data_5-116 _audit_creation_date 2018-11-14 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _shelx_SHELXL_version_number '2018/3' _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_name '' _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C28 H26 I O4 P' _chemical_formula_sum 'C28 H26 I O4 P' _chemical_formula_weight 584.36 _chemical_absolute_configuration ? _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'I' 'I' -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'P' 'P' 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'orthorhombic' _space_group_IT_number 19 _space_group_name_H-M_alt 'P 21 21 21' _space_group_name_Hall 'P 2ac 2ab' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' _cell_length_a 7.9972(3) _cell_length_b 16.3553(5) _cell_length_c 18.8545(6) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 2466.10(14) _cell_formula_units_Z 4 _cell_measurement_reflns_used 10369 _cell_measurement_temperature 100.00(10) _cell_measurement_theta_max 29.0110 _cell_measurement_theta_min 2.7010 _shelx_estimated_absorpt_T_max ? _shelx_estimated_absorpt_T_min ? _exptl_absorpt_coefficient_mu 1.396 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.21004 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.43f (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.574 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description block _exptl_crystal_F_000 1176 _exptl_crystal_size_max 0.15 _exptl_crystal_size_mid 0.13 _exptl_crystal_size_min 0.12 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0524 _diffrn_reflns_av_unetI/netI 0.0555 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.930 _diffrn_reflns_limit_h_max 8 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 22 _diffrn_reflns_limit_k_min -22 _diffrn_reflns_limit_l_max 26 _diffrn_reflns_limit_l_min -25 _diffrn_reflns_number 20726 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.889 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 29.513 _diffrn_reflns_theta_min 2.160 _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100.00(10) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 5.2684 _diffrn_detector_type AtlasS2 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.930 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -57.00 37.00 1.00 1.50 -- 11.74 -57.00 30.00 94 2 \w -20.00 5.00 1.00 1.50 -- 11.74 -99.00 30.00 25 3 \w -78.00 16.00 1.00 1.50 -- -11.59 -77.00 -90.00 94 4 \w -15.00 81.00 1.00 1.50 -- 11.74 57.00-180.00 96 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at zero, AtlasS2' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0380509000 _diffrn_orient_matrix_UB_12 0.0364151000 _diffrn_orient_matrix_UB_13 0.0125963000 _diffrn_orient_matrix_UB_21 0.0084191000 _diffrn_orient_matrix_UB_22 -0.0141583000 _diffrn_orient_matrix_UB_23 0.0353672000 _diffrn_orient_matrix_UB_31 0.0797173000 _diffrn_orient_matrix_UB_32 0.0188079000 _diffrn_orient_matrix_UB_33 0.0022267000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Mo) X-ray Source' _reflns_Friedel_coverage 0.699 _reflns_Friedel_fraction_full 1.000 _reflns_Friedel_fraction_max 0.836 _reflns_number_gt 5726 _reflns_number_total 6113 _reflns_odcompleteness_completeness 99.90 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 26.32 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'CrysAlisPro 1.171.38.43f (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.38.43f (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.43f (Rigaku OD, 2015)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _refine_diff_density_max 0.496 _refine_diff_density_min -0.814 _refine_diff_density_rms 0.132 _refine_ls_abs_structure_details ; Flack x determined using 2111 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.021(12) _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.076 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 311 _refine_ls_number_reflns 6113 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0389 _refine_ls_R_factor_gt 0.0347 _refine_ls_restrained_S_all 1.076 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0231P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0642 _refine_ls_wR_factor_ref 0.0674 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2.a Aromatic/amide H refined with riding coordinates: C25(H25), C26(H26), C4(H4), C16(H16), C17(H17), C20(H20), C3(H3), C10(H10), C23(H23), C2(H2), C11(H11), C22(H22), C12(H12), C19(H19) 2.b Idealised Me refined as rotating group: C7(H7A,H7B,H7C), C27(H27A,H27B,H27C), C14(H14A,H14B,H14C), C28(H28A,H28B,H28C) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group I1 I 0.97729(3) 0.44987(2) 0.40646(2) 0.02317(8) Uani 1 1 d . . . . . P1 P 0.45907(14) 0.50426(6) 0.24274(5) 0.0164(2) Uani 1 1 d . . . . . O1 O 0.4785(3) 0.44991(14) 0.31381(12) 0.0174(5) Uani 1 1 d . . . . . O004 O 0.2892(3) 0.53502(17) 0.22807(14) 0.0212(6) Uani 1 1 d . . . . . O3 O 0.7389(4) 0.28253(17) 0.02363(14) 0.0250(7) Uani 1 1 d . . . . . O2 O 0.9502(4) 0.77404(16) 0.27624(14) 0.0213(6) Uani 1 1 d . . . . . C25 C 0.8928(5) 0.6348(2) 0.2624(2) 0.0206(9) Uani 1 1 d . . . . . H25 H 1.007160 0.624662 0.264315 0.025 Uiso 1 1 calc R . . . . C26 C 0.7816(5) 0.5709(2) 0.2543(2) 0.0184(9) Uani 1 1 d . . . . . H26 H 0.821904 0.517743 0.250466 0.022 Uiso 1 1 calc R . . . . C9 C 0.5403(5) 0.2884(2) 0.41382(19) 0.0179(8) Uani 1 1 d . . . . . C13 C 0.8132(5) 0.3492(2) 0.4018(2) 0.0174(8) Uani 1 1 d . . . . . C4 C 0.4805(5) 0.5425(2) 0.51825(19) 0.0236(9) Uani 1 1 d . . . . . H4 H 0.482634 0.563512 0.564059 0.028 Uiso 1 1 calc R . . . . C8 C 0.6421(5) 0.3584(2) 0.4161(2) 0.0165(8) Uani 1 1 d . . . . . C5 C 0.5648(5) 0.4700(2) 0.5035(2) 0.0213(9) Uani 1 1 d . . . . . C16 C 0.6529(5) 0.3719(2) 0.1949(2) 0.0191(9) Uani 1 1 d . . . . . H16 H 0.689534 0.365487 0.241342 0.023 Uiso 1 1 calc R . . . . C15 C 0.5351(5) 0.4317(2) 0.17910(18) 0.0171(8) Uani 1 1 d . . . . . C17 C 0.7168(5) 0.3216(2) 0.1418(2) 0.0194(9) Uani 1 1 d . . . . . H17 H 0.794084 0.281047 0.152915 0.023 Uiso 1 1 calc R . . . . C18 C 0.6639(5) 0.3324(2) 0.0718(2) 0.0178(9) Uani 1 1 d . . . . . C20 C 0.4796(5) 0.4400(2) 0.10952(19) 0.0199(8) Uani 1 1 d . . . . . H20 H 0.400378 0.479683 0.098654 0.024 Uiso 1 1 calc R . . . . C3 C 0.3939(6) 0.5836(2) 0.4661(2) 0.0242(10) Uani 1 1 d . . . . . H3 H 0.337394 0.631576 0.477233 0.029 Uiso 1 1 calc R . . . . C10 C 0.6113(5) 0.2132(2) 0.3966(2) 0.0208(9) Uani 1 1 d . . . . . H10 H 0.543838 0.166902 0.395467 0.025 Uiso 1 1 calc R . . . . C7 C 0.6551(6) 0.4252(3) 0.5619(2) 0.0247(10) Uani 1 1 d . . . . . H7A H 0.772886 0.424695 0.552112 0.037 Uiso 1 1 calc GR . . . . H7B H 0.614625 0.369983 0.564549 0.037 Uiso 1 1 calc GR . . . . H7C H 0.635281 0.452266 0.606285 0.037 Uiso 1 1 calc GR . . . . C23 C 0.6615(5) 0.7303(3) 0.2642(2) 0.0201(9) Uani 1 1 d . . . . . H23 H 0.621727 0.783673 0.266933 0.024 Uiso 1 1 calc R . . . . C27 C 0.8916(5) 0.8568(2) 0.2811(2) 0.0231(9) Uani 1 1 d . . . . . H27A H 0.825569 0.869592 0.240093 0.035 Uiso 1 1 calc GR . . . . H27B H 0.985525 0.893241 0.283560 0.035 Uiso 1 1 calc GR . . . . H27C H 0.824546 0.862897 0.323035 0.035 Uiso 1 1 calc GR . . . . C2 C 0.3900(5) 0.5544(2) 0.3975(2) 0.0210(8) Uani 1 1 d . . . . . H2 H 0.330563 0.581703 0.362322 0.025 Uiso 1 1 calc R . . . . C11 C 0.7795(6) 0.2058(3) 0.3810(2) 0.0227(9) Uani 1 1 d . . . . . H11 H 0.823930 0.155207 0.368633 0.027 Uiso 1 1 calc R . . . . C24 C 0.8324(6) 0.7146(2) 0.2677(2) 0.0184(9) Uani 1 1 d . . . . . C22 C 0.5514(5) 0.6655(2) 0.25649(19) 0.0198(9) Uani 1 1 d . . . . . H22 H 0.437091 0.675765 0.254347 0.024 Uiso 1 1 calc R . . . . C12 C 0.8817(6) 0.2741(2) 0.3840(2) 0.0213(9) Uani 1 1 d . . . . . H12 H 0.995223 0.269682 0.374063 0.026 Uiso 1 1 calc R . . . . C14 C 0.3553(5) 0.2946(3) 0.4269(2) 0.0238(10) Uani 1 1 d . . . . . H14A H 0.335812 0.323336 0.470504 0.036 Uiso 1 1 calc GR . . . . H14B H 0.308264 0.240752 0.429947 0.036 Uiso 1 1 calc GR . . . . H14C H 0.303732 0.323802 0.388480 0.036 Uiso 1 1 calc GR . . . . C6 C 0.5636(5) 0.4393(2) 0.43417(19) 0.0151(8) Uani 1 1 d . . . . . C1 C 0.4770(5) 0.4831(2) 0.38230(18) 0.0156(8) Uani 1 1 d . . . . . C21 C 0.6090(5) 0.5850(2) 0.2519(2) 0.0158(8) Uani 1 1 d . . . . . C19 C 0.5412(6) 0.3896(2) 0.0558(2) 0.0225(9) Uani 1 1 d . . . . . H19 H 0.500533 0.394257 0.009811 0.027 Uiso 1 1 calc R . . . . C28 C 0.7012(7) 0.2957(3) -0.0502(2) 0.0333(12) Uani 1 1 d . . . . . H28A H 0.769776 0.260519 -0.078812 0.050 Uiso 1 1 calc GR . . . . H28B H 0.723177 0.351665 -0.062338 0.050 Uiso 1 1 calc GR . . . . H28C H 0.585448 0.283580 -0.058802 0.050 Uiso 1 1 calc GR . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 I1 0.02063(13) 0.02047(13) 0.02840(14) -0.00292(11) 0.00171(11) -0.00218(12) P1 0.0195(5) 0.0145(4) 0.0151(5) 0.0017(4) -0.0020(4) -0.0004(5) O1 0.0253(14) 0.0142(11) 0.0127(12) 0.0008(10) 0.0004(11) 0.0009(16) O004 0.0199(14) 0.0199(15) 0.0238(15) 0.0036(12) -0.0036(12) 0.0012(13) O3 0.0364(19) 0.0219(15) 0.0167(15) -0.0036(12) 0.0001(14) -0.0022(14) O2 0.0183(16) 0.0183(13) 0.0274(15) -0.0034(11) 0.0000(13) -0.0030(13) C25 0.017(2) 0.026(2) 0.018(2) -0.0004(17) 0.0007(18) 0.003(2) C26 0.024(2) 0.0144(19) 0.017(2) 0.0005(15) 0.0005(17) 0.0032(18) C9 0.020(2) 0.0187(17) 0.0147(18) 0.0016(15) 0.0007(18) 0.0009(17) C13 0.022(2) 0.0181(18) 0.0121(18) -0.0001(16) -0.0035(18) -0.0038(17) C4 0.029(2) 0.0248(19) 0.0169(18) -0.0071(16) 0.0071(17) -0.001(2) C8 0.022(2) 0.0166(18) 0.0113(19) -0.0008(15) -0.0032(16) 0.0039(17) C5 0.022(2) 0.022(2) 0.020(2) 0.0004(16) 0.0028(17) -0.0007(18) C16 0.023(2) 0.020(2) 0.0145(19) 0.0030(16) -0.0036(17) -0.0032(19) C15 0.021(2) 0.0174(17) 0.0132(18) 0.0007(13) -0.0010(16) -0.0017(18) C17 0.020(2) 0.017(2) 0.021(2) 0.0021(16) -0.0036(18) -0.0012(18) C18 0.022(2) 0.0129(18) 0.018(2) -0.0018(15) 0.0031(17) -0.0029(18) C20 0.023(2) 0.0175(17) 0.0195(18) 0.0044(14) -0.0041(16) 0.000(2) C3 0.027(2) 0.0173(19) 0.028(2) -0.0024(17) 0.006(2) 0.0041(19) C10 0.028(2) 0.0156(18) 0.019(2) -0.0005(16) -0.0044(19) -0.0020(18) C7 0.030(2) 0.031(2) 0.013(2) -0.0033(17) -0.0019(18) 0.002(2) C23 0.026(2) 0.019(2) 0.016(2) -0.0001(16) -0.0004(18) 0.004(2) C27 0.024(2) 0.0177(19) 0.027(2) 0.0008(18) -0.0020(19) -0.004(2) C2 0.021(2) 0.0201(19) 0.022(2) 0.0031(18) 0.0018(17) 0.0019(19) C11 0.026(2) 0.019(2) 0.023(2) -0.0063(17) -0.0054(18) 0.005(2) C24 0.024(2) 0.020(2) 0.0108(19) 0.0023(16) 0.0002(17) -0.0039(19) C22 0.021(2) 0.023(2) 0.0147(19) 0.0031(15) -0.0035(17) 0.0018(19) C12 0.023(2) 0.021(2) 0.020(2) -0.0023(16) -0.0007(18) 0.0048(19) C14 0.020(2) 0.023(2) 0.029(3) 0.0039(18) 0.0001(18) -0.004(2) C6 0.0156(19) 0.0131(17) 0.0167(18) -0.0010(14) 0.0033(15) -0.0003(17) C1 0.0176(19) 0.0148(16) 0.0145(17) 0.0007(13) 0.0034(16) -0.0019(18) C21 0.019(2) 0.0176(18) 0.0110(18) 0.0021(15) 0.0008(16) -0.0020(17) C19 0.031(3) 0.0213(19) 0.0149(19) 0.0030(15) -0.0043(19) -0.007(2) C28 0.048(3) 0.037(3) 0.015(2) -0.0067(19) 0.002(2) 0.002(3) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag I1 C13 2.108(4) . ? P1 O1 1.615(2) . ? P1 O004 1.475(3) . ? P1 C15 1.794(4) . ? P1 C21 1.792(4) . ? O1 C1 1.401(4) . ? O3 C18 1.360(5) . ? O3 C28 1.441(5) . ? O2 C27 1.435(5) . ? O2 C24 1.362(5) . ? C25 C26 1.380(6) . ? C25 C24 1.396(6) . ? C26 C21 1.400(6) . ? C9 C8 1.405(5) . ? C9 C10 1.393(5) . ? C9 C14 1.503(6) . ? C13 C8 1.403(6) . ? C13 C12 1.385(5) . ? C4 C5 1.392(5) . ? C4 C3 1.378(6) . ? C8 C6 1.503(5) . ? C5 C7 1.507(6) . ? C5 C6 1.400(5) . ? C16 C15 1.390(5) . ? C16 C17 1.392(5) . ? C15 C20 1.391(5) . ? C17 C18 1.397(5) . ? C18 C19 1.389(6) . ? C20 C19 1.395(5) . ? C3 C2 1.379(6) . ? C10 C11 1.383(6) . ? C23 C24 1.393(6) . ? C23 C22 1.386(6) . ? C2 C1 1.387(5) . ? C11 C12 1.386(6) . ? C22 C21 1.398(5) . ? C6 C1 1.396(5) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 P1 C15 99.10(15) . . ? O1 P1 C21 105.12(16) . . ? O004 P1 O1 115.59(16) . . ? O004 P1 C15 114.35(17) . . ? O004 P1 C21 112.54(17) . . ? C21 P1 C15 108.97(18) . . ? C1 O1 P1 123.4(2) . . ? C18 O3 C28 117.7(3) . . ? C24 O2 C27 117.0(3) . . ? C26 C25 C24 119.6(4) . . ? C25 C26 C21 120.9(4) . . ? C8 C9 C14 120.6(4) . . ? C10 C9 C8 119.4(4) . . ? C10 C9 C14 119.9(4) . . ? C8 C13 I1 121.0(3) . . ? C12 C13 I1 117.2(3) . . ? C12 C13 C8 121.8(4) . . ? C3 C4 C5 121.1(4) . . ? C9 C8 C6 118.8(3) . . ? C13 C8 C9 118.1(4) . . ? C13 C8 C6 123.1(3) . . ? C4 C5 C7 120.0(4) . . ? C4 C5 C6 119.2(4) . . ? C6 C5 C7 120.7(4) . . ? C15 C16 C17 120.7(4) . . ? C16 C15 P1 123.5(3) . . ? C20 C15 P1 117.3(3) . . ? C20 C15 C16 119.1(3) . . ? C16 C17 C18 119.5(4) . . ? O3 C18 C17 115.0(4) . . ? O3 C18 C19 124.8(4) . . ? C19 C18 C17 120.3(4) . . ? C15 C20 C19 120.9(4) . . ? C4 C3 C2 120.8(4) . . ? C11 C10 C9 121.6(4) . . ? C22 C23 C24 119.2(4) . . ? C3 C2 C1 118.2(4) . . ? C10 C11 C12 119.6(4) . . ? O2 C24 C25 115.9(4) . . ? O2 C24 C23 123.6(4) . . ? C23 C24 C25 120.6(4) . . ? C23 C22 C21 121.2(4) . . ? C13 C12 C11 119.5(4) . . ? C5 C6 C8 121.6(3) . . ? C1 C6 C8 120.0(3) . . ? C1 C6 C5 118.2(3) . . ? C2 C1 O1 121.3(3) . . ? C2 C1 C6 122.4(3) . . ? C6 C1 O1 116.2(3) . . ? C26 C21 P1 122.8(3) . . ? C22 C21 P1 118.6(3) . . ? C22 C21 C26 118.6(4) . . ? C18 C19 C20 119.3(4) . . ? loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma 0 0 -2 4.85 0.94 0 0 2 4.88 0.9 0 0 -3 0.68 0.54 0 0 -3 0.18 0.24 0 0 -4 4.39 1.24 0 0 -4 4.09 0.88 0 0 -4 3.87 1.13 0 0 -5 1.48 1.03 0 0 -5 0.78 1.47 0 0 -5 1.22 1.18 0 0 5 0.05 1 0 0 -6 9999 324.75 0 0 6 8795.17 323.1 0 0 -7 2.74 2.05 0 0 -7 1.37 0.71 0 0 7 -0.11 1.69 0 0 -7 0.96 1.65 0 0 -8 753.95 32.24 0 0 8 804.44 31.81 0 0 -8 751.19 31.04 0 0 -8 821.67 27.89 0 0 -9 0.51 0.69 0 0 -9 1.07 0.88 0 0 -9 2.16 1.96 0 0 9 1.91 1.65 0 0 -10 799.21 34.57 0 0 10 770.13 32.79 0 0 -10 726.68 31.92 0 0 -11 1.97 1.89 0 0 11 -0.24 1.05 0 0 12 1697.36 65.19 0 0 12 1762.16 64.64 0 0 -12 1798.09 67.14 0 0 13 1.55 2.26 0 0 -13 4.03 2.86 0 0 13 4.14 3.15 0 0 -13 1.29 2 0 0 -14 707.09 34.71 0 0 14 735.71 36.68 0 0 14 764.49 36.37 0 0 -15 0.39 1.49 0 0 15 0.8 0.86 0 0 16 132.54 13.66 0 0 -16 85.52 10.84 0 0 17 3.26 2.75 0 0 18 125.16 14.76 0 0 19 5.65 4.65 0 0 20 181.03 19.1 0 0 21 5.03 4.07 0 0 22 92.3 14.73 0 0 23 5.81 3.76 0 0 24 22.65 7.58 0 0 25 3.75 3.62 0 0 26 63.94 13.58 0 -1 -2 2191.14 65.39 0 1 -2 2196.74 64.47 0 1 -2 2122.69 66.19 0 -1 2 2266.94 64.97 0 1 2 2323.5 65.44 0 1 3 52.65 3.72 0 -1 -3 50.56 3.75 0 -1 -3 46 3.69 0 1 -3 47.14 4.2 0 -1 3 57.57 3.88 0 1 3 57.24 4.08 0 1 -3 55.32 3.37 0 -1 -4 2155.63 68.15 0 1 4 2157.65 69.34 0 -1 -4 2223.85 68.88 0 -1 4 2252.68 68.84 0 1 -4 2349.59 67.8 0 -1 -4 2138.37 69.86 0 1 4 2268.67 68.33 0 1 -4 2158.82 70.47 0 -1 -5 3985 123.73 0 1 5 4325.79 122.96 0 -1 -5 3864.84 124.94 0 -1 5 3746.86 123.36 0 1 -5 4313.77 122.94 0 -1 -5 4612.5 123.22 0 1 5 3813.1 124.19 0 1 -5 3833.89 125.56 0 -1 -6 1050.5 34.83 0 -1 6 924.31 36.11 0 -1 6 1064.89 36.29 0 1 -6 980.09 38.48 0 1 6 967.26 36.74 0 -1 -6 1016.46 37.45 0 -1 -6 1071.85 36.52 0 1 -6 1023.21 35.63 0 -1 -7 1.9 1.36 0 -1 7 3.07 2.28 0 -1 7 0.35 0.38 0 1 7 1.53 0.96 0 -1 -7 1.36 1.43 0 1 -7 0.83 1.26 0 -1 -7 0.35 0.72 0 1 -7 2.57 1.26 0 1 -7 1.4 0.56 0 1 8 1786.44 61.38 0 -1 -8 1780.59 61.09 0 1 -8 1931.38 55.48 0 -1 8 1803.9 60.84 0 1 -8 1592.18 63.51 0 -1 -8 1756.15 57.86 0 1 -8 1796.3 60.38 0 -1 8 1562.77 60.85 0 -1 -8 1876.54 62.92 0 1 -9 33.6 3.2 0 -1 -9 45.85 5.79 0 1 9 47.48 5.77 0 -1 9 46.73 6.28 0 1 -9 42.6 6.5 0 -1 9 35.85 4.95 0 1 -9 42.55 5.22 0 -1 -9 37.06 5.67 0 1 10 658.77 28.18 0 1 -10 584.86 26.27 0 -1 -10 592.5 28.52 0 1 -10 566.89 21.36 0 -1 -10 635.31 28.28 0 -1 10 623.46 29 0 1 -10 645.59 31.73 0 1 11 1377.67 51.03 0 -1 -11 1310.67 51.11 0 -1 11 1327.12 50.63 0 -1 11 1313.41 52.41 0 1 -11 1323.89 49.29 0 1 -11 1383.84 56.08 0 -1 12 971.05 41.04 0 -1 12 1048.22 43.88 0 1 12 1005.79 41.44 0 -1 -12 1030.4 42.47 0 1 -12 977.18 46.04 0 -1 -12 925.49 42.06 0 1 -13 42.07 8.13 0 1 -13 52.01 6.79 0 1 13 59.67 7.87 0 -1 -13 37.81 6.77 0 -1 13 48.35 7.23 0 -1 13 44.46 7.82 0 -1 -13 40.65 6.77 0 1 14 483.18 26.06 0 -1 -14 436.15 26.5 0 1 -14 439 24.32 0 -1 14 492.53 26.58 0 -1 14 437.43 27.15 0 -1 15 2.7 2.02 0 1 15 0.63 0.68 0 -1 -15 1.96 1.08 0 1 -15 1.94 1.88 0 -1 15 -2.17 0.71 0 -1 16 1.73 2.66 0 -1 16 4.51 2.37 0 1 -16 7.19 3.08 0 1 16 6.5 3.1 0 -1 17 81.84 11.98 0 -1 17 87.17 11.29 0 1 17 105.91 12.48 0 -1 18 558.59 35.41 0 1 18 570.69 33.54 0 -1 19 47.59 9.9 0 1 19 30.34 7.45 0 -1 20 227.8 22.65 0 1 20 221.29 20.94 0 -1 21 -3.89 3.71 0 1 21 -3.4 2.33 0 -1 22 0.68 3.66 0 1 22 5.77 4.18 0 1 23 33.05 9.15 0 -1 23 53.12 11.36 0 -1 24 95.25 15.68 0 1 24 88.24 15.11 0 1 25 1.15 3.74 0 -1 25 0.33 2.75 0 2 0 2273.41 68.23 0 -2 0 2201.52 68.47 0 2 1 727.93 24.57 0 2 -1 677.86 26.02 0 -2 -1 730.85 24.73 0 -2 2 24.19 2.42 0 2 -2 22.81 2.48 0 2 2 28.15 2.79 0 2 2 15.81 2.22 0 2 -2 19.37 2.91 0 -2 2 21.46 2.9 0 2 -3 3714.12 114.31 0 2 -3 3803.71 110.55 0 -2 3 3828.07 112.88 0 2 3 3962.17 112.09 0 -2 3 3698.22 111.13 0 2 -4 88.54 7.38 0 2 4 96.36 6.5 0 2 -4 88.03 5.29 0 -2 4 90.71 6.15 0 2 4 103.58 6.56 0 -2 4 98.46 6.68 0 -2 5 186.86 10.53 0 2 -5 200.85 12.63 0 2 5 205.9 10.93 0 -2 5 189.08 10.47 0 2 -5 195.63 9.09 0 -2 -5 193.96 10.51 0 2 5 204.69 10.58 0 -2 6 739.74 27.74 0 -2 -6 732.3 27.89 0 -2 6 713.25 28.83 0 2 6 709.88 28.25 0 2 -6 741.63 25.91 0 2 -6 742.1 31.81 0 -2 -6 727.2 30.27 0 2 6 737.36 27.58 0 -2 7 2.19 0.99 0 2 -7 4.79 1.37 0 2 -7 0.66 1.19 0 -2 7 2.22 1.1 0 -2 -7 4.47 1.62 0 2 7 1.38 1.06 0 -2 -7 2.01 1.17 0 2 7 0.97 0.53 0 -2 -8 26.77 4.92 0 2 8 27.22 4.32 0 2 -8 20.4 3.19 0 -2 8 23.62 4.35 0 -2 -8 25.54 3.85 0 2 -8 25.17 5.1 0 -2 8 22.94 3.75 0 2 -9 2316.62 87.66 0 2 -9 2405.96 79.1 0 -2 -9 2503.01 84.93 0 2 -9 2582.27 73.33 0 2 9 2312.26 81.33 0 -2 -9 2436.05 80.65 0 -2 -10 663.31 28.54 0 2 10 701.11 29.6 0 2 -10 642.17 26.85 0 2 -10 607.94 21.1 0 2 -10 632.15 34.25 0 -2 11 160.39 12.05 0 2 11 182.31 13.4 0 2 -11 176.08 11.91 0 -2 11 160.94 14.35 0 -2 -11 174.17 12.89 0 2 -11 155.36 7.47 0 2 -11 139.8 15.17 0 -2 12 940.9 38.69 0 2 -12 887.38 46.41 0 2 12 920.01 39.32 0 -2 -12 922.8 42.46 0 -2 -12 960.85 39.79 0 -2 12 908.21 42.89 0 -2 13 178.09 16.49 0 -2 13 170.58 13.52 0 2 13 183.79 14.26 0 -2 -13 173.76 15.82 0 2 -13 174.23 18.45 0 -2 -13 181.45 14.29 0 2 -14 376.78 21.4 0 -2 14 390.5 22.83 0 -2 14 388.69 26.45 0 -2 -14 367.67 25.25 0 2 14 452.08 24.49 0 2 -15 328.02 20.76 0 -2 15 367.14 22.58 0 2 15 410.25 23.92 0 -2 15 396.42 27.34 0 -2 16 35.44 8.06 0 -2 16 35.04 6.59 0 2 -16 25.25 5.3 0 2 16 38.62 6.93 0 -2 17 20.06 5.43 0 -2 17 19.18 5.95 0 2 17 23.91 6.16 0 2 18 85.87 11.36 0 -2 18 59.32 9.46 0 -2 18 67.88 11.88 0 -2 19 47.67 9.98 0 -2 19 53.7 9.38 0 2 19 60.33 10.36 0 2 20 305.19 24.3 0 -2 20 256.45 25.12 0 2 21 37.09 8.33 0 -2 21 29.56 8.12 0 2 22 46.22 10.1 0 -2 22 44.36 10.46 0 2 23 61.45 11.98 0 -2 23 101.9 16.41 0 -2 24 1.08 1.93 0 2 24 -2.85 4.26 0 -2 25 2.53 3.43 0 2 25 8.45 4.65 0 3 0 -0.06 0.52 0 -3 0 0.01 0.29 0 3 -1 731.26 26.28 0 -3 1 750.27 29.62 0 -3 1 735.13 26.37 0 -3 -1 715.33 26.99 0 3 1 746.26 26.46 0 3 2 1234.72 43.21 0 -3 2 1305.06 45.97 0 -3 2 1278.31 42.49 0 3 -2 1356.59 43.23 0 3 -2 1322.18 46.42 0 -3 -2 1310.07 44.14 0 3 -3 -0.12 0.37 0 3 3 0.71 0.69 0 3 -3 0.72 0.77 0 -3 3 0.61 0.93 0 3 -4 82.62 5.69 0 3 4 71.39 6.14 0 -3 4 74.75 6.69 0 3 -4 87.89 8.23 0 3 4 84.53 6.43 0 3 -4 85.12 6.62 0 -3 5 270.37 14.45 0 3 5 293.69 14.39 0 3 -5 287.96 12.62 0 3 5 296.44 14.46 0 3 -5 285.75 16.98 0 -3 5 269.67 13.71 0 -3 6 414.76 19.26 0 3 -6 430.93 23.12 0 3 6 465.94 19.73 0 3 -6 404.18 16.76 0 -3 6 412.15 19.24 0 3 6 433.62 19.43 0 3 -7 1041.35 43.87 0 3 7 979.68 37.87 0 -3 7 1028.35 37.53 0 -3 -7 978.46 41.43 0 3 -7 1014.65 34.57 0 -3 -7 1005.64 37.52 0 -3 7 988.62 38.62 0 3 7 1055.49 37.66 0 -3 -8 139.61 12.43 0 -3 8 140.61 9.97 0 -3 8 135.54 11.17 0 3 -8 138.93 13.51 0 3 -8 136.63 8.47 0 3 8 140.16 10.63 0 -3 -8 139.59 10.02 0 3 8 146.85 10.21 0 -3 9 172.02 13.65 0 3 -9 159.02 10.1 0 -3 -9 178.33 11.79 0 3 9 155.56 12.06 0 3 -9 169.57 16.11 0 3 -10 158.37 10.46 0 -3 10 145.61 13.44 0 3 -10 150.94 6.64 0 3 10 162.5 12.52 0 -3 -10 174.69 12.08 0 3 -10 147.45 15.87 0 -3 -11 300.05 17.36 0 -3 11 300.37 17.07 0 3 -11 298.91 24.46 0 3 -11 254.18 10.06 0 3 -11 291.77 15.92 0 -3 11 292.3 20.7 0 3 11 296.77 18.31 0 -3 -11 318.14 21.76 0 -3 -12 528.31 26.21 0 -3 12 518.51 25.54 0 3 12 539.49 27.2 0 -3 -12 534.2 31.01 0 -3 12 480.14 29.94 0 3 -12 512.67 24.17 0 3 -12 537.61 36.04 0 -3 -13 357.59 21.27 0 -3 13 327.09 24.57 0 -3 13 347.28 20.38 0 3 -13 354.89 29.77 0 3 13 373.59 21.89 0 -3 -13 352.51 25.08 0 -3 -14 15.95 5.22 0 -3 14 2.85 1.24 0 -3 14 10.73 3.48 0 3 -14 8.12 2.67 0 3 14 11.18 3.76 0 -3 15 197.94 15.76 0 -3 15 231.07 21.32 0 3 -15 200.61 14.69 0 3 15 244.02 17.81 0 -3 16 96.48 13.96 0 3 -16 79.72 9.26 0 3 16 95.3 11.02 0 -3 16 79.66 9.87 0 -3 17 148.3 14.36 0 3 17 182.59 16.19 0 -3 17 187.4 20.23 0 3 -17 134.45 12.94 0 3 18 309.58 22.39 0 -3 18 301.18 26.99 0 -3 18 242.76 19.79 0 -3 19 3.99 2.66 0 -3 19 5.3 4.19 0 3 19 5.92 3.65 0 3 20 9.37 4.34 0 -3 20 10.75 5.67 0 -3 20 16.78 5.55 0 -3 21 190 22.73 0 3 21 191.11 19.47 0 -3 22 16.97 7.41 0 3 22 11.54 5.44 0 -3 23 47.13 11.68 0 3 23 51.77 10.85 0 -3 24 57.81 13.36 0 3 24 92.9 15.05 0 3 25 22.97 7.96 0 -4 0 1601.1 54.34 0 4 0 1607.02 53.33 0 -4 -1 404.51 19.19 0 4 -1 439.19 18.48 0 -4 1 438.19 22.24 0 4 1 417.59 18.17 0 -4 1 401.59 18.18 0 4 -2 0.65 0.85 0 4 -2 1.39 0.92 0 -4 2 -0.33 0.65 0 -4 2 2.98 1.67 0 4 2 0.52 0.76 0 -4 -2 1.03 1.04 0 -4 3 1771.37 63.41 0 -4 3 1810.25 59.04 0 4 3 1851.04 60.67 0 4 -3 1947.29 60.65 0 -4 -3 1761.81 61.87 0 4 -3 1745.34 64.88 0 4 3 1854.42 60.63 0 -4 4 6.48 2.05 0 4 -4 6.98 1.93 0 4 -4 7.14 2.05 0 4 4 5.43 1.58 0 4 4 4.02 1.42 0 4 -4 6.64 2.47 0 4 5 73.05 6.74 0 4 -5 86.08 7.6 0 4 5 93.83 7.61 0 -4 5 74.27 7.54 0 4 -5 71.48 8.59 0 4 -5 79.08 6.19 0 -4 6 338.03 18.17 0 4 -6 390.62 19.13 0 4 6 341.82 17.57 0 4 6 342.87 17.54 0 4 -6 355.38 21.72 0 4 -6 357.53 15.64 0 4 7 468.49 21.9 0 4 7 461.56 21.79 0 -4 7 444.26 21.63 0 4 -7 465.7 19.05 0 -4 7 484.71 22.36 0 4 -7 468.7 27.05 0 -4 8 723.91 29.91 0 -4 -8 676.59 29.2 0 4 8 677.24 29.97 0 -4 8 693.72 30.75 0 4 -8 746.08 37.56 0 4 8 748.56 30.25 0 4 -8 701.92 26.24 0 4 9 1356.13 50.98 0 4 -9 1442.04 47.43 0 4 -9 1476.94 62.21 0 4 9 1425.06 52.41 0 -4 -9 1369.04 50.78 0 -4 9 1338.47 53.34 0 -4 10 117.96 11.98 0 4 -10 148.98 16.66 0 4 -10 129.51 8.83 0 -4 -10 114.52 10 0 4 10 124.05 11.02 0 -4 -10 113.58 12.98 0 4 10 125.14 10.41 0 4 -11 130.12 9.69 0 -4 11 115.94 12.77 0 4 -11 137.32 17.12 0 -4 -11 147.12 11.49 0 -4 11 125.8 10.46 0 4 11 117.65 11.3 0 -4 -11 123.03 14.02 0 4 12 74.13 8.97 0 -4 -12 75.9 8.44 0 4 -12 67.76 12.58 0 4 -12 68.68 7.2 0 -4 12 79.82 10.94 0 -4 12 73.56 8.1 0 -4 -12 79.26 11.49 0 -4 13 693.9 39.48 0 -4 13 700.11 32.45 0 4 13 750.13 34.97 0 -4 -13 664.78 39.3 0 4 -13 742.12 47.96 0 4 14 118.44 11.99 0 -4 14 103.97 10.52 0 -4 14 93.03 13.34 0 -4 15 3.55 2.02 0 -4 15 0.8 1.66 0 4 -15 0.93 0.83 0 4 15 0.78 1.68 0 -4 16 16.25 5.89 0 4 16 26.42 5.9 0 -4 16 18.93 4.81 0 4 -16 21.36 4.49 0 -4 17 130.35 17.79 0 4 17 180.08 16.09 0 4 -17 138.24 12.58 0 -4 17 156.92 14.49 0 -4 18 -0.42 1 0 -4 18 -1.83 2.52 0 -4 19 146.08 15.18 0 4 19 177.68 17.3 0 -4 20 1.83 1.98 0 4 20 0.59 2.85 0 -4 20 -1.14 3.28 0 -4 21 -1.86 2.39 0 4 21 2.24 2.7 0 -4 21 6.61 2.59 0 4 22 5.57 2.54 0 -4 22 4.66 3.67 0 -4 22 7.14 5.61 0 -4 23 170.83 23.1 0 4 23 153.45 18.99 0 4 24 0.67 3.08 0 -5 0 0.01 0.41 0 5 0 0.87 0.7 0 5 1 1997.63 65.93 0 -5 -1 2011.12 68.55 0 5 -1 2079.83 66.45 0 -5 1 2055.36 72.88 0 -5 1 1836.98 66.23 0 -5 2 24.38 4.7 0 5 -2 28.92 4.1 0 5 2 24.64 3.87 0 -5 2 27.05 4.02 0 -5 -2 21.96 4.03 0 5 -3 412.9 23.57 0 -5 3 428.29 19.32 0 5 3 436.76 20.12 0 -5 -3 378.19 20.75 0 5 3 448.31 20.44 0 5 -3 433.02 19.82 0 -5 3 388.12 22.3 0 5 -4 58.36 6.2 0 5 4 57.92 6.17 0 5 -4 62.88 8.37 0 -5 4 61.66 7.66 0 -5 4 57.82 5.69 0 5 4 50.52 5.89 0 -5 -4 51.56 6.68 0 5 -5 1286.76 46.36 0 5 -5 1277.15 52.48 0 5 5 1228.97 45.46 0 -5 5 1193.1 48.06 0 5 5 1286.96 46.43 0 5 -5 1235.34 44.18 0 5 -6 0.83 1.28 0 5 6 2.05 1.33 0 5 -6 0.63 0.5 0 5 -6 2.37 1.83 0 5 6 0.73 1.29 0 -5 6 -0.91 1.06 0 5 7 1095.37 41.95 0 5 -7 1136.46 43.58 0 5 -7 1026.5 48.18 0 5 -7 1089.68 38.4 0 -5 7 1058.83 42.47 0 5 7 1036.24 40.97 0 5 -8 3.53 1.89 0 5 -8 3.03 1.44 0 5 8 3.06 1.79 0 5 8 3.29 1.88 0 5 -8 1.56 1.42 0 5 9 202 14.16 0 5 -9 218.45 11.63 0 5 -9 203.75 19.42 0 5 9 207.46 14.45 0 -5 10 264.4 18.57 0 5 -10 313.18 15.11 0 5 10 293.57 18.07 0 -5 10 317.28 18.2 0 5 10 287.19 18.35 0 -5 -10 314.1 18.09 0 5 -10 319.41 26.18 0 -5 -10 312.19 24.04 0 5 11 696.18 34.13 0 -5 11 758.92 32.96 0 -5 -11 737.31 41.79 0 5 -11 790.9 29.95 0 -5 -11 745.45 33.02 0 5 11 703.36 32.95 0 -5 11 701.16 36.23 0 -5 12 -1.14 1.23 0 -5 -12 4.43 3.24 0 5 -12 1.7 3.07 0 5 12 -0.09 1.76 0 5 -12 0.23 0.48 0 -5 -12 0.91 1.29 0 -5 12 0.52 1.36 0 -5 13 85.02 9.26 0 5 13 93.53 10.76 0 -5 13 79.96 11.66 0 5 -13 77.99 14.96 0 5 14 185.58 16.21 0 -5 14 203.39 20.18 0 -5 14 199.9 15.24 0 5 15 62.78 9.14 0 -5 15 48.72 10.14 0 5 -15 41.27 6.1 0 -5 15 42.45 6.87 0 -5 16 1.81 1.9 0 5 16 -0.05 1.66 0 5 -16 -0.3 1.79 0 5 -17 70.28 8.61 0 5 17 110.34 12.61 0 -5 17 92.6 15.41 0 -5 17 90.15 10.77 0 5 -18 6.37 2.34 0 5 18 11.37 3.94 0 -5 18 13.37 5.91 0 -5 18 2.07 1.51 0 5 19 6.84 3.86 0 -5 19 13.7 5.59 0 -5 19 6.05 3.25 0 5 20 33.63 7.71 0 -5 20 23.62 8.7 0 -5 20 22.56 6.1 0 5 21 247.04 22.29 0 -5 21 220.46 20.34 0 -5 21 206.5 25.77 0 -5 22 6.14 4.66 0 -5 22 11.23 4.55 0 5 22 13.88 5.24 0 -5 23 15.97 7.68 0 -5 23 30.7 7.96 0 5 23 37.34 9.32 0 5 24 13.35 6.06 0 6 0 354.11 17.99 0 -6 0 325.27 19.03 0 -6 -1 352.67 20.33 0 -6 1 332.92 18.7 0 6 -1 343.63 18.04 0 6 1 351.74 18.04 0 -6 1 371.87 23.22 0 6 -2 291.14 16.06 0 6 2 287.11 16.31 0 -6 2 262.41 15.91 0 -6 2 290.7 19.92 0 -6 -2 288.06 17.97 0 -6 3 2799.69 91.25 0 6 3 2703.92 91.56 0 -6 -3 2680.51 94.24 0 6 -3 2888.67 91.44 0 6 3 2812.24 91.67 0 -6 3 2896.16 97.82 0 -6 4 78.75 7.37 0 -6 -4 85.27 9.46 0 6 -4 87.19 8.31 0 -6 4 93.55 10.12 0 6 4 74.18 7.73 0 6 -4 76.24 10 0 6 4 94.84 8.79 0 6 -5 7.13 2.44 0 -6 5 4.88 2.18 0 6 5 11.67 3.09 0 6 5 11.24 2.77 0 -6 -5 8.21 2.82 0 6 -5 9.73 3.4 0 -6 -6 11.05 3.4 0 6 -6 11.22 3.9 0 6 6 14.91 3.53 0 6 6 16.44 3.46 0 6 -6 11.03 3.35 0 -6 6 8.05 2.83 0 6 -6 13.28 2.99 0 6 7 255.49 15.92 0 6 -7 255.33 14.06 0 6 -7 268.33 17.01 0 6 7 247.31 16.22 0 -6 -7 238.74 19.45 0 6 -7 230.77 20.03 0 -6 7 247.48 17.03 0 6 -8 217.18 15.82 0 6 -8 214.86 12.45 0 6 -8 207.46 19.28 0 6 8 227.22 15.44 0 6 8 211.7 14.63 0 6 -9 769.68 29.53 0 6 9 724.07 33.59 0 6 -9 784.11 43.34 0 6 9 731.65 33.45 0 6 -9 777.03 36.47 0 -6 10 132.5 11.63 0 6 -10 147.25 14.08 0 6 10 131.5 11.81 0 6 -10 136.41 9.26 0 6 -10 145.49 17.52 0 6 10 131.93 11.86 0 -6 -10 127.01 15.8 0 -6 -11 109.05 14.86 0 6 11 98.07 10.59 0 -6 -11 95.06 9.64 0 6 -11 113.77 8.31 0 6 11 80.59 9.35 0 -6 11 97.51 9.83 0 6 -11 93.92 11.79 0 6 -11 99.72 15.45 0 6 12 -0.15 1.5 0 -6 12 2.81 2.08 0 6 -12 -1.13 2.9 0 6 -12 1.11 1.37 0 6 -12 -0.14 2.9 0 -6 13 857.32 37.29 0 6 13 790.21 39.45 0 6 14 24.61 5.67 0 -6 14 21.56 4.7 0 6 -15 255.5 16.9 0 -6 15 295.75 25.39 0 -6 15 334.01 20.88 0 6 15 302.76 22.03 0 -6 16 61.24 11.59 0 6 -16 61.4 7.63 0 -6 16 57.46 8.43 0 6 16 72.61 10.37 0 -6 17 -1.55 3.03 0 6 -17 4.04 2.05 0 -6 17 2.45 1.66 0 -6 18 5.09 3.89 0 -6 18 7.34 3.51 0 6 18 4.16 2.51 0 -6 19 155.18 15.28 0 -6 19 119.18 18.73 0 6 19 144.4 16 0 -6 20 2.21 1.81 0 6 20 6.16 3.48 0 -6 20 -2.11 3.54 0 -6 21 36.41 10.84 0 -6 21 40.23 8.52 0 6 21 48.45 10.06 0 -6 22 16 5.29 0 6 22 18 6.09 0 6 23 33.69 9.05 0 -6 23 31.24 7.74 0 7 0 0.49 1.06 0 -7 0 2.55 1.69 0 -7 1 1272.48 51.7 0 7 1 1361.56 50.16 0 -7 -1 1388.37 54.77 0 7 -1 1402.06 50.82 0 -7 1 1388.62 58.42 0 -7 -2 546.16 29.18 0 7 -2 575.66 26.42 0 -7 2 601 32.77 0 7 2 579.69 26.96 0 -7 2 532.19 26.81 0 7 2 560.44 26.6 0 7 3 123.45 10.59 0 -7 3 128.24 13.36 0 7 3 137.69 11.31 0 7 -3 116.29 10.08 0 -7 -3 116.06 11.82 0 -7 3 110.29 10.34 0 -7 -4 183.2 15.39 0 7 4 200.12 13.81 0 7 -4 165.46 16.59 0 -7 4 182.68 15.96 0 -7 4 170.32 12.46 0 7 4 203.38 14.4 0 7 -4 208.51 13.97 0 7 5 280.34 17.46 0 7 5 274.92 16.88 0 7 -5 259.6 21.29 0 7 -5 265.75 16.87 0 -7 -5 250.44 19 0 -7 5 274.17 19.46 0 -7 5 252.5 15.28 0 -7 6 44.66 7.31 0 7 -6 40.6 6.03 0 7 -6 37.49 7.61 0 7 6 40.92 6.05 0 7 6 29.45 5.33 0 7 -6 29.09 4.85 0 -7 -6 41.8 7.5 0 7 -7 760.58 31.5 0 7 -7 717.16 41.14 0 7 -7 744.7 34.56 0 7 7 758.59 34.7 0 7 7 798.03 34.23 0 -7 -7 764.78 40.44 0 7 8 658.24 31.61 0 7 -8 649.44 38.84 0 7 -8 654.51 27.48 0 7 8 645.77 30.67 0 -7 -8 646.72 37.98 0 7 -8 624.33 31.73 0 -7 9 441.08 25.2 0 -7 -9 469.5 32.4 0 7 9 474.08 24.96 0 7 9 459.29 25.24 0 7 -9 465.28 21.31 0 -7 -9 418.11 31.09 0 7 -9 497.9 34.07 0 7 -9 450.97 26.24 0 7 -10 146.68 14.17 0 7 10 124.02 12.05 0 7 -10 133.17 17.48 0 -7 10 140.7 12.71 0 -7 -10 140.7 17.35 0 -7 -10 130.3 16.77 0 7 -10 139.56 9.75 0 7 10 131.93 12.26 0 7 11 441.3 25.45 0 7 11 440.45 25.39 0 -7 11 437.46 24.65 0 -7 -11 408.94 23.43 0 7 -11 495.18 20.98 0 -7 -11 421.53 33.55 0 7 -11 429.02 34.59 0 7 -11 467.09 28.79 0 7 12 2.57 2.22 0 7 -12 3.89 1.04 0 -7 12 8.14 3.14 0 7 12 0.85 0.82 0 7 -12 6.54 3.52 0 7 -12 5.78 2.24 0 7 -12 2.68 3.07 0 7 -13 24.82 2.22 0 -7 13 30.73 5.81 0 7 -13 30.69 4.62 0 7 -13 33.11 7.68 0 7 13 33.15 6.49 0 7 14 172.12 16.32 0 -7 14 180.55 14.84 0 7 -14 191.21 20.29 0 7 -15 309.83 27.81 0 7 15 273.44 21.7 0 -7 15 302.37 20.29 0 7 16 -0.64 2.24 0 7 -16 0.06 1.96 0 7 -16 0.67 1.16 0 -7 16 2.3 2.19 0 7 -17 42.41 6.46 0 7 -17 34.61 10.06 0 7 17 54.15 9.26 0 -7 17 41.47 7.46 0 7 -18 27.38 8.83 0 7 18 32.32 7.17 0 -7 18 30.77 6.7 0 7 19 7 4.34 0 7 -19 -1.76 3.27 0 -7 19 0.72 1.75 0 7 -20 217.99 28.12 0 -7 20 211.45 19.35 0 7 20 275.56 23.45 0 -7 21 210.8 19.67 0 7 -21 206.73 28.36 0 7 21 203.55 20.78 0 -7 22 38.36 8.3 0 7 22 45.97 10.01 0 -7 23 30.87 7.75 0 8 0 2066.51 71.19 0 -8 0 1985.33 75.27 0 -8 1 306.32 20.01 0 -8 -1 310.39 21.61 0 8 -1 345.49 19.16 0 8 1 311.98 18.35 0 -8 1 282.2 22.87 0 8 2 1005.17 42.33 0 8 -2 1053.29 42.05 0 -8 2 1049.88 50.11 0 -8 2 984.81 43.23 0 -8 -2 1070.43 47.4 0 8 2 1057.74 42.91 0 8 3 1211.78 48.81 0 8 3 1195.92 48.08 0 8 -3 1253.7 47.87 0 -8 3 1228.54 55.48 0 -8 3 1255.95 49.58 0 -8 -3 1177.99 52.56 0 8 4 1519.21 57.41 0 8 -4 1488.95 56.13 0 -8 4 1512.03 63.22 0 8 4 1509.06 56.59 0 -8 -4 1437.42 61.28 0 -8 4 1486.61 56.51 0 8 -5 2.24 2.18 0 8 -5 -0.3 0.76 0 -8 -5 2.86 2.66 0 -8 5 -0.21 1.41 0 8 5 2.32 2.18 0 8 5 0.11 1.3 0 8 6 447.44 24.09 0 -8 -6 454.54 29.27 0 8 -6 416.45 23.75 0 8 -6 463.99 31.71 0 8 6 435.99 24.81 0 8 -7 261.3 23.72 0 8 7 309.92 19.92 0 8 7 272.04 18.09 0 -8 -7 267.23 22.64 0 8 -7 286.9 19.07 0 8 -7 288.27 17.33 0 8 8 137.55 12.89 0 8 -8 152.63 11.44 0 -8 -8 145.31 16.98 0 -8 8 142.54 13.67 0 8 -8 143.39 13.26 0 8 -8 142.91 17.32 0 8 8 146.12 12.82 0 8 -9 373.86 19.12 0 8 9 371.17 22.18 0 -8 -9 360.88 29.32 0 8 -9 356.06 29.4 0 8 -9 370.02 23.34 0 -8 9 352.81 22.96 0 8 9 341.15 22.27 0 8 -10 673.14 43.84 0 8 10 690.77 33.69 0 8 -10 661.4 35.41 0 8 -10 728.4 29.19 0 -8 -10 686.11 44.14 0 8 10 664.7 34.05 0 -8 10 649.9 33.68 0 8 11 31.62 6.29 0 8 -11 24.08 3.99 0 8 -11 26.86 7.75 0 -8 11 19.45 4.58 0 8 -11 24.52 6.12 0 8 11 31.54 6.05 0 8 -12 209.19 10.71 0 8 -12 218.27 19.86 0 -8 12 222.86 17.12 0 8 12 220.35 17.66 0 8 -12 217.84 13.15 0 8 12 210.8 17.45 0 8 -13 182.26 8.9 0 8 -13 230.96 21.26 0 -8 13 220.54 16.78 0 8 13 209.11 17.7 0 8 -13 171.83 11.87 0 8 13 195.37 16.79 0 8 -14 27.32 7.23 0 8 14 33.61 6.97 0 -8 14 34.73 6.56 0 -8 15 1.31 1.69 0 8 -15 1.88 2.62 0 8 -16 199.37 14.79 0 8 16 224.42 20 0 -8 16 220.58 17.77 0 -8 17 31.97 6.61 0 8 17 45.85 8.95 0 8 -17 46.35 11.92 0 8 -18 16.05 7.28 0 8 18 10.7 5.11 0 -8 18 15.18 4.62 0 8 -19 155.83 22.98 0 -8 19 136.09 14.85 0 8 19 158.75 17.45 0 8 -20 34.58 11.46 0 -8 20 28.86 7.07 0 8 20 30.48 7.72 0 8 21 0.71 3.02 0 -8 21 1.71 2.22 0 8 22 83.47 13.66 0 -8 22 79.2 12.17 0 9 0 4.04 2.26 0 -9 0 1.94 1.75 0 -9 1 246.52 19.03 0 9 1 283.12 18.76 0 9 -1 277.06 17.63 0 -9 -1 293.91 21.96 0 9 1 289.64 18.78 0 -9 2 1088.05 48.17 0 9 2 1173.66 47.81 0 9 2 1123.34 46.84 0 9 -2 1134.68 45.88 0 -9 -2 1178.95 52.94 0 9 3 4.41 2.47 0 9 -3 3.82 2.4 0 -9 -3 6.63 3.01 0 -9 3 5.09 2.18 0 9 3 3.33 2 0 -9 -4 444.57 29.42 0 9 4 469.27 25.53 0 9 4 503.68 27.18 0 9 -4 441.62 24.58 0 -9 4 481.95 26.21 0 -9 5 67.19 8.27 0 9 5 76.78 9.06 0 9 5 78.17 9.66 0 -9 -5 81.45 11.73 0 9 -5 77.63 8.94 0 9 6 6.37 2.39 0 -9 6 6.56 2.45 0 9 -6 4.87 2.23 0 9 6 9.78 3.43 0 -9 -6 7.07 3.31 0 9 -6 0.81 1.1 0 -9 7 3.7 2.16 0 9 7 4.69 2.29 0 9 7 6.37 2.4 0 -9 -7 1.11 2.03 0 9 -7 6.54 4.55 0 9 -7 1.23 1.47 0 9 -7 5.44 2.18 0 9 -8 1065.47 57.56 0 9 -8 1042.34 46.53 0 9 8 1065.39 45.81 0 -9 -8 1044.48 55.46 0 9 8 1113.53 47.88 0 -9 8 1036.4 48.74 0 9 -8 1100.79 43.12 0 9 -9 59.85 8.92 0 9 -9 56.43 7.02 0 9 -9 69.85 12.82 0 9 9 72.47 9.24 0 -9 9 66.7 9.51 0 9 9 78.34 10.24 0 -9 -9 60.1 11.81 0 9 -10 77.53 10.44 0 9 -10 88.41 8.37 0 9 -10 83.23 14.61 0 -9 10 83.42 10.71 0 9 10 89.22 11.04 0 9 10 82.77 10.2 0 9 11 49.88 8.3 0 9 -11 64.4 6.11 0 -9 11 60.24 8.9 0 9 -11 58.57 9.31 0 9 -11 61.59 6.67 0 9 11 60.71 8.72 0 9 -12 399.76 17.88 0 9 -12 414.15 28.73 0 9 12 388.29 25.92 0 9 12 402.22 25.78 0 -9 12 426.8 25.8 0 9 -12 426.54 20.33 0 9 13 1.01 1.34 0 9 -13 0.83 1.59 0 9 -13 -0.09 0.8 0 -9 13 1.87 2.07 0 9 13 -2.47 2.21 0 9 -14 475.8 34.3 0 9 14 498.47 30.7 0 9 -14 448.46 17.03 0 -9 14 487.69 27.97 0 -9 15 112.76 12.43 0 9 -15 119.92 17.14 0 9 15 109.95 13.66 0 9 16 15.62 5.51 0 -9 16 6.66 2.84 0 9 -16 21.66 7.86 0 9 17 16.21 5.53 0 -9 17 10.56 4.02 0 9 -17 15.93 7.6 0 -9 18 217.49 18.93 0 9 -18 252.01 29.56 0 9 18 227.26 21.42 0 -9 19 -1.1 1.54 0 9 19 2.17 1.82 0 -9 20 194.05 18.54 0 9 20 192.63 20.41 0 -9 21 71.13 11.11 0 9 21 75.69 12.83 0 -9 22 104.03 13.95 0 -10 0 1578.86 66.66 0 10 0 1582.8 61.95 0 10 0 1566.47 59.7 0 10 -1 4.11 2.79 0 10 1 6.85 2.71 0 10 1 15.35 4.37 0 -10 -1 11.89 4.22 0 -10 1 6.94 2.84 0 10 -1 8.22 3.13 0 10 2 159.98 13.98 0 10 2 147.06 14.02 0 10 -2 159.87 13.24 0 -10 -2 145.49 16.5 0 -10 2 164.64 15.23 0 -10 3 14.16 4.21 0 -10 -3 11.79 4.92 0 10 3 21.75 5.35 0 10 3 15.89 4.23 0 10 -3 12.38 3.53 0 10 4 928.68 41.48 0 -10 -4 951.43 48.8 0 10 4 930.25 43.11 0 -10 4 918.23 42.51 0 10 -4 905.99 40.16 0 10 5 29 6.01 0 10 -5 28.7 5.52 0 -10 5 25.34 5.27 0 -10 -5 27.87 7.24 0 10 5 26.04 5.98 0 -10 5 29.3 7.24 0 -10 6 583.09 28.96 0 10 6 567.38 31.74 0 -10 6 566.72 35.11 0 10 6 589.8 30.56 0 10 -6 591.33 30.36 0 -10 -6 556.19 36.47 0 -10 -7 8.53 4.72 0 10 7 13.78 3.9 0 10 7 12.46 4.17 0 10 -7 4.32 3.73 0 10 -7 5.01 1.99 0 -10 7 9.62 4.29 0 10 -8 77.24 10.06 0 10 -8 77.06 9.07 0 -10 8 75.59 11.12 0 10 -8 74.64 13.94 0 -10 -8 83.75 13.95 0 10 8 78.79 10.02 0 10 8 83.55 10.89 0 10 -9 4.27 2.09 0 -10 9 4.84 1.87 0 10 9 5.33 3.17 0 10 9 3.4 2.45 0 10 -9 -1.08 3.19 0 10 -9 0.67 1.69 0 10 10 1431.65 62.89 0 10 -10 1530.16 63.97 0 10 -10 1489.68 54.73 0 -10 10 1491.96 63.68 0 10 10 1576.85 62.64 0 10 -10 1611.25 56.64 0 10 11 65.13 9.87 0 10 -11 54.23 6.52 0 10 11 65.57 9.47 0 -10 11 51.33 8.41 0 10 -11 64.79 6.75 0 10 -11 57.9 9.44 0 10 -12 327.76 17.6 0 10 -12 276.58 23.11 0 10 12 308.95 22.53 0 10 12 305.66 23.25 0 10 -12 308.5 15.9 0 -10 12 334.5 23.02 0 -10 13 0.87 1.81 0 10 -13 2.07 1.18 0 10 13 -0.86 1.02 0 10 -13 4 3.01 0 10 13 -0.28 1.59 0 10 -14 15.16 2.43 0 -10 14 23.04 5.88 0 10 -14 18.53 6.34 0 10 14 14.18 4.93 0 -10 15 2.4 1.9 0 10 -15 5.18 4.9 0 10 15 3.12 1.84 0 10 16 540.17 35.14 0 10 -16 545.8 40.74 0 -10 16 537.47 31.18 0 10 17 3.4 2.32 0 10 -17 2.76 1.53 0 -10 17 4.97 3.36 0 10 18 9.16 3.72 0 -10 18 9.82 3.91 0 -10 19 6.94 3.75 0 10 19 6.24 3.53 0 -10 20 44.96 8.71 0 10 20 50.57 10.71 0 -10 21 13.06 4.55 0 11 0 5.96 3.69 0 11 0 3.23 2.09 0 -11 0 4.95 3.36 0 11 1 22.38 5.12 0 -11 1 28.1 6.9 0 -11 1 21.08 6.79 0 11 -1 29.29 6.2 0 11 -1 26.07 5.49 0 11 1 32.25 6.94 0 -11 -1 35.27 8.24 0 11 2 1294.74 54.63 0 11 -2 1360.83 53.38 0 -11 -2 1412.43 64.53 0 -11 2 1296.64 64.33 0 11 -2 1285.58 54.91 0 11 2 1433.15 57.8 0 -11 2 1219.4 56.64 0 -11 3 49.66 10.11 0 11 3 62.55 9.35 0 -11 3 51.94 8.68 0 11 3 49.63 8.02 0 11 -3 53.33 7.67 0 -11 -3 49.86 10.19 0 11 -3 51.94 8.1 0 -11 4 688.64 41.47 0 -11 4 607.8 33.81 0 11 4 669.55 35.24 0 -11 -4 656.83 40.72 0 11 -4 623.05 31.78 0 11 4 632.93 32.82 0 11 -4 603.5 31.9 0 11 5 17.67 5.15 0 -11 -5 16.22 6.16 0 11 -5 15.22 4.34 0 -11 5 6.91 2.85 0 -11 5 14.02 4.06 0 11 5 16.8 4.51 0 -11 6 319.41 25.97 0 -11 6 306.95 20.18 0 11 -6 282.51 19.78 0 11 6 315.22 22.67 0 -11 -6 270.88 25.64 0 11 6 305.58 21.1 0 11 -6 279.1 19.15 0 -11 7 58.39 10.49 0 11 7 72.15 10.68 0 -11 -7 73.26 13.08 0 11 7 72.54 9.67 0 11 -7 61.81 8.63 0 11 -7 76.9 9.21 0 11 -8 1105.34 63.28 0 11 -8 1059.51 47.96 0 -11 8 1069.47 52.98 0 11 8 1091.66 48.43 0 11 -8 1156.23 47.33 0 11 -8 1086.4 44.95 0 11 8 1033.53 49.89 0 11 9 77.39 10.91 0 11 -9 60.89 7.95 0 11 -9 76.81 8.56 0 -11 9 57.21 9.93 0 11 9 68.69 9.85 0 11 -9 67.93 9.63 0 11 10 364.79 24.33 0 11 -10 377.03 25.28 0 11 -10 335.44 19.91 0 11 10 373.03 25.92 0 11 -10 330.84 19.3 0 -11 10 321.47 24.69 0 11 11 18.72 5.87 0 11 11 17.02 4.76 0 11 -11 24.62 4.34 0 -11 11 16.47 4.4 0 11 -11 21.67 4.16 0 11 -11 20.03 5.91 0 -11 12 76.12 10.76 0 11 12 78.28 11 0 11 -12 65.77 7.22 0 11 -12 64.68 6.94 0 11 -12 66.07 10.64 0 11 12 70.33 10.95 0 11 13 0.27 1.99 0 11 -13 2.52 2.17 0 11 13 2.26 1.74 0 -11 13 1.31 2 0 11 -13 0.31 0.74 0 11 -14 379.68 29.74 0 11 14 325.63 26.06 0 11 -14 353.73 16.57 0 -11 14 389.87 25.92 0 11 14 363.63 26.78 0 11 -15 4.94 4.79 0 11 15 2.18 2.47 0 -11 15 2.19 2.35 0 -11 16 28.5 6.73 0 11 16 11.17 5.06 0 11 -16 16.63 6.02 0 11 17 66.89 11.77 0 -11 17 90.54 11.76 0 11 18 42.54 9.37 0 -11 18 72.85 10.55 0 -11 19 8.24 4.06 0 11 19 4.74 2.4 0 -11 20 236.42 21.19 0 -11 21 24.67 6.91 0 12 0 1109.24 50.27 0 -12 0 1189.09 58.08 0 12 0 1189.23 52.75 0 12 -1 370.06 25.21 0 -12 -1 380.82 29.95 0 12 -1 377.12 23.07 0 12 1 388.08 25.92 0 -12 1 342.46 29.94 0 -12 1 345.95 26.77 0 12 1 390.09 24.92 0 12 2 331.1 22.97 0 -12 2 359.1 26.19 0 -12 2 394.7 31.56 0 12 -2 348.95 22.18 0 12 2 421.2 26.87 0 12 -2 334.54 23.85 0 -12 -2 380.89 30.5 0 12 -3 271.45 19.08 0 -12 3 294.95 26.82 0 12 3 324.51 23.21 0 12 -3 273.31 20.72 0 -12 -3 299.52 27.03 0 -12 3 246.36 21.12 0 12 3 263.07 19.95 0 12 -4 497.09 29.3 0 -12 4 485.01 35.88 0 12 -4 505.91 28.1 0 -12 -4 529.49 37.29 0 12 4 509.44 29.4 0 -12 4 443.28 29.41 0 12 4 541.16 31.85 0 12 -5 37.55 6.82 0 -12 5 21.42 6.41 0 -12 5 37.11 7.14 0 -12 -5 44.57 9.96 0 12 -5 37.37 6.91 0 12 5 43.32 7.9 0 12 5 39.45 7.98 0 12 -6 180.82 15.82 0 -12 -6 180.07 21.3 0 -12 6 202.96 16.37 0 12 6 200.09 18.52 0 -12 6 217.49 21.9 0 12 -6 197.84 16.23 0 12 6 181.71 16.37 0 12 -7 120.49 12.64 0 12 7 125.73 13.5 0 -12 7 133.82 16.51 0 12 -7 123.34 12.45 0 12 7 123.48 14.33 0 12 8 39.3 8.17 0 -12 8 36.25 8.49 0 12 8 58.27 8.98 0 12 -8 53.36 7.96 0 12 -8 31.81 6.48 0 12 -8 42.54 7.22 0 -12 9 365.54 27.81 0 12 -9 350.44 24.46 0 12 9 386.75 25.56 0 12 9 389.55 27.43 0 12 -9 365.59 22.53 0 12 -9 377.86 22.4 0 12 -10 1098.44 51.66 0 12 -10 1203.1 46.84 0 12 10 1211.65 52.81 0 12 10 1110.03 54.07 0 12 -10 1054.29 45.67 0 -12 10 1147.89 55.03 0 12 11 42.26 8.68 0 12 -11 39.81 8.06 0 12 -11 37.29 6.01 0 12 11 44.25 8.45 0 12 -11 42.25 6.31 0 -12 11 43.63 8.49 0 12 12 11.93 4.97 0 -12 12 18.92 5.34 0 12 12 24.88 6.55 0 12 -12 14.65 4.6 0 12 -12 17.7 3.88 0 12 13 211.08 20.74 0 -12 13 228.07 19.99 0 12 -13 256.88 23.04 0 12 13 242.65 21.37 0 12 -13 218.06 14.39 0 12 -14 6.09 4.49 0 12 14 3.73 2.11 0 12 14 9.88 4.87 0 -12 14 3.31 3.08 0 12 15 60.96 11.27 0 -12 15 87.55 11.88 0 12 16 397.49 30.62 0 -12 16 386.49 26.64 0 -12 17 35.05 7.66 0 12 17 23.94 7.22 0 -12 18 13.2 4.92 0 12 18 8.17 4.29 0 12 19 45.02 10.01 0 -12 19 29.31 7.33 0 -12 20 6.9 3.58 0 13 0 5.4 3.2 0 13 0 2.43 1.92 0 -13 0 1.33 2.74 0 -13 0 8.13 4.5 0 13 1 528.75 32.65 0 13 -1 516.46 30.35 0 13 1 525.69 30.44 0 13 -1 530.4 32.36 0 -13 1 501.38 37.96 0 -13 1 479.32 33.6 0 -13 -1 523.63 37.76 0 13 -2 175.22 17.25 0 13 2 163.95 15.67 0 13 2 181.04 18.06 0 13 -2 189.62 15.74 0 -13 -2 157.53 20.02 0 -13 2 174.61 21.16 0 -13 2 171.53 18.26 0 -13 3 30.53 8.73 0 13 3 27.71 7.1 0 13 -3 22.84 5.15 0 -13 -3 30.43 8.81 0 13 -3 16.94 5.18 0 13 3 16.97 4.96 0 -13 3 16.31 5.77 0 13 -4 42.72 7.15 0 13 4 41.02 7.95 0 13 -4 36.81 7.45 0 -13 -4 43.14 10.58 0 13 4 46.99 9.15 0 -13 4 49.45 10.56 0 -13 4 47.17 8.93 0 13 -5 1149.65 52.66 0 13 5 1164.13 52.62 0 13 -5 1186.64 50.96 0 -13 5 1325.02 65.32 0 -13 5 1164.27 53.72 0 13 5 1197.81 56.38 0 13 -6 2.05 2.35 0 13 -6 5.43 2.55 0 -13 6 1.67 1.22 0 13 6 3.59 2.26 0 -13 6 2.92 2 0 13 6 7.82 4.1 0 -13 7 212.39 22.56 0 13 -7 248.39 19.11 0 13 -7 228.22 18.46 0 -13 7 238.76 18.17 0 13 7 227.41 20.84 0 13 7 228.81 19.1 0 13 8 201.7 19.8 0 13 8 224.63 19.08 0 13 -8 212.67 17.31 0 -13 8 230.18 22.66 0 13 -8 214.88 17.85 0 13 -9 7.34 3.26 0 13 -9 1.28 1.4 0 -13 9 2.39 4.16 0 13 9 2.4 3.06 0 13 9 2.66 2.02 0 13 10 87.12 11.91 0 13 -10 98.72 10.57 0 13 10 68.33 11.35 0 13 -10 75.69 10.63 0 -13 10 81.52 12.48 0 13 -11 498.3 31.57 0 -13 11 492.68 33.26 0 13 -11 526.93 26.95 0 13 11 486.2 33.43 0 13 11 522.25 32.25 0 13 12 26.77 6.48 0 13 12 35.42 8.93 0 -13 12 36.08 8.06 0 13 -12 35.39 7.81 0 13 -12 29.54 5.1 0 -13 13 30.61 7.52 0 13 13 40.81 8.73 0 13 -13 38.99 5.65 0 13 13 31.45 8.31 0 13 -13 31.08 7.57 0 13 14 79.17 13.18 0 13 14 92.18 13.51 0 -13 14 95.35 12.88 0 13 15 16.03 5.21 0 -13 15 20.49 6.33 0 -13 16 4.41 3.21 0 13 16 2.44 3.18 0 13 17 229.62 23.77 0 -13 17 263.56 21.87 0 13 18 21.14 6.93 0 -13 18 27.47 7.05 0 -13 19 2.92 1.9 0 -13 20 20.38 5.93 0 -14 0 241.86 26.44 0 14 0 223.29 19.1 0 -14 0 208.36 23.15 0 14 0 273.12 22.8 0 -14 1 371.86 33.29 0 14 -1 396.41 26.63 0 14 1 399.73 26.65 0 14 -1 425.98 29.67 0 -14 -1 422.49 34.67 0 -14 1 409.59 31.6 0 14 1 432.35 29.94 0 -14 -2 105.19 17 0 14 -2 130.65 15.21 0 -14 2 106.52 16.81 0 -14 2 99.42 14.13 0 14 2 114.17 13.14 0 14 2 99.73 13.91 0 -14 3 219.66 24.89 0 -14 3 219.14 21.35 0 14 -3 263.64 22.17 0 -14 -3 235.91 26.4 0 14 -3 266.06 19.49 0 14 3 274.51 21.03 0 14 3 262.73 22.99 0 -14 4 120.2 17.75 0 14 -4 105.9 13.41 0 14 4 122.68 15.15 0 -14 4 90.43 12.85 0 14 4 106.59 13.07 0 14 -4 104.04 11.66 0 14 5 151.29 17.41 0 14 5 123.98 14.08 0 14 -5 144.35 13.95 0 -14 5 136.64 15.36 0 -14 5 130.09 18.62 0 14 -5 152.79 15.99 0 -14 6 130.12 18.18 0 14 -6 131.75 14.48 0 14 6 123.28 15.4 0 14 6 118.93 13.82 0 -14 6 120.09 13.42 0 14 -6 118.6 12.78 0 14 7 167.68 16.75 0 -14 7 178.31 16.24 0 14 -7 213.88 18.28 0 14 -7 193.01 16.81 0 14 7 210.17 20.48 0 -14 7 177.83 21.24 0 14 8 25.29 6.86 0 -14 8 38.33 9.43 0 14 -8 23.58 5.81 0 14 8 11.77 4.12 0 14 -8 23.56 5.9 0 14 -9 275.21 21.15 0 14 -9 272.83 20.17 0 14 9 271.13 24.1 0 -14 9 266.54 25.13 0 14 9 271.23 22.2 0 14 10 84.72 12.03 0 -14 10 83.4 13.19 0 14 -10 64.12 9.08 0 14 -10 83.3 11.23 0 14 10 66.14 11.29 0 14 11 18.42 6.05 0 14 -11 23.99 5.2 0 -14 11 21.4 6.41 0 14 -11 19.21 5.37 0 14 11 12.29 4.39 0 14 -12 9.6 3.01 0 14 12 13.62 5.24 0 14 12 11.62 4.89 0 -14 12 16.12 5.68 0 -14 13 405.72 29.75 0 14 13 461.42 31.6 0 14 13 378.02 30.93 0 14 14 47.75 10.85 0 -14 14 54 9.97 0 14 14 59.27 11.22 0 14 15 29.44 7.89 0 -14 15 27.32 7.07 0 -14 16 42.15 8.7 0 14 16 37.25 9.41 0 -14 17 9.54 4.28 0 14 17 8.42 4.64 0 -14 18 3.01 2.63 0 -14 19 266.29 23.05 0 15 0 6.2 4.1 0 15 0 0.31 0.85 0 -15 0 -1.4 3.07 0 -15 0 -0.82 3.08 0 -15 -1 195.11 25.48 0 15 -1 185.84 19.45 0 -15 1 181.46 23.53 0 -15 1 172.36 20.46 0 -15 -1 160.72 21.64 0 15 -1 184.31 17.31 0 15 1 173.31 19.11 0 15 1 149.83 15.85 0 15 -2 -0.32 1.47 0 15 2 1.21 2.26 0 15 2 1.81 2.58 0 -15 -2 4.59 4.89 0 15 -2 1.61 0.97 0 -15 2 0.98 2.82 0 -15 2 1.77 1.63 0 -15 3 4.33 3.46 0 -15 3 10.36 5.91 0 15 3 6.69 3.32 0 15 3 -0.69 1.99 0 15 -3 1.38 3.61 0 15 4 89.28 12.05 0 15 4 92.3 13.7 0 15 -4 81.69 12.21 0 -15 4 44.66 11.07 0 15 -4 70.91 9.79 0 -15 4 65.37 11.16 0 15 -5 51.65 8.32 0 15 5 47.57 8.82 0 15 5 56.78 10.91 0 -15 5 48.67 9.17 0 -15 5 34.59 9.63 0 15 -5 42.75 8.75 0 15 -6 24.61 5.59 0 15 -6 40.24 8.11 0 15 6 31.37 8.05 0 -15 6 29.58 6.69 0 -15 6 20.27 7.16 0 15 6 27.33 6.65 0 15 -7 210.19 17.98 0 -15 7 208.02 23.83 0 15 -7 227.31 20.07 0 15 7 240.57 23.08 0 15 7 223.72 19.87 0 -15 7 203.61 17.95 0 15 8 -2.32 3.81 0 15 -8 3.91 2.5 0 15 -8 0.64 1.83 0 15 8 2.79 2.02 0 -15 8 4.85 3.61 0 15 9 55.5 9.76 0 15 -9 49.28 8.53 0 -15 9 44.64 10.33 0 15 9 40.42 9.15 0 15 -9 44.26 8.1 0 15 10 23.06 6.99 0 15 10 28.41 7.11 0 15 -10 21.73 5.29 0 15 -10 21.91 5.81 0 -15 10 26.49 7.4 0 15 11 161.53 17.48 0 15 11 158.24 18.96 0 -15 11 178.62 20.08 0 15 -11 126.7 13.6 0 15 -12 31.67 6.07 0 -15 12 40.95 9.19 0 15 12 35.77 7.98 0 15 12 40.94 9.67 0 15 13 31.18 7.88 0 15 13 23.78 7.48 0 -15 13 25.09 7.17 0 -15 14 8.41 4.69 0 15 14 8.71 5.02 0 -15 15 199.14 20.17 0 15 15 189.72 21.16 0 15 16 69.29 12.88 0 -15 16 73.31 11.85 0 -15 17 103.4 14.04 0 -15 18 3.42 2.64 0 -16 0 27.51 9.13 0 -16 0 9.85 5.34 0 16 0 32.52 8.28 0 16 0 19.62 5.72 0 16 -1 293.94 23.08 0 16 -1 312 26.75 0 16 1 292.95 26.41 0 -16 1 284.59 30.62 0 16 1 286.06 22.87 0 -16 -1 289.03 32.55 0 -16 1 242.85 25.8 0 16 2 10.49 5.54 0 16 -2 13.04 4.61 0 -16 2 14.24 6.33 0 16 -2 15.67 5.98 0 16 2 16.22 5.01 0 -16 2 15.66 7.45 0 16 3 380.86 26.82 0 16 3 374.89 30.01 0 16 -3 366.77 29.05 0 -16 3 316.38 27.56 0 16 -3 354.43 25.97 0 -16 3 410.96 36.91 0 -16 4 33.77 10.43 0 -16 4 29.06 7.64 0 16 -4 35.81 7.42 0 16 -4 24.16 6.94 0 16 4 27.65 7.8 0 16 4 34.68 7.71 0 16 5 80.46 13.27 0 16 -5 109.02 12.46 0 -16 5 82.81 15.56 0 16 -5 83.17 12.86 0 16 5 73.75 11.68 0 16 -6 60.26 10.34 0 16 -6 55.87 8.98 0 -16 6 61.71 13.36 0 16 6 62.71 10.4 0 16 6 65.33 11.95 0 16 7 185.08 18.42 0 16 -7 187.23 18.95 0 -16 7 174.55 22.48 0 16 -7 185.1 16.7 0 16 7 196.79 21.25 0 16 -8 18.26 5.74 0 16 -8 12.14 4.07 0 16 8 18.45 6.04 0 16 8 22.69 6.3 0 -16 8 21.35 7.39 0 16 9 48.21 10.62 0 16 9 44.24 8.59 0 -16 9 36.34 9.33 0 16 -9 43.22 8.34 0 16 10 -0.18 2.86 0 -16 10 -0.31 1.85 0 16 10 -0.49 1.57 0 16 -10 -1.75 1.98 0 16 11 -1.97 3.06 0 16 11 3.74 2.88 0 -16 11 -0.74 3.65 0 16 -11 -0.93 2.35 0 16 12 53.79 11.48 0 -16 12 43.37 9.7 0 16 12 54.81 10.34 0 16 13 170.56 21.11 0 16 13 184.85 20.19 0 -16 13 171.06 19.57 0 16 14 24.28 7.1 0 -16 14 10.52 4.9 0 -16 15 5.24 3.6 0 -16 16 20.38 6.73 0 -16 17 10.98 4.88 0 17 0 12.79 5.01 0 -17 0 0.37 2.34 0 17 0 3.94 5.03 0 17 1 138.56 18.03 0 -17 -1 138.06 22.8 0 17 -1 108.31 16.37 0 17 1 114.88 14.2 0 -17 1 119.87 20.07 0 17 -1 119.04 14.29 0 17 2 70.38 12.62 0 -17 -2 67.39 16.29 0 17 -2 56.17 9.68 0 17 -2 65.41 12.23 0 17 2 54.84 9.88 0 -17 2 53.45 12.71 0 17 -3 84.56 12.05 0 17 3 96.27 15.31 0 -17 3 69.03 15 0 17 3 95.91 12.89 0 17 -3 94.36 14.6 0 17 4 24.83 8.04 0 17 4 28.52 7.15 0 17 -4 31.8 7.36 0 -17 4 24.8 9.17 0 17 -4 27.68 7.66 0 -17 5 228.09 27.15 0 17 5 223.33 20.57 0 17 -5 187.06 18.82 0 17 5 226.1 23.84 0 17 -5 201.76 21.63 0 17 -6 33.89 8.2 0 -17 6 31.5 9.88 0 17 6 39.01 8.48 0 17 6 23.38 7.69 0 17 7 37.99 8.46 0 -17 7 41.99 11.1 0 17 7 49.72 11.26 0 17 -7 39.67 8.84 0 17 8 108.43 16.64 0 17 8 110.37 14.55 0 -17 8 122.06 18.63 0 17 -8 119.48 14.93 0 -17 9 38.03 9.99 0 17 -9 58.41 9.94 0 17 9 62.58 12.52 0 17 9 51.45 9.89 0 17 10 6.34 2.84 0 17 10 6.81 4.19 0 -17 10 3.56 1.56 0 17 -10 8.41 3.33 0 17 11 321.18 29.85 0 -17 11 277.31 27.54 0 17 11 350.15 27.96 0 17 12 87.29 13.71 0 -17 12 83.26 14.18 0 17 12 58.31 12.75 0 17 13 6.63 3.25 0 17 13 8.62 3.51 0 -17 13 13.47 5.14 0 -17 14 31.59 8.22 0 -17 15 68.83 12.24 0 -17 16 1.97 2.76 0 -18 0 662.16 52.73 0 18 0 662.54 44.87 0 18 0 621.78 37.84 0 18 -1 31.2 8.93 0 18 1 38.81 9.82 0 -18 -1 42.69 13.87 0 -18 1 39.83 12.31 0 18 -1 34.1 8.06 0 18 1 34.97 7.97 0 18 -2 4.97 3.27 0 -18 -2 3.95 4.49 0 -18 2 2.66 3.23 0 18 -2 14.73 6.24 0 18 2 2.38 2.38 0 18 2 8.4 5.27 0 18 3 43.35 10.58 0 18 -3 66.37 12.76 0 -18 3 54.24 13.41 0 18 3 52.24 9.78 0 18 -3 56.24 10 0 18 -4 83.89 12.61 0 18 4 106.82 16.63 0 18 4 102.71 13.72 0 18 -4 94.08 14.96 0 -18 4 96.21 18.07 0 18 -5 90.65 14.7 0 18 -5 81.78 12.23 0 -18 5 104.78 18.7 0 18 5 89.4 15.46 0 18 5 93.43 13.43 0 -18 6 379.74 36.49 0 18 -6 343.4 27.19 0 18 6 396.69 28.98 0 18 -6 424.12 32.58 0 18 6 402.02 33.78 0 18 7 102.95 14.17 0 -18 7 90.37 16.81 0 18 -7 92.86 14.11 0 18 7 75.38 14.05 0 -18 8 4.45 4.4 0 18 8 4.7 3.73 0 18 -8 3.89 3.42 0 18 8 7.51 5.47 0 18 9 51.9 10.19 0 -18 9 37.63 10.52 0 18 9 40.82 10.11 0 18 -9 31.83 7.83 0 18 10 90.76 13.54 0 -18 10 76.48 14.64 0 18 10 78.42 14.48 0 -18 11 6.56 3.99 0 18 11 8.68 4.17 0 18 11 16.95 6.49 0 18 12 115.28 16.44 0 -18 12 110.74 16.96 0 -18 13 178.67 21.09 0 -18 14 59.96 11.82 0 -18 15 47.1 10.42 0 19 0 3.25 4.57 0 -19 0 5.55 5.64 0 19 0 2.64 2.48 0 19 -1 55.48 12.22 0 -19 -1 31.52 11.26 0 19 -1 43.14 8.94 0 19 1 55.28 12.5 0 -19 1 56.95 14.68 0 19 1 43.09 9.06 0 -19 2 290.94 34.01 0 19 2 326.75 30.94 0 19 -2 275.2 23.91 0 -19 -2 366.68 42.04 0 19 2 311.14 25.34 0 19 -2 293.54 29.15 0 -19 -3 37.81 14.32 0 19 3 27.86 9.54 0 19 -3 17.15 5.25 0 -19 3 22.41 8.36 0 19 -3 24.03 8.52 0 19 3 18.05 6.36 0 19 -4 93.16 15.48 0 19 4 88.95 15.59 0 -19 4 93.85 18.65 0 19 4 91.34 13.34 0 19 -4 83.71 12.62 0 -19 5 7.84 4.25 0 19 5 9.47 4.46 0 19 -5 16.69 6.52 0 19 5 20.04 7.36 0 -19 6 9.16 5.5 0 19 6 15.47 6.74 0 19 6 18.01 6.06 0 19 -6 18.53 6.75 0 19 7 29.76 7.93 0 -19 7 21.61 9.17 0 19 7 24.45 8.27 0 19 -7 33.1 8.36 0 19 8 249.3 23.34 0 19 -8 232.16 22.82 0 -19 8 208.94 26.46 0 19 8 231.84 26.24 0 -19 9 13.8 5.15 0 19 9 19.23 6.24 0 19 -9 13.52 5.2 0 19 10 170.03 19.76 0 -19 10 168.29 22.25 0 -19 11 39.98 10.33 0 -19 12 58.55 12.31 0 -19 13 2.58 2.1 0 -19 14 50.62 11.09 0 -20 0 244.82 33.36 0 20 0 255.38 28.08 0 20 0 214.31 21.15 0 20 1 2.25 3.06 0 20 -1 -1.63 2.14 0 20 1 1.27 3.85 0 -20 -1 -5.15 5.19 0 20 -1 6.93 5.05 0 20 2 45.37 9.4 0 20 -2 43.34 11.48 0 20 -2 47.31 9.78 0 -20 -2 44.2 14.93 0 20 2 45.82 11.66 0 -20 2 51.27 14.54 0 20 3 16.36 5.57 0 -20 -3 30.24 12.34 0 20 -3 35.44 10.46 0 -20 3 26.49 9.61 0 20 3 33.04 9.97 0 -20 -4 189.42 35.41 0 20 4 159.42 22.08 0 20 4 130.64 16.46 0 -20 4 185.33 26.49 0 20 -4 163.13 21.34 0 20 5 10.63 3.9 0 -20 5 3.07 3.49 0 20 5 4.3 5.26 0 -20 6 297.5 33.55 0 20 -6 246.78 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61.76 -1 -3 -4 1680.63 59.94 -1 3 4 1797.15 62.09 1 -3 4 1832.39 56.89 1 3 -4 1775.06 66.04 -1 -3 -3 156.65 9.57 -1 3 3 153.01 10.97 1 -3 3 149.82 7.81 1 -3 3 138.9 10.37 1 3 -3 130.88 11.63 -1 -3 -2 2989.28 89.3 1 -3 2 2973.16 87.91 1 -3 2 2671.32 92.72 -1 3 2 2832.53 93.64 1 3 -2 2774.75 95.44 -1 3 1 103.87 8.76 1 -3 1 101.14 6.26 1 3 -1 95.7 4.67 -1 -3 -1 107.89 6.3 1 -3 1 95.11 8.6 -1 -3 0 1095.17 32.01 1 3 0 906.19 31.64 -1 3 0 1050.53 38.71 1 -3 0 954.91 38.26 -1 -3 0 923.24 34.58 1 3 1 105.46 6.55 -1 3 -1 123.66 9.73 -1 -3 1 113.41 7.31 -1 -3 1 116.18 5.28 -1 -3 2 3052.84 86.23 -1 3 -2 2947.44 92.43 -1 3 -2 2795.63 86.83 -1 -3 3 151 7.66 -1 3 -3 154.62 9.25 1 3 3 127.2 8.8 -1 3 -3 165.45 12.08 -1 3 -4 1817.51 62.12 -1 -3 4 1866.71 55.08 1 3 4 1724.8 60.16 -1 3 -4 1701.58 59.51 1 -3 -4 1790.14 57.72 -1 3 -4 1904.28 64.99 1 -3 -5 695.74 26.26 -1 3 -5 670.84 28.68 1 3 5 706.57 28.72 -1 3 -5 706.7 31.77 -1 -3 5 704.33 23.57 -1 3 -5 699.96 28.65 1 3 6 211.54 13.12 -1 -3 6 203.05 9.96 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1 5 -4 1127.67 51.43 -1 5 4 1212.95 47.11 1 5 -4 1273.69 40.97 1 5 -3 3.16 1.65 1 5 -3 4.99 1.83 -1 5 3 2.47 1.44 1 -5 3 1.08 1.07 -1 -5 -3 3.76 1.75 1 -5 3 1.59 0.97 1 -5 2 1830.3 65.2 -1 -5 -2 1904.12 64.13 1 5 -2 2032.56 59.69 -1 5 2 1929.66 69.15 1 5 -2 1831.02 63.05 1 -5 2 1891.21 69.1 1 5 -1 17.72 3.28 -1 5 1 26.13 4.92 1 5 -1 19.9 2.47 1 -5 1 24.05 4.31 -1 -5 -1 19 3.13 1 -5 1 17.21 4.07 -1 -5 -1 16.56 3.4 1 5 0 14.56 3.06 -1 5 0 10.23 2.96 1 -5 0 10.69 3.27 -1 -5 0 14.24 2.35 1 5 0 17.09 2.45 -1 -5 0 12.94 2.75 1 5 1 24.06 3.14 -1 -5 1 28.38 3.85 -1 -5 1 24.45 3.05 1 5 1 21.57 3.97 1 -5 -1 22.26 4.84 -1 5 -1 28.7 5.07 1 5 2 2102.68 65.83 -1 5 -2 1981.29 72.44 1 5 2 1933.94 68.73 1 -5 -2 1970.13 74.02 -1 -5 2 2055.19 62.88 1 5 3 2.42 1.4 1 5 3 3.06 1.72 -1 -5 3 0.58 0.71 1 -5 -3 1.51 1.53 -1 5 -3 1.96 1.57 -1 5 -3 2.73 1.32 -1 5 -4 1142.21 45.74 -1 -5 4 1104.37 48.34 1 5 4 1163.01 44.94 -1 5 -4 1227.31 48.54 1 5 4 1191.18 42.52 -1 5 -5 15.31 3.68 -1 5 -5 8.28 2.98 1 5 5 12.96 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5.83 -2 13 17 137.62 17.69 2 -13 17 149.42 14.9 -2 13 17 144.66 18.13 -2 13 16 49.72 10.29 -2 13 16 51 10.42 2 -13 16 48.36 8.15 -2 13 15 147.58 17.64 2 -13 15 166.24 15 -2 13 15 131.45 16.96 -2 13 14 208.44 20.93 2 -13 14 230.82 17.61 -2 13 13 29.3 8 2 -13 13 21.56 5.28 -2 13 13 19.49 7.12 -2 13 12 20.13 5.84 -2 13 12 28.27 7.51 2 -13 12 29.18 5.9 -2 13 11 229.54 21.76 -2 13 11 249.22 23.03 2 -13 11 283.91 20.01 -2 13 10 9.02 4.5 2 -13 10 6.41 3.53 -2 13 10 2.73 1.11 -2 13 9 42.15 8.35 2 -13 9 51.54 8.06 -2 13 9 55.49 10.6 2 -13 8 526.77 37.05 -2 13 8 441.27 32.7 2 13 -8 521.25 18.06 2 13 -8 528.12 18.55 2 -13 8 518.58 30.31 2 -13 7 275.7 25.93 2 13 -7 256.18 13.11 2 -13 7 270.59 21.29 -2 13 7 309.76 25.82 2 13 -7 291.25 12.56 -2 13 6 17.99 5.97 2 -13 6 17.27 6.52 2 -13 6 12.58 4.53 2 13 -6 23.73 3.18 2 -13 5 183.84 21.41 2 13 -5 204.3 11.49 2 -13 5 182.41 17.82 -2 13 5 164.24 18.73 -2 -13 -5 161.88 18.92 2 -13 4 35.97 9.24 2 -13 4 28.04 6.58 2 13 -4 35.34 4.66 -2 -13 -4 25.82 6.69 -2 13 4 29.12 7.37 2 -13 3 2.78 2.85 -2 -13 -3 -2.78 2.41 2 13 -3 4.23 1.96 -2 13 3 2.12 2.51 2 -13 2 374.05 32.73 -2 -13 -2 372.8 28.18 -2 13 2 400.43 29.83 2 13 -2 397.43 20.61 -2 13 1 334.71 27.42 2 -13 1 297.02 29.64 -2 -13 -1 318.81 25.27 2 13 -1 336.14 19.11 2 -13 0 6.92 5.5 -2 -13 0 7.96 5.74 2 13 0 8.63 2.83 -2 13 0 1.04 2.17 -2 -13 0 5.35 3.67 -2 -13 1 327.34 23.09 -2 13 -1 344.98 28.6 -2 -13 1 359.93 33.74 2 13 1 332.79 20.28 -2 -13 2 307.84 31.64 2 13 2 349.15 21.38 -2 -13 2 350 22.34 -2 13 -2 382.96 30.18 -2 13 -3 5.55 3.69 2 13 3 0.26 0.67 -2 -13 3 0.07 3.58 -2 -13 3 3.41 2.4 -2 -13 4 56.31 6.38 2 13 4 56.4 8.33 -2 -13 4 55.48 13.03 -2 13 -4 54.47 11.03 -2 -13 5 207.34 10.34 2 13 5 192.22 16.6 -2 13 -5 162.34 19.88 2 13 6 28.2 6.15 -2 13 -6 36.16 9.01 -2 -13 6 17.18 7.11 -2 13 -7 265.5 26.34 2 13 7 288.12 21.94 -2 -13 7 284.87 29.82 -2 -13 8 508.55 40.43 2 13 8 530.91 31.67 -2 13 -8 467.08 36.63 -2 -13 9 58.05 12.69 2 13 9 62.72 10.06 -2 13 -9 40.09 10.13 -2 -13 10 11.33 5.89 2 13 10 7.6 2.94 -2 13 -10 7.05 3.92 -2 13 -11 264.42 28.11 2 13 11 264.13 22.33 -2 -13 11 284.12 27.43 -2 -13 12 16.34 5.28 2 13 12 25.73 6.92 -2 13 -12 34.07 10.24 -2 -13 13 7.36 4.61 2 13 13 22.98 6.47 -2 13 -13 18.26 7.82 2 13 14 202.26 19.8 -2 -13 14 208.03 22.09 -2 13 -14 157.85 23.38 2 13 15 171.3 18.58 -2 -13 15 152.93 18.64 -2 13 -15 159.95 24.64 2 13 16 68.95 11.69 -2 -13 16 60.25 11.3 -2 13 -16 46.6 13.45 2 13 17 166.38 19.12 -2 -13 17 171.14 19.18 -2 -13 18 19.27 5.97 -2 14 19 104.48 16.26 2 -14 19 134.86 14.94 -2 14 18 31.86 8.24 2 -14 18 32.81 6.75 -2 14 17 6.85 3.48 2 -14 17 3.8 2.15 -2 14 16 34.24 8.96 -2 14 16 41.45 9.77 2 -14 16 32.73 6.94 -2 14 15 8.81 4.26 -2 14 15 12.34 4.51 -2 14 14 17.91 6.57 -2 14 14 13.56 5.7 2 -14 14 10.9 3.88 -2 14 13 381.14 30.45 -2 14 13 393.66 30.53 2 -14 13 421.1 25.77 -2 14 12 58.45 11.06 -2 14 12 51.67 10.36 2 -14 12 52.99 8.51 -2 14 11 20.08 7.11 -2 14 11 24.88 6.3 2 -14 11 27.75 6.19 -2 14 10 106.02 14.52 2 -14 10 107.18 12.44 -2 14 10 113.9 15.56 -2 14 9 199.13 20.34 2 -14 9 263.45 20.5 -2 14 9 216.86 21.91 -2 14 8 1.26 1.33 2 14 -8 6.1 1.37 2 -14 8 2.53 1.58 -2 14 8 3.16 2.95 2 -14 7 226.17 24.15 -2 14 7 231.64 22.92 2 -14 7 233.49 20.46 2 14 -7 271.04 12.55 2 -14 6 1.76 2.5 -2 14 6 -0.22 2.76 2 14 -6 2.67 1.06 2 -14 6 -0.04 1.17 2 -14 5 150.27 19.95 -2 14 5 174.08 19.41 2 -14 5 183.15 18.6 2 14 -5 168.17 11.06 -2 14 4 25.69 7.71 2 -14 4 29.51 7.76 2 14 -4 21.93 3.89 -2 -14 -4 26.63 7.51 -2 14 4 21.38 7.03 2 -14 3 654.41 40.11 2 14 -3 662.41 28.92 -2 14 3 641.61 40.3 -2 -14 -3 565.93 38.76 -2 14 2 187.52 20.19 2 -14 2 192.23 20.6 -2 -14 -2 158.65 18.67 2 14 -2 194.1 13.74 -2 -14 -1 304.58 25.75 2 14 -1 317.18 19.09 -2 -14 -1 282.3 33.56 2 -14 1 348.92 28.62 -2 14 1 273.47 25.34 -2 -14 0 24.55 9.39 2 -14 0 15.26 5.22 2 14 0 27 5.21 -2 14 0 28.67 7.52 -2 -14 0 24.62 6.9 2 14 1 320.55 20.34 2 -14 -1 312.58 28.67 -2 -14 1 297.27 31.7 -2 14 -1 305.34 27.05 -2 -14 1 295.85 22.72 -2 -14 2 163.72 22.66 2 14 2 181.52 15.06 -2 14 -2 156.2 19.11 -2 -14 2 145.68 14.38 -2 -14 3 669.56 48.57 -2 -14 3 548.06 29.76 2 14 3 692.46 33.65 -2 14 -3 590.66 40.47 -2 -14 4 21.28 4.06 2 14 4 33.14 6.51 -2 -14 4 23.22 8.41 -2 14 -4 30.08 8.38 -2 -14 5 152.92 9.32 -2 -14 5 173.79 23.86 2 14 5 141.29 14.42 -2 14 -5 151.96 19.32 2 14 6 1.04 1.15 -2 -14 6 1.93 2.83 -2 14 -6 4 3.27 -2 -14 7 276.33 29.76 2 14 7 237.35 20.14 -2 14 -7 226.08 24.47 -2 -14 8 2.21 3.12 -2 14 -8 1.4 1.29 2 14 8 0.74 1.75 -2 -14 9 275.68 29.33 2 14 9 277.45 22.9 -2 14 -9 265.19 27.39 2 14 10 89.5 12.71 -2 -14 10 113.56 18.11 -2 14 -10 110.88 17.6 2 14 11 22.53 6.08 -2 14 -11 16.88 6.93 -2 -14 12 46.69 10.66 2 14 12 50.6 9.73 -2 14 -12 52.92 12.35 -2 14 -13 407.1 37.9 2 14 13 483.11 32.38 -2 -14 13 400.32 33.65 2 14 14 3.89 2.8 -2 -14 14 10.33 4.41 -2 14 -14 6.11 5.68 2 14 15 30.63 7.77 -2 -14 15 25.15 7.9 2 14 16 51.58 10.72 -2 -14 16 37.28 9.04 -2 -14 17 18.28 6.41 -2 15 17 105.42 16.44 2 -15 17 145.85 15.03 -2 15 16 60.37 12.14 2 -15 16 65.95 9.79 -2 15 15 56.23 11.46 2 -15 15 71.56 10.04 -2 15 15 50.37 10.54 2 -15 14 10.36 4.15 -2 15 14 6.69 4.17 -2 15 14 5.77 3.81 -2 15 13 5.78 4.07 -2 15 13 7.54 4.9 2 -15 13 16.04 4.76 -2 15 12 23.1 6.87 -2 15 12 18.8 7.47 2 -15 12 19.96 5.3 -2 15 11 350.48 29.44 -2 15 11 413 31.72 2 -15 11 435.81 27.53 2 -15 10 17.19 4.91 -2 15 10 35.52 8.79 -2 15 10 23.63 6.96 -2 15 9 79 13.19 -2 15 9 71.52 12.25 2 -15 9 74.54 11.07 -2 15 8 -3.11 2.86 2 -15 8 3.32 2.52 -2 15 8 4.16 4.01 -2 15 7 145.42 18.09 -2 15 7 125.8 16.11 2 15 -6 41.12 4.9 -2 15 6 23 6.89 2 -15 6 38.46 8.59 2 -15 5 569.24 36.36 2 15 -5 521.15 23.64 -2 15 4 5.97 1.62 2 -15 4 7.2 3.61 2 15 -4 10.39 2.9 -2 -15 -4 7.59 4.18 -2 -15 -3 83.75 14 2 -15 3 104.93 15.3 -2 15 3 110.86 15.43 2 15 -3 109.42 10.04 -2 15 2 0.17 1.22 2 -15 2 5.23 4.08 2 15 -2 1.65 0.58 -2 -15 -2 3.44 3.31 2 15 -1 308.52 19.19 -2 -15 -1 312.83 36.46 2 -15 1 264.71 26.17 -2 15 1 246.12 24.05 -2 -15 -1 257.48 24.58 2 15 0 88.33 9.99 2 -15 0 72.43 13.51 -2 -15 0 59.92 15.02 -2 15 0 79.09 13.32 -2 -15 0 74.56 12.01 -2 15 -1 267.27 25.51 2 -15 -1 288.84 28.6 -2 -15 1 249.29 29.97 -2 -15 1 254.13 21.6 2 15 1 299.23 20.11 2 15 2 5.68 2.75 -2 -15 2 7.25 4.9 -2 -15 2 3.77 2.62 -2 15 -2 10.11 5.11 -2 -15 3 104.8 19.04 -2 -15 3 94.96 10.71 2 15 3 111.63 12.37 -2 15 -3 90.19 14.74 2 15 4 15.21 4.61 -2 -15 4 11.05 5 -2 15 -4 18.32 6.76 -2 -15 5 492.95 42.4 2 15 5 475.62 29.47 -2 15 -5 436.76 35.19 2 15 6 39.32 7.97 -2 -15 6 29.8 9.76 -2 15 -6 28.87 8.46 -2 -15 7 187.22 25.17 2 15 7 202.46 18.85 -2 15 -7 200.59 23.21 -2 -15 8 0.49 3.81 -2 15 -8 3.47 3.54 2 15 8 0.33 2.03 2 15 9 91.72 13.03 -2 -15 9 88.96 16.83 -2 15 -9 99.82 16.58 -2 15 -10 30.84 9.16 2 15 10 26.92 6.9 -2 -15 10 26.41 8.81 -2 15 -11 339.21 33.42 2 15 11 390.96 29.27 -2 -15 11 402.37 35.62 -2 15 -12 9.38 5.98 -2 -15 12 24.47 8.27 2 15 12 14.52 5.82 2 15 13 9.23 4.76 -2 -15 13 13.77 6.59 -2 15 -13 9.68 5.15 -2 -15 14 4.02 3.03 2 15 14 11.49 4.82 2 15 15 80.12 13.03 -2 -15 15 57.17 12.05 -2 -15 16 82.38 14.12 2 -16 15 58.3 9.31 -2 16 15 50.78 11.48 -2 16 14 48.15 10.92 -2 16 14 75.25 13.59 2 -16 14 60.7 9.48 -2 16 13 302.37 27.13 2 -16 13 282.09 21.58 -2 16 12 30.41 8.9 -2 16 12 40.89 9.54 2 -16 12 38.13 7.69 -2 16 11 38.55 9.64 -2 16 11 45.39 10.44 2 -16 11 36.83 7.7 -2 16 10 7.97 5.2 2 -16 10 3.22 2.74 -2 16 9 149.21 18.68 2 -16 9 211.25 19.54 -2 16 9 194.45 21.2 -2 16 8 19.4 6.34 2 -16 8 14.75 5.1 -2 16 8 11.22 5.32 -2 16 7 136.43 17.45 -2 16 7 130.86 17.55 2 -16 7 147.47 17.14 -2 16 6 110.8 15.89 -2 16 6 102.05 14.6 2 -16 6 105.82 14.9 -2 16 5 67.08 12.12 2 -16 5 71.98 12.54 2 16 -5 81.54 7.96 -2 16 5 49.13 10.7 -2 16 4 26.18 7.75 2 16 -4 25.33 4.75 2 -16 4 19.17 6.63 2 -16 3 266.74 25.99 2 16 -3 224.38 15.53 -2 -16 -2 61.12 18.05 2 -16 2 41.87 10.17 2 16 -2 51.28 7.36 -2 -16 -2 56.15 11.64 -2 16 2 42.65 9.48 2 -16 1 146.34 19.92 -2 -16 -1 141.81 25.21 2 16 -1 168.21 14.22 -2 16 1 151.55 18.58 -2 -16 -1 152.13 19.19 -2 -16 0 227.79 30.32 2 -16 0 222.88 25.15 2 16 0 213.33 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169.69 8.73 -4 4 -10 168.09 13.79 4 4 10 164.87 19.7 4 -4 -10 161.69 21.27 -4 4 -11 77.46 13.7 -4 -4 11 70.35 5.36 4 -4 -11 87.64 12.4 -4 4 -11 68.55 8.96 -4 -4 11 76.14 10.02 4 4 11 83.15 14 -4 4 -12 230.32 25.13 -4 -4 12 313.96 13.73 -4 4 -12 269.08 20.21 4 4 12 273.13 27.59 -4 -4 12 303.04 21.39 -4 -4 13 318.31 13.59 -4 4 -13 297.29 29.33 -4 -4 13 429.09 17.06 -4 4 -13 367.69 24.83 4 4 13 402.89 34.65 -4 -4 13 417.39 25.23 -4 -4 14 183.62 10.72 -4 -4 14 177.06 15.76 -4 4 -14 144.19 15.54 4 4 14 165.54 22.85 -4 4 -15 13.35 6.51 -4 -4 15 18.75 3.57 -4 -4 15 19.91 5.1 4 4 15 24.45 8.38 -4 4 -16 39.67 10.63 -4 -4 16 50.18 8.38 4 4 16 49.29 12.35 -4 -4 16 49.2 6.03 -4 4 -17 61.1 14.19 -4 -4 17 74.79 8 4 4 17 69.29 14.89 -4 -4 17 60.99 9.7 -4 4 -18 64.54 14.75 -4 -4 18 80.78 11.33 4 4 18 98.21 18.36 -4 4 -19 49.44 12.83 -4 -4 19 67.45 10.52 -4 4 -20 62.76 15.44 4 4 20 69.18 16.01 -4 -4 20 66.07 10.5 -4 4 -21 6.42 5.15 4 4 21 8.96 7.23 -4 -4 21 8.93 3.99 -4 4 -22 1.42 2.59 -4 5 23 67.32 11.73 -4 5 22 33.19 7.87 -4 5 21 232.39 22.5 -4 5 20 39.89 8.66 -4 5 19 0.23 2.15 -4 5 18 25.1 5.46 -4 5 18 19.99 5.57 -4 5 17 158.48 14.24 -4 5 17 228.92 19.59 -4 5 16 170.72 16.83 -4 5 15 306.61 23.2 -4 5 14 109.17 12.94 4 5 -14 97.78 12.57 -4 5 13 53.19 9.15 4 5 -13 44.34 7.93 -4 5 12 34.45 7.11 4 5 -12 31.51 6.17 -4 5 11 525.27 31.56 4 5 -11 478.71 26.29 -4 5 10 256.34 21.41 -4 5 10 271.35 22.36 4 5 -10 274.56 17.55 -4 5 9 191.96 18.68 4 5 -9 215.1 14.31 -4 5 8 6.24 3.39 4 5 -8 6.5 2.2 4 5 -8 13.81 5.85 -4 -5 -8 9.94 3.71 4 5 -7 313.02 16.55 4 5 -7 327.93 29.97 -4 -5 -7 342.51 21.38 -4 5 7 293.89 24.22 -4 5 6 364.65 27.52 4 5 -6 356.06 17.96 4 5 -6 385.04 32.02 -4 -5 -6 383.06 22.13 4 -5 5 1093.15 55.79 4 5 -5 1068.2 58.77 -4 -5 -5 1190.57 45.61 -4 5 5 970 52.32 4 -5 4 334.59 27.16 -4 -5 -4 367.47 20.19 -4 5 4 316.08 26.19 4 -5 3 59.34 10.84 -4 5 3 78.04 12.2 -4 -5 -2 8.33 3.53 -4 5 2 3.69 2.9 -4 -5 -1 656.17 32.55 -4 -5 -1 642.58 26.95 -4 -5 0 180.69 14.67 -4 5 0 191.53 19.98 -4 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23.13 4 -5 -7 313.85 19.36 4 5 7 323.01 23.92 4 -5 -7 274.37 27.46 -4 5 -7 276.77 27.37 -4 5 -8 2.71 1.4 4 -5 -8 3.43 2.11 -4 5 -8 5.86 2.29 -4 -5 8 3.85 1.27 -4 5 -8 10.24 3.43 4 -5 -8 4.46 1.24 4 5 8 2.87 1.9 -4 5 -9 168.12 21.46 -4 5 -9 199.82 15.06 -4 -5 9 178.46 17.02 4 -5 -9 173.9 15.68 4 5 9 185.19 19.79 4 -5 -9 177.58 22.46 -4 5 -10 228.46 25.03 -4 -5 10 211.23 8.82 -4 5 -10 247.87 18.34 -4 -5 10 233.81 19.4 4 -5 -10 230.28 19 4 5 10 206.18 21.79 -4 5 -11 484.34 39.13 -4 5 -11 534.1 31.66 -4 -5 11 579.99 33.04 4 -5 -11 562.51 33.65 4 5 11 648.52 41.71 -4 -5 11 582.44 20.47 -4 -5 12 45.32 4.06 -4 5 -12 37.83 10.31 -4 -5 12 42.93 7.96 -4 5 -12 37.23 7.82 -4 -5 12 50.56 4.41 4 5 12 38.49 9.66 -4 5 -13 42.95 10.92 -4 5 -13 21.99 6.4 -4 -5 13 56.14 5.27 -4 -5 13 47.66 8.37 4 5 13 43.56 11.07 -4 5 -14 96.47 16.81 -4 5 -14 89.8 13.62 -4 -5 14 109.68 8.47 -4 -5 14 95.44 11.96 4 5 14 93.31 16.28 -4 -5 15 331.65 23.33 -4 -5 15 339.55 17.85 4 5 15 292.24 30.3 -4 5 -16 127.46 20.54 -4 -5 16 177.37 13.11 4 5 16 199.02 25 -4 -5 16 168.25 16.31 -4 5 -17 194.55 26.04 4 5 17 251.43 28.53 -4 -5 17 230.44 19.72 -4 5 -18 17.17 8.81 4 5 18 48.96 12.78 -4 -5 18 41.45 8.19 -4 5 -19 3.72 5.03 4 5 19 3.13 3.27 -4 -5 19 0.32 1.1 -4 5 -20 30.01 10.95 4 5 20 43.51 12.31 -4 -5 20 40.69 8.39 -4 5 -21 170.44 27.23 -4 -5 21 251.83 22.24 -4 5 -22 30.37 12.02 -4 6 23 100.69 14.68 -4 6 22 53 10.97 -4 6 21 40.79 9.58 -4 6 20 30.36 7.84 -4 6 19 178.35 18.95 -4 6 18 38.89 6.9 -4 6 18 27.16 6.84 -4 6 17 43.54 7.45 -4 6 17 42.57 8.02 -4 6 16 83.45 11.83 -4 6 15 210.56 19.35 -4 6 14 74.54 11.08 4 6 -14 73.97 9.77 -4 6 13 580.6 34.62 4 6 -13 558.84 29.11 -4 6 12 233.57 20.49 4 6 -12 231.43 15.71 -4 6 11 186.78 17.98 4 6 -11 147.39 11.07 -4 6 10 176.93 17.96 -4 6 10 187.88 18.77 4 6 -10 181.1 11.03 4 6 -9 622.68 23.44 -4 6 9 565.29 36.07 -4 -6 -8 320.11 22 -4 6 8 306.64 24.96 4 6 -7 351.09 32.03 -4 -6 -7 339.33 22.33 -4 6 7 309.31 25.53 4 -6 6 40.2 9.15 4 6 -6 56.13 12.3 -4 -6 -6 62.73 8.53 -4 6 6 54.97 10.22 4 -6 5 9.66 4.78 -4 6 5 14.35 4.84 -4 -6 -5 18.48 4.27 4 -6 4 94.35 14.19 -4 -6 -4 111.86 10.83 -4 6 4 76.03 12.46 4 -6 3 1009.77 55.43 -4 -6 -3 1170.74 45.68 -4 6 3 1069.56 55.65 4 -6 2 330.3 28.62 -4 -6 -2 392.2 21.16 -4 6 2 382.95 29.52 -4 -6 -1 852.94 37.9 4 6 -1 766.4 32.8 -4 -6 -1 773.58 33.2 -4 6 1 766.9 45.45 4 -6 1 762.42 46.15 4 -6 0 17.45 5.9 -4 -6 0 32.12 5.85 -4 -6 0 30.54 7.58 4 6 0 20.64 4.24 -4 -6 0 28.77 4.5 -4 6 0 20.59 6.62 -4 -6 1 749.35 32.84 -4 -6 1 705.13 42.03 -4 -6 1 634.62 27.88 4 6 1 744.53 32.4 -4 6 -1 733.52 44.21 4 -6 -1 619.29 42.27 -4 -6 2 342.86 27.51 -4 -6 2 327.34 16.19 4 -6 -2 356.9 14.47 4 6 2 332.18 20.2 -4 6 -2 385.67 30.69 4 -6 -2 339.26 29.88 -4 -6 2 347.57 19.39 -4 -6 3 1044.62 53.79 -4 -6 3 951.05 35.63 4 -6 -3 1055 36.5 4 6 3 1084.92 44.63 -4 -6 3 1114.85 41.42 -4 6 -3 1145.09 58.99 4 -6 -3 1145.75 60.14 -4 -6 4 55.5 10.28 -4 -6 4 61.28 4.55 4 -6 -4 61.12 6.01 4 6 4 62.52 8.74 -4 -6 4 72.83 6.65 4 -6 -4 79.81 14.36 -4 6 -4 84.01 14.23 -4 6 -5 9.78 4.58 -4 -6 5 5.62 2.75 4 6 5 17.36 4.8 4 -6 -5 14.24 3.14 -4 -6 5 11.16 2.12 -4 -6 5 9.21 1.13 4 -6 -5 8.41 3.81 -4 6 -6 51.42 11.49 -4 6 -6 39.34 4.88 -4 -6 6 25.9 7.04 -4 6 -6 39.19 9.26 4 -6 -6 48.59 6.31 4 -6 -6 38.87 10.17 4 6 6 37.73 7.23 -4 6 -7 269.41 27.94 -4 6 -7 289.75 17.06 -4 -6 7 306.72 24.67 4 -6 -7 292.79 18.27 4 6 7 288.4 22.72 4 -6 -7 265.66 27.92 4 6 8 332.67 25.61 -4 6 -8 344.93 19.96 -4 -6 8 288.65 24.05 4 -6 -8 299.21 19.74 -4 -6 9 561.49 24.98 -4 6 -9 591.9 30.5 -4 -6 9 561.1 34.44 4 -6 -9 553.97 30.05 4 6 9 604.25 37.48 -4 6 -9 645.69 45.08 -4 6 -10 167.99 22.4 -4 -6 10 151.83 10.17 -4 6 -10 192.25 16.45 -4 -6 10 173.18 17.24 4 -6 -10 163.51 15.08 4 6 10 187.47 20.1 -4 6 -11 175.81 22.62 -4 -6 11 156.48 9.51 -4 6 -11 161.54 16.24 -4 -6 11 163.85 16.79 4 -6 -11 178.64 16.44 4 6 11 176.28 20.15 -4 6 -12 213.09 26.01 -4 -6 12 214.37 10.39 -4 6 -12 234.93 21.39 -4 -6 12 246.68 20.49 4 6 12 241.21 24.41 -4 6 -13 587.4 45.75 -4 6 -13 571.86 38.22 -4 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33.25 -4 7 6 329.88 27.38 4 -7 5 762.61 46.04 -4 -7 -5 834.87 37.7 4 -7 4 220.72 23 -4 -7 -4 240.13 17.21 -4 7 4 221.85 22.35 -4 -7 -3 444.4 24.26 -4 7 3 439.54 32.66 4 -7 3 419.06 32.98 4 -7 2 92.27 14.67 -4 -7 -2 89.9 9.31 -4 7 2 98.49 14.6 4 7 -1 564.61 26.16 -4 -7 -1 590.89 27.15 -4 7 1 574.48 38.52 4 -7 1 535.15 38.74 -4 -7 0 512.99 26.65 -4 -7 0 508.14 36.2 4 7 0 478.11 24.17 -4 -7 0 489.59 22.88 -4 7 0 505.43 36.01 4 -7 0 494.2 36.91 -4 -7 1 497.55 25.2 -4 -7 1 451.13 34.24 4 7 1 469.99 24.55 4 -7 -1 499.88 17.2 -4 -7 1 519.98 22.17 -4 7 -1 472.53 35.29 4 -7 -1 520.11 38.32 -4 -7 2 66.36 11.97 4 7 2 71.17 8.34 4 -7 -2 68.44 4.85 -4 -7 2 64.36 5.53 -4 7 -2 65.28 12.21 -4 -7 2 61.41 6.98 4 -7 -2 78.97 14.04 -4 -7 3 425.53 17.13 -4 -7 3 461.75 33.77 4 7 3 466.1 25.02 4 -7 -3 440.57 18.23 -4 7 -3 428.42 34.22 4 -7 -3 470.82 36.91 -4 -7 3 430.7 20.86 -4 -7 4 211.37 22.1 -4 -7 4 198.51 8.68 4 7 4 219.5 16.69 4 -7 -4 198.87 11.53 -4 -7 4 190.62 10.66 4 -7 -4 206.24 24.13 -4 7 -4 234.86 24.69 -4 -7 5 715.54 34.96 -4 -7 5 793.65 46.19 4 7 5 806.19 38.48 4 -7 -5 765.59 30.64 4 -7 -5 777.42 51 -4 7 -5 739.85 48.95 -4 -7 6 374.84 21.16 4 7 6 346.04 24.05 -4 7 -6 409.55 32.17 -4 -7 6 350.72 28.34 4 -7 -6 323.21 18.21 4 -7 -6 349.81 33.03 -4 7 -6 382.88 33.43 -4 -7 7 242.99 15.92 -4 7 -7 291.09 17.16 -4 -7 7 223.52 22.24 4 -7 -7 232.45 15.56 4 7 7 276.31 21.65 -4 7 -7 240.47 26.81 -4 -7 8 259.15 15.75 -4 7 -8 285.38 18.59 -4 -7 8 260.65 23.52 4 -7 -8 296.32 18.28 4 7 8 284.1 23.17 -4 7 -8 254.43 28.04 -4 -7 9 232.66 13.95 -4 7 -9 250.35 18.52 -4 -7 9 223.37 21.25 4 7 9 213.42 20.77 4 -7 -9 237.61 17.03 -4 7 -9 245.59 27.34 -4 -7 10 203.98 12.3 -4 7 -10 213.33 18.26 -4 -7 10 223.39 20.84 4 -7 -10 236.81 17.54 4 7 10 207.98 21.14 -4 7 -10 242.52 27.65 -4 -7 11 494.7 21.13 -4 7 -11 557.18 33.46 -4 -7 11 574.23 34.69 4 -7 -11 503.98 29.04 4 7 11 585.46 38 -4 7 -11 503.43 42.08 4 7 12 31.58 8.05 -4 7 -12 18.33 8.14 -4 7 -12 16.29 5.32 -4 -7 12 10.89 3.81 4 7 13 38.82 9.36 -4 7 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7 7 124.83 17.87 -7 -7 7 135 18.23 -7 -7 7 164.85 12.84 -7 7 -7 172.89 27.05 7 7 8 120.66 18.2 -7 -7 8 120.94 16.94 -7 7 -8 111.28 22.25 7 7 9 177.88 23.28 -7 -7 9 196.14 21.66 -7 7 -9 210.22 30.58 -7 7 -10 14 6.5 7 7 10 26 9.58 -7 -7 10 21.92 6.41 -7 7 -11 24.79 11.19 7 7 11 50.8 13.08 -7 -7 11 29.41 7.8 -7 7 -12 80.8 19.07 -7 -7 12 111.81 15.37 7 7 12 116.72 20.89 -7 7 -13 73.38 18.26 7 7 13 109.19 21.2 -7 -7 13 108.02 15.11 -7 7 -14 99.19 21.56 7 7 14 78.15 18.65 -7 -7 14 108.11 14.89 -7 7 -15 88.86 20.52 7 7 15 104.59 22.53 -7 -7 15 111.87 15.06 -7 -7 16 21.78 6.64 -7 8 17 5.55 4.32 -7 8 16 19.64 6.5 -7 8 15 101.33 15.85 -7 -8 -14 47.8 13.12 -7 8 14 51.41 11.14 -7 8 13 8.58 4.26 -7 -8 -13 8.11 5.46 -7 -8 -12 75.74 15.98 -7 8 12 105.66 17.08 -7 8 12 87.69 16.3 -7 -8 -11 46.18 12.03 -7 8 11 59.6 13.73 -7 -8 -10 22.71 7.94 -7 8 10 31.32 9.96 -7 -8 -9 70.2 14.18 -7 8 9 73.56 15.28 -7 -8 -8 126.69 19.19 -7 8 8 175.45 23.93 -7 -8 -7 30.5 9.25 -7 8 7 29.27 9.4 -7 -8 -6 38.34 9.94 -7 8 6 53.4 12.86 -7 -8 -5 93.83 15.54 -7 -8 -5 100.38 18.08 -7 8 5 84.63 16.74 -7 -8 -4 242.01 25.58 -7 -8 -4 200.69 26.4 -7 8 4 274.75 30.85 -7 -8 -3 111.34 16.65 -7 -8 -3 107.74 18.83 -7 8 3 117.41 19.86 -7 -8 -2 280.67 26.74 -7 -8 -2 298.9 31.38 -7 -8 -2 255.58 20.47 -7 8 2 271.59 31.24 -7 -8 -1 78.68 15.71 -7 -8 -1 76.75 10.58 -7 8 1 100.43 18.76 -7 -8 -1 95.91 14.76 -7 -8 0 3.1 2.99 -7 -8 0 -0.56 1.61 -7 8 0 -0.3 1.6 -7 -8 1 78.56 15.12 -7 -8 1 68.13 9.21 -7 8 -1 75.14 16.36 -7 -8 1 87.5 12.9 -7 -8 2 236.8 27.29 -7 8 -2 307.52 34.88 -7 -8 2 241.13 21.49 -7 -8 3 130.75 19.38 -7 -8 3 113.17 13.57 -7 8 -3 146.38 24.19 -7 -8 4 230.52 26.15 -7 -8 4 210.67 17.69 -7 8 -4 190.77 28.87 -7 -8 5 106.34 17.09 -7 -8 5 80.47 9.59 -7 8 -5 115.05 22.14 7 8 6 58.02 11.71 -7 -8 6 41.73 9.81 -7 8 -6 68.3 17.14 7 8 7 27.47 8.4 -7 -8 7 43.4 10.68 -7 8 -7 41.27 13.47 7 8 8 138.56 19.81 -7 -8 8 182.16 22.04 -7 8 -8 147.03 26.09 7 8 9 103.43 17.36 -7 -8 9 89.71 14.83 -7 8 -9 89.91 20.38 7 8 10 49.68 12.68 -7 -8 10 39.45 9.78 -7 8 -10 38.93 12.9 -7 8 -11 40 14.09 7 8 11 56.44 13.98 -7 -8 11 38.01 9.4 -7 8 -12 96.6 21.18 7 8 12 113.03 21.13 -7 -8 12 93.92 14.97 -7 8 -13 7.68 7.68 7 8 13 17.04 7.65 -7 -8 13 20.06 6.52 -7 8 -14 44.16 14.74 -7 -8 14 44.71 9.84 7 8 15 115.6 23.65 -7 -8 15 108.37 15.67 -7 9 16 41.9 10.1 -7 9 15 20.25 7.37 -7 9 14 43.08 10.92 -7 9 13 5.07 2.17 -7 -9 -12 104.56 18.67 -7 9 12 167.14 23 -7 9 12 128.78 19.52 -7 -9 -11 73.67 15.48 -7 9 11 78.28 15.85 -7 -9 -10 55.95 12.52 -7 9 10 52.37 12.55 -7 -9 -9 17.05 7.23 -7 9 9 12.41 7.09 -7 -9 -8 41.04 10.31 -7 9 8 60.37 13.73 -7 -9 -7 82.69 14.61 -7 9 7 89.64 17.51 -7 -9 -6 360.38 31.62 -7 9 6 413.21 38.74 -7 -9 -5 172 21.2 -7 -9 -5 168.59 24.81 -7 9 5 198.56 26.48 -7 -9 -4 39.29 10.1 -7 -9 -4 64.76 15.16 -7 9 4 51.93 13.51 -7 -9 -3 40.56 9.9 -7 -9 -3 38.69 11.23 -7 9 3 28.03 9.52 -7 -9 -2 -9.7 5.8 -7 9 2 -1.38 3.24 -7 -9 -1 107.34 19 -7 9 1 113.62 20.29 -7 -9 -1 108.01 15.7 -7 -9 0 526.78 44.36 -7 9 0 600.23 49.86 -7 -9 0 547.17 36.66 -7 -9 1 137.38 21.18 -7 9 -1 117.77 21.87 -7 -9 1 111.71 14.27 -7 -9 2 6.56 4.68 -7 9 -2 9.31 6.31 -7 -9 2 10.47 3.93 -7 -9 3 29.51 9.32 -7 9 -3 35.61 11.88 -7 -9 3 34.09 6.59 -7 -9 4 41.96 11.02 -7 9 -4 48.91 14.85 7 9 5 160.93 19.46 -7 -9 5 206.1 25.07 -7 9 -5 165.99 27.82 7 9 6 393.33 32.23 -7 -9 6 429.21 36.77 -7 9 -6 381.88 43.48 -7 -9 7 79.95 15.2 7 9 7 96.07 15.72 -7 9 -7 101.57 21.97 -7 -9 8 67.1 13.47 7 9 8 48.91 11.26 -7 9 -8 39.86 14.43 -7 -9 9 8.49 4.28 7 9 9 8.3 5.55 -7 9 -9 7.23 4.8 -7 -9 10 80.06 14.26 7 9 10 98.02 17.4 -7 9 -10 73.15 18.73 7 9 11 102.38 19.28 -7 -9 11 95.64 15.59 -7 9 -11 68.15 18.62 -7 -9 12 139.5 18.92 7 9 12 143.13 23.76 -7 9 -12 123.18 24.75 7 9 13 14.86 6.34 -7 -9 13 25.92 7.86 -7 9 -13 23.14 11.09 -7 9 -14 25.19 12.48 7 9 14 64.52 17.08 -7 -9 14 54.8 11.29 -7 10 14 46.26 11.68 -7 10 13 1.27 2.13 -7 10 12 128.93 20.09 -7 10 12 166.93 23.15 -7 10 11 12.02 6.45 -7 -10 -10 26.18 8.69 -7 10 10 35.22 10.66 -7 -10 -9 44.97 10.87 -7 10 9 45.1 12.02 -7 -10 -8 161.4 20.92 -7 10 8 243.89 29.2 -7 -10 -7 43.51 10.4 -7 10 7 40.45 11.77 -7 -10 -6 165.14 20.76 -7 10 6 166.55 24.56 -7 -10 -5 11.51 5.69 -7 -10 -5 16.47 8.55 -7 10 5 7.94 6.94 -7 -10 -4 275.69 26.43 -7 -10 -4 282.6 33.5 -7 10 4 250.67 30.87 -7 -10 -3 142.61 18.58 -7 -10 -3 170.82 25.8 -7 10 3 173.82 25.64 -7 -10 -2 300.12 27.36 -7 -10 -2 341.33 36.24 -7 10 2 341.78 36.64 -7 -10 -1 27.03 7.23 -7 -10 -1 23.04 9.02 -7 10 1 35.7 11.86 -7 -10 0 15.18 5.37 -7 -10 0 17.47 7.37 -7 10 0 11.73 7.29 -7 -10 1 25.14 9.15 -7 10 -1 26.73 10.49 -7 -10 1 24.17 6.49 -7 -10 2 345.81 35.22 -7 10 -2 293.91 35.56 -7 -10 3 172.58 24.29 -7 10 -3 160.4 26.4 -7 -10 4 252.26 29.51 7 10 4 283.38 25.35 -7 10 -4 306.88 37.64 -7 -10 5 17.09 7.21 7 10 5 14.26 5.92 -7 10 -5 33.16 12.6 -7 -10 6 197.15 25.16 7 10 6 174.35 20.84 -7 10 -6 192.65 30.3 -7 -10 7 49.97 12.5 7 10 7 49.52 11.08 -7 10 -7 47.34 15.92 7 10 8 261.08 27.21 -7 -10 8 227.89 26.91 -7 10 -8 229.5 33.9 -7 -10 9 57.33 12.65 7 10 9 42.94 11.89 -7 10 -9 50.62 16.18 -7 -10 10 22.66 7.82 7 10 10 34.83 10.37 -7 10 -10 32.8 12.59 -7 -10 11 9.87 4.57 7 10 11 10.97 6.1 -7 10 -11 6.95 3.85 -7 -10 12 174.81 21.77 7 10 12 157.5 24.71 -7 10 -12 163.93 30.15 7 10 13 9.41 4.94 -7 -10 13 30.93 8.88 -7 10 -13 18 9.27 7 10 14 50.15 14.71 -7 11 12 175.06 23.97 -7 11 11 34.25 11.01 -7 11 10 78.77 16.76 -7 -11 -9 21.8 7.78 -7 11 9 41.81 12.01 -7 -11 -8 26.63 7.96 -7 11 8 60.51 14.33 -7 -11 -7 25.42 7.49 -7 11 7 21.66 8.91 -7 -11 -6 354.12 30.5 -7 11 6 451.38 41.36 -7 -11 -5 85.59 14.18 -7 -11 -5 96.83 19.73 -7 11 5 86.28 17.58 -7 -11 -4 111.94 16.12 -7 -11 -4 137.12 23.72 -7 11 4 113.78 20.59 -7 -11 -3 46.84 10.48 -7 -11 -3 57.27 15.6 -7 11 3 46.74 13.39 -7 -11 -2 66.11 12 -7 -11 -2 53.56 13.95 -7 11 2 50.03 13.96 -7 -11 -1 75.78 12.34 -7 -11 -1 62.98 15.51 -7 11 1 81.13 17.76 -7 -11 0 346.57 37.23 -7 11 0 424.55 42.31 -7 -11 0 322.75 26.01 -7 -11 1 60.7 15.01 -7 11 -1 75.41 17.28 -7 -11 2 49.29 13.6 -7 11 -2 45.62 14.12 -7 -11 3 49.33 13.22 -7 11 -3 61.23 16.42 7 11 4 125.56 16.57 -7 -11 4 126.08 20.88 -7 11 -4 114.86 23.16 -7 -11 5 67.8 15.39 7 11 5 87.43 14.33 -7 11 -5 117.94 24.01 -7 -11 6 427.82 39.75 7 11 6 428.01 34.1 -7 11 -6 435.48 47.32 -7 -11 7 29.55 9.9 7 11 7 13.16 6.46 -7 11 -7 12.92 7.24 -7 -11 8 45.14 12.17 7 11 8 53.84 12.19 -7 11 -8 34.84 13.47 -7 -11 9 48.47 12.37 7 11 9 28.58 8.97 -7 11 -9 33.58 13.39 -7 -11 10 83.69 15.99 7 11 10 92.15 17.2 -7 11 -10 91.65 22.38 -7 -11 11 33.51 10.2 7 11 11 41.76 11.89 -7 11 -11 32.47 12.77 7 11 12 168.23 25.49 -7 -11 12 145.52 20.63 -7 11 -12 161.06 30.39 7 11 13 17.26 8.19 -7 12 10 41.18 12.47 -7 -12 -9 19.56 7.27 -7 12 9 27.59 9.95 -7 -12 -8 61.82 12.57 -7 12 8 90.77 18.32 -7 -12 -7 43.09 9.86 -7 12 7 33.98 10.58 -7 -12 -6 69.63 12.74 -7 -12 -6 85.71 19.31 -7 12 6 108.41 20.21 -7 -12 -5 130.57 17.23 -7 -12 -5 131.83 24.13 -7 12 5 143.35 23.23 -7 -12 -4 118.23 16.2 -7 -12 -4 123.03 23.59 -7 12 4 128.74 22.33 -7 -12 -3 24.06 7.19 -7 -12 -3 25.68 11.16 -7 12 3 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-1 12 48.68 8.42 -9 2 12 40.91 10.49 -9 -2 -11 39.49 13.44 -9 2 11 38.45 9.92 -9 -2 -10 12.24 7.76 -9 2 10 7.68 6.15 -9 -2 -9 33.69 12.29 -9 2 9 27.06 9.59 -9 -2 -8 116.97 22.55 -9 2 8 143.55 21.88 -9 -2 -7 32.14 11.7 -9 2 7 21.75 8.87 -9 -2 -6 30.19 11.37 -9 2 6 20.31 7.85 -9 -2 -5 130.16 23.47 -9 2 5 141.21 22.65 -9 -2 -4 159.61 25.93 -9 2 4 158.82 23.92 -9 2 3 -3.16 5.48 -9 -2 -3 0.36 2.59 -9 -2 -2 148.08 16.68 -9 2 2 137.26 22.57 -9 -2 -2 155.66 24.43 -9 -2 -1 64.82 10.64 -9 2 1 84.2 17.86 -9 -2 -1 63.86 15.44 -9 -2 0 48.61 8.94 -9 2 0 42.42 13.28 -9 -2 0 35.63 11.12 -9 -2 1 66.93 10.4 -9 -2 1 80.42 16.45 -9 2 -1 56.51 14.95 -9 -2 2 128.88 14.42 -9 -2 2 125.8 20.23 -9 2 -2 152.9 25.62 -9 -2 3 0.68 1.41 -9 -2 3 -0.09 3.57 -9 2 -3 -0.26 4.93 -9 -2 4 152.7 15.23 -9 -2 4 148.64 21.63 -9 2 -4 143.44 25.27 -9 -2 5 136.37 14.27 -9 -2 5 158.56 22.15 -9 2 -5 144.91 25.83 -9 -2 6 32.46 6.76 -9 -2 6 25.19 8.49 -9 2 -6 25.13 9.5 -9 -2 7 24.48 5.71 -9 -2 7 15.1 6.76 -9 2 -8 159.79 27.27 -9 -2 8 159.41 15.13 -9 -2 8 123.03 17.84 -9 2 -9 35.41 12.66 -9 -2 9 42.22 7.62 -9 2 -10 11.81 7.33 -9 -2 10 19.77 5.17 -9 -2 11 52.38 8.64 -9 -2 12 55.67 9.11 -9 -2 13 31.04 6.73 -9 -2 14 129.45 14.75 -9 3 13 87.75 15.96 -9 3 12 29.28 9.62 -9 -3 -11 15.31 7.51 -9 3 11 11.68 6.41 -9 -3 -10 67.71 16.88 -9 3 10 76.15 15.71 -9 -3 -9 107.59 21.22 -9 3 9 103.07 18.73 -9 -3 -8 9.68 5.55 -9 3 8 11.08 5.63 -9 -3 -7 116.96 22.06 -9 3 7 104.79 19.59 -9 -3 -6 72.39 17.2 -9 3 6 49.39 13.27 -9 -3 -5 12.61 6.87 -9 3 5 16.16 7.54 -9 -3 -4 119.47 22.33 -9 -3 -4 130.39 17.92 -9 3 4 145.51 23.63 -9 -3 -3 112.87 16.02 -9 3 3 131.27 21.83 -9 -3 -3 105.2 20.38 -9 -3 -2 36.33 8.51 -9 3 2 36.28 11.66 -9 -3 -2 31.52 11.41 -9 -3 -1 78.13 12.85 -9 3 1 68.04 16.39 -9 -3 -1 57.58 14.53 -9 -3 0 13.04 5.1 -9 3 0 13.82 6.29 -9 -3 0 16.73 8 -9 -3 1 64.3 11.27 -9 3 -1 69.09 17.56 -9 -3 1 74.13 15.77 -9 -3 2 34.37 8.17 -9 -3 2 43.63 12.23 -9 3 -2 52.12 14.92 -9 -3 3 83.42 12.2 -9 -3 3 83.07 15.99 -9 3 -3 84.72 19.41 -9 -3 4 133.69 15.45 -9 -3 4 125.45 19.28 -9 3 -4 122.84 23.81 -9 -3 5 13.81 4.87 -9 -3 5 5.43 4.1 -9 3 -5 9.38 6 -9 -3 6 51.27 9.04 -9 -3 6 47.22 11.2 -9 3 -6 51.53 15.48 -9 -3 7 128.99 14.72 -9 -3 7 101.06 16.12 -9 3 -7 101.89 21.77 -9 3 -8 27.21 11.22 -9 -3 8 20.77 5.8 -9 3 -9 72.67 18.72 -9 -3 9 123.42 14.1 -9 3 -10 51.04 15.08 -9 -3 10 104.24 12.79 -9 -3 11 19.25 5.5 -9 -3 12 24.45 6.21 -9 -3 13 81.77 11.52 -9 -3 14 6.63 3.58 -9 4 13 29.54 9.7 -9 4 12 3.58 3.5 -9 -4 -11 129.38 23.51 -9 4 11 122.98 19.8 -9 -4 -10 3.27 2.34 -9 4 10 -2.48 5.72 -9 -4 -9 90.51 18.86 -9 4 9 103.1 19.27 -9 -4 -8 47.68 13.53 -9 4 8 48.58 13.58 -9 -4 -7 74.71 17.15 -9 4 7 76.41 16.84 -9 -4 -6 15.31 9.47 -9 -4 -6 11.75 4.55 -9 4 6 10.76 6.18 -9 -4 -5 272.2 28.2 -9 4 5 292.88 34 -9 -4 -5 281.26 34.45 -9 -4 -4 5.46 4.58 -9 -4 -4 12.2 5.51 -9 4 4 15.79 8.4 -9 -4 -3 6.14 5.72 -9 -4 -3 11.86 6.05 -9 4 3 8.59 5.18 -9 -4 -2 30.73 8.29 -9 4 2 20.28 8.24 -9 -4 -2 29.27 10.37 -9 -4 -1 150.74 19.52 -9 4 1 166.43 25.99 -9 -4 -1 191.75 25.91 -9 -4 0 123.36 16.95 -9 4 0 110.83 21.24 -9 -4 0 76.13 15.98 -9 -4 1 176.85 20.18 -9 -4 1 140.24 21.23 -9 4 -1 171.16 27.37 -9 -4 2 36.23 8.68 -9 -4 2 20.04 6.67 -9 4 -2 23.3 11.12 -9 -4 3 4.58 3.64 -9 -4 3 6.58 4.23 -9 4 -3 5.26 7.08 -9 -4 4 5.47 3.09 -9 -4 4 4.58 2.77 -9 4 -4 -2.96 6 -9 -4 5 224.93 21.64 -9 -4 5 213.61 24.11 -9 4 -5 249.88 34.68 -9 -4 6 18.21 5.89 -9 4 -6 11.49 6.34 -9 -4 7 81.64 12.13 -9 4 -7 74.65 18.86 -9 -4 8 43.07 8.74 -9 4 -8 6.45 4.66 -9 -4 9 106.36 13.95 -9 4 -9 92.6 21.01 -9 -4 10 0.46 1.54 -9 -4 11 117.85 14.4 -9 -4 12 12.9 4.7 -9 -4 13 28.18 7.14 -9 -4 14 20.18 5.95 -9 5 13 150.51 21.05 -9 5 13 174.6 23.74 -9 5 12 4.82 2.9 -9 -5 -11 0.51 3.11 -9 5 11 3.32 4.12 -9 -5 -10 7.3 1.8 -9 5 10 16.19 6.88 -9 -5 -9 98.11 20.06 -9 5 9 119.18 21.11 -9 -5 -8 83.72 18.37 -9 -5 -8 66.01 13.8 -9 5 8 65.58 15.94 -9 -5 -7 163.69 26.17 -9 -5 -7 146.61 21.18 -9 5 7 173.08 25.94 -9 -5 -6 12.2 7.39 -9 -5 -6 2.61 2.64 -9 5 6 3.37 3.78 -9 -5 -5 6.62 4.29 -9 -5 -5 -4.64 4.53 -9 5 5 -0.41 4.34 -9 -5 -4 31.77 11.07 -9 -5 -4 44.83 11.34 -9 5 4 33.91 12.33 -9 -5 -3 220.04 25.77 -9 5 3 218.54 29.88 -9 -5 -3 228.19 30.34 -9 -5 -2 69.11 13.8 -9 5 2 49.68 14.03 -9 -5 -2 63.08 15.23 -9 -5 -1 46.34 11.25 -9 5 1 71.76 17.54 -9 -5 -1 50.44 12.6 -9 -5 0 30.4 8.84 -9 5 0 32.61 11.52 -9 -5 0 19.04 8.14 -9 -5 1 40.09 10.36 -9 5 -1 48.13 14.32 -9 -5 1 30.59 9.72 -9 -5 2 72.72 13.27 -9 -5 2 40.52 10.44 -9 5 -2 61.32 17.14 -9 -5 3 245.57 24.49 -9 -5 3 208.69 24.59 -9 5 -3 253.71 34.66 -9 -5 4 42.97 9.79 -9 -5 4 23.42 8.21 -9 5 -4 41.55 13.85 -9 -5 5 3.69 2.5 -9 5 -5 -15.35 8.64 -9 -5 6 5.72 3.43 -9 5 -6 3.07 3.76 -9 -5 7 173.3 19.27 -9 5 -7 194.04 30.95 -9 -5 8 75.87 12.65 -9 5 -8 56.85 16.74 -9 -5 9 102.5 14.35 -9 -5 10 12.36 5.44 -9 -5 11 0.77 1.27 -9 -5 12 6.89 4.11 -9 -5 13 202.48 19.98 -9 6 13 3.55 2.03 -9 6 12 60.94 14.59 -9 -6 -11 88.44 19.12 -9 6 11 111.09 19.86 -9 -6 -10 28.96 10.48 -9 6 10 10.59 6.45 -9 -6 -9 77.59 17.86 -9 -6 -9 64.62 14.08 -9 6 9 94.31 18.92 -9 -6 -8 37.45 12.41 -9 -6 -8 17.69 7.41 -9 6 8 40.27 12.1 -9 -6 -7 49.73 14.32 -9 -6 -7 60.49 13.76 -9 6 7 73.96 16.6 -9 -6 -6 60.29 15.51 -9 -6 -6 76.68 15.98 -9 6 6 81.76 17.87 -9 -6 -5 243.49 28.93 -9 6 5 299.13 35.72 -9 -6 -5 255.77 31.86 -9 -6 -4 44.14 12.43 -9 -6 -4 25.92 9.65 -9 6 4 36.65 12.23 -9 -6 -3 63.72 15.42 -9 -6 -3 34.63 10 -9 6 3 43.23 12.69 -9 -6 -2 48.09 11.88 -9 6 2 34.91 11.6 -9 -6 -2 38.56 11.23 -9 -6 -1 152.66 21.7 -9 6 1 198.61 29.35 -9 -6 -1 171.95 23.98 -9 -6 0 47.38 11.66 -9 6 0 32.48 13.28 -9 -6 0 23.39 9.59 -9 -6 1 160.18 21.63 -9 -6 1 175.32 22.72 -9 6 -1 187.37 29.04 -9 -6 2 36.33 9.98 -9 6 -2 44.5 14.74 -9 -6 2 25.58 8.66 -9 -6 3 38.86 10.26 -9 6 -3 46.64 14.96 -9 -6 4 33 9.01 -9 6 -4 41.37 15.17 -9 -6 5 260.81 26.18 -9 6 -5 298.93 39.25 -9 -6 6 90.18 14.66 -9 6 -6 68.15 18.53 -9 -6 7 83 14.09 -9 6 -7 82.74 21.12 -9 -6 8 29.35 8.13 -9 -6 9 103.47 14.98 -9 -6 10 36.34 9.15 -9 -6 11 92.62 13.92 -9 -6 12 57.34 10.89 -9 -7 -11 8.99 6.18 -9 -7 -10 30.01 11.23 -9 7 10 25.54 9.79 -9 -7 -9 74.64 17.26 -9 -7 -9 47.86 12.42 -9 7 9 75.67 17.47 -9 -7 -8 21.73 8.96 -9 -7 -8 19.02 7.82 -9 7 8 16.91 8.76 -9 -7 -7 112.79 20.74 -9 -7 -7 103.49 18.48 -9 7 7 121.82 22.12 -9 -7 -6 86.57 18.15 -9 -7 -6 96.66 18.08 -9 7 6 132.23 23.31 -9 -7 -5 15.35 7.67 -9 -7 -5 11.86 6.47 -9 7 5 28.56 10.71 -9 -7 -4 30.33 10.6 -9 -7 -4 22.33 9.15 -9 7 4 12.59 6.46 -9 -7 -3 102.01 19.3 -9 -7 -3 105.32 18.95 -9 7 3 129.76 23.1 -9 -7 -2 11.94 6.75 -9 7 2 11.05 6.98 -9 -7 -2 3.39 2.83 -9 -7 -1 50.69 12.39 -9 7 1 56.69 15.61 -9 -7 -1 35.31 10.43 -9 -7 0 198.66 25.46 -9 7 0 172.61 28.48 -9 -7 0 123.45 19.36 -9 -7 1 55.88 13.27 -9 7 -1 42.71 13.87 -9 -7 2 5.85 5.36 -9 7 -2 12.2 7.65 -9 -7 3 107.55 17.71 -9 7 -3 106.28 23.43 -9 -7 4 20.43 7.54 -9 7 -4 17.31 9.55 -9 -7 5 27.16 8.75 -9 7 -5 22.01 10.15 -9 -7 6 87.07 15.4 -9 7 -6 97.46 22.87 -9 -7 7 156.12 20.3 -9 -7 8 13.26 5.61 -9 -7 9 62.13 12.27 -9 -7 10 31.56 8.5 -9 -7 11 2.71 3.19 -9 -8 -10 31.84 11.04 -9 -8 -9 31.63 10.33 -9 -8 -9 37.55 10.79 -9 -8 -8 78.29 16.76 -9 -8 -8 99.81 17.97 -9 -8 -7 26.21 9.97 -9 -8 -7 9.6 6 -9 8 7 19.69 7.47 -9 -8 -6 44.43 12.95 -9 -8 -6 48.85 13.09 -9 8 6 60.76 15.95 -9 -8 -5 47.17 13.26 -9 -8 -5 41.42 12.23 -9 8 5 49.94 14.32 -9 -8 -4 73.58 16.41 -9 -8 -4 84.32 17.96 -9 8 4 90.46 19.82 -9 -8 -3 46.6 12.54 -9 -8 -3 62.38 15.38 -9 8 3 46 14.34 -9 -8 -2 116.72 19.71 -9 -8 -2 106.86 19.8 -9 8 2 121.95 23.32 -9 -8 -1 42.03 11.88 -9 8 1 46.1 14.89 -9 -8 0 -1.59 4.17 -9 8 0 1.76 4.57 -9 -8 1 55.8 13.68 -9 8 -1 52.25 14.93 -9 -8 2 101.92 18.56 -9 8 -2 115.8 23.91 -9 -8 3 45.75 12.42 -9 8 -3 52.86 15.38 -9 -8 4 83.46 15.92 -9 8 -4 82.77 20.58 -9 -8 5 40.42 11.44 -9 -8 6 58.23 12.99 -9 -8 7 19.2 7.29 -9 -8 8 99.35 16.13 -9 -8 9 50.75 11.5 -9 -8 10 24.01 8.11 -9 -9 -10 49.17 12.91 -9 -9 -10 32.5 9.97 -9 -9 -9 11.94 6.58 -9 -9 -9 8.44 5.73 -9 -9 -8 7.29 5.01 -9 -9 -8 11.31 6.67 -9 -9 -7 19.02 7.73 -9 -9 -7 5.89 2.96 -9 -9 -6 195.95 27.05 -9 -9 -6 173.62 24.9 -9 -9 -5 9.72 5.36 -9 -9 -5 7.53 6.83 -9 -9 -4 25.11 9.45 -9 -9 -4 34.13 10.59 -9 9 4 32.14 11.42 -9 -9 -3 20.29 9.05 -9 9 3 30.32 11.04 -9 -9 -2 8.5 7.83 -9 9 2 6.85 5.04 -9 -9 -1 11.35 7.91 -9 9 1 7.01 6.44 -9 -9 0 166.91 25.17 -9 9 0 209.93 31.94 -9 -9 1 1.97 2.81 -9 9 -1 12.45 9.93 -9 -9 2 1.43 3.63 -9 -9 3 33.53 10.85 -9 -9 4 46.69 12.1 -9 -9 5 28.47 9.35 -9 -9 6 219.37 26.61 -9 -9 7 31.68 9.57 -9 -9 8 5.89 3.16 -9 -9 9 15.56 6.2 -9 -10 -10 14.99 6.86 -9 -10 -9 2.7 3.1 -9 -10 -9 -2.61 2.5 -9 -10 -8 95.17 17.66 -9 -10 -8 81.33 16.77 -9 -10 -7 2.95 4.78 -9 -10 -7 11.91 7.07 -9 -10 -6 30.49 10.9 -9 -10 -5 0.03 2.73 -9 -10 -4 144.47 23.8 -9 -10 -3 20.52 10.06 -9 -10 -2 190.51 27.9 -9 -10 -1 2.05 2.69 -9 -10 0 -2.71 5.18 -9 -10 1 -3.36 3.41 -9 -10 2 149.7 23.88 -9 -10 3 2.29 1.75 -9 -10 4 168.22 24.69 -9 -10 5 -3.08 4 -9 -10 6 51.01 13.16 -9 -10 7 7.4 5.51 -9 -11 -7 36.69 12.03 -9 -11 -6 156.19 24.86 -9 -11 -5 17.79 8.01 -9 -11 -4 65.61 16.48 -9 -11 -3 13.54 8.23 -9 -11 -2 -0.78 3.8 -9 -11 -1 29.26 11.36 -9 -11 0 210.52 29.96 -9 -11 1 26.49 10.54 -9 -11 2 -0.68 3.23 -9 -11 3 16.93 7.91 -9 -11 4 68.62 15.86 -10 0 0 32.16 13.01 -10 0 1 223.92 30.67 -10 0 -1 250.68 33.64 -10 0 2 5.48 4.25 -10 0 -2 4.78 4.22 -10 0 3 2.3 4.45 -10 0 -3 13.52 8.52 -10 0 4 26.58 10.34 -10 0 -4 29.75 11.41 -10 0 5 145.81 23.1 -10 0 -5 120.71 25.01 -10 0 6 2.22 4.35 -10 0 -6 9.94 7.45 -10 0 7 26.72 9.52 -10 0 8 8.13 5.13 -10 1 9 102.69 18.3 -10 1 8 4.94 3.88 -10 -1 -7 184.97 30.53 -10 1 7 198.98 26.96 -10 1 6 6.33 4.48 -10 -1 -6 25.08 10.97 -10 1 5 33.56 11.61 -10 -1 -5 29.43 12.16 -10 1 4 13.12 7.42 -10 -1 -4 18.2 7.9 -10 1 3 123.98 22.46 -10 -1 -3 183.11 28.98 -10 1 2 16.95 8.54 -10 -1 -2 21.57 10.62 -10 1 1 135.13 23.84 -10 -1 -1 163.82 26.86 -10 1 0 16.39 8.56 -10 -1 0 9.75 7.5 -10 -1 1 158.88 25.29 -10 1 -1 158.4 26.81 -10 -1 2 12.1 7.65 -10 1 -2 8.14 5.58 -10 -1 3 88.57 18.42 -10 1 -3 147.42 26.67 -10 -1 4 14.89 7.7 -10 1 -4 10.66 6.48 -10 -1 5 16.68 8.42 -10 1 -5 28.04 11.79 -10 -1 6 18.41 7.38 -10 1 -6 -13.54 8.36 -10 2 10 12.65 6.87 -10 2 9 12.02 6.16 -10 2 8 46.37 12.85 -10 -2 -7 36.69 12.94 -10 2 7 47.5 13.78 -10 2 6 11.48 8.47 -10 -2 -6 14.85 9.97 -10 2 5 116.66 21.12 -10 -2 -5 129.19 24.91 -10 2 4 14.74 7.75 -10 -2 -4 7.27 6.63 -10 2 3 -3.97 4.49 -10 -2 -3 2.59 4.32 -10 2 2 88.08 18.63 -10 -2 -2 63.64 16.71 -10 2 1 163.56 26.5 -10 -2 -1 122.07 22.76 -10 2 0 7.18 6.41 -10 -2 0 8.93 5.33 -10 -2 1 136.81 23 -10 2 -1 137.25 25.35 -10 -2 2 39.31 11.54 -10 2 -2 66.23 17.65 -10 -2 3 -2.23 5.09 -10 2 -3 -2.37 2.71 -10 -2 4 11.61 7.38 -10 2 -4 15.43 8.87 -10 -2 5 91.63 17.3 -10 2 -5 141.45 27.63 -10 3 10 78.63 16.25 -10 3 9 28.26 9.97 -10 3 8 5.59 5.66 -10 -3 -7 95.27 21.62 -10 3 7 125.1 21.92 -10 -3 -6 77.11 18.71 -10 3 6 92.4 19.15 -10 3 5 9.76 8.58 -10 -3 -5 10.69 8.93 -10 3 4 71.6 17.21 -10 -3 -4 52.04 15.19 -10 3 3 51.47 15.03 -10 -3 -3 72.43 17.12 -10 3 2 48.9 14.22 -10 -3 -2 38.78 12.48 -10 3 1 86.8 19.92 -10 -3 -1 87.49 19.05 -10 3 0 120.22 23.57 -10 -3 0 113.03 21.39 -10 -3 1 82.96 17.92 -10 3 -1 95.02 20.99 -10 -3 2 31.01 10.43 -10 3 -2 42.79 14.54 -10 -3 3 46.31 12.33 -10 3 -3 65.2 17.91 -10 3 -4 71.37 19.04 -10 4 10 64.64 15.21 -10 4 9 45.2 13.87 -10 4 8 171.05 26.21 -10 -4 -7 5.29 7.13 -10 4 7 -1.24 3.92 -10 -4 -6 7.72 5.59 -10 4 6 22.12 9.44 -10 -4 -5 30.02 11.14 -10 4 5 54.07 15.29 -10 4 4 88.05 19.43 -10 -4 -4 123.32 23.51 -10 4 3 38.33 13.45 -10 -4 -3 23.04 10.27 -10 4 2 267.31 34.7 -10 -4 -2 215.14 30.31 -10 4 1 37.87 11.91 -10 -4 -1 21.83 9.56 -10 4 0 30.18 10.95 -10 -4 0 18.07 8.6 -10 4 -1 59.55 16.89 -10 -4 1 28.44 9.48 -10 -4 2 170.32 24.42 -10 4 -2 231.41 34.12 -10 4 -3 33.37 13.79 -10 -5 -8 1 4.08 -10 -5 -7 6.23 5.11 -10 5 7 1.1 3.74 -10 -5 -6 156.76 27.32 -10 5 6 151.18 25.55 -10 -5 -5 4.52 5.81 -10 5 5 4.3 5.75 -10 5 4 153.94 26.29 -10 -5 -4 146.29 25.42 -10 5 3 19.88 10 -10 -5 -3 11.26 9.69 -10 5 2 50.38 15.03 -10 -5 -2 43.62 12.45 -10 5 1 14.24 8.75 -10 -5 -1 7.25 3.99 -10 5 0 261.72 35.68 -10 -5 0 263.34 31.65 -10 5 -1 2.39 3.5 -10 -6 -8 121.11 23.42 -10 -6 -7 26.08 10.61 -10 -6 -6 23.42 10.42 -10 -6 -5 0.84 2.77 -10 -6 -4 57.78 16.03 -10 -6 -3 1.71 4.06 -10 -6 -2 183.01 26.95 -10 -7 -7 32.26 12.6 -10 -7 -6 55.94 15.41 -10 -7 -5 2.46 5.64 -10 -7 3 104.54 17.36 -10 -7 4 61.47 12.96 -10 -7 5 3.17 1.92 -10 -7 6 86.22 15.05 -10 -7 7 33.78 9.26 -10 -8 0 34.23 10.91 -10 -8 1 104.24 19.08 -10 -8 2 39.16 11.62 -10 -8 3 11.81 5.71 -10 -8 4 6.44 2.6 -10 -8 5 77.74 14.97 -10 -9 -2 11.31 7.27 -10 -9 -1 32.14 11.15 -10 -9 0 -3.14 5.98 -10 -9 1 24.87 9.94 -10 -9 2 11.93 7.43 -10 -9 3 153.02 23.23 -11 0 1 22.07 8.99 -11 0 2 147.34 25.59 -11 -1 -1 0.9 5.9 -11 -1 0 26.85 9.94 -11 -1 1 23.02 9.35 -11 -1 2 0.6 4.09 -11 -2 -2 39.71 13.99 -11 -2 -1 44.22 14.91 -11 -2 0 14.6 9.08 _iucr_refine_instructions_details ; TITL 5-116_a.res in P2(1)2(1)2(1) 5-116.res created by SHELXL-2018/3 at 12:10:40 on 14-Nov-2018 REM Old TITL 5-116 in P2(1)2(1)2(1) REM SHELXT solution in P2(1)2(1)2(1): R1 0.056, Rweak 0.034, Alpha 0.005 REM 1.206 for 25 systematic absences, Orientation as input REM Flack x = -0.008 ( 0.012 ) from 2022 Parsons' quotients REM Formula found by SHELXT: C27 N O4 P I CELL 0.71073 7.9972 16.3553 18.8545 90 90 90 ZERR 4 0.0003 0.0005 0.0006 0 0 0 LATT -1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H I O P UNIT 112 104 4 16 4 L.S. 20 PLAN 20 BOND list 4 fmap 2 53 ACTA REM REM REM WGHT 0.023100 FVAR 0.29653 I1 3 0.977286 0.449866 0.406464 11.00000 0.02063 0.02047 = 0.02840 -0.00292 0.00171 -0.00218 P1 5 0.459068 0.504257 0.242741 11.00000 0.01947 0.01452 = 0.01511 0.00165 -0.00196 -0.00040 O1 4 0.478524 0.449909 0.313807 11.00000 0.02529 0.01416 = 0.01269 0.00077 0.00039 0.00087 O004 4 0.289172 0.535017 0.228066 11.00000 0.01987 0.01988 = 0.02376 0.00361 -0.00363 0.00119 O3 4 0.738877 0.282535 0.023633 11.00000 0.03636 0.02190 = 0.01673 -0.00362 0.00008 -0.00221 O2 4 0.950174 0.774035 0.276241 11.00000 0.01830 0.01827 = 0.02741 -0.00340 -0.00003 -0.00299 C25 1 0.892806 0.634762 0.262418 11.00000 0.01724 0.02636 = 0.01826 -0.00036 0.00066 0.00270 AFIX 43 H25 2 1.007160 0.624662 0.264315 11.00000 -1.20000 AFIX 0 C26 1 0.781605 0.570894 0.254346 11.00000 0.02408 0.01445 = 0.01675 0.00046 0.00054 0.00320 AFIX 43 H26 2 0.821904 0.517743 0.250466 11.00000 -1.20000 AFIX 0 C9 1 0.540340 0.288392 0.413821 11.00000 0.02044 0.01870 = 0.01469 0.00161 0.00067 0.00091 C13 1 0.813228 0.349168 0.401772 11.00000 0.02188 0.01810 = 0.01214 -0.00010 -0.00346 -0.00376 C4 1 0.480485 0.542466 0.518246 11.00000 0.02910 0.02475 = 0.01692 -0.00710 0.00711 -0.00137 AFIX 43 H4 2 0.482634 0.563512 0.564059 11.00000 -1.20000 AFIX 0 C8 1 0.642096 0.358373 0.416119 11.00000 0.02159 0.01661 = 0.01134 -0.00081 -0.00316 0.00394 C5 1 0.564802 0.469955 0.503496 11.00000 0.02232 0.02181 = 0.01980 0.00045 0.00281 -0.00069 C16 1 0.652937 0.371921 0.194857 11.00000 0.02308 0.01981 = 0.01448 0.00296 -0.00362 -0.00322 AFIX 43 H16 2 0.689534 0.365487 0.241342 11.00000 -1.20000 AFIX 0 C15 1 0.535098 0.431700 0.179098 11.00000 0.02081 0.01740 = 0.01316 0.00066 -0.00101 -0.00166 C17 1 0.716797 0.321566 0.141825 11.00000 0.02022 0.01733 = 0.02059 0.00205 -0.00359 -0.00124 AFIX 43 H17 2 0.794084 0.281047 0.152915 11.00000 -1.20000 AFIX 0 C18 1 0.663893 0.332370 0.071834 11.00000 0.02202 0.01292 = 0.01844 -0.00182 0.00310 -0.00292 C20 1 0.479614 0.439994 0.109525 11.00000 0.02265 0.01748 = 0.01952 0.00435 -0.00407 0.00046 AFIX 43 H20 2 0.400378 0.479683 0.098654 11.00000 -1.20000 AFIX 0 C3 1 0.393875 0.583570 0.466055 11.00000 0.02707 0.01729 = 0.02828 -0.00242 0.00640 0.00413 AFIX 43 H3 2 0.337394 0.631576 0.477233 11.00000 -1.20000 AFIX 0 C10 1 0.611264 0.213214 0.396559 11.00000 0.02801 0.01562 = 0.01892 -0.00046 -0.00437 -0.00201 AFIX 43 H10 2 0.543838 0.166902 0.395467 11.00000 -1.20000 AFIX 0 C7 1 0.655092 0.425160 0.561912 11.00000 0.03000 0.03087 = 0.01336 -0.00326 -0.00186 0.00200 AFIX 137 H7A 2 0.772886 0.424695 0.552112 11.00000 -1.50000 H7B 2 0.614625 0.369983 0.564549 11.00000 -1.50000 H7C 2 0.635281 0.452266 0.606285 11.00000 -1.50000 AFIX 0 C23 1 0.661504 0.730335 0.264176 11.00000 0.02552 0.01923 = 0.01557 -0.00007 -0.00041 0.00353 AFIX 43 H23 2 0.621727 0.783673 0.266933 11.00000 -1.20000 AFIX 0 C27 1 0.891605 0.856792 0.281137 11.00000 0.02441 0.01772 = 0.02732 0.00077 -0.00201 -0.00446 AFIX 137 H27A 2 0.825569 0.869592 0.240093 11.00000 -1.50000 H27B 2 0.985525 0.893241 0.283560 11.00000 -1.50000 H27C 2 0.824546 0.862897 0.323035 11.00000 -1.50000 AFIX 0 C2 1 0.389975 0.554364 0.397472 11.00000 0.02060 0.02014 = 0.02236 0.00309 0.00177 0.00187 AFIX 43 H2 2 0.330563 0.581703 0.362322 11.00000 -1.20000 AFIX 0 C11 1 0.779539 0.205791 0.381007 11.00000 0.02579 0.01902 = 0.02339 -0.00630 -0.00543 0.00519 AFIX 43 H11 2 0.823930 0.155207 0.368633 11.00000 -1.20000 AFIX 0 C24 1 0.832447 0.714642 0.267717 11.00000 0.02413 0.02043 = 0.01075 0.00229 0.00020 -0.00391 C22 1 0.551365 0.665516 0.256494 11.00000 0.02139 0.02328 = 0.01466 0.00306 -0.00346 0.00181 AFIX 43 H22 2 0.437091 0.675765 0.254347 11.00000 -1.20000 AFIX 0 C12 1 0.881664 0.274147 0.383960 11.00000 0.02311 0.02053 = 0.02035 -0.00228 -0.00074 0.00479 AFIX 43 H12 2 0.995223 0.269682 0.374063 11.00000 -1.20000 AFIX 0 C14 1 0.355318 0.294635 0.426867 11.00000 0.01978 0.02277 = 0.02888 0.00395 0.00008 -0.00437 AFIX 137 H14A 2 0.335812 0.323336 0.470504 11.00000 -1.50000 H14B 2 0.308264 0.240752 0.429947 11.00000 -1.50000 H14C 2 0.303732 0.323802 0.388480 11.00000 -1.50000 AFIX 0 C6 1 0.563556 0.439250 0.434167 11.00000 0.01558 0.01309 = 0.01673 -0.00095 0.00329 -0.00030 C1 1 0.477019 0.483126 0.382302 11.00000 0.01762 0.01476 = 0.01450 0.00068 0.00339 -0.00186 C21 1 0.609036 0.584974 0.251915 11.00000 0.01887 0.01763 = 0.01099 0.00211 0.00078 -0.00198 C19 1 0.541212 0.389589 0.055842 11.00000 0.03142 0.02125 = 0.01485 0.00300 -0.00433 -0.00662 AFIX 43 H19 2 0.500533 0.394257 0.009811 11.00000 -1.20000 AFIX 0 C28 1 0.701171 0.295671 -0.050248 11.00000 0.04846 0.03667 = 0.01471 -0.00672 0.00215 0.00176 AFIX 137 H28A 2 0.769776 0.260519 -0.078812 11.00000 -1.50000 H28B 2 0.723177 0.351665 -0.062338 11.00000 -1.50000 H28C 2 0.585448 0.283580 -0.058802 11.00000 -1.50000 AFIX 0 HKLF 4 REM 5-116_a.res in P2(1)2(1)2(1) REM wR2 = 0.0674, GooF = S = 1.076, Restrained GooF = 1.076 for all data REM R1 = 0.0347 for 5726 Fo > 4sig(Fo) and 0.0389 for all 6113 data REM 311 parameters refined using 0 restraints END WGHT 0.0253 0.0000 REM Highest difference peak 0.496, deepest hole -0.814, 1-sigma level 0.132 Q1 1 1.0722 0.4406 0.5044 11.00000 0.05 0.50 Q2 1 0.7981 0.9377 0.1593 11.00000 0.05 0.49 Q3 1 0.7631 0.3801 0.5021 11.00000 0.05 0.45 Q4 1 0.5038 0.1590 0.5002 11.00000 0.05 0.45 Q5 1 0.8479 0.4705 0.4997 11.00000 0.05 0.43 Q6 1 0.3786 0.5217 -0.0037 11.00000 0.05 0.42 Q7 1 0.8177 0.6018 0.3442 11.00000 0.05 0.41 Q8 1 0.1207 0.5210 0.3428 11.00000 0.05 0.41 Q9 1 0.8887 0.4044 0.4954 11.00000 0.05 0.41 Q10 1 0.6021 0.4197 0.0003 11.00000 0.05 0.41 Q11 1 0.7855 0.5322 0.4983 11.00000 0.05 0.41 Q12 1 0.1771 0.3563 0.4985 11.00000 0.05 0.40 Q13 1 0.7718 0.4181 0.3342 11.00000 0.05 0.39 Q14 1 0.3074 0.4597 0.4992 11.00000 0.05 0.39 Q15 1 1.1538 0.4832 0.4853 11.00000 0.05 0.38 Q16 1 0.2981 0.4552 0.3196 11.00000 0.05 0.38 Q17 1 0.8880 0.8774 0.1577 11.00000 0.05 0.38 Q18 1 0.4554 0.4228 -0.0026 11.00000 0.05 0.38 Q19 1 0.5491 0.4942 0.0013 11.00000 0.05 0.38 Q20 1 0.2710 0.4869 0.1712 11.00000 0.05 0.37 REM The information below was added by Olex2. REM REM R1 = 0.0347 for 5726 Fo > 4sig(Fo) and 0.0389 for all 20790 data REM n/a parameters refined using n/a restraints REM Highest difference peak 0.50, deepest hole -0.81 REM Mean Shift 0, Max Shift -0.001. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0389 REM R1_gt = 0.0347 REM wR_ref = 0.0674 REM GOOF = 1.076 REM Shift_max = -0.001 REM Shift_mean = 0 REM Reflections_all = 20790 REM Reflections_gt = 5726 REM Parameters = n/a REM Hole = -0.81 REM Peak = 0.50 REM Flack = -0.021(12) ; _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling - Detector area scaling ; _oxdiff_exptl_absorpt_empirical_full_max 3.530 _oxdiff_exptl_absorpt_empirical_full_min 0.481