data_lub129 _audit_creation_date 2018-10-05 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _shelx_SHELXL_version_number '2018/3' _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_name '' _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2008). Acta Cryst. A64, 112-122. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C18 H17 I N2 O5' _chemical_formula_sum 'C18 H17 I N2 O5' _chemical_formula_weight 468.23 _chemical_absolute_configuration ad _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0137 0.0067 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'I' 'I' 0.0030 5.4349 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0241 0.0134 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0389 0.0241 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'orthorhombic' _space_group_IT_number 19 _space_group_name_H-M_alt 'P 21 21 21' _space_group_name_Hall 'P 2ac 2ab' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' _cell_length_a 9.4104(6) _cell_length_b 13.1390(8) _cell_length_c 14.3976(9) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 1780.17(19) _cell_formula_units_Z 4 _cell_measurement_reflns_used 9952 _cell_measurement_temperature 150 _cell_measurement_theta_max 60.793 _cell_measurement_theta_min 3.964 _shelx_estimated_absorpt_T_max 0.505 _shelx_estimated_absorpt_T_min 0.284 _exptl_absorpt_coefficient_mu 9.882 _exptl_absorpt_correction_T_max 0.2103 _exptl_absorpt_correction_T_min 0.0948 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1250 before and 0.0738 after correction. The Ratio of minimum to maximum transmission is 0.4508. The \l/2 correction factor is Not present.' _exptl_absorpt_special_details ? _exptl_crystal_colour 'clear light colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier light _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.747 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description Plate _exptl_crystal_F_000 928 _exptl_crystal_recrystallization_method ? _exptl_crystal_size_max 0.17 _exptl_crystal_size_mid 0.13 _exptl_crystal_size_min 0.08 _exptl_special_details ; X-ray crystallographic data for I were collected from a single crystal sample, which was mounted on a loop fiber. Data were collected using a Bruker Venture diffractometer equipped with a Photon 100 CMOS Detector, a Helios MX optics and a Kappa goniometer. The crystal-to-detector distance was 4.0 cm, and the data collection was carried out in 1024 x 1024 pixel mode. ; _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0478 _diffrn_reflns_av_unetI/netI 0.0442 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.969 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_limit_l_min -16 _diffrn_reflns_number 11595 _diffrn_reflns_point_group_measured_fraction_full 0.996 _diffrn_reflns_point_group_measured_fraction_max 0.957 _diffrn_reflns_theta_full 53.594 _diffrn_reflns_theta_max 60.790 _diffrn_reflns_theta_min 3.963 _diffrn_ambient_temperature 150 _diffrn_detector 'CMOS Area detector' _diffrn_detector_area_resol_mean 10.24 _diffrn_detector_type 'Bruker Photon 100 CMOS Detector' _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.969 _diffrn_measurement_device 'k-geometry diffractometer' _diffrn_measurement_device_type 'Bruker Venture Metaljet' _diffrn_measurement_method '\w and \f scans' _diffrn_radiation_collimation 'Focusing mirrors' _diffrn_radiation_monochromator 'Helios MX Mirror Optics' _diffrn_radiation_probe X-ray _diffrn_radiation_type GaK\a _diffrn_radiation_wavelength 1.34139 _diffrn_source 'Metal Jet' _diffrn_source_target Ga _diffrn_source_type 'Gallium Liquid Metal Jet Source' _reflns_Friedel_coverage 0.732 _reflns_Friedel_fraction_full 0.991 _reflns_Friedel_fraction_max 0.940 _reflns_number_gt 3767 _reflns_number_total 3923 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'SAINT (2013) V8.38A; Integration Software for Single Crystal Data. Bruker AXS Inc., Madison, WI 53719-1173.' _computing_data_collection ; APEX 2 (2013) Bruker AXS Inc., Madison, WI 53719-1173. ; _computing_data_reduction 'SAINT (2013) V8.38A; Integration Software for Single Crystal Data. Bruker AXS Inc., Madison, WI 53719-1173.' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _computing_structure_solution 'XT (Sheldrick, 2015)' _refine_diff_density_max 0.514 _refine_diff_density_min -1.022 _refine_diff_density_rms 0.079 _refine_ls_abs_structure_details ; Flack x determined using 1531 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.031(5) _refine_ls_extinction_coef 0.0046(3) _refine_ls_extinction_expression 'Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^' _refine_ls_extinction_method 'SHELXL-2018/3 (Sheldrick 2018)' _refine_ls_goodness_of_fit_ref 1.069 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 237 _refine_ls_number_reflns 3923 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0333 _refine_ls_R_factor_gt 0.0319 _refine_ls_restrained_S_all 1.069 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0337P)^2^+1.4597P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0813 _refine_ls_wR_factor_ref 0.0827 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C2(H2), C4(H4), C5(H5), C8(H8) 2.b Secondary CH2 refined with riding coordinates: C3(H3A,H3B), C6(H6A,H6B), C7(H7A,H7B) 2.c Aromatic/amide H refined with riding coordinates: C13(H13), C14(H14), C15(H15), C16(H16) 2.d Idealised Me refined as rotating group: C10(H10A,H10B,H10C) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group I1 I 0.64236(4) 0.32494(3) 0.17585(2) 0.04389(15) Uani 1 1 d . . . . . O1 O 0.8377(3) 0.3723(3) 0.4811(2) 0.0322(7) Uani 1 1 d . . . . . O2 O 0.6892(4) 0.0557(3) 0.4488(3) 0.0368(8) Uani 1 1 d . . . . . O3 O 0.5457(4) 0.3377(3) 0.6090(3) 0.0412(8) Uani 1 1 d . . . . . O4 O 0.5609(4) 0.6205(3) 0.4770(3) 0.0433(9) Uani 1 1 d . . . . . O5 O 0.7474(5) 0.7091(3) 0.4206(3) 0.0441(9) Uani 1 1 d . . . . . N1 N 0.6618(4) 0.4438(3) 0.3919(3) 0.0277(8) Uani 1 1 d . . . . . N2 N 0.6268(4) 0.2122(3) 0.5105(3) 0.0250(7) Uani 1 1 d . . . . . C1 C 0.7248(5) 0.3674(3) 0.4391(3) 0.0260(9) Uani 1 1 d . . . . . C2 C 0.6342(5) 0.2718(3) 0.4269(3) 0.0267(8) Uani 1 1 d . . . . . H2 H 0.676961 0.229828 0.378061 0.032 Uiso 1 1 calc R . . . . C3 C 0.4899(5) 0.3131(4) 0.3907(4) 0.0302(9) Uani 1 1 d . . . . . H3A H 0.453768 0.270541 0.340960 0.036 Uiso 1 1 calc R . . . . H3B H 0.420220 0.315011 0.440307 0.036 Uiso 1 1 calc R . . . . C4 C 0.5213(5) 0.4214(4) 0.3548(4) 0.0293(10) Uani 1 1 d . . . . . H4 H 0.453404 0.468105 0.383999 0.035 Uiso 1 1 calc R . . . . C5 C 0.5174(6) 0.4397(4) 0.2503(4) 0.0350(11) Uani 1 1 d . . . . . H5 H 0.418520 0.435222 0.229352 0.042 Uiso 1 1 calc R . . . . C6 C 0.5735(6) 0.5459(4) 0.2276(4) 0.0366(11) Uani 1 1 d . . . . . H6A H 0.576150 0.554496 0.160727 0.044 Uiso 1 1 calc R . . . . H6B H 0.508882 0.596358 0.252771 0.044 Uiso 1 1 calc R . . . . C7 C 0.7218(6) 0.5639(4) 0.2671(4) 0.0368(11) Uani 1 1 d . . . . . H7A H 0.748494 0.634279 0.256610 0.044 Uiso 1 1 calc R . . . . H7B H 0.789234 0.521218 0.234214 0.044 Uiso 1 1 calc R . . . . C8 C 0.7311(5) 0.5406(3) 0.3721(4) 0.0300(10) Uani 1 1 d . . . . . H8 H 0.831670 0.534280 0.388652 0.036 Uiso 1 1 calc R . . . . C9 C 0.6670(5) 0.6259(4) 0.4306(3) 0.0321(10) Uani 1 1 d . . . . . C10 C 0.7053(8) 0.7996(4) 0.4704(5) 0.0475(14) Uani 1 1 d . . . . . H10A H 0.673719 0.850235 0.426996 0.071 Uiso 1 1 calc GR . . . . H10B H 0.784920 0.825334 0.504821 0.071 Uiso 1 1 calc GR . . . . H10C H 0.629438 0.783298 0.512358 0.071 Uiso 1 1 calc GR . . . . C11 C 0.6548(5) 0.1077(3) 0.5148(3) 0.0266(8) Uani 1 1 d . . . . . C12 C 0.6347(5) 0.0784(3) 0.6136(3) 0.0275(9) Uani 1 1 d . . . . . C13 C 0.6522(6) -0.0142(4) 0.6571(4) 0.0359(10) Uani 1 1 d . . . . . H13 H 0.682281 -0.071219 0.624243 0.043 Uiso 1 1 calc R . . . . C14 C 0.6233(6) -0.0197(5) 0.7524(4) 0.0408(12) Uani 1 1 d . . . . . H14 H 0.634955 -0.081106 0.783522 0.049 Uiso 1 1 calc R . . . . C15 C 0.5778(6) 0.0651(5) 0.8005(4) 0.0441(13) Uani 1 1 d . . . . . H15 H 0.557131 0.059216 0.863482 0.053 Uiso 1 1 calc R . . . . C16 C 0.5619(6) 0.1594(4) 0.7571(3) 0.0371(11) Uani 1 1 d . . . . . H16 H 0.533452 0.216741 0.790048 0.044 Uiso 1 1 calc R . . . . C17 C 0.5904(5) 0.1640(4) 0.6623(3) 0.0298(9) Uani 1 1 d . . . . . C18 C 0.5825(5) 0.2507(4) 0.5964(3) 0.0296(9) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 I1 0.0540(2) 0.0394(2) 0.0383(2) -0.00928(14) 0.00441(15) 0.00097(16) O1 0.0225(15) 0.0341(16) 0.0401(18) 0.0077(14) -0.0047(14) -0.0020(13) O2 0.053(2) 0.0237(16) 0.0338(19) -0.0022(14) 0.0059(15) 0.0056(14) O3 0.052(2) 0.0291(18) 0.042(2) -0.0079(16) 0.0062(16) 0.0074(16) O4 0.046(2) 0.0324(19) 0.051(2) -0.0061(17) 0.0079(19) -0.0027(16) O5 0.057(2) 0.0269(17) 0.049(2) -0.0010(16) 0.0014(19) -0.0112(16) N1 0.0263(18) 0.0201(16) 0.037(2) 0.0045(15) -0.0029(16) -0.0014(14) N2 0.0260(17) 0.0205(15) 0.0283(18) 0.0006(13) 0.0033(15) 0.0007(14) C1 0.024(2) 0.026(2) 0.028(2) 0.0032(18) 0.0032(17) 0.0023(16) C2 0.028(2) 0.0229(19) 0.029(2) 0.0007(17) 0.0019(19) -0.0019(18) C3 0.0259(19) 0.028(2) 0.036(2) 0.005(2) -0.0029(17) -0.0026(18) C4 0.026(2) 0.028(2) 0.034(2) 0.0017(19) -0.0024(18) 0.0004(17) C5 0.039(3) 0.030(3) 0.036(3) -0.001(2) -0.004(2) 0.004(2) C6 0.051(3) 0.028(2) 0.031(3) 0.006(2) 0.003(2) 0.004(2) C7 0.047(3) 0.028(2) 0.036(3) 0.004(2) 0.007(2) -0.005(2) C8 0.030(2) 0.021(2) 0.039(3) 0.0039(19) -0.0025(18) -0.0043(17) C9 0.038(3) 0.028(2) 0.030(2) 0.0059(18) -0.007(2) -0.0023(19) C10 0.064(4) 0.030(3) 0.049(3) -0.005(2) -0.010(3) -0.002(2) C11 0.027(2) 0.0220(19) 0.031(2) 0.0026(16) 0.0001(19) -0.0016(17) C12 0.0242(19) 0.031(2) 0.027(2) 0.0023(17) 0.0002(18) -0.0040(18) C13 0.037(2) 0.031(2) 0.039(3) 0.008(2) -0.001(2) -0.003(2) C14 0.040(3) 0.046(3) 0.036(3) 0.017(2) 0.000(2) -0.008(2) C15 0.043(3) 0.059(3) 0.031(3) 0.011(2) 0.000(2) -0.010(3) C16 0.042(2) 0.045(3) 0.025(2) -0.006(2) 0.0045(19) -0.004(2) C17 0.0272(18) 0.033(2) 0.030(2) 0.001(2) 0.0008(16) -0.0021(17) C18 0.030(2) 0.030(2) 0.029(2) -0.0065(19) 0.0011(18) -0.0037(18) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag I1 C5 2.192(5) . ? O1 C1 1.224(6) . ? O2 C11 1.215(6) . ? O3 C18 1.209(6) . ? O4 C9 1.203(6) . ? O5 C9 1.337(6) . ? O5 C10 1.443(7) . ? N1 C1 1.350(6) . ? N1 C4 1.456(6) . ? N1 C8 1.458(6) . ? N2 C2 1.438(6) . ? N2 C11 1.399(6) . ? N2 C18 1.399(6) . ? C1 C2 1.529(6) . ? C2 H2 0.9800 . ? C2 C3 1.553(6) . ? C3 H3A 0.9700 . ? C3 H3B 0.9700 . ? C3 C4 1.543(7) . ? C4 H4 0.9800 . ? C4 C5 1.524(8) . ? C5 H5 0.9800 . ? C5 C6 1.527(7) . ? C6 H6A 0.9700 . ? C6 H6B 0.9700 . ? C6 C7 1.526(8) . ? C7 H7A 0.9700 . ? C7 H7B 0.9700 . ? C7 C8 1.544(7) . ? C8 H8 0.9800 . ? C8 C9 1.526(7) . ? C10 H10A 0.9600 . ? C10 H10B 0.9600 . ? C10 H10C 0.9600 . ? C11 C12 1.485(6) . ? C12 C13 1.379(7) . ? C12 C17 1.389(7) . ? C13 H13 0.9300 . ? C13 C14 1.400(8) . ? C14 H14 0.9300 . ? C14 C15 1.380(9) . ? C15 H15 0.9300 . ? C15 C16 1.396(8) . ? C16 H16 0.9300 . ? C16 C17 1.392(7) . ? C17 C18 1.484(7) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C9 O5 C10 117.7(5) . . ? C1 N1 C4 115.7(4) . . ? C1 N1 C8 123.5(4) . . ? C4 N1 C8 120.7(4) . . ? C11 N2 C2 124.2(4) . . ? C18 N2 C2 123.9(4) . . ? C18 N2 C11 111.8(4) . . ? O1 C1 N1 126.2(4) . . ? O1 C1 C2 125.8(4) . . ? N1 C1 C2 108.0(4) . . ? N2 C2 C1 112.2(4) . . ? N2 C2 H2 108.4 . . ? N2 C2 C3 115.5(4) . . ? C1 C2 H2 108.4 . . ? C1 C2 C3 103.8(4) . . ? C3 C2 H2 108.4 . . ? C2 C3 H3A 110.6 . . ? C2 C3 H3B 110.6 . . ? H3A C3 H3B 108.8 . . ? C4 C3 C2 105.5(4) . . ? C4 C3 H3A 110.6 . . ? C4 C3 H3B 110.6 . . ? N1 C4 C3 103.8(4) . . ? N1 C4 H4 108.0 . . ? N1 C4 C5 110.6(4) . . ? C3 C4 H4 108.0 . . ? C5 C4 C3 118.1(4) . . ? C5 C4 H4 108.0 . . ? I1 C5 H5 108.5 . . ? C4 C5 I1 111.2(3) . . ? C4 C5 H5 108.5 . . ? C4 C5 C6 110.3(4) . . ? C6 C5 I1 109.8(4) . . ? C6 C5 H5 108.5 . . ? C5 C6 H6A 109.2 . . ? C5 C6 H6B 109.2 . . ? H6A C6 H6B 107.9 . . ? C7 C6 C5 112.2(4) . . ? C7 C6 H6A 109.2 . . ? C7 C6 H6B 109.2 . . ? C6 C7 H7A 109.1 . . ? C6 C7 H7B 109.1 . . ? C6 C7 C8 112.7(4) . . ? H7A C7 H7B 107.8 . . ? C8 C7 H7A 109.1 . . ? C8 C7 H7B 109.1 . . ? N1 C8 C7 109.8(4) . . ? N1 C8 H8 108.0 . . ? N1 C8 C9 110.9(4) . . ? C7 C8 H8 108.0 . . ? C9 C8 C7 111.9(4) . . ? C9 C8 H8 108.0 . . ? O4 C9 O5 125.3(5) . . ? O4 C9 C8 126.2(4) . . ? O5 C9 C8 108.5(4) . . ? O5 C10 H10A 109.5 . . ? O5 C10 H10B 109.5 . . ? O5 C10 H10C 109.5 . . ? H10A C10 H10B 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? O2 C11 N2 124.6(4) . . ? O2 C11 C12 129.6(4) . . ? N2 C11 C12 105.8(4) . . ? C13 C12 C11 130.5(4) . . ? C13 C12 C17 121.4(4) . . ? C17 C12 C11 108.1(4) . . ? C12 C13 H13 121.1 . . ? C12 C13 C14 117.9(5) . . ? C14 C13 H13 121.1 . . ? C13 C14 H14 119.6 . . ? C15 C14 C13 120.8(5) . . ? C15 C14 H14 119.6 . . ? C14 C15 H15 119.2 . . ? C14 C15 C16 121.6(5) . . ? C16 C15 H15 119.2 . . ? C15 C16 H16 121.4 . . ? C17 C16 C15 117.2(5) . . ? C17 C16 H16 121.4 . . ? C12 C17 C16 121.2(5) . . ? C12 C17 C18 108.3(4) . . ? C16 C17 C18 130.6(5) . . ? O3 C18 N2 124.1(5) . . ? O3 C18 C17 130.1(5) . . ? N2 C18 C17 105.8(4) . . ? _shelx_res_file ; TITL lub129_a.res in P2(1)2(1)2(1) lub129.res created by SHELXL-2018/3 at 09:23:09 on 05-Oct-2018 REM Old TITL lub129 in P2(1)2(1)2(1) REM SHELXT solution in P2(1)2(1)2(1) REM R1 0.100, Rweak 0.032, Alpha 0.007, Orientation as input REM Flack x = 0.086 ( 0.005 ) from Parsons' quotients REM Formula found by SHELXT: C18 N3 O4 I CELL 1.34139 9.4104 13.139 14.3976 90 90 90 ZERR 4 0.0006 0.0008 0.0009 0 0 0 LATT -1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H I N O DISP C 0.0137 0.0067 57.1 DISP H -0 0 0.6481 DISP I 0.003 5.4349 41754.3 DISP N 0.0241 0.0134 109.9 DISP O 0.0389 0.0241 193.4 UNIT 72 68 4 8 20 L.S. 30 PLAN 10 SIZE 0.08 0.13 0.17 TEMP 0 BOND $H list 4 fmap 2 53 acta REM REM REM WGHT 0.033700 1.459700 EXTI 0.004560 FVAR 0.56188 I1 3 0.642364 0.324944 0.175854 11.00000 0.05398 0.03937 = 0.03830 -0.00928 0.00441 0.00097 O1 5 0.837653 0.372314 0.481128 11.00000 0.02253 0.03406 = 0.04009 0.00767 -0.00469 -0.00204 O2 5 0.689160 0.055735 0.448781 11.00000 0.05287 0.02370 = 0.03376 -0.00223 0.00594 0.00556 O3 5 0.545717 0.337703 0.609028 11.00000 0.05239 0.02914 = 0.04196 -0.00793 0.00619 0.00743 O4 5 0.560919 0.620477 0.477038 11.00000 0.04643 0.03238 = 0.05114 -0.00615 0.00786 -0.00267 O5 5 0.747364 0.709127 0.420610 11.00000 0.05670 0.02686 = 0.04869 -0.00100 0.00144 -0.01118 N1 4 0.661818 0.443815 0.391863 11.00000 0.02627 0.02009 = 0.03688 0.00450 -0.00290 -0.00142 N2 4 0.626805 0.212213 0.510541 11.00000 0.02599 0.02053 = 0.02835 0.00055 0.00328 0.00071 C1 1 0.724793 0.367366 0.439116 11.00000 0.02384 0.02645 = 0.02763 0.00316 0.00317 0.00234 C2 1 0.634153 0.271751 0.426914 11.00000 0.02800 0.02287 = 0.02913 0.00069 0.00191 -0.00186 AFIX 13 H2 2 0.676961 0.229828 0.378061 11.00000 -1.20000 AFIX 0 C3 1 0.489881 0.313122 0.390678 11.00000 0.02586 0.02816 = 0.03643 0.00469 -0.00293 -0.00263 AFIX 23 H3A 2 0.453768 0.270541 0.340960 11.00000 -1.20000 H3B 2 0.420220 0.315011 0.440307 11.00000 -1.20000 AFIX 0 C4 1 0.521294 0.421443 0.354829 11.00000 0.02584 0.02768 = 0.03427 0.00168 -0.00239 0.00043 AFIX 13 H4 2 0.453404 0.468105 0.383999 11.00000 -1.20000 AFIX 0 C5 1 0.517401 0.439711 0.250312 11.00000 0.03900 0.03035 = 0.03578 -0.00059 -0.00443 0.00447 AFIX 13 H5 2 0.418520 0.435222 0.229352 11.00000 -1.20000 AFIX 0 C6 1 0.573491 0.545869 0.227615 11.00000 0.05095 0.02759 = 0.03123 0.00614 0.00280 0.00425 AFIX 23 H6A 2 0.576150 0.554496 0.160727 11.00000 -1.20000 H6B 2 0.508882 0.596358 0.252771 11.00000 -1.20000 AFIX 0 C7 1 0.721839 0.563897 0.267103 11.00000 0.04671 0.02805 = 0.03554 0.00381 0.00702 -0.00513 AFIX 23 H7A 2 0.748494 0.634279 0.256610 11.00000 -1.20000 H7B 2 0.789234 0.521218 0.234214 11.00000 -1.20000 AFIX 0 C8 1 0.731064 0.540639 0.372056 11.00000 0.02957 0.02131 = 0.03909 0.00387 -0.00252 -0.00432 AFIX 13 H8 2 0.831670 0.534280 0.388652 11.00000 -1.20000 AFIX 0 C9 1 0.666959 0.625914 0.430590 11.00000 0.03839 0.02770 = 0.03028 0.00592 -0.00740 -0.00230 C10 1 0.705346 0.799562 0.470357 11.00000 0.06366 0.02956 = 0.04920 -0.00469 -0.00975 -0.00217 AFIX 137 H10A 2 0.673719 0.850235 0.426996 11.00000 -1.50000 H10B 2 0.784920 0.825334 0.504821 11.00000 -1.50000 H10C 2 0.629438 0.783298 0.512358 11.00000 -1.50000 AFIX 0 C11 1 0.654793 0.107745 0.514807 11.00000 0.02717 0.02197 = 0.03069 0.00261 0.00010 -0.00164 C12 1 0.634733 0.078403 0.613570 11.00000 0.02423 0.03106 = 0.02725 0.00229 0.00017 -0.00400 C13 1 0.652234 -0.014205 0.657099 11.00000 0.03722 0.03114 = 0.03946 0.00812 -0.00112 -0.00315 AFIX 43 H13 2 0.682281 -0.071219 0.624243 11.00000 -1.20000 AFIX 0 C14 1 0.623324 -0.019670 0.752356 11.00000 0.03983 0.04607 = 0.03643 0.01695 -0.00032 -0.00795 AFIX 43 H14 2 0.634955 -0.081106 0.783522 11.00000 -1.20000 AFIX 0 C15 1 0.577761 0.065072 0.800538 11.00000 0.04253 0.05900 = 0.03083 0.01093 0.00024 -0.01012 AFIX 43 H15 2 0.557131 0.059216 0.863482 11.00000 -1.20000 AFIX 0 C16 1 0.561887 0.159391 0.757065 11.00000 0.04156 0.04475 = 0.02492 -0.00573 0.00449 -0.00447 AFIX 43 H16 2 0.533452 0.216741 0.790048 11.00000 -1.20000 AFIX 0 C17 1 0.590407 0.163973 0.662290 11.00000 0.02723 0.03263 = 0.02954 0.00103 0.00081 -0.00210 C18 1 0.582465 0.250658 0.596366 11.00000 0.02955 0.03021 = 0.02906 -0.00649 0.00109 -0.00368 HKLF 4 REM lub129_a.res in P2(1)2(1)2(1) REM wR2 = 0.0827, GooF = S = 1.069, Restrained GooF = 1.069 for all data REM R1 = 0.0319 for 3767 Fo > 4sig(Fo) and 0.0333 for all 3923 data REM 237 parameters refined using 0 restraints END WGHT 0.0336 1.4589 REM Highest difference peak 0.514, deepest hole -1.022, 1-sigma level 0.079 Q1 1 0.6416 0.3779 0.1266 11.00000 0.05 0.51 Q2 1 0.5073 0.3173 0.1756 11.00000 0.05 0.45 Q3 1 0.7685 0.3153 0.1774 11.00000 0.05 0.43 Q4 1 0.6434 0.3794 0.2254 11.00000 0.05 0.40 Q5 1 0.6513 0.2760 0.1328 11.00000 0.05 0.34 Q6 1 0.6404 0.3231 0.4715 11.00000 0.05 0.32 Q7 1 0.3639 0.5251 0.3239 11.00000 0.05 0.31 Q8 1 0.6490 0.2711 0.2205 11.00000 0.05 0.29 Q9 1 0.3920 0.3271 0.1763 11.00000 0.05 0.29 Q10 1 0.8550 0.3574 0.4408 11.00000 0.05 0.27 ; _shelx_res_checksum 10564 _shelx_hkl_file ; 1 0 0 0.40 0.60 2 0 0 888.91 59.49 3 0 0 13.30 2.60 4 0 0 5856.81 388.66 5 0 0 0.20 1.60 6 0 0 1355.56 91.69 7 0 0 -3.10 2.00 7 0 0 0.80 2.20 8 0 0 499.35 36.40 8 0 0 529.95 36.90 9 0 0 2.30 2.80 9 0 0 3.10 3.10 10 0 0 754.62 51.09 10 0 0 696.83 50.39 11 0 0 8.70 4.40 11 0 0 1.30 2.60 12 0 0 6.00 2.60 0 1 0 0.40 0.20 0 1 0 0.80 0.40 1 1 0 2380.06 151.28 1 1 0 2184.38 151.28 1 1 0 2451.75 151.48 -1 1 0 2267.27 151.38 -1 1 0 2137.39 151.08 2 1 0 6989.10 523.25 2 1 0 8934.11 523.75 2 1 0 7802.12 523.45 3 1 0 61.59 5.20 3 -1 0 59.19 5.30 4 -1 0 79.69 6.90 4 1 0 78.79 6.80 5 1 0 16.50 3.40 5 -1 0 13.40 3.20 6 -1 0 1986.80 130.19 6 1 0 1901.81 130.19 6 1 0 1926.81 129.89 7 -1 0 67.29 7.50 7 1 0 70.89 7.70 7 1 0 78.59 7.10 8 1 0 495.55 34.00 8 1 0 439.26 33.10 8 -1 0 495.75 33.70 8 -1 0 444.56 33.50 9 -1 0 245.88 18.30 9 1 0 206.88 17.40 9 1 0 252.67 18.60 9 -1 0 206.48 17.80 10 -1 0 136.99 13.00 10 1 0 145.59 13.50 10 1 0 147.49 12.40 10 -1 0 155.38 12.80 11 1 0 31.50 6.00 11 1 0 23.00 4.90 11 -1 0 25.90 5.00 12 -1 0 100.19 9.00 12 1 0 94.69 8.50 0 2 0 1776.92 112.69 0 2 0 1614.04 112.49 1 2 0 654.63 42.80 1 2 0 627.94 42.50 -1 2 0 661.23 42.80 1 2 0 610.14 42.60 -2 2 0 7.00 1.80 2 -2 0 7.40 1.50 2 2 0 6.80 1.30 3 2 0 450.05 27.90 3 -2 0 397.16 28.50 3 2 0 397.86 28.50 4 2 0 1007.30 77.19 4 2 0 1306.27 77.69 4 -2 0 1133.09 77.29 5 -2 0 54.79 5.20 5 2 0 41.50 5.10 6 2 0 27.80 3.80 6 -2 0 26.60 4.10 6 2 0 20.50 4.30 7 -2 0 1662.63 112.59 7 2 0 1668.43 112.39 7 2 0 1679.83 112.99 8 2 0 252.67 19.20 8 2 0 257.07 20.10 8 -2 0 260.77 19.60 9 2 0 42.90 6.00 9 2 0 47.30 7.20 9 -2 0 50.59 6.90 9 -2 0 39.40 6.50 10 -2 0 57.49 7.40 10 2 0 53.29 6.70 10 2 0 66.79 8.80 10 -2 0 62.39 7.80 11 -2 0 108.09 10.10 11 2 0 97.39 9.30 11 2 0 119.49 11.80 11 -2 0 104.79 11.00 12 -2 0 7.00 3.10 12 2 0 5.70 2.30 0 3 0 6.20 1.70 0 3 0 4.40 1.10 1 3 0 6960.70 414.06 -1 3 0 5786.22 414.36 1 3 0 6287.87 413.96 1 3 0 5976.20 414.26 2 3 0 645.64 41.70 -2 3 0 718.63 41.20 2 3 0 602.14 41.90 2 3 0 570.24 41.90 -2 3 0 573.14 42.10 3 3 0 799.32 57.99 3 3 0 944.21 57.79 3 3 0 880.91 57.79 -3 3 0 865.71 57.19 -3 3 0 864.01 58.29 3 -3 0 821.32 58.09 4 -3 0 43.80 4.80 4 3 0 44.60 4.80 4 3 0 52.39 3.90 5 -3 0 3583.84 238.58 5 3 0 3416.56 238.68 5 3 0 3996.70 238.58 5 -3 0 3340.77 238.28 6 -3 0 257.17 16.70 6 -3 0 225.18 17.20 6 3 0 212.28 17.40 7 3 0 23.00 4.00 7 3 0 16.60 3.90 7 -3 0 18.50 4.30 8 3 0 8.30 3.00 8 3 0 7.10 3.30 8 -3 0 13.40 3.30 9 -3 0 741.73 53.79 9 -3 0 802.22 53.29 9 3 0 693.73 52.89 9 3 0 839.62 54.19 10 3 0 1.40 2.20 10 -3 0 0.60 3.30 10 -3 0 2.90 3.10 10 3 0 -2.30 3.30 11 -3 0 66.69 7.60 11 3 0 59.49 6.40 12 -3 0 27.10 5.60 12 3 0 20.70 4.40 0 4 0 2109.59 126.09 0 4 0 1667.83 125.49 1 4 0 3940.31 258.07 1 4 0 3572.74 257.57 -1 4 0 4012.70 258.17 1 4 0 4019.00 257.57 2 4 0 56.59 4.80 2 4 0 65.09 4.50 2 4 0 51.89 4.70 -2 4 0 52.59 5.00 3 -4 0 4304.17 300.27 -3 4 0 4550.94 300.67 3 4 0 4442.36 300.27 3 4 0 4665.13 300.07 3 4 0 4780.72 299.97 -3 4 0 4400.46 299.37 4 -4 0 127.69 9.90 4 4 0 126.99 9.90 5 4 0 4.60 1.90 5 4 0 2.90 1.50 6 4 0 281.67 20.70 6 4 0 277.87 19.90 6 -4 0 264.67 19.80 6 -4 0 278.17 20.10 7 4 0 494.95 36.00 7 4 0 510.25 36.70 7 -4 0 547.25 36.30 8 -4 0 24.60 4.40 8 4 0 29.30 4.50 9 4 0 4.80 3.30 9 -4 0 -0.20 2.80 10 4 0 75.59 8.70 10 -4 0 58.09 7.90 10 4 0 55.39 6.50 10 -4 0 72.39 8.30 11 4 0 187.28 14.40 11 -4 0 190.98 15.30 0 5 0 5.20 1.40 0 5 0 3.70 1.40 1 5 0 681.73 51.79 1 5 0 750.22 52.19 -1 5 0 775.82 52.39 -1 5 0 806.32 51.99 1 5 0 838.82 51.79 2 5 0 1001.00 69.59 2 5 0 1088.59 70.19 -2 5 0 990.40 68.99 2 5 0 1008.90 69.79 -2 5 0 1121.99 70.49 3 -5 0 26.20 3.50 3 5 0 28.50 3.00 -3 5 0 29.80 2.20 3 5 0 29.40 3.50 3 5 0 35.00 3.50 -3 5 0 32.90 4.10 -4 5 0 21.10 3.90 -4 5 0 15.30 1.50 4 5 0 16.60 2.50 4 -5 0 17.60 3.20 4 5 0 16.20 1.30 4 5 0 17.60 3.10 5 5 0 1282.47 75.19 5 5 0 1016.30 75.09 5 -5 0 1040.20 74.99 6 -5 0 253.07 18.60 6 5 0 253.97 18.90 7 -5 0 81.19 7.40 7 5 0 77.09 7.40 7 -5 0 79.79 7.80 7 5 0 87.39 8.30 8 -5 0 7.70 2.90 8 5 0 5.50 2.30 8 5 0 8.90 3.20 9 -5 0 237.98 19.70 9 5 0 280.47 20.50 9 5 0 265.97 19.40 10 5 0 89.79 8.40 10 -5 0 92.29 10.40 10 -5 0 98.09 9.70 10 5 0 95.99 10.00 11 5 0 29.70 4.80 11 -5 0 30.40 5.90 0 6 0 3399.06 211.98 0 6 0 2957.90 211.08 1 6 0 1479.75 101.59 -1 6 0 1517.85 101.79 -1 6 0 1679.73 100.29 1 6 0 1498.85 100.99 -1 6 0 1391.26 101.19 -2 6 0 55.69 4.00 2 6 0 53.59 4.80 2 6 0 55.99 4.90 -2 6 0 64.89 5.90 -3 6 0 517.45 39.30 3 6 0 610.94 38.50 3 -6 0 509.05 38.50 -3 6 0 651.13 37.70 3 6 0 553.74 38.80 3 6 0 557.24 38.60 4 6 0 1979.00 123.89 -4 6 0 1889.31 122.69 4 6 0 1890.81 123.79 -4 6 0 1824.72 124.79 4 6 0 1793.32 122.59 4 -6 0 1760.72 123.79 4 6 0 1838.12 123.89 4 6 0 1844.02 123.59 5 -6 0 3.80 1.90 5 6 0 2.20 1.60 5 6 0 5.90 1.70 6 -6 0 332.27 23.80 6 6 0 360.46 23.50 6 6 0 276.97 22.70 7 6 0 921.31 55.79 7 -6 0 810.72 55.49 7 6 0 740.43 55.89 7 -6 0 782.42 55.59 8 -6 0 200.28 15.10 8 6 0 195.28 15.30 8 6 0 176.28 14.40 9 6 0 146.49 12.80 9 6 0 142.79 11.80 9 -6 0 148.19 13.90 10 -6 0 141.79 12.30 10 6 0 135.49 11.20 11 6 0 1.60 2.10 11 -6 0 -1.80 2.90 0 7 0 1.50 1.60 0 7 0 -0.10 0.40 0 7 0 2.00 1.40 0 7 0 0.70 1.20 1 7 0 236.88 15.60 -1 7 0 252.17 15.60 1 7 0 226.88 16.50 -1 7 0 215.58 16.70 -2 7 0 4271.57 256.87 -2 7 0 3922.61 255.77 2 7 0 3835.32 255.77 2 7 0 3940.21 256.67 -2 7 0 3675.33 256.97 2 7 0 3817.32 256.57 2 7 0 3813.82 257.37 -2 7 0 3911.81 257.77 2 7 0 3594.84 256.47 3 7 0 97.89 7.40 3 7 0 97.39 7.90 3 -7 0 83.79 7.40 -3 7 0 94.79 8.50 -3 7 0 92.59 6.30 3 7 0 82.49 7.40 3 7 0 92.49 6.20 3 7 0 93.39 7.30 -4 7 0 322.27 21.40 4 7 0 310.77 22.50 4 7 0 329.67 21.30 4 -7 0 304.77 22.50 4 7 0 356.26 22.60 4 7 0 335.37 22.90 -4 7 0 288.07 23.50 4 7 0 314.57 22.40 5 -7 0 199.08 14.90 5 7 0 202.58 15.00 6 7 0 531.65 38.00 6 7 0 528.75 37.80 6 -7 0 581.44 38.00 7 7 0 33.20 4.80 7 -7 0 22.80 4.00 7 -7 0 37.40 6.00 7 7 0 26.80 4.20 8 7 0 441.76 37.10 8 -7 0 491.85 35.00 8 7 0 556.44 36.20 8 -7 0 548.05 36.10 9 7 0 4.10 2.50 9 7 0 -0.10 3.20 10 -7 0 3.90 3.10 10 7 0 -0.30 2.00 10 7 0 1.70 4.50 11 7 0 1.50 2.40 11 -7 0 0.10 3.20 0 8 0 4228.28 315.47 0 8 0 4664.83 314.47 0 8 0 4686.23 313.57 0 8 0 5372.26 314.67 -1 8 0 672.53 49.70 -1 8 0 689.13 49.99 -1 8 0 733.03 48.90 1 8 0 812.12 50.99 1 8 0 700.03 49.80 1 8 0 728.73 49.80 1 8 0 739.33 48.80 -1 8 0 811.52 51.19 -2 8 0 39.50 4.80 2 8 0 40.10 4.30 -2 8 0 36.70 5.50 2 8 0 36.30 4.80 2 8 0 47.80 2.90 3 -8 0 1034.90 74.79 -3 8 0 1118.49 73.99 3 8 0 1102.99 73.89 -3 8 0 1148.69 76.39 3 8 0 1156.58 74.99 3 8 0 1274.07 75.99 3 8 0 999.20 74.89 3 8 0 1159.58 74.99 -3 8 0 1044.00 75.49 4 8 0 309.07 19.30 -4 8 0 246.78 19.80 4 8 0 277.37 17.80 4 -8 0 258.97 19.00 4 8 0 259.87 19.10 -4 8 0 238.68 20.30 4 8 0 266.27 19.00 4 8 0 259.07 19.60 -4 8 0 282.57 17.90 5 8 0 45.20 4.90 5 -8 0 37.00 5.20 5 8 0 35.70 4.70 6 8 0 255.57 17.90 6 -8 0 222.08 18.70 7 8 0 540.75 40.00 7 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2 586.74 40.70 6 8 -2 206.88 15.00 6 -8 2 194.08 15.20 6 8 -2 196.38 14.90 6 8 2 203.58 15.40 6 -8 -2 221.08 16.00 6 8 2 187.08 15.00 -6 8 -2 185.68 16.20 7 8 -2 117.99 10.40 7 -8 2 130.59 10.50 7 8 -2 141.09 10.90 -7 8 -2 134.29 12.50 7 8 2 156.28 11.80 7 -8 -2 156.98 12.50 7 8 2 109.89 10.90 8 -8 2 178.58 12.80 8 8 -2 147.59 13.00 8 8 -2 188.58 14.90 8 8 2 161.58 15.90 -8 8 -2 142.09 15.90 9 8 -2 162.38 13.40 9 8 -2 156.68 12.30 9 8 2 176.58 14.40 9 8 2 172.68 13.40 -9 8 -2 172.58 15.20 10 -8 2 148.19 12.80 10 8 2 106.69 8.90 0 9 2 2533.15 167.88 0 9 -2 2257.27 165.48 0 9 -2 2463.05 165.88 0 9 2 2491.65 165.88 0 9 -2 2614.44 166.38 0 9 2 2593.74 166.38 -1 9 2 1155.78 77.49 -1 9 2 1149.98 77.29 -1 9 2 1139.69 76.29 1 9 -2 1133.69 77.19 -1 9 2 1220.98 78.79 1 9 -2 1097.49 76.39 1 9 -2 1156.48 77.59 -1 9 -2 976.30 65.59 1 9 2 1024.10 66.89 -1 9 -2 957.40 64.99 1 9 2 946.01 65.29 -1 9 -2 966.20 64.09 -1 9 -2 922.31 66.79 2 9 -2 186.48 14.10 -2 9 2 179.48 14.00 -2 9 2 201.08 12.60 -2 9 2 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6.80 9 1 -3 25.20 4.90 9 -1 3 34.20 5.60 9 -1 3 24.10 6.20 9 -1 -3 31.50 6.80 9 -1 -3 25.30 5.10 9 1 3 21.20 5.60 9 1 3 31.70 5.70 10 -1 3 346.17 26.40 10 1 -3 360.06 25.60 10 -1 3 345.97 25.90 10 1 -3 362.36 26.80 10 1 3 330.67 25.00 10 1 3 347.67 25.10 10 -1 -3 336.87 24.50 10 -1 -3 324.67 25.50 11 1 -3 29.30 5.80 11 -1 3 41.70 8.50 11 1 -3 34.70 5.30 11 -1 3 36.00 6.20 11 1 3 28.80 5.50 11 -1 -3 33.40 5.10 12 1 -3 12.40 2.90 12 -1 3 8.00 3.90 12 -1 -3 19.30 4.50 12 1 3 19.50 4.00 0 2 -3 107.49 8.80 1 -2 3 2914.71 210.08 -1 2 3 3156.38 210.88 1 2 -3 3448.46 210.58 1 2 3 3211.08 212.38 1 2 3 3254.07 213.08 -1 2 -3 3140.29 212.48 2 -2 3 3571.74 225.08 -2 2 3 3206.48 225.48 2 2 -3 3268.27 225.58 2 2 -3 3540.75 225.38 2 2 3 3823.42 252.37 2 2 3 3768.62 251.87 3 2 -3 262.27 19.00 3 2 -3 270.57 18.60 -3 2 3 262.07 18.50 3 -2 3 271.47 18.30 3 2 3 542.35 36.00 3 2 3 514.95 36.30 4 2 -3 1154.38 82.99 -4 2 3 1191.18 82.29 4 2 -3 1171.18 82.49 4 -2 3 1353.96 82.39 -4 2 3 1323.67 81.59 4 -2 3 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7.70 4.40 11 2 3 13.20 3.70 11 2 3 14.70 5.30 11 -2 -3 7.60 2.90 12 2 -3 37.00 5.30 12 -2 3 43.70 7.40 12 -2 -3 38.30 5.20 12 2 3 43.00 6.30 0 3 -3 17.00 2.70 1 3 -3 2441.76 160.08 1 3 -3 2412.76 160.48 -1 3 3 2386.06 160.78 -1 3 -3 2889.21 197.18 1 3 3 3171.08 197.78 1 3 3 2843.22 196.98 2 -3 3 689.13 44.40 -2 3 3 656.63 45.10 2 3 -3 635.04 44.80 2 3 -3 679.03 44.90 2 3 3 839.42 55.59 2 3 3 813.32 56.09 3 -3 3 3141.19 196.88 3 3 -3 3003.90 197.18 3 3 -3 2842.12 197.18 -3 3 3 2877.01 197.18 3 3 3 3301.97 227.58 3 3 3 3233.88 227.78 3 3 3 3733.43 227.58 4 3 -3 168.88 13.10 4 -3 3 188.68 13.40 4 3 -3 183.68 13.50 -4 3 3 180.78 13.10 4 -3 3 182.88 12.90 4 3 3 211.98 15.70 4 3 3 219.98 15.80 5 3 -3 531.55 36.20 5 3 -3 505.15 35.60 5 -3 3 513.15 35.50 5 -3 3 527.55 35.50 5 3 3 382.76 25.20 5 -3 -3 325.27 25.90 5 3 3 347.77 25.30 5 3 3 344.57 24.30 5 3 3 380.66 25.10 6 -3 3 20.00 3.50 6 3 -3 26.30 3.90 6 3 -3 14.60 4.60 6 -3 3 20.20 3.30 6 -3 -3 6.20 3.00 6 3 3 4.70 2.10 6 3 3 7.00 2.10 7 3 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224.98 19.20 9 4 3 277.77 20.60 9 -4 -3 277.07 20.30 10 4 -3 82.69 8.00 10 4 -3 97.69 9.60 10 -4 3 93.69 9.60 10 4 3 95.89 9.20 10 4 3 110.59 11.00 10 -4 -3 104.79 9.70 10 -4 -3 103.89 10.50 11 -4 3 28.30 6.20 11 4 -3 23.70 5.40 11 4 3 31.30 5.00 11 -4 -3 33.70 5.30 0 5 3 1385.36 97.99 0 5 -3 1480.35 98.79 0 5 3 1565.94 99.49 1 5 -3 1270.97 88.39 -1 5 3 1275.67 89.59 -1 5 3 1392.66 88.99 1 5 -3 1391.06 89.29 -1 5 -3 1104.79 79.79 1 5 3 1350.76 79.69 1 5 3 1108.89 80.19 -2 5 3 694.13 49.70 2 5 -3 736.03 48.80 -2 5 3 746.93 49.10 2 5 -3 737.63 49.40 2 5 3 753.22 43.90 -2 5 -3 645.24 44.60 2 5 3 585.84 44.20 2 5 3 618.94 44.70 -3 5 3 2220.48 158.38 3 5 -3 2432.76 158.28 3 -5 3 2508.95 157.48 3 5 -3 2331.87 157.88 3 5 3 2264.47 166.38 3 5 3 2249.38 166.58 3 5 3 2972.10 165.88 4 -5 3 1329.67 105.09 4 5 -3 1582.34 105.19 4 5 -3 1514.95 104.79 4 5 -3 1583.54 104.99 4 -5 3 1738.63 104.69 -4 5 3 1705.13 105.59 -4 5 3 1533.75 103.99 4 5 3 1430.66 94.99 4 5 3 1509.85 95.39 4 5 3 1347.17 94.39 4 5 3 1377.06 95.29 -5 5 3 176.28 14.10 5 5 -3 179.08 13.60 -5 5 3 172.48 12.20 5 -5 3 182.28 16.30 5 5 -3 175.68 13.70 5 5 -3 197.98 13.50 5 -5 3 193.28 13.20 5 5 3 136.19 10.20 5 5 3 129.59 9.60 5 -5 -3 118.99 11.10 5 5 3 141.79 10.30 5 5 3 117.79 10.80 6 5 -3 774.22 52.49 6 -5 3 768.02 51.99 6 -5 3 774.52 52.29 6 5 -3 751.62 52.09 6 5 3 726.23 51.89 6 -5 -3 751.62 52.29 6 5 3 776.12 51.39 7 5 -3 1039.70 72.09 7 -5 3 1069.89 72.09 7 -5 3 1098.69 72.09 7 5 -3 1060.09 72.59 7 5 3 827.92 57.49 7 5 3 829.12 56.69 7 -5 -3 830.52 57.49 8 5 -3 208.38 15.50 8 -5 3 191.08 14.30 8 5 -3 171.58 14.50 8 -5 3 210.48 15.40 8 5 3 236.88 17.50 8 -5 -3 230.28 17.40 8 5 3 183.28 16.10 9 5 -3 66.89 6.70 9 -5 3 78.09 8.50 9 5 -3 54.79 9.80 9 5 3 61.69 6.60 9 -5 -3 48.60 10.40 10 -5 3 139.49 12.40 10 5 -3 164.08 12.70 10 5 -3 122.29 11.00 10 5 3 116.89 10.30 10 -5 -3 128.19 11.10 10 -5 -3 126.39 12.00 11 5 -3 22.80 4.70 11 -5 3 27.80 6.70 11 5 3 19.00 4.40 0 6 -3 4.00 1.80 0 6 3 3.70 1.20 0 6 -3 3.60 1.80 0 6 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6 3 25.70 5.50 7 -6 -3 35.60 6.10 8 6 -3 417.06 27.30 8 -6 3 381.76 26.20 8 6 -3 327.57 26.20 8 6 3 379.06 26.00 8 6 3 297.87 24.70 8 -6 -3 365.76 25.70 9 6 -3 76.79 7.40 9 -6 3 88.19 8.90 9 6 -3 68.99 8.10 9 6 3 55.09 7.60 9 6 3 54.99 6.10 9 -6 -3 47.50 7.50 10 6 -3 94.29 9.10 10 -6 3 124.99 10.60 10 6 -3 124.09 10.80 -10 6 -3 86.29 11.00 10 6 3 98.99 8.70 10 -6 -3 90.99 11.30 10 6 3 111.49 11.10 11 -6 3 4.80 4.30 11 -6 -3 4.20 2.60 11 6 3 1.00 2.00 0 7 3 3326.77 220.78 0 7 3 3292.97 222.28 0 7 -3 3416.56 221.58 0 7 -3 3440.76 220.38 0 7 3 3638.44 221.48 0 7 -3 2857.41 222.18 -1 7 3 613.84 43.50 -1 7 3 719.03 44.60 1 7 -3 663.23 43.80 1 7 -3 652.43 42.50 1 7 -3 612.64 44.40 -1 7 3 579.94 43.20 -1 7 -3 555.04 38.00 -1 7 -3 525.55 37.40 1 7 3 606.84 38.70 1 7 3 510.85 37.50 -2 7 3 195.38 14.80 2 7 -3 198.28 13.90 -2 7 3 169.98 14.00 2 7 -3 176.88 13.30 2 7 -3 200.58 14.30 -2 7 3 214.28 14.10 2 7 3 302.47 18.90 -2 7 -3 245.98 19.30 2 7 3 239.78 19.40 3 7 -3 89.09 7.20 3 7 3 226.98 16.20 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542.85 35.80 -6 8 -3 504.55 36.80 6 8 3 500.75 36.00 7 -8 3 41.00 4.60 7 8 -3 30.60 4.90 7 8 -3 33.30 5.20 -7 8 -3 21.20 5.20 7 -8 -3 25.50 4.90 7 8 3 21.30 4.40 7 8 3 26.80 5.00 8 -8 3 158.48 10.90 8 8 -3 140.89 11.70 8 8 -3 121.59 10.90 8 -8 -3 137.19 13.10 8 8 3 155.38 12.20 8 8 3 137.19 11.50 -8 8 -3 134.59 13.10 9 8 -3 127.49 12.90 9 -8 3 144.59 12.00 9 -8 3 144.89 10.60 -9 8 -3 120.79 10.90 9 8 3 95.79 8.90 10 -8 3 11.70 4.70 10 8 3 4.60 2.20 0 9 3 293.07 20.40 0 9 -3 273.17 19.80 1 9 -3 679.83 46.50 -1 9 3 712.13 47.50 1 9 -3 642.24 45.70 -1 9 3 666.63 46.00 -1 9 3 680.33 46.20 -1 9 -3 730.43 56.59 1 9 3 808.22 55.39 1 9 3 899.11 56.69 -2 9 3 384.96 24.80 2 9 -3 391.46 26.50 2 9 -3 370.06 26.00 -2 9 3 395.36 26.20 -2 9 3 359.06 27.20 -2 9 3 328.97 25.90 2 9 3 494.35 32.30 2 9 3 466.95 33.10 -2 9 -3 420.76 32.50 -3 9 3 1731.23 102.09 -3 9 3 1372.26 100.49 3 9 -3 1286.07 100.29 3 9 -3 1569.44 100.99 -3 9 3 1528.75 99.19 -3 9 -3 1600.94 113.59 3 9 3 1868.81 114.09 3 9 3 1584.24 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4 -4 325.47 22.60 7 -4 4 298.07 21.50 7 -4 4 311.77 21.90 7 4 -4 280.37 21.70 7 4 4 270.97 20.70 7 4 4 286.47 21.40 7 -4 -4 290.77 22.10 8 4 -4 534.65 34.90 8 -4 4 488.55 33.50 8 4 -4 440.56 33.70 8 -4 4 495.05 34.10 8 -4 4 474.65 35.10 8 4 4 420.16 29.10 8 4 4 369.26 28.10 8 -4 -4 392.26 29.20 9 -4 4 13.80 4.10 9 4 -4 6.40 3.00 9 -4 4 12.70 4.30 9 4 -4 10.30 2.80 9 4 4 42.80 5.80 9 -4 -4 35.00 7.30 9 4 4 38.10 6.70 10 4 -4 96.29 8.80 10 4 -4 107.39 10.30 10 -4 4 115.09 10.50 10 4 4 63.79 7.40 10 -4 -4 65.09 7.20 10 4 4 72.99 9.30 10 -4 -4 73.09 9.10 11 -4 4 60.09 8.00 11 4 4 59.09 6.80 11 -4 -4 57.49 6.40 0 5 -4 1832.42 117.49 0 5 4 1684.03 118.09 -1 5 4 2108.29 141.89 1 5 -4 2229.28 142.19 1 5 -4 2037.10 141.19 -1 5 4 2151.48 142.79 1 5 4 2019.20 125.89 1 5 4 1837.12 126.69 -1 5 -4 1700.73 125.99 1 5 4 1988.10 125.59 2 5 -4 233.78 15.70 2 5 -4 217.48 16.40 -2 5 4 236.18 16.10 -2 5 4 220.78 16.70 2 5 4 250.27 19.30 2 5 4 311.47 18.90 -2 5 -4 262.97 19.70 2 5 4 261.47 20.00 3 -5 4 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4.60 10 -7 4 0.80 3.60 10 7 4 2.10 2.20 0 8 -4 544.35 38.50 0 8 4 608.24 38.60 0 8 4 521.65 39.30 -1 8 4 1225.78 72.89 1 8 -4 1047.80 72.79 -1 8 4 957.70 73.39 1 8 4 919.21 72.29 1 8 4 1218.18 71.89 -1 8 -4 1041.30 71.89 -2 8 4 275.97 22.50 -2 8 4 262.17 19.10 -2 8 -4 322.67 25.60 -3 8 4 158.28 13.80 -3 8 4 195.48 14.80 -3 8 4 191.88 13.90 3 8 -4 190.48 14.30 3 8 4 195.28 14.50 -3 8 -4 170.88 15.10 3 8 4 211.78 15.50 4 8 -4 262.77 19.80 -4 8 4 267.07 17.90 4 -8 4 229.48 19.30 -4 8 4 306.87 20.60 4 8 4 236.98 20.30 -4 8 -4 258.07 21.10 4 8 4 328.77 21.40 4 8 4 308.97 21.00 5 8 -4 744.03 50.09 -5 8 4 693.63 50.39 5 -8 4 742.83 49.70 5 8 -4 711.63 49.20 -5 8 4 722.93 48.00 5 8 4 784.02 50.79 5 8 4 717.93 51.09 -5 8 -4 759.72 51.69 5 8 4 778.42 51.19 5 -8 -4 655.23 51.19 6 8 -4 271.07 19.60 6 -8 4 265.87 19.50 6 -8 -4 161.28 14.60 6 8 4 204.68 14.60 -6 8 -4 177.58 15.10 6 8 4 163.38 13.60 7 8 -4 6.30 3.20 7 8 4 5.10 2.90 -7 8 -4 6.50 3.80 7 -8 -4 4.10 4.00 8 -8 4 100.69 8.00 8 8 -4 90.69 9.60 8 -8 -4 123.09 12.50 -8 8 -4 125.59 12.20 9 -8 4 68.39 6.00 9 -8 4 60.89 7.40 9 8 4 119.99 10.30 9 8 4 127.09 11.70 -9 8 -4 136.89 12.70 10 -8 4 53.59 7.80 10 8 4 33.40 4.90 0 9 -4 540.15 39.80 0 9 4 611.84 41.00 -1 9 4 416.86 31.90 1 9 -4 470.05 31.10 1 9 4 521.25 32.90 1 9 4 419.06 33.60 -1 9 -4 467.55 33.00 2 9 -4 7.80 2.30 -2 9 4 13.50 3.90 -2 9 4 10.60 2.50 -2 9 -4 1.80 2.30 2 9 4 1.20 1.90 2 9 4 3.80 2.30 -3 9 4 380.96 23.80 3 9 -4 352.36 25.60 -3 9 4 333.57 26.20 -3 9 -4 352.16 27.10 3 9 4 351.36 27.20 3 9 4 417.06 26.70 -4 9 4 1104.89 67.69 4 -9 4 844.92 66.19 -4 9 4 1004.60 64.79 4 9 -4 1015.50 66.79 -4 9 4 906.21 66.29 -4 9 -4 851.21 60.59 4 9 4 1010.80 60.99 4 9 4 776.02 59.79 -5 9 4 68.09 8.20 5 -9 4 61.69 6.50 -5 9 4 63.59 4.70 5 9 -4 65.59 7.30 5 9 4 38.20 5.20 5 -9 -4 41.10 7.10 5 9 4 49.10 6.20 -5 9 -4 45.30 6.60 6 -9 4 219.48 16.30 -6 9 -4 176.38 15.30 6 -9 -4 181.98 15.60 6 9 4 188.88 14.70 7 -9 4 152.28 11.60 7 9 4 205.08 14.80 7 9 4 171.08 16.30 7 -9 -4 161.38 18.20 -7 9 -4 220.18 20.10 8 -9 4 71.49 6.30 -8 9 -4 64.59 9.00 8 9 4 73.89 8.20 8 9 4 66.19 6.80 9 -9 4 13.50 4.00 9 9 4 32.10 4.60 10 -9 4 42.60 7.10 10 9 4 64.19 6.20 0 10 4 86.99 8.80 0 10 4 84.99 7.90 0 10 -4 85.49 8.00 1 10 -4 34.50 5.00 -1 10 4 39.80 5.30 -1 10 4 46.90 6.20 1 10 4 37.50 5.70 -1 10 -4 29.60 4.80 1 10 4 30.00 4.90 -2 10 4 1303.67 93.09 -2 10 4 1341.07 91.69 2 10 -4 1439.96 93.39 -2 10 4 1445.66 94.49 2 10 4 1463.45 103.39 2 10 4 1561.44 104.49 -2 10 -4 1581.94 103.79 3 10 -4 -0.80 2.30 -3 10 4 3.40 0.80 -3 10 4 6.90 3.00 -3 10 -4 12.10 3.50 3 10 4 12.00 3.00 -4 10 4 311.57 24.20 -4 10 4 325.27 21.20 4 10 -4 324.37 23.30 4 -10 4 302.97 22.90 -4 10 -4 248.88 18.90 4 10 4 240.68 18.10 4 -10 -4 212.28 18.80 4 10 4 267.07 19.00 5 -10 4 53.89 6.40 -5 10 4 63.79 11.20 -5 10 4 61.39 8.80 5 10 -4 75.59 7.70 -5 10 4 63.49 4.60 5 10 4 55.19 4.40 5 10 4 66.39 7.30 -5 10 -4 50.89 7.50 5 -10 -4 51.79 8.60 5 10 4 44.80 6.00 6 -10 4 347.47 24.60 -6 10 -4 345.07 24.70 6 10 4 304.37 23.30 7 -10 4 27.70 3.60 7 10 4 6.40 2.70 -7 10 -4 3.60 4.20 8 -10 4 162.88 13.50 8 -10 4 167.88 12.20 8 10 4 141.89 11.60 -8 10 -4 152.68 13.70 9 -10 4 12.70 4.20 9 -10 4 10.10 2.20 9 10 4 8.00 3.50 0 11 4 467.15 33.80 0 11 4 491.05 35.20 0 11 -4 487.55 33.90 -1 11 4 127.59 8.90 -1 11 4 154.68 12.50 1 11 -4 134.09 10.90 -1 11 4 109.69 10.60 -1 11 -4 177.58 14.60 1 11 4 195.58 15.90 -2 11 4 252.37 17.50 2 11 -4 255.67 19.40 -2 11 4 253.27 20.50 -2 11 4 282.67 19.50 2 11 4 217.28 17.80 -2 11 -4 224.88 17.10 2 11 4 223.58 16.80 -3 11 4 637.44 42.80 3 11 -4 590.44 41.50 -3 11 4 556.04 39.60 -3 11 -4 591.14 44.30 3 11 4 678.73 45.20 -4 11 4 386.26 26.20 4 -11 4 385.96 27.90 4 11 -4 408.86 28.40 -4 11 4 386.06 29.40 4 11 4 449.36 29.90 -4 11 -4 449.16 32.20 4 11 4 425.56 31.60 4 11 4 467.25 32.60 -5 11 4 8.00 4.40 5 11 -4 11.20 4.00 -5 11 -4 0.30 3.20 5 11 4 -1.00 2.20 5 11 4 1.40 4.90 6 -11 4 200.88 14.90 -6 11 -4 158.28 13.80 6 11 4 158.18 12.60 7 -11 4 100.89 8.10 7 11 4 55.09 6.00 8 -11 4 56.39 5.30 8 -11 4 65.19 8.70 8 11 4 64.69 6.40 9 11 4 2.80 2.00 0 12 4 677.33 45.60 0 12 4 641.04 43.90 0 12 4 661.53 47.10 0 12 -4 657.13 45.60 1 12 -4 50.69 6.40 -1 12 4 49.20 3.70 1 12 4 98.69 9.60 -1 12 -4 83.69 8.20 1 12 4 72.19 5.80 2 12 -4 383.96 28.10 -2 12 4 404.96 26.20 -2 12 4 385.86 29.40 2 12 4 349.07 23.70 2 12 4 318.77 21.70 2 12 4 303.47 24.60 -2 12 -4 324.37 23.80 -3 12 4 115.49 7.70 3 12 -4 119.79 10.20 -3 12 4 111.89 11.50 3 -12 4 96.59 9.60 3 12 4 166.08 14.00 3 12 4 148.69 13.40 -3 12 -4 172.18 13.40 3 12 4 157.98 10.90 4 -12 4 282.57 19.90 -4 12 4 250.47 21.70 4 12 -4 278.97 20.60 -4 12 4 264.37 18.10 4 12 4 263.47 18.60 -4 12 -4 284.97 21.30 4 12 4 270.07 22.20 4 12 4 292.47 20.50 5 12 -4 408.16 31.10 5 -12 4 448.36 30.20 -5 12 -4 417.96 28.80 5 12 4 372.86 28.10 6 -12 4 77.39 6.70 -6 12 -4 75.39 9.30 6 12 4 89.09 7.90 7 -12 4 39.70 4.20 7 12 4 39.80 5.20 7 -12 -4 46.30 6.30 8 -12 4 37.10 3.80 8 12 4 33.00 4.50 0 13 -4 95.79 9.10 0 13 4 79.29 9.90 0 13 4 102.09 6.60 1 13 -4 325.47 23.50 -1 13 4 298.97 23.30 -1 13 4 345.67 25.40 -1 13 4 321.67 21.70 -1 13 -4 285.77 20.70 1 13 4 311.77 22.30 1 13 4 242.28 20.30 1 13 4 276.47 18.70 2 13 -4 49.10 9.60 -2 13 4 62.29 4.10 2 -13 4 45.90 6.10 2 13 4 57.19 9.40 2 13 4 52.59 3.80 -2 13 -4 57.09 9.40 2 13 4 41.40 6.00 3 -13 4 433.76 31.50 -3 13 4 439.76 30.00 -3 13 4 475.95 33.70 3 13 -4 446.86 32.00 3 13 4 296.67 23.90 3 13 4 335.37 22.30 3 13 4 358.56 25.60 -3 13 -4 343.17 24.50 -4 13 4 19.20 2.40 4 -13 4 27.80 4.20 4 13 4 18.10 2.20 -4 13 -4 13.80 4.20 4 13 4 21.60 4.30 5 -13 4 100.69 8.40 -5 13 -4 69.39 8.80 5 13 4 84.99 7.50 6 -13 4 33.50 4.00 6 13 4 36.00 4.90 7 -13 4 189.68 13.50 7 -13 -4 211.88 14.90 7 13 4 194.78 14.90 0 14 4 72.79 7.10 0 14 -4 63.69 8.50 0 14 4 72.69 5.20 0 -14 4 69.49 7.30 0 14 4 78.09 9.00 -1 14 4 151.18 10.00 -1 14 4 132.79 11.70 1 -14 4 135.59 11.70 -1 14 4 163.98 14.10 -1 14 -4 171.78 14.00 1 14 4 157.18 13.10 1 14 4 168.18 11.50 1 14 4 175.88 15.20 -1 -14 4 171.98 13.60 -2 14 4 107.29 7.40 -2 14 4 118.79 11.60 2 -14 4 89.19 8.90 2 14 4 101.09 6.90 -2 14 -4 92.29 9.80 -3 14 4 181.18 12.00 -3 14 4 151.38 15.60 3 -14 4 193.08 13.50 3 14 4 151.48 11.30 3 14 4 136.59 13.10 3 14 4 125.59 9.40 -3 14 -4 134.39 12.10 4 -14 4 33.40 4.40 4 14 4 15.70 3.90 -4 14 -4 15.90 6.70 5 14 4 225.28 16.60 6 -14 4 23.10 3.20 6 14 4 16.30 3.90 0 15 4 95.49 7.00 0 -15 4 101.59 9.10 1 -15 4 116.39 9.60 -1 15 4 94.89 8.40 -1 15 4 120.39 12.10 1 15 4 121.09 13.20 1 15 4 153.08 11.10 2 -15 4 29.40 4.70 2 15 4 39.70 10.60 2 15 4 31.00 4.60 3 -15 4 133.29 10.50 3 15 4 132.79 10.60 4 -15 4 103.59 8.40 4 15 4 96.69 9.50 5 -15 4 2.60 1.70 5 15 4 4.50 2.40 0 -16 4 12.80 4.10 1 -16 4 81.19 8.30 2 -16 4 157.28 12.20 2 16 4 140.59 10.90 3 -16 4 42.60 5.20 3 16 4 46.80 5.10 0 0 -5 0.40 0.90 1 0 -5 329.37 22.10 -1 0 -5 320.47 22.20 2 0 -5 6398.36 410.16 -2 0 -5 6183.58 410.16 2 0 5 5988.90 410.16 3 0 5 984.30 62.59 3 0 -5 956.50 62.89 3 0 5 965.50 62.89 -3 0 5 839.12 63.29 4 0 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767.62 51.79 5 -2 5 714.93 51.99 5 2 -5 825.52 52.19 5 2 -5 768.82 52.99 5 2 5 668.33 42.50 5 2 5 580.84 42.70 5 2 5 646.14 41.50 5 2 5 561.34 42.10 6 2 -5 273.67 20.20 6 -2 5 267.37 20.90 6 2 -5 312.97 21.50 6 -2 5 286.87 20.30 6 -2 5 278.47 19.80 6 -2 -5 242.48 21.90 6 2 5 306.67 21.20 6 2 5 296.97 20.80 6 2 5 287.67 20.90 7 2 -5 241.58 17.30 7 -2 5 208.58 15.20 7 -2 5 189.98 16.40 7 -2 5 214.28 15.90 7 2 -5 207.78 15.80 7 2 5 192.98 14.60 7 -2 -5 183.28 16.10 7 2 5 190.08 14.70 7 2 5 173.78 13.30 8 -2 5 178.78 13.70 8 -2 5 161.58 14.40 8 2 -5 169.38 13.40 8 2 -5 200.08 15.10 8 -2 5 162.08 12.70 8 2 5 163.18 14.00 8 -2 -5 177.38 15.40 8 2 5 178.08 14.00 9 -2 5 233.08 18.70 9 2 -5 209.38 17.30 9 2 -5 274.37 19.20 9 -2 5 227.18 17.90 9 -2 -5 195.08 14.90 9 2 5 180.08 15.10 9 -2 -5 181.68 16.30 9 2 5 186.58 15.30 10 -2 5 28.70 5.50 10 -2 5 17.40 4.20 10 2 -5 29.60 6.40 10 2 -5 21.00 4.80 10 -2 -5 19.90 4.80 10 2 5 20.40 5.40 10 -2 -5 31.50 7.00 11 -2 5 8.90 3.90 11 -2 -5 18.40 4.50 11 2 5 15.20 4.00 0 3 5 22.90 3.80 -1 3 5 3136.59 212.88 1 3 -5 3249.87 212.28 1 3 5 2990.50 197.28 -1 3 -5 2913.51 196.38 2 3 -5 1642.44 106.39 -2 3 5 1650.93 106.89 2 -3 5 1457.05 106.09 2 3 -5 1610.44 106.19 2 3 5 1624.74 113.09 2 3 5 1764.02 112.69 2 3 5 1705.73 114.09 -2 3 -5 1676.03 113.29 3 3 -5 2803.92 176.68 3 -3 5 2712.63 175.98 -3 3 5 2526.25 176.68 3 -3 5 2593.94 176.38 3 3 -5 2620.64 176.58 -3 3 -5 2188.28 155.68 3 3 5 2195.58 156.28 3 3 5 2740.43 155.08 3 3 5 2203.78 155.48 4 -3 5 217.58 15.50 4 3 -5 205.78 15.90 4 -3 5 225.78 15.30 4 3 -5 212.58 15.70 -4 3 5 215.78 15.60 4 3 5 169.48 13.20 4 3 5 172.28 13.90 4 3 5 175.28 13.20 4 3 5 189.78 12.60 5 3 -5 31.80 4.60 5 -3 5 38.10 4.30 5 3 -5 45.00 5.10 5 3 -5 35.30 4.40 -5 3 5 37.60 4.90 5 -3 5 30.00 4.00 5 3 5 18.80 3.50 5 3 5 19.10 4.00 6 -3 5 1113.29 72.59 6 3 -5 1052.09 72.59 6 -3 5 1048.00 72.59 6 3 -5 1095.39 73.49 6 -3 5 1082.29 73.49 6 3 5 1051.39 69.69 6 3 5 1055.59 69.69 6 3 5 1063.19 69.59 6 3 5 1070.29 68.59 6 -3 -5 867.61 70.49 7 3 -5 993.50 67.29 7 3 -5 1031.20 68.29 7 -3 5 1024.60 67.09 7 -3 5 946.01 67.29 7 -3 5 976.70 68.19 7 3 5 900.01 61.59 7 3 5 940.11 62.99 7 3 5 986.60 62.99 7 -3 -5 844.42 63.99 8 3 -5 66.09 7.10 8 3 -5 84.89 8.50 8 -3 5 76.59 6.90 8 -3 5 72.59 8.10 8 -3 5 89.89 8.10 8 -3 -5 94.69 11.00 8 3 5 114.19 10.00 9 -3 5 4.50 3.80 9 -3 5 5.30 3.50 9 3 -5 5.30 3.30 9 -3 -5 3.00 3.70 9 3 5 0.80 2.70 9 3 5 3.00 3.20 10 -3 5 32.40 5.90 10 3 -5 34.50 6.00 10 3 -5 24.20 5.00 10 3 5 18.80 4.20 -10 3 -5 32.50 6.30 10 -3 -5 21.70 5.00 10 -3 -5 28.40 5.70 10 3 5 29.90 6.80 11 -3 5 43.30 7.50 11 3 5 53.09 6.50 11 -3 -5 39.20 7.90 0 4 -5 559.84 35.50 0 4 5 476.65 34.90 0 4 5 514.35 36.20 1 -4 5 1667.43 105.49 -1 4 5 1707.33 105.19 -1 4 5 1464.45 106.19 1 4 -5 1643.04 105.69 1 4 -5 1412.96 104.89 1 4 5 1498.35 115.09 1 4 5 1856.31 114.29 -1 4 -5 1626.44 114.39 1 4 5 1863.51 113.99 2 4 -5 245.78 17.50 2 -4 5 225.68 17.20 -2 4 5 251.47 17.90 2 4 -5 247.68 16.90 2 4 5 285.07 19.60 2 4 5 243.88 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5 -5 749.33 52.19 3 5 5 859.71 51.29 3 5 5 726.43 52.49 -4 5 5 351.36 25.30 4 5 -5 375.96 25.60 4 -5 5 315.57 25.00 4 -5 5 382.76 25.40 4 5 -5 363.56 24.90 4 5 5 149.29 12.40 -4 5 -5 140.69 12.30 4 5 5 150.18 12.10 4 5 5 166.98 11.20 4 5 5 153.78 12.90 5 5 -5 789.22 54.59 5 -5 5 822.22 54.09 -5 5 5 805.72 54.89 -5 5 5 740.53 53.29 5 -5 5 841.52 54.69 5 5 -5 822.22 55.09 5 5 5 723.93 49.00 5 5 5 748.63 49.20 -5 5 -5 620.64 48.90 5 5 5 727.03 48.60 5 5 5 716.73 47.90 6 -5 5 87.29 7.70 6 5 -5 97.09 8.20 6 -5 5 81.69 8.20 6 5 5 106.49 9.30 6 5 5 114.49 10.10 6 5 5 104.79 8.50 6 5 5 117.99 9.80 6 -5 -5 105.49 11.10 7 -5 5 258.37 18.60 7 5 -5 218.38 18.00 7 -5 5 246.48 17.60 7 -5 -5 241.18 20.40 7 5 5 262.17 20.00 7 5 5 269.47 19.30 8 -5 5 69.39 6.80 8 -5 5 69.59 8.00 8 5 -5 81.99 8.00 8 5 5 104.29 10.00 8 5 5 80.19 8.70 8 -5 -5 110.19 10.90 -8 5 -5 99.39 10.50 9 -5 5 158.48 12.50 9 -5 5 164.78 13.90 9 5 -5 184.18 14.10 -9 5 -5 111.89 12.20 9 -5 -5 127.69 11.90 9 5 5 104.59 10.10 9 5 5 127.29 11.60 10 5 -5 31.70 5.50 10 -5 5 30.20 6.00 -10 5 -5 25.40 6.20 10 5 5 20.10 4.60 10 -5 -5 21.80 4.60 10 -5 -5 29.50 5.90 10 5 5 25.80 5.60 11 -5 5 58.29 8.20 11 -5 -5 45.50 5.80 11 5 5 44.10 6.00 0 6 -5 416.86 29.10 1 6 -5 945.01 62.79 -1 6 5 939.01 62.59 -1 6 5 899.71 63.49 1 6 5 939.71 57.09 -1 -6 5 715.93 56.49 -1 6 -5 845.02 57.29 1 6 5 813.32 57.99 1 6 5 892.71 56.69 2 6 -5 1130.29 76.49 -2 6 5 1125.29 76.99 2 -6 5 1137.89 77.19 -2 6 5 1146.09 77.99 2 6 -5 1202.38 77.59 2 6 5 954.50 60.79 2 6 5 885.81 61.69 -2 6 -5 833.22 60.99 2 6 5 910.41 60.29 -3 6 5 1207.98 85.49 3 6 -5 1331.07 85.19 -3 6 5 1297.07 86.29 3 6 -5 1261.67 85.99 3 6 5 1351.16 85.69 -3 6 -5 1216.68 85.09 3 6 5 1179.58 84.89 3 6 5 1299.77 84.09 3 6 5 1233.48 84.79 4 6 -5 262.47 19.20 4 -6 5 261.07 18.60 -4 6 5 255.17 19.00 4 6 -5 252.37 18.20 4 6 5 221.48 16.90 4 6 5 227.18 17.10 4 6 5 214.18 16.30 -4 6 -5 216.88 16.90 -5 6 5 869.91 60.29 -5 6 5 829.52 61.99 5 6 -5 898.91 61.59 5 6 -5 933.41 62.39 5 -6 5 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120.39 12.70 9 -7 -5 132.49 12.70 9 7 5 140.89 12.40 9 7 5 120.09 10.60 10 -7 5 85.29 10.10 10 7 5 84.69 7.90 0 8 5 342.67 22.60 0 8 -5 278.27 24.00 1 8 -5 463.05 34.30 -1 8 5 519.95 35.40 -1 8 -5 470.65 31.40 1 8 5 473.05 32.30 1 8 5 391.26 31.00 2 8 -5 1061.19 69.29 -2 8 5 1057.99 68.99 -2 8 5 939.91 69.79 2 8 5 1010.10 73.69 2 8 5 1157.28 72.89 -2 8 -5 1058.89 73.19 3 8 -5 325.27 22.50 -3 8 5 313.47 22.90 3 -8 5 308.57 22.10 -3 8 5 284.07 21.90 3 8 5 290.47 21.30 3 8 5 270.27 20.20 -3 8 -5 276.57 21.00 4 -8 5 951.10 65.49 -4 8 5 962.90 63.99 4 8 -5 932.91 65.89 -4 8 5 1007.60 66.39 4 8 5 780.42 54.59 -4 8 -5 728.93 55.09 4 8 5 884.61 55.69 -5 8 5 70.79 5.50 -5 8 5 89.09 8.80 5 -8 5 77.59 7.10 5 8 -5 83.79 8.10 5 8 5 125.49 10.00 -5 8 -5 99.49 10.00 5 8 5 93.59 8.90 5 -8 -5 95.59 10.40 6 -8 5 321.87 22.80 6 8 -5 319.07 23.80 6 8 5 278.27 21.60 6 8 5 311.17 22.50 6 -8 -5 285.17 22.80 -6 8 -5 318.87 23.00 7 -8 5 267.97 19.20 7 -8 -5 229.88 18.30 -7 8 -5 231.38 18.20 7 8 5 227.18 17.60 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373.76 27.10 7 -1 -8 382.06 29.40 7 1 8 396.86 29.50 7 1 8 376.76 28.00 7 1 8 416.06 28.10 -7 1 -8 406.66 28.80 8 -1 8 161.98 13.50 8 -1 8 156.78 12.30 8 1 -8 168.98 14.20 8 -1 8 167.88 14.00 8 1 8 82.69 8.10 8 1 8 107.89 9.50 8 -1 -8 102.39 10.70 -8 1 -8 108.59 12.00 8 1 8 100.69 9.50 9 -1 8 98.39 11.30 9 -1 8 99.99 8.50 9 -1 8 101.29 9.60 9 1 -8 121.19 10.60 9 1 8 99.49 10.10 9 -1 -8 114.19 10.60 9 1 8 100.39 9.70 10 -1 8 26.50 5.70 10 -1 -8 20.30 5.20 10 1 8 16.50 4.00 11 -1 8 20.70 4.20 11 1 8 25.60 6.60 0 2 8 2542.25 152.28 0 2 8 2020.20 153.98 0 -2 -8 2377.86 151.98 0 2 -8 2137.59 152.58 0 -2 8 2369.36 152.28 -1 -2 -8 807.22 51.59 -1 2 8 822.72 52.09 1 -2 8 761.52 52.09 1 2 -8 736.03 52.49 -1 2 8 741.43 53.79 1 2 8 824.62 52.29 -1 -2 8 733.23 52.19 1 -2 -8 804.82 52.19 -1 2 -8 796.22 52.69 1 2 8 730.23 54.29 -2 2 8 988.60 66.39 -2 2 8 1042.40 68.19 2 2 -8 1035.10 67.09 2 -2 8 902.51 66.49 2 2 8 1230.38 78.29 -2 2 -8 1153.08 78.49 2 2 8 1175.98 78.09 2 2 8 1108.29 80.09 3 2 -8 1949.51 128.19 -3 2 8 1878.51 128.79 -3 2 -8 1817.12 120.99 3 2 8 1751.02 122.69 3 2 8 1853.31 121.69 -4 2 8 502.15 37.10 4 2 -8 526.55 37.20 4 2 -8 516.65 37.40 4 -2 8 588.84 36.60 4 2 8 645.84 38.20 -4 2 -8 591.94 39.00 -4 -2 8 531.65 39.00 4 2 8 523.35 40.60 4 2 8 506.35 43.00 5 2 -8 179.08 13.80 5 -2 8 185.08 12.80 5 2 -8 164.18 13.20 5 -2 8 146.59 13.90 5 -2 8 157.08 12.40 -5 2 -8 204.68 16.30 5 2 8 194.08 15.10 5 2 8 225.78 16.10 5 2 8 232.08 17.90 5 -2 -8 194.18 17.10 5 2 8 220.28 16.00 6 2 -8 485.55 34.10 6 -2 8 458.15 32.90 6 -2 8 485.55 33.10 6 -2 8 471.85 33.20 6 2 8 413.16 29.10 6 -2 -8 407.76 30.70 6 2 8 433.26 30.70 6 2 8 394.56 29.00 -6 2 -8 426.16 29.60 6 2 8 381.66 28.10 7 -2 8 258.07 19.50 7 -2 8 247.88 19.40 7 -2 8 261.47 19.00 7 2 -8 286.77 20.50 7 -2 -8 316.47 24.10 7 2 8 300.67 22.40 7 2 8 310.97 22.30 7 2 8 280.77 21.20 -7 2 -8 310.67 23.20 8 -2 8 291.27 23.30 8 -2 8 318.07 23.70 8 -2 8 321.17 22.80 8 2 -8 358.46 24.40 8 2 8 260.57 20.00 8 -2 -8 294.37 20.80 -8 2 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3 8 309.67 21.70 5 3 -8 1152.38 78.29 5 -3 8 1160.08 77.59 5 -3 8 1139.19 78.19 5 3 -8 1152.18 78.29 5 3 8 898.31 62.69 5 3 8 897.61 61.89 5 3 8 965.60 62.69 5 3 8 966.70 64.29 -5 3 -8 867.21 62.89 6 3 -8 284.57 20.30 6 -3 8 279.27 19.60 6 -3 8 263.37 19.30 6 -3 8 245.98 19.50 -6 3 -8 215.28 16.60 6 3 8 220.08 16.00 6 -3 -8 193.48 17.40 6 3 8 220.78 17.30 6 3 8 194.88 15.70 6 3 8 191.08 14.80 7 3 -8 24.50 5.60 7 -3 8 35.10 4.50 7 -3 8 30.60 5.40 -7 3 -8 32.40 5.70 7 3 8 39.40 5.70 7 3 8 32.60 4.10 7 -3 -8 37.30 7.80 7 3 8 28.50 5.20 8 -3 8 375.06 25.30 8 -3 8 350.36 25.70 8 3 -8 343.77 26.30 8 3 8 394.26 28.30 -8 3 -8 384.76 29.10 8 -3 -8 398.76 29.80 8 3 8 375.66 27.00 8 3 8 398.56 28.30 9 -3 8 286.57 20.20 9 -3 8 262.07 20.80 9 3 -8 305.67 21.70 9 -3 -8 337.47 26.00 9 3 8 354.56 25.10 9 -3 -8 352.36 24.60 9 3 8 349.27 25.20 -9 3 -8 302.97 26.40 10 -3 8 20.50 6.20 10 3 8 10.10 3.80 0 -4 8 103.99 8.20 0 4 8 91.39 8.30 0 4 8 106.89 8.20 0 4 -8 127.99 8.90 1 4 -8 1526.55 102.79 -1 4 8 1647.44 102.29 -1 4 8 1461.15 103.99 1 -4 8 1573.24 102.19 -1 4 8 1648.83 102.29 1 4 -8 1327.07 102.09 1 4 8 1246.18 93.69 -1 4 -8 1382.86 92.19 -1 -4 8 1292.77 91.49 1 4 8 1502.05 91.99 1 4 8 1433.96 91.79 2 4 -8 331.37 22.00 -2 4 8 292.77 21.10 2 -4 8 283.07 21.50 -2 4 8 301.47 21.20 2 4 -8 308.37 21.30 2 4 8 172.88 13.20 2 4 8 157.08 13.60 -2 4 -8 200.28 14.10 2 4 8 211.88 15.90 3 4 -8 1746.93 119.99 3 4 -8 1797.62 120.49 3 -4 8 1932.21 119.89 -3 4 8 1696.93 120.89 3 4 8 1759.12 129.09 3 4 8 2013.70 125.19 -3 4 -8 1849.52 125.89 4 -4 8 122.79 10.30 -4 4 8 134.89 11.20 4 4 -8 142.99 11.50 4 4 -8 139.19 10.80 4 4 8 105.69 8.50 -4 4 -8 123.19 10.10 4 4 8 104.29 9.30 5 4 -8 82.99 8.50 5 -4 8 80.29 7.40 5 4 -8 92.49 8.00 5 4 8 56.69 5.30 5 4 8 48.70 6.30 5 4 8 71.89 6.80 -5 4 -8 66.19 7.30 6 -4 8 212.58 15.90 6 4 -8 240.78 16.60 6 -4 8 191.88 16.10 -6 4 -8 245.88 18.80 6 4 8 267.47 18.50 6 -4 -8 222.88 19.80 6 4 8 279.87 19.70 6 4 8 204.18 17.90 6 4 8 225.38 17.10 7 -4 8 702.13 46.90 7 4 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5 -8 232.58 17.80 4 -5 8 229.18 16.70 4 5 -8 232.98 16.90 4 5 8 128.19 11.40 -4 5 -8 154.98 12.30 4 5 8 154.68 13.00 4 5 8 133.09 10.70 5 5 -8 443.36 31.30 5 -5 8 483.45 31.10 5 5 -8 410.66 31.90 -5 5 -8 423.76 33.10 5 5 8 453.65 34.00 5 5 8 497.45 32.10 5 5 8 480.05 32.90 6 -5 8 334.67 24.00 6 5 -8 337.27 25.20 6 5 -8 340.37 24.40 6 5 8 293.17 20.80 6 5 8 273.97 21.60 6 5 8 319.87 22.20 -6 5 -8 290.17 22.30 7 -5 8 65.59 9.40 7 -5 8 79.79 8.40 7 5 8 69.59 6.60 7 -5 -8 61.69 10.00 7 5 8 84.79 8.30 -7 5 -8 76.99 8.90 8 5 -8 183.98 14.70 8 -5 8 188.68 13.50 8 -5 8 160.28 14.30 8 5 8 147.19 13.20 8 -5 -8 162.18 14.80 -8 5 -8 165.98 14.30 8 5 8 140.09 12.60 9 -5 8 149.19 10.70 9 -5 8 121.09 11.90 9 -5 -8 99.69 12.10 -9 5 -8 114.49 13.00 9 5 8 111.39 9.90 10 -5 -8 21.90 5.10 0 6 8 1594.04 110.59 0 6 8 1583.64 112.49 0 -6 8 1677.83 110.29 0 6 8 1738.73 110.89 0 6 -8 1675.13 111.09 1 6 -8 452.95 30.70 1 -6 8 416.16 29.80 -1 6 8 472.85 32.20 -1 6 8 403.96 30.10 -1 -6 8 532.65 38.20 1 6 8 538.65 38.50 1 6 8 560.34 39.00 1 6 8 599.14 40.90 -1 6 -8 592.74 39.30 -2 6 8 231.38 16.70 2 6 -8 217.98 17.30 2 -6 8 239.78 16.50 -2 6 8 233.48 18.40 2 6 8 224.88 18.90 -2 6 -8 240.38 17.90 2 6 8 241.38 17.60 -3 6 8 523.55 38.40 3 -6 8 565.64 37.00 3 6 -8 528.55 37.80 3 6 8 485.95 38.10 -3 6 -8 525.25 37.20 3 6 8 554.94 37.00 3 6 8 545.15 36.30 -4 6 8 831.32 58.09 4 -6 8 831.62 56.99 4 6 -8 862.91 58.09 -4 6 -8 737.83 52.29 4 6 8 774.32 53.39 4 6 8 746.13 51.99 4 6 8 761.72 51.29 5 6 -8 482.15 34.60 -5 6 8 498.05 34.50 5 -6 8 469.15 33.40 -5 6 -8 337.27 25.00 5 6 8 321.27 24.40 5 6 8 351.96 23.70 6 6 -8 369.76 27.70 6 -6 8 379.86 26.40 6 6 8 407.76 27.70 6 6 8 363.96 25.60 6 6 8 342.17 26.50 -6 6 -8 349.87 27.10 7 -6 8 100.89 8.40 7 -6 -8 49.70 9.20 7 6 8 62.59 6.00 -7 6 -8 54.89 8.30 7 6 8 68.69 7.30 8 -6 8 175.08 13.20 8 6 8 133.69 11.50 8 -6 -8 134.39 14.00 -8 6 -8 137.29 13.40 9 -6 8 41.30 4.90 9 6 8 28.10 5.60 9 -6 -8 42.30 8.20 10 -6 -8 53.29 6.30 0 -7 8 229.58 15.80 0 7 -8 212.58 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9 6.20 3.40 5 5 9 1.60 2.30 -5 5 -9 3.60 3.20 5 5 9 6.00 1.90 6 5 -9 279.37 20.80 6 -5 9 283.87 20.30 -6 5 -9 353.26 24.10 6 -5 -9 272.77 25.00 6 5 9 318.47 23.40 6 5 9 325.87 22.50 7 -5 9 353.96 24.60 7 5 -9 337.37 25.70 7 -5 -9 253.17 22.90 -7 5 -9 304.27 22.00 7 5 9 279.57 21.10 7 5 9 283.47 19.90 8 -5 9 114.69 9.50 8 -5 -9 98.59 11.90 8 5 9 115.09 8.70 8 5 9 104.49 9.70 -8 5 -9 93.39 11.80 9 -5 9 8.60 2.60 9 -5 -9 0.50 10.70 9 5 9 1.60 3.20 9 -5 -9 -2.80 3.60 10 5 9 25.20 6.60 0 6 -9 278.17 19.00 0 6 9 235.88 20.50 -1 6 9 795.62 50.69 1 6 -9 727.13 50.99 -1 6 9 697.23 52.39 1 -6 9 755.12 50.29 -1 6 -9 818.62 57.99 1 6 9 799.92 59.69 -1 -6 9 832.42 57.09 1 6 9 948.71 57.99 1 6 9 843.82 57.49 -2 6 9 756.52 48.50 -2 6 9 594.34 46.10 2 -6 9 656.13 46.00 2 6 -9 713.53 47.00 2 6 9 817.92 59.99 2 6 9 795.12 59.49 2 6 9 948.71 62.29 -2 6 -9 966.00 60.49 3 -6 9 144.49 10.70 3 6 -9 144.59 11.80 -3 6 9 135.29 12.60 -3 6 -9 148.39 12.10 3 6 9 137.69 10.90 3 6 9 138.19 13.20 3 6 9 145.29 11.80 -4 6 9 479.85 35.40 4 -6 9 521.95 34.10 4 6 -9 480.35 35.10 4 6 9 411.76 28.50 4 6 9 385.36 29.90 4 6 9 403.86 27.80 -4 6 -9 388.86 28.80 5 6 -9 2.70 3.10 5 -6 9 14.40 3.00 5 6 9 15.70 3.70 5 6 9 15.10 3.30 -5 6 -9 24.20 4.60 5 6 9 21.50 6.00 6 -6 9 207.98 18.90 6 6 -9 254.37 18.60 6 6 9 296.47 23.20 -6 6 -9 324.47 24.00 6 6 9 345.47 24.70 6 6 9 302.17 25.20 7 -6 9 40.40 4.80 -7 6 -9 23.60 5.70 7 -6 -9 19.30 5.90 7 6 9 24.60 5.30 8 -6 9 171.58 12.90 8 -6 -9 148.09 15.60 -8 6 -9 179.48 14.80 8 6 9 157.18 13.20 9 -6 9 5.50 2.50 9 6 9 3.50 3.60 0 -7 9 1394.66 95.09 0 7 9 1440.96 97.79 0 7 -9 1449.06 96.09 0 7 9 1407.56 95.79 1 7 -9 555.84 38.70 1 -7 9 538.45 37.70 -1 7 9 539.85 40.10 -1 7 9 582.84 38.40 1 7 9 513.45 34.00 1 7 9 460.15 33.40 1 7 9 468.15 35.70 -1 7 -9 510.55 34.20 -1 -7 9 463.35 32.90 -2 7 9 21.80 5.30 2 7 -9 25.50 4.60 2 7 9 11.40 2.50 -2 7 -9 10.20 3.40 3 -7 9 35.20 3.90 -3 7 9 32.10 6.30 3 7 -9 37.00 5.30 3 7 9 31.80 6.40 -3 7 -9 25.00 5.20 3 7 9 31.60 4.20 3 7 9 27.60 5.00 4 -7 9 476.55 36.10 -4 7 9 562.64 38.00 4 7 -9 546.65 37.50 4 7 9 490.65 32.70 -4 7 -9 465.95 31.30 4 7 9 381.96 30.70 4 7 9 395.86 30.10 5 7 -9 393.26 28.80 5 7 9 234.78 16.70 5 7 9 232.08 17.60 -5 7 -9 215.88 17.90 5 7 9 226.08 18.70 6 7 -9 207.48 16.80 6 -7 9 213.38 15.50 -6 7 -9 196.08 15.90 6 7 9 173.68 15.00 6 7 9 189.68 14.20 6 7 9 210.28 17.00 7 -7 9 68.59 6.20 7 7 9 47.10 6.10 7 -7 -9 34.90 7.30 8 -7 9 171.98 12.70 -8 7 -9 132.59 12.60 8 7 9 110.79 10.20 8 -7 -9 115.59 13.60 9 -7 9 8.70 2.00 9 7 9 10.80 5.10 0 -8 9 284.47 20.70 0 8 9 295.07 21.80 0 8 9 298.17 23.50 0 8 -9 315.57 22.10 1 -8 9 526.75 38.00 1 8 -9 589.64 39.20 -1 8 9 591.44 40.70 -1 8 9 527.45 38.60 -1 -8 9 637.84 48.60 1 8 9 741.93 49.80 -1 8 -9 752.52 49.99 1 8 9 749.33 51.59 -2 8 9 1070.19 70.99 2 8 -9 1012.80 71.39 2 -8 9 1049.89 70.49 -2 8 9 1056.79 72.69 2 8 9 970.00 68.29 -2 8 -9 992.40 66.89 2 8 9 963.30 66.69 3 8 -9 592.74 41.10 3 -8 9 603.54 40.10 -3 8 9 563.04 41.90 3 8 9 459.05 31.60 3 8 9 416.76 32.70 -3 8 -9 452.85 31.60 3 8 9 430.16 30.70 4 -8 9 327.47 23.10 4 8 -9 333.47 24.30 -4 8 9 326.37 24.90 4 8 9 291.17 21.60 -4 8 -9 279.17 20.40 4 8 9 252.77 19.30 4 8 9 250.77 20.10 5 -8 9 433.96 30.80 5 8 -9 459.45 32.20 5 8 9 302.27 25.10 -5 8 -9 346.37 25.50 5 8 9 392.06 26.80 6 -8 9 278.47 19.80 6 8 -9 279.47 21.20 -6 8 -9 250.67 18.90 6 -8 -9 216.48 20.00 6 8 9 243.98 18.30 7 -8 9 38.60 4.30 7 -8 -9 22.60 6.90 7 8 9 28.80 5.30 8 -8 9 107.69 8.40 8 8 9 114.19 10.20 9 -8 9 45.60 4.50 9 8 9 61.09 7.60 0 9 9 234.38 16.20 0 9 9 184.58 17.10 0 9 -9 189.08 15.90 0 -9 9 210.98 14.90 -1 9 9 1048.10 73.09 -1 9 9 1079.49 71.49 1 -9 9 1048.10 70.59 1 9 -9 1023.80 71.59 1 9 9 1036.00 69.69 1 9 9 987.00 71.19 -1 9 -9 1037.40 69.79 -2 9 9 169.98 13.60 -2 9 9 175.08 15.00 2 -9 9 164.88 12.70 2 9 -9 178.98 14.00 2 9 9 150.28 13.30 -2 9 -9 167.38 13.70 2 9 9 168.58 14.60 3 -9 9 1019.70 70.09 -3 9 9 1054.09 72.09 3 9 -9 1050.59 71.09 3 9 9 986.10 73.69 3 9 9 1113.09 75.29 -3 9 -9 1147.59 73.99 -4 9 9 60.59 8.30 4 -9 9 60.49 5.70 4 9 -9 56.69 6.90 4 9 9 54.69 7.90 -4 9 -9 55.69 7.30 4 9 9 64.39 7.40 5 9 -9 275.07 21.70 5 -9 9 303.97 20.60 -5 9 -9 345.97 25.40 5 9 9 316.87 26.00 5 9 9 372.56 25.40 6 -9 9 95.59 7.30 6 9 -9 71.29 8.70 6 9 9 96.69 8.90 -6 9 -9 105.59 9.90 6 -9 -9 69.99 11.60 7 -9 9 210.68 15.10 -7 9 -9 238.68 17.80 7 9 9 182.98 16.50 7 -9 -9 269.67 23.80 8 -9 9 92.29 7.50 8 9 9 103.09 12.10 0 10 9 159.88 13.50 0 -10 9 151.68 12.30 0 10 -9 178.08 13.60 0 10 9 173.88 14.80 1 10 -9 735.53 49.60 1 -10 9 713.23 48.50 -1 10 9 743.13 50.99 -1 10 9 667.53 49.30 1 10 9 725.83 50.09 1 10 9 678.13 48.60 -1 10 -9 692.83 48.60 -2 10 9 83.69 11.10 -2 10 9 94.19 10.10 2 10 -9 103.19 9.20 2 -10 9 83.89 9.90 -2 10 -9 134.09 11.60 2 10 9 112.79 12.10 2 10 9 143.19 12.60 3 10 -9 198.98 15.80 3 -10 9 205.38 14.80 -3 10 9 200.18 17.00 3 10 9 216.08 17.70 3 10 9 226.88 16.70 -3 10 -9 186.28 16.50 4 -10 9 176.88 12.00 -4 10 9 140.59 14.30 4 10 -9 152.38 12.90 -4 10 9 156.08 10.70 4 10 9 152.58 13.00 -4 10 -9 168.18 13.40 4 10 9 152.58 14.10 5 10 -9 311.37 23.00 5 -10 9 307.47 21.70 5 10 9 330.67 23.50 5 10 9 263.37 21.90 -5 10 -9 302.87 22.40 6 -10 9 44.80 4.60 -6 10 -9 51.69 7.50 6 10 9 56.59 6.60 7 -10 9 18.90 3.00 7 10 9 15.30 4.00 0 11 9 29.10 5.90 0 -11 9 45.60 5.10 1 -11 9 327.57 21.80 -1 11 9 321.67 22.90 -1 11 9 281.77 25.10 1 11 -9 301.07 24.30 1 11 9 322.77 24.20 -1 11 -9 387.16 27.00 1 11 9 287.77 27.00 -2 11 9 90.89 10.50 2 11 -9 104.09 9.70 2 -11 9 113.39 8.50 -2 11 -9 66.99 7.60 2 11 9 71.99 7.70 2 11 9 59.39 8.00 3 11 -9 252.17 19.40 3 -11 9 265.77 18.30 -3 11 9 265.97 20.80 -3 11 9 241.28 17.20 3 11 9 214.68 17.10 -3 11 -9 192.08 16.10 3 11 9 204.48 16.10 -4 11 9 81.99 6.50 4 11 -9 92.49 9.10 4 -11 9 92.99 7.40 -4 11 9 97.59 11.60 -4 11 -9 67.89 7.80 4 11 9 56.69 7.00 5 11 -9 48.40 7.40 5 -11 9 56.39 5.10 -5 11 -9 38.90 6.90 5 11 9 42.80 5.70 5 11 9 49.90 13.50 6 -11 9 23.60 3.30 6 11 9 15.00 3.30 7 -11 9 106.69 8.10 7 11 9 95.79 8.90 0 -12 9 138.39 10.20 0 12 9 112.79 12.00 0 12 -9 117.49 11.20 0 12 9 145.69 11.30 -1 12 9 39.80 7.30 1 -12 9 34.60 4.40 1 12 -9 32.70 6.10 -1 12 9 38.50 5.80 1 12 9 33.20 5.60 -1 12 -9 32.70 5.80 1 12 9 32.90 6.60 -2 12 9 477.35 32.70 -2 12 9 423.36 29.20 2 -12 9 427.96 30.00 2 12 -9 420.56 31.10 -2 12 -9 358.86 26.30 2 12 9 327.27 26.10 2 12 9 405.06 27.80 3 -12 9 19.60 3.30 -3 12 9 18.80 5.20 -3 12 9 15.30 2.10 3 12 9 15.90 4.40 3 12 9 11.00 3.20 -3 12 -9 11.80 3.70 4 -12 9 75.19 6.40 4 12 -9 75.79 8.50 4 12 9 100.59 12.40 4 12 9 73.79 8.00 -4 12 -9 83.09 8.80 5 -12 9 26.30 3.50 5 12 9 27.50 5.00 6 -12 9 52.09 4.80 6 12 9 63.09 6.80 0 13 9 464.95 34.00 0 13 -9 486.05 34.20 0 13 9 464.25 32.40 0 13 9 526.95 35.90 1 13 -9 33.50 6.80 1 -13 9 52.79 5.20 -1 13 9 61.19 8.60 -1 13 9 44.10 3.70 1 13 9 51.09 3.80 1 13 9 52.49 8.10 1 13 9 39.00 6.00 -1 13 -9 52.79 6.70 2 -13 9 43.70 4.60 2 13 -9 39.20 7.20 -2 13 9 36.70 8.20 -2 13 -9 39.40 7.00 2 13 9 51.79 7.80 2 13 9 60.79 6.50 3 -13 9 0.70 1.70 3 13 9 4.20 2.90 4 -13 9 82.19 6.90 4 13 9 84.19 8.00 5 -13 9 36.20 4.20 5 13 9 22.00 4.80 0 14 9 0.40 2.70 1 14 9 34.70 5.20 2 -14 9 192.78 14.00 2 14 9 137.09 11.10 3 -14 9 36.30 4.60 3 14 9 30.10 4.90 0 0 10 3.50 1.70 0 0 -10 0.60 1.80 -1 0 -10 1495.85 104.79 -1 0 10 1618.64 104.79 1 0 10 1568.14 104.79 1 0 -10 1594.34 104.99 -2 0 10 9.60 3.30 -2 0 10 13.20 2.80 2 0 10 12.70 2.80 -2 0 -10 13.30 2.90 2 0 -10 18.70 3.30 -3 0 -10 319.47 22.50 3 0 10 303.27 22.30 -3 0 10 326.57 24.40 3 0 -10 330.87 23.10 -4 0 -10 99.49 9.30 4 0 10 117.49 8.80 5 0 -10 874.01 58.39 5 0 10 814.22 56.59 5 0 10 841.32 59.69 5 0 10 813.52 56.99 6 0 10 9.60 3.00 6 0 10 1.00 3.70 6 0 -10 1.90 3.50 6 0 10 8.80 2.10 7 0 10 5.90 5.50 7 0 10 6.10 2.30 7 0 -10 -0.10 3.20 8 0 10 4.40 2.10 8 0 -10 4.30 3.50 8 0 10 2.10 2.90 9 0 10 104.59 8.20 9 0 -10 110.59 10.30 9 0 10 79.59 9.10 10 0 10 2.60 4.10 0 -1 10 925.01 60.59 0 1 -10 891.71 60.89 0 -1 -10 923.01 60.39 0 1 10 861.61 61.19 -1 1 10 609.04 38.70 -1 1 10 551.24 41.00 1 1 -10 564.24 39.10 -1 -1 -10 555.34 38.50 1 -1 10 566.44 38.80 -1 -1 10 481.65 33.60 1 -1 -10 502.85 33.60 -1 1 -10 481.55 33.90 1 1 10 504.85 33.70 -2 1 10 201.48 13.20 -2 1 10 146.09 14.60 2 -1 10 190.68 13.10 2 1 -10 169.18 13.40 -2 1 -10 155.78 12.30 2 -1 -10 144.19 12.00 2 1 10 189.28 12.10 3 -1 10 681.43 48.80 -3 1 10 701.13 50.49 3 1 -10 778.02 49.50 3 1 10 692.03 50.79 3 1 10 698.53 48.10 -3 -1 10 660.63 49.90 -3 1 -10 787.62 48.40 4 -1 10 253.47 18.40 4 1 -10 244.88 19.70 4 1 -10 273.57 19.20 -4 1 10 254.97 19.80 -4 -1 10 222.08 20.90 4 1 10 236.78 17.40 4 1 10 247.28 20.40 -4 1 -10 255.87 18.00 4 1 10 255.37 17.80 5 -1 10 144.89 10.80 5 1 -10 130.09 12.40 5 1 10 107.29 8.60 5 1 10 95.69 7.90 -5 1 -10 87.99 9.20 5 -1 -10 90.19 9.90 5 1 10 95.39 10.80 6 -1 10 244.98 17.90 6 1 -10 245.18 19.30 6 1 10 205.18 14.70 6 1 10 178.88 17.20 6 1 10 192.38 14.20 6 -1 -10 187.98 16.30 7 1 -10 523.25 35.50 7 -1 10 470.45 34.00 7 -1 10 478.55 37.40 7 1 10 393.56 27.10 7 1 10 326.97 29.60 7 1 10 404.26 30.40 7 -1 -10 425.86 29.30 8 -1 10 78.79 7.20 8 -1 10 75.79 8.20 8 1 -10 82.69 9.00 8 1 10 71.99 6.70 8 1 10 71.69 7.60 8 -1 -10 77.19 9.10 9 1 -10 29.70 5.90 9 -1 10 36.00 4.70 9 -1 -10 16.10 4.70 9 1 10 11.60 2.60 9 1 10 7.10 3.50 10 1 10 29.40 6.60 0 2 -10 389.76 27.80 0 2 10 358.36 29.50 0 -2 10 439.76 27.40 -1 2 10 183.28 13.90 1 -2 10 187.58 13.20 1 2 -10 169.88 13.70 1 2 10 178.28 16.80 1 2 10 221.28 14.50 -1 2 -10 204.78 14.90 -1 -2 10 199.88 14.60 2 -2 10 1196.08 85.69 -2 2 10 1359.56 85.59 2 2 10 1252.67 87.19 -2 2 -10 1376.66 87.49 2 2 10 1276.37 89.79 3 2 -10 263.77 20.30 3 2 -10 280.77 19.20 -3 2 10 233.38 20.80 3 -2 10 249.28 18.40 -3 2 -10 318.17 21.80 3 2 10 280.47 23.90 3 2 10 321.77 21.70 3 2 10 299.57 21.40 4 -2 10 378.06 26.80 -4 2 10 350.76 27.80 4 2 -10 399.76 27.90 4 2 -10 401.36 27.60 -4 2 -10 446.36 30.30 4 2 10 414.36 29.60 4 2 10 404.36 32.30 4 2 10 454.25 30.10 5 2 -10 433.76 29.80 5 -2 10 384.36 28.50 5 2 10 384.66 28.50 5 -2 -10 328.37 27.30 5 2 10 378.46 25.90 -5 2 -10 380.96 26.40 5 2 10 352.26 25.40 6 2 -10 711.93 48.80 6 -2 10 681.83 47.70 6 2 10 734.53 49.20 6 2 10 642.14 46.40 6 2 10 611.14 46.00 -6 2 -10 725.83 47.30 6 -2 -10 675.73 48.20 7 2 -10 26.90 6.10 7 -2 10 18.60 3.90 7 -2 10 15.20 6.40 -7 2 -10 30.30 11.30 7 -2 -10 22.60 5.00 7 2 10 22.50 6.00 7 2 10 21.70 3.70 8 2 -10 339.67 24.30 8 -2 10 308.67 23.00 8 -2 -10 280.27 20.90 8 2 10 239.18 19.00 8 2 10 261.57 18.60 9 -2 10 44.60 5.20 9 2 10 15.00 3.50 9 -2 -10 14.60 4.80 9 2 10 10.80 2.90 10 2 10 8.00 3.80 0 3 10 1827.72 123.59 0 3 10 1852.91 126.09 0 3 -10 1877.01 124.09 -1 3 10 35.10 4.20 -1 3 10 45.40 6.90 1 3 -10 42.40 6.90 1 -3 10 34.60 4.20 1 3 10 51.69 6.10 -1 3 -10 65.59 6.00 1 3 10 55.29 5.30 1 3 10 70.69 8.20 -1 -3 10 55.29 5.80 2 -3 10 19.30 3.30 -2 3 10 14.20 3.90 -2 3 -10 3.80 2.90 2 3 10 7.50 2.60 2 3 10 1.90 2.70 2 3 10 5.80 1.70 3 3 -10 65.89 7.00 -3 3 10 55.59 7.60 3 3 -10 59.79 7.00 3 -3 10 72.19 6.00 3 3 10 83.79 10.40 3 3 10 118.39 8.80 -3 3 -10 95.89 8.70 3 3 10 101.99 8.00 -4 3 10 1779.62 123.09 4 3 -10 1949.60 122.69 4 -3 10 1769.72 121.99 4 3 -10 1790.62 122.69 4 3 10 1703.63 112.89 4 3 10 1720.93 115.39 4 3 10 1585.64 112.49 -4 3 -10 1723.63 113.19 5 -3 10 108.69 9.80 5 3 -10 120.69 11.00 5 3 -10 134.29 11.00 5 3 10 134.39 12.50 -5 3 -10 129.49 10.70 5 3 10 107.39 9.90 5 3 10 105.19 9.10 6 3 -10 579.54 38.70 6 -3 10 516.75 37.90 6 3 10 614.84 42.30 6 3 10 556.64 39.40 6 -3 -10 554.64 41.70 6 3 10 553.54 39.90 -6 3 -10 605.04 40.70 7 -3 10 15.50 3.10 7 3 -10 6.80 4.20 7 3 10 0.60 1.70 -7 3 -10 2.70 5.20 7 -3 -10 1.90 4.20 7 3 10 6.60 2.80 8 -3 10 170.08 12.60 8 3 -10 152.98 13.90 8 3 10 127.89 10.30 8 3 10 122.69 11.10 8 -3 -10 158.88 13.30 9 -3 10 7.90 2.40 9 -3 -10 5.80 6.40 9 3 10 11.70 3.50 10 3 10 91.19 9.00 0 4 10 7.50 3.00 0 4 -10 7.00 2.20 0 4 10 9.50 2.10 0 -4 10 10.20 2.10 0 4 10 11.60 2.80 -1 4 10 411.26 28.10 1 -4 10 412.96 28.00 -1 4 10 378.56 30.20 -1 4 10 424.06 28.10 1 4 -10 402.26 28.70 -1 4 -10 316.97 22.20 1 4 10 342.17 22.10 -1 -4 10 299.27 21.50 1 4 10 273.37 24.00 1 4 10 310.27 21.70 -2 4 10 1140.59 82.19 2 -4 10 1245.48 80.29 2 4 -10 1232.58 81.09 -2 4 10 1164.28 80.29 2 4 10 1139.49 82.79 2 4 10 1255.47 80.49 -2 4 -10 1246.58 80.79 2 4 10 1139.29 80.19 -3 4 10 365.76 25.90 3 -4 10 320.87 23.80 3 4 -10 334.77 24.80 -3 4 -10 298.57 18.90 3 4 10 224.28 18.10 3 4 10 231.38 17.70 -4 4 10 425.16 31.20 4 4 -10 412.66 30.80 4 -4 10 439.36 29.80 4 4 -10 433.26 30.30 4 4 10 451.35 32.80 -4 4 -10 482.55 33.80 4 4 10 495.65 35.70 4 4 10 481.25 33.40 5 -4 10 71.59 6.70 5 4 -10 78.59 7.80 5 4 -10 69.59 8.10 5 4 10 50.39 6.20 5 4 10 62.89 8.30 -5 4 -10 59.59 7.30 5 4 10 51.19 5.30 6 4 -10 423.66 29.40 6 -4 10 395.46 28.80 6 4 10 258.27 20.40 6 4 10 268.37 19.70 -6 4 -10 288.77 21.20 6 4 10 310.07 22.70 6 -4 -10 260.47 22.30 7 4 10 20.70 5.10 7 4 10 21.60 3.60 -7 4 -10 15.40 5.50 7 -4 -10 9.00 5.20 8 -4 10 77.69 7.20 8 4 10 61.09 7.10 -8 4 -10 63.09 12.20 8 4 10 67.09 6.10 8 -4 -10 55.29 9.90 9 -4 10 20.70 4.10 9 4 10 12.60 3.80 0 5 10 259.47 17.90 0 -5 10 262.57 17.70 0 5 10 218.18 19.90 0 5 -10 232.98 18.30 0 5 10 269.37 18.10 -1 5 10 360.36 24.40 -1 5 10 324.27 24.40 1 5 -10 354.66 25.10 1 -5 10 342.87 24.20 -1 5 10 362.46 26.80 1 5 10 477.55 31.80 -1 -5 10 448.06 31.30 -1 5 -10 470.15 32.10 1 5 10 428.96 31.50 1 5 10 460.55 34.20 2 -5 10 191.68 13.60 -2 5 10 186.18 15.90 2 5 -10 180.68 14.50 2 5 10 146.49 11.60 2 5 10 152.18 13.90 -2 5 -10 143.69 11.80 2 5 10 135.39 10.90 3 -5 10 886.21 60.59 3 5 -10 858.61 61.49 -3 5 10 945.51 62.59 3 5 10 773.22 58.19 -3 5 -10 949.31 59.29 3 5 10 856.81 58.79 3 5 10 871.51 60.99 4 -5 10 463.85 30.90 4 5 -10 431.36 31.90 -4 5 10 438.46 32.40 -4 5 -10 419.86 28.30 4 5 10 367.56 27.20 4 5 10 386.86 29.80 4 5 10 390.86 27.80 5 -5 10 42.40 4.70 5 5 -10 36.20 6.00 5 5 10 25.00 6.60 5 5 10 25.10 3.90 5 5 10 31.00 5.10 -5 5 -10 18.60 4.20 6 -5 10 213.88 15.80 -6 5 -10 154.18 13.10 6 -5 -10 122.59 13.90 6 5 10 136.39 12.70 6 5 10 165.88 14.20 6 5 10 153.58 11.30 7 -5 10 352.86 24.90 -7 5 -10 326.47 23.10 7 5 10 297.37 21.10 7 -5 -10 272.77 23.70 7 5 10 293.37 21.90 8 -5 10 137.99 10.80 -8 5 -10 98.29 12.20 8 5 10 85.99 8.70 8 -5 -10 92.19 11.60 8 5 10 82.69 7.60 9 -5 10 17.10 3.70 9 5 10 12.10 6.20 0 6 10 29.30 4.70 0 6 10 26.40 4.00 0 6 -10 39.60 5.00 0 -6 10 28.20 3.80 -1 6 10 1241.28 82.69 -1 6 10 1145.99 80.29 1 -6 10 1162.28 79.99 1 6 -10 1227.28 80.89 -1 -6 10 1239.48 86.69 -1 6 -10 1367.16 87.79 1 6 10 1291.97 87.29 1 6 10 1378.66 89.99 1 6 10 1207.48 87.09 -2 6 10 387.66 24.10 2 6 -10 312.47 24.50 -2 6 10 313.67 25.70 2 -6 10 339.17 23.60 2 6 10 382.56 27.70 2 6 10 364.16 30.10 2 6 10 442.16 28.40 -2 6 -10 395.56 28.40 3 6 -10 439.56 31.30 3 -6 10 432.16 30.20 -3 6 10 444.56 32.30 -3 6 -10 555.24 36.50 3 6 10 511.85 36.10 3 6 10 514.75 38.10 3 6 10 479.35 35.40 4 6 -10 223.68 18.00 4 -6 10 232.08 16.80 -4 6 10 241.38 18.80 4 6 10 162.98 13.60 4 6 10 199.98 16.30 -4 6 -10 204.68 15.00 4 6 10 170.98 14.50 5 -6 10 1157.08 79.29 5 6 -10 1200.58 80.59 5 6 10 1423.46 89.89 -5 6 -10 1335.97 88.39 5 6 10 1246.28 87.39 5 6 10 1193.98 87.89 6 -6 10 120.19 9.60 6 -6 -10 57.39 11.20 6 6 10 76.99 6.50 6 6 10 72.99 7.60 -6 6 -10 73.89 9.90 6 6 10 50.99 11.50 7 -6 10 13.90 2.60 7 6 10 3.70 2.90 7 6 10 4.90 2.10 -7 6 -10 3.20 4.50 7 -6 -10 8.70 5.30 8 -6 10 8.50 2.40 8 6 10 8.20 3.20 8 -6 -10 13.90 6.20 9 -6 10 163.58 12.00 9 6 10 156.58 13.30 0 7 -10 7.90 2.80 0 7 10 4.90 2.30 0 -7 10 1.90 1.80 -1 7 10 1107.19 73.09 1 7 -10 1091.29 73.49 -1 7 10 1084.09 75.19 1 -7 10 1042.20 72.49 1 7 10 1094.69 71.69 1 7 10 1051.09 73.79 1 7 10 988.40 71.29 -1 7 -10 1086.79 71.99 2 -7 10 10.00 1.90 2 7 -10 4.00 2.50 -2 7 10 7.00 3.30 2 7 10 18.00 4.60 2 7 10 16.50 3.50 -2 7 -10 17.40 3.70 -3 7 10 999.80 67.19 3 -7 10 934.71 65.09 3 7 -10 967.00 66.19 -3 7 -10 1396.76 91.99 3 7 10 1369.76 91.79 3 7 10 1371.26 93.69 3 7 10 1285.97 91.19 4 7 -10 29.50 5.60 4 -7 10 33.00 3.90 -4 7 10 28.40 7.00 4 7 10 41.90 7.10 4 7 10 50.09 6.30 -4 7 -10 42.90 6.30 4 7 10 42.90 5.10 5 -7 10 151.98 11.10 5 7 -10 134.19 12.50 5 7 10 142.99 10.70 -5 7 -10 126.49 11.90 5 7 10 140.19 13.00 5 7 10 130.89 11.70 6 -7 10 4.00 2.00 6 7 10 1.70 3.10 6 -7 -10 2.00 5.00 -6 7 -10 0.90 3.70 6 7 10 2.00 4.40 6 7 10 1.20 2.00 7 -7 10 479.95 33.00 -7 7 -10 461.45 31.50 7 7 10 409.66 30.80 8 -7 10 5.10 1.80 8 7 10 7.60 3.50 9 -7 10 9.80 2.10 9 7 10 12.00 4.00 0 -8 10 27.00 3.80 -1 8 10 642.64 42.80 -1 8 10 604.64 44.60 1 8 -10 627.24 43.20 1 -8 10 602.24 42.00 -1 8 -10 826.72 57.59 1 8 10 894.21 57.49 1 8 10 789.12 59.19 2 -8 10 186.08 13.50 -2 8 -10 294.27 22.30 2 8 10 305.57 24.10 -3 8 10 12.00 4.00 3 -8 10 11.50 2.30 3 8 10 30.90 5.50 3 8 10 33.30 6.80 3 8 10 26.10 4.40 -3 8 -10 29.30 5.90 4 -8 10 85.79 7.60 4 8 -10 89.59 9.00 -4 8 10 101.39 10.40 4 8 10 74.19 8.00 4 8 10 69.19 6.70 -4 8 -10 63.89 8.00 4 8 10 76.39 9.00 5 8 -10 411.86 30.80 5 -8 10 436.96 29.50 5 8 10 374.66 29.60 5 8 10 439.36 31.10 -5 8 -10 430.16 30.00 6 -8 10 145.89 11.10 6 8 10 113.49 10.10 6 -8 -10 99.79 12.70 7 -8 10 7.90 1.90 7 -8 -10 2.40 6.30 -7 8 -10 1.00 4.60 7 8 10 6.60 3.20 8 -8 10 89.59 8.90 8 8 10 59.59 11.30 0 9 -10 1041.50 65.79 0 -9 10 872.41 64.19 0 9 10 888.81 65.19 0 9 10 1029.60 67.39 1 -9 10 105.29 8.20 -1 9 10 118.99 9.40 1 9 -10 95.39 9.60 -1 9 10 90.99 10.60 -1 9 -10 78.39 8.30 1 9 10 80.29 8.20 1 9 10 77.79 9.50 -2 9 10 266.77 20.60 2 9 -10 263.87 19.40 -2 9 10 243.48 18.90 2 -9 10 243.98 18.10 -2 9 -10 328.57 23.60 2 9 10 319.97 24.90 2 9 10 300.07 23.40 3 9 -10 62.89 7.40 3 -9 10 79.39 6.10 -3 9 10 53.89 8.30 3 9 10 62.19 8.50 -3 9 -10 75.59 8.00 4 -9 10 284.77 20.50 -4 9 10 287.77 23.10 4 9 -10 300.77 21.90 4 9 10 363.86 27.30 4 9 10 333.47 26.00 -4 9 -10 373.26 26.10 5 -9 10 9.20 2.10 5 9 -10 1.10 3.30 5 -9 -10 4.60 5.30 5 9 10 2.00 4.00 -5 9 -10 6.20 3.70 5 9 10 1.60 3.00 6 -9 10 181.68 13.30 6 -9 -10 134.39 16.00 6 9 10 155.38 13.10 -6 9 -10 182.78 14.00 7 -9 10 84.89 6.90 7 9 10 65.29 7.60 8 -9 10 143.59 10.50 8 9 10 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13.20 1 13 10 167.58 13.40 2 -13 10 6.60 4.70 2 13 10 6.10 3.10 3 -13 10 257.27 18.10 3 13 10 232.68 17.50 4 -13 10 23.70 4.00 4 13 10 15.10 3.70 1 14 10 177.98 14.00 2 -14 10 8.30 2.70 2 14 10 0.20 3.00 0 0 11 -0.40 1.80 0 0 -11 1.80 2.10 -1 0 11 360.26 26.00 -1 0 11 403.66 29.20 1 0 -11 403.76 26.30 -1 0 -11 353.96 26.10 1 0 11 356.56 26.00 2 0 -11 1052.09 66.39 -2 0 11 1008.90 68.79 2 0 11 1032.60 66.19 -2 0 11 960.80 65.99 -2 0 -11 845.42 67.29 3 0 11 445.36 33.20 -3 0 11 492.35 35.60 3 0 -11 510.45 33.70 4 0 11 712.13 48.50 5 0 -11 5.80 3.40 5 0 11 2.80 2.00 5 0 11 -0.20 3.70 6 0 11 103.19 9.40 6 0 11 100.39 12.90 6 0 -11 124.09 11.20 7 0 11 227.88 21.20 7 0 11 211.58 16.80 7 0 -11 256.37 18.80 8 0 -11 130.99 12.20 8 0 11 137.59 10.60 0 1 -11 848.32 62.69 0 -1 11 967.80 62.59 0 1 11 893.41 65.19 0 1 11 1001.50 62.59 1 1 -11 379.16 26.40 -1 1 11 369.66 25.90 1 -1 11 336.27 25.90 -1 1 11 411.96 29.00 1 1 11 339.27 23.50 1 -1 -11 348.37 23.50 1 1 11 349.27 26.60 -1 1 -11 342.27 23.80 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1 -2 11 660.53 47.40 -1 2 11 713.83 50.09 -1 -2 11 664.33 45.90 1 2 11 746.63 46.20 1 2 11 621.54 48.60 2 -2 11 427.76 31.20 2 2 -11 436.86 31.80 -2 2 11 452.45 33.60 -2 2 11 487.75 31.20 2 2 11 251.17 22.00 -2 2 -11 270.87 19.80 2 2 11 291.87 19.40 3 2 -11 550.54 36.70 3 2 -11 509.85 36.80 -3 2 11 553.44 38.00 3 -2 11 472.35 35.80 -3 -2 11 453.85 42.10 3 2 11 437.16 32.00 -3 2 -11 521.35 32.50 3 2 11 445.16 34.90 4 2 -11 25.00 5.80 4 2 -11 27.30 5.70 4 -2 11 30.30 4.20 -4 2 11 33.70 8.00 4 2 11 89.29 7.20 4 2 11 71.29 9.90 -4 2 -11 83.39 8.30 5 2 -11 476.45 33.30 5 -2 11 447.26 32.20 5 2 11 505.25 36.10 5 2 11 534.95 39.00 -5 2 -11 593.34 36.80 5 2 11 498.35 35.80 5 -2 -11 475.55 37.70 6 2 -11 273.77 21.90 6 -2 11 304.97 21.30 6 2 11 152.28 15.50 6 2 11 168.38 12.50 6 -2 -11 158.28 14.40 6 2 11 144.99 12.60 7 -2 11 58.79 6.20 7 -2 11 70.39 13.10 7 2 11 89.19 16.40 7 2 11 61.49 7.30 7 -2 -11 75.29 9.40 7 2 11 70.79 6.50 8 -2 11 109.79 8.90 8 2 -11 97.59 10.90 8 -2 -11 125.39 11.80 8 2 11 105.49 10.10 8 2 11 122.99 9.50 9 -2 11 108.49 9.70 9 2 11 107.59 8.60 9 2 11 97.29 9.90 0 3 -11 3.10 2.30 0 -3 11 3.20 1.90 0 3 11 1.40 1.70 0 3 11 -0.30 2.60 1 -3 11 766.32 53.09 1 3 -11 808.32 53.79 -1 3 11 781.52 53.09 -1 3 11 781.22 55.59 -1 -3 11 756.22 52.99 -1 3 -11 834.12 53.59 1 3 11 748.73 55.79 1 3 11 801.52 53.19 2 3 -11 504.65 39.60 2 -3 11 543.05 39.20 2 3 -11 612.94 40.10 -2 3 11 641.84 41.90 -2 3 11 568.34 39.20 -2 3 -11 754.52 47.80 2 3 11 618.64 47.20 2 3 11 718.33 50.29 3 3 -11 1278.97 85.59 3 -3 11 1328.57 85.09 -3 3 11 1213.08 86.69 3 3 -11 1232.98 85.69 -3 3 -11 1335.57 85.79 3 3 11 1238.28 85.29 3 3 11 1358.96 85.49 3 3 11 1149.48 87.89 4 -3 11 20.60 3.90 4 3 -11 32.60 5.60 4 3 -11 27.50 5.70 -4 3 11 33.40 7.90 4 3 11 31.00 3.90 -4 3 -11 37.50 5.80 4 3 11 25.80 5.10 5 3 -11 171.78 13.90 5 -3 11 162.88 12.90 -5 3 -11 123.59 10.90 5 3 11 124.09 12.60 5 3 11 111.89 9.20 5 3 11 106.09 9.80 6 -3 11 17.70 3.80 6 3 -11 14.50 4.00 6 3 11 25.80 5.40 6 3 11 38.30 7.90 6 -3 -11 35.30 7.50 6 3 11 38.70 4.40 -6 3 -11 41.40 7.90 7 -3 11 348.07 31.60 7 -3 11 404.16 27.50 7 3 -11 410.56 28.40 7 -3 -11 369.66 26.70 7 3 11 322.27 24.60 7 3 11 349.77 24.30 8 -3 11 29.30 4.40 8 -3 -11 10.60 4.40 8 3 11 10.50 3.30 8 3 11 13.00 2.50 9 -3 11 34.50 4.60 9 3 11 19.80 4.30 0 -4 11 574.94 39.80 0 4 11 528.95 39.90 0 4 11 613.74 42.80 0 4 -11 623.24 40.50 -1 4 11 1749.82 115.99 1 -4 11 1828.92 115.89 1 4 -11 1731.03 116.49 -1 4 11 1623.84 118.19 -1 -4 11 1713.93 116.39 1 4 11 1566.44 118.99 1 4 11 1724.63 116.69 1 4 11 1898.21 116.69 -1 4 -11 1815.92 117.09 -2 4 11 208.88 16.40 2 4 -11 183.68 14.60 2 -4 11 167.88 13.60 -2 4 -11 215.88 15.10 2 4 11 176.48 14.60 2 4 11 181.88 14.30 2 4 11 213.48 17.50 -3 4 11 296.47 22.70 3 4 -11 298.47 21.60 3 -4 11 275.07 20.60 3 4 11 427.66 32.30 3 4 11 413.86 29.50 -3 4 -11 450.25 29.90 3 4 11 397.16 29.20 -4 4 11 634.14 43.40 4 4 -11 605.74 42.70 4 -4 11 582.84 41.60 -4 4 -11 756.52 46.60 4 4 11 610.04 45.90 4 4 11 592.34 45.60 4 4 11 727.63 48.80 5 -4 11 595.84 39.50 5 4 -11 549.05 40.40 5 4 11 655.53 47.80 5 4 11 673.53 47.60 5 4 11 690.03 50.29 -5 4 -11 780.22 48.60 6 -4 11 22.70 4.10 -6 4 -11 51.89 7.80 6 4 11 35.70 4.40 6 4 11 46.00 8.50 6 4 11 26.20 5.30 6 -4 -11 39.90 7.90 7 -4 11 101.99 8.60 7 4 11 74.79 7.80 -7 4 -11 105.29 14.20 7 4 11 81.99 7.10 8 -4 11 13.10 2.70 8 4 11 0.60 2.30 8 -4 -11 4.50 5.00 8 4 11 1.70 2.90 9 -4 11 120.59 9.40 9 4 11 97.59 9.30 0 5 11 500.05 36.60 0 5 11 529.35 39.20 0 -5 11 540.65 36.40 0 5 11 507.25 36.50 0 5 -11 588.14 37.30 -1 5 11 324.17 21.60 -1 5 11 280.27 23.70 1 5 -11 298.07 22.10 -1 5 11 294.77 21.50 1 -5 11 314.97 21.30 -1 -5 11 231.98 16.50 1 5 11 256.67 16.70 1 5 11 202.48 18.70 -1 5 -11 220.48 16.90 1 5 11 210.58 16.30 2 -5 11 415.46 30.60 -2 5 11 473.65 33.30 2 5 -11 448.96 31.70 2 5 11 444.76 31.40 2 5 11 424.66 31.20 -2 5 -11 458.35 31.80 2 5 11 474.95 34.20 3 -5 11 481.15 31.70 3 5 -11 471.55 32.70 -3 5 11 420.96 33.40 3 5 11 618.84 43.30 3 5 11 705.63 43.80 -3 5 -11 637.54 43.90 3 5 11 567.44 45.70 4 -5 11 324.47 22.40 4 5 -11 311.27 23.60 -4 5 11 310.27 24.20 -4 5 -11 400.96 26.70 4 5 11 368.26 28.30 4 5 11 345.47 25.50 4 5 11 347.47 26.00 5 -5 11 135.09 11.10 5 5 -11 130.89 12.00 5 5 11 71.29 7.10 -5 5 -11 63.29 7.80 5 5 11 55.29 7.00 6 -5 11 86.29 7.60 6 5 11 114.59 11.60 6 5 11 98.19 8.20 -6 5 -11 112.19 10.40 6 5 11 87.99 8.90 6 -5 -11 84.49 11.40 7 -5 11 161.58 12.30 7 5 11 149.99 12.40 7 5 11 162.48 11.90 -7 5 -11 165.08 14.50 7 -5 -11 142.39 14.70 8 -5 11 95.99 7.90 8 -5 -11 91.39 15.00 8 5 11 76.79 8.40 8 5 11 89.89 7.50 9 -5 11 10.80 2.20 9 5 11 10.80 3.90 0 6 11 71.59 9.60 0 -6 11 92.79 7.10 0 6 -11 75.09 7.90 0 6 11 91.89 7.50 1 -6 11 39.10 4.50 -1 6 11 48.60 5.60 -1 6 -11 97.69 9.50 1 6 11 115.09 8.90 -2 6 11 895.31 62.79 2 -6 11 895.51 60.39 2 6 -11 897.11 61.39 2 6 11 889.61 64.79 2 6 11 957.40 65.09 2 6 11 961.60 67.49 -2 6 -11 1024.20 65.49 3 6 -11 212.68 16.20 3 -6 11 196.98 15.00 -3 6 11 210.58 17.30 3 6 11 147.99 12.50 -3 6 -11 164.88 12.90 3 6 11 147.89 14.50 -4 6 11 152.48 13.60 4 -6 11 132.99 10.80 4 6 -11 138.39 12.20 4 6 11 153.08 12.40 -4 6 -11 177.28 13.90 4 6 11 155.28 13.00 4 6 11 169.38 15.00 5 6 -11 53.69 7.30 5 -6 11 56.99 5.50 5 6 11 76.29 6.50 5 6 11 60.19 9.20 5 6 11 71.89 7.60 -5 6 -11 60.69 7.90 6 -6 11 411.16 28.60 6 6 11 310.07 21.70 6 6 11 343.37 24.40 6 6 11 287.27 22.30 -6 6 -11 327.17 23.10 6 -6 -11 252.67 24.20 7 -6 11 21.60 3.60 7 6 11 15.90 3.00 7 6 11 11.10 3.70 7 -6 -11 16.40 6.40 -7 6 -11 19.00 5.90 8 -6 11 104.89 8.30 8 6 11 83.79 9.10 0 7 -11 1218.18 78.99 0 7 11 1120.09 80.69 0 7 11 1203.98 78.49 0 -7 11 1104.69 77.79 1 -7 11 90.99 7.40 1 7 11 92.89 8.00 1 7 11 89.39 8.40 2 7 -11 417.66 30.40 -2 7 11 435.06 31.90 2 -7 11 424.16 29.30 2 7 11 410.76 27.50 -2 7 -11 404.36 27.90 2 7 11 375.26 29.60 2 7 11 347.17 27.00 3 -7 11 47.80 5.20 3 7 -11 53.99 6.80 -3 7 11 66.69 8.20 -3 7 -11 31.70 6.00 3 7 11 25.10 5.20 3 7 11 26.80 4.20 4 7 -11 757.92 53.59 -4 7 11 774.32 54.59 4 -7 11 795.52 52.59 4 7 11 813.52 58.59 4 7 11 826.52 56.89 -4 7 -11 895.31 57.19 4 7 11 780.22 56.29 5 7 -11 101.89 9.70 5 -7 11 91.59 7.80 5 7 11 93.59 8.20 -5 7 -11 118.49 10.30 5 7 11 89.59 9.20 6 -7 11 214.68 15.60 -6 7 -11 178.38 14.00 6 7 11 156.38 12.10 6 7 11 154.58 15.10 6 7 11 148.29 12.90 7 -7 11 3.70 1.90 7 7 11 5.40 3.50 7 -7 -11 1.80 6.60 8 -7 11 27.30 3.60 8 7 11 43.40 7.20 0 8 -11 374.26 26.30 0 8 11 409.36 28.40 0 8 11 338.27 25.70 0 -8 11 329.47 25.00 1 -8 11 78.29 6.30 -1 8 11 65.69 7.10 1 8 11 160.58 14.60 -1 8 -11 140.79 12.60 2 -8 11 765.92 49.90 -2 8 11 706.33 51.99 2 8 -11 729.73 50.79 -2 8 -11 775.92 54.79 2 8 11 759.22 56.39 2 8 11 845.32 54.69 3 8 -11 72.79 8.00 3 -8 11 78.99 6.60 -3 8 11 78.49 9.40 3 8 11 129.49 13.20 3 8 11 147.49 11.90 -3 8 -11 132.09 12.10 4 -8 11 120.69 9.00 -4 8 11 114.09 12.50 4 8 -11 102.39 10.30 4 8 11 154.18 12.90 4 8 11 147.29 14.20 -4 8 -11 162.68 13.20 5 8 -11 147.69 12.50 5 -8 11 141.89 10.90 5 8 11 199.48 16.30 5 8 11 157.58 14.50 -5 8 -11 193.38 15.10 6 -8 11 111.79 8.80 6 8 11 57.79 7.10 6 -8 -11 53.59 10.80 -6 8 -11 56.39 8.10 7 -8 11 4.80 1.70 7 8 11 5.60 3.70 8 -8 11 39.50 4.10 8 8 11 37.80 7.10 0 9 -11 305.67 24.40 0 -9 11 358.56 23.60 -1 9 11 94.89 9.60 -1 9 11 119.79 11.50 1 9 -11 114.89 10.30 1 -9 11 108.79 8.60 -1 9 -11 118.99 10.20 1 9 11 117.09 11.70 1 9 11 96.79 9.90 2 9 -11 131.89 11.40 -2 9 11 130.09 13.10 2 -9 11 112.89 9.50 2 9 11 108.99 13.50 -2 9 -11 109.59 10.30 2 9 11 83.69 9.30 3 -9 11 209.38 15.90 -3 9 11 243.48 18.60 3 9 -11 212.28 17.20 -3 9 -11 278.47 20.80 3 9 11 282.87 22.10 3 9 11 261.07 20.50 4 9 -11 162.28 13.40 -4 9 11 153.68 15.40 4 9 11 80.59 9.90 -4 9 -11 94.89 9.30 5 9 -11 43.00 6.90 5 -9 11 38.20 4.30 5 9 11 14.80 3.90 5 -9 -11 14.20 6.70 -5 9 -11 16.70 4.80 5 9 11 27.20 8.10 6 -9 11 13.60 2.40 6 9 11 23.20 5.70 7 -9 11 102.69 8.30 7 9 11 46.20 7.40 0 10 11 230.98 18.60 0 10 -11 230.68 17.40 0 10 11 202.28 16.70 -1 10 11 312.07 23.10 -1 10 11 335.17 24.90 1 10 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53.39 1 -1 12 728.13 52.89 -1 1 12 776.82 55.99 -1 -1 12 708.83 46.20 -1 -1 12 603.74 49.30 1 1 12 648.44 49.40 1 1 12 752.42 46.40 2 1 -12 987.90 64.39 -2 1 12 874.71 63.59 2 -1 12 846.52 63.69 -2 1 12 1071.69 66.99 -2 1 -12 912.61 61.99 2 1 12 897.41 61.49 -2 -1 12 894.61 64.59 2 1 12 930.31 64.99 3 1 -12 538.85 37.30 -3 1 12 498.45 38.90 3 -1 12 555.84 36.70 -3 -1 12 506.55 41.30 3 1 12 644.84 38.80 3 1 12 530.05 41.80 4 -1 12 33.20 4.50 4 1 -12 42.00 6.80 4 1 12 6.10 2.40 4 1 12 6.80 4.10 5 -1 12 101.09 12.90 5 -1 12 93.29 8.60 5 1 -12 114.09 10.90 5 -1 -12 111.49 10.90 5 1 12 107.39 12.20 5 1 12 86.99 8.40 6 1 -12 166.38 18.70 6 1 12 265.87 19.30 7 -1 12 75.39 14.80 7 -1 12 106.29 8.40 7 1 -12 90.49 10.00 7 1 12 122.79 17.70 7 -1 -12 122.39 12.40 7 1 12 136.59 10.30 8 -1 12 54.09 5.90 8 1 12 69.99 6.80 8 -1 -12 74.59 10.40 9 -1 12 14.60 3.10 9 1 12 34.80 5.00 0 2 12 709.33 51.09 0 2 -12 717.73 48.50 0 2 12 720.33 48.10 0 -2 12 678.73 47.90 1 -2 12 425.06 29.20 1 2 -12 409.26 29.70 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3 12 593.54 43.50 1 -3 12 588.34 43.40 -1 3 12 705.63 46.60 1 3 -12 665.73 44.20 -1 -3 12 641.64 47.10 1 3 12 672.53 47.40 1 3 12 730.93 50.59 -1 3 -12 742.43 47.80 2 -3 12 238.98 17.20 2 3 -12 239.18 18.10 -2 3 12 228.58 19.70 -2 3 12 240.88 17.30 2 3 12 282.87 19.90 2 3 12 259.87 22.70 -2 3 -12 291.77 20.30 -3 3 12 62.39 9.10 3 -3 12 66.69 6.10 3 3 -12 57.69 7.70 3 3 12 102.89 12.10 -3 3 -12 126.99 10.20 -3 -3 12 101.29 13.80 3 3 12 119.99 9.20 4 3 -12 239.98 19.60 4 3 -12 253.17 19.70 4 -3 12 268.27 18.60 4 3 12 229.88 16.00 4 3 12 193.18 18.70 -4 3 -12 229.28 16.90 5 3 -12 675.93 44.20 5 -3 12 577.14 42.90 -5 3 -12 657.73 41.60 5 3 12 584.44 42.10 5 3 12 512.75 38.90 5 -3 -12 525.45 40.90 6 -3 12 64.59 6.40 6 3 12 93.49 7.80 6 3 12 103.79 11.60 6 -3 -12 80.19 10.10 6 3 12 82.99 8.70 7 -3 12 13.00 8.00 7 -3 12 14.00 2.90 7 -3 -12 5.70 4.50 7 3 12 7.70 2.40 7 3 12 7.90 3.80 8 -3 12 5.20 2.10 8 3 12 11.00 2.50 9 -3 12 144.49 10.90 0 4 12 65.49 8.50 0 4 12 45.50 5.60 0 4 -12 66.59 6.70 0 -4 12 55.39 5.50 -1 4 12 87.79 8.40 1 4 -12 112.29 9.30 -1 4 12 107.29 11.20 1 -4 12 94.89 8.00 1 4 12 51.99 7.90 -1 4 -12 46.50 6.10 2 -4 12 723.53 45.30 -2 4 12 609.54 47.50 2 4 -12 656.03 46.00 -2 4 -12 674.23 45.00 2 4 12 698.33 44.70 2 4 12 584.04 47.20 -3 4 12 499.95 35.40 3 4 -12 502.25 33.90 3 -4 12 426.46 32.70 -3 4 -12 449.76 31.20 3 4 12 432.96 33.50 4 -4 12 290.27 19.90 4 4 -12 262.87 21.10 4 4 12 322.47 27.00 4 4 12 361.46 24.70 -4 4 -12 354.66 25.00 4 4 12 338.67 24.30 5 -4 12 33.40 4.50 5 4 12 31.50 4.20 5 4 12 29.60 5.90 -5 4 -12 39.20 7.60 6 -4 12 128.39 10.30 6 4 12 124.99 10.70 6 -4 -12 117.09 12.60 6 4 12 134.09 10.00 6 4 12 124.29 13.50 7 -4 12 237.48 24.70 7 -4 12 285.07 19.10 7 4 12 227.08 16.90 7 -4 -12 240.68 19.40 8 -4 12 100.99 8.20 8 4 12 136.79 11.70 8 4 12 110.99 10.90 0 -5 12 563.64 34.80 0 5 -12 491.85 35.40 0 5 12 430.56 37.20 0 5 12 539.75 35.20 -1 5 12 158.28 13.10 1 -5 12 162.68 12.70 1 5 -12 179.18 13.80 -1 5 12 195.28 15.90 1 5 12 156.08 13.10 1 5 12 191.08 16.10 -1 5 -12 178.98 13.80 2 5 -12 676.03 44.80 -2 5 12 652.43 46.40 2 -5 12 603.54 43.70 -2 5 -12 729.83 47.10 2 5 12 661.53 46.60 2 5 12 714.93 49.60 2 5 12 624.34 46.50 -3 5 12 165.78 15.50 3 -5 12 168.78 12.70 3 5 -12 179.58 14.00 3 5 12 106.39 9.70 -3 5 -12 129.79 10.30 3 5 12 110.19 11.90 3 5 12 103.79 9.00 4 5 -12 380.56 27.10 4 -5 12 404.16 26.10 -4 5 12 325.07 28.40 4 5 12 367.56 25.90 4 5 12 378.96 26.30 4 5 12 338.97 28.30 -4 5 -12 386.76 26.70 5 5 -12 115.99 12.20 5 -5 12 89.89 8.10 5 5 12 48.80 6.40 5 5 12 51.49 5.30 6 -5 12 191.98 14.20 -6 5 -12 202.38 16.40 6 -5 -12 194.38 16.60 6 5 12 175.78 13.50 6 5 12 170.08 14.00 6 5 12 177.38 16.70 7 -5 12 9.70 2.20 7 -5 -12 12.50 5.50 7 5 12 12.10 3.40 7 5 12 8.90 2.40 8 -5 12 26.80 3.90 8 5 12 17.20 4.40 0 6 12 788.12 56.69 0 -6 12 792.42 56.39 0 6 12 896.91 59.69 0 6 -12 923.41 57.49 0 6 12 789.32 56.89 -1 6 12 164.38 12.70 1 6 -12 151.98 12.80 1 -6 12 156.98 11.80 -1 6 12 160.68 14.90 1 6 12 228.18 16.60 1 6 12 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0 13 149.39 15.20 2 0 13 59.09 9.80 -2 0 13 61.79 10.10 3 0 13 259.07 22.00 3 0 13 209.38 17.30 -3 0 13 247.98 21.40 4 0 13 27.60 8.40 4 0 13 36.60 5.90 4 0 -13 23.00 5.20 5 0 13 21.50 9.00 5 0 13 18.70 4.00 5 0 -13 24.10 7.30 6 0 13 50.79 5.50 6 0 -13 38.00 8.40 7 0 13 315.87 22.00 7 0 -13 300.17 23.30 8 0 13 12.40 3.10 0 -1 13 47.70 5.50 0 1 13 55.19 5.60 -1 1 13 334.77 25.60 1 1 -13 302.77 22.50 1 -1 13 282.17 21.70 -1 1 13 308.47 21.90 1 1 13 241.38 21.00 -1 -1 13 231.58 21.10 1 1 13 231.08 17.10 -1 -1 13 234.18 17.10 2 -1 13 349.77 26.10 -2 1 13 388.46 29.60 2 1 -13 380.56 27.00 2 1 13 375.46 28.80 2 1 13 350.46 25.00 -2 -1 13 335.77 28.40 3 1 -13 70.59 8.80 3 -1 13 66.39 6.70 -3 1 13 78.89 11.60 3 1 13 36.90 4.80 -3 -1 13 39.60 11.10 4 -1 13 117.69 14.80 4 1 -13 144.79 12.70 4 1 13 106.69 13.00 4 -1 -13 111.89 11.10 5 -1 13 709.83 48.60 5 1 13 628.54 43.20 6 -1 13 120.89 9.90 6 -1 13 126.39 15.40 6 1 -13 113.69 11.90 6 1 13 94.19 13.40 6 -1 -13 112.39 11.30 6 1 13 103.09 8.70 7 1 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15 138.49 11.00 6 -4 15 51.79 5.90 6 4 15 64.19 8.10 0 5 15 231.98 19.80 0 5 -15 220.68 18.00 -1 5 15 67.39 10.50 1 5 -15 64.99 9.00 1 -5 15 61.29 6.00 1 5 15 65.69 9.50 1 5 15 60.09 6.80 2 -5 15 132.29 9.80 2 5 -15 118.19 12.10 2 5 15 140.69 10.60 2 5 15 111.49 12.90 3 5 -15 95.39 10.40 3 -5 15 80.89 7.10 3 5 15 68.19 7.00 3 5 15 84.39 10.50 4 -5 15 87.49 7.20 4 5 15 91.89 8.20 4 5 15 100.89 11.50 5 -5 15 89.89 7.40 5 5 15 85.99 7.60 6 -5 15 32.70 4.00 6 5 15 9.00 2.40 0 6 15 48.20 8.80 0 6 -15 38.40 8.00 1 -6 15 72.09 6.40 1 6 -15 61.59 8.70 -1 6 15 62.49 10.50 -1 6 -15 93.59 10.50 1 6 15 82.29 10.70 2 -6 15 190.78 14.90 2 6 -15 201.98 16.60 -2 6 15 234.78 19.60 2 6 15 199.08 17.40 2 6 15 177.98 14.30 3 -6 15 161.48 11.40 3 6 -15 137.19 13.60 3 6 15 162.48 16.10 3 6 15 189.38 13.50 4 -6 15 31.80 4.10 4 6 15 40.60 5.00 5 -6 15 19.00 4.90 5 6 15 11.20 3.00 0 7 -15 79.59 10.10 0 7 15 95.29 11.10 1 7 -15 157.98 13.50 -1 7 15 147.49 15.20 1 7 15 167.18 15.60 -1 7 -15 160.88 14.90 2 7 -15 13.30 5.70 2 -7 15 8.70 2.60 2 7 15 11.40 5.00 3 -7 15 101.29 8.20 4 -7 15 121.19 10.50 5 -7 15 177.78 13.00 2 -8 15 19.20 3.50 3 -8 15 102.09 8.40 4 -8 15 29.90 4.50 3 -9 15 40.10 5.10 0 0 16 210.58 15.70 1 0 16 317.57 22.50 1 0 16 300.97 26.90 -1 0 16 329.77 27.30 2 0 16 30.90 4.60 -2 0 16 26.10 9.60 3 0 16 208.28 14.80 3 0 16 186.58 19.60 4 0 16 37.20 4.80 5 0 16 105.99 8.80 6 0 16 42.80 5.10 0 -1 16 206.38 20.10 0 -1 16 196.28 14.90 0 1 16 179.58 19.10 0 1 16 207.08 15.00 1 -1 16 117.79 14.90 -1 1 16 114.89 15.50 1 -1 16 136.89 10.00 1 1 16 114.09 9.80 -1 -1 16 131.69 15.90 1 1 16 103.59 14.60 -2 1 16 88.49 15.70 2 -1 16 69.99 11.60 2 1 16 89.99 8.10 3 -1 16 178.58 18.30 3 -1 16 174.28 13.20 3 1 16 127.39 9.60 3 1 16 97.69 14.20 4 -1 16 80.89 7.20 4 1 16 92.99 8.10 5 -1 16 35.10 4.60 5 1 16 38.30 5.00 6 -1 16 21.20 4.00 6 1 16 36.60 4.90 0 2 16 13.40 3.40 0 2 16 5.60 5.20 0 -2 16 13.10 3.30 0 -2 16 8.80 6.40 1 -2 16 184.78 13.10 1 -2 16 177.78 17.80 -1 2 16 158.58 17.60 1 2 16 136.09 16.40 -1 -2 16 168.18 18.10 1 2 16 171.68 12.60 -2 2 16 207.28 21.20 2 -2 16 204.88 19.80 2 -2 16 204.68 15.00 2 2 16 199.88 19.50 2 2 16 216.08 15.70 3 -2 16 27.60 4.10 3 2 16 15.20 3.10 3 2 16 14.10 5.70 3 -2 -16 9.10 6.70 4 -2 16 51.79 12.10 4 -2 16 64.79 5.90 4 2 16 48.50 5.90 4 2 16 65.99 11.50 5 -2 16 73.19 6.60 5 2 16 76.39 7.20 6 -2 16 49.90 5.20 6 2 16 79.29 7.30 0 3 16 688.23 47.30 0 3 16 661.73 50.49 0 -3 16 718.23 50.89 -1 3 16 52.39 11.20 1 -3 16 57.99 10.70 1 -3 16 72.99 6.30 -1 -3 16 71.89 13.80 1 3 16 69.79 11.10 1 3 16 87.89 7.90 2 -3 16 19.00 6.30 2 -3 16 21.70 3.90 -2 3 16 19.90 8.70 2 3 16 28.80 8.70 2 3 16 21.30 4.70 3 -3 16 54.79 5.40 3 -3 16 50.99 11.30 3 3 16 31.80 9.50 3 3 16 44.00 5.40 4 -3 16 291.77 20.50 4 3 16 330.67 23.50 5 -3 16 53.39 5.50 5 3 16 43.40 5.40 0 4 16 3.90 4.50 0 -4 16 7.80 5.70 1 -4 16 57.49 5.80 -1 4 16 42.60 11.10 1 -4 16 52.09 10.60 -1 -4 16 58.99 13.70 1 4 16 63.49 7.00 1 4 16 67.29 10.50 2 -4 16 494.35 33.90 2 -4 16 487.05 37.90 -2 4 16 506.95 38.80 2 4 16 497.15 37.40 2 4 16 488.95 34.30 3 -4 16 100.09 13.40 3 -4 16 136.39 9.50 3 4 16 134.19 10.90 4 -4 16 6.20 2.20 4 4 16 5.70 2.60 5 -4 16 31.60 4.40 5 4 16 34.00 5.20 0 -5 16 177.78 18.00 0 5 16 178.48 17.40 1 -5 16 105.19 8.30 1 -5 16 81.69 12.80 -1 5 16 86.09 12.60 1 5 16 104.19 12.90 2 -5 16 30.30 7.30 2 -5 16 26.60 4.50 2 5 16 31.60 9.00 2 5 16 21.70 4.70 3 -5 16 120.59 9.50 3 5 16 124.69 10.30 4 5 16 126.49 10.30 5 -5 16 38.90 4.70 5 5 16 41.60 5.60 3 -6 16 28.60 4.60 4 -6 16 28.40 4.50 2 -7 16 68.79 7.20 3 -7 16 185.38 13.60 0 0 17 -0.60 4.40 0 0 17 3.60 6.40 1 0 17 2.30 5.90 1 0 17 0.30 2.60 2 0 17 252.57 17.10 2 0 17 211.28 21.80 3 0 17 7.40 2.80 4 0 17 6.80 4.60 5 0 17 0.30 2.40 0 1 17 224.08 16.00 0 1 17 195.28 20.30 0 -1 17 205.18 20.60 1 -1 17 49.00 11.80 1 -1 17 51.09 6.20 1 1 17 41.50 11.30 1 1 17 44.40 5.90 2 -1 17 4.30 7.40 2 -1 17 5.10 2.70 2 1 17 7.60 6.40 2 1 17 9.90 3.00 3 -1 17 35.50 4.90 3 1 17 18.50 3.30 4 -1 17 163.98 14.40 5 -1 17 16.40 3.10 5 1 17 10.00 2.80 0 -2 17 -3.60 8.90 0 2 17 5.10 3.60 1 -2 17 196.58 15.50 1 -2 17 229.28 21.60 1 2 17 189.18 14.60 2 -2 17 139.29 10.90 2 2 17 168.88 13.10 3 -2 17 40.10 5.20 3 2 17 64.29 6.90 4 -2 17 28.90 4.70 4 2 17 26.90 5.20 1 3 17 118.89 10.40 2 -3 17 2.10 2.90 2 3 17 4.60 3.10 3 -3 17 229.58 17.10 3 3 17 231.88 17.20 4 -3 17 35.80 4.90 4 3 17 39.00 5.80 2 -4 17 5.00 2.90 2 4 17 18.70 4.10 3 -4 17 53.09 5.80 3 4 17 66.99 10.00 4 -4 17 12.80 2.70 4 4 17 4.50 3.40 2 -5 17 11.40 3.40 3 -5 17 160.08 12.00 1 0 18 70.09 8.10 2 0 18 9.00 3.40 3 0 18 27.40 5.00 1 1 18 67.49 7.90 2 -1 18 68.79 7.00 2 1 18 106.19 9.40 3 -1 18 176.88 13.10 3 1 18 196.28 14.60 1 2 18 51.99 7.00 2 -2 18 105.69 8.90 2 2 18 153.18 12.20 3 -2 18 5.60 2.60 3 2 18 19.20 3.60 2 -3 18 9.30 3.40 2 3 18 4.40 3.30 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 61246 _olex2_date_sample_data_collection 2018-10-04 _olex2_date_sample_submission 2018-10-04 _olex2_exptl_crystal_mounting_method 'mounted on a Cryoloop' _olex2_submission_original_sample_id PRA6-42 _olex2_submission_special_instructions 'No special instructions were received'