data_ome _audit_creation_date 2018-12-28 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _shelx_SHELXL_version_number '2018/3' _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_name '' _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C34 H28 O2 Si' _chemical_formula_sum 'C34 H28 O2 Si' _chemical_formula_weight 496.65 _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Si' 'Si' 0.2541 0.3302 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'monoclinic' _space_group_IT_number 14 _space_group_name_H-M_alt 'P 1 21/c 1' _space_group_name_Hall '-P 2ybc' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 10.48162(16) _cell_length_b 25.1927(3) _cell_length_c 10.92227(18) _cell_angle_alpha 90 _cell_angle_beta 112.6927(19) _cell_angle_gamma 90 _cell_volume 2660.87(8) _cell_formula_units_Z 4 _cell_measurement_reflns_used 9213 _cell_measurement_temperature 150.00(10) _cell_measurement_theta_max 73.3930 _cell_measurement_theta_min 3.5360 _shelx_estimated_absorpt_T_max 0.924 _shelx_estimated_absorpt_T_min 0.907 _exptl_absorpt_coefficient_mu 1.000 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.78640 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.44a (Rigaku Oxford Diffraction, 2018) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _exptl_crystal_colour ? _exptl_crystal_density_diffrn 1.240 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description block _exptl_crystal_F_000 1048 _exptl_crystal_size_max 0.1 _exptl_crystal_size_mid 0.09 _exptl_crystal_size_min 0.08 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0226 _diffrn_reflns_av_unetI/netI 0.0243 _diffrn_reflns_Laue_measured_fraction_full 0.987 _diffrn_reflns_Laue_measured_fraction_max 0.987 _diffrn_reflns_limit_h_max 6 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 30 _diffrn_reflns_limit_k_min -23 _diffrn_reflns_limit_l_max 13 _diffrn_reflns_limit_l_min -12 _diffrn_reflns_number 14642 _diffrn_reflns_point_group_measured_fraction_full 0.987 _diffrn_reflns_point_group_measured_fraction_max 0.987 _diffrn_reflns_theta_full 67.065 _diffrn_reflns_theta_max 67.065 _diffrn_reflns_theta_min 3.509 _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 150.00(10) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean ? _diffrn_measured_fraction_theta_full 0.987 _diffrn_measured_fraction_theta_max 0.987 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w 8.00 88.00 0.50 0.50 -- 0.00 38.00 -30.00 160 2 \w -22.00 6.00 0.50 0.50 -- 0.00 -57.00-180.00 56 3 \w -8.00 92.00 0.50 0.95 -- 5.00 72.00-180.00 200 4 \w -68.00 -42.00 0.50 0.95 -- -98.80 72.00 120.00 52 5 \w -156.00 -90.00 0.50 0.95 -- -98.80 -57.00 -30.00 132 6 \w -104.00 -47.00 0.50 0.95 -- -98.80 72.00 60.00 114 7 \w -103.00 -78.00 0.50 0.95 -- -98.80 72.00 150.00 50 8 \w -185.00-101.00 0.50 0.95 -- -98.80 -38.00 -90.00 168 9 \w -110.00 -19.00 0.50 0.95 -- -98.80 57.00 60.00 182 10 \w -71.00 -9.00 0.50 0.95 -- -98.80 72.00 150.00 124 11 \w -111.00 -25.00 0.50 0.95 -- -98.80 72.00-180.00 172 12 \w -94.00 -56.00 0.50 0.95 -- -98.80 72.00 90.00 76 13 \w -106.00 -81.00 0.50 0.95 -- -98.80 72.00 120.00 50 14 \w -185.00 -85.00 0.50 0.95 -- -98.80 -57.00 -60.00 200 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB AFC12 (RCD3): Kappa single' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0952499000 _diffrn_orient_matrix_UB_12 0.0350071000 _diffrn_orient_matrix_UB_13 0.1143889000 _diffrn_orient_matrix_UB_21 -0.0721624000 _diffrn_orient_matrix_UB_22 0.0500707000 _diffrn_orient_matrix_UB_23 -0.0765250000 _diffrn_orient_matrix_UB_31 -0.1053779000 _diffrn_orient_matrix_UB_32 -0.0025811000 _diffrn_orient_matrix_UB_33 0.0665812000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_source 'Rotating-anode X-ray tube (dual wavelength)' _diffrn_source_type 'Rigaku (Cu) X-ray DW Source' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 4271 _reflns_number_total 4690 _reflns_odcompleteness_completeness 98.49 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 66.97 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'CrysAlisPro 1.171.39.44a (Rigaku OD, 2018)' _computing_data_collection 'CrysAlisPro 1.171.39.44a (Rigaku OD, 2018)' _computing_data_reduction 'CrysAlisPro 1.171.39.44a (Rigaku OD, 2018)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _refine_diff_density_max 0.324 _refine_diff_density_min -0.287 _refine_diff_density_rms 0.037 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.052 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 336 _refine_ls_number_reflns 4690 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0381 _refine_ls_R_factor_gt 0.0346 _refine_ls_restrained_S_all 1.052 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0367P)^2^+1.2211P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0887 _refine_ls_wR_factor_ref 0.0907 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2.a Aromatic/amide H refined with riding coordinates: C008(H008), C00B(H00B), C00D(H00D), C00F(H00F), C00H(H00H), C00I(H00I), C00J(H00J), C00K(H00K), C00L(H00L), C00M(H00M), C00N(H00N), C00O(H00O), C00Q(H00Q), C00R(H00R), C00S(H00S), C00T(H00T), C00U(H00U), C00V(H00V), C00W(H00W), C00X(H00X), C00Y(H00Y), C00Z(H00Z) 2.b Idealised Me refined as rotating group: C010(H01A,H01B,H01C), C011(H01D,H01E,H01F) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Si01 Si 0.67579(4) 0.62120(2) 0.30128(4) 0.02306(11) Uani 1 1 d . . . . . O002 O 1.19675(11) 0.79819(5) 0.38647(13) 0.0423(3) Uani 1 1 d . . . . . O003 O 0.42795(13) 0.93431(4) 0.19225(11) 0.0406(3) Uani 1 1 d . . . . . C004 C 0.77148(14) 0.59201(5) 0.47011(13) 0.0232(3) Uani 1 1 d . . . . . C005 C 0.44638(14) 0.67710(6) 0.24499(14) 0.0256(3) Uani 1 1 d . . . . . C006 C 0.52376(14) 0.77336(6) 0.24100(14) 0.0254(3) Uani 1 1 d . . . . . C007 C 0.55920(14) 0.71584(6) 0.25986(14) 0.0254(3) Uani 1 1 d . . . . . C008 C 0.44172(14) 0.79251(6) 0.11607(14) 0.0267(3) Uani 1 1 d . . . . . H008 H 0.408643 0.769028 0.045001 0.032 Uiso 1 1 calc R . . . . C009 C 0.81620(14) 0.72476(6) 0.31107(14) 0.0255(3) Uani 1 1 d . . . . . C00A C 0.72907(14) 0.58383(6) 0.18069(14) 0.0269(3) Uani 1 1 d . . . . . C00B C 0.38755(15) 0.58439(6) 0.24951(14) 0.0294(3) Uani 1 1 d . . . . . H00B H 0.412663 0.548752 0.259081 0.035 Uiso 1 1 calc R . . . . C00C C 0.68749(14) 0.69523(6) 0.29091(14) 0.0252(3) Uani 1 1 d . . . . . C00D C 0.90126(15) 0.56799(6) 0.50517(15) 0.0280(3) Uani 1 1 d . . . . . H00D H 0.942902 0.566994 0.443868 0.034 Uiso 1 1 calc R . . . . C00E C 0.45577(15) 0.88094(6) 0.20117(15) 0.0275(3) Uani 1 1 d . . . . . C00F C 0.40793(14) 0.84609(6) 0.09495(14) 0.0269(3) Uani 1 1 d . . . . . H00F H 0.353831 0.858358 0.010462 0.032 Uiso 1 1 calc R . . . . C00G C 0.48566(14) 0.62301(6) 0.25952(14) 0.0252(3) Uani 1 1 d . . . . . C00H C 0.57221(15) 0.80923(6) 0.34632(15) 0.0293(3) Uani 1 1 d . . . . . H00H H 0.627586 0.797153 0.430626 0.035 Uiso 1 1 calc R . . . . C00I C 0.31045(15) 0.69132(6) 0.22256(15) 0.0314(3) Uani 1 1 d . . . . . H00I H 0.284512 0.726857 0.214452 0.038 Uiso 1 1 calc R . . . . C00J C 0.71289(15) 0.59290(6) 0.56489(15) 0.0296(3) Uani 1 1 d . . . . . H00J H 0.627444 0.609113 0.544586 0.036 Uiso 1 1 calc R . . . . C00K C 0.96874(16) 0.54569(6) 0.62954(15) 0.0314(3) Uani 1 1 d . . . . . H00K H 1.055433 0.530302 0.651653 0.038 Uiso 1 1 calc R . . . . C00L C 0.53883(15) 0.86252(6) 0.32681(15) 0.0305(3) Uani 1 1 d . . . . . H00L H 0.571950 0.886052 0.397758 0.037 Uiso 1 1 calc R . . . . C00M C 0.94139(15) 0.70578(6) 0.40352(16) 0.0344(4) Uani 1 1 d . . . . . H00M H 0.941160 0.675180 0.451060 0.041 Uiso 1 1 calc R . . . . C00N C 0.67462(17) 0.53316(6) 0.14016(15) 0.0324(3) Uani 1 1 d . . . . . H00N H 0.609965 0.519418 0.170716 0.039 Uiso 1 1 calc R . . . . C00O C 0.94671(16) 0.79590(7) 0.26340(17) 0.0366(4) Uani 1 1 d . . . . . H00O H 0.947779 0.826344 0.215631 0.044 Uiso 1 1 calc R . . . . C00P C 1.06879(15) 0.77636(6) 0.35694(16) 0.0316(3) Uani 1 1 d . . . . . C00Q C 0.82277(15) 0.77013(7) 0.24084(16) 0.0347(4) Uani 1 1 d . . . . . H00Q H 0.741707 0.783522 0.176982 0.042 Uiso 1 1 calc R . . . . C00R C 0.25143(16) 0.59889(6) 0.22513(15) 0.0334(3) Uani 1 1 d . . . . . H00R H 0.185772 0.572892 0.217416 0.040 Uiso 1 1 calc R . . . . C00S C 0.82569(15) 0.60317(7) 0.13251(15) 0.0326(3) Uani 1 1 d . . . . . H00S H 0.863418 0.636771 0.157793 0.039 Uiso 1 1 calc R . . . . C00T C 0.86638(16) 0.57286(7) 0.04714(16) 0.0373(4) Uani 1 1 d . . . . . H00T H 0.930664 0.586281 0.015689 0.045 Uiso 1 1 calc R . . . . C00U C 0.77921(17) 0.57018(7) 0.68849(16) 0.0370(4) Uani 1 1 d . . . . . H00U H 0.738020 0.570896 0.750169 0.044 Uiso 1 1 calc R . . . . C00V C 0.90693(16) 0.54637(6) 0.72038(15) 0.0345(4) Uani 1 1 d . . . . . H00V H 0.951199 0.530799 0.803276 0.041 Uiso 1 1 calc R . . . . C00W C 0.81115(17) 0.52289(7) 0.00928(15) 0.0368(4) Uani 1 1 d . . . . . H00W H 0.838678 0.502593 -0.047349 0.044 Uiso 1 1 calc R . . . . C00X C 0.71534(18) 0.50301(7) 0.05519(15) 0.0370(4) Uani 1 1 d . . . . . H00X H 0.677989 0.469399 0.029243 0.044 Uiso 1 1 calc R . . . . C00Y C 0.21410(15) 0.65177(7) 0.21246(16) 0.0344(4) Uani 1 1 d . . . . . H00Y H 0.123334 0.661119 0.196954 0.041 Uiso 1 1 calc R . . . . C00Z C 1.06512(16) 0.73088(7) 0.42662(17) 0.0387(4) Uani 1 1 d . . . . . H00Z H 1.146603 0.717232 0.489269 0.046 Uiso 1 1 calc R . . . . C010 C 0.3415(2) 0.95389(7) 0.06550(19) 0.0539(5) Uani 1 1 d . . . . . H01A H 0.385531 0.948319 0.004051 0.081 Uiso 1 1 calc GR . . . . H01B H 0.325897 0.991160 0.071689 0.081 Uiso 1 1 calc GR . . . . H01C H 0.254696 0.935436 0.034983 0.081 Uiso 1 1 calc GR . . . . C011 C 1.2026(2) 0.85034(8) 0.3410(3) 0.0614(6) Uani 1 1 d . . . . . H01D H 1.172085 0.850165 0.246092 0.092 Uiso 1 1 calc GR . . . . H01E H 1.295982 0.863149 0.379548 0.092 Uiso 1 1 calc GR . . . . H01F H 1.143665 0.873114 0.366589 0.092 Uiso 1 1 calc GR . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Si01 0.02116(19) 0.0212(2) 0.0239(2) 0.00131(14) 0.00552(15) 0.00066(14) O002 0.0242(5) 0.0358(6) 0.0641(8) 0.0072(6) 0.0141(5) -0.0051(5) O003 0.0536(7) 0.0227(6) 0.0399(6) -0.0005(5) 0.0119(5) 0.0088(5) C004 0.0241(7) 0.0172(6) 0.0249(7) -0.0012(5) 0.0058(6) 0.0001(5) C005 0.0223(7) 0.0253(7) 0.0248(7) 0.0010(6) 0.0043(6) -0.0008(6) C006 0.0182(6) 0.0242(7) 0.0318(7) 0.0017(6) 0.0075(6) -0.0001(5) C007 0.0229(7) 0.0242(7) 0.0251(7) 0.0018(6) 0.0048(6) -0.0005(6) C008 0.0221(7) 0.0247(7) 0.0290(7) -0.0026(6) 0.0050(6) -0.0002(6) C009 0.0225(7) 0.0240(7) 0.0270(7) 0.0002(6) 0.0064(6) 0.0003(6) C00A 0.0242(7) 0.0299(8) 0.0211(7) 0.0029(6) 0.0028(6) 0.0045(6) C00B 0.0294(7) 0.0266(8) 0.0288(7) -0.0011(6) 0.0075(6) -0.0035(6) C00C 0.0240(7) 0.0233(7) 0.0249(7) 0.0026(6) 0.0056(6) 0.0004(5) C00D 0.0278(7) 0.0265(8) 0.0293(7) 0.0000(6) 0.0106(6) 0.0030(6) C00E 0.0265(7) 0.0211(7) 0.0357(8) -0.0002(6) 0.0128(6) 0.0016(6) C00F 0.0228(7) 0.0256(7) 0.0280(7) 0.0024(6) 0.0050(6) 0.0031(6) C00G 0.0235(7) 0.0261(7) 0.0228(7) 0.0001(5) 0.0055(6) -0.0001(6) C00H 0.0234(7) 0.0304(8) 0.0287(7) 0.0023(6) 0.0041(6) 0.0008(6) C00I 0.0259(7) 0.0284(8) 0.0367(8) 0.0016(6) 0.0084(6) 0.0012(6) C00J 0.0260(7) 0.0310(8) 0.0299(8) 0.0001(6) 0.0087(6) 0.0053(6) C00K 0.0261(7) 0.0292(8) 0.0338(8) 0.0017(6) 0.0059(6) 0.0071(6) C00L 0.0284(7) 0.0291(8) 0.0310(8) -0.0063(6) 0.0082(6) -0.0026(6) C00M 0.0264(7) 0.0263(8) 0.0432(9) 0.0089(7) 0.0052(7) -0.0025(6) C00N 0.0386(8) 0.0291(8) 0.0291(8) 0.0036(6) 0.0125(7) 0.0016(7) C00O 0.0302(8) 0.0346(9) 0.0449(9) 0.0140(7) 0.0143(7) 0.0009(7) C00P 0.0235(7) 0.0308(8) 0.0407(9) -0.0011(7) 0.0126(7) -0.0036(6) C00Q 0.0237(7) 0.0371(9) 0.0394(9) 0.0123(7) 0.0076(7) 0.0024(6) C00R 0.0265(7) 0.0350(9) 0.0356(8) -0.0027(7) 0.0084(7) -0.0100(6) C00S 0.0264(7) 0.0380(9) 0.0291(8) -0.0030(6) 0.0061(6) -0.0028(6) C00T 0.0281(8) 0.0525(10) 0.0304(8) -0.0010(7) 0.0102(7) 0.0022(7) C00U 0.0363(8) 0.0461(10) 0.0298(8) 0.0052(7) 0.0142(7) 0.0059(7) C00V 0.0352(8) 0.0349(9) 0.0279(8) 0.0077(6) 0.0063(7) 0.0063(7) C00W 0.0385(9) 0.0438(10) 0.0253(8) -0.0016(7) 0.0093(7) 0.0124(7) C00X 0.0491(10) 0.0283(8) 0.0297(8) 0.0002(6) 0.0109(7) 0.0057(7) C00Y 0.0200(7) 0.0388(9) 0.0411(9) 0.0001(7) 0.0082(6) -0.0017(6) C00Z 0.0222(7) 0.0350(9) 0.0480(10) 0.0100(7) 0.0014(7) -0.0003(6) C010 0.0786(14) 0.0284(9) 0.0458(11) 0.0049(8) 0.0141(10) 0.0213(9) C011 0.0362(10) 0.0460(11) 0.1038(18) 0.0215(11) 0.0289(11) -0.0081(8) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Si01 C004 1.8763(14) . ? Si01 C00A 1.8710(15) . ? Si01 C00C 1.8754(15) . ? Si01 C00G 1.8655(15) . ? O002 C00P 1.3680(18) . ? O002 C011 1.414(2) . ? O003 C00E 1.3713(18) . ? O003 C010 1.419(2) . ? C004 C00D 1.4004(19) . ? C004 C00J 1.393(2) . ? C005 C007 1.4931(19) . ? C005 C00G 1.415(2) . ? C005 C00I 1.396(2) . ? C006 C007 1.490(2) . ? C006 C008 1.389(2) . ? C006 C00H 1.395(2) . ? C007 C00C 1.357(2) . ? C008 C00F 1.392(2) . ? C009 C00C 1.4808(19) . ? C009 C00M 1.396(2) . ? C009 C00Q 1.393(2) . ? C00A C00N 1.399(2) . ? C00A C00S 1.397(2) . ? C00B C00G 1.389(2) . ? C00B C00R 1.395(2) . ? C00D C00K 1.386(2) . ? C00E C00F 1.385(2) . ? C00E C00L 1.391(2) . ? C00H C00L 1.383(2) . ? C00I C00Y 1.392(2) . ? C00J C00U 1.382(2) . ? C00K C00V 1.379(2) . ? C00M C00Z 1.376(2) . ? C00N C00X 1.388(2) . ? C00O C00P 1.384(2) . ? C00O C00Q 1.387(2) . ? C00P C00Z 1.384(2) . ? C00R C00Y 1.380(2) . ? C00S C00T 1.393(2) . ? C00T C00W 1.381(2) . ? C00U C00V 1.383(2) . ? C00W C00X 1.378(2) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C00A Si01 C004 107.64(6) . . ? C00A Si01 C00C 114.43(7) . . ? C00C Si01 C004 115.25(6) . . ? C00G Si01 C004 111.44(6) . . ? C00G Si01 C00A 114.90(6) . . ? C00G Si01 C00C 92.84(6) . . ? C00P O002 C011 117.51(13) . . ? C00E O003 C010 116.64(13) . . ? C00D C004 Si01 122.18(11) . . ? C00J C004 Si01 120.15(10) . . ? C00J C004 C00D 117.65(13) . . ? C00G C005 C007 115.69(12) . . ? C00I C005 C007 124.28(13) . . ? C00I C005 C00G 120.00(13) . . ? C008 C006 C007 120.02(13) . . ? C008 C006 C00H 118.40(13) . . ? C00H C006 C007 121.57(13) . . ? C006 C007 C005 118.41(12) . . ? C00C C007 C005 116.36(13) . . ? C00C C007 C006 125.22(13) . . ? C006 C008 C00F 121.40(13) . . ? C00M C009 C00C 118.93(13) . . ? C00Q C009 C00C 124.48(13) . . ? C00Q C009 C00M 116.56(13) . . ? C00N C00A Si01 119.07(11) . . ? C00S C00A Si01 123.12(12) . . ? C00S C00A C00N 117.76(14) . . ? C00G C00B C00R 120.20(14) . . ? C007 C00C Si01 108.30(10) . . ? C007 C00C C009 127.10(13) . . ? C009 C00C Si01 124.59(10) . . ? C00K C00D C004 121.19(14) . . ? O003 C00E C00F 124.30(13) . . ? O003 C00E C00L 115.62(13) . . ? C00F C00E C00L 120.08(13) . . ? C00E C00F C008 119.28(13) . . ? C005 C00G Si01 106.75(10) . . ? C00B C00G Si01 133.69(11) . . ? C00B C00G C005 119.43(13) . . ? C00L C00H C006 120.77(14) . . ? C00Y C00I C005 119.36(14) . . ? C00U C00J C004 121.31(14) . . ? C00V C00K C00D 119.78(14) . . ? C00H C00L C00E 120.05(14) . . ? C00Z C00M C009 122.13(14) . . ? C00X C00N C00A 121.19(15) . . ? C00P C00O C00Q 120.05(14) . . ? O002 C00P C00O 125.06(14) . . ? O002 C00P C00Z 115.83(14) . . ? C00O C00P C00Z 119.11(14) . . ? C00O C00Q C009 121.89(14) . . ? C00Y C00R C00B 120.08(14) . . ? C00T C00S C00A 120.97(15) . . ? C00W C00T C00S 119.93(15) . . ? C00J C00U C00V 119.92(15) . . ? C00K C00V C00U 120.14(14) . . ? C00X C00W C00T 120.17(15) . . ? C00W C00X C00N 119.98(16) . . ? C00R C00Y C00I 120.91(14) . . ? C00M C00Z C00P 120.24(14) . . ? _shelx_res_file ; TITL ome_a.res in P2(1)/c ome.res created by SHELXL-2018/3 at 13:48:31 on 28-Dec-2018 REM Old TITL ome in P2(1)/c REM SHELXT solution in P2(1)/c: R1 0.156, Rweak 0.011, Alpha 0.029 REM 0.919 for 92 systematic absences, Orientation as input REM Formula found by SHELXT: C34 O2 Cl CELL 1.54184 10.48162 25.192747 10.922267 90 112.6927 90 ZERR 4 0.000162 0.000339 0.000178 0 0.0019 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H O Si UNIT 136 112 8 4 L.S. 4 0 0 PLAN 20 SIZE 0.1 0.09 0.08 list 4 fmap 2 53 ACTA SHEL 999 0.837 REM REM REM WGHT 0.036700 1.221100 FVAR 4.50724 SI01 4 0.675786 0.621202 0.301277 11.00000 0.02116 0.02121 = 0.02392 0.00131 0.00552 0.00066 O002 3 1.196748 0.798188 0.386473 11.00000 0.02422 0.03578 = 0.06414 0.00716 0.01412 -0.00514 O003 3 0.427949 0.934314 0.192247 11.00000 0.05361 0.02266 = 0.03986 -0.00054 0.01190 0.00884 C004 1 0.771483 0.592008 0.470114 11.00000 0.02413 0.01725 = 0.02488 -0.00125 0.00581 0.00013 C005 1 0.446377 0.677097 0.244986 11.00000 0.02233 0.02532 = 0.02480 0.00105 0.00433 -0.00081 C006 1 0.523762 0.773363 0.240998 11.00000 0.01820 0.02422 = 0.03185 0.00168 0.00745 -0.00009 C007 1 0.559203 0.715842 0.259864 11.00000 0.02285 0.02417 = 0.02506 0.00179 0.00483 -0.00048 C008 1 0.441717 0.792506 0.116068 11.00000 0.02213 0.02470 = 0.02895 -0.00262 0.00504 -0.00020 AFIX 43 H008 2 0.408643 0.769028 0.045001 11.00000 -1.20000 AFIX 0 C009 1 0.816201 0.724763 0.311067 11.00000 0.02253 0.02397 = 0.02704 0.00020 0.00638 0.00031 C00A 1 0.729067 0.583833 0.180687 11.00000 0.02424 0.02994 = 0.02111 0.00287 0.00278 0.00455 C00B 1 0.387547 0.584386 0.249507 11.00000 0.02941 0.02659 = 0.02881 -0.00113 0.00751 -0.00354 AFIX 43 H00B 2 0.412663 0.548752 0.259081 11.00000 -1.20000 AFIX 0 C00C 1 0.687493 0.695234 0.290912 11.00000 0.02395 0.02327 = 0.02493 0.00259 0.00558 0.00042 C00D 1 0.901260 0.567991 0.505167 11.00000 0.02783 0.02651 = 0.02928 0.00004 0.01055 0.00301 AFIX 43 H00D 2 0.942902 0.566994 0.443868 11.00000 -1.20000 AFIX 0 C00E 1 0.455770 0.880945 0.201167 11.00000 0.02647 0.02114 = 0.03569 -0.00024 0.01280 0.00160 C00F 1 0.407930 0.846090 0.094952 11.00000 0.02285 0.02565 = 0.02802 0.00241 0.00504 0.00307 AFIX 43 H00F 2 0.353831 0.858358 0.010462 11.00000 -1.20000 AFIX 0 C00G 1 0.485661 0.623012 0.259517 11.00000 0.02354 0.02610 = 0.02284 0.00010 0.00549 -0.00009 C00H 1 0.572207 0.809225 0.346322 11.00000 0.02339 0.03039 = 0.02874 0.00234 0.00412 0.00079 AFIX 43 H00H 2 0.627586 0.797153 0.430626 11.00000 -1.20000 AFIX 0 C00I 1 0.310452 0.691316 0.222562 11.00000 0.02593 0.02839 = 0.03667 0.00155 0.00841 0.00121 AFIX 43 H00I 2 0.284512 0.726857 0.214452 11.00000 -1.20000 AFIX 0 C00J 1 0.712894 0.592903 0.564892 11.00000 0.02599 0.03104 = 0.02985 0.00009 0.00869 0.00532 AFIX 43 H00J 2 0.627444 0.609113 0.544586 11.00000 -1.20000 AFIX 0 C00K 1 0.968740 0.545686 0.629537 11.00000 0.02606 0.02915 = 0.03379 0.00173 0.00592 0.00712 AFIX 43 H00K 2 1.055433 0.530302 0.651653 11.00000 -1.20000 AFIX 0 C00L 1 0.538833 0.862517 0.326814 11.00000 0.02839 0.02909 = 0.03103 -0.00633 0.00819 -0.00260 AFIX 43 H00L 2 0.571950 0.886052 0.397758 11.00000 -1.20000 AFIX 0 C00M 1 0.941386 0.705782 0.403522 11.00000 0.02639 0.02625 = 0.04318 0.00889 0.00516 -0.00249 AFIX 43 H00M 2 0.941160 0.675180 0.451060 11.00000 -1.20000 AFIX 0 C00N 1 0.674621 0.533157 0.140165 11.00000 0.03861 0.02908 = 0.02909 0.00359 0.01249 0.00157 AFIX 43 H00N 2 0.609965 0.519418 0.170716 11.00000 -1.20000 AFIX 0 C00O 1 0.946705 0.795905 0.263398 11.00000 0.03018 0.03456 = 0.04486 0.01401 0.01433 0.00086 AFIX 43 H00O 2 0.947779 0.826344 0.215631 11.00000 -1.20000 AFIX 0 C00P 1 1.068787 0.776364 0.356938 11.00000 0.02350 0.03080 = 0.04066 -0.00107 0.01261 -0.00362 C00Q 1 0.822769 0.770132 0.240836 11.00000 0.02367 0.03709 = 0.03938 0.01235 0.00765 0.00243 AFIX 43 H00Q 2 0.741707 0.783522 0.176982 11.00000 -1.20000 AFIX 0 C00R 1 0.251430 0.598888 0.225133 11.00000 0.02655 0.03500 = 0.03555 -0.00271 0.00841 -0.01002 AFIX 43 H00R 2 0.185772 0.572892 0.217416 11.00000 -1.20000 AFIX 0 C00S 1 0.825690 0.603171 0.132511 11.00000 0.02642 0.03797 = 0.02911 -0.00297 0.00611 -0.00277 AFIX 43 H00S 2 0.863418 0.636771 0.157793 11.00000 -1.20000 AFIX 0 C00T 1 0.866377 0.572865 0.047140 11.00000 0.02806 0.05246 = 0.03035 -0.00104 0.01020 0.00217 AFIX 43 H00T 2 0.930664 0.586281 0.015689 11.00000 -1.20000 AFIX 0 C00U 1 0.779206 0.570183 0.688490 11.00000 0.03634 0.04607 = 0.02980 0.00520 0.01417 0.00587 AFIX 43 H00U 2 0.738020 0.570896 0.750169 11.00000 -1.20000 AFIX 0 C00V 1 0.906933 0.546374 0.720379 11.00000 0.03523 0.03492 = 0.02786 0.00767 0.00626 0.00632 AFIX 43 H00V 2 0.951199 0.530799 0.803276 11.00000 -1.20000 AFIX 0 C00W 1 0.811153 0.522889 0.009278 11.00000 0.03851 0.04384 = 0.02532 -0.00163 0.00934 0.01237 AFIX 43 H00W 2 0.838678 0.502593 -0.047349 11.00000 -1.20000 AFIX 0 C00X 1 0.715342 0.503008 0.055194 11.00000 0.04906 0.02832 = 0.02965 0.00019 0.01085 0.00572 AFIX 43 H00X 2 0.677989 0.469399 0.029243 11.00000 -1.20000 AFIX 0 C00Y 1 0.214099 0.651774 0.212457 11.00000 0.02001 0.03880 = 0.04106 0.00009 0.00817 -0.00174 AFIX 43 H00Y 2 0.123334 0.661119 0.196954 11.00000 -1.20000 AFIX 0 C00Z 1 1.065124 0.730878 0.426616 11.00000 0.02218 0.03505 = 0.04797 0.00999 0.00136 -0.00032 AFIX 43 H00Z 2 1.146603 0.717232 0.489269 11.00000 -1.20000 AFIX 0 C010 1 0.341533 0.953889 0.065497 11.00000 0.07861 0.02839 = 0.04583 0.00495 0.01407 0.02130 AFIX 137 H01A 2 0.385531 0.948319 0.004051 11.00000 -1.50000 H01B 2 0.325897 0.991160 0.071689 11.00000 -1.50000 H01C 2 0.254696 0.935436 0.034983 11.00000 -1.50000 AFIX 0 C011 1 1.202589 0.850341 0.341027 11.00000 0.03622 0.04604 = 0.10379 0.02147 0.02891 -0.00809 AFIX 137 H01D 2 1.172085 0.850165 0.246092 11.00000 -1.50000 H01E 2 1.295982 0.863149 0.379548 11.00000 -1.50000 H01F 2 1.143665 0.873114 0.366589 11.00000 -1.50000 AFIX 0 HKLF 4 REM ome_a.res in P2(1)/c REM wR2 = 0.0907, GooF = S = 1.052, Restrained GooF = 1.052 for all data REM R1 = 0.0346 for 4271 Fo > 4sig(Fo) and 0.0381 for all 4690 data REM 336 parameters refined using 0 restraints END WGHT 0.0367 1.2213 REM Highest difference peak 0.324, deepest hole -0.287, 1-sigma level 0.037 Q1 1 0.7726 0.6543 0.3097 11.00000 0.05 0.32 Q2 1 0.7262 0.6052 0.3950 11.00000 0.05 0.25 Q3 1 0.7056 0.6652 0.2981 11.00000 0.05 0.22 Q4 1 0.5661 0.6176 0.2796 11.00000 0.05 0.21 Q5 1 0.6937 0.6008 0.2266 11.00000 0.05 0.19 Q6 1 0.5003 0.6976 0.2459 11.00000 0.05 0.19 Q7 1 0.7564 0.5992 0.5184 11.00000 0.05 0.18 Q8 1 0.9000 0.7009 0.3169 11.00000 0.05 0.17 Q9 1 0.0649 0.6392 0.0578 11.00000 0.05 0.17 Q10 1 0.8220 0.7555 0.3057 11.00000 0.05 0.17 Q11 1 0.5922 0.8408 0.3271 11.00000 0.05 0.17 Q12 1 0.8343 0.5931 0.4847 11.00000 0.05 0.16 Q13 1 0.7268 0.5618 0.1768 11.00000 0.05 0.15 Q14 1 0.4773 0.8182 0.1025 11.00000 0.05 0.15 Q15 1 0.9177 0.5470 0.5549 11.00000 0.05 0.14 Q16 1 0.8661 0.7221 0.3777 11.00000 0.05 0.14 Q17 1 0.6226 0.6996 0.2461 11.00000 0.05 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5 54620.7 1797.21 7 -2 -10 5 52902.5 1792.11 9 2 10 -4 13546.1 565.319 2 2 10 -4 14580.3 575.667 1 -2 10 4 14467.6 520.235 14 -2 10 4 14152.1 507.397 7 2 10 -3 4290.76 214.393 2 2 -10 -3 3864.24 159.931 3 -2 -10 3 3669.50 142.545 3 -2 10 3 4100.69 173.219 1 2 10 -3 3658.94 207.629 1 2 -10 -3 3914.35 159.101 2 2 -10 -2 3713.51 148.226 3 -2 -10 2 3663.86 139.004 3 2 10 -2 3371.17 136.325 3 2 10 -2 3243.13 184.124 2 -2 -10 1 15611.9 516.562 3 2 10 -1 15016.8 513.835 3 2 -10 -1 14034.7 515.633 3 -2 -10 0 56650.5 1927.95 2 2 -10 0 56253.0 1874.46 3 -2 10 0 54081.5 1881.98 2 -2 -10 0 56396.6 1877.28 3 2 10 0 58467.7 1876.82 3 -2 10 0 55354.3 1904.18 1 2 10 1 31631.4 1080.88 3 -2 10 -1 31337.0 1116.93 1 -2 -10 -1 31879.7 1132.07 2 -2 -10 -1 32559.8 1082.24 3 2 -10 2 5725.71 206.691 3 -2 10 -2 5225.98 256.004 1 2 10 2 5388.80 266.068 1 -2 -10 -2 5611.24 268.077 2 2 10 2 5437.76 217.957 3 -2 10 -3 742.289 67.7586 5 2 10 3 770.543 60.2672 3 2 10 4 14989.9 535.164 8 -2 10 -4 14413.4 533.993 5 -2 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4234.83 239.005 8 -2 19 -6 920.028 122.863 14 -2 19 -6 717.480 117.372 8 -2 19 -7 3023.84 174.355 8 -2 19 -7 3142.78 184.111 14 -2 19 -8 1957.19 124.739 14 -2 19 -8 1936.85 120.235 8 -2 20 9 197.806 50.1791 9 2 20 -9 193.070 52.6966 8 2 20 -8 1109.70 99.1302 8 -2 20 8 1203.15 98.9480 9 -2 20 7 1510.02 102.795 6 -2 20 7 1441.09 123.248 9 -2 20 6 39990.1 1405.56 9 2 20 -6 40732.6 1401.56 8 -2 20 5 277.852 83.9724 9 2 20 -5 424.795 90.6481 8 -2 20 4 10631.3 433.301 14 2 20 -4 10649.7 424.007 8 -2 20 3 2622.73 168.578 14 2 20 -3 2311.90 148.039 8 -2 20 2 62.2742 87.2089 14 2 20 -2 86.9295 64.8286 8 -2 20 1 6.32568 84.2348 14 2 20 -1 5.02071 63.0733 8 -2 20 0 9956.09 412.296 14 2 20 0 9623.69 386.785 8 -2 20 -1 2225.59 164.893 14 2 20 1 2211.18 139.187 8 2 20 2 541.135 83.2131 8 -2 20 -2 484.951 112.209 14 -2 20 -3 268.703 108.331 14 2 20 3 265.101 75.4915 8 -2 20 -4 1426.05 148.314 14 2 20 4 1696.98 118.829 8 -2 20 -5 2617.25 183.538 14 -2 20 -6 174.576 95.4195 14 -2 20 -6 38.4223 94.9427 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326.421 72.5409 5 -4 4 -9 589.061 75.2462 14 -4 -4 -9 555.014 70.7976 5 -4 -4 -9 527.259 57.9094 10 -4 -4 -10 340.905 38.9849 5 4 -5 -13 671.307 47.7774 5 4 5 -13 501.092 54.3961 14 -4 5 12 172.071 58.7058 6 -4 5 12 214.797 62.3525 9 -4 -5 12 158.905 59.0016 9 -4 5 11 1015.62 104.548 9 -4 5 11 1328.43 112.338 6 -4 -5 11 1371.31 104.023 9 -4 5 10 4976.46 236.873 6 -4 -5 10 5065.61 233.339 6 -4 5 10 4724.49 237.865 9 -4 -5 10 5136.47 234.586 9 -4 5 9 15240.4 561.401 13 -4 5 9 15116.3 564.929 12 -4 5 9 13473.5 556.553 6 -4 -5 9 15723.4 558.749 6 -4 5 9 14622.2 563.855 9 -4 -5 9 15297.3 557.971 9 -4 5 8 4815.90 222.745 13 -4 5 8 4776.40 222.828 12 -4 -5 8 4694.60 213.969 6 -4 5 8 4810.85 222.673 9 -4 -5 8 4688.81 213.322 9 -4 5 7 3807.72 184.302 13 -4 5 7 3855.58 171.567 7 -4 5 7 3844.51 182.177 6 -4 5 7 3790.04 183.304 12 -4 -5 7 3717.95 173.128 6 -4 5 7 3711.73 179.252 9 -4 -5 7 3649.89 170.507 9 -4 -5 6 51.9116 39.1028 6 -4 5 6 101.340 48.0008 9 -4 5 6 121.559 57.1471 12 -4 5 6 140.641 46.7033 7 -4 -5 6 196.885 40.1428 9 4 -5 -5 4910.96 186.775 3 4 5 -5 4184.10 229.131 2 4 5 -5 4694.36 228.365 1 4 5 -4 42585.9 1429.76 2 4 5 -4 40610.5 1362.27 3 4 5 -4 40713.4 1415.82 1 4 5 -3 1429.95 68.6926 3 4 5 -3 1493.21 110.690 2 4 5 -2 37214.2 1246.51 3 -4 -5 1 38148.0 1326.34 2 4 5 -1 38251.2 1280.44 3 -4 -5 1 38009.5 1280.74 3 -4 5 0 62233.6 2070.67 1 4 5 0 64073.8 2102.92 1 -4 -5 0 62793.9 2111.56 2 -4 -5 0 58229.1 2058.95 3 4 -5 0 61793.2 2071.90 1 4 -5 0 63825.9 2059.35 3 4 -5 1 39.9017 38.7987 1 -4 5 -1 153.579 44.7506 1 -4 -5 -1 70.9496 52.2300 2 4 5 1 123.912 50.5765 1 4 5 1 118.866 31.8576 3 4 -5 1 9.37172 26.6682 3 -4 5 -2 4627.79 195.924 5 4 5 2 4494.00 189.428 3 -4 5 -2 4532.57 222.732 1 4 -5 2 4510.27 180.818 3 4 -5 2 4800.91 232.148 1 -4 5 -3 49410.7 1700.96 14 -4 -5 -3 50307.9 1683.12 5 -4 5 -3 50631.4 1694.65 5 -4 5 -3 49341.4 1682.70 10 -4 5 -4 8886.03 353.620 14 -4 -5 -4 8124.29 328.020 5 -4 5 -4 8452.84 341.122 5 -4 5 -4 8297.77 324.259 10 -4 5 -5 3526.00 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3386.93 167.039 9 -4 -6 7 3326.85 158.227 9 -4 6 6 4252.30 181.908 8 -4 6 6 4369.76 193.224 12 -4 6 6 4214.74 184.251 7 -4 -6 6 4007.41 177.350 6 -4 6 6 4174.82 188.635 9 -4 -6 6 4079.71 174.819 9 -4 6 5 146.511 47.4336 4 4 6 -5 193.627 55.8840 1 -4 6 5 178.086 57.0076 14 -4 6 5 108.640 52.2314 7 4 6 -5 195.528 58.6312 2 4 6 -4 875.363 89.5292 1 4 6 -4 779.299 88.4749 2 4 6 -4 834.160 46.6771 3 4 6 -3 17996.4 623.909 3 4 6 -3 19660.7 689.330 2 4 6 -2 11834.8 426.905 3 -4 -6 2 12676.2 430.101 3 -4 -6 1 1944.03 130.331 2 4 6 -1 1908.06 93.2059 3 -4 -6 1 1902.42 91.1231 3 -4 6 0 194.807 38.8547 1 -4 -6 0 267.486 66.2609 2 4 6 0 449.617 45.1172 3 -4 -6 0 468.039 44.4545 3 -4 -6 -1 3433.93 192.819 2 4 6 1 3254.33 140.769 3 -4 6 -1 3253.51 159.352 1 4 6 1 3277.19 179.962 1 4 -6 1 2765.54 130.322 3 4 -6 1 3179.92 162.256 1 4 -6 2 376.936 62.0490 1 -4 6 -2 477.615 67.0408 1 -4 6 -2 489.160 61.4674 5 -4 6 -2 482.150 71.3964 14 4 6 2 302.952 45.2785 3 4 -6 2 305.758 35.3627 3 -4 6 -3 17270.0 623.049 14 -4 6 -3 16654.3 612.020 5 -4 6 -3 16836.2 598.611 10 -4 6 -4 2596.68 159.361 14 -4 6 -4 2275.37 123.039 10 -4 6 -5 6538.29 300.885 14 -4 -6 -5 6365.06 273.382 5 -4 6 -6 3758.33 216.378 14 -4 -6 -6 3449.95 186.346 5 -4 6 -7 27634.1 993.809 14 -4 -6 -7 27235.4 970.743 5 -4 6 -8 560.745 104.522 14 -4 -6 -8 614.074 83.4702 5 -4 6 -8 615.234 97.6828 5 -4 -6 -9 422.362 60.4020 5 -4 6 -9 326.485 68.9358 5 -4 6 -9 411.101 72.1542 14 -4 6 -10 146.586 35.1550 5 -4 7 12 19.4005 45.9256 6 4 7 -12 161.623 64.3804 14 -4 7 11 5478.02 234.074 6 -4 7 11 5046.56 236.059 9 -4 -7 11 4899.42 228.811 9 -4 7 10 2098.71 137.685 6 -4 7 10 1958.63 141.155 9 -4 -7 10 2043.79 132.486 9 -4 -7 9 175.962 73.7177 6 -4 7 9 66.2781 76.1556 9 -4 -7 9 92.5676 65.9313 9 -4 7 9 100.467 86.4495 13 -4 7 9 84.6735 74.6578 6 -4 7 8 53853.6 1794.40 13 -4 7 8 48795.9 1787.84 6 -4 -7 8 53536.9 1785.25 6 -4 7 8 51386.9 1793.41 9 -4 -7 8 54984.0 1786.14 9 -4 7 7 5606.09 254.265 13 -4 7 7 6079.81 248.317 7 -4 7 7 5677.47 251.860 9 -4 -7 7 5838.37 243.838 6 -4 -7 7 6040.55 243.401 9 -4 7 6 36012.2 1238.79 8 -4 7 6 37164.6 1239.49 11 -4 7 6 37609.9 1241.66 7 -4 7 6 36742.7 1247.19 9 -4 -7 6 35328.0 1232.22 6 -4 -7 6 35385.7 1231.25 9 -4 7 5 18381.7 666.054 14 -4 7 5 20164.8 666.286 7 4 7 -5 18077.7 710.183 1 -4 7 5 17838.0 659.305 9 -4 7 5 18761.9 657.826 4 4 7 -4 1396.24 117.863 2 4 7 -4 1353.79 64.3230 3 4 7 -4 1339.33 110.996 1 4 7 -3 542.508 82.7077 2 4 7 -3 348.066 34.4255 3 4 7 -2 25957.2 883.402 3 -4 -7 2 26194.2 885.345 3 -4 -7 1 9454.23 409.302 2 4 7 -1 10313.0 360.197 3 -4 -7 1 9845.48 359.465 3 -4 -7 0 41369.6 1441.49 2 4 7 0 41561.2 1381.40 3 -4 7 0 40132.9 1389.40 1 4 7 1 97800.2 3202.28 3 -4 -7 -1 95057.9 3268.95 2 4 7 1 93924.9 3257.72 1 -4 7 -1 95624.7 3227.33 1 4 -7 1 96804.7 3195.53 3 -4 7 -2 105.759 63.7933 14 -4 7 -2 319.429 60.6717 5 -4 7 -2 305.704 53.6136 1 -4 7 -2 154.284 45.9939 10 4 7 2 92.0525 35.7910 3 4 -7 2 112.274 27.4057 3 -4 7 -3 1769.80 129.530 14 -4 7 -3 1803.11 101.806 10 -4 7 -5 1251.24 134.950 14 -4 -7 -5 1314.93 100.565 5 -4 7 -6 846.687 119.882 14 -4 -7 -6 834.903 89.5357 5 -4 7 -6 610.862 107.044 5 -4 7 -7 13.6390 93.9459 14 -4 -7 -7 39.6310 66.4759 5 -4 7 -7 80.3273 88.4563 5 -4 7 -8 2698.52 175.012 14 -4 -7 -8 2968.78 152.631 5 -4 7 -8 2862.34 166.380 5 -4 7 -9 3092.60 155.276 14 -4 -7 -9 3070.86 142.012 5 -4 7 -9 2934.20 148.577 5 4 8 -12 2366.47 131.327 14 -4 8 12 2632.80 127.208 6 -4 8 11 5429.78 239.357 6 -4 8 11 5177.39 243.328 9 -4 -8 11 5888.39 242.390 9 -4 8 10 786.868 108.265 9 -4 8 10 770.882 112.022 12 -4 -8 10 938.736 100.380 9 -4 8 10 750.389 90.7740 6 -4 8 9 3082.71 176.659 12 -4 8 9 2950.72 176.530 13 -4 8 9 3038.62 171.097 6 -4 8 9 2965.83 175.157 9 -4 -8 9 3153.94 168.416 9 -4 8 8 2701.73 166.967 13 -4 8 8 2846.22 170.050 12 -4 8 8 3125.30 168.926 6 -4 8 8 2812.25 166.693 9 -4 -8 8 2910.00 154.461 6 -4 -8 8 3110.73 158.969 9 -4 8 7 1869.76 132.084 13 -4 8 7 2003.42 123.346 7 -4 8 7 1969.15 126.459 9 -4 -8 7 2020.40 117.482 6 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166.404 14 -4 -8 -6 1912.11 127.191 5 -4 8 -6 2025.87 146.672 5 -4 8 -7 4956.94 257.644 14 -4 -8 -7 4849.32 225.200 5 -4 8 -7 5042.21 241.875 5 -4 8 -8 174.821 89.5299 14 -4 -8 -8 60.4638 58.7430 5 -4 8 -8 61.3349 73.7236 5 -4 8 -9 143.106 61.7746 14 -4 -8 -9 144.879 42.9016 5 -4 8 -9 103.001 52.3424 5 4 9 -12 2372.83 122.262 14 -4 9 12 2478.09 119.054 6 4 9 -11 2107.11 136.715 14 -4 9 11 1933.13 123.651 6 -4 -9 10 1243.62 104.111 9 -4 9 10 1051.56 109.715 9 -4 9 10 1371.28 124.812 12 -4 9 10 1043.85 103.986 6 -4 9 9 273.667 89.2818 9 -4 9 9 443.797 95.3661 13 -4 9 9 414.055 93.4191 12 -4 -9 9 385.373 78.7081 9 -4 9 9 424.741 87.5796 6 -4 9 8 333.450 84.7121 9 -4 -9 8 456.571 72.1145 9 -4 9 8 350.992 92.2028 13 -4 9 8 349.339 86.1889 12 -4 9 8 373.487 79.4574 6 -4 9 7 2635.43 158.961 13 -4 9 7 3169.05 170.405 12 -4 9 7 3011.01 155.447 7 -4 9 7 2710.42 161.867 9 -4 -9 7 2877.77 147.149 6 -4 -9 7 3006.12 147.786 9 -4 9 6 8590.15 358.225 14 -4 9 6 9752.37 348.939 11 -4 9 6 8462.86 351.134 12 -4 9 6 8772.51 344.459 8 -4 9 6 8857.07 345.795 7 -4 9 6 9414.07 354.470 9 -4 -9 6 8485.11 333.955 6 -4 -9 6 8666.74 331.965 9 -4 9 5 761.053 76.1273 9 -4 9 5 667.134 76.0218 11 -4 9 5 690.529 69.4687 8 -4 9 5 848.275 82.9675 7 -4 9 5 788.995 86.7793 14 -4 -9 5 792.345 59.5974 6 -4 9 4 1613.11 105.289 11 -4 9 4 1714.17 111.861 14 -4 9 4 1728.22 98.3664 4 4 9 -4 1630.20 131.247 1 4 9 -3 2173.10 152.761 2 4 9 -3 2222.05 96.7555 3 -4 9 3 1981.71 115.623 11 -4 9 3 1956.69 111.723 10 4 9 -2 39788.0 1350.30 3 -4 -9 2 40618.2 1352.24 3 4 9 -1 5000.07 198.763 3 -4 -9 0 10436.7 471.448 2 4 9 0 11948.9 418.738 3 -4 9 -1 457.340 75.6648 14 4 -9 1 345.711 39.7124 3 -4 9 -2 2706.22 158.229 14 -4 9 -2 2758.91 145.906 5 -4 9 -2 2718.98 129.981 10 -4 9 -3 5761.80 267.906 14 -4 9 -3 5906.34 254.094 5 -4 9 -4 5966.15 292.384 14 -4 9 -4 6546.98 278.580 5 -4 9 -5 250.201 107.740 14 -4 -9 -5 258.360 60.0621 5 -4 9 -5 141.017 83.4603 5 -4 9 -6 2554.30 182.528 14 -4 9 -6 2556.49 165.274 5 -4 -9 -6 2353.44 140.014 5 -4 9 -7 1044.61 115.721 5 -4 9 -7 1019.77 127.883 14 -4 -9 -7 999.016 91.2309 5 -4 9 -8 1608.75 129.359 14 -4 -9 -8 1476.31 101.052 5 -4 9 -8 1698.09 117.951 5 -4 -9 -9 4376.83 181.661 5 -4 9 -9 4797.19 194.963 5 -4 9 -9 4560.32 200.791 14 -4 10 12 411.411 50.9135 6 4 10 -11 8198.74 335.198 14 -4 10 11 8451.10 330.336 6 -4 -10 10 5601.95 242.410 9 4 10 -10 5306.58 251.008 14 -4 10 10 5431.02 249.340 12 -4 10 10 5476.75 246.357 6 -4 10 10 4833.25 247.468 9 -4 10 9 103.731 79.1793 9 -4 -10 9 174.634 62.3440 9 -4 10 9 186.584 90.3925 12 -4 10 9 129.385 71.2567 6 -4 10 9 211.585 88.6335 13 -4 10 8 22628.8 831.238 12 -4 10 8 22862.1 830.772 6 -4 10 8 22771.5 831.461 9 -4 -10 8 23648.7 818.793 9 -4 10 7 3069.73 174.661 12 -4 10 7 3127.88 167.392 8 -4 10 7 3058.78 164.082 7 -4 10 7 3029.94 171.601 9 -4 -10 7 3243.95 156.759 9 -4 10 6 4404.14 213.976 14 -4 10 6 4533.05 199.710 7 -4 10 6 4057.80 195.187 8 -4 10 6 4458.84 200.593 11 -4 10 6 4253.83 205.673 12 -4 10 6 4376.04 205.754 9 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3511.49 174.870 11 -4 11 4 3955.25 181.148 7 -4 11 4 3774.39 169.983 4 4 11 -3 2034.40 94.5926 3 -4 11 3 1952.86 114.217 8 -4 11 3 1994.11 126.604 14 -4 11 3 2094.24 111.379 4 4 11 -2 648.874 51.3971 3 -4 11 2 743.090 85.7684 14 -4 11 2 639.819 75.2964 11 -4 11 2 577.693 66.4508 10 -4 11 1 5805.45 256.419 14 -4 11 1 6063.87 246.057 5 -4 11 1 6117.90 247.851 11 -4 11 1 6147.43 242.469 10 4 11 -1 5812.73 234.290 3 4 11 0 5715.13 235.944 3 -4 11 0 5540.56 243.166 8 -4 11 0 6213.30 248.178 5 -4 11 0 6108.24 246.258 11 -4 11 0 6138.70 239.421 10 -4 11 0 5813.97 259.011 14 -4 11 -1 3966.28 198.764 14 -4 11 -1 3815.10 184.235 8 -4 11 -1 3946.19 176.469 11 -4 11 -1 4115.89 184.724 5 -4 11 -1 3825.01 171.218 10 -4 11 -2 10148.2 412.237 14 -4 11 -2 10158.7 393.253 5 -4 11 -3 2175.76 157.619 14 -4 11 -3 1932.51 130.215 5 -4 11 -4 6465.87 308.026 14 -4 11 -4 6339.69 281.746 5 -4 11 -5 142.674 117.950 14 -4 11 -5 101.751 76.4870 5 -4 11 -6 5665.34 294.573 14 -4 11 -6 5939.39 273.005 5 -4 11 -7 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101.751 3 -5 -4 0 1722.75 126.487 2 5 4 0 1573.43 112.178 1 5 -4 0 1434.39 84.8160 3 -5 4 -1 51144.5 1766.22 5 5 4 1 55672.6 1768.85 3 -5 4 -1 51817.4 1765.32 11 5 -4 1 52108.6 1761.38 3 -5 4 -1 51842.4 1767.05 10 5 4 1 51933.3 1823.23 1 -5 4 -2 126.269 55.3039 5 -5 4 -2 91.4714 47.6264 11 -5 4 -2 67.8058 51.1076 10 5 -4 2 76.1725 28.3290 3 -5 4 -3 2534.04 150.812 14 -5 -4 -3 2892.22 141.273 5 -5 4 -3 3036.93 156.511 5 -5 4 -3 2464.62 142.398 10 -5 4 -4 14285.3 533.112 14 -5 -4 -4 13234.9 515.924 5 -5 4 -4 14293.0 531.068 5 -5 4 -4 13984.1 517.853 10 -5 4 -5 1612.77 135.456 14 -5 -4 -5 1935.00 126.785 5 -5 4 -5 1948.23 138.189 5 -5 -4 -5 1647.55 113.661 11 -5 4 -5 1888.60 119.100 10 -5 4 -6 1830.41 137.922 14 -5 -4 -6 2121.43 131.568 5 -5 4 -6 1965.81 141.492 5 -5 4 -6 1820.85 119.300 10 -5 4 -7 2544.15 150.182 14 -5 -4 -7 2161.44 135.985 5 -5 4 -7 2253.08 146.849 5 -5 -4 -8 128.028 55.7158 5 -5 4 -8 83.6010 65.4215 5 -5 -4 -8 183.890 58.2453 10 -5 -4 -9 390.301 43.5193 5 -5 4 -9 421.783 54.3256 5 -5 5 13 1014.07 65.5145 6 -5 5 13 960.335 65.9506 9 -5 5 12 159.667 61.3510 6 -5 5 12 99.3863 53.9576 9 -5 -5 12 118.080 52.0636 9 -5 -5 11 124.374 65.9712 6 -5 5 11 98.2574 66.9188 9 -5 -5 11 115.878 57.9795 9 -5 -5 10 130.675 72.9456 6 -5 5 10 83.3710 72.6162 9 -5 -5 10 257.784 69.6818 9 -5 5 10 118.041 90.3745 12 -5 -5 9 482.064 78.7665 6 -5 5 9 406.878 82.3483 9 -5 -5 9 462.335 73.7209 9 -5 5 9 582.433 87.4168 13 -5 5 9 439.168 89.4417 12 -5 5 9 489.965 85.1647 6 -5 5 8 8827.70 350.899 13 -5 5 8 8310.77 354.598 12 -5 5 8 8511.02 349.808 6 -5 -5 8 8552.59 340.525 6 -5 5 8 8769.60 350.364 9 -5 -5 8 8806.01 338.850 9 -5 5 7 13194.3 513.078 12 -5 5 7 13614.0 502.875 7 -5 5 7 13723.9 509.863 6 -5 -5 7 14290.6 503.645 6 -5 5 7 14241.9 511.328 9 -5 -5 7 13492.9 496.303 9 -5 5 6 43029.9 1501.73 12 -5 -5 6 41717.7 1485.82 6 -5 5 6 43561.0 1496.23 9 -5 5 5 654.749 69.3396 14 -5 5 5 567.659 64.4643 11 -5 5 5 560.561 65.4841 10 -5 5 5 569.479 63.9326 4 5 5 -4 19865.1 740.669 2 5 5 -4 19683.3 676.004 3 5 5 -4 20171.6 723.882 1 -5 5 4 19177.0 690.148 10 -5 5 4 20064.5 689.887 4 5 5 -3 5645.60 215.993 3 5 5 -2 38935.5 1311.73 3 5 5 -1 699.403 77.3247 1 -5 -5 1 898.990 97.4174 2 5 5 -1 851.623 61.0337 3 5 -5 -1 846.691 59.8152 3 -5 -5 0 6515.29 308.972 2 -5 5 0 6044.47 258.946 11 5 5 0 6799.10 298.456 1 -5 5 0 6932.95 263.400 10 5 -5 0 6714.30 255.798 3 5 5 1 3213.51 147.551 3 -5 5 -1 3112.20 150.242 11 -5 5 -1 3201.81 152.208 5 -5 5 -1 3020.81 149.006 10 5 -5 1 3209.87 142.731 3 -5 5 -2 2212.40 130.697 14 -5 5 -2 1948.54 120.581 5 -5 5 -2 2186.61 118.190 11 -5 5 -2 2112.96 119.929 10 -5 5 -3 7754.19 323.403 14 -5 5 -3 8009.53 320.106 5 -5 5 -3 7541.34 308.567 10 -5 -5 -4 1527.65 104.955 5 -5 5 -4 1418.22 120.903 14 -5 5 -4 1352.00 117.435 5 -5 5 -4 1528.21 104.910 10 -5 5 -5 384.869 96.7655 14 -5 -5 -5 424.896 76.3047 5 -5 5 -5 514.568 96.7799 5 -5 5 -5 548.832 74.7742 10 -5 5 -6 801.130 107.746 14 -5 -5 -6 717.395 87.7372 5 -5 5 -6 814.524 111.290 5 -5 5 -7 174.102 75.6808 14 -5 -5 -7 187.588 61.8833 5 -5 5 -7 94.6686 76.8947 5 -5 -5 -8 1892.54 111.964 5 -5 5 -8 1979.71 124.376 5 -5 -5 -8 1933.36 113.904 10 -5 5 -9 746.525 60.2329 5 -5 -5 -9 657.989 48.2839 5 -5 6 13 1716.42 88.3539 9 5 6 -12 2296.00 132.643 14 -5 6 12 2676.92 135.705 6 -5 6 12 2868.82 138.934 9 -5 -6 12 2405.31 127.814 9 -5 6 11 298.663 73.9506 9 -5 -6 11 142.501 63.3613 9 -5 6 11 176.947 81.5867 6 -5 -6 10 787.424 94.5178 6 -5 6 10 954.589 105.641 9 -5 -6 10 852.001 89.3963 9 -5 -6 9 641.365 81.1925 6 -5 6 9 559.089 88.4901 9 -5 -6 9 715.248 80.9009 9 -5 6 9 654.949 107.514 12 -5 6 9 717.198 99.2880 13 -5 6 9 551.108 89.4915 6 -5 -6 8 136.688 60.8488 6 -5 6 8 153.266 62.8736 9 -5 -6 8 169.355 55.2965 9 -5 6 8 203.864 79.5083 13 -5 6 8 140.446 79.6224 12 -5 6 8 220.395 70.1735 6 -5 6 7 6399.19 271.573 12 -5 6 7 6617.33 257.744 7 -5 6 7 5924.67 260.896 6 -5 -6 7 5869.37 248.697 6 -5 6 7 6262.75 262.173 9 -5 -6 7 5884.67 245.313 9 -5 6 6 2185.87 123.370 11 -5 -6 6 2343.08 115.128 6 -5 6 6 2139.30 124.596 9 -5 6 5 795.030 79.2743 14 -5 6 5 1041.90 80.1761 11 -5 6 5 958.402 74.2325 9 -5 6 5 894.140 76.3650 4 5 6 -4 17093.4 666.461 2 5 6 -4 17567.8 597.460 3 -5 6 4 17527.4 616.711 11 -5 6 4 17122.3 615.028 10 -5 6 4 17391.8 612.839 4 5 6 -4 16702.6 648.920 1 5 6 -3 9140.28 333.332 3 -5 6 3 9271.36 345.962 10 5 6 -2 39859.6 1342.93 3 -5 -6 1 9374.25 387.587 2 5 6 -1 8767.16 326.240 3 -5 6 1 8393.52 331.010 10 5 -6 -1 8913.82 327.655 3 -5 6 0 3687.51 161.602 5 -5 6 0 3288.43 159.440 11 5 6 0 3619.55 196.020 1 5 6 0 3329.20 154.546 3 -5 6 0 3596.37 161.790 10 5 -6 0 3538.88 154.248 3 -5 6 -1 6818.81 281.263 14 -5 6 -1 6971.04 274.815 5 -5 6 -1 7008.52 272.880 11 -5 6 -1 6585.19 270.812 10 5 -6 1 6710.10 263.882 3 -5 6 -2 1500.53 112.297 14 -5 6 -2 1525.05 108.664 5 -5 6 -2 1540.25 97.3692 11 -5 6 -2 1576.12 100.195 10 -5 6 -3 42311.9 1443.64 14 -5 6 -3 41561.0 1436.73 5 -5 6 -3 41417.5 1423.71 10 -5 6 -4 393.896 95.5904 14 -5 -6 -4 308.181 61.5605 5 -5 6 -4 477.236 84.4697 5 -5 6 -4 251.472 63.5028 10 -5 6 -5 12132.7 475.106 14 -5 -6 -5 11243.8 446.325 5 -5 6 -5 11521.2 468.323 5 -5 6 -5 12074.2 443.996 10 -5 6 -6 1661.34 139.039 14 -5 -6 -6 1471.97 112.295 5 -5 6 -6 1349.65 125.335 5 -5 6 -7 48.1966 70.8149 14 -5 -6 -7 110.386 60.1462 5 -5 6 -7 41.5468 78.5830 5 -5 6 -8-3.71371 52.6856 14 -5 -6 -8-6.39492 46.6425 5 -5 7 13 259.741 37.3772 6 -5 7 13 232.929 38.6103 9 -5 7 12 214.790 55.6315 6 -5 7 12 281.669 60.0336 9 -5 7 11 1555.92 116.908 6 -5 7 11 1632.40 118.686 9 -5 -7 11 1662.82 109.133 9 -5 7 10 254.489 84.1577 9 -5 -7 10 136.784 68.7715 9 -5 7 10 113.239 89.9931 12 -5 -7 9 301.104 72.7011 6 -5 7 9 282.470 86.9898 9 -5 7 9 237.747 88.3530 13 -5 7 9 260.487 88.7344 12 -5 -7 9 297.392 65.5528 9 -5 -7 8 1026.09 87.9997 6 -5 7 8 1062.18 99.0059 9 -5 7 8 871.049 104.442 13 -5 7 8 1101.87 111.217 12 -5 7 8 1026.83 99.7127 6 -5 -7 8 1054.11 87.1913 9 -5 7 7 1211.61 96.1250 7 -5 7 7 1287.83 101.299 6 -5 7 7 1284.30 112.985 12 -5 7 7 1199.70 100.589 9 -5 -7 7 1286.17 90.0365 6 -5 7 6 45.2989 55.2817 9 -5 -7 6 59.7805 35.0942 6 -5 7 6 61.6919 67.0546 14 -5 7 6 145.765 54.2137 11 -5 7 6-20.3375 58.7446 7 -5 7 5 26715.5 933.217 11 -5 7 5 27109.1 931.526 9 -5 7 5 27600.7 933.044 4 -5 7 5 25975.4 938.668 14 5 7 -4 6681.16 306.959 1 -5 7 4 6660.28 274.041 14 5 7 -4 6465.06 249.553 3 -5 7 4 7046.29 274.849 11 -5 7 4 6959.62 270.609 10 -5 7 4 6873.40 267.630 4 5 7 -3 55572.9 1860.28 3 -5 7 3 57429.8 1877.62 11 -5 7 3 54228.5 1872.01 10 -5 7 2 40862.9 1389.18 5 5 7 -2 39734.5 1381.51 3 -5 7 2 42801.4 1393.36 10 -5 -7 1 5984.74 304.579 2 -5 7 1 6480.82 262.513 11 5 7 -1 6461.38 253.363 3 -5 7 1 6383.45 258.476 5 -5 7 1 6926.60 261.599 10 -5 7 0 32944.1 1127.06 5 5 7 0 33148.9 1124.30 3 -5 7 0 32547.7 1126.83 11 -5 7 0 32957.8 1125.41 10 5 -7 0 32704.1 1121.46 3 -5 7 -1 20531.5 716.379 14 -5 7 -1 19542.5 705.417 5 -5 7 -1 19512.6 702.621 11 -5 7 -1 19822.0 701.795 10 5 -7 1 20094.5 697.186 3 -5 7 -2 111.608 68.7678 14 -5 7 -2 190.737 54.8158 11 -5 7 -2 119.033 60.2499 5 -5 7 -2 203.862 56.0091 10 -5 7 -3 5669.85 262.450 14 -5 7 -3 5544.38 250.391 5 -5 7 -3 5587.81 238.096 10 -5 7 -4 13827.9 535.386 14 -5 7 -4 14049.4 527.690 5 -5 7 -4 13281.0 502.778 10 -5 7 -5 37778.4 1345.84 14 -5 -7 -5 38016.8 1316.96 5 -5 7 -5 39084.7 1339.10 5 -5 7 -6 57.5161 89.6770 14 -5 -7 -6 54.3965 61.7332 5 -5 7 -7 167.289 78.9813 14 -5 -7 -7 211.500 58.0816 5 -5 7 -8 3457.65 166.789 14 -5 -7 -8 3566.83 155.432 5 -5 8 13 137.113 28.7757 6 -5 8 13 98.8572 32.2717 9 -5 8 12 234.528 57.1918 6 -5 8 12 129.229 55.0360 9 -5 8 11 614.140 82.8751 9 -5 -8 11 813.291 78.5607 9 -5 8 11 754.712 89.0458 6 -5 8 10 37.4313 76.5506 9 -5 -8 10 71.5102 59.9913 9 -5 8 9 7466.65 319.118 13 -5 8 9 7359.28 319.847 9 -5 -8 9 7440.29 307.942 6 -5 -8 9 7399.80 303.224 9 -5 8 8 6342.16 284.395 12 -5 8 8 6231.81 279.916 6 -5 8 8 6326.43 282.708 13 -5 8 8 6327.94 281.819 9 -5 -8 8 6163.58 264.284 6 -5 -8 8 6560.88 264.242 9 -5 8 7 1847.28 130.111 12 -5 8 7 1712.59 108.276 11 -5 8 7 1604.07 112.369 7 -5 8 7 1431.19 114.872 9 -5 -8 7 1750.30 104.834 6 -5 8 6 1950.64 131.002 14 -5 8 6 1936.49 115.668 11 -5 8 6 1922.99 120.923 7 -5 8 6 1748.37 116.881 9 -5 -8 6 1605.87 94.3627 6 -5 8 5 198.444 57.8700 9 -5 8 5 86.8571 62.3884 14 -5 8 5 131.996 59.9539 11 -5 8 5 119.476 55.8755 4 5 8 -4 1953.71 143.028 1 -5 8 4 1972.01 124.878 14 -5 8 4 1996.51 119.214 11 -5 8 4 2100.38 118.469 10 -5 8 4 2005.21 112.683 4 -5 8 3 337.678 64.8374 14 -5 8 3 248.628 62.2401 11 5 8 -3 312.633 39.5781 3 5 8 -2 2330.99 113.026 3 -5 8 2 2326.42 130.965 11 -5 8 2 2350.15 124.634 10 -5 8 1 170.748 59.9674 14 -5 8 1 186.515 56.9710 11 -5 8 1 180.935 50.4348 5 -5 8 1 190.607 52.2243 10 5 8 -1 243.464 40.0930 3 -5 8 0 14510.8 538.584 14 -5 8 0 14360.5 528.717 11 -5 8 0 15100.5 531.938 5 -5 8 0 14599.8 527.634 10 5 -8 0 14422.4 523.107 3 -5 8 -1 106.055 63.2546 14 -5 8 -1 33.7778 47.5854 11 -5 8 -1 73.7036 55.2385 5 -5 8 -1 50.7534 50.3237 10 -5 8 -2 28799.2 988.962 14 -5 8 -2 28305.5 976.888 5 -5 8 -2 27504.1 965.500 11 -5 8 -2 27111.9 963.719 10 -5 8 -3 13274.6 496.393 14 -5 8 -3 12459.8 479.842 5 -5 8 -3 12001.1 461.561 10 -5 8 -4 4571.32 237.337 14 -5 8 -4 4491.11 225.423 5 -5 8 -4 4337.77 198.441 10 -5 8 -5 901.628 123.070 14 -5 8 -6 1742.50 146.480 14 -5 -8 -6 1501.29 104.903 5 -5 8 -7 193.855 81.3213 14 -5 -8 -7 247.326 54.9304 5 -5 8 -8 369.515 65.0722 14 -5 8 -8 503.405 73.1045 5 -5 8 -9 1499.63 79.2452 5 -5 9 13 1031.15 57.9851 9 -5 9 12-18.3923 42.3254 6 -5 9 12-9.73489 48.3137 9 -5 9 11 3501.94 176.273 6 -5 9 11 3575.62 178.203 9 -5 9 10 149.569 79.7722 9 -5 -9 10 208.713 65.1642 9 -5 9 10 201.203 77.8224 6 -5 9 9 5170.54 252.621 13 -5 9 9 5384.35 253.650 9 -5 -9 9 5559.71 237.545 9 -5 9 8 21.7665 67.9756 9 -5 -9 8-20.4365 47.6050 9 -5 9 8 21.4975 77.7415 13 -5 9 7 30.5963 67.4403 9 -5 -9 7 104.435 49.6064 6 -5 9 7 69.8322 65.8021 7 -5 9 6 2246.80 147.852 14 -5 9 6 2286.28 126.639 8 -5 9 6 2298.86 136.390 11 -5 9 6 2428.22 137.459 7 -5 9 6 2218.66 135.562 9 -5 9 5 4010.81 200.159 14 -5 9 5 4048.24 191.315 11 -5 9 5 4216.34 190.698 9 -5 9 4 366.303 73.1102 11 -5 9 4 467.537 69.2521 10 -5 9 3 37757.8 1272.82 14 5 9 -3 35855.6 1245.35 3 -5 9 3 38058.1 1266.60 11 -5 9 3 36620.1 1261.04 10 -5 9 2 35677.9 1207.65 14 5 9 -2 32714.4 1184.14 3 -5 9 2 35400.7 1201.00 11 -5 9 2 36973.4 1199.00 10 -5 9 1 1304.12 101.537 14 5 9 -1 1283.71 81.0343 3 -5 9 1 1388.41 94.9111 5 -5 9 1 1335.42 98.5064 11 -5 9 1 1429.66 95.4832 10 -5 9 0 25896.2 903.640 14 -5 9 0 25495.1 893.777 5 -5 9 0 25422.6 890.945 11 -5 9 0 25432.0 888.613 10 -5 9 -1 1529.75 118.356 14 -5 9 -1 1577.48 110.376 5 -5 9 -1 1546.79 104.176 11 -5 9 -1 1589.66 101.072 10 -5 9 -2 1488.23 125.354 14 -5 9 -2 1402.53 107.611 5 -5 9 -2 1343.80 95.3952 10 -5 9 -3 466.124 103.070 14 -5 9 -3 381.618 62.7336 10 -5 9 -4 5026.75 258.997 14 -5 9 -5 48.8929 97.7847 14 -5 9 -6 3338.25 201.590 14 -5 9 -7 5175.98 248.700 14 -5 9 -7 5502.09 247.095 5 -5 9 -8 217.208 58.6764 14 -5 9 -8 298.564 63.5138 5 -5 10 12-45.4795 44.1471 6 -5 10 12 9.19899 44.8279 9 -5 10 11 791.307 88.7302 9 -5 10 11 667.652 82.8405 6 -5 10 10 758.833 104.308 9 -5 10 10 873.546 107.879 12 -5 10 10 783.608 99.0318 6 -5 10 9 841.380 108.198 9 -5 10 9 913.112 112.480 13 -5 -10 9 802.937 83.8122 9 -5 10 8 7751.18 339.609 13 -5 10 8 7977.55 337.860 9 -5 -10 8 8093.47 317.385 9 -5 10 7 3737.79 184.173 7 -5 10 7 3421.39 186.479 9 -5 10 6 1569.50 131.020 14 -5 10 6 1901.83 115.502 8 -5 10 6 1807.25 123.094 11 -5 10 6 1959.49 124.231 7 -5 10 6 1763.80 126.201 9 -5 10 5 251.124 62.3434 9 -5 10 5 183.588 79.3618 14 -5 10 5 185.539 51.9885 8 -5 10 5 278.969 71.0174 11 -5 10 5 231.991 70.6288 7 -5 10 4 369.447 80.8906 14 -5 10 4 336.305 73.2965 11 -5 10 4 288.690 60.4655 4 -5 10 3 158.536 67.4454 14 -5 10 3 210.718 70.4284 11 -5 10 3 187.235 62.8156 10 5 10 -3 229.959 34.8068 3 -5 10 3 203.238 56.2591 4 -5 10 2 30876.0 1060.31 14 -5 10 2 30503.3 1051.41 11 -5 10 2 30541.8 1047.43 10 5 10 -2 29633.1 1035.87 3 -5 10 1 3648.10 184.491 14 -5 10 1 3605.79 172.732 5 -5 10 1 3616.38 173.955 11 -5 10 1 3505.20 169.068 10 -5 10 0 4592.03 216.656 14 -5 10 0 4387.53 203.482 5 -5 10 0 4531.01 202.435 11 -5 10 0 4358.35 196.035 10 -5 10 -1 1906.36 136.419 14 -5 10 -1 1923.08 117.001 11 -5 10 -1 1920.49 113.992 10 -5 10 -2 11.5444 48.6147 10 -5 10 -3 599.069 109.325 14 -5 10 -4 5695.31 285.153 14 -5 10 -5 17415.9 673.983 14 -5 10 -5 17612.8 656.525 5 -5 10 -6 5671.70 280.990 14 -5 10 -6 6054.04 272.140 5 -5 10 -7 15557.6 602.609 14 -5 10 -7 16921.8 598.917 5 -5 10 -8 6635.96 270.873 14 -5 10 -8 7157.49 273.492 5 -5 11 12 3969.77 167.672 6 -5 11 12 4022.70 170.759 9 -5 11 11 100.513 60.6502 9 -5 11 11 200.615 62.2819 6 -5 11 10 3058.65 181.565 12 -5 11 10 3552.82 182.527 6 -5 11 10 3688.45 187.960 9 -5 11 9 1110.48 113.745 9 -5 11 9 1125.31 119.803 13 -5 11 9 801.434 112.719 12 -5 11 9 1101.40 114.309 6 -5 11 8 3189.77 195.191 13 -5 11 8 3824.56 204.706 12 -5 11 8 3766.67 200.772 9 -5 11 7 5.60048 73.0872 9 -5 11 7 44.8729 85.1767 12 -5 11 7 43.8455 64.5665 8 -5 11 7 89.3085 69.1529 7 -5 11 6 1069.86 103.260 9 -5 11 6 1209.02 120.916 14 -5 11 6 1461.89 102.119 8 -5 11 6 1347.03 112.778 11 -5 11 6 1233.82 105.882 7 -5 11 5 12861.9 479.180 8 -5 11 5 12769.8 486.900 11 -5 11 5 12760.0 499.141 14 -5 11 5 13081.9 493.509 7 -5 11 5 12840.4 482.759 4 -5 11 4 78.0703 50.0590 8 -5 11 4 120.149 68.7097 11 -5 11 4 96.1544 73.2825 14 -5 11 4 43.7491 53.4190 4 -5 11 3 12228.7 471.536 14 -5 11 3 12246.1 455.066 4 -5 11 3 12222.3 457.817 10 -5 11 2 920.194 100.873 14 -5 11 2 1076.54 93.5856 11 -5 11 2 926.168 84.8335 10 -5 11 1 837.775 96.8678 14 -5 11 1 913.885 86.1894 11 -5 11 1 965.308 88.1372 5 -5 11 1 851.250 81.6799 10 -5 11 0 1986.59 141.649 14 -5 11 0 2243.00 124.082 8 -5 11 0 2178.78 128.674 11 -5 11 0 2395.61 127.376 10 -5 11 -1 2497.58 163.569 14 -5 11 -1 2578.03 140.218 8 -5 11 -1 2863.52 145.145 11 -5 11 -1 2457.06 134.563 10 -5 11 -2 8528.54 371.424 14 -5 11 -2 9199.09 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379.730 77.7226 13 -7 19 7 521.324 90.3235 12 -7 19 6 1657.48 139.120 14 -7 19 6 1720.02 136.975 12 -7 19 6 1893.50 124.495 7 -7 19 6 1453.88 114.516 9 -7 19 5 2139.45 156.972 14 -7 19 5 2037.90 138.323 7 -7 19 5 2009.74 135.104 9 -7 19 4 900.069 94.6158 7 -7 19 4 951.036 123.823 14 -7 19 3 6786.58 310.283 14 -7 19 3 6634.39 292.519 11 -7 19 3 6228.02 274.142 7 -7 19 3 6520.26 278.309 4 -7 19 2 1288.10 135.260 14 -7 19 2 1123.57 100.004 7 -7 19 2 1288.44 118.190 11 -7 19 2 1259.25 106.325 4 -7 19 1 8602.13 363.224 14 -7 19 1 7915.18 335.637 11 -7 19 1 8306.81 324.065 7 -7 19 1 8274.12 331.102 4 -7 19 0 910.629 122.302 14 -7 19 0 928.087 85.2457 4 -7 19 -1-22.5192 87.4365 14 -7 19 -1 61.0926 49.5263 4 -7 19 -2 2830.60 157.589 14 -7 19 -2 2648.26 127.083 4 -7 19 -3 1624.02 111.630 14 -7 19 -4 2987.80 144.787 14 -7 -19 -4 3968.44 154.163 11 -7 20 9 6315.85 232.636 12 -7 20 9 5811.45 229.457 9 -7 20 8 75.7595 47.4143 9 -7 20 8 113.805 54.6829 13 -7 20 8 55.4099 55.9579 12 -7 20 8-3.41801 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350.252 58.4986 6 -8 2 9 13216.1 485.263 12 -8 2 9 12923.7 483.256 6 -8 -2 9 12775.5 475.396 6 -8 2 8 559.805 76.5687 13 -8 2 8 548.074 76.6092 12 -8 2 8 552.070 67.0911 6 -8 2 7 1564.77 110.960 12 -8 2 7 1971.55 124.343 7 -8 2 6 7970.21 334.407 11 -8 2 6 8316.06 332.132 10 -8 2 6 8234.50 325.465 4 -8 -2 5 12311.9 477.247 11 -8 2 5 13535.1 488.940 11 -8 2 5 12423.7 477.675 10 -8 2 5 12075.1 467.768 4 -8 -2 4 4303.31 210.478 11 -8 2 4 4248.57 214.256 11 -8 -2 4 4271.16 200.394 10 -8 2 4 3973.02 193.600 4 -8 2 4 4331.05 207.333 10 -8 -2 3 383.188 82.7631 11 -8 2 3 639.154 99.2648 11 -8 -2 3 591.100 81.7064 10 -8 2 3 515.517 83.7951 10 -8 -2 2 39781.8 1362.92 11 -8 2 2 36969.2 1359.03 11 -8 -2 2 39346.1 1352.07 10 -8 2 2 40415.7 1357.60 10 -8 2 1 7821.28 324.476 11 -8 -2 1 7085.26 308.092 10 -8 2 1 6873.24 310.812 10 -8 -2 0 60123.7 1992.51 11 -8 2 0 58058.7 1988.61 11 -8 -2 0 56297.7 1980.17 10 -8 2 -1 5808.93 248.598 5 -8 -2 -1 5152.21 264.480 11 -8 2 -1 6149.07 271.097 11 -8 -2 -1 5106.86 262.817 10 -8 2 -1 5737.24 268.770 10 -8 -2 -2 1113.12 118.385 11 -8 2 -2 1119.89 113.204 11 -8 2 -2 1054.52 97.6504 5 -8 2 -2 1181.79 126.309 10 -8 2 -3 7858.15 323.205 5 -8 -2 -3 7821.44 331.496 11 -8 2 -3 8281.78 329.291 11 -8 -2 -3 7816.98 346.641 10 -8 2 -3 8036.51 341.447 10 -8 2 -4 3068.68 159.599 5 -8 -2 -4 3033.51 159.528 11 -8 -2 -4 3485.26 181.270 10 -8 2 -4 3457.72 174.081 10 -8 2 -5 4007.54 179.193 5 -8 2 -5 3916.85 185.318 10 -8 2 -6 4369.83 181.719 5 -8 2 -6 4763.59 183.625 10 -8 3 12 531.422 58.0394 6 -8 3 11 5610.49 231.599 6 -8 -3 11 5413.58 221.568 6 -8 3 10 4931.34 216.860 12 -8 3 10 4973.44 216.569 6 -8 -3 10 4641.38 205.097 6 -8 3 9 29.1855 57.3287 13 -8 3 9 139.601 65.4442 12 -8 3 9 31.0320 52.8358 6 -8 3 8 402.047 74.9615 13 -8 3 8 490.265 77.6555 12 -8 3 8 535.876 71.5959 6 -8 3 7 41.0831 58.5613 12 -8 3 7 208.113 75.5122 7 -8 3 6 48.7761 57.5580 12 -8 3 6-20.2171 66.9721 11 -8 3 6 43.3363 63.3189 10 -8 3 6 26.1715 57.3600 4 -8 -3 5 3801.99 198.155 11 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57.0381 5 -8 -3 -4 19.5225 75.9391 10 -8 3 -4 22.9821 68.5763 10 -8 3 -5 1102.55 82.0647 5 -8 -3 -5 1203.60 96.4603 10 -8 3 -5 1249.47 88.8219 10 -8 3 -6 3998.49 170.434 5 -8 -3 -6 5054.30 184.010 10 -8 4 12 964.559 69.5351 6 -8 4 11 1803.30 110.860 6 -8 4 10 6997.39 289.843 13 -8 4 10 7484.35 300.846 12 -8 4 10 7524.38 300.468 6 -8 4 9 4430.85 205.410 13 -8 4 9 4103.93 204.977 12 -8 4 9 4598.46 207.693 6 -8 4 8 15528.6 579.104 13 -8 4 8 15297.0 579.354 12 -8 4 8 15368.7 572.055 7 -8 4 8 16447.6 577.685 6 -8 4 7 946.931 98.6153 12 -8 4 7 995.832 98.3366 11 -8 4 7 989.880 103.472 7 -8 4 7 1080.52 88.7822 6 -8 4 6 31470.5 1136.09 12 -8 4 6 33368.3 1146.42 11 -8 4 6 34012.2 1144.27 10 -8 4 6 32227.0 1137.45 4 -8 -4 5 90364.3 3043.70 11 -8 4 5 93094.1 3055.99 11 -8 4 5 91731.5 3050.46 10 -8 4 5 88507.6 3044.33 4 -8 -4 4 26484.6 918.807 11 -8 4 4 26131.3 926.485 11 -8 4 4 25032.0 912.685 4 -8 4 4 25854.0 920.460 10 -8 -4 3 6897.50 303.495 11 -8 4 3 7029.52 311.904 11 -8 -4 3 7493.41 294.776 10 -8 4 3 6614.59 301.989 10 -8 -4 2 2887.14 172.385 11 -8 -4 2 2917.16 160.696 10 -8 4 2 2984.58 171.932 10 -8 4 1 4048.21 196.794 5 -8 -4 1 4064.65 216.267 11 -8 4 1 4075.50 220.513 11 -8 -4 1 4248.09 208.849 10 -8 4 0 7416.99 306.395 5 -8 -4 0 7003.72 326.161 11 -8 4 0 7241.17 322.001 11 -8 -4 0 7227.54 316.635 10 -8 4 0 7593.81 322.700 10 -8 4 -1 4224.16 208.305 5 -8 -4 -1 4457.01 230.848 11 -8 4 -1 4124.40 221.701 11 -8 -4 -1 4316.79 220.668 10 -8 4 -1 4275.24 220.846 10 -8 4 -2 10823.9 422.704 5 -8 -4 -2 10503.6 432.910 11 -8 4 -2 10614.6 424.184 11 -8 -4 -2 10578.0 432.849 10 -8 4 -2 11070.1 434.491 10 -8 4 -3 11603.4 442.943 5 -8 -4 -3 11274.2 447.219 11 -8 4 -3 11183.5 432.991 11 -8 4 -3 11503.4 448.418 10 -8 4 -4 3612.05 176.825 5 -8 -4 -4 3655.04 176.000 11 -8 -4 -4 3462.21 186.526 10 -8 4 -4 3520.70 179.961 10 -8 4 -5 1291.35 89.6044 5 -8 -4 -5 1325.29 103.033 10 -8 4 -5 1328.87 88.4296 10 -8 4 -6 31.5782 29.4992 5 -8 -4 -6 59.5746 41.3071 10 -8 5 12 1267.23 78.7164 6 -8 5 11 21.9529 52.7057 6 -8 5 10 373.259 68.1058 13 -8 5 10 144.044 69.6245 12 -8 5 10 229.098 62.1338 6 -8 5 9 1786.60 120.918 13 -8 5 9 1618.43 121.164 12 -8 5 9 1598.81 113.418 6 -8 5 8 5219.97 248.006 12 -8 5 8 5463.87 240.783 7 -8 5 8 5754.37 244.678 6 -8 5 7-20.3586 66.0594 12 -8 5 7-14.7502 67.2495 11 -8 5 7 57.7521 67.7836 7 -8 5 7 8.89673 54.4522 6 -8 5 6 170.812 79.7023 11 -8 5 6 57.4078 66.4448 4 -8 -5 5 51970.5 1792.71 11 -8 5 5 52058.9 1806.70 11 -8 5 5 52445.7 1802.00 10 -8 5 5 54342.1 1798.56 4 -8 -5 4 2579.60 149.812 11 -8 5 4 2393.22 158.905 11 -8 5 4 2269.74 143.720 4 -8 5 4 2339.88 151.029 10 -8 -5 3 9418.52 387.136 11 -8 5 3 9609.51 394.987 11 -8 -5 3 9605.76 373.525 10 -8 5 3 9470.89 389.635 10 -8 -5 2 2620.46 165.484 11 -8 -5 2 3037.00 161.472 10 -8 5 2 2760.16 167.342 10 -8 -5 1 779.152 106.193 11 -8 5 1 827.548 113.968 11 -8 5 1 674.328 84.0673 5 -8 -5 1 811.132 98.1446 10 -8 5 0 554.466 99.5719 11 -8 5 0 577.644 82.6327 5 -8 -5 0 574.434 96.5438 10 -8 5 0 533.545 101.590 10 -8 -5 -1 1103.45 128.792 11 -8 5 -1 1176.17 119.964 11 -8 5 -1 1116.75 104.996 5 -8 -5 -1 949.061 110.745 10 -8 5 -1 1157.19 118.812 10 -8 5 -2 5177.87 235.993 5 -8 -5 -2 5255.69 247.981 11 -8 5 -2 4751.12 232.115 11 -8 -5 -2 4701.39 241.852 10 -8 5 -2 5034.21 244.184 10 -8 5 -3 2488.26 151.258 5 -8 -5 -3 2542.90 156.491 11 -8 5 -3 2440.36 154.577 10 -8 5 -4 18715.4 688.922 5 -8 -5 -4 18928.6 685.942 11 -8 5 -4 19885.1 689.574 10 -8 5 -5 107.374 52.8080 5 -8 -5 -5 37.3765 61.0887 10 -8 5 -5 34.6203 43.8442 10 -8 5 -6 80.2299 32.0127 5 -8 -5 -6 51.1385 40.3703 10 -8 6 12 33.6243 39.4366 6 -8 6 11 2274.67 125.735 6 -8 6 10 836.777 85.9309 13 -8 6 10 803.427 90.9307 12 -8 6 10 732.489 82.3527 6 -8 6 9 454.177 87.6273 13 -8 6 9 566.676 89.5469 12 -8 6 9 383.147 67.5085 7 -8 6 9 541.303 76.8018 6 -8 6 8 891.185 103.814 12 -8 6 8 953.024 92.5538 7 -8 6 8 693.838 82.5284 6 -8 6 7 462.586 88.9416 12 -8 6 7 470.704 81.0039 11 -8 6 7 720.394 100.956 7 -8 6 7 560.685 73.9210 6 -8 6 6 438.579 85.2775 11 -8 6 6 478.675 68.4583 6 -8 6 6 485.978 84.6804 4 -8 -6 5 3052.33 160.028 11 -8 6 5 3041.75 176.216 11 -8 6 5 3275.60 174.369 10 -8 -6 4 652.451 89.9742 11 -8 6 4 743.066 107.750 11 -8 6 4 671.652 99.3641 10 -8 6 4 513.406 91.2233 4 -8 -6 3 6263.91 283.286 11 -8 6 3 6602.41 295.378 11 -8 -6 3 6371.43 270.279 10 -8 6 3 6535.68 288.216 10 -8 -6 2 4699.00 232.000 11 -8 6 2 4378.78 233.475 11 -8 -6 2 4852.10 218.333 10 -8 -6 1 35.6830 86.5885 11 -8 6 1 117.516 89.3988 11 -8 6 1 65.2750 62.9240 5 -8 -6 1-20.7976 69.0840 10 -8 6 1 113.732 88.0001 10 -8 6 0 7541.48 332.108 5 -8 6 0 8329.55 348.782 11 -8 -6 0 7927.21 340.166 10 -8 6 0 8459.17 347.570 10 -8 -6 -1 626.835 107.360 11 -8 6 -1 456.773 91.4534 11 -8 6 -1 453.977 83.0764 5 -8 -6 -1 481.606 97.0923 10 -8 6 -1 562.249 98.7937 10 -8 -6 -2 393.971 99.5313 11 -8 6 -2 529.048 85.8052 11 -8 6 -2 568.745 86.2503 5 -8 -6 -2 479.620 100.387 10 -8 6 -2 401.973 92.6483 10 -8 -6 -3 20.9601 72.5318 11 -8 6 -3 190.423 70.9663 5 -8 -6 -3 321.332 93.5369 10 -8 6 -3 163.158 75.2453 10 -8 6 -4 8254.75 342.280 5 -8 -6 -4 8892.69 343.242 11 -8 6 -4 8803.24 340.535 10 -8 6 -5 9312.78 364.155 5 -8 -6 -5 10217.3 373.141 10 -8 6 -6 446.767 42.6132 5 -8 -6 -6 419.347 49.8245 10 -8 7 12 855.424 64.1313 6 -8 7 11 1270.76 92.0589 6 -8 7 10 136.487 67.1439 13 -8 7 10 58.0795 68.6193 12 -8 7 10 194.889 64.4963 6 -8 7 9 1973.11 136.694 13 -8 7 9 1986.29 134.498 12 -8 7 9 1937.12 120.722 7 -8 7 9 1953.98 126.662 6 -8 7 8 791.482 97.9941 12 -8 7 8 866.075 93.9159 7 -8 7 8 753.302 88.2650 6 -8 7 7 21116.0 775.937 12 -8 7 7 20653.2 770.811 11 -8 7 7 20616.9 765.169 6 -8 7 6 3898.12 207.378 11 -8 7 6 3778.69 184.075 6 -8 7 6 3719.31 198.295 4 -8 7 5 1963.13 146.928 11 -8 7 5 1943.20 141.086 10 -8 7 5 1955.20 137.292 4 -8 -7 4 9079.46 372.201 11 -8 7 4 9940.19 392.813 11 -8 7 4 9039.88 375.271 4 -8 7 4 9356.66 384.869 10 -8 -7 3 6264.46 285.698 11 -8 7 3 6379.12 297.100 11 -8 7 3 6885.00 295.563 10 -8 -7 2 2083.39 152.499 11 -8 7 2 2340.80 160.267 11 -8 -7 2 2582.74 144.353 10 -8 -7 1 4949.64 246.452 11 -8 -7 1 5250.48 233.892 10 -8 7 1 5157.64 245.952 10 -8 7 0 1405.74 120.692 5 -8 7 0 1498.88 131.515 11 -8 -7 0 1442.68 122.226 10 -8 7 0 1352.77 126.330 10 -8 7 -1 1296.65 116.263 5 -8 -7 -1 1435.93 132.955 11 -8 7 -1 1303.03 117.888 11 -8 -7 -1 1199.51 119.562 10 -8 7 -1 1416.82 123.913 10 -8 -7 -2 70.2820 93.8406 11 -8 7 -2 184.669 68.4547 11 -8 7 -2 86.0534 74.1961 5 -8 -7 -2 191.717 93.8725 10 -8 7 -2 75.0458 80.5455 10 -8 7 -3 1705.41 123.461 5 -8 -7 -3 1656.79 127.022 11 -8 -7 -3 1713.17 134.750 10 -8 7 -3 1762.27 123.291 10 -8 7 -4 1257.37 103.520 5 -8 -7 -4 1499.84 105.595 11 -8 7 -4 1263.35 95.0594 10 -8 7 -5 1526.00 95.8941 5 -8 -7 -5 1426.22 101.492 10 -8 7 -6 3141.70 134.142 5 -8 -7 -6 3466.79 140.640 10 -8 8 12-28.4593 34.8234 6 -8 8 11 411.377 63.5602 6 -8 8 10 958.645 96.4495 13 -8 8 10 1118.99 102.461 12 -8 8 10 1155.16 95.2811 6 -8 8 9 5468.29 247.600 13 -8 8 9 4933.12 240.531 12 -8 8 9 5396.41 238.072 6 -8 8 8 18010.6 668.023 12 -8 8 8 17789.4 653.145 11 -8 8 8 17971.6 658.035 7 -8 8 8 18353.8 662.100 6 -8 8 7 1720.66 140.527 12 -8 8 7 1866.29 137.228 11 -8 8 7 2193.38 147.705 7 -8 8 7 1980.76 129.594 6 -8 8 6 34648.6 1194.00 11 -8 8 6 33208.5 1186.27 4 -8 8 5 2417.89 160.413 11 -8 8 5 2260.29 154.959 10 -8 8 5 2260.88 151.107 4 -8 -8 4 11940.0 456.991 11 -8 8 4 11308.7 467.937 11 -8 8 4 12422.8 468.675 10 -8 8 4 11438.3 458.605 4 -8 -8 3 408.798 88.1251 11 -8 -8 2 14710.2 549.154 11 -8 8 2 14123.4 552.157 11 -8 -8 2 14318.6 531.060 10 -8 8 2 13672.1 545.852 10 -8 -8 1 3772.23 211.462 11 -8 8 1 3576.45 204.729 11 -8 -8 1 3911.63 197.792 10 -8 8 1 4020.07 209.994 10 -8 8 0 39.9457 81.1479 11 -8 8 0 27.3368 68.5063 5 -8 -8 0 27.5261 78.4576 10 -8 8 0 97.6313 87.7093 10 -8 -8 -1 79.5332 94.4824 11 -8 8 -1-5.35610 75.8182 11 -8 8 -1 11.0635 73.2939 5 -8 -8 -1-5.66121 80.3142 10 -8 8 -1-22.3024 82.5107 10 -8 -8 -2 650.666 114.169 11 -8 8 -2 761.158 89.1374 11 -8 8 -2 797.944 100.403 5 -8 -8 -2 870.397 104.379 10 -8 8 -2 866.413 101.574 10 -8 -8 -3 133.172 77.3658 11 -8 8 -3 256.162 78.0544 5 -8 -8 -3 87.0445 83.9681 10 -8 8 -3 183.504 66.3319 10 -8 8 -4 6370.67 268.643 5 -8 -8 -4 6610.03 264.701 11 -8 -8 -4 5977.94 267.622 10 -8 8 -4 6266.75 253.981 10 -8 8 -5-9.62228 46.7887 5 -8 8 -6 43.4821 26.9084 5 -8 -8 -6 29.3181 34.2333 10 -8 9 12 357.937 44.1262 6 -8 9 11 9965.94 373.523 6 -8 9 10 1179.68 100.610 13 -8 9 10 1353.26 106.540 12 -8 9 10 1204.16 96.5001 6 -8 9 10 1083.23 83.1467 9 -8 9 9 900.152 107.623 13 -8 9 9 1018.98 110.167 12 -8 9 9 1216.76 101.791 6 -8 9 8 1565.62 132.162 12 -8 9 8 1594.09 116.387 11 -8 9 8 1831.97 127.110 7 -8 9 8 1735.37 127.673 6 -8 9 7 3451.86 196.530 12 -8 9 7 3608.39 190.895 11 -8 9 7 3893.09 197.300 7 -8 9 7 3306.18 183.543 6 -8 9 6 2029.75 149.122 11 -8 9 6 1947.53 143.319 4 -8 9 5 13958.3 548.318 11 -8 9 5 14184.1 543.293 10 -8 9 5 14113.6 537.756 4 -8 -9 4 3555.04 183.836 11 -8 9 4 3504.11 202.958 11 -8 9 4 3297.45 197.657 10 -8 9 4 3422.02 187.948 4 -8 -9 3 19766.4 724.613 11 -8 -9 2 23.3557 86.0601 11 -8 9 2 65.8620 90.9101 11 -8 9 2-17.4229 88.3493 10 -8 -9 1 10031.3 419.630 11 -8 9 1 9886.91 411.717 11 -8 -9 1 10308.5 402.373 10 -8 9 1 10249.9 416.429 10 -8 -9 0 1753.40 147.371 11 -8 9 0 1486.10 123.036 5 -8 9 0 1584.72 132.270 11 -8 -9 0 1679.63 127.494 10 -8 9 0 1705.10 137.579 10 -8 9 -1 1684.32 135.091 5 -8 -9 -1 1964.20 152.375 11 -8 9 -1 1569.62 123.693 11 -8 -9 -1 2076.45 140.440 10 -8 9 -1 1823.62 135.368 10 -8 -9 -2 1426.75 127.124 11 -8 9 -2 1000.33 94.5721 11 -8 9 -2 1010.81 105.875 5 -8 -9 -2 1089.33 112.888 10 -8 9 -2 1078.81 106.094 10 -8 -9 -3 572.916 91.2795 11 -8 9 -3 846.302 96.2354 5 -8 -9 -3 634.427 94.6927 10 -8 9 -3 626.137 79.4461 10 -8 9 -4 4272.40 201.372 5 -8 -9 -4 4297.17 196.654 11 -8 -9 -4 4244.27 200.948 10 -8 9 -5 1143.71 81.3850 5 -8 -9 -6 255.604 37.1492 10 -8 10 12 262.555 36.5067 6 -8 10 11 4843.70 202.779 12 -8 10 11 4518.38 197.352 6 -8 10 10 404.913 57.9334 9 -8 10 10 369.392 74.3379 13 -8 10 10 446.546 77.3422 12 -8 10 10 416.111 73.4927 6 -8 10 9 9195.00 366.670 13 -8 10 9 8778.43 367.462 12 -8 10 9 9252.56 365.121 6 -8 10 9 8954.58 350.813 9 -8 10 8 2414.13 155.593 12 -8 10 8 2088.02 137.951 11 -8 10 8 2519.30 150.369 7 -8 10 8 2611.85 149.749 6 -8 10 7 20464.1 781.779 12 -8 10 7 21053.2 775.392 11 -8 10 7 22261.5 779.123 7 -8 10 7 21430.4 773.216 6 -8 10 6 269.643 86.4564 4 -8 10 6 343.911 101.330 11 -8 10 6 180.192 96.5315 7 -8 10 5 2266.86 144.369 14 -8 10 5 1815.72 151.637 11 -8 10 5 2122.48 146.647 4 -8 10 4 536.409 90.0164 14 -8 -10 4 283.921 77.7771 11 -8 10 4 476.293 106.072 11 -8 10 4 458.524 90.2139 4 -8 -10 3 44.5104 83.1982 11 -8 10 3 111.604 99.8905 10 -8 -10 2 583.836 104.399 11 -8 10 2 468.468 105.365 11 -8 10 2 507.529 108.154 10 -8 -10 1 16038.2 626.641 11 -8 10 1 16137.6 620.147 11 -8 -10 1 16941.6 611.825 10 -8 10 1 16830.6 623.324 10 -8 -10 0 8875.22 378.801 11 -8 10 0 8844.22 370.625 5 -8 10 0 8519.54 367.684 11 -8 -10 0 9162.71 367.765 10 -8 10 0 9149.76 371.255 10 -8 10 -1 360.684 82.7625 11 -8 10 -1 444.688 89.3205 5 -8 -10 -1 447.882 98.0371 10 -8 10 -1 347.462 86.6937 10 -8 10 -2 2130.53 146.134 5 -8 -10 -2 2256.88 159.857 11 -8 -10 -2 2245.19 149.073 10 -8 10 -2 2273.92 141.050 10 -8 -10 -3 465.392 91.5731 11 -8 10 -3 513.453 84.1692 5 -8 -10 -3 585.248 90.8233 10 -8 10 -3 541.333 72.8862 10 -8 10 -4 3176.49 159.204 5 -8 -10 -4 2972.31 152.048 11 -8 -10 -4 2791.10 152.958 10 -8 10 -5 148.857 45.8573 5 -8 -10 -5 162.786 54.2061 10 -8 11 12 2194.38 96.7360 6 -8 11 11 1073.40 83.7191 12 -8 11 11 1147.49 78.4598 6 -8 11 10-12.8655 43.4696 9 -8 11 10-11.7639 64.3787 13 -8 11 10 53.7316 69.5114 12 -8 11 10-43.7120 51.8487 6 -8 11 9 27.5084 51.4142 9 -8 11 9 19.2221 74.7690 13 -8 11 9-14.9525 82.5023 12 -8 11 9 56.5746 60.3870 6 -8 11 8 1695.16 138.316 12 -8 11 8 1742.32 126.755 7 -8 11 8 1860.44 126.565 6 -8 11 7 1767.35 142.290 12 -8 11 7 1940.21 143.829 11 -8 11 7 1869.41 139.017 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153.417 10 -9 4 6 2286.82 139.551 4 -9 -4 5 11889.7 478.903 11 -9 4 5 12586.4 491.761 11 -9 4 5 12499.8 486.900 10 -9 4 5 12808.9 478.816 4 -9 -4 4 1028.46 115.221 11 -9 4 4 1245.03 128.202 11 -9 -4 4 934.516 95.7990 10 -9 4 4 1143.15 118.263 10 -9 4 4 1034.12 105.714 4 -9 -4 3 79537.6 2661.52 11 -9 4 3 79666.9 2667.24 11 -9 -4 3 79526.7 2649.37 10 -9 4 3 75551.1 2659.52 10 -9 -4 2 7741.04 344.496 11 -9 -4 2 8149.43 333.312 10 -9 4 2 7574.74 339.451 10 -9 -4 1 15078.3 615.395 11 -9 -4 1 16177.3 608.777 10 -9 -4 0 16436.8 623.553 11 -9 4 0 16612.9 619.820 11 -9 -4 0 16652.5 614.305 10 -9 4 0 15375.6 615.261 10 -9 4 -1 7004.37 299.861 5 -9 -4 -1 7789.43 326.847 11 -9 4 -1 7482.03 322.388 11 -9 -4 -1 7305.19 321.380 10 -9 4 -1 7401.93 322.858 10 -9 4 -2 1088.19 90.4829 5 -9 -4 -2 1179.38 113.413 11 -9 4 -2 1205.80 104.751 11 -9 -4 -2 979.512 111.035 10 -9 4 -2 1036.92 115.893 10 -9 4 -3 5474.20 228.827 5 -9 -4 -3 5578.15 240.898 11 -9 4 -3 5605.90 244.663 10 -9 -4 -4 3080.87 144.808 10 -9 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2735.03 167.948 10 -9 -10 -1 7396.61 320.907 11 -9 10 -1 7096.15 301.105 11 -9 -10 -1 8013.06 311.741 10 -9 10 -1 7255.27 309.914 10 -9 -10 -2 158.864 75.0256 11 -9 -10 -2 53.7804 62.9540 10 -9 10 -2-3.72976 55.7759 10 -9 -10 -3 230.047 65.1500 11 -9 -10 -3 119.013 57.2038 10 -9 10 -3 181.016 41.5722 10 -9 -10 -4 1913.55 92.1160 11 -9 -10 -4 2043.10 102.124 10 -9 11 11 129.624 32.8679 6 -9 11 10 186.057 61.0092 13 -9 11 10 158.674 59.1076 12 -9 11 10 311.068 54.8171 6 -9 11 9 101.926 71.7191 13 -9 11 9-16.7662 64.2504 12 -9 11 9-11.2093 49.6328 6 -9 11 8 3512.20 186.108 12 -9 11 8 3281.18 172.347 7 -9 11 8 3633.77 173.319 6 -9 11 7 3832.69 203.607 12 -9 11 7 3857.19 202.920 11 -9 11 7 4209.10 204.383 7 -9 11 7 3889.23 189.287 6 -9 11 6 15345.9 568.524 11 -9 11 6 16479.2 578.317 7 -9 11 6 14777.9 559.096 4 -9 11 5 4914.98 248.686 11 -9 11 5 4828.61 237.109 4 -9 -11 4 1271.57 107.422 11 -9 11 4 1057.22 133.483 11 -9 11 4 1363.79 123.362 4 -9 -11 3 297.236 91.5655 11 -9 11 3 405.590 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1431.14 95.0149 6 -9 13 8 1915.81 126.618 13 -9 13 8 1788.55 121.903 12 -9 13 8 1857.55 122.420 7 -9 13 8 1636.77 110.187 6 -9 13 7 10434.9 420.296 12 -9 13 7 10912.7 419.823 11 -9 13 7 10619.6 414.852 7 -9 13 7 10575.0 407.516 6 -9 13 6 49.6644 78.9767 11 -9 13 6-78.7352 87.5848 7 -9 13 6-30.6714 53.6408 6 -9 13 5 898.498 96.8245 14 -9 13 5 1215.18 127.865 11 -9 13 5 1203.07 118.056 4 -9 -13 4 52.4605 62.5710 11 -9 -13 3 4277.25 216.667 11 -9 13 3 4294.32 227.886 11 -9 13 3 4661.85 228.290 10 -9 -13 2 5500.21 256.417 11 -9 13 2 5766.88 262.197 11 -9 13 2 5140.02 250.467 10 -9 -13 1 116.261 83.5622 11 -9 13 1 166.252 80.1045 11 -9 13 1 179.323 80.1215 10 -9 -13 0 2842.62 163.248 11 -9 13 0 2491.06 145.437 11 -9 13 0 2444.34 145.678 10 -9 -13 -1 235.261 57.9973 10 -9 13 -1 291.071 59.1786 10 -9 -13 -2 2671.66 139.228 11 -9 -13 -2 2360.25 123.820 10 -9 -13 -3 615.781 62.2707 11 -9 -13 -3 580.144 53.5865 10 -9 14 10 400.340 51.8921 13 -9 14 10 454.297 54.5565 12 -9 14 10 360.893 42.9655 6 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95.5095 13 -9 18 7 1342.57 93.5088 12 -9 18 7 1243.72 81.4199 6 -9 18 6 128.398 64.5139 12 -9 18 6 181.384 63.8703 7 -9 18 6 168.033 47.7210 6 -9 18 5 67.1448 64.0450 7 -9 18 4 2483.85 143.433 14 -9 18 4 2792.72 155.271 11 -9 18 4 2843.67 144.722 7 -9 18 4 3071.43 150.675 4 -9 18 3 269.107 63.2587 14 -9 18 3 446.770 77.9293 11 -9 18 3 457.618 68.5906 7 -9 18 3 331.589 67.7169 4 -9 18 2 2706.99 143.235 14 -9 -18 2 2976.22 147.475 11 -9 18 2 2840.51 149.118 11 -9 18 2 2992.57 141.216 7 -9 18 2 2920.81 147.039 4 -9 18 1 1057.68 81.8632 14 -9 -18 1 1251.13 96.1545 11 -9 18 1 1116.14 74.6126 7 -9 18 1 1263.75 88.6241 4 -9 -18 0 147.447 59.5370 11 -9 18 0 71.7590 42.2934 4 -9 -18 -1 33.6147 45.3090 11 -9 18 -1 17.7318 29.6915 4 -9 19 8 2123.38 97.6631 13 -9 19 8 1840.05 88.8400 6 -9 19 7 1038.49 76.7819 13 -9 19 7 1041.77 68.1783 6 -9 19 6 1442.93 95.7183 13 -9 19 6 1242.40 81.5632 6 -9 19 5 1031.05 79.7766 7 -9 19 4 420.936 65.9929 14 -9 19 4 399.871 60.8570 7 -9 19 3 2228.84 125.346 14 -9 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341.125 10 -10 3 1 1217.70 129.866 11 -10 -3 1 1192.28 118.384 10 -10 3 1 1352.31 130.357 10 -10 -3 0 6620.43 301.103 11 -10 3 0 6467.82 294.357 11 -10 -3 0 6837.70 292.490 10 -10 -3 -1 2298.26 144.629 11 -10 3 -1 2164.53 139.900 11 -10 -3 -1 2427.20 146.935 10 -10 3 -1 2306.06 147.375 10 -10 -3 -2 4007.04 185.780 11 -10 3 -2 3939.28 176.650 11 -10 -3 -2 4011.14 186.968 10 -10 3 -2 4072.32 190.624 10 -10 -3 -3 1002.09 67.4299 11 -10 3 -3 1132.96 77.6938 10 -10 4 7 20921.5 784.468 11 -10 4 7 23252.9 792.321 7 -10 4 6-21.7829 58.1589 4 -10 4 6 75.8013 83.1494 11 -10 -4 5 64.1774 76.0845 11 -10 4 5 146.761 86.2075 11 -10 4 5 21.5015 81.0262 10 -10 4 5 93.1738 68.8521 4 -10 -4 4 13453.7 516.387 11 -10 4 4 13057.6 522.713 11 -10 -4 4 12745.6 496.433 10 -10 4 4 13726.3 517.224 10 -10 4 4 13264.3 502.386 4 -10 -4 3 9494.46 397.100 11 -10 4 3 9694.40 406.720 11 -10 -4 3 9529.61 385.839 10 -10 4 3 9934.77 386.285 4 -10 4 3 9005.76 390.942 10 -10 -4 2 4425.84 239.951 11 -10 -4 2 4910.16 230.173 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4751.55 245.921 11 -10 -5 2 4158.60 214.181 10 -10 5 2 4311.24 228.546 10 -10 -5 1 17993.8 694.875 11 -10 5 1 18545.0 694.571 11 -10 -5 1 19481.9 688.649 10 -10 -5 0 400.086 102.586 11 -10 5 0 560.128 96.4666 11 -10 -5 0 653.178 96.4296 10 -10 5 0 611.905 97.8030 10 -10 -5 -1 505.273 88.5155 11 -10 5 -1 537.520 78.8880 11 -10 -5 -1 299.532 79.6720 10 -10 5 -1 350.264 77.7264 10 -10 -5 -2 5688.28 234.180 11 -10 5 -2 5156.29 216.827 11 -10 -5 -2 5403.31 232.128 10 -10 5 -2 5921.75 236.558 10 -10 -5 -3-8.94059 36.6958 11 -10 -5 -3-19.2675 47.8604 10 -10 5 -3 41.2723 39.7927 10 -10 6 9 106.460 51.0405 13 -10 6 8 2453.91 137.561 13 -10 6 8 2599.08 136.551 7 -10 6 7 181.211 77.1287 11 -10 6 7 212.462 81.7704 7 -10 6 6 304.264 77.5959 4 -10 6 6 251.309 90.6073 11 -10 -6 5 4515.27 210.862 11 -10 6 5 4187.31 224.176 11 -10 6 5 4147.36 214.423 10 -10 6 5 4090.86 206.410 4 -10 -6 4 1198.21 115.935 11 -10 6 4 1302.61 136.680 11 -10 6 4 1035.54 119.563 10 -10 6 4 1083.76 109.739 4 -10 -6 3 17317.8 660.330 11 -10 -6 3 17503.6 642.554 10 -10 6 3 18016.3 651.824 4 -10 6 3 17661.1 659.126 10 -10 -6 2 484.739 108.486 11 -10 6 2 408.332 104.052 11 -10 -6 2 480.186 77.3310 10 -10 6 2 379.148 102.147 10 -10 -6 1 2760.99 175.693 11 -10 6 1 2646.75 175.486 11 -10 -6 1 2799.84 160.605 10 -10 6 0 1466.85 122.042 11 -10 -6 0 1274.63 130.590 11 -10 -6 0 1572.27 118.655 10 -10 6 0 1631.10 127.837 10 -10 -6 -1 4633.25 221.904 11 -10 6 -1 4750.99 213.934 11 -10 -6 -1 4940.42 218.361 10 -10 6 -1 4930.59 222.937 10 -10 -6 -2 676.389 75.5130 11 -10 -6 -2 709.348 78.3013 10 -10 6 -2 705.094 75.2591 10 -10 -6 -3 11201.1 409.177 11 -10 -6 -3 11902.3 417.660 10 -10 6 -3 11735.9 410.415 10 -10 7 10 1095.15 70.4569 12 -10 7 9 2322.71 122.400 13 -10 7 9 2242.85 119.604 12 -10 7 8 118.258 66.0946 13 -10 7 8 164.429 59.3262 12 -10 7 8 114.971 58.3906 7 -10 7 7 3367.21 172.607 12 -10 7 7 3477.52 185.175 11 -10 7 6 3914.38 191.125 12 -10 7 6 3965.53 209.557 11 -10 7 6 4166.85 200.065 4 -10 -7 5 65795.9 2319.05 11 -10 7 5 69499.7 2336.92 11 -10 7 5 68298.4 2328.61 10 -10 7 5 71534.2 2324.72 4 -10 -7 4 21242.3 780.184 11 -10 7 4 21607.0 789.591 11 -10 7 4 21397.2 783.496 10 -10 7 4 21563.8 775.895 4 -10 -7 3 63.3089 85.3860 11 -10 7 3-5.66507 93.9586 10 -10 7 3 160.801 76.1964 4 -10 -7 2 353.503 97.7216 11 -10 7 2 141.171 98.2440 11 -10 -7 2 304.861 76.3839 10 -10 -7 1 520.576 109.267 11 -10 7 1 768.998 108.642 11 -10 -7 1 499.431 85.3249 10 -10 7 1 774.797 114.093 10 -10 7 0 1929.92 133.288 11 -10 -7 0 1875.08 127.583 10 -10 7 0 1809.64 133.379 10 -10 -7 -1 398.422 83.0019 11 -10 7 -1 398.640 68.7717 11 -10 -7 -1 444.799 75.2668 10 -10 7 -1 487.792 78.9017 10 -10 -7 -2 556.818 71.5690 11 -10 -7 -2 577.982 71.1122 10 -10 7 -2 425.241 64.3443 10 -10 -7 -3 508.849 46.8934 11 -10 -7 -3 587.634 56.3302 10 -10 8 10 1203.11 73.7638 13 -10 8 10 1262.14 75.5006 12 -10 8 9 80.0618 54.1597 13 -10 8 9 212.247 55.2065 12 -10 8 8 85.9221 64.1971 13 -10 8 8 183.103 62.1277 12 -10 8 8 240.754 60.2090 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1762.96 89.1246 13 -10 19 6 1790.36 88.0762 12 -10 19 5 334.952 46.8430 12 -10 19 5 353.235 44.1299 7 -10 19 4 48.7630 31.1845 7 -10 20 4 299.444 37.1900 12 -11 0 6 159.417 65.3418 11 -11 0 5 29.9375 73.5521 11 -11 0 5 51.2850 60.1102 10 -11 0 4 74.4478 85.4622 11 -11 0 4 93.0253 69.0281 10 -11 0 3-10.8347 87.6145 11 -11 0 3-23.8727 73.4633 10 -11 0 2 3291.29 175.791 10 -11 0 1 115.014 76.7451 11 -11 0 1 194.305 77.6229 10 -11 0 0 859.130 90.9885 11 -11 0 0 857.321 89.0430 10 -11 0 -1 41.4695 50.0663 11 -11 0 -1 38.0480 53.7552 10 -11 0 -2 4565.49 182.867 10 -11 -1 6 2467.99 146.495 11 -11 1 6 3000.50 155.535 11 -11 -1 5 1365.24 113.992 11 -11 1 5 1536.61 127.589 11 -11 -1 5 1580.70 106.445 10 -11 1 5 1580.53 110.735 10 -11 -1 4 1610.36 131.428 11 -11 1 4 1478.31 129.931 11 -11 -1 4 1628.70 115.324 10 -11 1 4 1618.16 123.369 10 -11 -1 3 6016.93 272.613 11 -11 1 3 5649.02 267.008 11 -11 -1 3 5911.45 259.418 10 -11 1 3 5951.70 262.850 10 -11 -1 2 4820.53 247.614 11 -11 -1 2 5540.95 243.564 10 -11 1 2 5604.28 247.080 10 -11 -1 1 10249.5 394.159 11 -11 1 1 9807.37 390.434 11 -11 1 1 9455.29 363.600 4 -11 -1 1 10091.1 386.165 10 -11 1 1 9637.89 384.208 10 -11 -1 0 672.013 85.9883 11 -11 1 0 848.205 87.6271 11 -11 -1 0 662.886 84.2334 10 -11 1 0 688.552 80.2474 10 -11 -1 -1 779.328 71.0689 11 -11 1 -1 668.737 65.8220 11 -11 -1 -1 665.427 71.5959 10 -11 1 -2 191.846 42.5116 10 -11 2 7 8388.01 327.238 11 -11 -2 6 3245.62 164.648 11 -11 2 6 3180.05 168.813 11 -11 -2 5 519.308 89.3331 11 -11 2 5 348.959 83.7531 11 -11 2 5 466.766 78.1350 10 -11 -2 4 663.208 104.676 11 -11 2 4 773.579 101.235 11 -11 -2 4 722.076 85.7303 10 -11 2 4 849.338 97.9367 10 -11 -2 3 4035.19 210.078 11 -11 2 3 3744.00 204.424 11 -11 -2 3 4001.57 195.417 10 -11 2 3 4348.18 205.491 10 -11 2 3 3877.36 180.623 4 -11 -2 2 264.405 88.7516 11 -11 -2 2 342.156 74.8439 10 -11 2 2 227.226 82.5815 10 -11 2 2 274.251 59.1896 4 -11 2 1 16413.1 580.102 11 -11 2 1 15633.1 556.650 4 -11 -2 1 15161.3 570.022 10 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113.647 64.7582 11 -11 -3 0 209.599 66.3931 10 -11 -3 -1 177.119 52.9581 11 -11 3 -1 125.891 45.5987 11 -11 -3 -1 155.221 52.1330 10 -11 3 -1 146.697 54.6684 10 -11 -3 -2 35.8354 35.5784 10 -11 3 -2 30.5606 33.2453 10 -11 4 7 478.029 70.4586 11 -11 4 7 451.626 65.9687 7 -11 4 6 270.591 77.9989 11 -11 -4 5 2939.40 162.481 11 -11 4 5 2967.55 170.364 11 -11 4 5 2916.82 159.706 10 -11 4 5 2812.36 146.388 4 -11 -4 4 2213.09 141.250 11 -11 4 4 2052.95 147.063 11 -11 4 4 2183.96 141.216 10 -11 4 4 2108.42 125.065 4 -11 -4 3 289.333 84.4023 11 -11 4 3 535.084 102.561 11 -11 -4 3 354.602 71.2140 10 -11 4 3 250.600 81.4135 10 -11 4 3 420.179 67.8153 4 -11 -4 2 606.987 91.9510 11 -11 4 2 317.601 94.3222 11 -11 -4 2 529.621 80.3209 10 -11 4 2 766.525 99.0882 10 -11 4 2 449.538 69.2339 4 -11 4 1 278.942 79.2005 11 -11 -4 1 80.4975 61.3325 10 -11 4 1 164.337 72.9180 10 -11 4 1 163.055 56.4443 4 -11 -4 0 6767.00 270.763 11 -11 4 0 6630.72 266.293 11 -11 -4 0 6140.16 261.857 10 -11 -4 -1 218.291 55.5525 11 -11 4 -1 161.000 42.4067 11 -11 -4 -1 151.526 48.4759 10 -11 4 -1 159.379 53.6734 10 -11 -4 -2 1985.06 95.1966 10 -11 4 -2 2179.97 96.1326 10 -11 5 7 328.473 66.8989 11 -11 5 7 364.281 64.7258 7 -11 5 6 31.9444 73.3088 11 -11 -5 5 8328.92 340.691 11 -11 5 5 8794.42 351.121 11 -11 5 5 8487.82 343.008 10 -11 5 5 8433.84 332.043 4 -11 -5 4 1603.73 121.287 11 -11 5 4 1734.57 132.838 11 -11 5 4 1639.59 126.414 10 -11 5 4 1474.47 108.717 4 -11 -5 3 8834.13 362.893 11 -11 -5 3 8597.45 343.933 10 -11 5 3 9116.41 360.402 10 -11 5 3 8953.08 347.084 4 -11 -5 2 1605.92 124.213 11 -11 5 2 1585.79 128.044 11 -11 -5 2 1499.84 108.437 10 -11 5 2 1637.96 125.339 10 -11 5 2 1657.98 105.720 4 -11 5 1 2634.21 149.550 11 -11 -5 1 2343.56 135.734 10 -11 5 1 2652.67 134.991 4 -11 -5 0 10493.3 399.309 11 -11 5 0 10664.0 395.027 11 -11 -5 0 10399.6 391.755 10 -11 5 0 10410.4 396.123 10 -11 5 -1 877.084 61.3553 11 -11 -5 -1 800.620 71.7637 11 -11 5 -1 875.504 69.6060 10 -11 -5 -1 734.218 67.0766 10 -11 6 8 3196.50 142.456 7 -11 6 7 14447.1 532.679 11 -11 6 7 14849.0 532.312 7 -11 6 6 4358.81 208.150 11 -11 -6 5 779.346 86.0765 11 -11 6 5 1019.59 108.161 11 -11 6 5 788.594 81.4522 4 -11 -6 4 62.0526 74.4658 11 -11 6 4 123.285 86.3132 11 -11 6 4 102.455 79.7224 10 -11 6 4 104.224 61.2953 4 -11 -6 3 892.951 104.287 11 -11 6 3 962.288 103.806 10 -11 6 3 906.958 87.1820 4 -11 -6 2 1515.46 117.946 11 -11 6 2 1493.35 119.562 11 -11 -6 2 1174.02 95.0069 10 -11 6 2 1474.89 115.085 10 -11 6 2 1566.03 104.677 4 -11 -6 1 550.471 84.4991 11 -11 6 1 458.423 80.2224 11 -11 -6 1 478.339 67.1123 10 -11 6 1 493.502 63.7350 4 -11 -6 0 1156.57 97.9051 11 -11 6 0 1277.86 90.8671 11 -11 -6 0 1260.88 88.5954 10 -11 6 0 1338.04 96.5936 10 -11 -6 -1 9054.58 327.110 11 -11 -6 -1 8245.26 319.845 10 -11 6 -1 9008.32 324.651 10 -11 7 8 541.084 60.2398 13 -11 7 8 826.497 65.2290 7 -11 7 7 51.9801 57.4092 11 -11 7 7 122.315 58.8405 7 -11 7 6 238.808 73.0600 11 -11 7 6 388.633 80.3088 7 -11 -7 5 754.887 83.5052 11 -11 7 5 1032.85 108.120 11 -11 7 5 1004.50 86.0355 4 -11 -7 4 4793.94 222.542 11 -11 7 4 4903.93 231.653 11 -11 7 4 4405.73 220.428 10 -11 7 4 5029.97 216.059 4 -11 -7 3 397.991 82.6512 11 -11 7 3 445.736 87.4652 10 -11 7 3 456.092 73.8444 4 -11 -7 2 7572.94 309.119 11 -11 7 2 7811.99 314.301 11 -11 -7 2 6782.36 287.490 10 -11 7 2 7749.42 299.098 4 -11 -7 1 145.888 68.1345 11 -11 7 1 99.0634 70.2515 11 -11 -7 1 151.742 52.7286 10 -11 7 1 153.777 69.6104 10 -11 7 1 138.680 55.5375 4 -11 -7 0 101.913 67.1403 11 -11 7 0 72.4487 50.1209 11 -11 -7 0 132.808 47.3226 10 -11 7 0 29.6279 55.5177 10 -11 7 0 74.5998 44.6412 4 -11 -7 -1 2796.90 130.496 11 -11 -7 -1 2607.31 122.199 10 -11 7 -1 3012.14 125.690 4 -11 7 -1 2879.23 127.123 10 -11 8 8 148.549 47.3722 13 -11 8 8 41.6827 41.4402 7 -11 8 7 1036.14 88.5770 11 -11 8 7 1147.47 88.5605 7 -11 8 6 3405.34 178.987 11 -11 8 6 3766.51 183.452 7 -11 8 5 612.710 74.1571 4 -11 -8 5 642.658 72.5302 11 -11 8 5 594.328 92.7402 11 -11 -8 4 148.905 68.5651 11 -11 8 4 63.2895 82.5602 11 -11 8 4 4.43308 68.3901 10 -11 8 4 105.497 60.5166 4 -11 -8 3 9258.41 368.345 11 -11 8 3 9202.44 367.238 10 -11 8 3 9328.33 359.360 4 -11 -8 2 3844.98 189.957 11 -11 8 2 3707.96 190.512 11 -11 8 2 3717.19 176.228 4 -11 -8 1 27.8262 62.1875 11 -11 8 1 93.1259 65.8101 11 -11 -8 1-11.7208 46.2554 10 -11 8 1 37.3119 64.9758 10 -11 8 1 3.27695 52.2774 4 -11 8 0 27.3591 45.5240 11 -11 -8 0 35.8931 38.5735 10 -11 8 0-3.04784 49.9737 10 -11 8 0 107.733 48.4715 4 -11 -8 -1 387.519 49.2318 11 -11 -8 -1 389.966 41.6820 10 -11 8 -1 346.289 44.3421 10 -11 8 -1 352.014 44.1826 4 -11 9 9 1034.49 61.1765 13 -11 9 8 79.9102 46.2712 13 -11 9 8 81.0410 42.4055 7 -11 9 7 627.381 73.9903 11 -11 9 7 626.501 69.7127 7 -11 9 6 992.072 98.4512 11 -11 9 6 1007.55 94.4804 7 -11 9 5 1205.28 109.954 11 -11 9 5 1096.90 91.2413 4 -11 -9 4 1107.59 94.4200 11 -11 9 4 1029.78 105.734 11 -11 9 4 1218.27 92.0328 4 -11 -9 3 551.111 81.6973 11 -11 9 3 559.117 94.1669 11 -11 9 3 552.880 76.3946 4 -11 -9 2 741.276 87.6961 11 -11 9 2 376.940 80.4431 11 -11 9 2 585.034 82.0112 10 -11 9 2 533.439 71.3952 4 -11 -9 1 4352.65 209.392 11 -11 9 1 4864.72 209.142 11 -11 9 1 5051.74 210.021 10 -11 9 1 5032.13 204.846 4 -11 9 0 96.1165 40.3861 11 -11 -9 0 58.3740 34.3662 10 -11 9 0 107.817 46.8711 10 -11 9 0 107.332 43.4951 4 -11 -9 -1 119.457 40.7927 11 -11 9 -1 147.788 33.4284 4 -11 10 8 1288.01 81.2194 13 -11 10 8 1308.57 79.2601 7 -11 10 7 206.104 60.5315 11 -11 10 7 295.446 58.9004 7 -11 10 6 892.664 91.1767 11 -11 10 6 909.996 88.5847 7 -11 10 5 9677.93 375.877 11 -11 10 5 9325.49 361.361 4 -11 -10 4 11347.6 416.713 11 -11 10 4 11849.7 417.366 4 -11 -10 3 628.862 80.1246 11 -11 10 3 626.770 91.0579 11 -11 10 3 551.585 72.7004 4 -11 -10 2-3.90603 59.2035 11 -11 10 2 73.3480 66.1442 11 -11 10 2 96.2039 66.4833 10 -11 10 2 10.0726 53.1981 4 -11 -10 1 6014.22 256.436 11 -11 10 1 6465.38 253.426 11 -11 10 1 6318.66 253.747 10 -11 10 1 6486.05 251.803 4 -11 10 0 44.3066 31.5854 11 -11 10 0 36.5881 39.4677 10 -11 10 0 26.9228 41.7565 4 -11 11 8 2161.38 108.809 13 -11 11 8 2263.99 106.600 7 -11 11 7 157.947 43.3025 12 -11 11 7 196.825 57.0557 11 -11 11 7 210.605 53.4327 7 -11 11 6 7155.31 270.782 11 -11 11 6 7373.54 269.411 7 -11 11 5 766.823 77.6680 4 -11 11 5 570.417 61.9007 12 -11 11 5 819.913 91.7117 11 -11 11 5 855.354 88.4529 7 -11 -11 4 1821.04 109.792 11 -11 11 4 2039.91 115.593 4 -11 11 3 1404.80 105.007 11 -11 11 3 1222.75 94.6266 4 -11 -11 2 8853.53 350.141 11 -11 11 2 9171.69 350.265 11 -11 11 2 9303.00 346.031 4 -11 -11 1 3487.52 163.863 11 -11 11 1 3707.41 159.312 11 -11 11 1 3588.52 158.028 4 -11 -11 0 2958.93 137.357 11 -11 11 0 3092.66 132.032 4 -11 12 8 2855.81 126.945 13 -11 12 7 2575.89 125.062 12 -11 12 7 3442.74 139.836 7 -11 12 6 319.219 50.5733 12 -11 12 6 384.832 69.4667 11 -11 12 6 348.813 64.1821 7 -11 12 5 2694.24 144.044 11 -11 12 5 2930.70 143.000 7 -11 12 4 84.5757 56.7946 4 -11 -12 3-29.9416 51.7920 11 -11 12 3 57.1301 52.5669 4 -11 -12 2 369.299 61.6454 11 -11 12 2 449.657 66.2881 11 -11 12 2 454.016 62.6258 4 -11 -12 1 334.534 57.9030 11 -11 12 1 259.392 44.6602 11 -11 12 1 325.203 49.7423 4 -11 -12 0 1460.18 82.2062 11 -11 12 0 1433.81 74.9705 4 -11 13 8 1805.40 89.0015 13 -11 13 7 96.1808 45.0223 13 -11 13 7 114.113 35.1698 12 -11 13 7 39.0245 40.8585 7 -11 13 6 2201.58 115.260 11 -11 13 6 2058.11 107.757 7 -11 13 5 1055.82 72.8585 12 -11 13 5 1273.84 93.2664 11 -11 13 4 4464.18 182.033 7 -11 13 4 3992.59 167.373 4 -11 -13 3 1381.21 87.3715 11 -11 13 3 1575.51 102.100 11 -11 13 3 1635.88 101.569 7 -11 13 3 1349.94 89.7611 4 -11 -13 2 115.004 50.3631 11 -11 13 2-2.80720 46.9198 11 -11 13 2-21.4900 43.0066 4 -11 -13 1 12.7373 38.8442 11 -11 13 1 50.2833 35.8526 7 -11 13 1 43.4795 42.6240 4 -11 14 7 5337.15 212.609 13 -11 14 7 5629.93 212.404 7 -11 14 6 2992.58 135.343 12 -11 14 6 3572.65 146.214 7 -11 14 5 1062.00 70.0694 12 -11 14 5 1285.52 89.6489 11 -11 14 4 1062.69 82.6244 11 -11 14 4 1025.66 77.0013 7 -11 14 4 912.534 71.7664 4 -11 14 3 2242.83 114.823 11 -11 14 3 2561.54 118.512 7 -11 14 3 2280.30 110.135 4 -11 14 2 564.976 54.5895 11 -11 14 2 666.936 58.0081 7 -11 -14 1 9112.17 328.577 11 -11 15 7 1563.19 80.7815 13 -11 15 6 1297.64 70.3510 12 -11 15 5 2165.19 108.254 11 -11 15 5 2000.31 98.1654 7 -11 15 4 4193.82 172.052 11 -11 15 4 4776.12 169.598 7 -11 15 3 9987.05 352.153 11 -11 15 3 9280.78 345.548 7 -11 16 6 39.9604 31.3392 13 -11 16 5 43.9714 32.0815 7 -11 16 4 41.0158 30.9127 7 -12 0 6 286.640 55.5296 11 -12 0 5-10.8925 56.2819 11 -12 0 4 253.345 69.1303 11 -12 0 4 234.793 54.4531 10 -12 0 3-37.7493 62.9981 11 -12 0 3-38.2237 48.1920 10 -12 0 2 3376.54 154.523 10 -12 0 1-42.2491 47.3686 11 -12 0 1 28.2142 39.2415 10 -12 0 0 81.0296 32.2489 10 -12 -1 6 2403.33 122.878 11 -12 1 6 2534.78 127.615 11 -12 -1 5 2625.55 138.587 11 -12 1 5 2596.31 138.530 11 -12 -1 4 1684.11 109.792 11 -12 1 4 1719.23 111.835 11 -12 -1 4 1425.04 90.9838 10 -12 1 4 1437.76 95.6626 10 -12 -1 3 1436.58 103.417 11 -12 1 3 1401.05 103.360 11 -12 -1 3 1274.22 88.3434 10 -12 1 3 1361.43 92.6457 10 -12 -1 2 174.140 64.2989 11 -12 -1 2 220.969 52.8351 10 -12 1 2 182.217 53.4981 10 -12 -1 1 717.928 66.9029 11 -12 1 1 693.242 65.5621 11 -12 1 1 745.704 62.4179 10 -12 -1 1 557.026 58.0203 10 -12 1 0-13.6244 29.4407 10 -12 -2 6 114.934 47.5157 11 -12 2 6 77.1249 54.1408 11 -12 -2 5 817.894 79.1020 11 -12 2 5 799.813 81.2420 11 -12 -2 4 212.650 64.4135 11 -12 2 4 161.246 64.7727 11 -12 2 4 200.357 56.7046 10 -12 -2 3 5776.98 233.753 11 -12 2 3 5432.33 232.589 11 -12 -2 3 5125.89 217.384 10 -12 2 3 5508.57 225.597 10 -12 -2 2 3220.76 151.261 11 -12 -2 2 2857.31 137.267 10 -12 2 2 3021.61 142.629 10 -12 -2 1 6687.06 253.126 11 -12 2 1 6852.38 252.776 11 -12 2 1 6796.36 250.300 10 -12 2 0 134.603 34.8723 10 -12 3 6 9996.17 378.218 11 -12 3 6 10319.8 374.820 7 -12 -3 5 1169.48 87.9935 11 -12 3 5 1224.48 95.2284 11 -12 -3 4 25.4507 60.4782 11 -12 3 4 11.4206 63.0176 11 -12 3 4 42.8711 53.1607 10 -12 -3 3 4925.11 210.094 11 -12 3 3 5095.30 213.542 11 -12 -3 3 4392.97 191.341 10 -12 3 3 4859.17 204.214 10 -12 -3 2-3.30668 55.3555 11 -12 3 2 9.93552 57.5083 11 -12 -3 2 5.19819 42.0437 10 -12 3 2 105.526 51.5020 10 -12 -3 1 907.371 73.2843 11 -12 3 1 919.667 70.4763 11 -12 -3 1 1023.14 64.9164 10 -12 3 1 998.453 71.0052 10 -12 4 6 2192.48 119.317 11 -12 4 6 2241.86 116.539 7 -12 -4 5 16.0283 49.0548 11 -12 4 5 54.1187 60.6849 11 -12 -4 4 2693.35 136.362 11 -12 4 4 2391.35 135.090 11 -12 4 4 2417.26 129.553 10 -12 -4 3 24.5446 58.4567 11 -12 4 3 54.2775 69.5316 11 -12 4 3 122.316 56.0162 10 -12 -4 2 5639.45 223.283 11 -12 4 2 6017.95 224.869 11 -12 4 2 5619.01 219.250 10 -12 4 1 445.585 53.8397 11 -12 -4 1 402.634 43.4481 10 -12 4 1 391.436 52.1841 10 -12 5 7 174.612 40.6949 11 -12 5 6 7235.73 288.664 11 -12 5 6 7690.93 286.263 7 -12 -5 5 781.281 70.8415 11 -12 5 5 837.260 83.4828 11 -12 -5 4 870.472 78.8697 11 -12 5 4 914.748 87.1478 11 -12 -5 3 899.779 81.9523 11 -12 5 3 855.345 76.8832 10 -12 -5 2 968.240 79.4606 11 -12 5 2 981.855 77.7843 11 -12 5 2 965.182 74.0531 10 -12 5 2 794.469 53.6413 4 -12 5 1 222.154 43.6486 11 -12 6 7 721.822 57.7826 11 -12 6 7 779.572 55.9184 7 -12 6 6 1379.84 92.9948 11 -12 6 6 1526.35 89.7054 7 -12 -6 5 1810.41 103.175 11 -12 6 5 2288.79 120.072 11 -12 6 4 152.068 36.6416 4 -12 -6 4 95.0411 52.2697 11 -12 6 4 113.167 59.7195 11 -12 -6 3 4100.16 179.808 11 -12 6 3 4383.06 180.808 10 -12 6 3 3871.05 162.900 4 -12 -6 2 398.157 59.1344 11 -12 6 2 410.645 60.4794 11 -12 6 2 427.714 54.2841 10 -12 6 2 353.568 38.9361 4 -12 -6 1 5247.89 208.133 11 -12 6 1 5350.56 203.944 11 -12 7 7 138.656 37.0012 11 -12 7 7 168.313 36.0259 7 -12 7 6 8472.15 326.557 11 -12 7 6 8929.44 324.209 7 -12 7 5 98.6597 56.9694 11 -12 7 5 194.701 55.4271 7 -12 7 4 56.9323 36.9387 4 -12 -7 4 46.8447 46.5775 11 -12 7 4 70.9747 57.8407 11 -12 -7 3 221.517 53.7267 11 -12 7 3 158.227 37.6465 4 -12 -7 2 2362.20 116.744 11 -12 7 2 2557.91 119.001 11 -12 7 2 2151.73 100.829 4 -12 -7 1 1087.77 69.0472 11 -12 7 1 1215.08 67.9833 10 -12 8 7 88.5683 38.0428 11 -12 8 7 119.506 33.3103 7 -12 8 6 2806.57 130.509 11 -12 8 6 2660.39 125.247 7 -12 8 5 814.482 75.9626 11 -12 8 5 848.946 74.4436 7 -12 8 4 1315.03 91.6049 11 -12 8 4 1209.62 72.2506 4 -12 -8 3 3053.53 140.831 11 -12 8 3 2981.48 131.048 4 -12 8 2 1766.80 91.6354 11 -12 8 2 1607.96 78.0195 4 -12 9 7 3793.26 149.915 7 -12 9 6 3804.64 163.489 11 -12 9 6 3862.84 159.564 7 -12 9 5 2472.07 128.794 11 -12 9 5 2835.91 130.525 7 -12 9 4 1054.76 79.4443 11 -12 9 4 924.630 61.0404 4 -12 -9 3 70.8092 36.6080 11 -12 9 3 49.2527 49.2520 11 -12 9 3 38.0212 30.6615 4 -12 -9 2 1012.02 68.3244 11 -12 9 2 1290.60 71.9815 11 -12 10 6 171.574 43.0315 11 -12 10 6 133.579 36.9370 7 -12 10 5 43.1586 44.0678 11 -12 10 5-7.34299 37.7328 7 -12 10 4 308.846 53.3665 7 -12 10 3 7.43048 26.5316 4 -12 10 3 34.3402 42.2130 11 -12 11 6 277.753 40.9961 11 -12 11 6 337.339 40.1177 7 -12 11 5 6531.73 249.157 11 -12 11 5 6530.71 244.749 7 -12 11 4 3834.08 159.416 7 -12 11 3 2327.39 108.173 11 -12 11 3 2447.62 110.790 7 -12 12 5 3956.73 162.032 11 -12 12 5 4080.21 158.051 7 0 0 0 0.00 0.00 0 TITL ome in P2(1)/c REM P2(1)/c (#14 in standard setting) CELL 1.54184 10.481620 25.192747 10.922267 90.0000 112.6927 90.0000 ZERR 12.00 0.000162 0.000339 0.000178 0.0000 0.0019 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C H N O UNIT 132.00 120.00 12.00 12.00 TREF HKLF 4 END ; _shelx_hkl_checksum 53238 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.390 _oxdiff_exptl_absorpt_empirical_full_min 0.797