60 17 0 -1 8.80 7.90 17 0 -1 6.20 6.90 -17 1 1 2.80 5.10 -17 1 1 -1.60 6.30 17 -1 -1 -3.50 7.50 17 -1 -1 -9.40 6.30 -17 2 1 1.40 5.80 -17 2 1 -8.30 6.40 17 -2 -1 -11.00 7.10 17 -2 -1 8.40 8.10 -17 3 1 1.50 6.30 -17 3 1 -6.20 6.80 17 -3 -1 6.80 10.00 17 -3 -1 21.10 7.90 -17 4 1 -3.20 6.00 -17 4 1 -1.20 7.00 17 -4 -1 -6.30 7.80 17 -4 -1 -7.50 11.00 -16 -6 1 -0.40 9.60 -16 -6 1 4.20 8.10 -16 -6 1 2.30 8.30 16 6 -1 8.50 10.30 -16 -5 1 -1.00 7.90 -16 -5 1 8.00 9.50 -16 -5 1 6.40 7.40 16 5 -1 12.70 10.10 16 5 -1 -9.70 8.00 -16 -4 1 -5.30 6.60 -16 -4 1 1.90 7.00 16 4 -1 7.40 9.00 16 4 -1 0.30 8.00 -16 -3 1 0.40 5.20 -16 -3 1 10.40 6.50 -16 -3 1 -4.70 5.60 16 3 -1 4.70 6.60 16 3 -1 11.10 7.80 -16 -2 1 8.60 4.60 -16 -2 1 3.10 6.10 -16 -2 1 12.80 5.90 16 2 -1 5.60 6.50 16 2 -1 1.40 6.30 -16 -1 1 0.00 4.90 -16 -1 1 10.10 3.90 -16 -1 1 -6.00 6.10 16 1 -1 6.20 6.60 16 1 -1 -0.20 5.50 -16 0 1 0.40 7.50 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-4 1 8.90 5.50 14 4 -1 15.40 6.60 14 4 -1 -1.10 8.20 -14 -3 1 7.70 4.70 -14 -3 1 5.20 5.00 -14 -3 1 -2.20 4.80 14 3 -1 6.20 5.40 14 3 -1 -0.20 5.60 -14 -2 1 11.20 4.50 -14 -2 1 10.10 4.80 -14 -2 1 15.80 5.30 14 2 -1 16.20 5.80 14 2 -1 29.50 6.60 -14 -1 1 1.30 3.70 -14 -1 1 -1.20 3.20 -14 -1 1 -1.20 4.70 14 1 -1 -4.90 4.40 14 1 -1 0.40 4.20 -14 0 1 -2.10 4.40 -14 0 1 -4.80 4.90 -14 0 1 -3.90 2.90 14 0 -1 2.00 4.70 14 0 -1 -3.30 4.40 -14 1 1 -3.90 4.40 -14 1 1 1.20 4.70 14 -1 -1 -1.30 5.00 14 -1 -1 4.90 4.40 -14 2 1 12.20 5.00 -14 2 1 9.20 4.80 14 -2 -1 17.80 5.70 14 -2 -1 12.60 5.80 -14 3 1 2.60 4.30 -14 3 1 5.20 4.70 14 -3 -1 8.30 6.10 14 -3 -1 13.40 5.10 -14 4 1 9.00 4.70 -14 4 1 3.00 4.00 14 -4 -1 1.00 6.80 14 -4 -1 7.00 6.70 -14 5 1 4.70 5.00 14 -5 -1 1.10 6.30 14 -5 -1 -12.70 7.20 -14 6 1 1.00 6.20 -14 6 1 18.10 6.00 14 -6 -1 13.40 11.00 14 -6 -1 9.30 7.30 -14 7 1 -5.20 8.50 14 -7 -1 16.80 10.60 -13 -8 1 2.10 7.30 -13 -8 1 -5.80 8.50 13 8 -1 0.90 9.30 13 8 -1 3.10 11.00 -13 -7 1 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-4 185.98 16.20 6 -7 -4 170.08 16.30 6 -7 -4 161.58 17.30 -6 8 4 3.20 4.00 -6 8 4 -1.10 5.20 6 -8 -4 6.00 4.00 6 -8 -4 -5.80 4.90 -6 9 4 4.20 5.60 6 -9 -4 2.00 5.00 6 -9 -4 11.00 6.70 -6 10 4 -3.90 7.10 6 -10 -4 11.40 6.30 6 -10 -4 7.00 7.50 -6 11 4 1.80 7.20 6 -11 -4 34.40 10.40 6 -11 -4 -4.00 7.90 -5 -11 4 7.00 7.80 -5 -11 4 13.40 7.90 5 11 -4 -1.10 11.10 5 11 -4 26.30 12.00 -5 -10 4 -6.60 6.10 -5 -10 4 9.80 6.10 5 10 -4 6.90 9.00 5 10 -4 8.70 8.30 -5 -9 4 10.70 5.40 5 9 -4 12.10 7.90 5 9 -4 6.60 7.80 -5 -8 4 4.80 4.60 -5 -8 4 10.20 5.10 5 8 -4 12.80 6.10 5 8 -4 1.50 5.90 -5 -7 4 70.69 8.20 -5 -7 4 68.99 8.20 -5 -7 4 55.39 5.80 5 7 -4 57.39 9.50 5 7 -4 63.19 9.30 5 7 -4 53.79 5.90 -5 -6 4 25.30 4.30 -5 -6 4 18.40 3.40 -5 -6 4 23.00 4.40 5 6 -4 25.10 4.90 5 6 -4 23.80 3.50 5 6 -4 27.90 5.20 -5 -5 4 7.50 3.00 -5 -5 4 7.40 3.10 -5 -5 4 10.10 2.40 5 5 -4 11.50 2.30 5 5 -4 6.00 3.20 5 5 -4 9.90 3.40 -5 -4 4 168.38 14.80 -5 -4 4 146.39 14.30 -5 -4 4 163.78 14.60 -5 -4 4 167.98 14.80 5 4 -4 171.38 14.60 5 4 -4 165.68 14.30 5 4 -4 149.79 15.00 5 4 -4 166.28 15.00 -5 -3 4 79.89 7.70 -5 -3 4 82.49 8.00 -5 -3 4 78.99 8.10 -5 -3 4 90.99 8.40 -5 -3 4 83.39 8.10 5 3 -4 83.19 8.00 5 3 -4 81.79 8.30 5 3 -4 88.69 7.70 5 3 -4 76.79 7.80 -5 -2 4 6.20 1.90 -5 -2 4 3.60 1.60 -5 -2 4 2.00 1.50 -5 -2 4 7.40 1.60 5 2 -4 5.40 1.70 5 2 -4 4.40 1.80 5 2 -4 3.90 2.10 5 2 -4 5.00 1.50 -5 -1 4 48.50 4.70 -5 -1 4 51.49 5.20 -5 -1 4 51.59 5.10 -5 -1 4 47.20 5.10 -5 -1 4 44.50 5.20 5 1 -4 57.99 5.10 5 1 -4 51.39 5.10 5 1 -4 47.20 4.70 5 1 -4 55.39 5.30 5 1 -4 52.39 5.00 -5 0 4 1.00 0.70 -5 0 4 -1.50 1.50 -5 0 4 0.80 0.60 -5 0 4 0.00 1.70 -5 0 4 -1.80 1.20 -5 0 4 -0.50 1.20 5 0 -4 1.80 1.20 5 0 -4 0.00 1.20 5 0 -4 1.10 1.50 5 0 -4 0.10 1.50 -5 1 4 55.19 4.90 -5 1 4 54.49 5.30 5 -1 -4 48.20 5.40 5 -1 -4 50.99 4.90 5 -1 -4 48.50 5.10 5 -1 -4 51.19 5.40 5 -1 -4 50.79 5.20 -5 2 4 2.80 1.80 -5 2 4 4.20 1.10 5 -2 -4 4.40 1.20 5 -2 -4 5.40 1.90 5 -2 -4 3.50 1.60 -5 3 4 82.69 8.30 -5 3 4 88.19 7.50 -5 3 4 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4 1.50 4.30 4 8 -4 -4.70 5.60 4 8 -4 -3.60 5.60 -4 -7 4 91.99 9.50 -4 -7 4 122.49 11.20 -4 -7 4 121.49 11.30 4 7 -4 114.09 12.20 4 7 -4 99.39 12.40 -4 -6 4 3.80 2.80 -4 -6 4 -4.60 2.90 -4 -6 4 2.50 1.70 4 6 -4 -0.30 1.80 4 6 -4 0.30 3.30 4 6 -4 2.60 3.70 -4 -5 4 141.39 13.60 -4 -5 4 166.98 14.30 -4 -5 4 160.08 14.60 -4 -5 4 156.88 14.20 4 5 -4 160.78 14.80 4 5 -4 145.99 14.80 4 5 -4 156.08 13.60 -4 -4 4 4.30 2.30 -4 -4 4 2.20 2.20 -4 -4 4 0.60 2.20 -4 -4 4 0.50 1.60 -4 -4 4 -0.20 2.20 4 4 -4 -0.60 1.80 4 4 -4 -0.40 1.50 4 4 -4 -1.40 2.10 4 4 -4 1.80 1.90 4 4 -4 0.20 2.90 -4 -3 4 33.40 4.50 -4 -3 4 43.20 4.00 -4 -3 4 28.30 4.20 -4 -3 4 37.00 4.40 4 3 -4 33.50 4.10 4 3 -4 39.00 3.90 4 3 -4 33.20 3.90 4 3 -4 42.50 5.40 -4 -2 4 72.49 7.40 -4 -2 4 88.19 7.30 -4 -2 4 78.59 7.60 -4 -2 4 81.19 7.40 4 2 -4 78.39 7.30 4 2 -4 81.29 7.50 4 2 -4 82.29 7.40 4 2 -4 76.89 7.50 4 2 -4 84.29 7.70 -4 -1 4 73.19 7.00 -4 -1 4 76.09 7.00 -4 -1 4 85.09 6.80 4 1 -4 72.39 6.70 4 1 -4 73.49 7.00 4 1 -4 78.09 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25.20 4.40 2 4 -10 18.80 3.60 2 4 -10 20.60 4.30 -2 -3 10 10.30 3.50 -2 -3 10 16.20 2.50 -2 -3 10 9.80 3.40 -2 -3 10 14.90 3.30 2 3 -10 15.70 2.40 2 3 -10 20.60 3.60 2 3 -10 10.80 3.30 -2 -2 10 3.40 2.40 -2 -2 10 2.80 2.40 -2 -2 10 1.50 2.90 -2 -2 10 5.60 2.70 2 2 -10 4.20 2.10 2 2 -10 4.50 1.30 -2 -1 10 26.30 3.50 -2 -1 10 21.70 4.00 -2 -1 10 22.80 4.00 -2 -1 10 27.30 4.60 2 1 -10 28.70 3.60 2 1 -10 28.30 4.30 2 1 -10 27.00 4.20 2 1 -10 26.50 3.00 2 1 -10 31.30 2.90 -2 0 10 24.80 4.00 -2 0 10 26.20 4.40 -2 0 10 24.90 3.10 -2 0 10 28.90 4.30 2 0 -10 29.00 4.20 2 0 -10 23.00 3.10 2 0 -10 22.60 2.80 2 0 -10 18.10 3.50 -2 1 10 20.10 3.30 -2 1 10 31.70 3.50 -2 1 10 24.30 3.90 -2 1 10 31.90 4.30 -2 1 10 30.20 3.70 -2 1 10 17.80 3.50 2 -1 -10 27.50 4.60 2 -1 -10 23.00 3.70 -2 2 10 2.60 2.30 -2 2 10 1.00 2.00 -2 2 10 3.70 2.70 -2 2 10 5.90 1.80 -2 2 10 3.20 1.80 -2 2 10 4.90 2.20 2 -2 -10 4.90 2.40 2 -2 -10 3.80 2.60 -2 3 10 11.20 2.20 -2 3 10 17.20 3.70 -2 3 10 18.70 3.70 -2 3 10 12.40 2.30 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8.50 7.30 1 -10 10 9.00 7.70 -1 10 -10 16.80 10.40 -1 10 -10 -10.40 6.70 1 -9 10 7.10 10.10 1 -9 10 -5.30 5.50 1 -9 10 -6.20 5.40 -1 9 -10 10.80 9.10 -1 9 -10 -4.10 5.40 1 -8 10 2.40 4.20 1 -8 10 11.30 5.30 -1 8 -10 1.10 4.20 -1 8 -10 5.60 6.70 1 -7 10 1.70 4.10 1 -7 10 4.60 4.20 1 -7 10 8.60 4.60 -1 7 -10 6.20 3.40 -1 7 -10 5.40 5.90 1 -6 10 -2.00 3.60 1 -6 10 2.70 3.80 1 -6 10 1.30 4.20 -1 6 -10 -5.60 4.60 1 -5 10 3.70 3.70 1 -5 10 5.70 3.70 1 -5 10 7.90 3.70 1 -5 10 7.60 3.60 -1 5 -10 6.40 4.30 1 -4 10 0.80 1.70 1 -4 10 1.30 2.90 1 -4 10 -4.30 3.10 -1 4 -10 1.60 2.60 -1 4 -10 4.10 3.50 -1 4 -10 1.70 1.40 1 -3 10 85.39 7.80 1 -3 10 71.89 7.70 1 -3 10 67.89 7.90 -1 3 -10 55.49 7.70 -1 3 -10 72.19 7.50 1 -2 10 93.49 9.00 1 -2 10 83.09 8.40 1 -2 10 85.49 8.80 -1 2 -10 83.59 8.40 1 -1 10 -2.50 2.40 1 -1 10 2.40 1.70 1 -1 10 3.80 3.20 -1 1 -10 1.40 1.60 -1 1 -10 2.30 2.00 1 0 10 1.00 1.90 1 0 10 -0.30 0.80 1 0 10 -1.70 2.10 1 0 10 -0.70 2.70 1 0 10 -2.80 1.80 1 0 10 1.10 2.30 -1 0 -10 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0 -21 11.00 6.80 1 1 21 0.10 5.50 -1 -1 -21 0.00 6.50 1 2 21 2.00 7.20 -1 -2 -21 2.30 7.70 1 3 21 1.00 7.50 -1 -3 -21 -0.60 7.50 2 -3 21 9.50 6.90 2 -2 21 -6.70 6.30 2 -2 21 -19.80 9.90 -2 2 -21 -1.70 8.20 2 -1 21 4.80 6.50 2 -1 21 -9.00 9.40 -2 1 -21 2.10 7.70 2 0 21 2.20 5.90 2 0 21 -10.10 8.50 -2 0 -21 8.10 7.50 2 1 21 -4.50 5.80 2 1 21 11.60 8.40 -2 -1 -21 11.50 7.40 2 2 21 37.60 9.60 2 2 21 0.20 7.00 -2 -2 -21 0.00 7.60 2 3 21 -4.80 8.30 3 -2 21 3.70 6.80 3 -2 21 -9.50 10.10 -3 2 -21 -7.40 8.50 3 -1 21 2.60 6.80 3 -1 21 0.00 9.60 -3 1 -21 5.20 7.20 3 0 21 -8.80 9.70 3 0 21 7.00 6.70 -3 0 -21 5.80 8.00 3 1 21 8.10 6.80 3 1 21 1.20 9.50 -3 -1 -21 19.40 7.90 3 2 21 4.90 6.60 3 2 21 0.50 9.10 -3 -2 -21 3.90 7.70 4 -1 21 -4.40 10.60 4 -1 21 -1.20 6.80 4 0 21 -2.30 6.90 4 0 21 2.50 9.90 -4 0 -21 15.10 8.20 4 1 21 -2.30 7.00 4 1 21 4.90 10.30 -3 -1 22 4.70 6.30 -3 0 22 0.10 6.70 -3 0 22 9.20 9.10 -3 1 22 3.10 6.70 -2 -1 22 5.20 6.90 -2 0 22 0.10 6.60 -2 0 22 4.20 8.70 -2 1 22 10.40 7.20 -1 -1 22 4.10 6.80 -1 0 22 6.10 9.30 -1 0 22 5.70 6.50 1 0 -22 4.30 8.00 -1 1 22 1.10 6.70 0 0 22 16.60 9.90 0 0 22 7.90 7.10 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 95629