data_NiBr2 _audit_creation_date 2017-03-05 _audit_creation_method ; Olex2 1.2 (compiled 2016.02.19 svn.r3266 for OlexSys, GUI svn.r5155) ; _publ_contact_author_address ? _publ_contact_author_email ? _publ_contact_author_name '' _publ_contact_author_phone ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C21 H22 Br2 N2 Ni O2' _chemical_formula_sum 'C21 H22 Br2 N2 Ni O2' _chemical_formula_weight 552.94 _chemical_absolute_configuration syn _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Br' 'Br' -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Ni' 'Ni' 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system 'orthorhombic' _space_group_IT_number 19 _space_group_name_H-M_alt 'P 21 21 21' _space_group_name_Hall 'P 2ac 2ab' loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 'x, y, z' 2 '-x+1/2, -y, z+1/2' 3 '-x, y+1/2, -z+1/2' 4 'x+1/2, -y+1/2, -z' _cell_length_a 8.9454(9) _cell_length_b 11.7746(13) _cell_length_c 20.350(3) _cell_angle_alpha 90.00 _cell_angle_beta 90.00 _cell_angle_gamma 90.00 _cell_volume 2143.4(4) _cell_formula_units_Z 4 _cell_measurement_reflns_used 9730 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 36.36 _cell_measurement_theta_min 2.49 _exptl_absorpt_coefficient_mu 4.652 _exptl_absorpt_correction_T_max 0.7471 _exptl_absorpt_correction_T_min 0.5792 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0940 before and 0.0687 after correction. The Ratio of minimum to maximum transmission is 0.7753. The \l/2 correction factor is Not present. ; _exptl_crystal_colour purple _exptl_crystal_colour_primary ? _exptl_crystal_density_diffrn 1.713 _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 1104 _exptl_crystal_size_max 0.24 _exptl_crystal_size_mid 0.22 _exptl_crystal_size_min 0.12 _exptl_special_details ; ? ; _diffrn_reflns_av_R_equivalents 0.0384 _diffrn_reflns_av_unetI/netI 0.0227 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 19 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_l_max 33 _diffrn_reflns_limit_l_min -33 _diffrn_reflns_number 126446 _diffrn_reflns_theta_full 36.36 _diffrn_reflns_theta_max 36.36 _diffrn_reflns_theta_min 2.65 _diffrn_ambient_temperature 100(2) _diffrn_detector_area_resol_mean ? _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_source 'fine-focus sealed tube' _diffrn_special_details ? _diffrn_standards_decay_% ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_number 0 _reflns_number_gt 9775 _reflns_number_total 10383 _reflns_threshold_expression >2sigma(I) _computing_cell_refinement 'SAINT v8.37A (Bruker, 2015)' _computing_data_collection ? _computing_data_reduction 'SAINT v8.37A (Bruker, 2015)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'XT (Sheldrick, 2015)' _refine_diff_density_max 0.390 _refine_diff_density_min -0.903 _refine_diff_density_rms 0.069 _refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881' _refine_ls_abs_structure_Flack 0.000(3) _refine_ls_extinction_coef ? _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.043 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 256 _refine_ls_number_reflns 10383 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0214 _refine_ls_R_factor_gt 0.0184 _refine_ls_restrained_S_all 1.043 _refine_ls_shift/su_max 0.005 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0190P)^2^+0.2220P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0419 _refine_ls_wR_factor_ref 0.0425 _refine_special_details ? _olex2_refinement_description ; 1. Twinned data refinement Scales: 0.983(3) 0.017(3) 2. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 3.a Ternary CH refined with riding coordinates: C1(H1), C9(H9) 3.b Secondary CH2 refined with riding coordinates: C2(H2A,H2B), C8(H8A,H8B) 3.c Aromatic/amide H refined with riding coordinates: C11(H11), C12(H12), C13(H13), C14(H14), C15(H15), C17(H17), C18(H18), C19(H19), C20(H20), C21(H21) 3.d Idealised Me refined as rotating group: C5(H5A,H5B,H5C), C6(H6A,H6B,H6C) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symetry_multiplicity _atom_site_calc_flag _atom_site_disorder_assembly _atom_site_disorder_group _atom_site_refinement_flags_posn Br1 Br 0.254812(13) 0.150098(9) 0.636974(6) 0.02118(2) Uani 1 1 d . . . Br2 Br 0.613542(11) 0.342555(10) 0.601647(6) 0.02216(2) Uani 1 1 d . . . Ni1 Ni 0.359853(13) 0.334718(10) 0.628833(6) 0.01247(2) Uani 1 1 d . . . O1 O -0.04505(9) 0.48420(8) 0.58341(4) 0.02113(16) Uani 1 1 d . . . O2 O 0.22080(9) 0.54773(7) 0.77793(4) 0.01602(13) Uani 1 1 d . . . N1 N 0.18461(10) 0.40955(7) 0.58803(4) 0.01341(14) Uani 1 1 d . . . N2 N 0.32961(9) 0.42278(7) 0.71058(4) 0.01126(13) Uani 1 1 d . . . C1 C 0.14441(13) 0.40805(10) 0.51633(5) 0.01745(18) Uani 1 1 d . . . H1 H 0.1650 0.3315 0.4971 0.021 Uiso 1 1 calc . . R C2 C -0.02396(14) 0.42965(13) 0.51931(6) 0.0260(2) Uani 1 1 d . . . H2A H -0.0563 0.4803 0.4832 0.031 Uiso 1 1 calc . . R H2B H -0.0806 0.3575 0.5166 0.031 Uiso 1 1 calc . . R C3 C 0.07591(10) 0.45652(8) 0.61868(5) 0.01379(16) Uani 1 1 d . . . C4 C 0.06308(11) 0.48071(9) 0.69143(5) 0.01384(16) Uani 1 1 d . . . C5 C -0.03031(13) 0.38367(12) 0.72204(6) 0.0260(2) Uani 1 1 d . . . H5A H -0.1317 0.3853 0.7038 0.039 Uiso 1 1 calc . . GR H5B H -0.0349 0.3937 0.7698 0.039 Uiso 1 1 calc . . GR H5C H 0.0165 0.3105 0.7119 0.039 Uiso 1 1 calc . . GR C6 C -0.01503(14) 0.59547(12) 0.70201(7) 0.0259(2) Uani 1 1 d . . . H6A H 0.0517 0.6570 0.6882 0.039 Uiso 1 1 calc . . GR H6B H -0.0396 0.6045 0.7486 0.039 Uiso 1 1 calc . . GR H6C H -0.1070 0.5981 0.6759 0.039 Uiso 1 1 calc . . GR C7 C 0.21325(10) 0.48164(8) 0.72502(5) 0.01140(14) Uani 1 1 d . . . C8 C 0.37404(12) 0.53987(9) 0.80280(5) 0.01711(17) Uani 1 1 d . . . H8A H 0.3748 0.5195 0.8500 0.021 Uiso 1 1 calc . . R H8B H 0.4277 0.6127 0.7969 0.021 Uiso 1 1 calc . . R C9 C 0.44594(11) 0.44519(8) 0.76097(5) 0.01201(15) Uani 1 1 d . . . H9 H 0.5377 0.4755 0.7390 0.014 Uiso 1 1 calc . . R C10 C 0.23635(12) 0.49770(9) 0.48190(5) 0.01490(16) Uani 1 1 d . . . C11 C 0.37375(14) 0.46872(11) 0.45421(6) 0.0227(2) Uani 1 1 d . . . H11 H 0.4056 0.3917 0.4543 0.027 Uiso 1 1 calc . . R C12 C 0.46475(15) 0.55200(13) 0.42642(7) 0.0307(3) Uani 1 1 d . . . H12 H 0.5583 0.5318 0.4076 0.037 Uiso 1 1 calc . . R C13 C 0.41861(15) 0.66402(13) 0.42629(7) 0.0297(3) Uani 1 1 d . . . H13 H 0.4810 0.7209 0.4077 0.036 Uiso 1 1 calc . . R C14 C 0.28158(15) 0.69363(11) 0.45312(6) 0.0241(2) Uani 1 1 d . . . H14 H 0.2498 0.7706 0.4526 0.029 Uiso 1 1 calc . . R C15 C 0.19095(12) 0.61084(10) 0.48068(5) 0.01806(19) Uani 1 1 d . . . H15 H 0.0970 0.6315 0.4989 0.022 Uiso 1 1 calc . . R C16 C 0.48637(9) 0.34075(8) 0.80027(5) 0.01179(14) Uani 1 1 d . . . C17 C 0.39301(11) 0.24642(8) 0.80506(5) 0.01426(16) Uani 1 1 d . . . H17 H 0.3032 0.2435 0.7802 0.017 Uiso 1 1 calc . . R C18 C 0.43081(11) 0.15640(9) 0.84611(5) 0.01596(16) Uani 1 1 d . . . H18 H 0.3670 0.0921 0.8488 0.019 Uiso 1 1 calc . . R C19 C 0.56119(12) 0.15981(10) 0.88317(5) 0.01847(17) Uani 1 1 d . . . H19 H 0.5859 0.0987 0.9117 0.022 Uiso 1 1 calc . . R C20 C 0.65517(13) 0.25356(11) 0.87814(6) 0.0235(2) Uani 1 1 d . . . H20 H 0.7447 0.2563 0.9032 0.028 Uiso 1 1 calc . . R C21 C 0.61875(11) 0.34328(10) 0.83661(6) 0.01947(17) Uani 1 1 d . . . H21 H 0.6842 0.4065 0.8330 0.023 Uiso 1 1 calc . . R loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Br1 0.02850(5) 0.01219(4) 0.02285(5) -0.00096(3) 0.00004(4) -0.00229(4) Br2 0.01490(4) 0.02404(5) 0.02752(5) -0.01100(4) 0.00578(4) -0.00235(4) Ni1 0.01388(5) 0.01220(5) 0.01132(5) -0.00264(4) 0.00074(4) 0.00118(4) O1 0.0125(3) 0.0354(5) 0.0154(3) 0.0021(3) -0.0038(3) -0.0015(3) O2 0.0172(3) 0.0179(3) 0.0130(3) -0.0054(3) -0.0010(3) 0.0040(3) N1 0.0165(3) 0.0141(3) 0.0097(3) -0.0004(3) -0.0015(3) -0.0017(3) N2 0.0120(3) 0.0120(3) 0.0098(3) -0.0004(3) -0.0003(2) 0.0005(2) C1 0.0217(5) 0.0201(4) 0.0106(4) -0.0038(3) -0.0035(3) -0.0045(4) C2 0.0210(5) 0.0412(7) 0.0158(5) -0.0020(5) -0.0070(4) -0.0105(5) C3 0.0126(3) 0.0155(4) 0.0132(4) 0.0009(3) -0.0020(3) -0.0021(3) C4 0.0111(3) 0.0187(4) 0.0117(4) 0.0011(3) 0.0006(3) 0.0014(3) C5 0.0190(5) 0.0397(7) 0.0192(5) 0.0081(5) 0.0015(4) -0.0107(4) C6 0.0231(5) 0.0316(6) 0.0232(5) -0.0047(5) -0.0038(4) 0.0154(5) C7 0.0136(3) 0.0113(3) 0.0093(3) 0.0003(3) 0.0010(3) 0.0004(3) C8 0.0198(4) 0.0155(4) 0.0161(4) -0.0047(3) -0.0051(4) 0.0024(3) C9 0.0121(3) 0.0126(4) 0.0113(4) 0.0000(3) -0.0007(3) -0.0013(3) C10 0.0169(4) 0.0193(4) 0.0085(4) -0.0006(3) -0.0021(3) 0.0007(3) C11 0.0232(5) 0.0271(5) 0.0178(5) 0.0007(4) 0.0028(4) 0.0086(4) C12 0.0246(6) 0.0416(7) 0.0259(6) 0.0051(5) 0.0104(5) 0.0057(5) C13 0.0292(6) 0.0362(7) 0.0236(6) 0.0121(5) 0.0038(4) -0.0032(5) C14 0.0295(6) 0.0231(5) 0.0196(5) 0.0076(4) -0.0037(4) 0.0025(4) C15 0.0184(4) 0.0218(5) 0.0140(4) 0.0003(4) -0.0021(3) 0.0046(4) C16 0.0115(3) 0.0125(3) 0.0113(4) -0.0001(3) -0.0001(3) 0.0014(3) C17 0.0153(4) 0.0143(4) 0.0132(4) 0.0010(3) -0.0010(3) -0.0014(3) C18 0.0199(4) 0.0132(4) 0.0147(4) 0.0008(3) 0.0000(3) -0.0002(3) C19 0.0204(4) 0.0164(4) 0.0186(4) 0.0037(4) -0.0015(3) 0.0050(4) C20 0.0186(4) 0.0255(5) 0.0264(6) 0.0077(4) -0.0086(4) 0.0000(4) C21 0.0141(4) 0.0198(4) 0.0245(5) 0.0059(4) -0.0060(3) -0.0022(4) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Br1 Ni1 2.3740(3) . ? Br2 Ni1 2.3376(3) . ? Ni1 N1 1.9808(9) . ? Ni1 N2 1.9788(8) . ? O1 C2 1.4663(16) . ? O1 C3 1.3387(12) . ? O2 C7 1.3303(12) . ? O2 C8 1.4641(13) . ? N1 C1 1.5028(13) . ? N1 C3 1.2808(13) . ? N2 C7 1.2845(12) . ? N2 C9 1.4846(12) . ? C1 H1 1.0000 . ? C1 C2 1.5286(17) . ? C1 C10 1.5105(15) . ? C2 H2A 0.9900 . ? C2 H2B 0.9900 . ? C3 C4 1.5120(14) . ? C4 C5 1.5464(16) . ? C4 C6 1.5364(16) . ? C4 C7 1.5073(13) . ? C5 H5A 0.9800 . ? C5 H5B 0.9800 . ? C5 H5C 0.9800 . ? C6 H6A 0.9800 . ? C6 H6B 0.9800 . ? C6 H6C 0.9800 . ? C8 H8A 0.9900 . ? C8 H8B 0.9900 . ? C8 C9 1.5431(14) . ? C9 H9 1.0000 . ? C9 C16 1.5108(13) . ? C10 C11 1.3944(16) . ? C10 C15 1.3930(16) . ? C11 H11 0.9500 . ? C11 C12 1.3944(19) . ? C12 H12 0.9500 . ? C12 C13 1.382(2) . ? C13 H13 0.9500 . ? C13 C14 1.3865(19) . ? C14 H14 0.9500 . ? C14 C15 1.3864(17) . ? C15 H15 0.9500 . ? C16 C17 1.3931(13) . ? C16 C21 1.3965(13) . ? C17 H17 0.9500 . ? C17 C18 1.3913(14) . ? C18 H18 0.9500 . ? C18 C19 1.3895(14) . ? C19 H19 0.9500 . ? C19 C20 1.3914(17) . ? C20 H20 0.9500 . ? C20 C21 1.3916(16) . ? C21 H21 0.9500 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Br2 Ni1 Br1 115.907(7) . . ? N1 Ni1 Br1 97.09(3) . . ? N1 Ni1 Br2 130.66(3) . . ? N2 Ni1 Br1 111.54(3) . . ? N2 Ni1 Br2 108.12(2) . . ? N2 Ni1 N1 90.64(3) . . ? C3 O1 C2 105.45(9) . . ? C7 O2 C8 106.88(7) . . ? C1 N1 Ni1 126.24(7) . . ? C3 N1 Ni1 126.07(7) . . ? C3 N1 C1 107.23(9) . . ? C7 N2 Ni1 125.86(7) . . ? C7 N2 C9 108.31(8) . . ? C9 N2 Ni1 125.31(6) . . ? N1 C1 H1 110.3 . . ? N1 C1 C2 101.27(9) . . ? N1 C1 C10 108.17(8) . . ? C2 C1 H1 110.3 . . ? C10 C1 H1 110.3 . . ? C10 C1 C2 116.02(10) . . ? O1 C2 C1 103.58(8) . . ? O1 C2 H2A 111.0 . . ? O1 C2 H2B 111.0 . . ? C1 C2 H2A 111.0 . . ? C1 C2 H2B 111.0 . . ? H2A C2 H2B 109.0 . . ? O1 C3 C4 114.69(8) . . ? N1 C3 O1 117.23(9) . . ? N1 C3 C4 128.01(9) . . ? C3 C4 C5 107.23(9) . . ? C3 C4 C6 109.72(9) . . ? C6 C4 C5 110.35(10) . . ? C7 C4 C3 112.19(8) . . ? C7 C4 C5 107.71(8) . . ? C7 C4 C6 109.60(9) . . ? C4 C5 H5A 109.5 . . ? C4 C5 H5B 109.5 . . ? C4 C5 H5C 109.5 . . ? H5A C5 H5B 109.5 . . ? H5A C5 H5C 109.5 . . ? H5B C5 H5C 109.5 . . ? C4 C6 H6A 109.5 . . ? C4 C6 H6B 109.5 . . ? C4 C6 H6C 109.5 . . ? H6A C6 H6B 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? O2 C7 C4 114.62(8) . . ? N2 C7 O2 117.36(8) . . ? N2 C7 C4 127.92(9) . . ? O2 C8 H8A 110.9 . . ? O2 C8 H8B 110.9 . . ? O2 C8 C9 104.20(8) . . ? H8A C8 H8B 108.9 . . ? C9 C8 H8A 110.9 . . ? C9 C8 H8B 110.9 . . ? N2 C9 C8 102.55(8) . . ? N2 C9 H9 109.3 . . ? N2 C9 C16 112.88(8) . . ? C8 C9 H9 109.3 . . ? C16 C9 C8 113.32(8) . . ? C16 C9 H9 109.3 . . ? C11 C10 C1 119.76(10) . . ? C15 C10 C1 121.19(10) . . ? C15 C10 C11 118.93(10) . . ? C10 C11 H11 119.8 . . ? C12 C11 C10 120.43(11) . . ? C12 C11 H11 119.8 . . ? C11 C12 H12 120.1 . . ? C13 C12 C11 119.84(11) . . ? C13 C12 H12 120.1 . . ? C12 C13 H13 119.9 . . ? C12 C13 C14 120.22(12) . . ? C14 C13 H13 119.9 . . ? C13 C14 H14 120.0 . . ? C15 C14 C13 119.97(12) . . ? C15 C14 H14 120.0 . . ? C10 C15 H15 119.7 . . ? C14 C15 C10 120.61(11) . . ? C14 C15 H15 119.7 . . ? C17 C16 C9 122.86(8) . . ? C17 C16 C21 119.23(9) . . ? C21 C16 C9 117.77(9) . . ? C16 C17 H17 119.9 . . ? C18 C17 C16 120.25(9) . . ? C18 C17 H17 119.9 . . ? C17 C18 H18 119.7 . . ? C19 C18 C17 120.52(10) . . ? C19 C18 H18 119.7 . . ? C18 C19 H19 120.3 . . ? C18 C19 C20 119.35(10) . . ? C20 C19 H19 120.3 . . ? C19 C20 H20 119.8 . . ? C19 C20 C21 120.37(10) . . ? C21 C20 H20 119.8 . . ? C16 C21 H21 119.9 . . ? C20 C21 C16 120.26(10) . . ? C20 C21 H21 119.9 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Br1 Ni1 N1 C1 -82.05(8) . . . . ? Br1 Ni1 N1 C3 89.16(9) . . . . ? Br1 Ni1 N2 C7 -85.61(8) . . . . ? Br1 Ni1 N2 C9 103.70(7) . . . . ? Br2 Ni1 N1 C1 51.35(9) . . . . ? Br2 Ni1 N1 C3 -137.43(8) . . . . ? Br2 Ni1 N2 C7 145.83(8) . . . . ? Br2 Ni1 N2 C9 -24.86(8) . . . . ? Ni1 N1 C1 C2 155.83(8) . . . . ? Ni1 N1 C1 C10 -81.75(10) . . . . ? Ni1 N1 C3 O1 -168.12(7) . . . . ? Ni1 N1 C3 C4 8.89(15) . . . . ? Ni1 N2 C7 O2 -170.96(7) . . . . ? Ni1 N2 C7 C4 12.92(14) . . . . ? Ni1 N2 C9 C8 166.25(7) . . . . ? Ni1 N2 C9 C16 -71.47(10) . . . . ? O1 C3 C4 C5 79.07(11) . . . . ? O1 C3 C4 C6 -40.79(12) . . . . ? O1 C3 C4 C7 -162.87(9) . . . . ? O2 C8 C9 N2 8.03(10) . . . . ? O2 C8 C9 C16 -113.95(9) . . . . ? N1 Ni1 N2 C7 12.27(8) . . . . ? N1 Ni1 N2 C9 -158.43(8) . . . . ? N1 C1 C2 O1 21.98(12) . . . . ? N1 C1 C10 C11 92.05(11) . . . . ? N1 C1 C10 C15 -83.95(12) . . . . ? N1 C3 C4 C5 -98.01(12) . . . . ? N1 C3 C4 C6 142.13(11) . . . . ? N1 C3 C4 C7 20.05(15) . . . . ? N2 Ni1 N1 C1 166.15(8) . . . . ? N2 Ni1 N1 C3 -22.63(9) . . . . ? N2 C9 C16 C17 -20.60(13) . . . . ? N2 C9 C16 C21 163.80(9) . . . . ? C1 N1 C3 O1 4.47(13) . . . . ? C1 N1 C3 C4 -178.52(10) . . . . ? C1 C10 C11 C12 -175.40(11) . . . . ? C1 C10 C15 C14 175.25(10) . . . . ? C2 O1 C3 N1 10.74(13) . . . . ? C2 O1 C3 C4 -166.67(9) . . . . ? C2 C1 C10 C11 -155.06(10) . . . . ? C2 C1 C10 C15 28.94(14) . . . . ? C3 O1 C2 C1 -20.40(12) . . . . ? C3 N1 C1 C2 -16.74(12) . . . . ? C3 N1 C1 C10 105.67(10) . . . . ? C3 C4 C7 O2 151.76(9) . . . . ? C3 C4 C7 N2 -32.02(14) . . . . ? C5 C4 C7 O2 -90.46(11) . . . . ? C5 C4 C7 N2 85.76(12) . . . . ? C6 C4 C7 O2 29.61(12) . . . . ? C6 C4 C7 N2 -154.17(11) . . . . ? C7 O2 C8 C9 -7.76(10) . . . . ? C7 N2 C9 C8 -5.81(10) . . . . ? C7 N2 C9 C16 116.47(9) . . . . ? C8 O2 C7 N2 4.59(12) . . . . ? C8 O2 C7 C4 -178.77(8) . . . . ? C8 C9 C16 C17 95.42(11) . . . . ? C8 C9 C16 C21 -80.18(11) . . . . ? C9 N2 C7 O2 1.05(12) . . . . ? C9 N2 C7 C4 -175.08(9) . . . . ? C9 C16 C17 C18 -174.91(9) . . . . ? C9 C16 C21 C20 174.43(10) . . . . ? C10 C1 C2 O1 -94.83(11) . . . . ? C10 C11 C12 C13 0.0(2) . . . . ? C11 C10 C15 C14 -0.78(16) . . . . ? C11 C12 C13 C14 -0.6(2) . . . . ? C12 C13 C14 C15 0.5(2) . . . . ? C13 C14 C15 C10 0.18(18) . . . . ? C15 C10 C11 C12 0.69(17) . . . . ? C16 C17 C18 C19 0.53(15) . . . . ? C17 C16 C21 C20 -1.34(16) . . . . ? C17 C18 C19 C20 -0.97(16) . . . . ? C18 C19 C20 C21 0.25(18) . . . . ? C19 C20 C21 C16 0.91(19) . . . . ? C21 C16 C17 C18 0.63(15) . . . . ? _iucr_refine_instructions_details ; TITL mo_p16324_0m_a.res in P2(1)2(1)2(1) REM Old TITL mo_p16324_0m in P212121 #19 REM SHELXT solution in P2(1)2(1)2(1) REM R1 0.076, Rweak 0.025, Alpha 0.004, Orientation as input REM Flack x = 0.049 ( 0.004 ) from Parsons' quotients REM Formula found by SHELXT: C21 Br2 N Ni O3 CELL 0.71073 8.9454 11.7746 20.3499 90 90 90 ZERR 4 0.0009 0.0013 0.0027 0 0 0 LATT -1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H Br N Ni O UNIT 84 88 8 8 4 8 L.S. 10 PLAN 20 SIZE 0.12 0.22 0.24 TEMP -173(2) BOND $H LIST 6 MORE -1 CONF fmap 2 acta TWIN -1 0 0 0 -1 0 0 0 -1 2 REM REM REM WGHT 0.019000 0.222000 BASF 0.01746 FVAR 0.41019 BR1 3 0.254812 0.150098 0.636974 11.00000 0.02850 0.01219 = 0.02285 -0.00096 0.00004 -0.00229 BR2 3 0.613542 0.342555 0.601647 11.00000 0.01490 0.02404 = 0.02752 -0.01100 0.00578 -0.00235 NI1 5 0.359853 0.334718 0.628833 11.00000 0.01388 0.01220 = 0.01132 -0.00264 0.00074 0.00118 O1 6 -0.045045 0.484205 0.583409 11.00000 0.01252 0.03542 = 0.01544 0.00206 -0.00381 -0.00151 O2 6 0.220803 0.547731 0.777931 11.00000 0.01716 0.01789 = 0.01302 -0.00537 -0.00096 0.00400 N1 4 0.184610 0.409551 0.588028 11.00000 0.01651 0.01405 = 0.00967 -0.00044 -0.00154 -0.00167 N2 4 0.329611 0.422785 0.710578 11.00000 0.01202 0.01196 = 0.00980 -0.00038 -0.00033 0.00045 C1 1 0.144406 0.408048 0.516332 11.00000 0.02172 0.02007 = 0.01057 -0.00379 -0.00347 -0.00451 AFIX 13 H1 2 0.165037 0.331514 0.497056 11.00000 -1.20000 AFIX 0 C2 1 -0.023961 0.429646 0.519307 11.00000 0.02102 0.04125 = 0.01582 -0.00198 -0.00697 -0.01046 AFIX 23 H2A 2 -0.056340 0.480300 0.483180 11.00000 -1.20000 H2B 2 -0.080565 0.357546 0.516619 11.00000 -1.20000 AFIX 0 C3 1 0.075907 0.456522 0.618682 11.00000 0.01262 0.01553 = 0.01321 0.00092 -0.00201 -0.00206 C4 1 0.063078 0.480713 0.691431 11.00000 0.01114 0.01873 = 0.01167 0.00105 0.00064 0.00137 C5 1 -0.030310 0.383675 0.722040 11.00000 0.01900 0.03967 = 0.01920 0.00807 0.00149 -0.01070 AFIX 137 H5A 2 -0.131724 0.385318 0.703848 11.00000 -1.50000 H5B 2 -0.034920 0.393690 0.769804 11.00000 -1.50000 H5C 2 0.016531 0.310520 0.711864 11.00000 -1.50000 AFIX 0 C6 1 -0.015032 0.595472 0.702009 11.00000 0.02307 0.03156 = 0.02321 -0.00474 -0.00383 0.01541 AFIX 137 H6A 2 0.051690 0.657027 0.688211 11.00000 -1.50000 H6B 2 -0.039566 0.604537 0.748649 11.00000 -1.50000 H6C 2 -0.107045 0.598054 0.675914 11.00000 -1.50000 AFIX 0 C7 1 0.213248 0.481636 0.725018 11.00000 0.01361 0.01125 = 0.00933 0.00026 0.00097 0.00041 C8 1 0.374044 0.539873 0.802798 11.00000 0.01979 0.01545 = 0.01609 -0.00472 -0.00514 0.00241 AFIX 23 H8A 2 0.374798 0.519473 0.849992 11.00000 -1.20000 H8B 2 0.427672 0.612711 0.796895 11.00000 -1.20000 AFIX 0 C9 1 0.445940 0.445190 0.760969 11.00000 0.01215 0.01259 = 0.01131 0.00005 -0.00067 -0.00129 AFIX 13 H9 2 0.537676 0.475503 0.739038 11.00000 -1.20000 AFIX 0 C10 1 0.236354 0.497695 0.481901 11.00000 0.01691 0.01933 = 0.00846 -0.00057 -0.00210 0.00068 C11 1 0.373746 0.468719 0.454214 11.00000 0.02318 0.02708 = 0.01775 0.00067 0.00278 0.00855 AFIX 43 H11 2 0.405551 0.391740 0.454288 11.00000 -1.20000 AFIX 0 C12 1 0.464755 0.552001 0.426419 11.00000 0.02459 0.04163 = 0.02591 0.00508 0.01045 0.00575 AFIX 43 H12 2 0.558252 0.531791 0.407619 11.00000 -1.20000 AFIX 0 C13 1 0.418610 0.664020 0.426286 11.00000 0.02920 0.03625 = 0.02357 0.01214 0.00383 -0.00317 AFIX 43 H13 2 0.480988 0.720917 0.407748 11.00000 -1.20000 AFIX 0 C14 1 0.281579 0.693631 0.453119 11.00000 0.02954 0.02312 = 0.01962 0.00758 -0.00375 0.00255 AFIX 43 H14 2 0.249806 0.770613 0.452619 11.00000 -1.20000 AFIX 0 C15 1 0.190947 0.610841 0.480680 11.00000 0.01844 0.02176 = 0.01397 0.00031 -0.00207 0.00462 AFIX 43 H15 2 0.097013 0.631464 0.498900 11.00000 -1.20000 AFIX 0 C16 1 0.486368 0.340752 0.800269 11.00000 0.01151 0.01255 = 0.01131 -0.00014 -0.00009 0.00140 C17 1 0.393009 0.246416 0.805061 11.00000 0.01533 0.01431 = 0.01315 0.00100 -0.00104 -0.00142 AFIX 43 H17 2 0.303196 0.243541 0.780204 11.00000 -1.20000 AFIX 0 C18 1 0.430807 0.156399 0.846112 11.00000 0.01993 0.01321 = 0.01473 0.00078 -0.00005 -0.00021 AFIX 43 H18 2 0.366967 0.092093 0.848827 11.00000 -1.20000 AFIX 0 C19 1 0.561190 0.159808 0.883170 11.00000 0.02035 0.01644 = 0.01863 0.00368 -0.00149 0.00499 AFIX 43 H19 2 0.585924 0.098722 0.911663 11.00000 -1.20000 AFIX 0 C20 1 0.655172 0.253564 0.878139 11.00000 0.01860 0.02551 = 0.02640 0.00772 -0.00859 0.00003 AFIX 43 H20 2 0.744703 0.256343 0.903195 11.00000 -1.20000 AFIX 0 C21 1 0.618750 0.343284 0.836607 11.00000 0.01414 0.01976 = 0.02452 0.00588 -0.00603 -0.00223 AFIX 43 H21 2 0.684204 0.406507 0.832961 11.00000 -1.20000 HKLF 4 REM mo_p16324_0m_a.res in P2(1)2(1)2(1) REM R1 = 0.0184 for 9775 Fo > 4sig(Fo) and 0.0214 for all 10383 data REM 256 parameters refined using 0 restraints END WGHT 0.0194 0.2220 REM Highest difference peak 0.390, deepest hole -0.903, 1-sigma level 0.069 Q1 1 0.5411 0.3378 0.8191 11.00000 0.05 0.39 Q2 1 0.4711 0.3987 0.7775 11.00000 0.05 0.31 Q3 1 0.3459 0.3382 0.6868 11.00000 0.05 0.30 Q4 1 0.1365 0.4808 0.7074 11.00000 0.05 0.30 Q5 1 0.4999 0.1561 0.8595 11.00000 0.05 0.29 Q6 1 0.2767 0.4602 0.7178 11.00000 0.05 0.27 Q7 1 0.4224 0.4994 0.7796 11.00000 0.05 0.27 Q8 1 0.3506 0.6774 0.4406 11.00000 0.05 0.26 Q9 1 0.2249 0.6591 0.4607 11.00000 0.05 0.25 Q10 1 0.4120 0.1938 0.8232 11.00000 0.05 0.25 Q11 1 0.3040 0.4836 0.4725 11.00000 0.05 0.24 Q12 1 0.4198 0.5054 0.4332 11.00000 0.05 0.23 Q13 1 0.1290 0.4191 0.6075 11.00000 0.05 0.23 Q14 1 0.2638 0.1524 0.6968 11.00000 0.05 0.22 Q15 1 0.4368 0.3016 0.8019 11.00000 0.05 0.22 Q16 1 0.2314 0.5577 0.4889 11.00000 0.05 0.22 Q17 1 -0.0969 0.5064 0.4983 11.00000 0.05 0.21 Q18 1 0.6207 0.1941 0.8726 11.00000 0.05 0.21 Q19 1 0.2590 0.2576 0.7681 11.00000 0.05 0.21 Q20 1 0.2197 0.3377 0.4629 11.00000 0.05 0.21 REM The information below was added by Olex2. REM REM R1 = 0.0184 for 9775 Fo > 4sig(Fo) and 0.0214 for all 126716 data REM n/a parameters refined using n/a restraints REM Highest difference peak 0.39, deepest hole -0.90 REM Mean Shift 0, Max Shift -0.005. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0214 REM R1_gt = 0.0184 REM wR_ref = 0.0425 REM GOOF = 1.043 REM Shift_max = -0.005 REM Shift_mean = 0 REM Reflections_all = 126716 REM Reflections_gt = 9775 REM Parameters = n/a REM Hole = -0.90 REM Peak = 0.39 REM Flack = 0.000(3) ; _olex2_date_sample_data_collection 2016-08-13 _olex2_date_sample_submission 2016-08-11 _olex2_submission_original_sample_id ((R,R)-Ph-BOX)NiBr2 _olex2_submission_special_instructions 'No special instructions were received' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma 1 0 0 0.4 0.3 -1 0 0 1.2 0.4 -1 0 0 0.1 0.2 1 0 0 -0.2 0.9 1 0 0 0.8 0.3 1 0 0 -0.3 0.9 1 0 0 0.7 0.4 1 0 0 0 0.2 1 0 0 0.1 0.2 -1 0 0 0.6 0.3 -1 0 0 1 0.4 -2 0 0 383.16 21.4 2 0 0 372.96 24.2 2 0 0 372.46 21.5 -2 0 0 403.76 21.6 2 0 0 379.96 21.5 2 0 0 385.06 21.4 -2 0 0 380.76 21.5 2 0 0 381.96 21.5 2 0 0 358.46 23.9 -3 0 0 1.9 0.8 3 0 0 4.3 4.2 3 0 0 -1.7 4 3 0 0 1.4 1 -3 0 0 0.6 1.1 3 0 0 1.8 0.9 3 0 0 2.6 0.8 -3 0 0 1.2 0.8 4 0 0 615.84 36.5 -4 0 0 614.34 44.1 -4 0 0 646.84 36.5 -4 0 0 592.84 44.4 4 0 0 658.03 42.5 4 0 0 642.44 41.8 4 0 0 670.63 36.6 -4 0 0 691.33 36.3 -4 0 0 660.03 36.8 -4 0 0 652.53 36.5 4 0 0 637.84 36.7 -5 0 0 2.8 6.7 5 0 0 -0.3 1.7 5 0 0 3 6.9 5 0 0 2.4 1.6 5 0 0 2 1.5 5 0 0 0.3 8 -5 0 0 2.2 2.1 -5 0 0 2.4 6.9 -5 0 0 1.5 0.7 -5 0 0 2 1.5 -5 0 0 2.3 1.3 -6 0 0 923.31 52.49 6 0 0 907.91 53.19 6 0 0 932.71 53.09 -6 0 0 927.31 61.89 6 0 0 916.91 53.29 6 0 0 938.21 53.09 -6 0 0 916.91 62.29 6 0 0 991 62.79 -6 0 0 922.61 52.89 -6 0 0 921.31 52.99 6 0 0 1042.2 62.39 -6 0 0 942.41 53.39 7 0 0 7.7 11.5 -7 0 0 20.5 11.3 7 0 0 0.2 2.3 -7 0 0 5.1 1.9 7 0 0 5.3 3 7 0 0 4.8 3 -7 0 0 12.5 11.5 -7 0 0 0.9 3 -7 0 0 1 2.3 7 0 0 2.2 2.6 7 0 0 5 13 -8 0 0 2324.07 127.89 8 0 0 2386.66 141.29 -8 0 0 2225.28 128.59 8 0 0 2229.78 128.39 -8 0 0 2244.68 139.89 -8 0 0 2289.87 128.09 8 0 0 2318.97 128.49 -8 0 0 2189.78 140.49 8 0 0 2181.18 128.29 8 0 0 2264.07 128.19 8 0 0 2326.27 139.79 8 0 0 2341.77 128.29 -9 0 0 1.1 14.6 -9 0 0 4.7 3 9 0 0 -0.8 4 9 0 0 2.9 3.7 -9 0 0 -0.4 2.6 9 0 0 28 17.8 -9 0 0 37 18.4 9 0 0 4.4 4.1 9 0 0 0.9 4.3 -9 0 0 4.3 4.7 9 0 0 3.8 3.4 9 0 0 22.8 18.2 -10 0 0 255.87 15.8 10 0 0 247.78 16.8 10 0 0 258.87 16.7 10 0 0 234.28 17.1 10 0 0 237.38 16.4 10 0 0 236.88 16.7 -10 0 0 256.17 16.3 -10 0 0 247.28 17.4 -10 0 0 255.57 15.4 11 0 0 5.9 5 -11 0 0 3.4 4.9 11 0 0 9.5 6.1 -11 0 0 -0.7 3.8 -11 0 0 5 6.4 11 0 0 6.5 5.2 11 0 0 3.6 5.6 -12 0 0 83.99 8.8 -12 0 0 89.69 10.6 12 0 0 82.19 11.1 12 0 0 92.39 10.3 12 0 0 97.89 11.6 -12 0 0 98.59 10.8 13 0 0 -3.4 6.5 -13 0 0 -2.8 8.5 13 0 0 0.4 7.3 13 0 0 -4.2 7 -13 0 0 -1.2 6 14 0 0 17.7 8 14 0 0 19.2 8.7 -14 0 0 13.7 10.2 14 0 0 14.6 9.2 -14 0 0 16.7 7.8 1 -1 0 1621.04 89.59 -1 -1 0 1563.14 89.59 -1 1 0 1508.15 89.59 -1 -1 0 1606.24 89.49 -1 -1 0 1653.63 89.59 -1 1 0 1616.24 89.59 1 1 0 1542.75 89.59 -1 1 0 1639.44 89.59 -1 1 0 1656.63 91.39 -1 1 0 1657.53 89.59 1 -1 0 1599.64 89.59 1 -1 0 1507.35 89.49 -1 1 0 1562.04 89.59 1 1 0 1666.53 89.59 1 1 0 1613.84 89.59 -2 1 0 272.07 18.3 2 -1 0 270.27 15.2 -2 1 0 259.97 17.9 2 -1 0 264.87 15.2 -2 -1 0 271.67 15.2 -2 1 0 255.97 15.1 2 -1 0 274.17 18.3 2 1 0 254.47 15.3 2 1 0 252.47 18.2 2 1 0 285.17 15 2 1 0 251.97 18 2 1 0 266.87 15.2 2 -1 0 260.67 18 2 1 0 262.17 15.1 -2 -1 0 269.37 15.2 2 -1 0 267.87 15.2 -2 1 0 266.77 15.2 2 -1 0 272.17 15.2 -2 -1 0 279.17 15 -2 1 0 274.37 15.2 -3 -1 0 32.3 2.1 -3 1 0 27.6 6.4 -3 1 0 30.8 5.9 3 1 0 35.6 2.5 3 -1 0 34.8 2.6 -3 1 0 28.8 2.6 3 -1 0 30.7 6.8 -3 1 0 27.6 2.4 3 -1 0 22.6 5.5 3 -1 0 28.5 2.4 3 -1 0 26.8 2.4 -3 1 0 30 2.3 3 -1 0 29.3 2.5 3 1 0 29.1 2 3 1 0 26.7 5.9 3 1 0 30.8 2.6 3 1 0 35.1 6.7 -3 -1 0 30.6 2.4 -3 -1 0 28.8 2.4 3 1 0 34.1 2.3 4 1 0 337.37 19.6 -4 1 0 336.17 19.8 4 -1 0 346.97 19.8 4 1 0 344.77 19.6 4 -1 0 358.86 25.5 4 1 0 369.16 26.3 -4 -1 0 340.87 19.6 -4 1 0 349.17 26 4 -1 0 326.77 19.7 -4 -1 0 349.17 19.4 4 1 0 323.07 19.8 -4 1 0 329.47 19.6 4 -1 0 376.66 26.3 4 -1 0 330.97 19.6 -4 -1 0 348.27 19.8 4 -1 0 335.37 19.7 4 1 0 370.36 25.8 -4 1 0 342.97 19.6 4 -1 0 326.27 19.6 -4 1 0 358.86 25.6 5 -1 0 792.72 49.99 5 1 0 744.53 42.8 5 -1 0 807.12 50.79 5 1 0 834.72 50.49 5 -1 0 732.03 42.8 5 1 0 789.52 42.8 -5 -1 0 653.03 51.89 -5 1 0 751.42 43 5 -1 0 765.52 42.8 5 -1 0 749.33 42.9 -5 -1 0 769.92 43 -5 1 0 756.82 50.39 -5 -1 0 651.43 52.69 5 -1 0 751.62 42.9 -5 -1 0 700.63 42.6 -5 1 0 793.92 50.09 5 1 0 742.33 42.9 -5 1 0 743.63 42.7 5 -1 0 746.63 42.8 -5 -1 0 751.52 42.7 5 1 0 820.42 51.09 -5 1 0 771.42 42.7 -6 1 0 226.28 22.8 -6 1 0 199.98 12.9 -6 -1 0 204.68 12.4 -6 -1 0 212.78 22.8 -6 -1 0 206.28 13 6 -1 0 201.58 12.6 -6 1 0 206.58 12.4 6 -1 0 208.68 12.6 6 1 0 219.68 24.2 6 -1 0 207.48 12.7 6 -1 0 211.68 23 6 -1 0 194.98 12.6 6 -1 0 198.08 12.8 -6 -1 0 211.18 12.1 -6 1 0 207.38 13.1 -6 1 0 215.58 12 6 1 0 205.68 12.5 -6 1 0 204.08 23.1 -6 -1 0 189.68 23.3 6 -1 0 214.88 23.7 6 1 0 254.57 23.8 6 1 0 206.48 12.6 6 1 0 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8.4 6 -4 0 100.79 17.8 -6 -4 0 118.39 8.2 6 -4 0 114.99 8.2 6 4 0 87.09 17.1 -6 4 0 122.59 7.9 -6 4 0 116.69 8.3 -6 4 0 84.99 15.4 6 -4 0 142.69 22.4 6 -4 0 117.49 8.6 6 4 0 135.99 19.7 6 4 0 126.29 8.2 -6 4 0 117.79 8.7 6 4 0 119.09 8.7 -6 -4 0 119.19 19 7 4 0 1217.88 67.39 7 -4 0 1249.68 80.79 7 -4 0 1186.88 67.59 -7 -4 0 1167.08 67.29 7 4 0 1167.08 79.59 -7 -4 0 1135.29 79.99 7 4 0 1126.49 67.69 -7 -4 0 1200.48 79.69 -7 4 0 1208.88 67.49 -7 4 0 1170.68 68.39 7 -4 0 1207.78 67.39 -7 4 0 1200.98 67.19 7 -4 0 1164.78 67.59 7 4 0 1156.28 79.99 -7 4 0 1183.38 79.89 7 4 0 1194.08 67.29 -7 4 0 1190.78 67.19 -7 4 0 1145.19 78.59 -7 4 0 1237.88 67.59 -7 -4 0 1232.48 67.79 7 -4 0 1160.08 79.29 -8 4 0 1085.29 77.79 8 4 0 1028.7 77.49 -8 4 0 1119.59 62.19 8 4 0 1014.4 62.19 8 4 0 1100.39 61.89 -8 -4 0 1063.19 62.29 -8 4 0 1081.49 61.59 -8 4 0 1093.79 61.89 -8 4 0 1161.98 76.79 -8 4 0 1124.19 61.69 8 -4 0 1034.7 62.09 8 -4 0 1094.99 62.19 8 -4 0 1091.59 61.89 8 -4 0 1169.38 78.79 8 -4 0 1139.79 77.09 -8 4 0 1099.49 62.09 8 4 0 1062.29 61.79 8 4 0 991.4 75.79 -9 4 0 148.59 10.2 9 -4 0 157.68 31.3 9 4 0 147.99 12.3 -9 4 0 154.88 11.1 -9 4 0 163.98 11.2 9 4 0 115.49 34.9 -9 -4 0 181.78 12.8 9 4 0 157.18 11.7 -9 -4 0 154.78 11.6 9 4 0 192.88 42.6 -9 4 0 157.98 12.3 9 -4 0 179.28 31.1 9 4 0 153.38 11.5 9 -4 0 151.28 12.2 -9 4 0 158.18 12.4 9 -4 0 141.89 12.3 9 -4 0 156.88 11.7 -9 4 0 155.08 12.1 -10 4 0 3.6 5.1 10 -4 0 5.2 4.6 10 -4 0 6.6 5.4 -10 4 0 5.1 4.3 10 4 0 8.4 5.4 10 4 0 9.1 4.6 10 -4 0 2.9 5.5 -10 4 0 8.2 4.5 -10 -4 0 9.5 6.2 -10 4 0 10.2 4.1 -10 4 0 5.7 5.5 10 4 0 12.8 4.9 -10 -4 0 1.7 4.5 -11 4 0 54.39 6.8 -11 -4 0 62.39 7.4 11 4 0 63.09 7.4 11 -4 0 62.19 8.3 -11 4 0 67.29 9.1 11 4 0 53.49 7.8 11 -4 0 51.09 7.2 -11 4 0 64.99 8.4 -11 4 0 76.79 10.1 -11 -4 0 61.29 8.5 -11 4 0 66.49 8.4 11 -4 0 55.99 8.2 11 4 0 60.29 7.3 -12 -4 0 6.8 8.1 -12 4 0 8.7 5.4 12 -4 0 9 7.2 12 -4 0 4.6 6.3 12 4 0 9.7 6.3 -12 -4 0 3.7 4.6 12 -4 0 2 7 -12 4 0 10.3 7.4 -12 4 0 5.7 5.5 -12 -4 0 11.8 6.3 -12 4 0 8 4.9 12 4 0 8.9 6.1 12 4 0 15.1 7.4 12 4 0 4.3 6.7 13 -4 0 91.89 10.5 -13 -4 0 83.09 10 -13 4 0 93.69 11.5 -13 4 0 85.99 11.6 13 4 0 103.39 13.2 -13 -4 0 85.39 16.2 13 4 0 82.99 13.4 14 4 0 43.7 9.3 14 -4 0 43.9 9.2 14 4 0 56.09 9.2 14 4 0 28 9.2 -14 -4 0 46.1 9.2 -14 -4 0 48.9 12 14 4 0 56.59 10.6 -14 4 0 48.7 10.6 14 -4 0 24.9 9.8 14 4 0 34.7 9.1 14 -4 0 47.5 10.4 0 5 0 -1.8 7.6 0 5 0 2.1 1.2 0 5 0 0.5 1 0 -5 0 0.9 0.8 0 5 0 0.6 1.6 0 5 0 10.7 8 0 -5 0 1.1 1.4 0 5 0 0.6 1.2 0 -5 0 2.8 1.1 0 5 0 -1.3 4.6 0 5 0 2.6 5.2 -1 5 0 60.89 4 1 5 0 55.59 9.5 1 5 0 39.5 8 -1 -5 0 69.79 4.2 -1 5 0 61.29 4.4 1 5 0 59.39 4.8 1 -5 0 62.79 4.2 1 -5 0 63.29 3.9 -1 -5 0 68.79 4.5 -1 5 0 68.09 10.8 -1 5 0 65.39 10.8 1 5 0 65.39 4.2 1 5 0 62.79 4.3 -1 -5 0 72.59 13.3 -1 5 0 58.99 4.5 -1 5 0 57.79 4.6 2 -5 0 125.69 7.3 -2 -5 0 119.69 7.3 2 -5 0 106.29 14.6 2 -5 0 119.19 6.9 2 5 0 111.69 7.8 -2 5 0 123.99 14.7 2 5 0 113.29 14.8 2 -5 0 119.09 7.7 -2 5 0 120.69 14.2 -2 5 0 111.69 7.7 -2 5 0 110.59 7.6 -2 -5 0 107.69 14.2 2 -5 0 112.39 7.5 -2 5 0 119.99 7.4 2 5 0 117.99 7.3 -2 -5 0 113.39 7.4 2 5 0 115.79 7 -2 -5 0 127.79 7.3 2 -5 0 115.99 7.4 -2 -5 0 127.49 14.1 -2 5 0 112.99 7.5 2 -5 0 126.19 15.3 2 5 0 119.29 7.3 2 5 0 140.69 15.8 3 5 0 -4.4 7.9 -3 5 0 4.4 1.5 3 -5 0 1.6 1.9 -3 -5 0 3.9 6.6 3 5 0 4.4 1.7 -3 5 0 3.3 1.6 -3 -5 0 7.2 1.7 3 -5 0 4.1 1.5 -3 5 0 3.4 2.1 3 -5 0 9.1 8.4 3 -5 0 4.4 1.5 3 5 0 5.4 2.1 -3 -5 0 -4.7 6.3 -3 5 0 3.4 5.1 -3 5 0 0.6 5.9 3 5 0 4.7 1.5 3 -5 0 5.1 8.3 -3 5 0 2.6 2 3 -5 0 3.4 1.2 -3 -5 0 2.3 1.6 3 5 0 7.1 8 3 -5 0 3.3 2.2 -4 5 0 490.75 28.1 -4 -5 0 498.35 36.5 -4 -5 0 500.85 28.2 -4 5 0 510.95 36.6 -4 -5 0 495.75 28.1 -4 5 0 500.35 36.8 -4 5 0 499.25 28.2 -4 5 0 497.35 28.4 4 -5 0 479.45 28.2 4 -5 0 504.55 37.9 4 5 0 477.85 28.1 4 -5 0 481.55 28.3 4 5 0 500.25 28.6 4 -5 0 478.45 28.4 -4 -5 0 528.45 36.4 4 5 0 459.05 36.7 4 -5 0 495.05 37 4 5 0 470.35 28.1 -4 5 0 482.05 28.5 4 5 0 496.85 37.7 5 5 0 34.5 11.6 5 -5 0 44.7 5 5 -5 0 44.7 12.3 5 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507.55 29.4 8 5 0 499.55 48.1 8 -5 0 535.55 50.29 -8 5 0 454.85 46.2 -8 5 0 505.85 29.7 8 -5 0 474.45 47.6 -8 -5 0 454.75 50.19 8 5 0 501.65 29.3 -8 -5 0 500.45 29.4 -8 -5 0 498.35 30 -8 5 0 491.65 45.7 8 -5 0 466.15 29.8 -8 5 0 518.85 29.6 -8 5 0 531.15 30 -8 -5 0 473.15 49.1 8 5 0 526.45 49.2 8 -5 0 515.55 29.5 8 -5 0 499.95 29.8 -8 5 0 506.05 29.1 8 5 0 446.86 29.8 -9 5 0 84.59 9.3 9 5 0 100.39 9.1 9 5 0 91.49 8.7 -9 5 0 78.89 9.2 -9 5 0 76.89 9 9 5 0 88.09 9.4 -9 5 0 84.09 8.1 9 -5 0 91.19 9.7 -9 -5 0 97.59 8.9 -9 5 0 86.39 8.5 -9 -5 0 83.69 10 9 -5 0 94.79 9.1 9 -5 0 72.59 9.5 -9 5 0 79.49 7.4 -10 5 0 18.6 3.7 -10 5 0 12.5 5.9 -10 5 0 24.1 5.4 10 -5 0 13.4 6 -10 5 0 20.1 4.7 -10 5 0 30 6.1 10 -5 0 15.5 5.2 10 5 0 14.7 5.3 -10 -5 0 15.4 5.3 -10 5 0 19.6 4.6 10 5 0 11.7 4.8 -10 -5 0 19.6 6.6 10 -5 0 19 6.2 10 5 0 12.5 5.9 11 5 0 6.6 5.4 -11 5 0 15.8 6.3 -11 -5 0 6.4 7.3 -11 5 0 5.2 4.7 11 5 0 7.6 5.7 -11 5 0 5.4 6.5 11 -5 0 6.2 6.4 -11 -5 0 4 5.7 11 5 0 7.1 6.3 11 -5 0 7.8 6.7 11 -5 0 9.8 5.8 -12 -5 0 343.07 25.4 12 5 0 353.06 23.7 -12 -5 0 377.46 23.8 12 5 0 364.06 24 12 -5 0 360.56 23.8 -12 5 0 355.26 23.4 -12 5 0 362.56 24.5 12 -5 0 328.57 24.4 12 -5 0 355.46 24.5 -12 5 0 353.46 22.4 12 5 0 346.37 24.1 13 5 0 21.8 8 13 -5 0 24.7 9 13 5 0 4.4 7.7 13 -5 0 16 8.8 -13 -5 0 28.1 10.2 -13 -5 0 25.1 8 13 5 0 21.3 7.6 -13 5 0 31.2 9 13 5 0 19.5 9.4 -14 -5 0 62.69 12.4 14 5 0 46.2 9.4 14 5 0 61.69 10 -14 5 0 45.1 10.8 14 5 0 58.89 10.3 14 5 0 42.3 9.6 14 -5 0 56.99 11 -14 -5 0 61.79 9.9 14 -5 0 56.59 9.6 14 5 0 53.89 11.3 14 -5 0 57.99 11 0 6 0 9482.35 530.95 0 6 0 9568.54 530.55 0 6 0 9302.37 530.65 0 6 0 9142.39 530.75 -1 6 0 424.56 32.1 -1 6 0 445.96 24.7 -1 -6 0 448.46 24.7 1 -6 0 436.66 24.5 1 -6 0 436.86 24.2 -1 6 0 422.96 24.5 1 6 0 415.56 24.5 -1 6 0 412.86 32.3 -1 6 0 426.36 24.6 -1 -6 0 402.46 31 -1 -6 0 455.25 24.4 1 6 0 418.66 24.9 1 6 0 446.66 24.5 1 6 0 424.26 32.2 1 -6 0 432.46 24.7 -1 6 0 423.46 31.7 -1 -6 0 400.86 31.4 -1 -6 0 408.96 24.4 1 6 0 422.86 24.5 -1 6 0 425.66 24.9 1 6 0 416.26 31.6 -1 6 0 418.36 31.4 -2 6 0 406.76 30.3 -2 -6 0 382.86 22.2 -2 -6 0 386.86 29.9 2 -6 0 380.26 22.3 2 6 0 389.06 31.1 -2 6 0 398.36 30.5 -2 -6 0 383.76 22.5 -2 6 0 401.56 22.2 2 6 0 365.96 22.7 -2 6 0 391.66 22.5 -2 6 0 386.16 22.7 -2 -6 0 401.56 22.3 -2 6 0 389.26 22.4 2 -6 0 393.16 31.1 2 -6 0 384.76 22.5 2 -6 0 375.86 22.4 2 -6 0 394.06 22 2 6 0 422.46 30.9 2 -6 0 379.16 30.6 2 6 0 376.86 22.4 2 6 0 384.46 22.3 -2 -6 0 386.16 29.4 2 -6 0 373.56 22.6 2 6 0 396.46 22.1 3 -6 0 7.7 8 3 -6 0 10.9 9.2 -3 -6 0 5.8 7.1 3 -6 0 4.9 2.6 -3 6 0 3.3 2.4 -3 -6 0 4.6 1.9 3 -6 0 1.7 2 3 -6 0 2.3 1.8 -3 6 0 6.5 6.9 3 6 0 4.9 2.5 -3 6 0 1.6 1.5 -3 6 0 5.3 6.5 -3 -6 0 4.3 1.8 3 6 0 2.9 8.7 3 6 0 2 8.3 -3 6 0 1.5 2.1 3 -6 0 3.8 1.8 -3 -6 0 1.3 7 -3 6 0 2.3 1.9 3 6 0 2.1 1.7 3 6 0 2.1 1.8 3 -6 0 1 1.1 -4 6 0 380.26 22.5 4 6 0 380.46 22.1 4 -6 0 379.66 22.2 4 6 0 378.96 22.8 4 6 0 396.36 22.3 4 -6 0 378.26 22.4 4 -6 0 372.46 22.6 -4 -6 0 387.86 31.8 -4 6 0 371.46 32.5 4 6 0 432.96 33.6 4 -6 0 374.16 33.1 4 -6 0 392.36 21.9 4 6 0 392.06 33.8 -4 6 0 388.66 22.3 -4 6 0 388.46 22.7 -4 -6 0 379.56 22.2 -4 -6 0 365.96 22.2 -4 -6 0 409.16 31.6 4 -6 0 354.26 22.2 -4 6 0 380.66 22.1 -4 6 0 387.16 31.9 4 -6 0 378.46 32.6 5 6 0 150.88 10.6 5 -6 0 168.28 25.1 5 6 0 155.18 9.8 5 -6 0 155.28 25.3 -5 -6 0 162.48 21.3 -5 -6 0 150.68 9.9 5 -6 0 158.88 10 -5 6 0 152.18 10.4 -5 6 0 150.38 22.8 5 -6 0 164.28 10.3 5 -6 0 153.08 10.5 -5 -6 0 150.38 8.7 5 6 0 160.28 24.9 -5 -6 0 152.48 10 -5 -6 0 162.28 21.7 5 6 0 134.79 20.4 -5 -6 0 136.49 8.7 -5 6 0 155.18 22.1 -5 6 0 152.78 9.8 -5 6 0 152.08 10 5 -6 0 152.58 9.9 -5 6 0 150.18 10.5 5 6 0 158.38 10 6 -6 0 1266.07 72.99 -6 6 0 1313.07 72.79 -6 -6 0 1300.67 72.79 -6 6 0 1298.47 72.79 6 6 0 1314.47 72.89 6 -6 0 1391.06 86.99 6 6 0 1248.88 71.99 -6 6 0 1301.07 85.59 -6 6 0 1312.17 73.29 6 6 0 1259.17 73.29 6 -6 0 1319.27 85.19 -6 -6 0 1269.67 73.09 -6 -6 0 1278.17 83.49 6 6 0 1305.37 86.29 -6 -6 0 1275.67 84.09 -6 -6 0 1266.67 72.79 6 -6 0 1207.28 73.19 -6 6 0 1382.46 84.99 6 -6 0 1235.38 72.89 -6 6 0 1276.07 73.09 6 6 0 1252.97 72.69 6 6 0 1294.77 85.29 -7 -6 0 15.4 3.7 -7 6 0 17 3.7 7 6 0 14.9 4.6 7 6 0 5.6 15.9 7 -6 0 16 3.5 -7 -6 0 15.4 5 7 6 0 30.6 18.8 7 6 0 13.7 3.7 -7 6 0 15.3 4.2 -7 6 0 20.7 3.7 -7 6 0 21.1 15.1 -7 -6 0 36 15.4 7 -6 0 13.4 16.1 7 -6 0 20.4 4.4 7 6 0 16 3.8 7 -6 0 15.8 16.7 7 -6 0 19.9 4.6 -7 -6 0 -0.3 12.9 -7 6 0 18.5 4.3 -7 6 0 16.3 16 -8 6 0 1715.03 95.39 8 -6 0 1829.32 113.09 -8 -6 0 1638.04 94.89 8 6 0 1706.73 94.89 -8 -6 0 1791.12 109.79 8 6 0 1711.33 112.99 -8 6 0 1732.33 95.29 8 -6 0 1694.03 95.29 8 6 0 1600.94 95.39 8 -6 0 1743.73 95.09 8 6 0 1700.53 111.49 -8 6 0 1484.15 96.29 -8 6 0 1624.74 110.89 -8 -6 0 1758.22 110.19 -8 6 0 1755.52 94.89 -8 -6 0 1634.84 95.39 8 -6 0 1641.04 110.69 -8 -6 0 1646.24 94.99 8 -6 0 1550.74 95.29 -8 6 0 1655.33 109.69 -9 -6 0 32.3 5.5 -9 6 0 42.5 5.4 9 6 0 38.3 5.7 -9 6 0 43.9 6.1 -9 6 0 38.6 6 9 -6 0 35 5.4 9 6 0 32.5 6.4 9 6 0 42.1 5.6 -9 6 0 49.6 6.5 9 -6 0 38.8 6.2 -9 6 0 37.6 4.8 9 -6 0 44.7 6.8 -9 -6 0 50.39 7.1 10 6 0 114.59 10.8 -10 6 0 111.09 10.2 10 -6 0 119.19 12.2 10 6 0 111.89 11.2 -10 6 0 119.19 11.3 10 -6 0 119.09 11.2 10 -6 0 108.09 12.2 -10 -6 0 101.59 12.2 -10 -6 0 108.69 11.1 -10 6 0 112.79 9.3 10 6 0 97.19 11.9 -10 6 0 129.29 11.6 11 6 0 15.8 5.9 -11 6 0 17 6.6 11 6 0 16.9 6.5 11 -6 0 18.3 6.1 11 6 0 16.8 6.2 -11 6 0 20.7 6.3 -11 -6 0 25.9 6.5 -11 6 0 14.6 7.3 -11 6 0 18.4 5.2 11 -6 0 24.8 7.5 11 -6 0 9.9 6.9 -11 -6 0 28.7 7.8 -12 6 0 63.09 9.2 -12 6 0 55.99 6.9 12 6 0 60.59 8.2 12 -6 0 64.49 9.7 -12 -6 0 62.49 8.5 12 -6 0 62.09 8.6 -12 -6 0 58.99 10.2 12 6 0 50.99 8.4 -12 6 0 56.69 8.1 12 6 0 48.8 8.8 12 -6 0 61.29 9.5 13 -6 0 36.3 10.1 13 6 0 29 8.6 -13 -6 0 47.4 11 -13 6 0 45.3 14.1 -13 6 0 34.5 7.5 13 -6 0 47.7 9.7 13 6 0 24.8 9.3 13 6 0 47.1 8.7 13 -6 0 32 8.2 13 6 0 39.1 8.2 -14 6 0 -2.5 9.4 14 6 0 0.9 8.2 14 -6 0 4.8 9.5 -14 -6 0 11.8 11.1 -14 -6 0 0.6 8.8 14 6 0 10.6 8.8 14 6 0 6.9 8.6 14 6 0 9.1 8.5 14 -6 0 5.9 8.5 14 6 0 2.7 9.6 14 -6 0 -7 9.6 0 -7 0 1 1.2 0 7 0 2.3 1.8 0 7 0 -1.3 7.6 0 7 0 -1.6 8.8 0 -7 0 1.8 1.6 0 7 0 5.1 7.4 0 7 0 -2.9 7.6 0 -7 0 2.1 2 0 7 0 -2.2 1.8 0 7 0 1.7 1.9 0 7 0 -0.9 2.4 -1 -7 0 2041.3 116.09 -1 7 0 2041.3 124.09 1 -7 0 1970 115.89 -1 7 0 2098.89 116.09 1 7 0 2053.39 116.09 1 7 0 2019.1 116.39 -1 -7 0 2138.39 115.89 1 7 0 2151.48 124.79 -1 7 0 2189.28 124.19 1 -7 0 1996.6 116.09 -1 7 0 2160.48 124.99 -1 7 0 2032.3 123.89 -1 7 0 2070.89 116.39 1 7 0 2172.28 124.19 1 7 0 2061.89 115.99 -1 7 0 1988.2 116.09 -1 -7 0 1976 115.89 1 7 0 2039.8 115.99 1 -7 0 2104.59 115.69 -1 7 0 2047.3 115.99 -2 7 0 8.9 1.7 2 -7 0 0.2 9.9 2 7 0 12 2.3 2 7 0 9.8 2.4 -2 7 0 9.9 2.6 -2 7 0 7.8 2.7 2 7 0 10.2 2.9 -2 7 0 8.8 8.6 2 7 0 8.6 1.7 -2 -7 0 12.2 7.6 -2 7 0 5.8 1.8 -2 7 0 4.8 2.1 2 -7 0 9.5 2 -2 -7 0 7.9 1.9 2 -7 0 5.5 2 -2 7 0 16 9.4 -2 -7 0 16.5 2.2 2 -7 0 9.8 2.4 -2 -7 0 6.8 2.4 -2 -7 0 -3.3 6.7 2 7 0 25.1 10.5 2 -7 0 14.6 2.8 2 7 0 13.4 10.4 2 -7 0 11.9 1.4 3 -7 0 131.69 21.5 3 7 0 139.99 8.9 3 7 0 142.09 9.1 3 -7 0 142.19 8.2 -3 -7 0 142.89 19.3 -3 7 0 126.99 9.1 -3 7 0 160.08 19.4 -3 7 0 201.68 28.6 -3 7 0 143.79 9.6 -3 7 0 130.99 9.3 3 7 0 164.98 21.3 3 -7 0 137.59 9.2 3 -7 0 135.69 9.5 3 -7 0 144.89 20.6 3 7 0 153.88 22.3 -3 -7 0 134.69 8.8 -3 7 0 134.49 8.6 3 -7 0 140.69 9 -3 -7 0 133.49 19.4 -3 -7 0 136.59 9.2 -3 -7 0 134.19 8.9 3 7 0 128.09 9.7 3 -7 0 135.29 8.9 -4 7 0 327.87 18.9 4 7 0 332.77 19.1 -4 -7 0 365.46 30.4 4 -7 0 323.37 32.4 4 7 0 330.07 32.3 -4 -7 0 304.57 19 4 7 0 333.77 33.5 4 7 0 329.77 19.2 -4 7 0 340.27 19.2 -4 7 0 326.17 31.5 -4 7 0 314.27 19.5 -4 -7 0 328.67 29.5 4 -7 0 324.67 19.1 4 -7 0 296.47 19.6 4 -7 0 316.47 19.2 4 -7 0 322.77 18.6 4 -7 0 303.77 32 -4 7 0 313.87 30.6 -4 -7 0 321.57 19.1 -4 7 0 325.97 19.7 4 -7 0 316.57 19.3 4 7 0 328.07 19.8 -5 -7 0 490.65 41.5 5 7 0 503.55 30.7 5 -7 0 511.85 30.3 5 7 0 564.74 45.6 -5 7 0 527.25 30.6 5 -7 0 527.65 30 5 7 0 513.75 44.5 -5 7 0 474.55 42.6 -5 -7 0 539.25 41.6 5 7 0 506.05 30 5 -7 0 511.65 43.9 -5 7 0 525.05 30.5 -5 7 0 509.25 30.1 -5 -7 0 512.25 30.1 -5 7 0 496.25 42.1 5 -7 0 514.95 30.6 -5 7 0 528.55 30 -5 -7 0 526.25 30 5 -7 0 523.85 30.2 5 7 0 524.25 30.1 5 -7 0 530.65 44.5 5 -7 0 529.85 29.6 6 7 0 1.4 4.3 -6 -7 0 2.9 2.8 6 7 0 3.4 1.6 -6 7 0 -0.6 3 -6 7 0 4.1 3.4 6 -7 0 1.5 2 -6 -7 0 6.6 11.7 -6 7 0 3.5 2.9 -6 -7 0 1.5 3.3 -6 7 0 6.4 15.9 6 7 0 9.2 16.5 -6 -7 0 2.4 11.9 6 7 0 -1.1 2.6 6 -7 0 -5.6 15.8 6 -7 0 4.6 2.9 6 -7 0 9.8 16.9 6 7 0 0.1 3 6 -7 0 0.5 3.1 -6 7 0 -17 13.1 6 -7 0 1.5 4.8 6 7 0 12.9 15.5 -6 -7 0 3.2 3.7 -6 7 0 -1.2 3.5 6 -7 0 2.2 4 7 -7 0 817.42 50.09 7 7 0 846.32 50.19 7 -7 0 823.02 50.09 7 -7 0 865.41 68.49 -7 7 0 862.91 65.89 -7 -7 0 910.11 64.39 -7 -7 0 882.21 49.99 7 -7 0 855.91 49.9 7 7 0 882.81 68.59 7 -7 0 819.92 50.29 -7 7 0 878.31 49.5 -7 7 0 876.61 49.6 7 -7 0 850.01 66.49 -7 -7 0 863.71 49.6 -7 7 0 874.81 49.99 7 7 0 898.71 49.6 -7 7 0 864.21 64.59 -7 7 0 885.91 50.19 7 7 0 850.31 49.5 -7 -7 0 935.31 63.99 7 7 0 877.31 67.19 -7 -7 0 835.12 49.6 -8 7 0 446.56 27.7 8 7 0 461.25 27.4 -8 7 0 463.05 27.9 -8 7 0 471.55 27.2 8 7 0 443.66 28.2 -8 -7 0 455.55 27.8 8 7 0 460.15 27.3 8 -7 0 382.76 53.09 8 -7 0 465.65 27.5 8 -7 0 437.26 27.6 -8 -7 0 477.35 27.4 8 -7 0 430.46 28.1 -8 -7 0 457.65 27.3 8 -7 0 442.86 56.39 -9 7 0 31.6 5.7 -9 7 0 28.5 6.5 9 -7 0 26.3 6.6 9 -7 0 27.3 5.3 -9 -7 0 41.5 6.2 9 7 0 29.4 6.5 -9 7 0 35.8 5.3 -9 7 0 37.7 6.4 -9 -7 0 31.6 6.6 9 7 0 36.9 5.4 9 -7 0 29.1 6.2 9 7 0 32.4 5.6 10 7 0 -3.3 4.8 -10 -7 0 2.7 6.6 -10 7 0 -0.2 4.2 -10 7 0 11.1 6.2 -10 7 0 -0.5 4.5 10 -7 0 2.9 6.5 10 7 0 -7.9 5.7 10 -7 0 2.2 6.2 10 -7 0 5.1 5.6 -10 -7 0 2.4 5.5 -10 7 0 2.9 5.6 -10 7 0 1.3 5.3 10 7 0 4.2 5.3 11 7 0 0.1 5.7 -11 -7 0 1.9 6.1 -11 7 0 7.6 6.1 -11 7 0 -0.8 6.3 11 -7 0 4.4 6 11 7 0 1.5 6 -11 7 0 3.3 5.1 11 -7 0 -1.3 7 11 -7 0 0.9 6.6 -11 -7 0 3.9 7.7 11 7 0 5.3 6.6 12 7 0 149.88 15.6 12 -7 0 137.49 15.9 12 7 0 171.48 15.4 12 7 0 160.28 15.2 -12 7 0 161.48 13.5 -12 7 0 152.08 15.4 -12 -7 0 169.88 15.2 12 -7 0 172.28 15.5 -12 -7 0 130.89 16.7 -12 7 0 160.78 15.3 12 -7 0 141.49 16.6 -13 -7 0 76.09 10.5 13 -7 0 77.99 11.2 13 -7 0 104.79 14.3 13 7 0 82.19 11.1 13 -7 0 84.79 12.1 13 7 0 98.89 13.8 -13 -7 0 90.19 12.8 -13 7 0 62.39 13.4 -13 7 0 86.29 10.2 13 7 0 80.59 16.4 0 -8 0 13 2.3 0 8 0 10.4 9.5 0 8 0 25.1 2.9 0 8 0 13.8 12.6 0 8 0 14.8 2.6 0 8 0 40.9 14.3 0 -8 0 17.7 2.6 0 8 0 18.3 10.9 0 -8 0 15.3 3 0 8 0 14.7 3.3 0 8 0 15.2 2.6 1 8 0 767.12 54.09 1 8 0 758.42 43.4 1 8 0 775.52 43.5 -1 -8 0 752.72 43.6 -1 8 0 782.12 43.5 -1 8 0 759.12 43.5 1 -8 0 785.32 43 1 -8 0 736.93 43.6 -1 8 0 805.42 53.99 -1 8 0 710.33 52.79 -1 8 0 742.23 52.69 -1 8 0 744.53 43.4 -1 8 0 734.53 43.9 1 8 0 725.63 43.9 1 8 0 762.12 53.49 -1 8 0 748.93 54.29 1 8 0 785.42 43.4 1 8 0 771.82 54.29 -1 -8 0 843.32 43.2 1 8 0 777.02 53.39 1 -8 0 757.52 43.3 -1 -8 0 741.43 43.3 2 8 0 95.79 18.2 -2 -8 0 76.79 5.8 -2 -8 0 55.69 12.1 -2 -8 0 68.59 13.8 2 -8 0 70.59 6 -2 8 0 74.49 6.5 2 -8 0 75.19 5.8 -2 8 0 53.29 11.8 2 8 0 72.49 5.4 2 8 0 79.19 5.9 -2 8 0 52.69 14 -2 8 0 74.89 6.4 -2 8 0 70.99 6.1 -2 -8 0 82.39 5.6 2 8 0 75.29 6.1 2 8 0 82.19 17 -2 8 0 52.69 13.6 -2 8 0 73.79 5.8 -2 8 0 60.49 12.4 2 8 0 75.39 6.8 2 -8 0 72.69 4.8 3 -8 0 1409.76 89.29 3 8 0 1379.86 77.49 -3 8 0 1374.96 77.19 3 -8 0 1358.16 76.99 3 -8 0 1388.96 77.59 -3 8 0 1347.17 88.49 3 -8 0 1333.27 77.79 3 8 0 1446.56 89.69 3 8 0 1354.46 77.39 3 -8 0 1330.07 77.39 -3 8 0 1398.26 77.39 -3 -8 0 1418.36 88.09 -3 8 0 1353.46 77.89 -3 8 0 1357.26 87.59 -3 8 0 1386.46 77.59 3 8 0 1328.97 77.99 -3 -8 0 1371.36 77.39 -3 -8 0 1472.15 87.79 -3 8 0 1318.77 77.69 3 -8 0 1315.67 77.59 -3 -8 0 1355.76 77.59 3 8 0 1442.96 88.89 4 -8 0 284.07 32.8 -4 8 0 279.97 18.1 4 -8 0 288.27 16.7 -4 -8 0 297.97 17.3 4 8 0 287.07 17.4 4 -8 0 281.17 18.1 4 8 0 298.67 17.6 -4 8 0 268.77 30.7 4 -8 0 266.87 33 4 -8 0 294.47 17.6 4 8 0 346.97 35.2 -4 8 0 289.47 17.1 -4 -8 0 306.47 30.4 -4 -8 0 275.97 17.5 4 8 0 286.87 32.9 -4 8 0 283.67 17.6 4 -8 0 282.77 17.4 -4 -8 0 321.87 31 -4 8 0 295.27 18 -4 8 0 289.17 30.7 4 8 0 288.67 18.3 4 -8 0 280.37 17.7 5 -8 0 700.13 40.7 -5 -8 0 676.53 53.09 -5 8 0 711.73 40.9 -5 8 0 695.33 40.2 -5 -8 0 710.13 40.5 -5 -8 0 717.63 40.4 -5 8 0 698.83 54.79 5 -8 0 671.73 41.1 5 8 0 711.43 40.4 -5 8 0 693.13 53.89 5 8 0 728.73 56.39 -5 8 0 731.63 41.2 5 8 0 694.03 40.5 5 -8 0 720.23 40.6 5 8 0 671.93 41.2 5 -8 0 711.93 40.4 5 -8 0 683.23 56.09 5 8 0 717.73 56.99 -5 -8 0 700.33 52.89 5 -8 0 679.63 55.59 -5 8 0 722.93 40.6 5 -8 0 707.53 39.9 6 8 0 132.69 25 -6 8 0 141.89 11.1 6 8 0 141.39 11.2 6 -8 0 127.89 11.2 6 -8 0 138.49 10.8 -6 -8 0 146.89 10.4 -6 -8 0 139.99 10.1 6 -8 0 179.88 28.7 -6 8 0 130.79 25 6 -8 0 144.69 10.4 6 8 0 140.49 10.2 -6 8 0 128.09 10.2 6 8 0 138.19 9.9 6 8 0 92.49 23 -6 8 0 133.79 9.6 -6 -8 0 134.69 10.2 6 -8 0 143.39 9 6 -8 0 139.39 25.5 -6 -8 0 161.68 25.9 -6 -8 0 161.38 23.5 6 -8 0 136.59 10 -6 8 0 97.59 20.7 -7 8 0 1078.29 60.79 -7 8 0 1061.39 60.99 7 8 0 1081.29 60.99 -7 -8 0 1052.19 61.29 -7 8 0 1096.09 61.49 -7 -8 0 1089.99 77.19 7 -8 0 985.1 61.49 7 8 0 1043.5 60.89 7 8 0 1078.09 61.69 7 8 0 1088.79 80.39 -7 8 0 1091.79 77.49 -7 -8 0 1065.89 60.89 -7 -8 0 1058.69 60.99 7 -8 0 1076.39 61.09 7 -8 0 1024.1 79.79 7 -8 0 1050.59 61.29 7 -8 0 1074.39 60.89 7 -8 0 1120.69 60.39 7 -8 0 1074.29 80.69 -7 8 0 1061.39 78.59 -7 8 0 1102.39 61.69 -7 -8 0 962.8 76.99 7 8 0 1078.69 81.69 -8 8 0 -1.6 4.1 8 -8 0 -0.8 4.1 8 8 0 -3 5.3 8 -8 0 2.8 5.7 -8 -8 0 3.7 5.1 8 8 0 4.8 4.5 -8 8 0 -1 4.3 -8 8 0 3.7 5.4 8 -8 0 3.8 3.1 -8 -8 0 5.6 4.7 -8 8 0 4.8 5 -8 -8 0 0.6 4.7 8 -8 0 4.3 4.2 8 -8 0 -1.4 5 8 8 0 8.1 4.3 -9 8 0 380.36 24.8 -9 -8 0 381.66 24.6 9 8 0 364.26 24.3 -9 8 0 386.76 24.3 -9 8 0 378.26 23.5 9 -8 0 394.26 23.7 9 -8 0 366.76 24.4 9 -8 0 343.27 24.6 -9 -8 0 370.06 23.7 9 8 0 397.86 23.7 -9 8 0 389.26 23.6 9 8 0 381.06 23.9 -9 -8 0 361.56 23.7 9 -8 0 367.26 23.8 -10 -8 0 7.7 6.8 -10 -8 0 5 5.8 -10 8 0 0.2 6.6 10 -8 0 11.3 5.9 -10 8 0 1 5.1 10 8 0 8.1 5.7 -10 8 0 6.9 4.9 10 -8 0 8 7.2 10 8 0 9.7 5.3 10 -8 0 14.1 6.4 10 8 0 -2.4 6.4 -10 8 0 10.3 5.8 -10 8 0 9.8 6.2 10 -8 0 5 5.5 -11 8 0 43.8 7.7 -11 8 0 42.8 7.7 11 -8 0 24.7 8.6 11 -8 0 37.3 7 11 -8 0 36.4 8 11 -8 0 38.8 7.5 -11 -8 0 42.8 7.8 11 8 0 33 8.2 11 8 0 31.6 7.4 11 8 0 33.2 7 -11 8 0 35.6 6.4 -11 -8 0 33.9 8.9 12 -8 0 14.3 9 -12 8 0 8.8 7.3 -12 8 0 24.7 8.2 12 8 0 29.4 13.2 12 8 0 12.6 8.5 12 8 0 12.8 7.7 12 -8 0 13.5 7.4 12 -8 0 13.6 7.1 -12 8 0 6.2 5.8 12 -8 0 12.2 8.6 -12 -8 0 25.4 7.8 -13 -8 0 99.59 13.5 13 -8 0 92.89 12.4 13 8 0 102.29 11.3 13 8 0 81.99 11.7 -13 -8 0 120.59 15.4 13 8 0 111.99 11.9 13 -8 0 124.99 14.9 -13 8 0 94.59 11.5 13 -8 0 96.69 13.1 -13 8 0 102.09 12.4 13 -8 0 101.69 11.5 0 9 0 1.7 2.3 0 9 0 4.7 2.6 0 9 0 7.4 11.8 0 -9 0 3.9 3 0 -9 0 2.3 2.2 0 9 0 -2.4 11 0 9 0 0.4 3.6 0 -9 0 1.7 1.6 0 9 0 -10 12.6 0 9 0 2 2.5 0 9 0 11.7 11.9 1 9 0 161.48 11.8 -1 9 0 200.18 27.2 -1 9 0 162.58 11 -1 9 0 164.08 22.7 1 9 0 181.18 11.1 -1 9 0 163.98 27.6 1 -9 0 173.68 10.1 1 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22.2 1 0 -3 414.46 22.1 -2 0 -3 120.49 7.1 2 0 3 120.29 7.1 -2 0 3 110.09 8.8 2 0 3 160.18 15.2 -2 0 3 109.29 7.2 2 0 -3 124.19 6.9 2 0 3 114.29 7.2 -2 0 -3 119.99 7 2 0 3 122.69 7 2 0 3 117.39 7.1 -2 0 3 127.39 7.1 -2 0 -3 118.79 11.1 2 0 -3 116.19 6.9 -2 0 -3 110.99 10.6 2 0 3 107.69 11.1 2 0 -3 119.99 6.9 2 0 -3 118.89 8.6 2 0 -3 127.49 8.6 -2 0 -3 128.29 6.9 2 0 3 120.99 6.9 -2 0 3 122.89 7 -2 0 3 126.59 8.9 2 0 -3 131.29 6.9 -3 0 -3 1866.71 107.09 3 0 3 1791.02 107.19 3 0 3 1805.72 107.09 3 0 3 2090.69 112.99 -3 0 -3 2033.6 112.39 -3 0 -3 1818.32 106.99 3 0 -3 2019.6 109.59 -3 0 -3 1861.21 106.99 3 0 -3 1912.91 106.99 -3 0 3 1946.21 109.89 3 0 -3 1870.41 106.99 3 0 -3 2001.2 109.89 -3 0 -3 1995.9 112.69 -3 0 3 1880.91 106.99 -3 0 3 1852.01 106.89 -3 0 3 1875.61 107.09 -3 0 3 1894.61 110.09 -3 0 3 1964.9 106.89 -3 0 3 1893.51 107.19 3 0 3 1993.3 112.19 3 0 -3 1905.41 106.99 3 0 3 1870.81 107.09 -3 0 3 1866.31 106.99 -4 0 3 2091.69 116.09 -4 0 3 2001 115.79 4 0 3 1954.9 115.99 -4 0 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166.68 0 2 3 2943.41 164.08 0 -2 3 2692.53 163.98 0 2 -3 3023.1 165.98 1 -2 3 2019.5 122.19 -1 -2 -3 1977.9 119.49 1 -2 3 2010.6 119.49 1 -2 3 2048.79 122.59 -1 2 3 1981.1 119.49 -1 -2 -3 1998.6 119.49 -1 2 3 2047.6 119.49 1 -2 3 2110.89 119.59 -1 2 3 2084.79 119.49 1 2 -3 2077.89 121.29 -1 -2 -3 2130.69 122.69 1 -2 3 1973 119.49 -1 2 3 2005.6 119.39 -1 2 3 1987.4 119.49 1 2 -3 2090.09 121.19 1 2 -3 2078.69 119.39 1 2 -3 1942.41 119.49 -1 2 3 2066.29 121.79 -1 -2 -3 2057.99 122.79 -1 2 3 2096.59 121.69 1 -2 3 2033.2 119.49 -1 -2 3 2512.55 119.39 1 2 3 2504.95 119.49 -1 2 -3 2444.16 119.59 -1 -2 3 2446.76 119.49 -1 -2 3 2441.76 119.59 1 -2 -3 2451.75 119.59 2 2 -3 497.15 23.7 -2 2 3 410.96 26.4 -2 2 3 510.15 23.6 -2 2 3 413.96 26.6 2 -2 -3 416.16 26.2 2 2 3 392.36 28.2 -2 -2 3 410.66 23.6 2 2 3 391.86 27.9 2 -2 -3 437.16 26.5 -2 2 -3 409.16 23.5 -2 -2 3 414.56 25.7 2 2 3 404.16 23.5 -2 -2 3 401.16 23.5 2 2 3 406.56 23.4 -2 -2 3 403.66 23.4 -2 2 -3 413.86 23.6 2 -2 -3 392.96 23.4 2 -2 -3 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8.9 -4 5 -3 10.1 1.9 -4 5 -3 6.2 2.3 -4 5 -3 11.7 8.9 -4 5 -3 15.6 9.8 4 5 3 7.6 2 -4 -5 3 5.9 2.1 4 5 3 8.2 2.7 -4 5 -3 8.8 2.5 4 -5 -3 6.8 2.2 4 -5 -3 8.1 2.5 4 -5 -3 14.1 9.1 4 -5 -3 12.5 7.8 -4 -5 3 10.3 1.9 -4 -5 3 16.5 7.8 4 5 3 9.6 2.3 4 5 3 11.9 10.8 -4 -5 3 9.9 2.3 -5 5 3 139.99 8.8 -5 5 3 152.08 19.8 5 -5 3 142.39 20.9 5 5 -3 146.99 19.3 5 -5 3 146.39 9.3 -5 5 3 137.69 8.9 -5 -5 -3 152.68 8.6 5 -5 3 168.18 25.2 5 -5 3 140.29 8.7 5 5 -3 131.59 8.9 -5 5 3 142.09 8.3 -5 -5 -3 89.39 16 -5 5 3 140.59 20.2 5 5 -3 141.19 8.2 -5 -5 -3 143.39 8.6 5 5 -3 140.89 8.3 -5 -5 -3 138.19 21 5 5 -3 159.78 19.9 5 -5 3 149.49 8.7 -5 5 3 145.49 8.6 -5 5 -3 84.39 15.3 5 -5 -3 146.29 20.2 5 -5 -3 134.29 19.8 -5 -5 3 114.59 17.9 5 5 3 100.79 18.5 -5 5 -3 108.09 8.9 -5 -5 3 112.59 8.4 -5 5 -3 115.29 8.5 -5 -5 3 117.49 8.3 5 5 3 116.39 8.5 5 -5 -3 114.29 8.8 -5 5 -3 126.79 9.1 5 5 3 95.69 17.7 5 -5 -3 111.79 8.7 -5 5 -3 123.39 20.2 -5 -5 3 124.39 8.6 5 -5 -3 105.69 8.3 5 5 3 109.99 9.2 -5 -5 3 107.39 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-14 5 -3 28.1 9.9 14 -5 -3 30 10.4 -14 -5 3 28.9 11.3 0 6 3 93.59 7 0 6 3 101.39 6.4 0 -6 -3 95.29 14.4 0 6 -3 97.79 6.5 0 6 -3 96.99 15.2 0 6 -3 100.29 6.5 0 6 3 105.19 6.6 0 6 3 95.59 14.8 0 6 -3 104.59 13.6 0 6 3 101.79 6.6 0 -6 -3 105.89 6.5 0 6 -3 96.99 7 0 6 -3 99.49 6.4 0 6 3 98.99 15.5 0 -6 -3 105.89 6.6 0 6 -3 103.79 16 0 6 -3 79.79 12.9 0 -6 3 92.59 5.8 0 -6 3 102.09 6.1 0 -6 3 90.89 6.6 0 -6 3 100.39 6.3 -1 -6 -3 2038.7 118.99 -1 6 3 2029.2 118.69 1 6 -3 1919.41 111.09 -1 6 3 2044.9 118.59 1 6 -3 1999.7 111.09 1 -6 3 1968.3 111.09 1 6 -3 1949.01 111.49 1 -6 3 1928.41 110.79 -1 6 3 2010.5 111.29 1 -6 3 1973.6 110.99 -1 6 3 1950.1 111.19 -1 -6 -3 1956.8 111.19 -1 6 3 1991.3 111.49 -1 6 3 2002.6 117.79 -1 6 3 2012.5 118.39 -1 6 3 2036.3 111.19 1 6 -3 2206.08 118.89 1 -6 3 2005.6 111.29 1 -6 3 1936.81 111.29 1 6 -3 2127.99 117.99 1 6 -3 2012.7 117.39 1 -6 3 1929.91 118.59 -1 -6 -3 2009.2 111.19 -1 6 3 1899.21 110.79 -1 -6 -3 2039.9 118.49 1 6 -3 2038.1 111.19 1 6 -3 2023.1 117.59 1 6 3 1965 111.19 -1 6 -3 1914.51 111.19 -1 6 -3 1939.01 117.79 1 6 3 1977.7 111.59 -1 -6 3 1928.81 110.99 -1 -6 3 1931.91 111.29 1 -6 -3 1959.9 111.29 -1 6 -3 1932.11 111.49 -1 6 -3 1930.71 117.29 1 6 3 2004.9 118.29 1 -6 -3 1915.01 111.19 -1 6 -3 1942.21 111.29 -1 -6 3 1963.5 111.09 1 6 3 1928.61 111.19 -2 6 3 82.29 6.1 2 6 -3 83.09 5.5 2 -6 3 69.89 12 2 -6 3 82.59 14 2 -6 3 84.69 6.3 2 6 -3 106.09 14.7 -2 -6 -3 98.19 14.6 2 -6 3 82.79 5.3 2 -6 3 75.69 5.8 -2 -6 -3 84.89 14.1 -2 6 3 88.29 14.5 2 6 -3 84.99 5.2 -2 6 3 82.39 13.6 -2 -6 -3 80.69 5.7 2 6 -3 89.79 5.6 -2 6 3 100.19 14.9 2 6 -3 86.89 6.2 -2 6 3 83.09 5.6 2 -6 3 82.99 5.7 -2 6 3 83.39 5.6 -2 6 3 55.69 10.9 -2 6 3 85.29 6 -2 -6 -3 80.29 5.6 2 -6 3 87.59 5.3 -2 6 3 86.59 5.4 2 6 -3 99.69 15.1 -2 6 -3 68.59 12.8 -2 6 -3 77.79 6 2 6 3 78.59 6.4 2 6 3 92.19 18.4 2 6 3 62.49 12 -2 6 -3 69.39 6.2 -2 -6 3 71.19 5.8 2 6 3 78.99 5.7 -2 6 -3 74.89 4.9 -2 -6 3 77.49 14.6 -2 -6 3 70.49 5.2 -2 6 -3 74.09 13.3 -2 -6 3 79.79 5.6 2 -6 -3 72.29 5.6 2 -6 -3 77.99 5.8 2 -6 -3 72.79 5.7 2 6 3 74.39 5.5 -2 6 -3 79.19 5.8 -2 -6 3 80.09 14.2 3 6 -3 1827.92 102.89 -3 6 3 1778.22 102.79 -3 -6 -3 1772.62 102.89 3 -6 3 1693.73 102.79 3 6 -3 1741.63 102.79 3 6 -3 1745.83 103.19 -3 -6 -3 1812.12 111.99 3 6 -3 1749.72 102.49 3 -6 3 1929.71 112.49 -3 -6 -3 1816.92 111.29 -3 6 3 1745.93 103.19 3 -6 3 1745.23 102.99 3 6 -3 1880.81 110.79 -3 6 3 1806.42 102.89 3 -6 3 1780.72 103.29 3 -6 3 1775.92 102.99 -3 6 3 1779.22 102.89 -3 6 3 1689.13 102.99 3 6 -3 1860.91 111.09 -3 6 3 1818.02 110.49 3 -6 3 1825.42 111.59 3 -6 3 1729.83 102.79 -3 6 3 1792.92 111.09 3 -6 -3 1843.42 102.39 -3 6 -3 1790.42 102.79 3 6 3 1845.32 102.89 3 6 3 1868.91 102.99 -3 6 -3 1886.01 111.49 3 6 3 1935.91 112.79 3 6 3 1936.81 103.49 3 6 3 1938.41 111.99 -3 -6 3 1899.71 102.89 -3 -6 3 1826.02 102.79 3 -6 -3 1840.32 103.09 3 -6 -3 1837.02 102.99 -3 -6 3 1843.22 102.89 3 -6 -3 1871.91 103.09 3 -6 -3 1824.42 102.89 -3 6 -3 1887.31 103.29 -3 -6 3 1905.81 102.99 3 -6 -3 1986.4 111.39 -3 6 -3 1914.51 110.99 -3 6 -3 1955.3 103.19 3 -6 -3 1862.51 111.19 -3 6 -3 1890.11 102.99 -4 6 3 718.03 42.1 -4 6 3 738.83 41.7 -4 -6 -3 731.03 52.49 -4 6 3 781.52 51.99 4 6 -3 739.53 50.49 4 -6 3 761.22 41.7 -4 6 3 737.43 50.79 -4 -6 -3 710.33 41.9 4 -6 3 713.33 41.9 4 6 -3 697.63 42.2 -4 6 3 738.43 41.9 4 -6 3 701.93 41.7 4 -6 3 721.33 42 -4 -6 -3 708.33 41.8 4 6 -3 711.63 41.8 -4 6 3 715.23 41.8 4 -6 3 707.43 42.3 -4 -6 -3 705.73 51.59 -4 6 3 714.43 42.1 4 6 -3 759.92 51.29 4 -6 3 710.23 52.99 4 -6 3 676.43 51.89 4 6 -3 702.83 41.7 -4 -6 3 734.73 41.9 4 6 3 728.33 42.4 4 6 3 740.73 53.09 4 -6 -3 739.93 42.1 -4 6 -3 747.13 42.3 4 6 3 738.63 41.9 4 -6 -3 714.83 50.99 -4 6 -3 748.53 42.2 4 -6 -3 753.72 41.9 -4 6 -3 733.93 51.99 4 -6 -3 712.63 42.2 -4 -6 3 735.33 49.5 -4 6 -3 768.92 51.69 -4 6 -3 743.83 42 4 -6 -3 769.32 51.49 -4 -6 3 746.43 41.7 4 -6 -3 765.82 41.3 4 6 3 789.62 54.49 4 6 3 752.12 41.5 4 -6 -3 756.92 41.9 -4 -6 3 748.83 41.9 -4 6 -3 748.63 41.6 -4 -6 3 749.13 42 4 6 3 774.82 41.9 -4 -6 3 763.62 50.19 -5 6 3 850.71 49.3 5 -6 3 863.31 61.39 -5 6 3 836.62 49.1 5 -6 3 816.12 49.7 5 -6 3 836.82 49.4 5 -6 3 838.22 49.4 5 6 -3 824.92 49.1 5 6 -3 793.62 49.6 -5 6 3 820.22 59.29 5 -6 3 897.21 62.49 5 6 -3 819.02 58.29 -5 6 3 834.42 49.6 -5 -6 -3 883.71 61.09 -5 -6 -3 845.72 49.3 5 -6 3 852.11 49.1 5 6 -3 844.22 49.2 5 6 -3 820.92 58.79 -5 -6 -3 898.21 60.59 -5 -6 -3 868.01 49.3 -5 6 3 879.61 59.49 -5 6 3 810.82 49.4 -5 -6 3 923.31 49.4 5 -6 -3 916.71 60.19 5 -6 -3 891.71 49.5 -5 -6 3 862.11 57.99 5 6 3 872.81 49.4 5 -6 -3 885.61 49.3 -5 -6 3 929.71 58.09 5 6 3 897.51 48.8 -5 6 -3 914.31 60.59 5 6 3 932.21 63.39 5 -6 -3 896.71 59.49 5 6 3 853.41 49.2 5 6 3 867.11 49.9 -5 6 -3 872.11 49.6 -5 -6 3 884.61 49.2 5 -6 -3 860.81 49.6 5 -6 -3 877.11 49.3 -5 6 -3 896.11 49.4 -5 6 -3 890.21 49.8 -5 6 -3 881.31 49.1 -5 -6 3 854.61 49.3 -5 6 -3 918.41 61.59 5 6 3 897.21 62.09 -6 -6 -3 91.59 7.6 -6 -6 -3 88.79 6.1 -6 6 3 85.39 7.2 -6 6 3 83.09 7.9 -6 6 3 104.79 18.8 6 6 -3 100.39 19.3 6 -6 3 85.09 8.4 -6 -6 -3 91.69 7.5 6 -6 3 94.99 21.4 -6 6 3 84.69 7.7 -6 6 3 87.99 8 6 6 -3 80.29 8.2 6 6 -3 116.49 19.3 6 6 -3 83.89 7.1 -6 -6 -3 144.59 22.7 -6 -6 -3 96.49 19.1 6 -6 3 80.19 7.8 6 -6 3 72.69 18.3 6 6 -3 92.09 7.3 6 6 3 133.09 24.7 -6 6 -3 104.59 8.5 -6 6 -3 99.59 7.7 6 6 3 104.79 7.9 -6 -6 3 99.59 7.7 6 -6 -3 94.29 8.1 6 6 3 104.39 7.6 -6 -6 3 108.39 7.5 -6 -6 3 97.49 16.5 6 -6 -3 94.79 19 6 -6 -3 109.39 8.2 -6 6 -3 146.69 22.3 -6 6 -3 140.39 23.3 6 -6 -3 95.09 19.3 -6 -6 3 107.49 8 6 -6 -3 104.09 7.5 6 6 3 102.19 22.9 6 6 3 115.59 8.8 6 6 3 101.39 5.9 -6 -6 3 84.09 15.6 -6 6 -3 102.19 8.5 -6 6 -3 99.59 7.2 7 -6 3 256.67 37.9 -7 6 3 255.17 16.2 7 -6 3 222.68 32.6 -7 -6 -3 251.87 15.9 -7 6 3 259.97 31.4 -7 -6 -3 236.18 33.4 -7 -6 -3 276.17 34.4 7 6 -3 247.48 15.4 -7 6 3 263.17 15.4 7 -6 3 256.37 16 7 6 -3 264.17 15.6 7 6 -3 274.67 32.3 7 6 -3 236.88 16.4 -7 6 3 258.77 16 -7 6 3 258.27 15.5 7 -6 3 246.18 16.1 7 -6 3 237.88 16.6 -7 6 3 262.17 16.2 -7 -6 -3 252.67 15.7 -7 -6 -3 232.28 14.7 7 6 -3 322.07 33.9 -7 6 3 253.67 32.2 7 6 3 235.08 16.7 -7 -6 3 235.98 15.6 -7 -6 3 235.98 30.3 -7 6 -3 255.17 33.3 -7 6 -3 255.97 16.5 7 6 3 257.87 15.9 -7 6 -3 241.08 15.6 7 6 3 280.77 39.6 -7 6 -3 258.67 34.2 7 6 3 239.98 37.9 7 -6 -3 249.48 16.4 7 -6 -3 245.98 15.7 -7 6 -3 247.88 15.9 -7 -6 3 216.88 29.4 7 -6 -3 233.08 16.1 7 -6 -3 246.48 32.9 -7 -6 3 246.98 15.8 7 6 3 247.08 15.8 7 -6 -3 215.08 32.2 -7 -6 3 259.67 16.2 8 -6 3 19.4 24.1 -8 -6 -3 11.7 4.3 -8 6 3 17.5 3.9 -8 6 3 21.2 4.7 -8 6 3 7.3 4.3 8 6 -3 17.5 4.9 8 -6 3 8 22.3 8 6 -3 15.6 4 8 6 -3 17.5 4.1 -8 -6 -3 15.5 4.1 -8 -6 -3 5.8 16.2 -8 6 3 -1.3 19.3 8 6 -3 22.4 17.6 -8 6 3 65.59 25.2 8 -6 3 16.1 4.2 -8 6 3 17.4 3.6 8 6 -3 11.3 17.8 -8 -6 -3 11.6 16.5 8 -6 3 24.9 5.8 -8 6 3 18 4.8 -8 -6 -3 16.9 5.6 8 -6 3 21.9 4.7 8 6 3 15.1 4.4 8 6 3 14.1 22.9 -8 -6 3 17.8 4.8 8 -6 -3 16.5 5 -8 6 -3 22.4 5.4 -8 6 -3 23.5 17.6 8 -6 -3 12.5 3.8 -8 6 -3 12 4.7 -8 -6 3 12 16.5 8 6 3 15.8 5.5 8 -6 -3 34.8 20.4 8 -6 -3 -3.8 18.4 -8 6 -3 18 4.4 -8 6 -3 -2.4 17 -8 -6 3 0.1 16.1 8 -6 -3 13.6 5.2 -8 6 -3 16.7 4.4 -8 -6 3 20.2 5.3 8 6 3 14.7 4.1 8 6 3 17.2 21.2 9 -6 3 274.07 17.9 9 -6 3 280.47 17.9 -9 -6 -3 280.57 17.6 9 6 -3 290.17 17.3 9 6 -3 256.97 17.8 -9 6 3 279.67 16.7 9 -6 3 255.87 18.4 -9 6 3 276.57 17.9 -9 6 3 290.17 17.9 -9 -6 -3 279.87 18.7 -9 6 3 279.97 17.9 -9 6 3 282.77 16.8 9 6 -3 285.37 17.5 -9 -6 -3 294.07 17.4 -9 6 -3 244.68 17.4 9 -6 -3 236.88 17.8 -9 6 -3 247.38 17.4 9 6 3 256.37 17.5 -9 6 -3 251.07 18.1 -9 -6 3 261.07 17.5 9 -6 -3 251.37 18.2 9 6 3 250.67 17.8 9 -6 -3 236.68 17.2 -9 6 -3 258.67 18.8 9 6 3 243.78 18.3 -9 -6 3 239.18 18.2 -10 6 3 126.99 9.5 10 -6 3 139.59 11.9 -10 -6 -3 135.69 11.1 10 6 -3 124.89 11.1 10 -6 3 116.79 13 -10 -6 -3 119.19 12.8 -10 6 3 131.59 11.3 -10 6 3 129.79 9.7 10 6 -3 134.89 10.7 -10 6 3 119.89 11.7 10 -6 3 125.29 11.9 10 6 -3 114.19 11.4 10 6 3 101.69 12.5 10 -6 -3 95.49 11.8 -10 6 -3 94.99 10.9 -10 6 -3 111.19 12.1 10 6 3 117.29 11.4 -10 6 -3 106.89 12.5 -10 -6 3 106.39 11.2 10 -6 -3 96.39 12.2 10 -6 -3 101.59 10.8 10 6 3 113.79 11.5 -10 -6 3 110.19 12.2 -10 6 -3 103.09 11.3 -11 -6 -3 45.5 8.9 11 6 -3 58.89 7.5 11 -6 3 47.7 7.5 -11 6 3 52.59 7.4 11 6 -3 48.9 7.7 -11 -6 -3 61.59 7.7 11 -6 3 57.29 9 11 -6 3 49 7.9 -11 6 3 58.99 7.5 -11 6 3 52.79 8.3 11 6 -3 53.29 7.1 -11 6 -3 62.19 8.9 11 6 3 60.79 8.1 11 -6 -3 55.29 7.3 -11 6 -3 54.79 8 -11 6 -3 50.59 8 -11 -6 3 56.69 8.7 11 -6 -3 67.69 9.3 -11 6 -3 48.3 7.2 11 6 3 58.99 8.7 11 -6 -3 51.29 8.4 -11 -6 3 50.99 7.6 11 6 3 48.5 7.4 -12 -6 -3 92.69 11.8 -12 6 3 85.09 10.2 -12 -6 -3 91.19 11.6 12 6 -3 92.49 11.6 12 -6 3 85.69 11 12 6 -3 77.49 9.2 -12 6 3 82.39 8.8 12 6 -3 77.19 9.3 12 -6 3 91.89 10 12 -6 3 72.29 9.9 12 -6 -3 82.79 11.7 12 6 3 76.69 9.2 -12 -6 3 89.29 11.1 -12 6 -3 86.49 10.1 -12 -6 3 81.59 9.9 -12 6 -3 91.79 9.8 -12 6 -3 71.19 12.3 12 6 3 77.79 9.7 12 -6 -3 64.79 10.1 -12 6 -3 70.39 8.5 12 -6 -3 69.89 10.1 12 6 3 62.79 10.1 13 -6 3 42 10.4 13 6 -3 44.3 8.1 -13 -6 -3 47.8 8.9 13 -6 3 36 9.3 13 6 -3 44.2 8.5 -13 -6 -3 54.19 11.3 13 -6 3 41.1 10.2 13 6 -3 40.2 8.4 -13 6 3 45.2 10 13 -6 -3 38.7 9.5 13 6 3 45 11.5 -13 6 -3 37.6 9.4 13 6 3 31.1 9.4 13 -6 -3 39.5 8.3 -13 6 -3 33.2 7.4 -13 -6 3 48.9 9.2 -13 -6 3 50.49 10.7 13 -6 -3 50.09 10.1 -13 6 -3 38.1 8.3 13 6 3 41.1 9.4 13 6 3 46.6 8.9 14 6 -3 -5.6 8.4 14 6 -3 -6.3 7.4 -14 6 3 19.7 10 14 6 -3 -0.5 7.8 14 6 -3 2.8 8 -14 -6 -3 6.3 11.6 14 6 -3 -6.5 9.9 14 -6 3 0.3 8.7 14 -6 3 -2.9 10.3 14 -6 3 1 8.7 -14 -6 -3 -8.6 8.1 -14 6 -3 -2.8 9.4 14 6 3 -4.5 9 14 6 3 20 9.3 14 6 3 -2.9 9.1 14 -6 -3 18.4 10.1 -14 -6 3 4.6 10.7 14 6 3 8.9 8.3 14 -6 -3 4.4 7.9 14 6 3 -6.9 9.2 -14 -6 3 12 9 14 -6 -3 1.8 9.7 0 -7 3 1784.42 102.99 0 7 -3 1837.42 110.49 0 7 3 1839.22 111.39 0 7 -3 1799.32 109.99 0 7 -3 1746.93 102.89 0 7 -3 1845.92 102.89 0 7 -3 1860.71 102.89 0 7 -3 1826.22 103.29 0 7 -3 1925.51 111.09 0 7 3 1857.01 103.29 0 7 3 1828.92 110.59 0 7 3 1838.02 102.99 0 7 3 1845.42 111.79 0 7 3 1788.02 102.79 0 -7 -3 1799.02 102.99 0 -7 -3 1767.02 102.89 0 -7 3 1824.02 102.69 0 -7 3 1824.02 102.79 0 7 3 1815.92 102.89 0 7 -3 1917.51 111.69 0 7 3 1907.61 112.49 -1 -7 -3 92.79 15.3 1 7 -3 98.99 16 1 7 -3 98.59 15.8 1 7 -3 105.79 7.6 -1 7 3 106.69 7.8 1 7 -3 109.19 16.2 -1 7 3 110.49 16.9 -1 7 3 108.79 17.4 1 7 -3 109.49 7.7 -1 7 3 101.79 8 -1 -7 -3 121.09 17 -1 -7 -3 104.89 7.9 1 7 -3 102.99 8.3 1 -7 3 111.79 7.5 1 7 -3 113.09 7.9 -1 7 3 88.69 14.4 1 7 -3 126.49 19.4 -1 7 3 97.29 8.4 -1 7 3 103.29 7.6 1 -7 3 105.79 7.4 -1 7 3 115.69 19.3 1 7 3 138.69 7.9 -1 7 -3 136.59 17.4 1 -7 -3 132.19 7.9 1 7 3 139.39 20.3 1 7 3 135.59 8.7 -1 -7 3 140.59 7.5 1 7 3 137.19 19.4 1 7 3 137.49 8 1 -7 -3 142.69 8.1 -1 -7 3 140.39 8.1 -1 7 -3 133.99 8.2 -1 7 -3 136.09 8 -1 -7 3 139.89 7.8 -1 7 -3 139.89 8.6 -2 7 3 173.98 22.6 2 7 -3 176.68 10.5 2 -7 3 190.08 22.9 2 7 -3 176.68 10.9 -2 -7 -3 202.38 21.7 2 -7 3 182.38 10.6 2 7 -3 171.08 11.5 2 -7 3 167.98 10.9 -2 7 3 188.48 20.9 -2 -7 -3 176.68 11 -2 7 3 173.78 11.4 2 -7 3 173.78 11.4 -2 7 3 180.98 21.5 -2 7 3 179.38 10.8 -2 7 3 177.58 11.2 2 7 -3 174.78 10.8 2 7 -3 171.88 20.9 -2 7 3 175.88 10.8 -2 7 3 166.18 10.9 -2 7 3 174.08 20.9 2 -7 3 183.98 10.6 -2 -7 -3 160.18 21.5 2 7 -3 174.78 21.5 2 -7 3 174.98 22.6 2 -7 3 178.08 11.1 -2 -7 -3 176.88 10.9 -3 7 3 305.37 27 -3 7 3 296.97 16.1 -3 7 3 267.07 16.6 3 7 -3 276.87 16.1 -3 7 3 287.87 16.2 -3 -7 -3 288.17 27.6 3 -7 3 274.47 16.3 -3 7 3 260.47 26.8 -3 7 3 261.77 16.4 -3 -7 -3 279.17 26.9 3 7 -3 273.17 16.1 3 -7 3 277.37 15.9 -3 -7 -3 279.07 16.2 -3 -7 -3 279.17 16.3 3 7 -3 274.07 27.9 3 -7 3 280.07 15.9 3 -7 3 288.87 29.5 3 -7 3 278.87 16.8 3 7 -3 286.27 27.4 3 7 -3 258.27 16.7 3 -7 3 281.47 16.4 3 7 -3 274.87 15.6 3 -7 3 248.68 28.3 -3 7 3 278.67 16.1 3 -7 -3 260.17 16.4 3 -7 -3 259.37 16.2 -3 7 -3 257.67 16.5 -3 7 -3 239.68 25.7 -3 -7 3 268.87 15.9 3 7 3 259.37 16.1 -3 7 -3 264.07 15.6 3 7 3 264.67 16.9 3 -7 -3 272.77 15.3 -3 -7 3 278.77 16 -3 -7 3 247.08 16.1 -3 7 -3 269.47 26.6 3 -7 -3 251.97 16.2 3 7 3 271.77 29.9 3 7 3 293.57 29.4 -3 7 -3 264.57 16.8 3 7 3 260.57 16.2 -3 -7 3 270.97 16.2 -3 7 -3 270.27 16.3 -4 7 3 292.17 17.8 4 -7 3 290.67 17.9 4 7 -3 294.97 30 4 -7 3 283.47 17.6 4 7 -3 290.77 17.7 4 7 -3 282.07 17.6 4 7 -3 280.87 18.3 4 -7 3 284.07 17.5 -4 -7 -3 281.97 17.8 4 -7 3 275.37 18.4 -4 -7 -3 287.57 17.8 4 7 -3 264.87 28.7 -4 7 3 313.07 29.1 -4 7 3 343.67 30.5 -4 7 3 271.77 18.1 4 -7 3 281.57 18 -4 7 3 288.87 18.2 4 -7 3 271.47 31.4 4 -7 3 289.57 32.3 -4 7 3 295.47 17.8 -4 -7 -3 300.77 31.1 -4 -7 -3 342.37 30.9 4 7 3 318.27 18.7 4 -7 -3 287.27 30 4 7 3 297.87 32.7 -4 7 -3 309.07 18.1 4 -7 -3 316.87 17.9 -4 7 -3 308.67 18.5 4 7 3 302.47 17.8 -4 7 -3 306.47 29.5 -4 -7 3 300.67 17.7 -4 -7 3 319.27 18 -4 -7 3 313.97 17.7 4 -7 -3 304.17 17.9 4 -7 -3 300.17 18.1 4 7 3 322.37 17.4 4 7 3 308.87 33.4 -4 7 -3 313.17 29.9 4 -7 -3 331.77 31.2 4 -7 -3 296.57 18.2 -4 7 -3 299.77 17.4 -4 7 -3 305.67 18.3 -4 -7 3 304.97 17.8 4 -7 -3 324.87 17 4 7 3 301.07 18 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-3 -4 45.7 6.4 -11 3 4 44.4 8 11 3 -4 45.9 6.5 11 -3 4 43.7 7.9 -11 3 4 37.5 6.6 11 -3 -4 57.19 6.6 -11 3 -4 56.29 8.2 11 3 4 56.69 7.9 11 3 4 47.4 7.7 -11 3 -4 58.69 7.7 -11 3 -4 58.89 6.8 -11 3 -4 59.49 8.1 11 3 4 60.19 7.4 11 3 4 49.5 6.9 -11 -3 4 75.69 9.9 11 -3 -4 62.49 8.3 11 -3 -4 60.69 7.3 -11 -3 4 60.99 8.4 -11 3 -4 65.09 7 -12 3 4 36 7.1 -12 -3 -4 33.9 9 -12 3 4 36.1 8.5 12 3 -4 28.7 6.3 12 -3 4 30 7.5 12 3 -4 26.1 6.6 12 -3 4 27.1 7.4 12 3 -4 29.1 6.7 12 3 -4 29.5 6.6 12 -3 4 28.5 8.2 12 3 -4 29.4 8.5 -12 -3 -4 31.1 6.5 12 -3 -4 39.2 6.6 12 3 4 39.6 7.5 12 -3 -4 30.9 8.1 12 3 4 27.7 7.6 12 -3 -4 38.6 7.3 12 3 4 31.8 7.2 -12 3 -4 44.6 6.1 12 3 4 32.1 7.8 12 3 4 32.5 8.1 -12 3 -4 41.1 8.7 -12 3 -4 45.3 6.8 -12 3 -4 45.4 8.6 -12 3 -4 37 6.6 -12 -3 4 34.8 7.4 -12 -3 4 24.1 8.2 13 3 -4 249.28 19.1 13 3 -4 242.18 18.2 -13 3 4 272.07 24.4 13 -3 4 248.58 19.8 13 -3 4 279.37 20.2 -13 3 4 274.07 19.5 -13 -3 -4 297.67 18.8 13 3 4 233.18 19.5 -13 3 -4 242.68 17.3 13 3 4 214.58 19.6 13 -3 -4 224.98 19.1 -13 -3 4 261.97 19.7 -13 3 -4 246.38 18.2 -13 3 -4 234.78 21.1 13 3 4 257.07 19.7 14 -3 4 51.69 9.6 14 3 -4 49.2 10.6 -14 3 4 61.19 9.5 14 3 -4 36.6 8.2 14 -3 4 33.8 10.6 -14 -3 -4 47.7 8.9 14 -3 4 43.7 9.4 -14 -3 -4 44.3 12 14 3 -4 42.8 9.2 14 3 -4 37.6 8.5 -14 3 4 54.09 11.1 14 3 4 40.8 9.6 14 -3 -4 47 10.4 -14 3 -4 35.2 10.4 -14 3 -4 32.6 10.8 14 3 4 34.8 8.9 14 -3 -4 39.2 8.3 14 -3 -4 39.4 9.3 -14 -3 4 42.4 9.5 14 3 4 46.3 9.8 14 3 4 35.1 10 -14 -3 4 38.3 11.4 14 3 4 37.6 9.7 0 4 4 5044.1 286.77 0 4 4 5276.97 291.47 0 4 -4 5113.09 286.57 0 -4 4 5131.99 290.97 0 4 -4 5353.06 290.47 0 4 4 5316.37 291.17 0 4 -4 5052.69 286.57 0 -4 4 5004.4 290.87 0 -4 4 4736.53 286.57 0 4 -4 5270.77 290.67 0 -4 -4 5090.49 291.67 0 -4 -4 5105.69 291.27 -1 4 4 2174.68 120.89 -1 -4 -4 2109.09 120.69 1 4 -4 2349.67 124.79 1 4 -4 2266.47 124.49 -1 4 4 2329.17 126.09 1 -4 4 2168.28 120.69 -1 -4 -4 2258.57 126.09 -1 4 4 2295.17 125.29 -1 4 4 2192.68 120.69 1 4 -4 2243.28 120.59 1 -4 4 2224.08 125.99 1 4 -4 2146.59 120.79 -1 4 4 2214.08 120.59 1 -4 4 2292.17 120.89 -1 -4 -4 2272.07 126.49 1 -4 4 2176.08 120.49 -1 -4 -4 2218.28 120.59 -1 4 4 2302.47 125.99 1 4 -4 2011 120.69 1 -4 4 2153.98 120.59 -1 4 4 2205.78 120.59 -1 4 4 2317.97 125.69 1 4 -4 2200.18 124.49 1 4 -4 2356.86 125.19 1 -4 4 2195.98 120.69 -1 4 4 2128.59 120.69 1 4 4 2184.48 125.79 1 -4 -4 1949.7 120.69 -1 4 -4 2032 120.79 1 4 4 2189.58 126.19 -1 -4 4 1985.8 120.49 -1 -4 4 2103.49 120.69 1 4 4 2134.29 120.89 1 4 4 2106.69 120.59 1 4 4 1980.5 120.59 -1 4 -4 1940.01 124.89 1 4 4 2016.7 120.59 -1 4 -4 2016.7 124.69 -1 4 -4 2044.6 120.69 -1 4 -4 2067.49 120.69 1 -4 -4 2014.6 120.59 -1 -4 4 2063.49 120.39 -1 -4 4 2108.79 120.59 -1 -4 4 2080.09 120.69 2 -4 4 1892.31 104.39 -2 -4 -4 1964.1 110.79 2 4 -4 1971.1 104.19 2 4 -4 2091.79 109.19 -2 4 4 1954.4 104.49 -2 -4 -4 1918.31 104.39 2 4 -4 1921.31 104.49 -2 4 4 1958.1 104.29 2 4 -4 2059.09 108.79 2 -4 4 1920.71 104.59 2 4 -4 1916.81 104.39 2 -4 4 1840.22 104.39 2 -4 4 1907.81 104.39 -2 4 4 1974.7 109.19 2 4 -4 1884.61 104.29 -2 4 4 1918.21 104.49 -2 -4 -4 1913.71 104.39 -2 4 4 1968.4 104.29 2 -4 4 1914.51 110.69 2 -4 4 1925.11 110.29 -2 -4 -4 2005.7 111.29 2 -4 4 1837.42 104.19 -2 4 4 1909.01 104.59 -2 4 -4 1730.93 104.09 -2 4 -4 1759.22 104.39 2 -4 -4 1769.12 104.39 -2 4 -4 1751.82 104.59 -2 -4 4 1746.33 104.29 -2 -4 4 1729.83 104.19 2 4 4 1820.42 104.29 2 -4 -4 1782.12 104.39 -2 -4 4 1911.71 108.09 2 4 4 1821.02 110.69 2 -4 -4 1770.62 104.39 -2 -4 4 1755.42 104.39 -2 4 -4 1747.53 109.19 2 4 4 1765.82 104.39 2 4 4 1715.03 104.29 2 4 4 1830.92 104.69 -2 -4 4 1827.12 108.29 2 -4 -4 1791.72 104.39 -2 4 -4 1691.23 109.49 -2 4 -4 1793.92 104.49 -3 -4 -4 1865.21 114.89 3 -4 4 1892.31 107.39 3 4 -4 1839.32 107.29 -3 -4 -4 1857.91 107.49 -3 4 4 1901.21 107.49 -3 4 4 1879.71 107.59 3 -4 4 1844.72 107.69 3 -4 4 2023.6 114.69 -3 4 4 1910.91 107.59 -3 4 4 1749.72 107.79 -3 -4 -4 1863.21 114.39 3 4 -4 2068.69 112.79 3 -4 4 1785.42 107.49 3 -4 4 1809.92 107.49 3 4 -4 1946.11 107.39 3 -4 4 2015.1 115.29 3 4 -4 2004.2 112.29 3 4 -4 1899.21 107.59 -3 4 4 1910.81 107.29 -3 4 4 1895.41 107.39 -3 4 -4 1972.9 116.99 -3 4 -4 1919.61 117.69 -3 -4 4 1900.91 107.59 3 -4 -4 1905.11 107.49 3 -4 -4 1937.81 107.59 3 4 4 1967.1 107.49 3 4 4 1884.41 107.49 -3 -4 4 1882.61 107.29 -3 -4 4 2072.49 111.89 -3 -4 4 1879.81 107.49 -3 4 -4 1919.31 107.59 3 -4 -4 1944.61 115.89 -3 4 -4 1948.71 107.79 -3 -4 4 1960.5 111.89 -3 -4 4 1850.11 107.39 3 4 4 1986.5 107.89 3 -4 -4 1905.01 107.39 3 4 4 2014.4 114.99 -3 4 -4 1925.31 107.69 3 4 4 1914.01 115.09 3 -4 -4 1934.21 107.59 -4 -4 -4 362.96 21.4 4 -4 4 361.76 21.7 4 4 -4 367.96 21.5 -4 -4 -4 385.66 21.3 4 4 -4 387.46 28.1 -4 -4 -4 361.46 31 -4 4 4 375.86 21.2 4 4 -4 371.06 27.6 4 4 -4 360.36 21.1 4 4 -4 382.06 21.2 -4 4 4 359.06 21.4 4 -4 4 383.06 31.4 -4 4 4 376.46 21.4 -4 4 4 382.56 21.5 -4 4 4 362.26 21.5 -4 -4 -4 365.06 30.3 4 -4 4 353.06 21.4 4 -4 4 380.86 32.1 -4 4 4 354.66 21.5 4 -4 4 347.27 21.4 4 -4 -4 376.26 21.5 -4 -4 4 366.66 21.4 4 4 4 382.96 22.6 4 -4 -4 405.96 28.6 4 4 4 359.36 31.6 4 4 4 354.16 21.3 -4 -4 4 382.86 27.4 -4 4 -4 363.36 21.5 4 4 4 370.16 21 4 4 4 362.36 21.6 -4 -4 4 376.56 21.4 -4 -4 4 379.96 21.3 -4 4 -4 368.86 21.7 -4 -4 4 367.76 21.5 -4 4 -4 391.76 30.3 4 -4 -4 371.36 21.3 4 -4 -4 366.86 21.6 4 -4 -4 362.96 27.7 -4 4 -4 371.46 21.9 -4 -4 4 361.76 26.6 -4 4 -4 367.26 21.2 -5 -4 -4 572.84 44.5 -5 -4 -4 552.14 34.4 5 4 -4 536.45 34.3 -5 -4 -4 548.75 34.5 -5 4 4 524.75 42.1 5 4 -4 529.15 34.6 5 -4 4 578.44 46.2 -5 4 4 539.15 43 -5 4 4 544.05 34.4 5 4 -4 577.24 41.9 -5 4 4 546.55 34.2 -5 4 4 535.15 34.5 5 4 -4 527.75 34.2 -5 4 4 533.05 34.6 5 -4 4 552.74 34.8 5 -4 4 525.95 34.5 -5 4 4 559.64 34.5 5 4 -4 540.35 41.3 5 -4 4 533.35 45 5 -4 4 547.35 34.5 -5 4 4 512.55 34.4 -5 -4 -4 506.25 44.3 -5 -4 -4 553.24 34.2 -5 -4 4 665.53 41.8 5 -4 -4 677.53 34.8 5 4 4 684.43 34 -5 -4 4 671.03 34.8 -5 4 -4 621.34 44.7 5 4 4 671.63 35.1 5 -4 -4 717.83 43.4 -5 4 -4 668.63 34.5 -5 -4 4 714.33 41.9 5 -4 -4 673.83 42.6 5 4 4 668.83 34.7 5 4 4 710.93 48.2 -5 4 -4 654.13 44.5 5 -4 -4 681.63 34.7 -5 4 -4 676.63 34.9 5 4 4 672.23 46.8 -5 4 -4 669.03 35 -5 -4 4 669.63 34.6 5 4 4 662.13 34.6 -5 4 -4 667.83 34.7 5 -4 -4 662.13 34.5 6 -4 4 885.11 55.39 6 4 -4 915.61 55.09 -6 4 4 882.91 55.39 6 4 -4 900.21 55.39 6 -4 4 841.52 66.89 -6 -4 -4 927.31 55.29 6 4 -4 967.2 63.19 -6 4 4 895.21 64.99 -6 4 4 929.51 55.29 -6 4 4 922.11 55.29 -6 -4 -4 938.91 67.49 -6 4 4 936.61 54.99 -6 4 4 886.71 64.09 6 4 -4 997.9 64.09 6 -4 4 909.41 67.89 6 -4 4 920.61 55.39 -6 -4 -4 937.01 54.89 -6 -4 -4 930.41 55.19 -6 4 4 881.41 55.19 6 -4 4 890.01 55.59 6 4 -4 882.21 54.99 -6 4 4 935.21 55.09 -6 -4 -4 962.3 66.79 -6 4 -4 948.11 66.09 -6 4 -4 1025.2 55.39 -6 4 -4 1071.29 55.79 6 -4 -4 1035.2 55.59 6 4 4 1039 55.89 -6 4 -4 1034.7 55.59 6 4 4 1067.69 69.29 -6 -4 4 1053.59 63.89 6 -4 -4 1141.89 65.19 -6 -4 4 1082.49 55.59 -6 -4 4 1043.9 63.29 6 -4 -4 1013.1 55.19 6 -4 -4 1048.8 63.79 -6 -4 4 1060.99 55.39 6 4 4 1032.8 55.39 6 -4 -4 1010.7 55.39 6 4 4 1114.59 70.39 -6 4 -4 996.3 67.49 -6 4 -4 1045.8 55.49 6 4 4 1021.2 55.39 7 4 -4 939.51 53.99 -7 4 4 987 53.69 -7 4 4 977.1 53.99 -7 4 4 979.3 65.39 7 -4 4 960.2 53.99 7 4 -4 979.9 53.79 -7 4 4 945.31 53.89 7 -4 4 957.3 69.49 7 4 -4 986 63.49 -7 4 4 953.5 54.09 7 4 -4 995.7 53.79 -7 -4 -4 954.2 68.89 -7 4 4 973.4 53.99 -7 -4 -4 965.8 53.39 7 4 -4 1004.3 64.49 -7 4 4 902.21 65.69 7 -4 4 991.4 54.09 -7 -4 -4 1015.4 53.99 -7 4 4 993.2 53.49 -7 -4 -4 985.9 53.79 7 -4 4 952.8 54.39 -7 -4 -4 934.01 67.29 7 -4 4 993.5 70.29 7 4 4 862.91 68.49 7 -4 -4 914.91 53.79 -7 -4 4 931.61 63.69 -7 -4 4 852.21 62.29 -7 4 -4 916.91 54.09 7 -4 -4 951.5 64.19 7 -4 -4 915.91 54.19 7 4 4 914.91 53.99 7 4 4 946.51 70.59 -7 -4 4 947.11 53.89 -7 4 -4 927.21 53.99 7 4 4 924.71 53.89 7 4 4 911.01 54.39 -7 4 -4 917.11 68.19 -7 4 -4 909.81 66.69 -7 4 -4 957.5 54.39 -7 4 -4 912.01 53.99 7 -4 -4 877.71 53.89 -7 4 -4 903.51 53.49 -7 -4 4 917.01 54.19 7 -4 -4 912.61 63.39 -8 -4 -4 1046 57.39 8 -4 4 967.9 57.99 -8 4 4 1072.89 56.99 -8 4 4 1051.39 57.49 -8 -4 -4 1027.4 73.69 -8 -4 -4 1014.2 75.49 8 -4 4 1068.89 76.99 8 4 -4 996.6 68.79 -8 -4 -4 1008.6 56.79 8 4 -4 981.1 57.59 -8 -4 -4 987 57.49 -8 4 4 1001 72.89 -8 4 4 940.71 70.59 -8 -4 -4 989.7 58.09 8 -4 4 1028.8 57.69 -8 4 4 964 57.39 8 -4 4 1030.1 57.69 8 4 -4 1064.09 70.39 8 4 -4 1002.6 57.29 -8 4 4 1066.99 57.09 8 4 -4 1006.3 57.29 -8 4 4 1029.1 57.79 8 -4 4 1090.29 78.19 -8 4 4 1013.8 57.49 -8 4 -4 1019.4 73.59 8 4 4 962.9 57.59 -8 4 -4 1035.3 57.69 -8 4 -4 1025.1 57.79 -8 -4 4 923.61 68.39 8 4 4 963.8 58.09 8 4 4 967.3 75.19 8 -4 -4 994.4 57.89 8 -4 -4 1097.69 70.09 -8 -4 4 930.51 67.59 -8 -4 4 988 57.89 -8 4 -4 1011.8 56.99 8 -4 -4 1008.9 57.39 -8 -4 4 971 57.49 8 -4 -4 941.71 57.49 -8 4 -4 968.8 74.09 -8 4 -4 1025.4 58.09 8 4 4 1015.1 76.89 8 4 4 948.01 58.09 -8 4 -4 1005.5 57.59 8 -4 -4 1077.09 70.59 -9 -4 -4 71.69 7.5 -9 4 4 72.19 7.4 9 4 -4 70.89 7.5 -9 4 4 79.29 6.3 9 -4 4 61.09 25 9 -4 4 82.89 27.6 9 -4 4 78.29 8.5 9 -4 4 75.49 8.6 9 4 -4 71.59 7.3 -9 -4 -4 62.89 7.7 9 4 -4 62.99 7.7 -9 4 4 74.19 7.8 -9 4 4 75.09 6.2 9 -4 4 70.49 9.3 -9 4 4 74.49 7.9 -9 4 4 68.49 8.5 9 4 4 65.89 8.1 9 -4 -4 53.19 7.3 -9 4 -4 62.79 6.6 -9 4 -4 63.99 7.1 -9 4 -4 64.99 6.4 -9 -4 4 47.4 6.2 -9 4 -4 66.89 9.3 -9 4 -4 65.69 8.7 9 -4 -4 52.99 7.9 9 4 4 69.29 8.3 -9 -4 4 50.19 7.1 -9 -4 4 61.59 5.1 9 -4 -4 46.7 6.7 9 4 4 51.09 7.3 10 4 -4 99.69 9.6 10 -4 4 92.99 10.6 10 4 -4 87.99 9.9 -10 4 4 87.19 10.7 10 -4 4 84.99 11.2 -10 4 4 90.49 9.1 10 4 -4 87.39 9.3 -10 4 4 83.69 9.9 -10 -4 -4 93.59 9.4 -10 4 4 99.19 9.4 -10 -4 -4 89.89 12 -10 4 4 99.19 7.9 10 -4 4 87.59 10.3 10 -4 -4 103.49 11.2 -10 4 -4 122.59 11.1 10 -4 -4 106.49 10.3 -10 -4 4 116.89 10.1 10 4 4 102.19 10.3 -10 -4 4 118.99 11.4 -10 4 -4 105.39 10.4 -10 4 -4 107.99 10 -10 4 -4 128.49 12 10 4 4 104.19 10.5 10 4 4 95.89 11.2 -10 4 -4 104.49 8.6 10 -4 -4 100.29 9.6 -11 4 4 72.89 10.3 11 -4 4 71.89 9.5 11 4 -4 65.29 9.4 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9.1 -13 7 -7 26.5 11.3 -13 -7 7 25.2 10.3 13 7 7 11 8.3 -13 7 -7 13.2 8.7 -13 7 -7 28.6 8.5 13 -7 -7 12.3 9.4 13 -7 -7 17.1 8.3 13 -7 -7 17.3 7.3 13 7 7 14.5 9.5 13 7 7 14.6 8.8 0 8 -7 1065.09 70.99 0 -8 -7 1145.49 74.89 0 8 7 1023.1 74.19 0 -8 -7 1118.79 63.19 0 -8 7 1132.79 63.09 0 8 -7 1179.18 74.79 0 -8 7 1090.19 62.59 0 8 -7 1133.89 63.59 0 8 7 1143.59 63.09 0 8 7 1075.79 63.19 0 -8 -7 1117.09 63.09 0 8 -7 1104.19 63.19 0 8 7 1073.29 74.09 0 8 -7 1159.88 74.09 0 8 -7 1136.79 63.19 0 8 -7 1077.19 71.79 0 8 7 1109.59 62.89 0 -8 7 1085.69 63.19 0 8 7 1159.28 63.69 0 -8 -7 1135.69 74.09 -1 -8 -7 120.29 8.7 -1 -8 -7 119.59 8.9 1 8 -7 114.79 18.4 1 8 -7 128.69 19 -1 8 7 109.59 8.8 -1 8 7 98.09 16.9 1 -8 7 106.89 18 1 -8 7 119.39 8.8 1 8 -7 118.39 21.6 1 -8 7 133.39 7.8 1 8 -7 130.19 8.7 -1 8 7 123.69 9.4 1 8 -7 122.99 8.5 1 8 -7 122.59 9.4 -1 8 7 121.29 8.4 -1 8 7 152.68 22.9 1 -8 7 99.49 19.1 1 8 -7 124.19 8.5 1 8 -7 111.69 20.8 -1 8 7 97.99 18.1 1 -8 7 124.29 8.7 -1 8 7 110.89 8.6 1 8 7 167.18 25.4 1 8 7 160.78 25.8 -1 8 -7 140.59 20.7 1 -8 -7 167.48 9.1 -1 8 -7 172.18 20.9 1 -8 -7 155.08 9.1 -1 8 -7 162.28 10 -2 8 7 27.2 12.9 2 8 -7 34.4 4.3 -2 8 7 49.9 14.3 2 -8 7 39.2 4.9 -2 -8 -7 32.1 13.5 -2 8 7 32.8 4.2 -2 8 7 35.2 12.1 2 -8 7 39 14.8 2 -8 7 37.6 4.7 -2 -8 -7 27.3 3.7 -2 -8 -7 26.8 13.4 2 8 -7 38.7 12.6 -2 8 7 26.2 3.9 2 8 -7 38 10.6 2 -8 7 38.7 3.2 2 8 -7 26.3 10.2 2 -8 7 41.9 16 -2 8 7 32.5 4.1 2 8 -7 33.4 12.8 -2 8 7 32.5 12.5 -2 8 7 38 4.4 2 8 -7 29.1 3.6 -2 8 7 22.4 4.3 2 8 -7 30.4 3.9 2 8 -7 35.1 4.5 -2 8 7 33.3 4.5 2 -8 7 36.6 4.7 -2 -8 -7 40.7 4.6 -2 8 -7 32.4 4.7 -2 8 -7 41 13.4 2 8 7 48.2 17.4 2 -8 -7 33.8 4 -2 -8 7 37.2 5 2 -8 -7 30.3 3.9 -2 8 -7 38.6 4.5 -2 -8 7 33.1 4 2 8 7 40.4 5.1 2 8 7 69.59 18.1 2 8 7 38.5 4.6 2 8 7 38.6 4.3 -2 8 -7 33.8 4 2 8 7 38.2 4.9 -2 -8 7 31.1 4.4 -2 -8 7 36.6 3.4 -2 8 -7 61.59 15.8 -2 -8 7 38.7 3.1 -3 8 7 2006.5 122.59 -3 8 7 2025.5 111.29 -3 8 7 2019.1 121.79 3 -8 7 1939.61 111.49 -3 -8 -7 1883.81 124.49 -3 8 7 2036.9 111.69 3 8 -7 2001.3 111.09 3 8 -7 2029.2 119.69 -3 8 7 2041.3 111.69 3 8 -7 2010.9 111.49 -3 -8 -7 2015.6 124.49 3 -8 7 1981.1 111.09 3 -8 7 2021.7 112.09 3 -8 7 1907.71 123.89 3 8 -7 2124.39 121.79 -3 8 7 1972.9 111.79 3 8 -7 1945.11 111.39 3 -8 7 2007.7 111.59 3 8 -7 1949.6 111.89 -3 8 7 1975.2 123.19 3 -8 7 1900.61 111.59 3 -8 7 1922.01 124.49 3 8 -7 2020.2 119.89 -3 -8 -7 2005.7 111.59 -3 -8 -7 2037.1 111.49 -3 8 7 1991 111.39 -3 8 7 2080.89 122.79 3 8 -7 2094.99 120.99 -3 8 7 2055.49 111.99 -3 -8 7 1947.81 111.39 -3 8 -7 1917.71 121.49 -3 8 -7 1921.01 122.09 3 -8 -7 1902.01 111.59 3 8 7 1977.2 125.19 -3 -8 7 1932.51 111.59 -3 -8 7 1854.71 111.09 -3 8 -7 1971.3 111.89 -3 8 -7 2031.5 112.19 3 8 7 2056.89 111.39 3 -8 -7 1901.31 111.59 3 8 7 1976.1 112.19 3 8 7 1937.01 111.49 -3 -8 7 1897.11 111.09 -3 8 -7 1978.6 111.69 3 8 7 1913.81 111.49 4 -8 7 1693.03 95.69 4 -8 7 1692.03 96.09 4 -8 7 1730.93 111.29 4 8 -7 1675.53 95.99 -4 8 7 1618.94 96.29 4 -8 7 1681.93 96.19 4 8 -7 1737.13 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15.1 14 -2 9 215.28 18.8 14 -2 9 155.38 20.4 14 -2 -9 158.78 15.3 14 2 9 158.78 19.4 -14 2 -9 177.08 17.9 -14 -2 9 176.68 19.7 14 2 9 150.58 16.8 -14 -2 9 179.08 18.4 -14 2 -9 186.38 21 14 2 9 170.18 18.2 14 -2 -9 165.28 15.8 14 -2 -9 197.78 18.8 0 -3 -9 843.92 54.39 0 3 -9 849.61 48.8 0 3 -9 859.21 48.7 0 3 9 870.41 48.8 0 -3 -9 879.41 48.8 0 3 -9 826.42 52.09 0 -3 9 848.22 49.1 0 -3 9 836.22 52.99 0 -3 9 886.71 49.1 0 3 -9 866.41 52.59 0 3 9 833.42 53.99 0 -3 9 960.4 49 0 -3 -9 842.32 53.99 0 -3 9 868.51 48.8 0 -3 -9 878.61 48.9 0 3 9 870.41 48.7 0 3 9 907.51 49 0 -3 -9 859.71 48.7 0 3 -9 905.91 49.1 0 3 -9 879.91 48.9 0 3 9 859.11 49 0 3 9 837.22 53.59 0 -3 9 820.72 53.09 1 3 -9 1503.15 85.19 1 -3 9 1451.35 90.49 -1 3 9 1434.46 85.19 1 3 -9 1498.85 87.59 -1 -3 -9 1466.35 85.09 1 -3 9 1534.25 85.59 -1 -3 -9 1563.04 92.09 -1 -3 -9 1510.15 85.39 1 3 -9 1557.24 87.99 -1 3 9 1519.85 85.09 1 -3 9 1526.55 85.19 1 -3 9 1523.05 84.99 -1 3 9 1648.24 85.39 1 3 -9 1517.65 85.29 -1 3 9 1500.55 89.59 -1 3 9 1524.15 85.49 1 -3 9 1586.64 85.49 1 3 -9 1547.55 85.39 1 -3 9 1486.15 91.09 -1 3 9 1509.45 85.09 -1 3 9 1540.15 85.59 -1 -3 -9 1425.96 91.09 1 3 -9 1532.95 85.09 1 -3 9 1471.55 85.49 -1 3 9 1549.05 89.39 -1 3 -9 1533.45 85.59 -1 3 -9 1536.45 85.29 1 -3 -9 1520.85 85.19 1 3 9 1591.14 85.29 -1 3 -9 1395.16 89.79 -1 -3 9 1538.65 85.19 -1 -3 9 1475.65 85.19 -1 -3 9 1472.45 88.39 1 -3 -9 1564.64 85.29 1 -3 -9 1528.15 89.79 1 3 9 1612.84 85.59 -1 3 -9 1592.34 90.09 -1 -3 9 1530.55 85.59 1 3 9 1478.85 85.29 1 3 9 1485.75 91.09 -1 -3 9 1475.25 85.49 1 -3 -9 1538.85 90.19 1 -3 -9 1561.34 85.39 1 3 9 1551.94 85.49 1 3 9 1459.55 91.39 -1 -3 9 1480.35 88.29 2 -3 9 2017.1 112.39 2 3 -9 2175.18 114.79 2 -3 9 2054.79 112.69 -2 3 9 1953.6 112.29 2 -3 9 1965.2 112.69 -2 -3 -9 2061.89 120.39 -2 3 9 2172.98 112.49 -2 3 9 2029.6 112.09 -2 3 9 2013.6 112.69 2 -3 9 2030.3 112.49 -2 3 9 2058.19 116.09 2 3 -9 2036.3 112.49 2 3 -9 2062.19 112.29 2 -3 9 2004.8 112.09 -2 3 9 2134.79 117.19 2 3 -9 1898.71 112.29 -2 -3 -9 1987.5 119.59 2 3 -9 2103.69 114.29 2 3 -9 2133.19 114.59 2 -3 9 1899.01 118.79 2 3 -9 2041.7 112.19 -2 3 9 1989.7 116.29 -2 -3 -9 2030 112.49 -2 3 9 1987 112.69 2 3 -9 1946.31 113.99 -2 3 9 2122.89 117.29 2 -3 9 2030.3 119.89 2 3 9 2039 112.79 2 -3 -9 1954.6 112.39 2 3 9 2005.4 119.39 2 -3 -9 1993.1 112.29 2 -3 -9 1777.82 112.49 -2 -3 9 1881.71 112.39 -2 -3 9 1907.61 112.39 2 3 9 1882.71 119.49 -2 3 -9 2074.69 118.99 -2 3 -9 2028.3 112.79 -2 3 -9 1980.5 118.19 -2 -3 9 1935.81 112.69 2 3 9 1940.91 112.49 2 3 9 1990.5 112.49 2 -3 -9 1956.7 112.49 -2 -3 9 1952.3 112.59 2 3 9 1994.1 112.59 -3 -3 -9 891.71 60.99 3 -3 9 941.21 52.19 -3 3 9 1017.8 56.79 3 3 -9 903.81 51.59 3 3 -9 969.1 51.49 3 3 -9 992 51.49 3 3 -9 969.1 53.69 3 3 -9 981 51.69 3 -3 9 943.41 51.99 3 3 -9 1028.1 53.99 -3 3 9 965.6 55.79 -3 3 9 938.21 51.69 3 -3 9 965.5 51.69 -3 3 9 968.8 56.99 -3 3 9 951.4 51.99 3 -3 9 964.6 51.89 3 -3 9 904.11 61.09 -3 3 9 942.81 56.09 3 3 -9 921.61 53.09 3 3 -9 961.4 53.29 3 3 -9 962.8 51.49 -3 -3 -9 980.1 51.89 -3 -3 -9 911.21 60.49 -3 3 9 1022.8 51.79 -3 3 9 920.01 51.89 3 -3 9 958.8 60.89 -3 3 9 961.1 52.19 -3 -3 9 839.92 51.79 3 3 9 860.71 51.89 3 3 9 878.31 51.89 3 3 9 841.12 59.99 -3 3 -9 844.62 58.49 -3 3 -9 866.21 52.19 3 -3 -9 872.01 51.89 3 3 9 896.41 52.29 -3 -3 9 848.32 51.79 3 -3 -9 883.61 51.59 -3 -3 9 874.31 51.89 3 3 9 858.51 60.79 3 -3 -9 854.81 51.89 3 -3 -9 787.62 51.79 -3 3 -9 836.92 58.89 3 -3 -9 855.21 51.59 -3 -3 9 857.31 52.19 3 3 9 882.11 51.89 -4 -3 -9 20.5 2.6 -4 3 9 16.9 2.9 4 -3 9 22.7 2.4 -4 3 9 19.1 6.7 4 -3 9 22.9 2.7 -4 3 9 22.7 2.3 -4 3 9 26.9 3.1 -4 3 9 21.8 2.8 4 3 -9 20.4 2.3 -4 -3 -9 24.9 11.4 4 3 -9 22 2.1 4 -3 9 15.3 11.7 4 3 -9 16.4 2 -4 -3 -9 27.6 11.7 4 3 -9 16.8 5 4 3 -9 18.9 4.9 4 3 -9 20.2 2.1 -4 3 9 24.1 7.9 -4 -3 -9 22.2 2.9 4 -3 9 13.6 12.8 -4 -3 -9 18.4 2.1 4 -3 9 24.1 3.2 -4 3 9 19.3 6.9 -4 3 9 26 8.1 4 -3 -9 16.4 1.9 -4 3 -9 21.1 11 4 3 9 2.4 9.7 -4 3 -9 10.6 9.6 4 3 9 14.1 2.6 -4 3 -9 13.4 3.1 -4 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1116.29 58.49 6 3 -9 1091.39 60.19 6 -3 9 1138.39 78.49 6 -3 9 1077.79 61.09 -6 3 9 1048 60.69 6 -3 9 1095.69 60.49 -6 -3 -9 1102.49 60.69 6 3 -9 1078.59 59.89 -6 3 9 1050.89 67.59 -6 3 9 1067.59 60.29 6 3 -9 1103.09 64.29 -6 -3 -9 1111.69 60.59 -6 3 9 1106.09 60.99 6 -3 9 1098.69 76.49 6 3 -9 1106.29 64.69 6 -3 9 1121.69 60.79 -6 -3 -9 1078.19 60.29 -6 -3 -9 1119.49 75.79 6 3 -9 1077.49 60.19 -6 -3 -9 1124.99 74.59 6 3 -9 1095.59 60.19 -6 3 9 995.1 67.89 -6 3 9 1094.79 60.59 6 3 9 997 75.99 6 -3 -9 1034.8 60.29 6 -3 -9 1059.29 66.69 -6 -3 9 1031.4 64.09 6 -3 -9 1019.2 66.19 6 -3 -9 1074.39 60.79 6 3 9 1055.79 61.19 -6 3 -9 1028.6 72.49 6 3 9 1032 60.59 -6 -3 9 1038.2 60.79 -6 -3 9 1024.3 60.79 -6 3 -9 1052.09 60.99 6 3 9 978.2 74.99 6 3 9 1032.5 60.69 -6 -3 9 1055.69 60.69 6 -3 -9 1080.69 60.49 -6 3 -9 1069.19 73.89 -6 -3 9 1006.8 64.29 -6 -3 9 1076.99 60.29 -6 3 -9 1064.09 60.69 6 3 9 1097.39 60.19 7 -3 9 551.64 30.7 -7 3 9 479.25 40.8 7 -3 9 549.65 30.3 7 -3 9 513.15 31 7 3 -9 548.45 30 -7 -3 -9 570.44 30.6 7 3 -9 548.95 30 -7 -3 -9 509.55 47.8 -7 -3 -9 491.55 46.1 7 3 -9 537.05 36 -7 3 9 528.65 30.6 -7 3 9 480.95 39.7 -7 3 9 545.85 30.3 7 3 -9 519.95 36.3 7 -3 9 512.35 54.09 -7 -3 -9 535.55 30.4 -7 -3 -9 540.95 30 -7 3 9 528.65 30.9 -7 3 -9 517.65 30.7 -7 3 -9 508.35 31 -7 -3 9 522.75 30.8 7 3 9 516.35 30.6 7 3 9 566.44 53.79 7 -3 -9 501.05 30 7 3 9 477.25 50.59 7 3 9 500.05 30.5 7 -3 -9 542.85 37.9 7 3 9 501.65 31.9 7 -3 -9 536.05 32.8 7 -3 -9 532.35 30.2 -7 -3 9 494.25 36.3 -7 -3 9 511.75 29.8 -7 3 -9 453.15 45.4 -7 -3 9 486.25 30.5 7 -3 -9 541.05 38.7 -7 -3 9 468.25 35.8 -7 3 -9 473.55 47.3 8 3 -9 53.39 12.9 8 -3 9 48.3 6.5 -8 3 9 46.6 5.7 -8 -3 -9 41.9 5.2 -8 3 9 46 15.7 8 -3 9 52.99 41.4 8 3 -9 45.1 6.7 8 -3 9 33.8 5 -8 -3 -9 31.3 4.9 -8 -3 -9 38.2 19 -8 3 9 41.7 16 8 3 -9 33.7 5 8 -3 9 44.9 5 -8 -3 -9 36 4.7 -8 3 9 39 5.8 8 -3 9 35 35.8 -8 3 9 44.6 5.4 8 3 -9 36.4 12.1 -8 -3 -9 30.2 15.9 8 3 -9 41.9 4.2 8 3 9 28.3 5.9 -8 -3 9 34.5 5.8 8 -3 -9 40.5 6 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37.1 6.6 10 -3 -9 39.7 7.2 -10 3 -9 32.9 7 -10 -3 9 24.6 6.1 -10 -3 9 46.3 7.5 10 3 9 34.8 6.5 10 3 9 25.6 5.7 -10 3 -9 34 6.7 10 -3 -9 40.2 5.1 10 -3 -9 36.7 5.7 -11 -3 -9 90.19 8.7 11 -3 9 78.39 10.2 -11 -3 -9 65.59 10.1 11 3 -9 72.19 8.7 11 3 -9 77.39 8.3 -11 3 9 86.29 11.9 11 3 -9 72.59 9.3 -11 3 9 78.89 11 11 -3 9 74.69 10.1 11 -3 9 73.79 8.6 11 -3 -9 56.29 8.8 11 -3 -9 72.99 9.4 11 3 9 72.29 8 -11 3 -9 66.79 8.6 11 3 9 82.79 11.5 -11 -3 9 76.19 9.4 -11 -3 9 73.59 8.7 -11 3 -9 77.99 8.8 -11 3 -9 85.89 9.6 11 -3 -9 62.59 8.6 11 3 9 64.99 9.4 11 3 9 77.59 8.9 -12 -3 -9 10.7 9 12 -3 9 12.8 7.1 12 -3 9 0.3 8.4 12 3 -9 8.7 5.1 -12 3 9 13.5 8 12 3 -9 4.7 5.2 -12 3 9 3.2 7 12 3 -9 7.6 7.8 12 -3 9 6.6 6.4 12 -3 -9 4.6 7.6 -12 3 -9 7.4 8.2 12 3 9 9.7 7.9 12 3 9 13.7 8.4 12 3 9 15.3 7.4 -12 -3 9 -0.9 7.9 -12 3 -9 -1.9 8.2 12 -3 -9 6.7 6.1 12 -3 -9 5.9 5.1 -12 3 -9 6.9 8.8 -12 -3 9 4.3 7 12 3 9 12.4 6.7 -12 3 -9 12.4 6.9 12 3 9 4.8 6.1 13 -3 9 52.79 11.5 13 3 -9 58.79 11.2 13 3 -9 55.59 7.9 13 -3 9 49 8.9 13 3 -9 59.59 7.8 -13 -3 -9 73.99 12.5 -13 3 9 50.59 9.8 -13 3 9 56.79 11 13 -3 9 75.99 10.1 13 -3 -9 72.89 10.7 -13 -3 9 97.59 11.8 -13 -3 9 75.49 10.3 13 3 9 63.59 10.1 -13 3 -9 55.59 9.5 13 -3 -9 86.49 10.8 13 3 9 69.69 11 13 3 9 75.59 11.3 13 3 9 84.79 10.3 13 -3 -9 87.39 13 -13 3 -9 69.49 10 -13 3 -9 83.79 13.1 13 3 9 76.29 9.2 -13 3 -9 79.09 11.8 14 3 -9 66.89 8.3 14 -3 9 62.39 12.4 -14 -3 -9 42.9 12.6 -14 3 9 66.69 10.6 -14 3 9 58.19 12.1 14 -3 9 57.69 9.4 14 3 -9 51.09 8.3 14 -3 9 60.49 10.3 14 3 -9 53.29 11.4 14 3 9 48.7 11.3 -14 -3 9 58.09 10.7 -14 3 -9 49.7 9.6 14 -3 -9 55.29 9.3 -14 -3 9 50.99 11.9 14 3 9 33.5 9.3 -14 3 -9 53.79 12.3 14 -3 -9 40.1 10.3 14 3 9 48 11.2 14 3 9 42.6 9.1 14 -3 -9 47.5 8 0 4 9 337.37 26.1 0 -4 9 333.67 25.3 0 4 -9 329.97 24.2 0 -4 9 369.86 19.6 0 4 -9 350.56 19.3 0 -4 9 339.77 19.7 0 4 9 294.37 19.5 0 -4 -9 355.76 19.5 0 4 9 338.87 19.3 0 4 9 297.57 19.2 0 4 -9 362.36 19.7 0 4 9 319.37 25.5 0 -4 -9 350.16 19.3 0 -4 -9 343.47 26 0 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-9 326.67 18.8 2 4 -9 66.39 4.7 -2 4 9 59.49 5.3 2 4 -9 77.69 10 -2 4 9 65.99 4 2 4 -9 66.89 4.3 -2 -4 -9 62.99 12.7 2 -4 9 49.5 11 2 4 -9 60.99 9.6 -2 4 9 64.49 10.7 -2 4 9 70.99 10.6 2 -4 9 68.69 5.3 -2 4 9 69.29 4.3 2 -4 9 67.29 4 2 -4 9 57.89 5.1 2 4 -9 60.09 8.4 2 -4 9 64.89 4.7 2 -4 9 65.89 3.8 -2 4 9 64.59 11.3 2 4 -9 67.69 4.6 2 4 -9 64.19 4.4 2 4 -9 64.69 8.7 2 -4 9 54.39 11.5 -2 4 9 66.29 10.5 -2 4 9 69.29 4.9 -2 4 9 68.99 4.2 -2 4 9 57.99 5.2 -2 -4 -9 52.79 12 2 -4 9 68.19 4.6 2 4 9 109.79 16.7 -3 -4 -9 430.76 22.6 -3 4 9 403.56 22.8 -3 4 9 400.76 22 3 4 -9 369.86 26.2 -3 4 9 387.66 28.4 3 4 -9 360.46 26.2 3 4 -9 415.36 22.1 -3 4 9 404.16 29.5 -3 4 9 427.86 22 -3 4 9 402.36 28.1 3 -4 9 426.06 22.7 -3 4 9 420.46 29.3 3 -4 9 429.46 22.9 3 4 -9 397.26 22.3 3 4 -9 419.26 22.1 3 4 -9 427.16 26.5 3 -4 9 417.06 22.5 3 -4 9 411.06 22.4 3 4 -9 433.16 22.2 -3 4 9 439.86 22.5 3 4 -9 430.66 22.2 3 -4 9 395.96 33.3 3 -4 9 421.36 34 -3 -4 -9 357.26 32 -3 4 9 431.06 22 3 4 -9 436.26 26.3 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9 665.03 36.2 4 -4 -9 693.83 36.3 -4 4 -9 676.43 46.8 4 4 9 674.23 36 4 4 9 640.64 36.2 -4 4 -9 670.73 36 4 -4 -9 665.83 35.9 5 4 -9 80.09 5.3 -5 4 9 85.39 5.4 5 -4 9 90.49 5.7 -5 4 9 83.19 14.2 -5 4 9 89.19 13.7 -5 -4 -9 86.99 17.6 -5 4 9 89.99 6 5 -4 9 86.89 18.9 5 -4 9 89.69 6.2 -5 -4 -9 69.29 16.3 -5 4 9 89.99 6.8 -5 -4 -9 89.49 6.1 -5 -4 -9 82.89 6.1 5 -4 9 81.19 6.9 5 4 -9 99.19 12.5 5 -4 9 82.29 18.7 5 4 -9 83.39 11.9 5 -4 -9 59.89 5.1 5 -4 -9 57.29 6.1 -5 4 -9 58.99 5.5 -5 -4 9 59.89 5.3 -5 4 -9 47.1 13.1 -5 -4 9 49.9 9.1 5 4 9 68.99 18.1 5 4 9 51.89 6.2 5 -4 -9 58.99 5.6 -5 -4 9 50.69 5.8 -5 4 -9 52.59 6.7 -5 4 -9 30.9 12.6 -5 -4 9 52.89 9 5 -4 -9 55.69 5.8 -5 -4 9 54.09 6.4 5 4 9 60.69 17.8 -5 -4 9 54.09 5.9 5 4 9 59.09 6.8 5 4 9 54.89 5.7 6 4 -9 918.21 51.59 6 4 -9 977 57.39 -6 4 9 930.11 51.79 6 4 -9 894.71 56.49 6 -4 9 922.31 52.59 -6 4 9 927.31 51.99 6 -4 9 934.01 51.89 6 -4 9 958.6 70.39 6 -4 9 867.51 67.59 -6 -4 -9 936.01 51.69 6 4 -9 907.91 51.69 -6 -4 -9 894.31 51.99 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19.8 8 2 -10 315.97 18.2 -8 2 10 277.67 29.8 -8 -2 -10 313.97 18.3 8 -2 10 314.47 19.4 -8 -2 -10 320.87 19.3 -8 -2 -10 280.17 39.6 -8 2 10 305.87 18.7 8 -2 10 310.87 20.2 8 -2 10 329.97 49.4 -8 2 10 298.87 30 -8 2 10 301.07 19.4 8 2 -10 320.27 18.4 8 2 -10 350.26 26.3 8 2 -10 309.87 18.4 8 -2 10 362.96 54.99 8 -2 10 307.87 18.9 8 2 -10 339.97 26.8 8 -2 -10 304.47 19.7 -8 2 -10 349.87 42.3 -8 -2 10 308.17 19.9 8 2 10 312.17 19.4 8 -2 -10 311.27 18.5 -8 2 -10 304.57 19.9 -8 -2 10 326.57 18.3 8 -2 -10 310.57 28.9 8 2 10 299.47 18.8 8 2 10 288.57 19.5 -8 2 -10 312.67 17.9 -8 -2 10 300.87 19.4 -8 -2 10 295.97 26.8 -8 -2 10 276.87 26.2 8 2 10 303.87 20.3 -8 2 -10 307.67 20 8 -2 -10 314.17 18.7 -8 2 -10 244.08 39.9 8 -2 -10 274.77 28.2 -9 2 10 472.85 29.1 -9 -2 -10 517.35 28.7 9 2 -10 492.75 38.5 9 -2 10 473.95 29.7 9 -2 10 604.74 70.69 -9 2 10 482.85 29.5 9 2 -10 495.15 28.1 -9 -2 -10 514.65 28 9 2 -10 497.75 28 9 -2 10 491.15 28.6 9 2 -10 485.85 27.9 -9 2 10 506.25 28.2 9 -2 10 483.65 30.1 9 -2 10 476.35 65.39 -9 -2 -10 472.65 29.9 9 2 -10 492.85 38 -9 2 -10 434.06 55.89 -9 -2 10 451.35 29.3 9 2 10 493.65 66.49 -9 2 -10 471.55 29.4 9 -2 -10 472.15 28 -9 -2 10 445.06 37.6 9 -2 -10 473.05 28.2 9 -2 -10 478.45 29.3 -9 -2 10 463.15 37.3 -9 -2 10 469.15 29 9 2 10 480.25 29.1 9 2 10 463.15 29.1 9 2 10 460.05 29.7 -9 2 -10 362.96 56.59 9 2 10 456.45 63.79 -9 2 -10 487.85 27.6 9 2 10 466.65 28.5 -9 2 -10 474.05 29.4 -10 -2 -10 103.09 8.1 10 -2 10 96.59 10.8 10 2 -10 91.19 9.1 -10 2 10 79.69 11.1 10 -2 10 89.09 12.2 -10 2 10 80.39 10.6 10 2 -10 86.59 8.3 10 -2 10 74.69 9.4 10 2 -10 86.49 8.1 -10 -2 -10 88.99 12.7 -10 -2 -10 89.99 9.9 10 2 -10 88.79 11.3 10 2 10 88.99 9.4 -10 -2 10 93.89 10.6 10 -2 -10 104.99 8.5 10 2 10 108.59 11 10 -2 -10 101.39 8.9 -10 2 -10 127.59 11.1 10 2 10 98.79 11.1 -10 2 -10 99.69 11.4 -10 -2 10 87.39 11.3 10 2 10 101.19 11.9 10 -2 -10 91.59 11.1 11 2 -10 58.19 8.7 11 2 -10 57.59 7.8 -11 2 10 64.49 9.1 -11 -2 -10 59.69 9.6 -11 -2 -10 71.89 7.8 -11 2 10 58.19 8.3 -11 -2 -10 60.99 6.9 11 -2 10 57.19 9.1 11 -2 10 53.89 7.6 11 -2 10 50.19 7.1 11 2 -10 61.29 7.7 11 2 10 57.59 9.2 -11 -2 10 51.19 7.8 11 -2 -10 54.29 6.8 -11 2 -10 57.79 9 -11 -2 10 46.7 8.6 -11 2 -10 55.19 7.9 11 2 10 54.99 8 11 2 10 52.69 7.1 11 -2 -10 55.39 8.6 11 2 10 44.4 7.9 11 2 10 42.1 9 11 -2 -10 43.5 5.9 -12 2 10 18.3 7.3 12 2 -10 21.6 5.4 -12 2 10 23.6 8.5 12 -2 10 29.9 6.7 12 -2 10 22.5 8.7 12 2 -10 27.7 8.2 12 2 -10 23.6 5.4 12 -2 10 30.2 7.6 -12 -2 -10 26.3 9.4 12 -2 -10 10.2 5.1 -12 -2 10 13.6 8.4 -12 2 -10 11.9 6.7 -12 2 -10 13.8 8.4 12 2 10 17.7 6.6 12 2 10 19.7 8.6 12 -2 -10 19.7 8.4 12 2 10 14.2 7.6 -12 2 -10 15.9 7.5 -12 -2 10 12.8 7.8 12 2 10 2.4 5.9 12 -2 -10 22.4 6.2 12 2 10 24 8.7 13 2 -10 25.4 9.2 -13 2 10 22.6 8.5 13 -2 10 23.6 7.3 -13 2 10 38.6 10.1 13 -2 10 19.2 10.2 13 -2 10 22.5 8.5 -13 -2 -10 17.3 10.7 13 2 -10 21.7 6 13 2 -10 27.1 6.4 -13 2 -10 21.7 8.6 13 2 10 30.3 9.8 -13 -2 10 29.8 9.8 13 2 10 18.5 7 13 -2 -10 15.2 9.1 13 -2 -10 22.5 6 13 2 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10 -1 3 10 185.08 10.3 1 -3 10 181.58 17.8 1 3 -10 177.98 9.9 1 -3 10 149.39 17.5 1 -3 10 178.98 10 1 3 -10 180.58 9.8 -1 -3 -10 174.58 10.2 1 3 -10 153.18 12.9 1 -3 10 176.78 10.6 1 -3 10 176.48 10 1 3 -10 177.28 13.5 -1 3 10 171.38 15.7 1 3 -10 170.58 10.1 -1 3 10 167.98 10.5 1 -3 10 176.78 9.7 -1 3 10 176.78 9.8 -1 -3 -10 168.78 17.4 1 -3 10 177.58 10.7 -1 -3 -10 165.08 17.9 -1 -3 -10 178.78 9.8 -1 3 10 178.28 10.7 1 -3 -10 174.98 10 -1 3 -10 167.58 10.6 1 3 10 164.08 17.4 1 3 10 162.18 10.5 1 3 10 167.48 10 1 -3 -10 163.38 10 1 3 10 165.88 10.1 -1 -3 10 162.68 10.1 -1 -3 10 152.98 14.3 -1 -3 10 167.38 10 -1 -3 10 162.58 10.6 1 3 10 154.48 18 1 -3 -10 160.58 15.4 1 -3 -10 156.28 14.9 -1 -3 10 158.18 14.4 -1 3 -10 165.28 15.5 -1 3 -10 160.08 10 -1 -3 10 159.88 10.5 1 3 10 173.28 10.5 -1 3 -10 156.38 15.8 1 -3 -10 163.98 10.3 2 3 -10 880.21 50.79 2 -3 10 907.61 50.69 -2 3 10 870.31 50.99 2 -3 10 884.71 50.59 -2 3 10 869.61 50.59 2 -3 10 898.21 50.99 2 3 -10 883.01 50.39 -2 3 10 932.21 50.69 2 3 -10 824.12 50.49 -2 3 10 881.11 55.59 -2 3 10 907.51 55.69 2 3 -10 870.21 52.19 2 -3 10 848.52 58.49 2 3 -10 867.61 52.59 -2 3 10 856.71 54.39 -2 -3 -10 848.32 58.69 2 3 -10 869.61 52.39 -2 3 10 883.71 50.99 2 3 -10 876.21 52.69 2 -3 10 887.81 50.99 -2 3 10 833.82 54.59 -2 -3 -10 875.61 58.29 2 -3 10 795.72 57.49 2 -3 10 832.92 50.89 -2 -3 -10 861.61 50.69 2 -3 -10 971.2 50.69 2 3 10 972.6 50.89 2 3 10 959.5 51.09 2 3 10 972.9 50.69 -2 -3 10 949.51 50.99 2 -3 -10 972 50.59 -2 3 -10 915.81 57.49 2 -3 -10 979.5 50.89 -2 -3 10 936.61 50.99 2 3 10 922.21 50.79 2 -3 -10 849.02 50.79 2 3 10 896.81 59.09 -2 -3 10 989.8 50.79 2 3 10 870.01 58.19 -2 3 -10 903.11 56.79 -2 -3 10 923.21 50.69 -2 3 -10 924.61 51.09 3 3 -10 1505.25 79.89 -3 3 10 1463.95 84.99 3 3 -10 1539.15 80.19 3 -3 10 1486.45 80.29 -3 3 10 1477.25 80.49 -3 3 10 1406.96 84.09 3 3 -10 1424.06 79.99 -3 3 10 1559.74 84.99 3 -3 10 1455.25 89.39 3 -3 10 1457.95 80.59 3 3 -10 1540.65 81.39 -3 -3 -10 1513.55 80.29 -3 3 10 1472.85 80.39 -3 3 10 1385.76 84.29 -3 -3 -10 1491.45 90.29 -3 3 10 1495.55 80.59 3 -3 10 1512.35 80.09 3 -3 10 1467.45 80.49 3 3 -10 1557.54 79.89 3 -3 10 1443.66 89.89 -3 3 10 1474.25 80.09 -3 -3 -10 1500.65 89.69 3 3 10 1397.26 80.29 3 -3 -10 1209.78 80.09 -3 -3 10 1361.06 80.29 3 -3 -10 1341.37 79.99 -3 -3 10 1385.66 80.39 -3 -3 10 1340.07 80.39 3 -3 -10 1394.16 80.29 -3 3 -10 1382.56 88.09 3 -3 -10 1372.46 80.29 3 -3 -10 1364.16 79.99 -3 3 -10 1344.97 87.29 3 3 10 1436.86 80.69 3 3 10 1286.77 89.09 3 3 10 1360.56 80.29 3 3 10 1316.67 88.59 -3 -3 10 1317.57 80.19 -3 3 -10 1352.96 80.59 -4 3 10 1886.31 106.49 4 3 -10 1945.11 105.79 -4 3 10 1910.41 106.39 -4 -3 -10 1872.71 117.19 -4 3 10 1957.9 106.39 4 3 -10 2005.5 107.39 4 3 -10 1975.7 105.89 4 3 -10 2037 107.29 -4 -3 -10 1881.61 106.49 -4 -3 -10 1921.21 106.29 -4 3 10 1848.12 105.99 -4 3 10 1905.11 110.29 4 3 -10 1855.01 105.89 4 -3 10 1937.61 118.09 4 -3 10 1919.81 116.89 -4 -3 -10 1797.72 115.99 -4 -3 -10 1938.01 106.09 4 -3 10 1890.01 106.59 -4 3 10 1923.31 109.99 4 3 -10 1998.6 105.99 4 -3 10 1882.41 106.39 -4 3 10 1989.4 110.99 4 -3 10 1916.21 106.29 4 -3 10 1895.71 106.09 -4 3 10 1899.01 111.19 -4 -3 10 1747.83 106.19 -4 -3 10 1886.61 106.29 -4 3 -10 1846.12 114.89 4 3 10 1841.22 106.29 -4 3 -10 1885.91 106.69 4 3 10 1936.11 106.69 4 3 10 1765.32 116.69 4 -3 -10 1721.63 106.09 -4 -3 10 1900.21 106.29 4 -3 -10 1783.32 105.99 4 3 10 1871.01 116.69 4 3 10 1898.61 106.19 4 3 10 1826.42 106.29 -4 3 -10 1791.12 115.39 -4 -3 10 1857.51 106.49 4 -3 -10 1940.31 106.39 4 -3 -10 1851.11 106.29 -5 -3 -10 1121.79 76.09 5 -3 10 1056.89 76.79 5 3 -10 1139.69 65.69 5 -3 10 1157.08 64.09 -5 3 10 1113.79 69.99 -5 3 10 1095.29 68.29 -5 -3 -10 1142.19 77.29 5 3 -10 1121.79 63.59 5 -3 10 1136.89 78.79 -5 -3 -10 1113.19 64.19 -5 3 10 1113.29 69.39 -5 3 10 1119.59 64.09 -5 3 10 1124.89 64.09 -5 -3 -10 1140.69 63.99 5 3 -10 1147.19 63.49 5 -3 10 1175.38 65.49 -5 -3 -10 1128.29 63.69 -5 3 10 1074.59 64.29 5 3 -10 1129.59 63.49 5 -3 10 1108.69 63.79 -5 3 10 1101.99 68.59 5 3 -10 1183.18 65.89 5 3 10 1139.19 63.79 5 3 10 1131.89 64.09 5 3 10 1156.68 77.29 5 -3 -10 1194.38 64.19 5 3 10 1146.39 63.99 5 3 10 1130.09 64.49 -5 -3 10 1101.89 64.19 -5 3 -10 1103.79 64.39 5 -3 -10 1216.38 63.79 5 -3 -10 1153.18 63.69 5 3 10 1121.19 78.39 -5 -3 10 1130.19 63.99 -5 -3 10 1155.08 63.99 -5 3 -10 1109.59 75.09 -5 -3 10 1123.29 64.09 -5 3 -10 1042.6 73.89 -6 -3 -10 464.75 26.4 6 -3 10 463.75 26.4 -6 -3 -10 490.25 42.4 6 -3 10 463.25 26.8 -6 3 10 453.85 26.6 -6 3 10 430.86 33.5 -6 -3 -10 474.45 26.3 6 -3 10 463.65 71.49 6 -3 10 470.15 26 6 3 -10 473.45 29.3 6 3 -10 463.15 25.6 -6 -3 -10 464.45 25.8 -6 3 10 432.86 34.1 6 3 -10 460.45 25.6 -6 3 10 458.35 26.2 -6 -3 -10 467.45 43.2 -6 3 10 457.65 26.4 6 3 -10 450.65 29.5 6 3 -10 461.35 25.4 -6 -3 10 443.66 25.9 6 3 10 424.86 26.3 6 -3 -10 467.55 32.8 -6 3 -10 444.76 26.4 -6 3 -10 430.16 26.7 6 -3 -10 449.06 25.9 -6 -3 10 419.26 29.4 -6 -3 10 439.16 26.5 -6 3 -10 395.86 46.5 6 3 10 458.95 25.7 -6 -3 10 429.06 26.5 -6 -3 10 427.56 26.2 6 -3 -10 452.65 26.5 -6 3 -10 472.35 50.19 6 3 10 409.16 45.3 6 3 10 429.76 26.2 -6 -3 10 416.96 29.7 6 3 10 430.86 26.9 6 -3 -10 433.46 25.7 6 -3 -10 408.76 32.4 6 3 10 435.56 45.2 -7 3 10 193.28 24.3 7 3 -10 186.28 10.9 -7 -3 -10 198.48 12.2 -7 -3 -10 188.08 11.1 7 -3 10 188.88 33.5 7 -3 10 224.58 35.8 7 -3 10 177.48 13 7 -3 10 189.58 11.6 -7 -3 -10 184.38 12 7 -3 10 196.38 12.2 7 3 -10 187.28 11 -7 -3 -10 131.79 21.1 -7 -3 -10 136.99 24.1 -7 3 10 173.28 12.2 7 3 -10 160.68 25.1 -7 3 10 183.98 11.7 7 3 -10 188.68 11.1 -7 3 10 178.38 12.7 -7 3 10 162.38 23.6 -7 -3 10 166.08 12.4 -7 3 -10 162.18 25.2 7 3 10 173.38 32.5 7 -3 -10 162.68 11.1 7 3 10 172.38 11.9 -7 3 -10 157.88 27.5 -7 3 -10 163.48 12.2 7 -3 -10 167.18 11.4 7 -3 -10 140.59 20.4 7 -3 -10 166.58 21 -7 -3 10 175.78 11.1 -7 -3 10 165.28 12 7 3 10 166.38 12.3 7 3 10 197.88 32.1 -8 -3 -10 45.7 5.4 -8 3 10 33.4 15.8 8 -3 10 52.69 30.8 8 -3 10 60.19 32.5 -8 3 10 42.6 14.7 8 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-11 3185.38 182.98 -3 -2 11 2963.8 175.58 -3 -2 11 3148.39 175.48 -3 2 -11 3146.79 183.48 3 2 11 3014.7 175.48 3 2 11 3235.58 184.28 -3 -2 11 2964.7 175.38 3 -2 -11 2963.8 175.18 3 -2 -11 3116.09 175.38 3 2 11 3100.29 175.48 -4 -2 -11 630.94 36.3 -4 -2 -11 602.14 37 -4 2 11 621.04 39.6 -4 -2 -11 619.54 47.6 4 -2 11 637.44 36.4 -4 2 11 687.33 36.9 -4 2 11 579.44 39.9 -4 2 11 576.24 39.1 -4 2 11 617.44 37 4 -2 11 634.24 49.8 -4 2 11 594.74 36.5 -4 -2 -11 623.94 36.6 4 -2 11 642.94 37 -4 2 11 629.94 36.8 4 -2 11 612.24 48.2 -4 2 11 625.94 39.1 4 -2 11 630.54 36.7 -4 -2 -11 633.84 48.4 -4 -2 11 662.83 37 -4 2 -11 673.13 37.2 4 2 11 673.03 37.2 4 2 11 669.83 36.7 4 2 11 702.93 49.8 4 2 11 644.94 36.8 4 -2 -11 666.03 36.7 -4 -2 11 646.44 36.7 -4 2 -11 671.83 47.8 4 2 11 666.53 36.7 4 2 11 647.54 48.6 4 -2 -11 662.23 36.2 -4 -2 11 682.53 36.9 -4 -2 11 650.63 36.8 -4 2 -11 709.63 47.1 -5 -2 -11 2077.69 126.19 -5 -2 -11 1988.1 114.39 5 -2 11 2102.29 114.19 -5 2 11 2118.99 116.99 -5 2 11 2067.99 117.19 -5 2 11 2051.69 114.19 -5 -2 -11 1979.1 113.69 5 2 -11 2099.19 113.59 -5 2 11 1968.6 113.99 5 2 -11 2067.89 113.59 -5 2 11 2084.79 114.49 5 -2 11 2072.39 114.59 -5 2 11 1886.71 117.49 -5 2 11 2068.79 117.39 5 -2 11 1793.92 133.39 -5 -2 -11 2079.29 114.09 5 -2 11 2093.39 114.49 -5 2 11 2055.69 114.29 5 2 -11 1991.6 113.49 5 -2 11 2017.2 113.89 -5 -2 -11 2070.59 126.89 5 -2 11 2053.09 137.79 5 2 11 1988.1 114.19 5 -2 -11 2100.59 113.79 5 2 11 2017.9 126.49 -5 -2 11 1958.2 114.09 5 2 11 2039.6 127.49 5 -2 -11 2149.98 114.29 5 -2 -11 1935.71 113.69 -5 -2 11 1977.1 114.29 -5 2 -11 2008.8 114.59 5 2 11 1947.41 113.79 5 2 11 2075.59 114.59 -5 -2 11 2000.1 114.09 5 2 11 2042.9 113.99 5 2 11 1988.3 114.19 -5 -2 11 1995.3 114.29 6 -2 11 95.29 6.1 -6 2 11 94.19 7.8 -6 -2 -11 68.99 19.2 -6 2 11 91.09 6.7 -6 -2 -11 104.89 6.8 6 -2 11 88.69 23.2 6 2 -11 95.29 5.5 -6 2 11 94.49 14.9 -6 2 11 96.59 7.2 6 -2 11 116.99 23.8 6 -2 11 103.69 7.1 -6 2 11 103.49 14.8 6 -2 11 102.19 7.9 -6 -2 -11 76.79 19.5 -6 -2 -11 105.49 7.4 -6 2 -11 63.59 7.7 6 2 11 63.69 6.8 -6 -2 11 61.69 6.2 -6 -2 11 63.49 6.8 6 2 11 64.79 7 6 2 11 67.19 5.8 6 -2 -11 64.39 7.1 6 2 11 72.99 7.8 -6 -2 11 57.39 7 6 -2 -11 62.89 5.8 -6 2 -11 58.89 16.8 -6 2 -11 43.9 17.6 6 2 11 67.79 5.9 -6 -2 11 63.49 7.2 7 -2 11 29.6 4.2 -7 -2 -11 42.6 20.1 7 2 -11 27.8 4.6 -7 -2 -11 35.2 4.2 -7 2 11 28 11.1 7 2 -11 29.6 3.4 -7 -2 -11 32.9 3.7 7 -2 11 29.8 3.6 -7 -2 -11 41 4.6 -7 2 11 32.5 5.3 7 2 -11 30.4 7.8 7 2 -11 34.4 7.7 -7 2 11 5.1 10.2 -7 2 11 30.4 3.9 -7 2 11 29.2 4.5 -7 -2 -11 41.6 20.1 7 2 -11 29.1 3.7 7 -2 11 47.6 21.3 7 -2 11 26.4 18.2 7 -2 11 32.3 5.4 -7 2 -11 25.3 17.7 -7 -2 11 23 4.6 7 -2 -11 30.3 10 -7 -2 11 29.2 7.8 -7 2 -11 -0.6 16.9 7 2 11 24.6 22.2 7 2 11 21 3.4 7 2 11 20.8 4.3 7 2 11 0.4 22.2 -7 -2 11 19.1 4.2 -7 2 -11 23.5 4.7 -7 -2 11 23.9 3.4 7 -2 -11 20.6 2.9 7 -2 -11 24.2 3.5 7 -2 -11 27.8 9.9 -7 -2 11 13.3 7.7 7 2 11 23.6 5.9 7 2 11 22.5 3.9 -8 -2 -11 254.57 40 8 -2 11 210.38 15 8 2 -11 253.57 21.4 -8 -2 -11 227.38 14.1 8 2 -11 215.18 12.5 -8 2 11 211.48 14.1 -8 2 11 210.98 13.2 -8 2 11 212.88 25.9 -8 -2 -11 191.68 30.8 8 2 -11 210.48 20.2 -8 2 11 217.78 26.6 8 -2 11 215.78 13.9 8 -2 11 210.38 13.2 8 2 -11 213.08 12.3 8 -2 11 221.98 37.9 8 -2 11 172.78 33.2 -8 2 11 210.18 14.5 8 2 -11 215.58 12.5 -8 -2 -11 216.98 12.4 8 -2 -11 200.38 12.9 8 2 11 177.48 14 -8 -2 11 196.38 12.7 8 2 11 236.38 41.3 8 2 11 197.68 13.8 -8 -2 11 178.58 13.8 -8 -2 11 163.78 19.9 8 2 11 193.78 37.5 -8 2 -11 201.48 14.6 -8 -2 11 160.78 19.5 -8 2 -11 125.29 26.7 8 -2 -11 198.88 14.4 8 -2 -11 187.38 12.5 8 -2 -11 158.58 28.7 8 2 11 183.98 14.8 8 2 11 186.78 13 -8 -2 11 190.48 14.3 -8 2 -11 199.98 14.5 -8 2 -11 134.39 26.5 -9 2 11 22.9 6.2 9 2 -11 23.3 3.7 9 2 -11 24.4 3.6 -9 -2 -11 22 4.9 9 -2 11 22.9 6.3 -9 2 11 19.9 5.7 -9 2 11 25.8 4.2 9 -2 11 10.4 34.9 9 -2 11 1.1 37 9 2 -11 45.6 13.4 -9 -2 -11 21.7 3.6 9 -2 11 20.1 4.6 9 2 -11 20.3 4.3 9 2 -11 -3.2 11.5 9 2 11 23.3 5.2 9 2 11 50.49 39.3 -9 2 -11 23.1 6.1 9 2 11 26.3 6.4 9 2 11 24.5 5.7 9 2 11 22.7 34.1 -9 2 -11 35.6 6.2 -9 -2 11 29.5 12.8 -9 -2 11 28 12.2 -9 -2 11 26 5.8 9 -2 -11 14.4 5.8 -9 -2 11 26.5 6.2 9 -2 -11 23.5 4.3 9 -2 -11 17.8 3.6 9 2 11 23.4 4.5 10 -2 11 51.79 7 -10 2 11 54.29 7.3 -10 -2 -11 52.19 6.4 -10 -2 -11 46.3 8.6 10 2 -11 44.7 7.5 10 2 -11 47.5 6.6 -10 2 11 36.8 7.2 10 -2 11 53.19 8.3 10 2 -11 57.49 6.4 10 -2 11 42.3 5.9 -10 -2 -11 48.8 6.1 10 2 11 45.5 6 10 -2 -11 40.9 7.2 -10 -2 11 38.8 6.6 10 -2 -11 43.4 5.7 10 2 11 48 7.1 10 2 11 48.5 6.6 10 2 11 37.8 7.5 -10 2 -11 39 6.9 10 -2 -11 39.3 5 -10 2 -11 38.3 7.4 -10 -2 11 38.2 7.6 11 -2 11 225.98 16.4 -11 -2 -11 206.68 17.7 11 2 -11 196.28 13.8 11 -2 11 198.08 17.3 11 2 -11 202.68 13.6 11 2 -11 201.08 17.2 -11 2 11 192.68 16.8 11 -2 11 196.08 14.9 -11 -2 -11 190.28 15.1 -11 2 11 201.88 16.1 -11 2 -11 203.98 16.4 11 2 11 198.68 16.3 11 -2 -11 193.48 13.9 -11 -2 11 197.68 17.1 11 -2 -11 198.78 16.6 -11 2 -11 200.48 17.2 11 2 11 210.98 16.1 -11 -2 11 197.98 16.2 11 2 11 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11 71.39 5 1 3 -11 64.29 4.5 1 3 -11 64.39 4.4 -1 3 11 62.59 4.7 -1 -3 -11 66.89 5 -1 -3 11 88.59 10.5 1 3 11 87.69 14 -1 -3 11 83.69 5.7 1 -3 -11 86.19 10.9 -1 -3 11 86.29 4.9 1 -3 -11 103.09 11.8 1 -3 -11 88.19 5.3 -1 -3 11 87.49 5.7 -1 -3 11 99.69 10.6 -1 3 -11 82.29 11.8 -1 3 -11 85.39 4.8 1 3 11 83.79 13 -1 -3 11 87.59 4.8 -1 3 -11 98.29 11.9 2 3 -11 409.66 23.8 -2 3 11 427.36 29.8 -2 3 11 416.66 29.8 -2 -3 -11 458.55 33.8 2 3 -11 421.56 23.7 -2 3 11 415.26 24.4 2 -3 11 404.46 32.4 2 3 -11 435.56 23.7 2 -3 11 418.16 24.4 2 -3 11 422.56 24.5 2 3 -11 431.26 24.1 2 -3 11 427.36 23.8 -2 -3 -11 382.76 32.2 2 -3 11 407.16 24 2 3 -11 432.76 26 2 -3 11 439.36 33.7 2 3 -11 436.86 26.2 -2 3 11 426.06 23.9 -2 3 11 415.96 24.5 -2 -3 -11 435.16 24.1 2 -3 11 433.76 24.3 2 3 -11 436.06 25.7 2 3 11 318.47 24.3 -3 3 11 121.29 12.6 -3 3 11 112.09 8 3 3 -11 112.49 6.7 3 -3 11 103.49 19.9 3 3 -11 109.29 7.3 3 -3 11 110.49 8 -3 3 11 104.29 13.6 3 -3 11 110.99 7.1 -3 -3 -11 125.49 19.8 -3 3 11 105.49 8.1 -3 -3 -11 145.39 19.9 -3 3 11 121.69 14 -3 -3 -11 117.19 7.6 -3 3 11 110.29 12.8 -3 3 11 112.39 7.1 3 -3 11 117.39 7.5 -3 3 11 112.99 7.8 3 -3 11 110.69 20.3 3 3 -11 111.69 6.7 3 3 -11 101.39 6.9 3 -3 11 110.09 7.9 3 3 11 115.69 7.4 3 3 11 112.79 7.7 3 -3 -11 105.89 7.3 -3 -3 11 120.39 7.6 3 -3 -11 125.09 7.5 3 -3 -11 118.79 7.1 3 3 11 88.09 14.6 3 3 11 123.69 19.9 -3 3 -11 114.69 8.4 -3 -3 11 117.29 7.5 3 3 11 120.19 7.6 -3 -3 11 126.39 8 3 -3 -11 117.99 7.7 3 -3 -11 124.79 7 -3 3 -11 131.59 18.1 -3 3 -11 101.99 16.4 3 3 11 123.29 8.3 -3 -3 11 120.39 8.1 -4 3 11 258.17 16.2 -4 -3 -11 259.17 28.8 -4 3 11 263.97 16.2 4 3 -11 265.97 15.9 -4 -3 -11 270.87 16.6 4 3 -11 256.27 15.9 -4 -3 -11 267.47 16.2 4 -3 11 265.97 17 -4 3 11 277.67 21.3 4 3 -11 266.57 16.3 4 -3 11 255.47 33.8 -4 3 11 263.17 16.8 -4 3 11 257.27 16.8 4 -3 11 264.57 16.6 4 -3 11 259.57 16.2 4 -3 11 259.37 16.8 -4 -3 -11 253.67 17 4 3 -11 273.17 15.9 -4 3 11 253.17 22.3 4 3 -11 274.27 15.9 -4 3 11 256.47 17 -4 3 11 261.47 20.9 -4 -3 -11 226.98 27.3 -4 3 11 234.78 22.4 4 -3 11 224.88 31.9 -4 -3 11 328.87 16.8 4 3 11 327.47 16.9 -4 -3 11 325.67 16.7 4 3 11 314.87 31.2 4 3 11 334.87 16.7 4 3 11 339.87 17.4 -4 -3 11 329.47 17.1 -4 3 -11 335.77 17.5 4 3 11 342.87 32.6 4 -3 -11 303.17 16.4 5 3 -11 189.28 11.9 -5 3 11 173.48 18 5 3 -11 179.88 11.6 -5 3 11 182.78 19.2 5 -3 11 175.08 27.3 -5 3 11 187.68 13.2 -5 3 11 177.58 12.7 -5 -3 -11 184.28 28 -5 -3 -11 191.08 12.5 5 -3 11 189.68 13.1 -5 3 11 165.98 19.5 5 -3 11 153.68 24.6 -5 -3 -11 178.68 11.9 -5 3 11 171.88 11.8 5 3 -11 193.48 11.7 5 -3 11 191.08 12.6 -5 -3 -11 187.58 12.8 -5 -3 -11 155.98 26.4 5 3 -11 183.58 11.7 -5 3 11 196.68 18 5 -3 11 190.88 12.1 -5 3 11 172.38 12.7 -5 3 -11 223.88 26.3 5 3 11 211.18 31.5 5 3 11 225.18 12.9 5 3 11 235.48 12.4 5 3 11 234.98 13.5 -5 -3 11 233.48 13.2 -5 -3 11 233.68 12.7 5 3 11 228.78 12.6 -5 3 -11 246.68 27.5 5 -3 -11 225.88 11.9 -5 3 -11 222.38 13.5 5 3 11 193.68 30.9 -5 -3 11 237.88 12.7 5 -3 -11 239.48 12.8 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37.7 6 -8 -4 -14 89.89 31.6 8 -4 14 18.4 40.6 8 4 -14 43.5 4 -8 4 14 38.1 6.2 8 4 -14 36.9 5.1 -8 -4 14 44.4 6.1 8 -4 -14 39.3 6.1 8 4 14 17 33 -8 -4 14 46.9 6.4 -8 4 -14 50.79 6.5 8 4 14 52.89 6 8 -4 -14 46.6 5.6 -8 4 -14 57.19 7.6 8 -4 -14 37.9 5.6 8 4 14 41.3 36.8 8 4 14 49.2 5.8 -8 -4 14 42.7 6.4 8 4 14 48.2 7.4 8 4 14 43.8 6.2 -9 4 14 123.69 12.4 9 -4 14 141.09 10.4 9 4 -14 132.09 9.2 9 4 -14 133.49 8.6 -9 4 14 134.09 13.4 9 -4 14 127.29 12.4 9 -4 14 158.38 12.1 -9 -4 -14 133.69 12 -9 4 14 127.39 11.3 9 -4 14 131.79 14.5 -9 -4 -14 129.99 11.6 9 -4 -14 112.59 9.5 9 4 14 114.99 10.1 9 4 14 126.99 12 -9 4 -14 118.29 11.9 -9 4 -14 128.99 13.3 -9 -4 14 115.99 12 -9 -4 14 121.99 12.4 9 -4 -14 128.39 11.7 9 4 14 134.69 12 9 -4 -14 118.79 12.2 9 4 14 130.09 13.7 -10 4 14 186.68 13.7 10 -4 14 190.08 17.7 10 -4 14 174.08 13.3 -10 4 14 202.58 16.1 10 4 -14 182.08 11.4 10 -4 14 184.78 17.5 -10 4 14 183.98 15.3 10 4 -14 188.58 12.1 -10 -4 -14 191.08 14.5 10 -4 14 173.98 15.2 10 4 14 201.98 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6 6 22 24.8 7 -6 -6 22 24.5 7.5 6 6 22 24.1 5.6 -7 6 22 140.69 14.4 -7 -6 -22 155.98 12.4 7 -6 22 126.79 13.9 -7 6 22 142.39 15 -7 -6 -22 141.29 14.8 -7 6 -22 122.29 15.6 7 6 22 126.99 14.1 7 6 22 113.19 12.3 -7 -6 22 137.89 12.6 7 -6 -22 133.09 11.4 7 6 22 143.99 12.6 7 -6 -22 131.79 12.7 -7 6 -22 109.49 13.4 -7 -6 22 109.49 15.2 -7 -6 22 135.39 12.3 7 6 22 126.39 12.5 -8 6 22 88.69 12.7 -8 -6 -22 85.79 9.1 8 -6 22 77.29 15.4 -8 -6 -22 80.99 10.7 -8 6 22 88.89 10.4 -8 -6 22 78.39 10.8 8 6 22 97.69 12.3 -8 6 -22 93.39 11.2 8 -6 -22 109.09 12.4 -8 -6 22 100.89 12 8 6 22 95.59 11.1 -8 -6 22 111.79 12 -8 6 -22 90.29 15.6 8 -6 -22 99.69 11 -9 6 22 83.19 12.5 9 -6 22 101.29 14.8 -9 6 22 91.29 13 -9 -6 -22 99.79 12.6 -9 -6 -22 88.39 11.4 9 -6 -22 121.79 13.4 -9 -6 22 103.19 13.4 -9 -6 22 99.59 12.1 -9 -6 22 98.59 13.1 -9 6 -22 111.49 12.5 -9 6 -22 105.09 13.6 9 6 22 110.39 14.9 -9 6 -22 87.69 13.3 9 -6 -22 106.19 12.3 9 6 22 117.69 13.5 10 -6 22 53.79 10.1 -10 6 22 72.69 11.8 -10 -6 -22 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12.6 -3 7 -22 167.88 16.3 -3 7 -22 195.88 14.5 3 7 22 184.58 13 -4 -7 -22 77.19 8.8 -4 -7 -22 59.49 6.9 4 7 -22 57.99 6.9 -4 7 22 71.99 9 4 7 -22 70.49 6.8 4 -7 22 54.29 7.8 4 7 22 60.89 8.2 -4 7 -22 61.69 7.8 4 7 22 67.09 8 -4 7 -22 63.49 9.4 -4 -7 22 59.89 8.8 4 -7 -22 60.59 6.9 -4 -7 22 64.99 7.9 -4 7 -22 70.39 8.8 4 7 22 63.19 8.1 -5 7 22 281.97 21.2 -5 -7 -22 314.37 21.5 -5 7 22 297.77 21.5 -5 -7 -22 291.97 19.5 5 -7 22 287.87 21.1 5 7 -22 318.17 17.9 5 7 22 290.07 20.1 -5 7 -22 296.37 21.8 5 -7 -22 291.27 19.8 -5 -7 22 301.27 19.2 5 7 22 309.77 19.3 5 7 22 294.97 19.3 -5 7 -22 293.07 22.7 -5 7 -22 270.47 20.9 5 7 22 319.87 20.8 -5 -7 22 278.57 21.8 6 -7 22 86.49 12.1 6 7 -22 76.09 6.5 -6 -7 -22 78.39 9.6 -6 7 22 80.99 10.6 -6 -7 -22 78.89 10.3 -6 7 22 79.69 9.8 -6 7 -22 97.49 13.1 6 7 22 89.99 10.9 -6 7 -22 99.29 12.9 6 7 22 80.59 9.8 -6 -7 22 79.79 10 -6 -7 22 62.89 9.6 6 -7 -22 79.19 10.6 6 7 22 83.09 9.7 -6 7 -22 61.89 10.4 6 7 22 78.79 9.9 -7 -7 -22 93.99 10.1 7 7 -22 84.99 6.3 7 -7 22 71.19 9.1 -7 7 22 98.79 12.8 -7 -7 -22 85.69 10.9 -7 7 22 100.99 11.4 7 7 22 72.19 9.8 -7 7 -22 78.09 10.2 -7 7 -22 65.89 10.8 -7 7 -22 57.79 10.9 7 -7 -22 71.59 9.3 7 -7 -22 60.09 8.3 -7 -7 22 68.29 8.1 7 7 22 56.39 7.6 -7 -7 22 63.19 10.3 7 7 22 67.29 8.2 -8 7 22 7.1 9.1 -8 -7 -22 4.8 7.5 8 7 -22 3.2 2.8 -8 -7 -22 15.9 6.5 -8 7 22 11.8 7.7 8 -7 22 8.1 7.5 -8 7 -22 0.1 9.6 8 7 22 9.6 9.5 8 7 22 10.1 8.2 8 -7 -22 2.6 5.9 8 -7 -22 4.8 12 -8 -7 22 9.3 6.8 -8 7 -22 1.6 10 -8 -7 22 7.1 8.1 -8 7 -22 2.7 9.7 -8 -7 22 10.9 10.2 -9 7 22 111.29 14.6 -9 -7 -22 100.19 13 -9 7 22 98.79 12.6 9 7 -22 79.19 7.4 9 -7 22 112.89 15.4 9 -7 -22 96.89 12.1 9 -7 -22 81.39 9.9 -9 7 -22 99.69 14 -9 -7 22 87.49 12 9 7 22 77.29 10.2 -9 -7 22 91.39 10.3 -9 7 -22 92.59 12.3 -9 7 -22 86.09 13.4 9 7 22 93.29 14.3 -10 7 22 44 11.5 10 -7 22 42.3 9.4 -10 7 22 40.3 9.2 10 7 -22 46.3 5.3 -10 7 -22 32.1 12.1 10 7 22 27.1 8.8 10 7 22 35.8 10.9 10 -7 -22 40.2 8.2 10 -7 -22 31.5 8.8 -10 7 -22 27.8 11 -10 7 -22 30.4 12.3 -10 -7 22 26.9 8.7 0 8 -22 36.9 7.2 0 -8 22 21.9 6.7 0 8 22 37 7.3 0 -8 -22 39.9 5.7 0 8 -22 28.6 5.6 0 8 -22 34.5 6.3 -1 -8 -22 87.49 9.3 1 -8 22 91.69 12.1 1 8 -22 71.59 8.2 1 8 -22 71.49 9.2 -1 8 22 96.79 11.8 1 -8 -22 63.29 7.1 -1 8 -22 65.19 7.4 -1 -8 22 70.89 9.1 -1 8 -22 69.79 8.2 1 8 22 69.99 8.6 -1 8 -22 71.49 9 2 8 -22 384.16 21.6 2 8 -22 364.86 20.6 2 -8 22 358.16 22.3 -2 -8 -22 383.56 20.9 -2 8 22 360.36 22.2 2 -8 -22 293.77 20.5 2 8 22 298.07 21.6 2 8 22 306.47 19.6 -2 8 -22 287.87 21.1 -2 -8 22 286.37 22.5 -2 8 -22 301.67 21.9 -2 8 -22 286.17 22.4 -2 -8 22 294.37 19.4 -3 -8 -22 61.59 7.3 3 8 -22 74.59 7.9 -3 8 22 69.09 8.7 3 8 -22 65.29 7.6 3 8 -22 62.69 7.5 3 -8 22 66.19 8.7 3 8 22 73.89 7.7 3 8 22 73.19 8 -3 8 -22 70.39 8.7 3 -8 -22 61.69 7.2 -3 -8 22 80.39 7.8 -3 8 -22 75.59 9.8 -3 -8 22 60.49 9.2 -3 8 -22 71.29 8.1 3 8 22 74.79 8.4 -4 8 22 19.3 7.1 -4 -8 -22 10.5 5.2 4 -8 22 6.1 6.5 4 8 -22 13.4 4 4 8 22 20.6 4.6 4 -8 -22 24.7 5.7 4 8 22 24.2 6.4 -4 -8 22 12.3 7 -4 8 -22 16.1 7.2 -4 8 -22 8.1 7.7 -4 8 -22 23.1 6.6 4 8 22 13.6 4.8 -4 -8 22 20.1 4.8 5 -8 22 11.7 7.1 -5 8 22 19.2 7.3 5 8 -22 21.1 4 -5 -8 -22 19.2 5.7 -5 -8 -22 24.3 7.4 5 8 22 13.4 5.3 -5 8 -22 11.7 8.2 -5 -8 22 9 7.6 5 8 22 10.6 4.7 5 8 22 27.5 10.7 5 -8 -22 6.7 5.6 -5 -8 22 16.6 5.2 5 8 22 17.7 6.4 -5 8 -22 21.4 7.1 -5 8 -22 5.1 7.8 6 8 -22 181.38 11.9 -6 -8 -22 177.78 14.7 -6 8 22 184.88 17.7 -6 8 22 172.68 17.3 6 -8 22 171.58 16.3 -6 -8 -22 156.58 16.2 6 8 22 175.38 13.9 6 8 22 178.38 16.5 -6 8 -22 177.88 18.8 6 8 22 180.78 14.9 -6 8 -22 203.18 17.2 -6 -8 22 192.38 14.2 6 8 22 177.38 14.3 -6 -8 22 190.58 17.3 6 -8 -22 181.18 14.7 -6 8 -22 188.68 17.8 7 8 -22 2.8 3.4 -7 -8 -22 2.8 6.3 -7 -8 -22 11.9 7.4 -7 8 22 0.8 8.8 -7 8 22 8.9 7.9 7 -8 -22 10.1 6.6 -7 -8 22 12.2 6.4 -7 8 -22 -2.9 9.2 -7 8 -22 5.7 8.7 7 8 22 16.3 6.2 7 8 22 18.3 7.8 -7 8 -22 5.6 8.2 7 8 22 5.9 5.6 -8 -8 -22 -3.1 7.4 -8 -8 -22 -10.8 11.3 -8 8 22 11.7 9.5 8 -8 22 -0.6 7.5 -8 8 22 -3.7 7.8 8 -8 -22 4.8 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79.49 9.4 -3 9 -22 68.39 9.5 -3 -9 22 52.89 9 3 9 22 63.69 8.1 -3 -9 22 65.79 7.7 3 -9 -22 80.99 10 3 9 22 71.19 8.5 -4 9 22 35.3 8.2 -4 -9 -22 30.3 6.2 4 9 -22 25.1 4.7 4 -9 22 32.9 7.8 -4 9 -22 14.5 8.3 4 -9 -22 18.9 6.2 4 9 22 16.5 5.2 -4 9 -22 22.6 7 -4 -9 22 2.9 7.5 4 9 22 19.6 6.8 -4 -9 22 22.4 5.2 -4 9 -22 26 8 -5 -9 -22 110.59 12.2 5 9 -22 107.49 9.9 -5 -9 -22 115.19 13.8 -5 9 22 104.19 14.3 5 -9 22 115.69 13.8 5 -9 -22 136.09 12.3 -5 -9 22 126.59 11.1 -5 9 -22 130.39 16.4 5 9 22 120.19 11.5 -5 -9 22 116.89 14.8 5 9 22 121.49 10.7 -5 9 -22 146.39 14.6 -5 9 -22 111.59 12.5 5 9 22 123.49 13 -6 9 22 71.89 10 -6 -9 -22 65.09 8.3 -6 -9 -22 84.69 9.9 6 9 -22 73.89 7.6 6 -9 22 94.29 13.6 6 9 22 66.29 10 6 9 22 63.09 8 6 9 22 66.49 8.3 -6 9 -22 72.19 10.1 6 9 22 64.99 9.5 6 -9 -22 70.79 8.6 -6 -9 22 73.39 10.3 -7 9 22 15.5 8.4 -7 -9 -22 6 6.9 -7 9 22 16.2 9.4 -7 -9 -22 7.8 7.5 7 -9 22 14.2 7.7 -7 -9 22 10.4 6.6 -7 9 -22 4.4 9.4 -7 9 -22 13.9 8.6 7 9 22 2.9 5.5 -7 -9 22 -0.9 8.7 7 -9 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9.9 -2 3 -28 69.69 9.6 -2 -3 28 86.69 12.2 2 3 28 84.09 10.2 2 -3 -28 67.89 9.2 2 3 28 65.79 9.1 -2 3 -28 78.99 9.8 3 3 -28 3.7 6.8 -3 3 28 13 8.3 3 -3 28 12 8.1 3 -3 28 10.1 6.9 -3 -3 -28 7.4 7.7 3 3 28 15.7 5.8 -3 -3 28 5.8 6.8 -3 3 -28 2.5 8.2 -3 -3 28 1.7 8.2 3 3 28 7.9 7.3 -3 3 -28 15.9 6.3 -4 3 28 276.37 21 4 3 -28 275.57 19.7 4 -3 28 250.57 20.4 -4 -3 -28 257.37 21.8 -4 -3 28 272.27 21.2 -4 3 -28 257.97 22.8 4 3 28 287.27 20.7 -4 3 -28 270.47 19.8 -4 -3 28 266.07 20.7 4 3 28 258.47 19.1 -5 -3 -28 36.2 9.7 5 3 -28 32 7.7 5 -3 28 24.4 7.9 5 3 28 49.5 8.7 5 3 28 48.8 7.5 -5 -3 28 49.5 6.7 -5 3 -28 40.3 10.2 -5 -3 28 49.4 9.9 -5 -3 28 44.4 8.9 6 -3 28 29.5 7.9 -6 -3 -28 21.6 9.2 -6 3 28 19 9 -6 3 28 22.7 9.5 -6 -3 28 14.6 6.1 -6 -3 28 12.9 9.7 -6 3 -28 9.7 10 6 3 28 9.7 7.9 -6 3 -28 13.7 8.2 -6 -3 28 8.2 14.8 6 3 28 13.2 9.1 -6 -3 28 4.8 7.3 7 -3 28 10.7 8.2 -7 3 28 31.2 9.3 -7 -3 -28 6.4 9.7 -7 3 28 11 9.7 7 3 28 7.6 7.2 -7 3 -28 10.4 9 -7 -3 28 -13.3 8.4 -7 -3 28 3.3 6.6 -7 -3 28 10.6 8.7 -7 -3 28 -2.3 8 7 3 28 -0.8 8.4 -7 3 -28 -0.5 9.9 8 -3 28 0.2 8.6 -8 3 28 11.4 10.1 -8 -3 -28 3.7 10.7 -8 3 28 9.6 9 -8 -3 28 8.1 8.2 -8 3 -28 -2.2 11.2 8 3 28 1.8 7.4 -8 -3 28 7.3 7.2 -8 3 -28 17.2 10.3 -8 -3 28 -5.6 8.5 -8 -3 28 4.5 8 0 -4 28 11.2 6.9 0 4 -28 4.7 7.2 0 -4 28 -4.1 8.1 0 4 28 9 4.9 0 4 -28 6.9 4.8 0 -4 -28 9.5 7.5 0 4 28 4.8 7.6 -1 4 28 68.49 9.5 1 4 -28 94.69 12.5 1 -4 28 77.19 10.6 1 -4 28 73.79 8.9 -1 -4 -28 78.99 9.8 1 -4 -28 59.89 9.3 1 4 28 61.39 9.2 1 4 28 70.19 9.5 -1 -4 28 56.29 9.1 -1 4 -28 53.19 9.4 -1 -4 28 59.89 9.9 -1 4 -28 59.59 7.2 2 4 -28 16.7 7.1 -2 4 28 4.8 7.4 2 -4 28 17.5 7.2 -2 -4 -28 14.7 8.1 -2 4 -28 19.7 6.3 2 4 28 15.3 7.8 -2 -4 28 11.6 7.3 2 4 28 13.5 5.4 -2 4 -28 9.9 8.2 -2 -4 28 24.7 9 -3 4 28 89.69 10.3 -3 -4 -28 107.19 11.4 3 4 -28 104.79 12.6 3 -4 28 83.59 9.7 3 4 28 72.39 10.4 -3 -4 28 67.39 9.4 -3 4 -28 73.29 11 3 -4 -28 77.59 8.7 3 4 28 61.59 9.4 -3 4 -28 81.39 9.1 -3 -4 28 63.59 10.6 4 4 -28 10.5 6.9 -4 4 28 28 13.3 4 -4 -28 25.5 5.3 4 4 28 22.6 7.8 -4 -4 28 15.9 8.9 -4 -4 28 16.7 7.9 4 4 28 19.7 6.2 -4 4 -28 21 7.1 -5 -4 -28 41.8 9.8 5 -4 28 32.1 8.1 -5 4 28 37.4 9.5 -5 -4 28 21.7 15 -5 4 -28 21.9 8.3 5 -4 -28 23.2 5.8 -5 4 -28 34.2 10.3 5 4 28 29.1 6.8 -5 -4 28 25.3 9.6 5 4 28 23 8.1 6 -4 28 92.19 10.7 -6 4 28 88.59 11.3 -6 -4 -28 66.59 11.4 6 4 28 77.69 10.5 -6 -4 28 77.19 11.3 6 -4 -28 82.19 11.4 -6 -4 28 78.29 10.8 -6 -4 28 97.09 12.1 -6 4 -28 85.09 12.7 -6 -4 28 80.69 11 -6 4 -28 97.99 11.4 6 4 28 75.59 11.4 -7 4 28 22.9 10.1 -7 -4 -28 23.5 9.9 -7 4 28 18.1 9.4 7 -4 28 22.6 8.6 -7 4 -28 28.3 9.6 -7 -4 28 21.5 6.9 -7 4 -28 27.5 11.3 7 -4 -28 16.4 6.9 -7 -4 28 21.1 9.2 7 4 28 19 7.6 -7 -4 28 10.5 8.8 0 -5 -28 0.2 7.5 0 5 -28 -2.2 7.4 0 5 28 -1.4 7.8 0 -5 -28 2.9 4.7 0 5 -28 5.7 4.9 0 -5 28 -1.3 7.3 -1 5 28 45.2 9.2 1 -5 28 40 8.4 -1 -5 -28 70.49 9.5 1 5 -28 62.49 9.2 -1 -5 28 49.2 10.3 -1 5 -28 62.09 7.2 -1 5 -28 42.2 9.3 1 5 28 45.5 8.9 -1 -5 28 60.29 9.1 1 -5 -28 62.39 6.3 -2 5 28 154.98 16.4 2 -5 28 156.38 16 2 5 -28 159.88 15.3 -2 -5 -28 167.88 16.7 2 5 28 150.88 12.6 -2 -5 28 157.38 15.9 2 -5 -28 149.49 11.9 -2 5 -28 138.89 13.4 -2 5 -28 128.89 16.9 2 5 28 135.89 15.2 -2 -5 28 144.39 16.5 -3 -5 -28 10.8 10.4 3 -5 28 27.2 8.6 -3 5 28 29 12.6 3 5 -28 21.9 7.2 -3 5 -28 12.2 10.1 -3 5 -28 10.9 8.9 -3 -5 28 8.9 8 3 5 28 23.4 8.1 3 5 28 11.7 5.4 -3 -5 28 3.2 8.5 3 -5 -28 16.8 5.1 4 -5 28 24.7 7.9 -4 5 28 39.1 9.2 4 5 -28 37.6 7.9 -4 -5 -28 35.9 9 -4 5 -28 26.5 9.8 4 5 28 33.9 6.5 -4 -5 28 28.2 10.7 4 -5 -28 26.7 5.9 4 5 28 27.3 10.1 -4 5 -28 39.4 8.9 -4 -5 28 24.9 10.2 5 -5 28 58.49 9.5 -5 5 28 54.59 10 -5 -5 -28 57.89 10.1 5 5 28 38 8.5 5 5 28 40 7.1 5 -5 -28 30.6 6.6 -5 -5 28 35.5 11.2 -5 -5 28 41.7 9.5 -5 5 -28 31 10.8 -5 5 -28 37 9 -6 5 28 68.99 10.6 -6 -5 -28 55.99 10.8 6 -5 28 67.19 10.1 -6 5 -28 59.99 10.4 6 5 28 54.99 8.8 -6 5 -28 59.99 12.2 6 5 28 67.19 10.9 -6 -5 28 54.79 10.4 6 -5 -28 60.39 7.9 -6 -5 28 61.59 9.6 -7 5 28 32.9 10.8 7 -5 28 23.2 8.9 -7 -5 -28 15.4 9.9 -7 5 28 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9.6 6 -6 -28 29.4 6.9 -6 -6 28 11.4 9.5 -6 6 -28 30.9 9.3 6 6 28 18.8 6.8 6 6 28 22.5 10.2 -6 6 -28 13.1 9.3 -6 6 -28 24.3 11 7 -6 28 0.5 8.7 -7 6 28 8.1 9.2 -7 -6 -28 3 9.5 7 6 28 3.2 6.8 -7 6 -28 2.2 11.1 -7 -6 28 -11.4 9.1 -7 -6 28 10.6 7.2 7 -6 -28 -1.1 6.7 -7 6 -28 9.9 9.2 -7 6 -28 7.4 9.8 0 -7 -28 16.9 5.6 0 7 -28 26.2 6.2 0 7 28 22.4 14.4 0 7 -28 15.4 12.3 0 -7 28 12.5 8.9 -1 -7 -28 134.69 11.6 1 7 -28 117.49 15.3 1 -7 28 117.99 15.4 -1 7 28 109.19 12.6 -1 7 -28 124.69 13.2 -1 7 -28 119.49 12.8 -1 -7 28 130.39 16.5 1 -7 -28 123.39 11.6 2 -7 28 137.49 16.2 -2 -7 -28 134.59 16.5 -2 7 28 118.99 16.3 -2 -7 -28 127.09 11.9 2 7 -28 125.59 15.2 -2 -7 28 143.29 16.8 -2 7 -28 134.09 18.6 -2 7 -28 141.69 14.2 2 -7 -28 132.49 12.4 -3 -7 -28 47.4 9.7 3 -7 28 52.99 9.4 -3 -7 -28 41.5 6.5 -3 7 28 34.3 9.5 3 7 -28 43.1 11.9 -3 7 -28 45.1 10.5 -3 -7 28 34 9.9 3 -7 -28 55.19 7.1 -4 7 28 234.38 20.6 4 -7 28 227.28 19.8 -4 -7 -28 228.28 20.6 4 7 28 207.68 20.8 -4 7 -28 231.68 18.9 -4 7 -28 219.68 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-31 92.99 11.5 -2 2 -31 95.29 11.6 2 2 31 91.89 11.8 -2 2 -31 128.59 15.7 -2 -2 31 103.59 12.5 2 2 31 104.59 12.6 -3 2 31 -4.7 9.1 3 -2 31 -0.4 9 3 -2 31 -0.7 7.6 -3 -2 -31 -3.8 9 3 2 -31 -5.9 11.3 3 2 31 12.6 12 -3 2 -31 8.2 7.6 -3 -2 31 9.3 10 3 -2 -31 2.9 8.1 -3 -2 31 -2.1 9.1 -3 2 -31 -5.3 9 3 2 31 -1.4 8.4 -4 2 31 66.39 11.3 -4 -2 -31 66.39 11.9 4 -2 31 70.19 10.1 -4 -2 31 70.69 10.1 -4 2 -31 76.59 9.9 -4 2 -31 89.09 13 4 2 31 77.89 11.2 -4 -2 31 64.49 11.5 4 -2 -31 93.99 10.9 4 2 31 76.79 9.4 -5 2 31 -2.6 9.4 -5 -2 -31 6.5 9.7 5 -2 31 12 8 -5 2 -31 7.5 8.1 -5 -2 31 -1 7.8 -5 -2 31 12.2 9.9 -5 2 -31 -4.9 10.3 5 -2 -31 14.7 8.5 5 2 31 8.5 7.2 5 2 31 17.9 9.2 0 -3 -31 5 8.9 0 -3 31 4.3 9.2 0 3 31 -3 8.4 0 3 -31 8.1 8.6 0 -3 31 2.3 7.5 -1 -3 -31 56.59 10.2 1 -3 31 38.6 10.2 1 -3 31 44.4 8.6 -1 3 31 49.8 10.2 -1 3 -31 34.1 6.4 -1 -3 31 30.9 8.4 1 3 31 27.1 9.3 -1 3 -31 55.89 10 -1 -3 31 15.1 9.8 1 -3 -31 42.2 9.4 1 3 31 33.6 6.8 -2 -3 -31 50.89 10.1 -2 3 31 47.3 10.2 2 -3 31 39.8 8.5 2 -3 31 35.7 10.6 -2 3 -31 33.7 10 -2 -3 31 40.6 8.8 2 3 31 48 10.1 2 -3 -31 37.2 9.5 -2 3 -31 46.4 7.5 -2 -3 31 49.4 11.1 2 3 31 44.4 7.4 -3 3 31 132.39 17.8 3 -3 31 135.99 16 -3 -3 -31 157.18 17.5 3 3 -31 158.48 17.7 -3 3 -31 98.79 13.6 3 3 31 130.59 15.3 3 3 31 120.09 16.1 -3 -3 31 129.99 15.6 -3 -3 31 127.59 14 3 -3 -31 124.89 13 -3 3 -31 107.19 13.8 -4 -3 -31 0.9 9.1 -4 3 31 -9.2 9.4 4 -3 31 10.2 8.5 -4 3 -31 2.6 7.3 -4 -3 31 -4.6 7.8 4 3 31 12.6 8.7 4 3 31 3.1 6.8 -4 -3 31 6.3 9.8 -4 3 -31 2.4 10.1 4 -3 -31 -2.1 8.5 -5 -3 -31 75.49 12.2 5 -3 31 62.39 10.2 -5 3 31 75.89 11.8 -5 -3 31 66.79 10.4 5 -3 -31 87.99 10.9 5 3 31 57.29 8.8 5 3 31 49.3 10.7 -5 3 -31 69.69 12.8 -5 3 -31 72.69 10.4 -5 -3 31 52.49 11.3 0 -4 -31 34.4 9.7 0 -4 31 34 8.8 0 -4 31 28.7 10.2 0 4 31 28.1 9.3 0 4 -31 28.9 9.5 1 -4 31 18.5 8.5 -1 4 31 17.5 9.6 1 4 -31 8.2 9.2 -1 -4 -31 22.8 9.5 -1 4 -31 31.1 9.9 1 -4 -31 23.5 9.1 1 4 31 28.8 9.3 -1 4 -31 34.1 7.6 -1 -4 31 27.7 8.7 -1 -4 31 37.6 10.5 -2 4 31 94.89 11.7 -2 -4 -31 81.19 11.8 2 -4 31 82.49 10.4 2 -4 -31 69.09 10.8 -2 -4 31 59.79 11.8 2 4 31 81.09 11.1 -2 4 -31 72.89 11.7 -2 4 -31 67.09 9.4 -2 -4 31 66.29 10.3 -3 -4 -31 14.6 9.4 -3 4 31 15.3 9.4 3 -4 31 17.5 8.5 -3 4 -31 20.6 7.8 -3 4 -31 5.2 9.8 3 4 31 15.6 6.5 3 -4 -31 15.1 8.9 -3 -4 31 7.1 8.2 3 4 31 4.9 8.7 -3 -4 31 -7.2 9.7 4 -4 31 66.69 10.7 -4 -4 -31 63.79 11.2 -4 4 31 88.69 11.9 4 -4 -31 76.09 10.9 -4 -4 31 71.39 10.7 -4 -4 31 58.89 11.6 -4 4 -31 75.79 10.2 4 4 31 66.59 10.9 4 4 31 71.99 8.8 -4 4 -31 50.49 12 -5 4 31 135.29 17.4 -5 -4 -31 75.09 12.7 5 -4 31 74.59 11.1 -5 -4 31 123.89 16.6 5 4 31 102.89 13.4 -5 -4 31 82.59 12.5 5 4 31 94.19 11.9 -5 4 -31 88.19 11.5 -5 4 -31 90.19 13.8 5 -4 -31 100.89 11.9 0 5 -31 153.98 17.1 0 -5 31 142.19 17.1 0 5 31 137.39 16.9 0 -5 -31 132.29 17.8 1 -5 31 1.6 8.1 -1 5 31 18.4 9.5 1 5 -31 1.8 8.4 -1 -5 -31 14.2 9.4 1 -5 -31 18.3 9 1 5 31 9.3 9.3 -1 -5 31 7 8.6 -1 5 -31 5.5 9.2 -1 5 -31 2.1 7.1 2 5 -31 -9.8 8.3 -2 -5 -31 6.8 9.4 2 -5 31 7.2 8.6 -2 5 31 1.2 9.2 -2 5 -31 -0.1 7.9 2 -5 -31 -3.2 8.9 2 5 31 1.2 8.7 -2 -5 31 -1.6 8.5 -2 5 -31 2.9 9.5 -3 -5 -31 51.79 10.8 -3 5 31 57.79 11.2 3 -5 31 70.29 10.4 -3 5 -31 75.19 12.2 -3 -5 31 63.09 10.7 3 5 31 60.69 10.2 3 -5 -31 81.69 11 -3 5 -31 67.29 9.4 4 -5 31 103.89 12.1 -4 -5 -31 103.59 12.9 -4 5 31 110.89 13 -4 5 -31 109.59 11.7 4 5 31 90.39 11.8 -4 5 -31 119.29 14.3 -4 -5 31 105.39 12.4 0 6 31 7.2 9.2 0 -6 -31 18.6 9.3 0 -6 31 18.7 9.2 0 6 -31 13.5 9.2 1 -6 31 13.4 8.9 1 6 -31 11 9 -1 -6 -31 12.6 9.6 -1 6 31 11.3 9.8 -1 6 -31 4.2 9.7 1 -6 -31 16.8 9.3 -1 -6 31 13.7 8.8 1 6 31 23.1 9.5 2 -6 31 57.19 10.4 -2 6 31 43.3 10.7 -2 -6 -31 55.69 11 2 6 -31 53.69 9.9 -2 -6 31 40 10.2 -2 6 -31 44.5 11.3 2 6 31 50.29 10.5 -2 6 -31 40.2 8.3 -3 6 31 12.1 9.9 3 -6 31 12.4 8.8 -3 -6 -31 13.6 9.8 -3 -6 31 -7 9.1 -3 6 -31 8.7 7.7 -3 6 -31 -0.7 10.2 3 6 31 -2.6 8.6 0 -7 -31 115.19 13.7 0 7 -31 120.19 13.5 0 -7 31 122.59 17.4 0 7 31 107.89 13 -1 -7 -31 -8.5 9.3 -1 7 31 14.2 9.9 1 -7 31 2.5 9.2 1 7 -31 -19.3 8.4 -1 -7 31 1.2 9 1 7 31 4.8 9.4 -1 7 -31 12.1 9.8 2 7 -31 33.3 9.7 -2 -7 -31 30.5 10.6 -2 7 31 47.3 10.7 2 -7 31 25 9.5 -2 7 -31 23.7 8 -2 -7 31 17.2 9.7 2 7 31 49.1 10 -2 7 -31 41.3 11.1 0 0 -32 19.2 9 0 0 32 16.9 9.8 1 0 -32 19 8.8 -1 0 -32 8.3 5.6 1 0 32 10.7 9.8 -1 0 32 5.7 9.1 1 0 32 13.2 7.1 -1 0 -32 4.4 9 -1 0 32 7.7 10.2 -2 0 -32 10.8 9.7 2 0 32 6 9.6 -2 0 32 7 9.7 2 0 -32 8 8.3 2 0 32 10.3 7.4 -2 0 32 13.8 10.7 -3 0 32 51.79 11 3 0 32 50.89 8.9 3 0 32 47.2 10.6 3 0 -32 60.59 9.9 -3 0 -32 37.2 10.4 -4 0 -32 96.89 12.9 -4 0 32 99.89 12.8 4 0 -32 95.89 11.5 4 0 32 105.69 14.8 4 0 32 92.39 12.6 0 -1 32 -3.9 7.2 0 1 -32 6.8 8.7 0 1 32 -5.1 6.5 0 1 32 -4.5 9.3 0 -1 32 -5.6 9.5 0 -1 -32 -2.9 8.2 -1 -1 -32 72.59 11.2 1 -1 32 58.89 9 1 -1 32 48.5 11.4 1 1 -32 46.8 10.1 -1 1 32 56.49 11 -1 1 32 52.29 8.4 -1 1 -32 78.69 11.1 -1 -1 32 69.29 11.1 -1 -1 32 70.09 9.5 1 1 32 75.49 11.2 1 -1 -32 73.59 10.8 -2 1 32 22.9 7.3 2 1 -32 22.1 9.1 -2 -1 -32 22.5 9.5 -2 1 32 29.9 10.1 2 -1 32 22.1 7.8 2 -1 32 19.6 10.4 2 1 32 29.7 7.6 2 -1 -32 40.3 9.5 2 1 32 31.3 9.9 -2 1 -32 36.7 9.8 -2 -1 32 41.2 8.2 -2 -1 32 29.1 10.4 -3 -1 -32 41.9 10.4 3 -1 32 54.49 9 3 -1 32 43.1 10.7 3 1 -32 49.6 9.7 -3 1 32 41.1 10.5 -3 -1 32 37.5 8.4 -3 1 -32 47.2 8.1 3 -1 -32 21.4 9.3 3 1 32 50.29 10.5 3 1 32 42 8.6 -3 -1 32 43.1 10.7 -3 1 -32 48.9 10.9 -4 -1 -32 12 10 4 -1 32 28.6 8.6 -4 1 32 29.7 10.2 4 1 -32 21.1 8.9 4 -1 32 18.6 10.1 -4 -1 32 22.4 8.2 4 1 32 21.7 9.8 4 1 32 25.7 8.2 -4 1 -32 21.5 10.7 -4 -1 32 19.5 9.9 4 -1 -32 16.8 9.2 0 -2 -32 -2.9 8.9 0 -2 32 3.9 9.9 0 2 32 -2.5 6.3 0 2 32 6.7 9.2 0 -2 32 -4.2 7.6 0 2 -32 0.4 8.8 -1 -2 -32 5.7 9.4 1 -2 32 16.5 10.3 -1 2 32 8 9.2 1 2 -32 -4.1 8.5 1 -2 32 9.4 7.6 1 -2 -32 -0.2 8.7 -1 -2 32 -3.4 9.5 -1 2 -32 1.4 8.8 1 2 32 3.5 9.2 -1 -2 32 5 7.6 1 2 32 2.6 6.3 2 -2 32 1.2 7.7 -2 -2 -32 17.2 9.3 2 -2 32 1.1 9.6 -2 2 32 16.3 9.3 2 2 -32 1.8 8.4 -2 -2 32 8.8 9.8 -2 2 -32 21.2 9.3 -2 -2 32 14.6 7.8 2 2 32 10.8 9.4 2 -2 -32 11 9 2 2 32 13.2 8.5 3 2 -32 51.49 9.5 3 -2 32 34.2 10.8 -3 2 32 44 10.5 3 -2 32 48.4 9.1 -3 -2 -32 45 10.3 3 -2 -32 38.3 9.9 -3 -2 32 46.5 9.1 3 2 32 48.3 8.3 -3 2 -32 45.2 11.3 -3 2 -32 45.5 8.1 3 2 32 39 10.3 -3 -2 32 41.7 10.9 4 2 -32 23.1 8.7 4 -2 32 16.4 8.5 -4 -2 -32 28.2 10.4 -4 2 32 15.8 9.8 4 -2 -32 19 8.9 -4 2 -32 6.3 10.6 -4 -2 32 26.6 10.5 4 2 32 15.4 9.6 -4 2 -32 9.7 7.8 -4 -2 32 14 8.2 4 2 32 15.6 7.6 0 -3 32 18 8.3 0 -3 -32 24 9.8 0 3 -32 24.3 9.3 0 -3 32 17.5 10.3 0 3 32 23.2 9.3 1 -3 32 85.49 10.5 -1 3 32 82.49 11.9 -1 -3 -32 103.59 12.3 1 -3 32 69.49 12.1 1 3 -32 86.49 11.1 1 3 32 68.39 10.9 -1 3 -32 55.49 11 1 -3 -32 75.99 11.3 -1 -3 32 62.09 10.2 -1 -3 32 53.89 11.8 2 -3 32 6.5 10.2 2 3 -32 15.6 8.7 -2 3 32 6.8 9.4 -2 -3 -32 18.9 9.6 2 -3 32 17 8.3 -2 -3 32 12.2 8.3 -2 3 -32 17.3 10.1 2 3 32 21.3 9.6 -2 3 -32 11 6.9 -2 -3 32 13.2 10.3 2 -3 -32 11.6 9.3 3 3 -32 17.9 8.4 -3 -3 -32 20.2 9.8 -3 3 32 17.1 9.7 3 -3 32 8.3 8.5 -3 -3 32 11.1 8.5 3 3 32 -13.7 8.7 -3 3 -32 -0.4 7.3 3 3 32 11.1 7.1 3 -3 -32 9.7 8.9 -3 3 -32 12.9 10.5 -3 -3 32 4.5 10.1 4 -3 32 212.58 19.7 -4 -3 -32 196.58 20.7 -4 3 32 224.88 21 -4 3 -32 198.08 17.8 -4 3 -32 217.48 21.8 4 3 32 197.48 20.1 4 3 32 204.18 17.6 -4 -3 32 203.38 21.2 -4 -3 32 180.08 19.2 4 -3 -32 191.28 20.2 0 4 32 -4.2 9 0 4 -32 -10.2 8.5 0 -4 -32 -0.2 9.1 0 -4 32 2.6 10.3 0 -4 32 -5.7 8.2 1 4 -32 5 9 -1 -4 -32 5.6 9.6 1 -4 32 13.8 8.4 -1 4 32 18.4 9.6 -1 4 -32 -2.5 9.3 1 4 32 -1.2 9.2 -1 -4 32 -11 9.9 -1 -4 32 13.8 8.3 1 -4 -32 11.6 9.5 2 -4 32 23.1 8.9 -2 -4 -32 14.7 9.4 -2 4 32 25.6 9.9 2 4 -32 1.2 8.8 -2 4 -32 1.3 6.7 2 4 32 23.1 9.5 2 -4 -32 14.1 9.4 -2 4 -32 1 9.6 -2 -4 32 3.3 10 -2 -4 32 3.7 8.5 -3 -4 -32 37.2 10.5 3 4 -32 26.8 9.2 -3 4 32 41.8 10.5 3 -4 32 36.6 9.4 -3 -4 32 12.4 10.8 -3 4 -32 24.5 8.1 3 4 32 24.4 9.8 3 -4 -32 17.1 9.3 -3 -4 32 10.5 8.8 -3 4 -32 19.2 10.5 0 5 32 42.1 10.5 0 5 -32 19 9.8 0 -5 32 35.7 9.4 0 -5 -32 26.5 10.1 1 -5 32 33.6 9.6 1 5 -32 25.4 9.8 -1 -5 -32 12.3 10.1 -1 5 32 37.1 10.3 1 -5 -32 39.9 10.2 -1 -5 32 31.5 9.5 1 5 32 23.9 9.9 -1 5 -32 43.1 10.8 -2 -5 -32 65.09 11.4 2 -5 32 55.59 10 2 5 -32 42.3 9.8 -2 5 32 53.39 11.3 2 5 32 39 10.1 -2 5 -32 37.9 11.1 -2 5 -32 35.2 8.3 2 -5 -32 48.9 10.4 -2 -5 32 46.3 10.2 -3 5 32 105.69 13.3 -3 -5 -32 108.09 13.2 3 -5 32 96.69 12.1 -3 5 -32 75.19 13.4 3 5 32 80.99 11.5 -3 -5 32 96.99 12.1 -3 5 -32 87.89 10.7 3 -5 -32 107.89 12.6 0 6 32 2 9.6 0 6 -32 6 9.8 0 -6 32 -4 8.8 0 -6 -32 -8.9 9.3 -1 -6 -32 96.99 12.8 1 -6 32 92.99 12 -1 6 32 83.09 12.4 1 6 -32 97.99 12.1 1 6 32 90.09 12.5 -1 6 -32 82.59 12.9 1 -6 -32 99.69 12.6 -1 -6 32 84.39 11.8 0 0 -33 2.6 8.9 0 0 33 5 9.7 0 0 33 8.3 7.3 1 0 33 57.49 9 1 0 -33 51.39 10.5 1 0 33 59.79 11.3 -1 0 33 53.19 8.7 -1 0 -33 49.8 10.8 -1 0 33 38.4 11.2 -2 0 -33 9.7 9.5 -2 0 33 17.1 10 -2 0 -33 13 6.8 2 0 33 15.4 10.3 2 0 -33 11.9 9 2 0 33 5.8 7.5 -2 0 33 7.7 7.3 -3 0 -33 67.79 11.8 3 0 -33 73.19 10.7 3 0 33 66.09 9.7 3 0 33 73.29 11.8 -3 0 33 64.89 12 0 1 33 15.8 10 0 -1 -33 48.1 10.4 0 -1 33 40.4 8.6 0 -1 33 36.5 11 0 1 -33 32.5 9.9 0 1 33 27.1 7.7 1 -1 33 -15.5 9.5 -1 1 33 11.6 9.6 1 1 -33 -7.2 8.7 -1 -1 -33 -9.4 8.8 -1 1 33 -8.1 6.6 1 -1 33 4.3 7.6 -1 -1 33 15.5 10.3 1 -1 -33 -1.3 8.8 -1 -1 33 8.1 7.4 -1 1 -33 -4.8 9.3 1 1 33 6.2 9.8 1 1 33 12.5 7.3 -2 1 33 15.1 10.5 2 -1 33 19.4 8 2 -1 33 12.2 10.3 2 1 -33 1.9 8.9 -2 -1 -33 11.8 10.1 -2 1 -33 12.9 9.8 2 1 33 13.5 7.3 2 -1 -33 15.4 9.3 -2 -1 33 6.9 10 2 1 33 15 9.9 -2 1 -33 -0.5 6.4 -2 -1 33 6.9 7.7 3 -1 33 10.4 8.3 3 1 -33 7.5 8.9 -3 1 33 1.6 9.9 -3 -1 -33 -2.4 9.6 3 -1 33 -3 10.2 -3 -1 33 5 7.7 3 -1 -33 4.1 8.7 3 1 33 2.7 9.7 -3 1 -33 1.4 7 -3 1 -33 11.5 9.9 -3 -1 33 8 10.3 3 1 33 15.6 7.6 0 -2 -33 48.8 10.9 0 2 -33 75.29 10.9 0 2 33 50.69 11 0 -2 33 63.09 9.8 0 -2 33 56.79 11.8 -1 -2 -33 83.89 11.6 1 -2 33 70.89 10.4 1 2 -33 86.99 11.7 -1 2 33 83.09 12.3 1 -2 33 92.79 13.1 1 2 33 79.99 9.5 -1 2 -33 91.39 12 1 2 33 59.69 11.6 1 -2 -33 76.69 11.5 -1 -2 33 77.69 12.9 -1 -2 33 74.29 10.4 -2 -2 -33 2.5 9.7 2 -2 33 9 10.2 2 2 -33 -12.1 8.5 -2 2 33 -2.1 9.3 2 -2 33 -2.9 7.7 2 2 33 5.4 9.4 2 2 33 0.5 6.7 -2 -2 33 1.5 9.8 2 -2 -33 0 9.2 -2 2 -33 7.5 6.8 -2 2 -33 -6.6 9.5 -2 -2 33 -0.5 7.9 3 2 -33 56.69 10.2 -3 2 33 35.5 10.5 -3 -2 -33 22.1 10.9 3 -2 33 49.6 11.7 3 -2 33 39.4 9.4 -3 2 -33 39.8 11.5 3 -2 -33 45.1 10.4 3 2 33 48.9 8.5 -3 -2 33 46.6 11.8 -3 -2 33 55.69 9.7 -3 2 -33 49.4 8.6 3 2 33 54.59 10.9 0 -3 33 2.6 10.5 0 -3 -33 5 9.6 0 -3 33 -0.4 8.3 0 3 33 -1.7 9.1 0 3 -33 7.8 9.3 1 -3 33 10.7 8.5 -1 3 33 19.9 10.1 1 -3 33 3.1 10.5 1 3 -33 24.6 9.2 -1 -3 -33 10.6 10.1 -1 3 -33 10.8 9.8 1 -3 -33 18.7 9.9 -1 -3 33 11 8.3 -1 -3 33 20.9 11 1 3 33 9.3 9.5 -2 -3 -33 30.2 10.2 2 3 -33 28.1 9.3 2 -3 33 24.8 8.9 -2 3 33 17.3 9.9 2 -3 -33 12 9.8 -2 -3 33 7.7 8.4 2 3 33 14 10.3 -2 3 -33 22.5 7.5 -2 3 -33 37.8 11.4 -2 -3 33 13.2 10.9 0 4 33 138.19 18.4 0 4 -33 132.89 18.1 0 -4 33 152.78 17.5 0 -4 -33 148.99 19.4 1 4 -33 75.09 11.4 -1 -4 -33 56.29 11.2 -1 4 33 64.19 11.6 1 -4 33 66.69 10.6 1 -4 -33 70.69 11.9 1 4 33 54.49 11.2 -1 -4 33 54.29 11.9 -1 -4 33 47 10.1 -1 4 -33 49.9 11.3 loop_ _twin_individual_id _twin_individual_mass_fraction_refined 1 0.983(3) 2 0.017(3) #===END data_NiBr _audit_creation_date 2017-03-04 _audit_creation_method ; Olex2 1.2 (compiled 2016.02.19 svn.r3266 for OlexSys, GUI svn.r5155) ; _publ_contact_author_address ? _publ_contact_author_email ? _publ_contact_author_name '' _publ_contact_author_phone ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ((R,R)-Ph-BOX)NiBr _chemical_name_systematic ? _chemical_formula_moiety 'C21 H22 Br N2 Ni O2' _chemical_formula_sum 'C21 H22 Br N2 Ni O2' _chemical_formula_weight 473.03 _chemical_absolute_configuration syn _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Br' 'Br' -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Ni' 'Ni' 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system 'orthorhombic' _space_group_IT_number 19 _space_group_name_H-M_alt 'P 21 21 21' _space_group_name_Hall 'P 2ac 2ab' loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 'x, y, z' 2 '-x+1/2, -y, z+1/2' 3 '-x, y+1/2, -z+1/2' 4 'x+1/2, -y+1/2, -z' _cell_length_a 9.457(2) _cell_length_b 13.597(3) _cell_length_c 15.622(4) _cell_angle_alpha 90.00 _cell_angle_beta 90.00 _cell_angle_gamma 90.00 _cell_volume 2008.7(8) _cell_formula_units_Z 4 _cell_measurement_reflns_used 9899 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 43.17 _cell_measurement_theta_min 2.52 _exptl_absorpt_coefficient_mu 2.973 _exptl_absorpt_correction_T_max 0.7486 _exptl_absorpt_correction_T_min 0.6630 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0879 before and 0.0682 after correction. The Ratio of minimum to maximum transmission is 0.8857. The \l/2 correction factor is Not present. ; _exptl_crystal_colour yellow _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 1.564 _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_description 'prism' _exptl_crystal_F_000 964 _exptl_crystal_recrystallization_method THF/n-pentane _exptl_crystal_size_max 0.289 _exptl_crystal_size_mid 0.151 _exptl_crystal_size_min 0.133 _exptl_special_details ; ? ; _diffrn_reflns_av_R_equivalents 0.0433 _diffrn_reflns_av_unetI/netI 0.0574 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_k_max 22 _diffrn_reflns_limit_k_min -26 _diffrn_reflns_limit_l_max 30 _diffrn_reflns_limit_l_min -30 _diffrn_reflns_number 58562 _diffrn_reflns_theta_full 26.00 _diffrn_reflns_theta_max 43.67 _diffrn_reflns_theta_min 2.61 _diffrn_ambient_temperature 100(2) _diffrn_detector_area_resol_mean ? _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.989 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_source 'fine-focus sealed tube' _diffrn_special_details ? _diffrn_standards_decay_% ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_number 0 _reflns_number_gt 11216 _reflns_number_total 15114 _reflns_threshold_expression >2sigma(I) _computing_cell_refinement 'SAINT v8.37A (Bruker, 2015)' _computing_data_collection ? _computing_data_reduction 'SAINT v8.37A (Bruker, 2015)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'XT (Sheldrick, 2015)' _refine_diff_density_max 0.527 _refine_diff_density_min -0.637 _refine_diff_density_rms 0.079 _refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881' _refine_ls_abs_structure_Flack 0.006(4) _refine_ls_extinction_coef ? _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.988 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 246 _refine_ls_number_reflns 15114 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0612 _refine_ls_R_factor_gt 0.0335 _refine_ls_restrained_S_all 0.988 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0090P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0511 _refine_ls_wR_factor_ref 0.0566 _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C1(H1), C9(H9) 2.b Secondary CH2 refined with riding coordinates: C2(H2A,H2B), C8(H8A,H8B) 2.c Aromatic/amide H refined with riding coordinates: C11(H11), C12(H12), C13(H13), C14(H14), C15(H15), C17(H17), C18(H18), C19(H19), C20(H20), C21(H21) 2.d Idealised Me refined as rotating group: C5(H5A,H5B,H5C), C6(H6A,H6B,H6C) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symetry_multiplicity _atom_site_calc_flag _atom_site_disorder_assembly _atom_site_disorder_group _atom_site_refinement_flags_posn Br1 Br 0.621602(12) 0.946817(8) 0.369936(7) 0.02329(3) Uani 1 1 d A 1 . Ni1 Ni 0.690902(14) 0.785053(10) 0.360876(8) 0.01632(3) Uani 1 1 d A 1 . O1 O 0.88261(8) 0.53663(6) 0.26327(5) 0.02219(15) Uani 1 1 d A . . O2 O 0.57671(8) 0.54512(6) 0.50704(5) 0.02160(15) Uani 1 1 d A . . N1 N 0.79400(9) 0.68439(7) 0.29940(5) 0.01713(16) Uani 1 1 d . . . N2 N 0.63390(9) 0.69038(7) 0.44774(5) 0.01675(15) Uani 1 1 d . . . C1 C 0.87251(11) 0.70309(9) 0.21812(6) 0.01990(19) Uani 1 1 d A . . H1 H 0.9489 0.7527 0.2279 0.024 Uiso 1 1 calc . . R C2 C 0.93779(12) 0.60169(10) 0.19726(7) 0.0256(2) Uani 1 1 d . . . H2A H 0.9086 0.5792 0.1397 0.031 Uiso 1 1 calc A . R H2B H 1.0423 0.6046 0.1996 0.031 Uiso 1 1 calc . . R C3 C 0.80237(10) 0.59261(8) 0.31599(6) 0.01670(17) Uani 1 1 d A . . C4 C 0.72452(10) 0.53345(8) 0.38277(6) 0.01681(18) Uani 1 1 d . . . C5 C 0.82617(13) 0.46727(10) 0.43373(9) 0.0310(3) Uani 1 1 d A . . H5A H 0.8817 0.4271 0.3940 0.046 Uiso 1 1 calc . . GR H5B H 0.7716 0.4243 0.4717 0.046 Uiso 1 1 calc . . GR H5C H 0.8899 0.5083 0.4679 0.046 Uiso 1 1 calc . . GR C6 C 0.61771(14) 0.46888(10) 0.33341(8) 0.0285(2) Uani 1 1 d A . . H6A H 0.5544 0.5110 0.2999 0.043 Uiso 1 1 calc . . GR H6B H 0.5620 0.4301 0.3741 0.043 Uiso 1 1 calc . . GR H6C H 0.6689 0.4245 0.2949 0.043 Uiso 1 1 calc . . GR C7 C 0.64418(10) 0.59722(8) 0.44537(6) 0.01616(17) Uani 1 1 d A . . C8 C 0.48814(12) 0.61712(9) 0.55205(8) 0.0239(2) Uani 1 1 d . . . H8A H 0.4927 0.6072 0.6148 0.029 Uiso 1 1 calc A . R H8B H 0.3884 0.6123 0.5333 0.029 Uiso 1 1 calc . . R C9 C 0.55207(11) 0.71654(9) 0.52678(6) 0.01889(18) Uani 1 1 d A . . H9 H 0.4750 0.7640 0.5121 0.023 Uiso 1 1 calc . . R C10 C 0.77123(11) 0.73944(8) 0.15028(6) 0.01829(19) Uani 1 1 d . . . C11 C 0.79868(13) 0.82473(9) 0.10400(8) 0.0259(2) Uani 1 1 d A . . H11 H 0.8811 0.8621 0.1161 0.031 Uiso 1 1 calc . . R C12 C 0.70583(16) 0.85579(11) 0.03984(9) 0.0345(3) Uani 1 1 d . . . H12 H 0.7261 0.9135 0.0079 0.041 Uiso 1 1 calc A . R C13 C 0.58466(14) 0.80261(11) 0.02295(8) 0.0317(3) Uani 1 1 d A . . H13 H 0.5216 0.8240 -0.0206 0.038 Uiso 1 1 calc . . R C14 C 0.55457(14) 0.71792(11) 0.06933(7) 0.0276(2) Uani 1 1 d . . . H14 H 0.4707 0.6817 0.0581 0.033 Uiso 1 1 calc A . R C15 C 0.64807(11) 0.68678(9) 0.13226(7) 0.02193(19) Uani 1 1 d A . . H15 H 0.6279 0.6286 0.1636 0.026 Uiso 1 1 calc . . R C16 C 0.65093(10) 0.76207(8) 0.59178(6) 0.01664(18) Uani 1 1 d . . . C17 C 0.75215(11) 0.70519(8) 0.63465(8) 0.02295(19) Uani 1 1 d A . . H17 H 0.7597 0.6369 0.6225 0.028 Uiso 1 1 calc . . R C18 C 0.84170(12) 0.74766(9) 0.69485(8) 0.0235(2) Uani 1 1 d . . . H18 H 0.9103 0.7085 0.7233 0.028 Uiso 1 1 calc A . R C19 C 0.83087(13) 0.84687(9) 0.71329(8) 0.0252(2) Uani 1 1 d A . . H19 H 0.8893 0.8755 0.7560 0.030 Uiso 1 1 calc . . R C20 C 0.73427(14) 0.90440(9) 0.66903(9) 0.0278(2) Uani 1 1 d . . . H20 H 0.7287 0.9730 0.6802 0.033 Uiso 1 1 calc A . R C21 C 0.64562(12) 0.86212(9) 0.60846(8) 0.0227(2) Uani 1 1 d A . . H21 H 0.5805 0.9023 0.5781 0.027 Uiso 1 1 calc . . R loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Br1 0.03022(5) 0.01564(4) 0.02401(5) 0.00129(4) -0.00695(4) 0.00318(4) Ni1 0.01966(5) 0.01508(6) 0.01422(5) 0.00028(5) -0.00243(5) 0.00084(5) O1 0.0233(3) 0.0236(4) 0.0197(3) -0.0010(3) 0.0061(3) 0.0052(3) O2 0.0240(3) 0.0198(4) 0.0210(4) -0.0003(3) 0.0072(3) -0.0039(3) N1 0.0181(4) 0.0205(4) 0.0127(3) 0.0004(3) 0.0001(3) 0.0007(3) N2 0.0182(4) 0.0182(4) 0.0138(3) -0.0009(3) 0.0010(3) 0.0026(3) C1 0.0182(4) 0.0258(5) 0.0156(4) 0.0011(4) 0.0024(3) -0.0030(4) C2 0.0244(5) 0.0344(7) 0.0180(5) 0.0031(4) 0.0046(4) 0.0087(5) C3 0.0144(4) 0.0212(5) 0.0145(4) -0.0025(3) -0.0008(3) 0.0019(4) C4 0.0165(4) 0.0163(4) 0.0177(4) -0.0001(3) 0.0002(3) 0.0013(3) C5 0.0240(5) 0.0332(7) 0.0358(6) 0.0150(5) 0.0057(5) 0.0118(5) C6 0.0293(5) 0.0297(6) 0.0266(5) -0.0091(5) 0.0032(5) -0.0099(5) C7 0.0151(4) 0.0191(5) 0.0143(4) -0.0001(3) 0.0001(3) -0.0017(3) C8 0.0216(5) 0.0274(6) 0.0229(5) -0.0036(4) 0.0073(4) -0.0035(4) C9 0.0171(4) 0.0226(5) 0.0170(4) -0.0017(4) 0.0021(3) 0.0022(4) C10 0.0223(4) 0.0187(5) 0.0139(4) 0.0011(3) 0.0041(3) 0.0013(4) C11 0.0291(5) 0.0214(5) 0.0273(5) 0.0056(4) 0.0094(4) 0.0007(5) C12 0.0452(8) 0.0274(7) 0.0310(6) 0.0139(5) 0.0107(6) 0.0122(6) C13 0.0392(7) 0.0361(8) 0.0197(5) 0.0026(5) -0.0002(4) 0.0178(6) C14 0.0294(5) 0.0335(7) 0.0199(5) -0.0046(5) -0.0050(4) 0.0053(5) C15 0.0264(5) 0.0212(5) 0.0182(4) 0.0000(4) -0.0021(4) -0.0013(4) C16 0.0187(4) 0.0180(5) 0.0133(4) 0.0001(3) 0.0035(3) 0.0024(3) C17 0.0271(5) 0.0162(4) 0.0255(5) 0.0008(4) -0.0026(4) 0.0031(4) C18 0.0243(5) 0.0217(6) 0.0246(5) 0.0046(4) -0.0047(4) -0.0001(4) C19 0.0275(5) 0.0235(6) 0.0245(5) -0.0025(4) -0.0032(4) -0.0024(4) C20 0.0357(6) 0.0163(5) 0.0312(6) -0.0036(5) -0.0033(5) 0.0042(5) C21 0.0265(5) 0.0190(5) 0.0226(5) -0.0005(4) -0.0012(4) 0.0068(4) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Br1 Ni1 2.2994(5) . ? Ni1 N1 1.9355(9) . ? Ni1 N2 1.9466(9) . ? O1 C2 1.4554(15) . ? O1 C3 1.3540(12) . ? O2 C7 1.3554(13) . ? O2 C8 1.4678(14) . ? N1 C1 1.4928(13) . ? N1 C3 1.2770(14) . ? N2 C7 1.2709(14) . ? N2 C9 1.5000(13) . ? C1 H1 1.0000 . ? C1 C2 1.5454(17) . ? C1 C10 1.5115(15) . ? C2 H2A 0.9900 . ? C2 H2B 0.9900 . ? C3 C4 1.5091(15) . ? C4 C5 1.5387(15) . ? C4 C6 1.5446(16) . ? C4 C7 1.5118(14) . ? C5 H5A 0.9800 . ? C5 H5B 0.9800 . ? C5 H5C 0.9800 . ? C6 H6A 0.9800 . ? C6 H6B 0.9800 . ? C6 H6C 0.9800 . ? C8 H8A 0.9900 . ? C8 H8B 0.9900 . ? C8 C9 1.5324(17) . ? C9 H9 1.0000 . ? C9 C16 1.5128(15) . ? C10 C11 1.3910(16) . ? C10 C15 1.3958(15) . ? C11 H11 0.9500 . ? C11 C12 1.3978(18) . ? C12 H12 0.9500 . ? C12 C13 1.380(2) . ? C13 H13 0.9500 . ? C13 C14 1.3899(19) . ? C14 H14 0.9500 . ? C14 C15 1.3884(16) . ? C15 H15 0.9500 . ? C16 C17 1.4011(15) . ? C16 C21 1.3859(16) . ? C17 H17 0.9500 . ? C17 C18 1.3912(16) . ? C18 H18 0.9500 . ? C18 C19 1.3831(17) . ? C19 H19 0.9500 . ? C19 C20 1.3873(17) . ? C20 H20 0.9500 . ? C20 C21 1.3888(17) . ? C21 H21 0.9500 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 Ni1 Br1 148.27(3) . . ? N1 Ni1 N2 91.02(4) . . ? N2 Ni1 Br1 120.71(3) . . ? C3 O1 C2 106.87(9) . . ? C7 O2 C8 105.10(9) . . ? C1 N1 Ni1 123.52(7) . . ? C3 N1 Ni1 128.43(7) . . ? C3 N1 C1 107.96(9) . . ? C7 N2 Ni1 128.14(7) . . ? C7 N2 C9 107.44(9) . . ? C9 N2 Ni1 124.05(7) . . ? N1 C1 H1 110.2 . . ? N1 C1 C2 103.07(9) . . ? N1 C1 C10 109.69(8) . . ? C2 C1 H1 110.2 . . ? C10 C1 H1 110.2 . . ? C10 C1 C2 113.39(9) . . ? O1 C2 C1 104.45(8) . . ? O1 C2 H2A 110.9 . . ? O1 C2 H2B 110.9 . . ? C1 C2 H2A 110.9 . . ? C1 C2 H2B 110.9 . . ? H2A C2 H2B 108.9 . . ? O1 C3 C4 113.22(9) . . ? N1 C3 O1 117.43(9) . . ? N1 C3 C4 129.12(9) . . ? C3 C4 C5 111.38(9) . . ? C3 C4 C6 106.08(9) . . ? C3 C4 C7 112.75(9) . . ? C5 C4 C6 109.54(11) . . ? C7 C4 C5 108.34(9) . . ? C7 C4 C6 108.69(9) . . ? C4 C5 H5A 109.5 . . ? C4 C5 H5B 109.5 . . ? C4 C5 H5C 109.5 . . ? H5A C5 H5B 109.5 . . ? H5A C5 H5C 109.5 . . ? H5B C5 H5C 109.5 . . ? C4 C6 H6A 109.5 . . ? C4 C6 H6B 109.5 . . ? C4 C6 H6C 109.5 . . ? H6A C6 H6B 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? O2 C7 C4 113.36(9) . . ? N2 C7 O2 117.66(9) . . ? N2 C7 C4 128.97(9) . . ? O2 C8 H8A 111.0 . . ? O2 C8 H8B 111.0 . . ? O2 C8 C9 103.88(8) . . ? H8A C8 H8B 109.0 . . ? C9 C8 H8A 111.0 . . ? C9 C8 H8B 111.0 . . ? N2 C9 C8 101.91(9) . . ? N2 C9 H9 109.9 . . ? N2 C9 C16 109.32(8) . . ? C8 C9 H9 109.9 . . ? C16 C9 C8 115.58(9) . . ? C16 C9 H9 109.9 . . ? C11 C10 C1 121.25(10) . . ? C11 C10 C15 118.59(11) . . ? C15 C10 C1 120.16(10) . . ? C10 C11 H11 119.8 . . ? C10 C11 C12 120.48(12) . . ? C12 C11 H11 119.8 . . ? C11 C12 H12 120.0 . . ? C13 C12 C11 120.02(12) . . ? C13 C12 H12 120.0 . . ? C12 C13 H13 119.9 . . ? C12 C13 C14 120.28(12) . . ? C14 C13 H13 119.9 . . ? C13 C14 H14 120.3 . . ? C15 C14 C13 119.43(12) . . ? C15 C14 H14 120.3 . . ? C10 C15 H15 119.4 . . ? C14 C15 C10 121.18(11) . . ? C14 C15 H15 119.4 . . ? C17 C16 C9 121.14(10) . . ? C21 C16 C9 120.36(10) . . ? C21 C16 C17 118.47(10) . . ? C16 C17 H17 119.7 . . ? C18 C17 C16 120.66(10) . . ? C18 C17 H17 119.7 . . ? C17 C18 H18 120.0 . . ? C19 C18 C17 120.04(11) . . ? C19 C18 H18 120.0 . . ? C18 C19 H19 120.2 . . ? C18 C19 C20 119.66(11) . . ? C20 C19 H19 120.2 . . ? C19 C20 H20 119.9 . . ? C19 C20 C21 120.25(12) . . ? C21 C20 H20 119.9 . . ? C16 C21 C20 120.83(11) . . ? C16 C21 H21 119.6 . . ? C20 C21 H21 119.6 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Br1 Ni1 N1 C1 -0.68(11) . . . . ? Br1 Ni1 N1 C3 -176.62(6) . . . . ? Br1 Ni1 N2 C7 168.04(8) . . . . ? Br1 Ni1 N2 C9 -4.13(9) . . . . ? Ni1 N1 C1 C2 178.61(7) . . . . ? Ni1 N1 C1 C10 -60.33(11) . . . . ? Ni1 N1 C3 O1 -179.62(7) . . . . ? Ni1 N1 C3 C4 6.38(16) . . . . ? Ni1 N2 C7 O2 -169.44(7) . . . . ? Ni1 N2 C7 C4 11.47(16) . . . . ? Ni1 N2 C9 C8 158.94(7) . . . . ? Ni1 N2 C9 C16 -78.26(10) . . . . ? O1 C3 C4 C5 53.60(12) . . . . ? O1 C3 C4 C6 -65.52(11) . . . . ? O1 C3 C4 C7 175.64(8) . . . . ? O2 C8 C9 N2 19.32(10) . . . . ? O2 C8 C9 C16 -99.10(10) . . . . ? N1 Ni1 N2 C7 -12.16(9) . . . . ? N1 Ni1 N2 C9 175.67(8) . . . . ? N1 C1 C2 O1 3.96(10) . . . . ? N1 C1 C10 C11 128.59(11) . . . . ? N1 C1 C10 C15 -52.09(13) . . . . ? N1 C3 C4 C5 -132.19(12) . . . . ? N1 C3 C4 C6 108.69(12) . . . . ? N1 C3 C4 C7 -10.15(15) . . . . ? N2 Ni1 N1 C1 179.65(8) . . . . ? N2 Ni1 N1 C3 3.70(9) . . . . ? N2 C9 C16 C17 -71.15(13) . . . . ? N2 C9 C16 C21 107.06(11) . . . . ? C1 N1 C3 O1 3.94(12) . . . . ? C1 N1 C3 C4 -170.07(9) . . . . ? C1 C10 C11 C12 178.21(11) . . . . ? C1 C10 C15 C14 -179.01(10) . . . . ? C2 O1 C3 N1 -1.16(13) . . . . ? C2 O1 C3 C4 173.78(8) . . . . ? C2 C1 C10 C11 -116.80(12) . . . . ? C2 C1 C10 C15 62.52(12) . . . . ? C3 O1 C2 C1 -2.03(11) . . . . ? C3 N1 C1 C2 -4.73(11) . . . . ? C3 N1 C1 C10 116.33(10) . . . . ? C3 C4 C7 O2 -178.40(8) . . . . ? C3 C4 C7 N2 0.73(15) . . . . ? C5 C4 C7 O2 -54.66(12) . . . . ? C5 C4 C7 N2 124.47(12) . . . . ? C6 C4 C7 O2 64.29(11) . . . . ? C6 C4 C7 N2 -116.58(12) . . . . ? C7 O2 C8 C9 -17.82(11) . . . . ? C7 N2 C9 C8 -14.61(11) . . . . ? C7 N2 C9 C16 108.19(10) . . . . ? C8 O2 C7 N2 9.54(12) . . . . ? C8 O2 C7 C4 -171.22(8) . . . . ? C8 C9 C16 C17 43.08(13) . . . . ? C8 C9 C16 C21 -138.71(11) . . . . ? C9 N2 C7 O2 3.77(12) . . . . ? C9 N2 C7 C4 -175.33(9) . . . . ? C9 C16 C17 C18 -179.43(10) . . . . ? C9 C16 C21 C20 178.92(11) . . . . ? C10 C1 C2 O1 -114.55(10) . . . . ? C10 C11 C12 C13 1.07(19) . . . . ? C11 C10 C15 C14 0.32(17) . . . . ? C11 C12 C13 C14 -0.2(2) . . . . ? C12 C13 C14 C15 -0.58(19) . . . . ? C13 C14 C15 C10 0.52(18) . . . . ? C15 C10 C11 C12 -1.12(17) . . . . ? C16 C17 C18 C19 0.35(18) . . . . ? C17 C16 C21 C20 -2.82(17) . . . . ? C17 C18 C19 C20 -2.56(19) . . . . ? C18 C19 C20 C21 2.1(2) . . . . ? C19 C20 C21 C16 0.65(19) . . . . ? C21 C16 C17 C18 2.32(16) . . . . ? _iucr_refine_instructions_details ; TITL mo_p17056_0m_a.res in P2(1)2(1)2(1) REM Old TITL mo_p17056_0m in P222 #16 REM SHELXT solution in P2(1)2(1)2(1) REM R1 0.068, Rweak 0.022, Alpha 0.002, Orientation as input REM Flack x = 0.029 ( 0.004 ) from Parsons' quotients REM Formula found by SHELXT: C21 N O3 Ni Br CELL 0.71073 9.4568 13.5967 15.6224 90 90 90 ZERR 4 0.0021 0.0031 0.0037 0 0 0 LATT -1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H Br N Ni O UNIT 84 88 4 8 4 8 L.S. 10 PLAN 20 SIZE 0.133 0.151 0.289 TEMP -173(2) BOND $H LIST 6 MORE -1 CONF fmap 2 acta 52 REM REM REM WGHT 0.009000 FVAR 0.51553 PART 1 BR1 3 0.621602 0.946817 0.369936 11.00000 0.03022 0.01564 = 0.02401 0.00129 -0.00695 0.00318 NI1 5 0.690902 0.785053 0.360876 11.00000 0.01966 0.01508 = 0.01422 0.00028 -0.00243 0.00084 PART 0 O1 6 0.882607 0.536631 0.263274 11.00000 0.02331 0.02357 = 0.01970 -0.00098 0.00610 0.00518 O2 6 0.576708 0.545119 0.507035 11.00000 0.02400 0.01978 = 0.02102 -0.00031 0.00716 -0.00393 N1 4 0.793998 0.684389 0.299398 11.00000 0.01811 0.02054 = 0.01273 0.00038 0.00012 0.00066 N2 4 0.633900 0.690380 0.447740 11.00000 0.01819 0.01824 = 0.01383 -0.00090 0.00105 0.00257 C1 1 0.872508 0.703090 0.218116 11.00000 0.01823 0.02584 = 0.01564 0.00113 0.00240 -0.00296 AFIX 13 H1 2 0.948948 0.752656 0.227878 11.00000 -1.20000 AFIX 0 C2 1 0.937794 0.601689 0.197264 11.00000 0.02437 0.03445 = 0.01800 0.00313 0.00465 0.00872 AFIX 23 H2A 2 0.908584 0.579168 0.139653 11.00000 -1.20000 H2B 2 1.042330 0.604556 0.199578 11.00000 -1.20000 AFIX 0 C3 1 0.802375 0.592612 0.315990 11.00000 0.01439 0.02117 = 0.01453 -0.00252 -0.00078 0.00191 C4 1 0.724518 0.533451 0.382768 11.00000 0.01648 0.01628 = 0.01768 -0.00014 0.00021 0.00127 C5 1 0.826166 0.467274 0.433733 11.00000 0.02401 0.03321 = 0.03577 0.01498 0.00569 0.01177 AFIX 137 H5A 2 0.881712 0.427057 0.393991 11.00000 -1.50000 H5B 2 0.771603 0.424291 0.471743 11.00000 -1.50000 H5C 2 0.889924 0.508325 0.467924 11.00000 -1.50000 AFIX 0 C6 1 0.617711 0.468876 0.333409 11.00000 0.02928 0.02971 = 0.02657 -0.00909 0.00323 -0.00991 AFIX 137 H6A 2 0.554444 0.511034 0.299911 11.00000 -1.50000 H6B 2 0.562012 0.430083 0.374133 11.00000 -1.50000 H6C 2 0.668909 0.424538 0.294867 11.00000 -1.50000 AFIX 0 C7 1 0.644180 0.597225 0.445373 11.00000 0.01510 0.01906 = 0.01432 -0.00007 0.00009 -0.00174 C8 1 0.488145 0.617125 0.552052 11.00000 0.02155 0.02743 = 0.02285 -0.00365 0.00735 -0.00349 AFIX 23 H8A 2 0.492735 0.607184 0.614768 11.00000 -1.20000 H8B 2 0.388375 0.612314 0.533321 11.00000 -1.20000 AFIX 0 C9 1 0.552070 0.716538 0.526782 11.00000 0.01711 0.02256 = 0.01701 -0.00173 0.00212 0.00219 AFIX 13 H9 2 0.474981 0.763976 0.512113 11.00000 -1.20000 AFIX 0 C10 1 0.771233 0.739437 0.150277 11.00000 0.02227 0.01870 = 0.01388 0.00113 0.00409 0.00125 C11 1 0.798683 0.824730 0.104002 11.00000 0.02908 0.02137 = 0.02725 0.00558 0.00937 0.00072 AFIX 43 H11 2 0.881137 0.862147 0.116091 11.00000 -1.20000 AFIX 0 C12 1 0.705833 0.855790 0.039844 11.00000 0.04521 0.02740 = 0.03104 0.01389 0.01070 0.01217 AFIX 43 H12 2 0.726127 0.913512 0.007857 11.00000 -1.20000 AFIX 0 C13 1 0.584664 0.802613 0.022951 11.00000 0.03921 0.03615 = 0.01967 0.00259 -0.00020 0.01782 AFIX 43 H13 2 0.521571 0.823992 -0.020557 11.00000 -1.20000 AFIX 0 C14 1 0.554572 0.717920 0.069328 11.00000 0.02940 0.03351 = 0.01992 -0.00465 -0.00501 0.00528 AFIX 43 H14 2 0.470748 0.681654 0.058062 11.00000 -1.20000 AFIX 0 C15 1 0.648074 0.686780 0.132260 11.00000 0.02637 0.02123 = 0.01820 0.00000 -0.00212 -0.00132 AFIX 43 H15 2 0.627866 0.628591 0.163619 11.00000 -1.20000 AFIX 0 C16 1 0.650927 0.762073 0.591782 11.00000 0.01869 0.01798 = 0.01326 0.00010 0.00345 0.00237 C17 1 0.752151 0.705186 0.634646 11.00000 0.02711 0.01620 = 0.02554 0.00079 -0.00264 0.00306 AFIX 43 H17 2 0.759711 0.636932 0.622473 11.00000 -1.20000 AFIX 0 C18 1 0.841698 0.747659 0.694855 11.00000 0.02426 0.02171 = 0.02460 0.00456 -0.00472 -0.00015 AFIX 43 H18 2 0.910325 0.708498 0.723323 11.00000 -1.20000 AFIX 0 C19 1 0.830870 0.846868 0.713291 11.00000 0.02748 0.02348 = 0.02449 -0.00248 -0.00319 -0.00243 AFIX 43 H19 2 0.889286 0.875467 0.756045 11.00000 -1.20000 AFIX 0 C20 1 0.734270 0.904396 0.669030 11.00000 0.03569 0.01632 = 0.03125 -0.00361 -0.00330 0.00418 AFIX 43 H20 2 0.728741 0.972970 0.680196 11.00000 -1.20000 AFIX 0 C21 1 0.645617 0.862120 0.608459 11.00000 0.02649 0.01899 = 0.02260 -0.00047 -0.00125 0.00679 AFIX 43 H21 2 0.580517 0.902282 0.578075 11.00000 -1.20000 HKLF 4 REM mo_p17056_0m_a.res in P2(1)2(1)2(1) REM R1 = 0.0335 for 11216 Fo > 4sig(Fo) and 0.0612 for all 15114 data REM 246 parameters refined using 0 restraints END WGHT 0.0094 0.0000 REM Highest difference peak 0.527, deepest hole -0.637, 1-sigma level 0.079 Q1 1 0.6629 0.9403 0.3409 11.00000 0.05 0.53 Q2 1 0.8055 0.7185 0.6686 11.00000 0.05 0.37 Q3 1 0.6328 0.3374 0.4299 11.00000 0.05 0.35 Q4 1 0.6967 0.7228 0.1368 11.00000 0.05 0.34 Q5 1 0.6134 0.7035 0.0970 11.00000 0.05 0.33 Q6 1 0.5875 0.7597 0.0499 11.00000 0.05 0.33 Q7 1 0.7953 0.7820 0.1300 11.00000 0.05 0.32 Q8 1 0.8101 0.7242 0.1821 11.00000 0.05 0.32 Q9 1 0.6854 0.8831 0.6406 11.00000 0.05 0.31 Q10 1 0.7128 0.7213 0.6000 11.00000 0.05 0.31 Q11 1 0.9185 0.8378 0.6155 11.00000 0.05 0.30 Q12 1 0.7695 0.8573 0.0612 11.00000 0.05 0.30 Q13 1 0.6564 0.9597 0.3005 11.00000 0.05 0.29 Q14 1 0.5118 0.6736 0.5404 11.00000 0.05 0.29 Q15 1 0.6827 0.5734 0.4138 11.00000 0.05 0.29 Q16 1 0.6849 0.7388 0.4186 11.00000 0.05 0.29 Q17 1 0.9077 0.6573 0.2050 11.00000 0.05 0.29 Q18 1 0.8262 0.6397 0.3131 11.00000 0.05 0.28 Q19 1 0.6515 0.6428 0.4483 11.00000 0.05 0.28 Q20 1 0.7705 0.6336 0.2970 11.00000 0.05 0.28 REM The information below was added by Olex2. REM REM R1 = 0.0335 for 11216 Fo > 4sig(Fo) and 0.0612 for all 58666 data REM n/a parameters refined using n/a restraints REM Highest difference peak 0.53, deepest hole -0.64 REM Mean Shift 0, Max Shift 0.002. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0612 REM R1_gt = 0.0335 REM wR_ref = 0.0566 REM GOOF = 0.988 REM Shift_max = 0.002 REM Shift_mean = 0 REM Reflections_all = 58666 REM Reflections_gt = 11216 REM Parameters = n/a REM Hole = -0.64 REM Peak = 0.53 REM Flack = 0.006(4) ; _olex2_submission_original_sample_id ((R,R)-Ph-BOX)NiBr _olex2_submission_special_instructions 'No special instructions were received' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma -1 0 0 -0.1 0.2 -1 0 0 -0.5 0.9 -2 0 0 6908.41 399.96 2 0 0 6973.9 399.96 3 0 0 2.2 2.6 3 0 0 -1.3 0.7 -3 0 0 -2.8 2.6 -3 0 0 -0.2 0.9 -4 0 0 5077.19 304.87 -4 0 0 5686.43 307.77 4 0 0 4949.21 304.67 4 0 0 5507.15 307.47 5 0 0 4.2 4.3 -5 0 0 4.2 1.1 5 0 0 2.6 1.5 -5 0 0 3 1.6 5 0 0 5.9 4.6 6 0 0 221.78 18 -6 0 0 220.28 13.1 6 0 0 214.88 17.7 -6 0 0 228.98 14.1 6 0 0 225.28 13.7 -7 0 0 6.3 1.6 7 0 0 10.6 5.7 7 0 0 4.4 2.1 7 0 0 -0.8 5.6 -7 0 0 2.9 2.8 -8 0 0 44.1 5.9 -8 0 0 41.2 3.2 8 0 0 40.5 5.1 -9 0 0 -0.6 3.1 9 0 0 -0.7 3 -10 0 0 104.89 9.9 10 0 0 115.29 9.7 11 0 0 7 4.3 -11 0 0 1.5 4.1 -12 0 0 364.06 23.8 12 0 0 343.67 23.2 -13 0 0 -0.3 6 -13 0 0 4.8 6 13 0 0 13 5.7 14 0 0 8.6 6.4 -14 0 0 -9 6 -14 0 0 4.9 6.8 15 0 0 4 6.8 -15 0 0 -1.1 7.4 16 0 0 118.69 14.2 -16 0 0 103.49 15.1 -17 0 0 8.2 9.4 17 0 0 5.1 7.9 18 0 0 7.4 8.8 -1 1 0 31.6 2.2 1 1 0 35 2 -1 -1 0 29.4 3 1 -1 0 32.8 2.2 -2 1 0 4913.21 266.37 2 1 0 4263.87 262.87 2 -1 0 5029.2 266.37 2 -1 0 4129.19 262.97 -3 1 0 8.8 1.9 3 -1 0 11.2 4.2 3 1 0 11.8 1.5 -3 1 0 14.1 1.2 3 -1 0 12.4 1.6 -3 1 0 9.6 4.4 3 -1 0 18.5 2 3 -1 0 12.9 1.1 -4 1 0 368.66 27.1 4 -1 0 344.27 22.3 -4 1 0 388.86 21.9 -4 1 0 379.06 22.4 4 1 0 382.06 22.1 4 -1 0 398.06 27.2 -4 -1 0 380.36 22.3 5 -1 0 546.45 38.3 -5 -1 0 564.94 32.9 5 1 0 566.94 32.7 -5 1 0 563.74 38.6 -5 1 0 557.34 33 -5 1 0 575.74 32.4 5 -1 0 536.05 32.7 6 -1 0 2.4 1.8 -6 1 0 4.3 1 -6 1 0 3.8 2.2 6 1 0 3.2 1.8 -6 -1 0 2.9 1.9 6 -1 0 -0.4 6.8 6 -1 0 7.3 6.6 7 -1 0 156.18 10.6 7 1 0 155.98 10.5 -7 1 0 173.68 11.2 -7 -1 0 170.88 11 7 -1 0 174.98 19.6 -7 -1 0 149.19 9.5 -7 1 0 163.58 9.8 7 -1 0 160.78 18.3 8 1 0 17.1 4.2 -8 1 0 15.3 2.5 -8 -1 0 12.3 3.2 -8 1 0 16.3 3.5 8 -1 0 8.6 8.5 8 -1 0 12.5 3 8 -1 0 23 9.9 -8 -1 0 15.8 1.9 9 -1 0 82.29 16.1 9 -1 0 83.99 7.8 -9 1 0 83.19 5.9 9 -1 0 97.49 17.4 -9 -1 0 82.49 8.1 9 1 0 88.19 7.5 -9 1 0 88.29 8.4 -10 -1 0 21.9 6.5 10 1 0 36.4 6.4 -10 1 0 30.2 7 -11 -1 0 172.78 13.7 11 -1 0 181.58 13.6 -11 1 0 184.28 14.3 11 1 0 177.08 13.2 -12 -1 0 31.5 8.6 12 1 0 18.2 5.3 12 -1 0 18.6 5.7 -12 1 0 19.7 5.7 -13 -1 0 5.2 5.4 -13 -1 0 -1.7 5.8 -13 1 0 5.7 6.2 -13 1 0 10.6 6.1 13 -1 0 -0.6 5.3 13 1 0 6.2 5.6 -14 -1 0 104.49 12.6 14 1 0 78.89 11.5 -14 1 0 69.29 12.9 -14 1 0 112.29 13.4 14 -1 0 82.79 11.4 -14 -1 0 83.59 13.2 15 -1 0 12.7 7 -15 1 0 22.5 8.3 15 1 0 17.5 7 -15 -1 0 9.8 7.2 16 -1 0 7.4 7.8 16 1 0 6.7 7.3 -16 -1 0 5.3 8.5 -16 1 0 6.3 8.3 -17 1 0 -0.1 9.2 -17 -1 0 3.5 9 17 1 0 21 8.3 17 -1 0 -4 8.2 18 1 0 -9 8.5 18 -1 0 1.8 8.8 -18 1 0 -12.9 9.3 0 -2 0 1472.05 86.39 0 -2 0 1498.55 89.69 0 2 0 1536.45 86.29 1 2 0 878.81 52.19 -1 2 0 878.91 49.6 1 2 0 726.93 49.5 1 -2 0 876.21 49.6 1 2 0 868.01 49.7 -1 -2 0 865.11 52.19 -1 2 0 909.41 53.99 1 -2 0 881.11 49.8 -1 2 0 862.91 49.8 -1 -2 0 845.22 49.7 1 2 0 899.91 49.6 2 -2 0 2280.07 128.59 -2 -2 0 2337.07 130.19 2 2 0 2244.88 128.49 -2 2 0 2215.38 128.59 2 -2 0 2218.18 128.79 -2 2 0 2124.79 128.79 3 -2 0 2406.86 140.39 3 -2 0 2379.36 134.89 -3 2 0 2256.57 134.89 3 -2 0 2336.97 134.69 -3 2 0 2303.37 134.49 -3 2 0 2366.06 140.29 3 2 0 2338.27 134.59 4 -2 0 1943.51 115.09 -4 2 0 1935.41 114.89 4 -2 0 1958.5 114.79 4 -2 0 2074.29 115.39 4 -2 0 2059.29 121.79 -4 2 0 2124.79 122.09 -4 2 0 1984.2 115.39 4 2 0 1917.71 114.99 -5 2 0 46.2 3.2 5 -2 0 41.3 2.9 -5 2 0 34.6 9.9 -5 2 0 47.2 4.5 5 -2 0 57.49 13.4 5 -2 0 45.2 3.9 5 2 0 47.5 3.7 -6 2 0 948.81 54.39 -6 2 0 938.91 55.19 6 -2 0 920.71 54.79 6 -2 0 941.51 62.99 6 2 0 933.51 54.69 -6 -2 0 961.3 54.99 -7 -2 0 64.89 6.3 -7 2 0 73.49 5 7 2 0 77.29 5.8 -7 2 0 78.39 6.7 7 -2 0 69.39 6.1 7 -2 0 63.29 17.3 7 -2 0 71.09 18.2 8 -2 0 1805.32 112.09 -8 -2 0 1813.52 103.29 8 -2 0 1712.13 103.09 8 2 0 1804.32 102.99 -8 2 0 1819.32 103.49 -8 2 0 1761.72 102.39 8 -2 0 1712.93 111.29 9 -2 0 268.77 29.9 -9 2 0 262.37 17.5 -9 -2 0 264.27 17.2 9 -2 0 197.68 35.1 9 -2 0 265.57 17 -9 2 0 258.07 15.8 9 2 0 270.27 16.7 10 -2 0 4.5 3.8 10 -2 0 -3.8 12.6 -10 2 0 2 3.8 -10 -2 0 -0.7 3.5 10 2 0 3 3.6 10 -2 0 3.9 13.9 11 -2 0 0.4 4.3 -11 -2 0 2.2 4.1 -11 2 0 -6.6 4.1 11 2 0 -3.4 4 12 -2 0 23.3 5.7 -12 2 0 33.3 9.1 -12 -2 0 20.1 5.3 12 2 0 20.2 5.3 -13 2 0 151.58 15.5 13 2 0 183.58 14.3 -13 -2 0 184.08 14.9 13 -2 0 172.48 14.8 -13 2 0 178.48 15.7 -13 -2 0 173.48 14.7 -14 -2 0 9.5 6.3 14 2 0 0.1 5.8 14 -2 0 2.1 6.4 -14 2 0 2.9 7.2 -14 2 0 -3.9 6.5 15 2 0 20.8 7 -15 2 0 25.4 8.4 15 -2 0 20.7 7.8 -15 -2 0 30.3 7.5 -15 2 0 4 8.2 16 2 0 -6.9 7 -16 2 0 -3.1 8.3 16 -2 0 7.5 8 17 -2 0 5.7 8.4 17 2 0 10.7 8.1 -17 2 0 12.8 9.3 18 2 0 26.9 9.1 18 -2 0 20.9 9.2 -18 2 0 24.7 10.6 0 3 0 1.2 3.4 0 3 0 1.3 0.4 0 3 0 0.6 0.6 0 -3 0 0.5 0.6 0 -3 0 0.5 3.5 -1 3 0 896.91 52.09 1 3 0 927.41 51.69 1 -3 0 892.11 51.89 -1 3 0 902.21 57.69 1 -3 0 895.91 52.09 -1 3 0 900.21 51.89 -1 -3 0 888.91 51.99 -1 -3 0 876.11 55.99 1 3 0 916.91 56.19 1 3 0 902.41 51.99 -2 -3 0 295.17 20.9 2 3 0 298.57 17.3 2 -3 0 294.67 17.6 2 -3 0 306.77 17.4 -2 3 0 287.27 17.6 -2 -3 0 298.77 17.4 2 -3 0 281.27 23.9 -2 3 0 300.47 24.4 -2 3 0 302.17 17.4 3 -3 0 503.35 29.6 -3 3 0 504.85 29.5 3 3 0 532.45 29.5 -3 -3 0 496.05 32 -3 -3 0 517.85 31.9 -3 3 0 515.75 29.9 -3 3 0 475.05 37.5 -4 3 0 105.29 6.7 4 3 0 109.29 6.8 -4 3 0 114.79 16.4 -4 3 0 106.29 7.4 4 -3 0 113.19 7 4 -3 0 100.59 15.7 5 -3 0 16.1 2.8 -5 3 0 19.4 3.5 5 -3 0 14.8 2 5 -3 0 21.9 9 -5 3 0 9.3 9.3 -5 3 0 16.9 2.2 5 3 0 16.8 2.4 6 3 0 1991.1 116.49 -6 3 0 2191.48 117.19 -6 3 0 1938.81 116.29 6 -3 0 1909.91 116.09 6 -3 0 1971.6 116.69 6 -3 0 2028.3 126.49 -6 3 0 2124.49 127.49 7 -3 0 700.33 43 7 -3 0 725.83 54.69 -7 -3 0 769.62 43.1 7 -3 0 714.33 54.49 -7 3 0 718.53 43.4 7 3 0 734.83 42.8 -7 3 0 736.73 42.5 -8 3 0 51.79 6.6 8 -3 0 27 15 8 -3 0 49.99 5.7 -8 3 0 41.7 4 8 3 0 47 5.2 -8 -3 0 40.4 5.6 8 -3 0 33.3 14.7 9 -3 0 757.92 56.49 9 -3 0 711.33 42.7 -9 3 0 700.23 41.9 -9 -3 0 731.13 42.9 -9 3 0 727.93 43.3 9 3 0 724.23 42.5 9 -3 0 667.23 54.99 10 3 0 648.14 37.4 -10 3 0 621.04 38.2 10 -3 0 604.44 37.7 10 -3 0 608.64 51.59 -10 -3 0 626.84 37.8 -11 3 0 -0.4 4.5 -11 -3 0 -0.1 4 11 3 0 -1.6 3.8 11 -3 0 -1.6 4.2 11 -3 0 9.4 18.3 12 -3 0 116.09 11.4 12 3 0 118.09 10.6 -12 -3 0 122.89 11.3 -12 3 0 109.49 12.5 -13 -3 0 88.79 12.3 -13 3 0 82.09 12.3 -13 -3 0 69.29 10.5 -13 3 0 75.69 12.2 13 3 0 76.49 10 13 -3 0 83.49 10.7 -14 3 0 22.8 8 14 -3 0 28.2 7.6 -14 -3 0 37.2 7.5 14 3 0 21.5 6.4 -14 3 0 33.9 8 -15 -3 0 16.4 7.1 -15 3 0 -11.6 7.6 15 3 0 3.4 6.6 15 -3 0 5.1 8 -15 3 0 2.6 7.9 16 3 0 6.1 7.4 -16 3 0 11 8.9 16 -3 0 7.6 8.1 17 3 0 3.4 8 -17 3 0 8.2 9.4 17 -3 0 -0.8 8.6 18 -3 0 -7.8 8.4 18 3 0 8 8.2 -18 3 0 -21.3 9.7 0 4 0 3100.89 186.68 0 -4 0 3059.19 180.28 0 -4 0 3251.07 187.08 1 4 0 1415.76 86.39 1 4 0 1339.17 80.49 -1 -4 0 1413.96 80.49 -1 4 0 1354.26 80.59 -1 4 0 1415.26 87.89 -1 -4 0 1413.96 86.39 1 4 0 1409.66 80.19 1 -4 0 1411.46 80.59 2 -4 0 354.06 29.8 2 4 0 355.26 26.4 -2 4 0 363.56 21.7 2 4 0 367.86 21.5 -2 4 0 350.66 29.7 2 4 0 381.66 21.2 -2 -4 0 351.66 26.5 -2 -4 0 363.76 21.5 2 4 0 378.96 21.2 2 -4 0 362.76 21.4 -2 4 0 371.46 21.4 3 -4 0 37.4 3.2 3 4 0 40.6 2.8 -3 -4 0 32 8 -3 4 0 44.9 12.9 3 -4 0 59.79 13.8 -3 -4 0 37.5 3.1 3 -4 0 39.5 3.6 -3 4 0 40.4 3.8 -3 4 0 44.8 3.1 -3 -4 0 40.3 8.8 -4 4 0 462.85 36.8 -4 4 0 449.95 26.1 -4 -4 0 400.16 28.4 -4 -4 0 453.75 28.8 -4 4 0 424.36 25.6 4 4 0 423.96 25.5 4 -4 0 455.75 25.7 5 4 0 3434.96 203.48 5 -4 0 3517.55 203.78 5 -4 0 3710.03 215.08 -5 4 0 3392.56 203.48 -5 4 0 3689.73 215.58 -5 4 0 3521.35 204.08 -6 4 0 1.7 2.4 -6 4 0 1 10.8 6 4 0 -0.2 1.7 6 -4 0 2.9 2.1 6 -4 0 -4.6 10 6 -4 0 1.1 1.3 7 4 0 1098.59 64.59 7 -4 0 1099.09 77.89 -7 4 0 1107.19 64.49 -7 4 0 1142.69 65.39 7 -4 0 1109.49 64.89 -8 4 0 34.2 6.5 8 -4 0 60.99 17.5 8 -4 0 35.3 5.6 8 4 0 40.9 4.7 -8 4 0 33.8 4 8 -4 0 18.5 16.6 -8 -4 0 37.8 5.3 9 -4 0 271.17 37.5 9 -4 0 274.97 38.7 -9 4 0 284.37 17.9 9 -4 0 300.67 19 9 4 0 300.57 18.5 -9 4 0 280.87 19.5 -9 -4 0 316.67 19 10 -4 0 13.7 4.5 10 4 0 10.4 3.7 10 -4 0 35 19.9 -10 -4 0 15.2 4.1 -10 4 0 10.9 4.7 11 4 0 359.86 22.2 -11 -4 0 342.47 22.5 11 -4 0 344.77 22.6 -11 4 0 337.47 23.4 12 -4 0 17.2 6 12 4 0 19.2 5 -12 -4 0 15.6 5.1 -13 4 0 27.5 7.3 13 4 0 28.2 5.9 -13 -4 0 23.7 6 13 -4 0 32.5 7.1 -13 4 0 26.2 7.7 -14 4 0 18.4 7.9 -14 -4 0 16.4 6.7 -14 4 0 22.2 7.6 14 -4 0 21.5 7.5 14 4 0 23.5 6.4 -15 4 0 4.4 8 15 4 0 6.3 6.6 15 -4 0 3.6 11.4 -15 4 0 -3.1 8.1 -16 4 0 20.4 9.5 16 -4 0 15.3 8.7 16 4 0 0 7.1 -17 4 0 28 10.6 17 -4 0 22.8 9.2 17 4 0 21.1 8.1 -18 4 0 -20.7 9.9 18 4 0 12.4 8 18 -4 0 -11 9.2 0 -5 0 1 0.9 0 5 0 0.4 1 0 5 0 1.7 0.7 0 -5 0 -4.9 6.4 0 5 0 -2.7 4.5 1 -5 0 30 10 -1 -5 0 34.3 11.2 -1 5 0 42.5 12.8 1 5 0 27.9 2.7 -1 -5 0 27 2.5 1 -5 0 26.1 2.7 -1 5 0 26.3 2.8 -1 5 0 26.2 2.3 1 5 0 28.5 1.9 1 5 0 27.9 8 2 5 0 3654.33 216.38 2 5 0 3956 223.38 2 -5 0 3789.42 226.48 2 -5 0 3675.73 216.58 -2 5 0 3930.41 226.68 -2 -5 0 3816.02 223.18 2 5 0 3834.72 215.98 2 -5 0 3706.53 216.18 -2 5 0 3636.54 216.48 -2 -5 0 3707.83 216.28 -2 5 0 3696.03 216.28 3 -5 0 483.85 27.6 -3 5 0 473.55 28 3 -5 0 461.25 38.7 -3 -5 0 470.55 33.8 -3 -5 0 451.75 27.7 -3 5 0 468.25 39.1 -3 -5 0 474.75 33.8 3 5 0 484.45 27.4 -4 5 0 61.19 18.4 -4 -5 0 62.19 11.6 -4 5 0 62.59 4.7 -4 -5 0 65.49 4.8 4 -5 0 77.09 18.6 -4 -5 0 76.29 11.3 4 -5 0 72.19 4.9 -4 5 0 61.69 5.6 4 5 0 64.99 4.4 -5 -5 0 121.09 12 5 5 0 115.99 7.1 5 -5 0 111.09 7.6 -5 5 0 132.89 25.1 -5 -5 0 107.29 7.4 -5 5 0 113.49 8.4 5 -5 0 72.09 20.5 -5 -5 0 106.79 11.3 -5 5 0 107.69 7.3 6 -5 0 10.9 11.8 -6 5 0 28.1 5.2 6 5 0 28.3 3.3 -6 5 0 74.39 23.1 6 -5 0 24.3 3.2 6 -5 0 27.2 4 -6 5 0 22.7 3.3 7 -5 0 962.6 54.09 7 -5 0 932.81 69.79 -7 5 0 931.51 54.29 7 -5 0 922.41 54.69 -7 5 0 923.01 55.19 7 5 0 926.61 54.39 8 -5 0 30 5.3 8 5 0 22.1 4.4 -8 5 0 25.4 6.4 -8 -5 0 27.2 5 8 -5 0 25.3 2.8 8 -5 0 17.8 16.4 -8 5 0 26.3 3.9 8 -5 0 11.6 17.7 9 -5 0 854.71 49.9 -9 -5 0 872.01 49.9 -9 5 0 823.62 50.49 9 -5 0 792.52 68.49 9 5 0 841.92 49.4 9 -5 0 822.02 68.39 -10 -5 0 18.8 4.2 10 5 0 19 3.9 -10 5 0 17 5.3 10 -5 0 17.9 4.8 11 -5 0 15.3 5.3 -11 -5 0 10.3 4.3 -11 5 0 16.3 5.6 11 5 0 11 4.2 -12 -5 0 47.9 8.5 12 5 0 49.6 8 12 -5 0 37.5 8.9 -12 5 0 34.6 7.7 -12 5 0 47.6 10.9 -13 5 0 1 7 -13 5 0 -3.8 6.1 -13 -5 0 4.2 5.1 13 5 0 3 5.2 13 -5 0 8.1 6.2 -14 5 0 57.39 10 14 -5 0 74.69 12.3 -14 5 0 55.19 13.4 14 5 0 65.29 10.3 -15 5 0 7.8 8.1 15 5 0 2.6 6.4 -15 5 0 -1.2 11 15 -5 0 5.8 7.5 16 5 0 3.1 6.9 16 -5 0 -1.2 8.3 -16 5 0 5.7 9.3 17 5 0 21 7.8 -17 5 0 18.1 10.7 17 -5 0 26.2 9.7 0 -6 0 1415.66 91.69 0 6 0 1366.86 81.39 0 -6 0 1405.76 81.39 0 6 0 1358.26 91.19 0 6 0 1475.35 80.99 1 6 0 1922.91 112.09 1 6 0 1937.71 121.49 -1 -6 0 1963.3 121.59 -1 6 0 1907.01 122.89 1 6 0 1978.4 111.69 -1 -6 0 1977 112.09 1 -6 0 1959.7 112.19 -1 6 0 1868.01 112.19 -1 6 0 1961 111.89 2 -6 0 12.5 9 -2 -6 0 5.9 1.4 -2 -6 0 13.4 7.7 2 6 0 7.6 1.7 2 6 0 3.6 6.7 2 -6 0 6.9 1.6 -2 6 0 3.3 1.8 -2 6 0 -1 8.6 2 6 0 7.8 1 3 -6 0 3809.22 226.68 -3 -6 0 3801.92 221.28 3 6 0 3568.74 213.28 -3 6 0 3621.24 213.88 -3 6 0 3680.63 213.48 -3 -6 0 3587.64 213.58 3 -6 0 3660.03 213.48 -3 6 0 3787.72 226.68 -3 -6 0 3927.01 221.38 4 -6 0 62.59 19.9 -4 -6 0 50.19 13.2 -4 6 0 65.59 17.6 -4 -6 0 55.79 4.4 4 6 0 54.89 3.9 -4 6 0 55.09 4.4 4 -6 0 54.09 4.5 -4 -6 0 49.4 13.6 -5 -6 0 19 7.6 -5 6 0 25.1 4.9 -5 6 0 28.9 3.5 5 -6 0 24 3.7 -5 -6 0 30.9 8.9 -5 6 0 35 13.7 5 6 0 32.6 3 -5 -6 0 30 3.4 5 -6 0 22.3 13.4 6 -6 0 29 16 6 6 0 13.3 2.8 -6 6 0 27.2 15.4 6 -6 0 11 2.8 -6 6 0 14.4 3.3 -6 6 0 18.1 5 7 -6 0 326.47 20.6 7 -6 0 342.17 42.2 -7 6 0 329.77 20.1 -7 6 0 323.67 21.3 7 6 0 335.07 20.1 7 -6 0 346.77 20 8 6 0 6.9 2.7 8 -6 0 5.3 3.4 8 -6 0 8.5 18.6 8 -6 0 16.1 19.1 8 -6 0 9.1 1.9 -8 6 0 12.7 4 9 -6 0 501.95 32 9 -6 0 500.45 30 -9 6 0 520.65 32.4 9 6 0 523.05 30.9 9 -6 0 494.45 56.39 -9 -6 0 544.95 31.5 -10 6 0 -1.2 4.6 -10 -6 0 6.1 3.6 10 6 0 3.1 3.4 10 -6 0 3.2 4.6 -11 -6 0 52.29 8.1 11 6 0 58.99 7.6 -11 6 0 62.79 10.3 11 -6 0 45.8 9 12 6 0 -0.2 4.4 12 -6 0 7.9 5.8 -12 6 0 3.6 6.4 -12 6 0 9.3 6 -12 -6 0 8.5 4.8 -13 6 0 320.87 23.6 -13 6 0 320.87 23.4 13 6 0 311.57 21.2 13 -6 0 305.97 22.2 -14 6 0 -4.5 7.9 14 -6 0 -5.6 6.8 -14 6 0 1.2 7.7 14 6 0 -2.1 5.6 15 6 0 31.3 7.1 15 -6 0 29.4 8.8 -15 6 0 33.7 9.5 -16 6 0 -4.8 9.5 16 -6 0 14.4 8.9 16 6 0 9.2 6.8 -17 6 0 9.6 10.4 17 -6 0 4.8 9.6 0 7 0 0.4 1.5 0 7 0 -4.4 9.5 0 -7 0 2.1 8.8 0 7 0 1.9 1 0 -7 0 0.5 1.3 1 -7 0 502.45 43.4 1 7 0 480.05 41.6 1 7 0 525.25 30.2 -1 -7 0 525.35 30.7 -1 7 0 533.95 44.2 -1 7 0 531.55 30.9 -1 7 0 540.35 30.5 1 7 0 528.35 30.8 -1 -7 0 490.05 41.4 2 7 0 1104.59 78.29 -2 7 0 1168.68 68.69 -2 -7 0 1169.48 78.89 -2 -7 0 1149.08 68.39 -2 7 0 1154.98 82.39 -2 7 0 1191.28 68.29 2 -7 0 1195.08 68.19 2 7 0 1222.98 67.89 2 7 0 1191.18 68.59 2 -7 0 1237.88 82.79 -3 7 0 -2.8 10.8 3 -7 0 -1.8 10.5 -3 -7 0 4 1.5 3 7 0 4.6 1.8 3 -7 0 1.8 1.5 -3 -7 0 -0.5 8.3 -3 -7 0 6.4 9.2 -3 7 0 2.4 2.4 -4 -7 0 88.79 6.4 -4 -7 0 102.49 18 4 -7 0 90.89 6.4 4 -7 0 81.09 24.7 -4 -7 0 83.29 16.9 -4 7 0 89.09 25 -4 7 0 97.29 7.4 4 7 0 86.69 6 5 -7 0 546.45 50.19 -5 -7 0 549.25 39.7 -5 7 0 514.25 49.9 -5 7 0 551.14 32.7 -5 -7 0 566.24 40.4 5 7 0 536.65 31.6 5 -7 0 527.55 32 -6 -7 0 171.08 17.6 6 7 0 155.48 9.9 -6 7 0 133.79 32.2 -6 7 0 155.28 11.5 6 -7 0 153.18 10.7 -6 -7 0 166.78 18.1 7 -7 0 2.6 3.4 7 -7 0 -1.2 2.8 7 7 0 5.3 2.1 -7 7 0 2.4 3.6 7 -7 0 20.6 19.9 8 -7 0 -6.7 20.8 8 7 0 5.5 2.5 8 -7 0 14 22.4 8 -7 0 1.5 3.5 8 -7 0 0.2 2.2 -8 7 0 3.7 3.9 -9 -7 0 170.58 12.3 9 7 0 174.38 11.7 9 -7 0 171.98 10.9 9 -7 0 177.58 12.9 -9 7 0 167.38 13.9 10 -7 0 38.5 7.9 -10 -7 0 37.2 7 -10 7 0 44 9.1 10 7 0 43.2 6.2 11 7 0 251.27 15.9 11 -7 0 211.18 17.1 -11 -7 0 232.68 16.4 -11 7 0 240.88 18.3 -11 7 0 231.08 17.8 -12 7 0 7.9 6.5 -12 7 0 -4.4 6.4 12 -7 0 4.3 5.9 12 7 0 6.7 4.3 13 7 0 15.2 5.3 13 -7 0 19.6 6.9 -13 7 0 10.4 7.5 -13 7 0 2.2 7.1 14 7 0 5 5.6 -14 7 0 2.4 8.4 14 -7 0 7.7 7.2 -14 7 0 -4.4 7.3 15 -7 0 40.7 9.5 15 7 0 39.8 7.1 -15 7 0 34.9 10.1 -16 7 0 2.6 9.6 16 7 0 6.1 9.5 16 -7 0 6.3 9.2 -17 7 0 8.5 10.7 17 -7 0 10.6 9.6 0 -8 0 3202.98 194.58 0 8 0 3218.28 194.88 0 8 0 3060.29 179.98 0 8 0 3062.99 180.48 -1 8 0 4 2 1 8 0 6.4 1.1 1 -8 0 9 11.8 -1 -8 0 11.6 11.2 1 8 0 3.2 9.5 1 8 0 7.4 2.1 -1 8 0 0.2 11.4 -1 8 0 6.5 1.5 -2 8 0 35.4 5.3 2 8 0 37.7 4.2 -2 -8 0 33.3 13.1 2 8 0 31.8 13 -2 8 0 53.29 17.9 2 -8 0 20.9 13.6 -2 8 0 33.1 3.6 2 -8 0 40 3.4 2 8 0 42.9 2.7 3 -8 0 603.14 34.9 -3 -8 0 588.54 47.2 -3 -8 0 573.04 47.1 3 -8 0 564.44 51.29 -3 8 0 600.94 35.1 3 8 0 624.74 35.3 -3 8 0 598.04 35.6 -3 8 0 559.44 52.29 -4 -8 0 1425.56 93.29 -4 8 0 1450.45 83.09 4 -8 0 1426.86 82.39 4 -8 0 1314.37 99.29 -4 -8 0 1471.55 93.09 -5 8 0 2215.88 128.29 -5 8 0 2216.78 147.39 5 -8 0 2209.48 127.69 5 8 0 2148.09 127.29 5 -8 0 2364.06 148.19 -5 -8 0 2129.49 136.19 -5 -8 0 2220.48 136.79 6 8 0 101.09 6.7 -6 8 0 68.79 21.5 -6 -8 0 104.59 18.5 6 -8 0 92.39 7.7 -6 -8 0 111.19 19.9 -6 8 0 95.39 8.9 6 -8 0 117.29 32 -7 8 0 931.21 56.29 7 8 0 942.41 54.89 7 -8 0 956.6 55.59 7 -8 0 945.81 55.19 8 8 0 220.58 12.8 -8 8 0 199.18 15 8 -8 0 168.88 36.3 8 -8 0 178.58 12.9 8 -8 0 207.68 13.9 8 -8 0 166.28 46.2 9 -8 0 121.79 10.7 -9 8 0 130.19 11.9 9 8 0 134.09 9 9 -8 0 103.09 8.4 -10 8 0 89.69 11.1 10 8 0 94.29 8 10 -8 0 90.59 9.9 -10 -8 0 87.39 8.8 -10 8 0 79.79 10.5 -11 8 0 288.37 20.8 11 8 0 273.97 18 -11 8 0 271.07 20.1 11 -8 0 274.37 19.4 -12 8 0 173.08 16.8 12 8 0 170.48 13 -12 8 0 173.78 15.8 12 -8 0 177.38 15.2 13 8 0 1.2 4.6 -13 8 0 -4.7 6.8 13 -8 0 3.3 6.6 -13 8 0 5.2 7.9 14 8 0 13 5.5 14 -8 0 -0.6 8.6 -14 8 0 1.2 7.9 -14 8 0 1.1 8.8 -15 8 0 20.7 9.9 15 -8 0 -5.8 8.2 15 8 0 -2.3 7.3 -16 8 0 69.39 16.6 16 -8 0 29.1 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-3 3 -2 97.89 5.8 3 3 2 100.49 5.5 4 3 -2 1213.58 76.19 4 -3 2 1263.67 72.69 4 3 -2 1211.48 72.39 -4 3 2 1263.87 81.69 4 -3 2 1252.67 81.29 -4 3 2 1235.08 72.49 -4 -3 -2 1284.77 74.59 4 -3 2 1259.17 81.49 4 -3 2 1195.28 73.09 4 -3 2 1230.58 72.39 -4 3 2 1218.48 72.99 4 -3 -2 1340.47 82.19 4 3 2 1273.17 74.59 -4 -3 2 1309.27 76.39 -4 -3 2 1334.97 72.29 -4 3 -2 1266.27 72.89 4 3 2 1224.48 72.49 4 -3 -2 1254.47 72.69 -5 3 2 3752.82 213.08 -5 -3 -2 3636.64 202.68 5 -3 2 3451.15 202.48 5 -3 2 3522.15 212.18 5 3 -2 3463.85 202.68 -5 3 2 3612.94 203.28 5 3 -2 3831.02 205.78 5 -3 2 3472.35 202.88 -5 3 2 3398.36 202.58 5 -3 2 3675.83 212.58 -5 3 -2 3381.96 203.08 -5 -3 2 3307.37 202.38 5 -3 -2 3603.74 212.78 5 3 2 3338.97 202.68 5 -3 -2 3366.46 202.78 -5 -3 2 3609.84 205.38 6 -3 2 44.8 4.5 -6 -3 -2 41.3 4 6 -3 2 45 13.7 -6 3 2 47.2 5.4 -6 3 2 41.7 3.6 -6 3 2 51.69 14.8 6 3 -2 40.2 3.9 6 -3 2 44 3 6 -3 2 44.2 12.3 6 -3 -2 34.9 12 6 -3 -2 36.7 4.4 6 3 2 47 4.2 -6 -3 2 40.5 2.9 7 -3 2 603.24 37 -7 3 2 652.73 50.19 -7 -3 -2 636.24 36.9 -7 3 2 635.34 37.7 7 3 -2 640.34 36.8 7 -3 2 623.34 48.9 7 -3 2 644.74 49.8 -7 3 2 613.24 36.6 -7 3 -2 653.43 37.5 7 -3 -2 632.04 49.4 7 3 2 638.84 36.9 -7 -3 2 584.74 36.2 7 -3 -2 605.94 37.1 7 -3 -2 633.24 36.1 8 -3 2 538.85 43.8 8 3 -2 531.55 30.1 -8 3 2 528.85 47.1 -8 -3 -2 533.25 30.2 -8 3 2 522.65 31.1 -8 3 2 525.15 29.7 8 -3 2 522.85 30.4 8 -3 2 448.06 43.3 8 3 2 471.35 30.1 -8 3 -2 482.35 30.6 8 -3 -2 459.95 30.2 8 -3 -2 475.65 43.3 -8 -3 2 495.95 30.7 9 -3 2 145.09 10.5 9 -3 2 132.39 29.1 -9 3 2 134.29 9.1 -9 -3 -2 139.09 10 9 -3 2 141.49 29.1 -9 3 2 135.49 11.5 9 3 -2 140.19 9.9 9 -3 -2 89.09 27.4 -10 3 2 29.3 8 -10 -3 -2 33.3 6.2 -10 3 2 36.7 4.8 10 -3 2 36.8 6.9 10 -3 2 8.6 17.7 -10 -3 -2 35.5 6.2 10 3 -2 32.2 5.8 10 3 2 54.49 8.6 -10 3 -2 45.1 7.7 -10 -3 2 45.7 7.5 10 -3 -2 40.1 18.7 -10 3 -2 42.6 7.8 10 -3 -2 40.8 7.1 11 -3 2 251.87 17.1 11 -3 2 218.28 34.4 11 3 -2 251.97 16.6 -11 3 2 249.38 18.3 -11 -3 -2 248.58 16.6 -11 -3 -2 256.37 16.7 11 3 2 241.08 16.8 -11 3 -2 242.28 17.6 -11 3 -2 239.08 17.7 11 -3 -2 240.68 17 -11 -3 2 237.18 17.5 -12 -3 -2 54.49 8.6 12 -3 2 50.99 9.5 -12 3 2 54.79 11 -12 -3 -2 62.89 8.2 12 3 -2 62.99 8.4 -12 -3 2 57.89 9.8 -12 3 -2 35.7 9.5 -12 3 -2 59.59 9.6 12 3 2 56.49 8.7 12 -3 -2 51.79 9.5 13 -3 2 -1.3 5.8 -13 3 2 0.1 6 13 3 -2 3.1 4.9 -13 -3 -2 4.2 5.3 13 3 2 2.4 5.3 13 -3 -2 15.7 6 -13 3 -2 -5.3 6.1 -13 3 -2 9.8 5.9 14 3 -2 23.5 6.3 14 -3 2 18.3 7.1 -14 3 2 17.8 7.6 -14 -3 -2 8.9 6 -14 -3 2 9.9 7.4 14 -3 -2 6.6 6.5 -14 3 -2 10.7 7.3 -14 3 -2 16.2 6.9 14 3 2 9.4 6.2 -15 3 2 10.9 8.7 -15 -3 -2 8 6.6 15 3 -2 3.8 7.1 -15 3 2 8.6 8.2 -15 -3 2 16.8 7.6 15 -3 -2 15.6 8.9 -15 3 -2 5 7.7 15 3 2 12.5 7.1 16 3 -2 4.2 6.8 -16 3 2 1.5 9.2 16 -3 2 6.2 8.2 16 -3 -2 0.4 7.9 -16 3 -2 -11.4 8.2 16 3 2 2 7.6 -16 -3 2 3.1 9.8 17 -3 2 11.4 8.5 -17 3 2 0.1 9.5 17 3 -2 -0.7 7.7 17 3 2 7.7 8.1 -17 3 -2 4.8 9.3 17 -3 -2 15.8 8.6 18 3 -2 -2.1 8.2 18 -3 2 -7.8 8.9 -18 3 2 -17.8 9.6 18 3 2 7.5 8.1 18 -3 -2 15.5 9.6 0 -4 -2 77.09 15.7 0 -4 2 55.29 11.5 0 -4 -2 52.69 3.7 0 -4 2 45.9 11.3 0 4 2 55.79 3.7 0 -4 2 57.99 3.4 0 4 2 51.99 11 0 4 2 53.39 3.7 0 -4 2 56.79 4 0 4 -2 57.49 3.7 0 4 -2 54.19 4.1 1 4 -2 1818.32 111.39 -1 4 2 1861.31 111.19 1 -4 2 1859.91 111.39 -1 -4 -2 1902.51 117.59 1 4 -2 1832.02 111.09 1 -4 2 1968.5 119.79 -1 -4 -2 1833.42 111.09 1 -4 2 1852.31 118.79 -1 4 2 1786.52 111.29 1 -4 2 1910.51 111.09 1 4 2 2074.59 118.09 1 -4 -2 2014.9 111.39 -1 4 -2 2018.3 111.19 -1 -4 2 2114.69 118.59 1 4 2 1924.71 111.09 1 -4 -2 2011.2 119.49 1 4 2 1972.4 111.09 -1 4 -2 1970.8 111.49 -1 -4 2 2018 111.39 -2 4 2 592.74 39.2 2 -4 2 612.24 39.2 -2 -4 -2 592.84 44 2 -4 2 637.34 38.9 2 -4 2 615.64 47.5 -2 4 2 614.14 39 2 4 -2 643.14 38.9 2 -4 2 566.64 46.5 -2 4 2 630.54 47.5 2 4 -2 628.34 38.7 -2 -4 -2 598.24 38.8 -2 4 -2 747.13 39.1 2 -4 -2 765.12 48.9 -2 -4 2 753.52 45.8 2 4 2 704.43 44.9 2 4 2 761.12 38.9 2 -4 -2 780.52 39.4 -2 4 -2 740.43 39.3 -2 -4 2 713.93 39.2 2 4 2 734.03 38.9 3 -4 2 46.1 3.8 -3 -4 -2 45.6 2.9 -3 4 2 45.1 13.7 3 -4 2 28.2 9.1 -3 -4 -2 46.6 3.1 3 -4 2 48.5 3.4 -3 4 2 46.3 3.4 -3 -4 -2 41.4 9 3 -4 2 43.1 11.3 3 4 -2 46.6 3 -3 4 2 49.5 4.1 3 4 -2 51.39 3.4 3 4 2 43.6 3.2 3 4 2 34.7 9.3 -3 4 -2 37.4 3.6 -3 -4 2 40 10.4 -3 4 -2 37.1 3.9 -3 -4 2 39.9 3.6 3 -4 -2 43 11.5 3 -4 -2 47.1 4.4 4 -4 2 1711.63 96.69 -4 4 2 1678.43 96.59 -4 -4 -2 1783.02 100.19 4 4 -2 1621.24 96.39 -4 4 2 1555.24 112.19 4 -4 2 1579.04 96.49 -4 4 2 1671.83 97.09 4 -4 2 1623.34 106.79 -4 -4 -2 1606.34 96.39 -4 4 -2 1733.63 96.99 4 -4 -2 1686.43 96.69 4 4 2 1693.83 96.49 4 4 2 1742.53 100.19 -4 -4 2 1712.13 101.29 -4 4 -2 1682.53 96.79 5 -4 2 346.37 21 -5 4 2 360.06 34.6 -5 4 2 306.37 22.3 5 -4 2 320.67 32.6 5 4 -2 345.77 21.1 5 -4 2 351.06 33.1 5 -4 2 338.87 21.3 -5 -4 2 384.56 25.9 5 4 2 369.96 21.2 -5 -4 2 386.16 25.6 -5 4 -2 382.46 21.8 5 -4 -2 372.56 21.4 5 -4 -2 392.26 34.6 6 -4 2 4261.17 249.38 6 -4 2 4307.57 249.58 -6 4 2 4256.47 249.97 6 -4 2 4025.7 237.08 -6 4 2 3959.6 237.48 6 4 -2 4025.2 236.78 -6 -4 -2 4077.89 236.88 -6 4 2 3978.8 236.78 6 -4 2 4001.6 236.58 6 4 2 4036.6 236.88 -6 -4 2 4026.1 236.48 6 -4 -2 4497.75 250.57 -6 4 -2 4260.67 237.48 6 -4 -2 4014 237.08 -7 4 2 35.9 3.6 7 -4 2 35.9 4.7 7 -4 2 20.6 13.9 7 -4 2 8 13.5 -7 4 2 34.5 14.5 7 4 -2 31.3 3.8 -7 4 2 26.5 5.7 -7 -4 -2 31.8 3.9 -7 -4 2 21.6 2.5 7 4 2 25.5 4 -7 4 -2 27.1 5.4 7 -4 -2 21.2 14.9 7 -4 -2 31.9 4.6 7 -4 -2 35.8 3 8 -4 2 125.49 9.7 -8 4 2 157.58 33.3 -8 -4 -2 136.39 9.2 -8 4 2 123.69 10.6 8 -4 2 82.39 27.2 -8 4 2 119.89 8.7 8 4 -2 127.19 9 8 -4 2 179.08 30.4 8 4 2 140.39 9.4 8 -4 -2 114.99 28.8 8 -4 -2 138.19 9.8 -8 4 -2 137.89 10.5 -9 4 2 92.89 25.2 9 -4 2 119.49 32.1 9 -4 2 109.19 9.6 -9 -4 -2 124.19 9.1 9 4 -2 115.49 8.9 -9 4 2 115.29 8.4 9 -4 2 78.79 22.1 -9 4 2 114.99 10.7 9 -4 -2 133.19 9.8 -9 4 -2 121.99 10.5 -9 4 -2 125.29 10.4 9 -4 -2 95.99 31.6 9 4 2 128.29 9.2 -9 -4 2 119.39 10.1 10 -4 2 637.54 38.3 10 4 -2 672.73 37.8 -10 -4 -2 668.63 37.9 -10 4 2 642.44 37.4 -10 -4 -2 653.03 38 10 -4 2 653.23 57.19 -10 4 2 645.64 39.1 -10 4 -2 615.94 38.7 -10 4 -2 590.04 38.5 10 -4 -2 608.14 38.3 10 4 2 565.84 39.3 10 -4 -2 684.23 80.49 -10 -4 2 625.34 38.6 -11 -4 -2 91.59 9.1 -11 -4 -2 78.69 8.7 11 4 -2 83.29 8.8 -11 4 2 80.79 11.1 11 -4 2 84.89 9.8 -11 4 -2 107.69 10.8 11 4 2 115.79 9.3 -11 4 -2 110.49 11.1 11 -4 -2 106.79 10.3 -11 -4 2 105.99 10.4 12 4 -2 16.7 4.7 -12 -4 -2 11.2 4.7 -12 4 2 15.1 5.9 12 -4 2 19.4 5.8 -12 4 -2 13.1 6.4 12 4 2 9.7 5 -12 -4 2 7.6 5.3 12 -4 -2 13.8 5.6 -12 4 -2 7.8 5.5 -13 -4 -2 16.8 5.5 -13 4 2 15 6.7 13 -4 2 21.1 6.6 13 4 -2 18.4 5.5 13 4 2 24.3 5.9 13 -4 -2 16.1 6.5 -13 4 -2 20.4 7.1 -13 4 -2 15.7 6.6 -14 4 2 16.6 7.8 14 -4 2 -7.4 6.7 14 4 -2 4.3 5.5 -14 -4 -2 18 5.9 -14 4 -2 10.8 7.3 -14 4 -2 -6.7 6.6 14 -4 -2 9.5 6.8 14 4 2 0.5 6 15 4 -2 35.3 7.2 15 -4 2 27.9 9.5 -15 4 2 20.8 14.3 -15 4 2 37.6 9.5 -15 -4 2 32.4 7.9 15 4 2 32.1 7.8 -15 4 -2 36.7 10.5 15 -4 -2 14.4 11.8 16 -4 2 5.7 8.5 16 4 -2 3 7 -16 4 2 -2.9 9.5 16 4 2 -0.3 7.3 16 -4 -2 -4.7 8 -16 4 -2 1.2 8.6 17 4 -2 6.8 7.9 17 -4 2 -5.8 8.6 -17 4 2 6 9.9 -17 4 -2 -3.5 9.1 17 -4 -2 5.7 8.8 17 4 2 8.7 7.8 18 -4 2 -2 10.1 -18 4 2 -1.2 11.3 18 4 2 5.8 7.7 -18 4 -2 -20.2 10.6 18 -4 -2 2.4 10.5 0 5 2 1535.45 97.19 0 5 2 1515.35 88.19 0 -5 2 1540.55 97.69 0 -5 -2 1532.85 97.09 0 -5 2 1485.05 96.89 0 5 -2 1572.84 88.19 0 -5 2 1564.84 87.99 0 5 2 1467.55 88.29 0 -5 2 1543.15 88.59 0 5 -2 1527.95 88.59 0 -5 -2 1549.24 88.39 1 -5 2 2012.4 112.09 -1 -5 -2 1999.1 120.09 -1 5 2 2027.3 121.89 -1 5 2 1961.6 111.99 1 5 -2 1981 111.69 1 5 -2 1911.71 112.09 1 -5 2 1980.5 121.49 1 -5 2 2011.9 122.09 -1 -5 -2 1964.8 111.79 -1 5 2 1922.41 111.79 1 -5 2 1992.8 111.59 1 -5 -2 1924.41 121.39 1 5 2 1858.11 119.49 -1 -5 2 1989.3 120.19 -1 -5 2 1869.41 120.29 1 5 2 1966 111.49 1 5 2 1860.01 111.79 -1 5 -2 1840.22 112.09 -1 -5 2 1909.41 111.99 1 -5 -2 1927.31 111.99 -1 5 -2 1869.31 111.79 2 -5 2 1970.1 109.59 2 -5 2 2025.5 120.69 2 5 -2 1988.7 109.59 2 -5 2 1975.1 120.49 -2 -5 -2 2026.3 117.29 -2 5 2 1989.9 109.99 2 -5 2 1916.51 109.99 -2 5 2 2105.49 121.39 -2 -5 -2 1943.41 109.59 2 5 -2 1938.91 109.99 2 5 2 1758.62 116.39 -2 -5 2 1895.11 117.69 -2 5 -2 1763.82 109.99 -2 -5 2 1829.12 109.89 2 5 2 1786.72 109.59 -2 5 -2 1821.02 109.69 2 -5 -2 1787.02 109.89 2 -5 -2 1832.72 119.79 -2 -5 2 1861.81 117.19 -3 -5 -2 2958 167.48 -3 5 2 2756.52 160.88 3 5 -2 2826.32 160.58 -3 5 2 2794.42 161.28 3 5 -2 2813.52 160.78 -3 -5 -2 2654.53 160.68 3 -5 2 2961.4 173.08 -3 5 2 2893.01 172.88 3 -5 2 2861.51 172.48 3 -5 2 2622.74 161.08 3 5 2 2701.53 166.98 -3 5 -2 2768.42 161.28 -3 5 -2 2679.93 160.98 3 -5 -2 2638.64 160.88 -3 -5 2 2711.93 161.08 3 -5 -2 2913.31 172.58 3 5 2 2790.92 160.78 -3 -5 2 2864.11 168.08 -3 -5 2 2993.7 168.68 -4 5 2 408.46 37.1 4 5 -2 394.66 23.5 -4 -5 -2 388.86 23.6 -4 5 2 385.96 24.3 4 -5 2 401.76 23.8 4 -5 2 371.06 35.8 -4 5 2 390.76 23.8 4 -5 2 400.56 23.8 -4 -5 -2 406.36 23.4 -4 -5 -2 372.16 28.8 4 -5 2 340.27 35.2 4 5 2 419.76 29.7 -4 5 -2 420.16 24.1 4 -5 -2 425.06 23.9 4 5 2 421.36 23.7 -4 -5 2 436.36 31.1 4 -5 -2 387.66 36.5 -4 -5 2 426.76 31.1 -4 5 -2 423.46 24.3 5 -5 2 65.19 19.8 -5 5 2 108.99 28 -5 -5 2 49.8 12.3 -5 5 -2 43.9 5.1 5 5 2 43.7 3.7 -5 5 -2 41.2 4.5 -5 -5 2 25.2 8.7 5 -5 -2 47.5 4.3 6 -5 2 188.58 11.4 6 5 -2 198.68 11.4 6 -5 2 190.38 28.6 -6 5 2 196.48 12.8 -6 5 2 192.08 11.6 -6 5 2 274.87 32.7 -6 -5 -2 182.28 11.5 6 -5 2 185.88 12 6 -5 2 170.38 28.6 6 -5 -2 171.48 11.9 -6 -5 2 167.48 16 -6 5 -2 171.88 12.2 6 5 2 179.88 11.6 -6 5 -2 181.38 12.6 6 -5 -2 187.08 29.5 -7 -5 -2 269.17 17.2 -7 5 2 254.97 18.2 7 5 -2 261.47 17 7 -5 2 260.27 35.2 7 -5 2 251.37 16.7 7 -5 2 212.48 34.2 -7 5 2 240.48 36.7 -7 5 2 248.58 17 7 -5 2 263.67 17.6 -7 5 -2 331.17 18.4 7 -5 -2 335.47 37.6 -7 5 -2 325.27 18.1 7 -5 -2 326.97 17.8 -7 -5 2 312.57 16.6 -8 -5 -2 310.97 18.8 8 -5 2 272.67 38.4 8 -5 2 300.27 17.8 -8 5 2 296.77 20 8 -5 2 263.97 38.4 -8 5 2 307.77 18.6 -8 5 2 298.97 42.3 8 5 -2 319.87 18.6 8 -5 2 300.17 19.2 -8 5 -2 300.67 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-2 5 453.85 26.3 -3 2 5 465.95 36.9 3 -2 5 463.65 26.4 -3 2 5 440.86 26.3 3 -2 5 408.86 35.4 -3 -2 -5 473.35 33.7 -3 -2 5 427.06 26.2 3 2 5 453.35 26.4 -3 -2 5 461.95 34.9 -3 2 -5 397.06 35.3 3 2 5 447.06 26.1 -3 2 -5 443.76 26.5 3 -2 -5 442.66 36 3 2 5 424.96 33.3 -3 2 -5 460.75 26.6 4 2 -5 2038.8 122.69 4 -2 5 1947.21 114.59 -4 -2 -5 1893.21 114.39 4 2 -5 1961.8 114.69 4 -2 5 1980.5 124.39 -4 -2 -5 1957.3 120.89 -4 2 5 2090.89 125.69 4 2 -5 1980 114.29 4 -2 5 1946.81 114.49 4 -2 5 1795.72 114.39 -4 2 5 1903.71 114.39 -4 -2 -5 2026.3 114.19 4 2 5 1968.2 121.09 -4 -2 5 2141.69 123.29 4 -2 -5 1981.8 114.49 -4 -2 5 1998.5 114.29 4 2 5 2028.8 114.49 -4 2 -5 2037.7 114.69 -4 2 -5 2080.29 124.89 -4 2 -5 2002.6 114.59 -5 2 5 2508.65 150.28 5 -2 5 2517.85 149.39 -5 -2 -5 2721.23 156.18 5 -2 5 2569.74 149.79 5 2 -5 2683.43 157.88 -5 -2 -5 2624.44 149.69 5 2 -5 2598.74 149.59 -5 2 5 2711.93 161.48 -5 -2 -5 2611.84 149.39 -5 2 5 2568.94 149.59 5 2 5 2512.75 149.69 5 -2 -5 2490.85 149.69 -5 2 -5 2527.45 149.88 5 -2 -5 2729.83 161.48 -5 -2 5 2788.22 158.38 -5 2 -5 2671.33 149.88 5 2 5 2707.33 156.98 -5 2 -5 2306.07 163.58 -5 -2 5 2534.85 149.49 -6 -2 -5 594.84 33 6 2 -5 574.44 33.1 6 -2 5 565.74 44.6 -6 2 5 586.74 46.8 -6 -2 -5 560.34 33.2 -6 2 5 587.34 33.2 -6 2 5 594.04 34.1 6 -2 5 582.94 32.6 -6 -2 -5 510.65 39.1 6 2 -5 561.64 42 6 -2 5 554.64 33.4 6 -2 5 588.74 46.6 6 -2 -5 549.95 33.3 6 2 5 524.05 33.2 -6 -2 5 551.24 42.4 6 2 5 555.44 39.2 -6 -2 5 556.44 32.9 -6 2 -5 533.65 33.5 6 -2 -5 574.74 45.7 -6 2 -5 586.84 33.5 -7 2 5 379.46 38.5 -7 -2 -5 352.36 21.9 7 -2 5 353.96 35.8 7 2 -5 331.47 30.9 7 -2 5 331.57 22.3 -7 2 5 333.17 23.1 -7 2 5 349.96 21.9 -7 -2 -5 355.46 22.1 7 2 -5 342.37 22 7 -2 5 320.87 35.5 7 2 5 388.36 22.4 7 2 5 392.76 28.5 -7 -2 5 392.36 32.5 7 2 5 407.16 27.6 -7 -2 5 398.46 21.7 -7 2 -5 390.66 22.6 -7 2 -5 380.56 23.2 7 -2 -5 410.96 37.1 7 -2 -5 400.56 22.4 -8 -2 -5 92.69 7 -8 2 5 46.3 19.7 8 -2 5 98.19 8.1 -8 2 5 102.59 9.3 8 -2 5 97.19 24.9 8 -2 5 79.79 25.2 8 2 -5 86.99 18.6 -8 -2 -5 97.39 7.6 8 2 -5 97.09 7.3 -8 2 5 95.79 7.1 8 2 5 96.39 8 8 -2 -5 106.59 26 -8 2 -5 108.69 8.1 -8 -2 5 85.89 22 -8 2 -5 95.79 8.3 8 -2 -5 104.39 7.9 -8 -2 5 94.69 6.6 -9 -2 -5 420.76 23.6 -9 2 5 392.06 47.2 -9 -2 -5 403.76 23.8 9 2 -5 414.06 23.7 -9 2 5 408.96 23.3 9 -2 5 415.96 24.2 -9 2 5 377.66 25.1 9 2 -5 385.06 31.1 9 -2 5 391.36 38.8 -9 2 -5 372.76 24 -9 -2 5 373.06 25 9 -2 -5 351.56 41.1 -9 2 -5 370.76 24.1 -9 -2 5 366.36 33.8 9 -2 -5 355.86 23.9 9 2 5 363.66 24 -10 -2 -5 327.77 20 -10 2 5 317.37 45.9 -10 -2 -5 339.87 20.4 10 -2 5 339.47 21 -10 2 5 327.57 22 10 -2 5 343.87 38.2 10 2 -5 345.27 20.3 -10 2 5 330.57 19.7 -10 2 -5 314.37 20.7 -10 2 -5 301.37 20.9 10 -2 -5 294.97 20.7 -10 -2 5 296.37 21.7 10 2 5 304.87 20.5 10 -2 -5 278.67 39.8 11 2 -5 264.57 16.8 -11 -2 -5 264.17 17.1 11 -2 5 241.28 17.5 -11 2 5 259.27 18.8 -11 -2 -5 236.68 16.2 11 -2 5 196.48 31.6 -11 2 -5 260.97 17.5 -11 2 -5 238.08 17.2 11 2 5 249.68 17.2 -11 -2 5 239.68 18.5 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21.6 0 3 5 215.58 12.5 -1 3 5 293.27 27.3 -1 -3 -5 247.38 25.1 1 -3 5 288.87 17.5 1 -3 5 287.07 17.3 1 3 -5 285.67 17.6 1 3 -5 254.47 25.7 -1 3 5 279.87 17.6 1 -3 5 260.27 26.6 1 -3 5 283.87 17.8 -1 -3 -5 295.27 17.4 1 -3 -5 304.67 17.6 1 3 5 307.87 17.3 -1 -3 5 315.47 27.1 -1 3 -5 310.77 17.9 1 3 5 317.77 17.4 -1 -3 5 311.47 17.5 1 -3 -5 287.67 26.9 -1 3 -5 305.57 27.4 1 3 5 301.87 26.6 -1 3 -5 332.57 17.7 2 3 -5 356.36 19.4 -2 3 5 339.97 19.6 -2 3 5 327.57 29.7 2 -3 5 331.87 19.3 2 -3 5 301.37 29.1 2 3 -5 355.46 18.9 -2 3 5 344.07 19.3 2 -3 5 349.57 19.1 -2 -3 -5 356.66 19.1 -2 -3 -5 332.27 27.4 2 -3 5 347.07 19.5 -2 3 -5 246.68 28.1 -2 -3 5 243.28 27.1 2 -3 -5 254.17 28 -2 -3 5 257.57 19.1 3 -3 5 1497.85 93.09 -3 3 5 1541.25 93.29 3 -3 5 1505.75 92.89 -3 -3 -5 1466.05 92.69 -3 -3 -5 1498.95 99.69 3 3 -5 1547.75 92.69 3 3 -5 1545.55 100.99 -3 3 5 1569.14 103.79 3 -3 5 1503.45 92.79 3 -3 5 1500.55 102.89 3 3 -5 1512.75 93.09 -3 3 -5 1695.43 104.09 -3 -3 5 1772.62 102.39 3 -3 -5 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2 -6 54.19 12 14 2 6 64.79 11.2 14 -2 -6 68.79 11.2 -14 -2 6 53.79 10.4 15 2 -6 9.8 6.5 15 -2 6 18 8 -15 -2 -6 19.3 8.8 15 2 6 10.9 7.6 -15 -2 6 5.5 8.9 -15 2 -6 17.2 8.2 16 2 -6 12.4 7 16 -2 6 2.8 8.3 16 -2 -6 8.3 7.8 16 2 6 5.5 8 -16 2 -6 11.1 8.9 17 2 -6 8.5 7.5 -17 2 6 15 10.5 17 -2 6 7.3 9.1 17 -2 -6 7.4 8.2 -17 2 -6 9.4 9.5 17 2 6 0 8.2 0 -3 -6 138.99 18.7 0 3 -6 123.49 7.9 0 3 -6 119.89 8.3 0 -3 6 123.29 18.8 0 3 6 122.69 19.1 0 -3 -6 124.59 7.7 0 3 -6 119.29 18.8 0 3 6 129.29 7.7 0 -3 6 119.19 8.1 1 3 -6 379.66 23.9 1 -3 6 343.57 34.2 -1 -3 -6 349.96 32.7 -1 3 6 377.46 23.7 -1 3 6 385.56 23.9 1 -3 6 395.46 23.5 -1 -3 -6 373.16 23.6 1 3 -6 391.56 33.8 1 -3 6 367.56 24 1 -3 6 384.26 23.8 1 -3 -6 421.46 35.1 1 -3 -6 432.56 23.9 -1 -3 6 444.46 34.4 1 3 6 445.06 23.6 1 3 6 430.56 23.7 -1 -3 6 430.46 23.8 -1 3 -6 434.16 24.2 -1 3 -6 435.66 23.9 -1 3 -6 428.86 35.7 1 3 6 421.56 33.9 2 -3 6 1902.31 113.89 -2 3 6 1990.2 125.79 2 -3 6 1981.2 125.49 2 -3 6 1971.3 114.29 2 -3 6 1936.61 114.09 -2 -3 -6 1961.3 113.99 -2 -3 -6 1999.7 123.39 2 3 -6 1995.8 114.29 -2 3 6 1939.81 114.09 2 3 -6 2030.7 124.29 -2 3 6 1921.31 114.39 2 -3 -6 2007.4 125.69 -2 3 -6 2032.8 125.79 -2 3 -6 1951.2 114.19 2 -3 -6 2007.2 114.29 -2 -3 6 2014.4 114.09 2 3 6 1919.81 113.99 -2 -3 6 2053.29 124.59 -2 3 -6 2020.7 114.39 2 3 6 1985.1 123.59 -3 3 6 153.28 10.6 3 3 -6 152.88 10.3 3 -3 6 152.88 10.6 3 -3 6 156.28 10 3 3 -6 161.38 9.7 -3 -3 -6 161.18 20 -3 3 6 147.09 23 3 -3 6 148.99 22.7 3 3 -6 176.98 21.5 -3 -3 -6 148.69 9.8 -3 3 6 156.28 10.1 3 -3 6 150.28 10 -3 -3 6 208.58 22.7 -3 3 -6 186.08 24 -3 3 -6 201.58 10.4 3 -3 -6 215.98 24.8 3 3 6 200.68 20.7 4 3 -6 894.61 55.09 4 3 -6 921.11 54.59 -4 3 6 927.51 54.79 4 -3 6 817.32 66.19 -4 3 6 944.71 68.29 4 -3 6 910.01 54.69 4 -3 6 926.41 54.79 4 3 -6 909.01 64.49 -4 -3 -6 885.31 62.99 -4 -3 -6 933.61 54.69 4 3 6 979.2 54.89 -4 -3 6 967.3 54.69 4 -3 -6 917.61 54.89 4 -3 -6 983 68.39 4 3 6 987.2 54.39 -4 3 -6 980.3 55.09 -4 3 -6 1026 55.19 -4 -3 6 1040.6 66.19 -4 3 -6 957.8 67.69 4 3 6 962.3 63.69 5 3 -6 1714.73 101.09 5 3 -6 1737.73 100.49 -5 3 6 1722.13 100.69 5 -3 6 1665.73 100.49 -5 -3 -6 1721.23 108.69 -5 3 6 1703.83 101.39 -5 3 6 1806.62 115.59 5 -3 6 1748.63 100.79 -5 -3 -6 1745.43 100.59 5 -3 6 1729.73 113.89 5 3 -6 1718.43 110.49 -5 3 -6 1852.51 101.09 -5 3 -6 1732.63 114.29 5 -3 -6 1745.23 100.89 5 3 6 1762.52 108.69 -5 3 -6 1775.92 100.99 -5 -3 6 1761.82 111.19 5 3 6 1732.93 100.79 -5 -3 6 1754.42 100.59 6 -3 6 276.07 35.3 6 3 -6 252.07 28.2 -6 -3 -6 297.07 26.9 -6 3 6 282.97 17.1 6 -3 6 281.27 16.7 -6 3 6 275.17 18.3 -6 -3 -6 300.07 16.6 -6 3 6 312.77 35.4 -6 -3 -6 288.77 17.1 6 -3 6 241.28 32.2 6 -3 6 283.27 17.4 6 3 -6 293.97 17 6 3 6 284.97 17.3 6 -3 -6 270.37 33.3 -6 -3 6 253.07 29.5 -6 3 -6 287.07 17.7 6 -3 -6 277.47 17.4 6 3 6 266.37 26 -6 -3 6 272.67 16.9 -7 3 6 802.42 65.09 7 -3 6 857.71 64.29 -7 -3 -6 762.42 53.19 7 -3 6 772.92 47 -7 3 6 757.02 47.8 -7 3 6 785.72 46.7 7 3 -6 758.82 56.29 -7 -3 -6 786.52 46.7 7 -3 6 696.13 61.39 7 3 -6 772.82 46.6 -7 -3 -6 783.02 46.6 -7 -3 6 869.11 58.69 7 3 6 837.62 53.49 -7 3 -6 786.62 47.2 7 3 6 813.02 47 -7 3 -6 852.81 47.3 -7 -3 6 835.02 46.5 7 -3 -6 814.32 47 7 -3 -6 867.51 64.39 -8 3 6 543.25 52.59 8 3 -6 474.25 42.2 8 -3 6 455.75 46.7 -8 -3 -6 524.85 29.6 -8 3 6 468.25 31.3 -8 -3 -6 509.95 30 -8 3 6 511.65 29.9 8 -3 6 496.25 30.4 8 -3 6 481.45 48.9 8 3 -6 501.35 29.9 -8 -3 6 466.35 42.7 -8 3 -6 502.95 30.5 8 -3 -6 501.55 30.4 8 3 6 524.55 30.3 -8 3 -6 539.95 30.6 8 -3 -6 472.15 48.9 -8 -3 6 502.15 29.6 -9 -3 -6 630.84 37.4 -9 3 6 625.04 37.2 9 -3 6 648.44 58.99 9 -3 6 586.84 38.5 -9 -3 -6 651.83 37 9 3 -6 665.53 47.1 -9 3 6 590.64 38.7 9 3 -6 617.04 37.3 -9 3 6 569.74 61.59 -9 -3 6 685.33 48.7 9 -3 -6 644.64 37.8 9 -3 -6 615.84 56.99 9 3 6 627.94 39.4 -9 3 -6 636.74 38 -9 3 -6 630.54 38 10 -3 6 96.99 9.3 -10 3 6 94.69 7.9 -10 -3 -6 98.69 7.4 -10 -3 -6 85.49 8.3 -10 3 6 87.09 11 10 3 -6 94.79 8.2 -10 -3 6 89.69 10.9 -10 3 -6 88.59 9.2 10 3 6 87.39 9.3 10 -3 -6 87.09 9.2 -10 3 -6 86.49 9.3 -11 -3 -6 120.79 9.8 11 -3 6 100.49 10.8 -11 3 6 80.29 16.2 11 3 -6 107.89 9.5 11 -3 -6 105.99 10.5 -11 -3 6 97.69 12 -11 3 -6 98.99 10.6 11 3 6 110.09 10.4 -11 3 -6 113.39 10.6 12 3 -6 110.29 9.7 -12 -3 -6 108.29 9.9 12 -3 6 109.99 11.3 -12 3 6 104.09 13.2 -12 3 -6 70.59 10.4 12 3 6 85.29 10.4 -12 3 -6 76.69 11.2 12 -3 -6 76.19 10.9 -12 -3 6 80.29 12.5 -13 -3 -6 3.5 5.2 13 -3 6 5.2 6.2 13 3 -6 1 4.8 -13 3 6 -2.3 6.9 -13 3 -6 4.2 6.6 13 3 6 5.8 6.2 13 -3 -6 -3.5 5.8 -13 -3 6 6.7 6.9 -14 3 6 20.9 8.5 14 3 -6 24.8 6.2 -14 -3 -6 39.7 10.2 14 -3 6 29.2 7.8 14 -3 -6 22.8 7.1 -14 3 -6 25.4 8.1 -14 -3 6 55.29 14.4 14 3 6 20.8 7.2 15 3 -6 1.5 6 15 -3 6 5 7.7 -15 -3 6 3.6 9 15 -3 -6 -1 7.1 15 3 6 8 7.3 16 -3 6 4 8.4 16 3 -6 3.1 6.7 16 3 6 3.6 7.9 16 -3 -6 5.3 7.9 -16 3 -6 21.6 9.1 -17 3 6 15.2 11.1 17 -3 6 2.3 9.1 -17 3 -6 22.8 10 17 -3 -6 -7 8.3 17 3 6 5.9 8 0 4 -6 270.27 28.1 0 4 6 269.17 16.2 0 4 -6 267.67 16.2 0 -4 -6 269.37 16 0 -4 -6 263.47 27.5 0 4 6 267.77 28.1 0 -4 6 246.08 27.3 0 -4 6 283.17 16.2 0 4 6 265.87 16 0 4 -6 270.97 16.6 1 -4 6 1132.49 62.29 -1 4 6 1147.09 75.29 1 4 -6 1148.59 62.39 -1 -4 -6 1138.59 73.49 -1 4 6 1086.99 62.39 1 -4 6 1143.29 61.99 1 4 -6 1109.09 73.89 -1 -4 -6 1165.68 62.09 1 4 -6 1104.79 62.79 1 -4 6 1033.5 73.89 -1 4 6 1104.29 62.19 -1 4 -6 1029.2 62.59 1 4 6 1008.3 72.69 1 4 6 1026 62.09 1 -4 -6 1004.7 62.29 -1 4 -6 983.6 73.59 -1 4 -6 1044.8 62.39 -1 -4 6 1013.4 73.29 1 4 6 1002.9 61.99 -1 -4 6 1040.8 62.19 -2 4 6 164.08 24.3 2 -4 6 158.48 10.4 2 4 -6 167.08 10.9 2 -4 6 164.48 10.7 2 -4 6 155.58 24.2 -2 -4 -6 167.48 10.4 -2 -4 -6 162.38 20.7 2 4 -6 178.68 22.7 2 4 -6 169.58 10.1 -2 4 6 156.38 11 -2 -4 6 155.28 11.2 -2 4 -6 196.28 11.3 -2 4 -6 194.68 11 2 4 6 198.88 10.5 -2 4 -6 172.78 24.5 2 -4 -6 211.58 24.9 -2 -4 6 189.28 23.1 2 4 6 195.28 22.1 -3 -4 -6 49.5 3.4 -3 4 6 44.3 3.9 3 -4 6 44.5 3.9 -3 4 6 40.1 14.8 3 -4 6 47 3.7 3 4 -6 44.3 4.2 3 4 -6 48.6 3.1 -3 -4 -6 58.69 15.8 3 4 -6 62.09 16.6 -3 4 6 37.5 4.7 3 -4 6 38.3 13 3 -4 -6 49.8 14.4 -3 4 -6 42 4.1 -3 -4 6 65.09 17.5 3 4 6 44.4 3.3 3 4 6 47.3 14.7 3 4 6 48.5 3.9 -3 -4 6 46.1 3.8 -3 4 -6 45.2 4.6 -3 4 -6 37.5 12.2 -4 -4 -6 780.62 44.5 4 4 -6 802.12 44.4 4 -4 6 775.52 44.7 -4 4 6 751.62 59.09 -4 4 6 753.22 45.3 -4 4 6 784.12 44.7 4 4 -6 807.02 56.09 4 4 -6 766.32 45 4 -4 6 751.72 58.99 4 -4 6 747.23 44.7 4 -4 -6 792.82 59.49 -4 4 -6 732.53 58.99 -4 -4 6 808.22 56.59 4 4 6 722.03 54.99 4 4 6 768.12 44.2 -4 4 -6 774.52 45.1 4 -4 -6 761.62 44.8 4 4 6 761.92 44.7 -4 4 -6 758.12 45 -4 -4 6 732.83 44.6 -5 -4 -6 282.97 25.3 -5 4 6 268.17 15.3 5 -4 6 250.87 32 5 -4 6 270.77 15.4 -5 4 6 256.27 32.7 5 4 -6 261.77 15.7 -5 -4 -6 260.87 15 -5 4 6 258.17 16.3 5 4 -6 263.47 14.9 5 4 -6 236.28 26.9 5 -4 6 259.87 15 5 -4 -6 230.98 15.4 -5 -4 6 230.48 15 -5 4 -6 217.38 15.5 5 4 6 195.78 24.8 -5 -4 6 219.28 28.2 5 4 6 235.88 15.3 6 -4 6 1055.59 60.49 6 -4 6 982.1 76.69 -6 -4 -6 1002.6 67.79 -6 4 6 1014.8 61.19 6 4 -6 1023.7 60.09 -6 -4 -6 1003.3 60.09 6 -4 6 1063.39 77.09 6 4 -6 1036.2 70.79 -6 4 6 1052.19 78.89 -6 4 6 1013.1 60.29 6 -4 6 1004.1 59.99 -6 4 -6 1032.6 60.69 -6 -4 6 1077.99 71.69 -6 -4 6 1055.39 60.09 6 4 6 1028.9 67.99 6 -4 -6 1092.19 77.39 6 -4 -6 1049.89 60.49 6 4 6 1039.1 60.39 -6 4 -6 1086.79 60.79 7 4 -6 311.87 32.5 -7 4 6 353.86 20.7 7 -4 6 346.87 42.3 7 -4 6 372.66 40.2 -7 -4 -6 361.16 28.5 -7 -4 -6 354.06 19.9 7 -4 6 348.97 21 7 -4 6 340.97 20.1 -7 4 6 330.27 21.9 -7 -4 -6 346.77 20.5 7 4 -6 355.36 20.4 -7 4 6 350.86 44.2 -7 -4 6 297.07 33.4 -7 4 -6 338.77 21.3 -7 4 -6 324.27 21.2 -7 -4 6 335.97 20.3 7 -4 -6 331.17 21 7 4 6 318.77 28 7 4 6 336.67 20.9 7 -4 -6 335.47 41.4 8 4 -6 17.2 13 8 -4 6 9.3 18.7 -8 4 6 -14.6 20.2 -8 -4 -6 21.5 2.8 -8 4 6 23.9 4.3 8 -4 6 15.1 3.6 8 -4 6 37.6 19 -8 -4 -6 21.9 4.1 -8 4 6 15.9 4.7 8 4 -6 18.3 4.4 -8 4 -6 15 4 -8 -4 6 21.5 14.6 -8 -4 6 13.5 3.3 8 -4 -6 7.9 18.2 -8 4 -6 7.1 3.5 8 4 6 8.8 3.4 8 -4 -6 11.6 3.8 -9 4 6 43.7 27.5 9 4 -6 7.6 3 9 -4 6 13 4.2 9 4 -6 14 12.5 -9 4 6 8.8 4.8 -9 4 6 10.4 3.1 9 -4 6 18.1 23.8 -9 -4 -6 12.2 3.3 -9 -4 -6 17 3.3 9 -4 -6 18.1 4.9 -9 -4 6 70.09 22.1 9 -4 -6 -2.5 21.3 -9 4 -6 9.9 4 -10 4 6 251.77 16 -10 -4 -6 265.77 16.2 10 -4 6 259.97 17.1 -10 4 6 262.17 18.6 10 4 -6 253.47 16 10 -4 -6 229.78 16.9 -10 -4 6 230.18 18.2 -10 4 -6 228.88 17.1 10 4 6 249.78 16.9 -10 4 -6 232.98 17.1 11 4 -6 111.59 9.5 -11 -4 -6 108.49 9.6 -11 4 6 109.19 12.9 -11 4 6 118.19 9.5 11 -4 6 97.49 10.9 11 4 6 112.29 10.5 -11 4 -6 109.79 11.5 11 -4 -6 124.59 10.9 -11 4 -6 98.39 10.9 -11 -4 6 116.39 12.8 12 -4 6 21.5 6.1 12 4 -6 19.9 5 -12 4 6 17.5 6.9 -12 -4 -6 32.2 7.4 12 4 6 26.7 6.1 12 -4 -6 21.2 6.3 -12 -4 6 16.1 6.6 -12 4 -6 17.1 6.3 -12 4 -6 29.1 6.2 13 -4 6 6.8 6.6 -13 4 6 17.9 7.9 13 4 -6 9.5 5.1 -13 -4 -6 12.4 6.9 13 4 6 17.1 6.3 13 -4 -6 14.6 6.4 -13 -4 6 17.7 7.4 -13 4 -6 18 7.4 -13 4 -6 10.4 6.3 14 4 -6 -3 5.1 14 -4 6 -3.3 6.7 -14 4 6 0.3 8.1 -14 4 -6 -1.3 7.4 14 -4 -6 5.3 6.6 14 4 6 1 6.2 -14 -4 6 -9.1 7.7 15 -4 6 9.1 7.9 15 4 -6 -0.9 5.7 -15 4 -6 6 8.3 15 -4 -6 6.5 7.4 15 4 6 8.6 7.1 16 -4 6 17.2 8.8 16 4 6 21.9 8.1 -16 4 -6 23.5 9.5 16 -4 -6 6.9 8 17 -4 6 2.3 9.1 -17 4 6 15.4 11.4 -17 4 -6 8.9 9.8 17 4 6 9.5 8.3 17 -4 -6 -3.2 8.5 0 -5 6 1558.84 101.79 0 5 -6 1527.85 88.69 0 -5 -6 1506.65 100.79 0 -5 6 1534.65 88.59 0 5 -6 1550.04 89.09 0 5 6 1526.55 88.49 0 5 -6 1544.95 101.69 0 5 6 1493.35 88.49 0 -5 -6 1577.84 88.49 0 5 6 1555.54 101.59 0 -5 6 1498.15 88.09 1 5 -6 1891.31 112.99 -1 5 6 1966.6 126.39 -1 -5 -6 1871.21 123.79 -1 5 6 1952.2 112.89 -1 5 6 1933.21 112.99 1 -5 6 1959.4 112.49 1 5 -6 2027.1 125.89 1 5 -6 1948.11 113.39 1 -5 6 1917.51 125.99 1 -5 6 1929.71 112.89 -1 -5 -6 1977.3 112.69 -1 5 -6 1970.2 112.99 -1 -5 6 1939.61 112.89 -1 5 -6 1983.2 113.39 1 5 6 1961.5 112.79 -1 5 -6 2077.59 127.19 1 5 6 1897.41 112.59 1 -5 -6 1985.2 126.29 1 5 6 2000.1 124.99 -1 -5 6 1974.2 125.59 2 -5 6 560.14 32.1 -2 -5 -6 527.95 43.2 2 -5 6 570.34 31.8 2 -5 6 531.85 46.1 -2 5 6 548.05 47 2 5 -6 571.94 32.2 2 5 -6 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54.69 -6 3 9 937.01 76.39 6 -3 9 915.31 53.79 6 3 -9 925.11 54.39 -6 -3 9 896.61 71.79 6 3 9 876.31 67.49 6 -3 -9 909.11 53.79 -6 3 -9 970.1 73.99 -6 -3 9 944.41 53.59 -6 3 -9 873.11 53.99 -6 3 -9 945.51 54.09 6 3 9 885.61 53.79 -7 3 9 874.41 49.6 7 -3 9 851.51 49.7 7 -3 9 882.31 71.49 7 3 -9 800.32 66.29 -7 -3 -9 766.22 63.89 -7 3 9 947.41 75.39 -7 -3 -9 852.81 49.4 7 3 -9 867.11 49.3 7 -3 9 846.92 48.9 -7 3 9 833.12 50.69 -7 3 -9 830.62 49.9 -7 -3 9 839.92 49.3 7 3 9 806.42 62.69 -7 3 -9 863.31 49.9 -7 -3 9 834.42 69.49 7 -3 -9 857.21 49.7 7 3 9 834.22 49.7 7 -3 -9 738.33 70.29 8 -3 9 61.29 7.5 -8 3 9 46.4 29.8 8 -3 9 53.39 25.8 8 3 -9 42.1 20.5 -8 3 9 75.49 6.9 -8 -3 -9 63.09 6.6 -8 3 9 54.09 9.2 -8 -3 -9 45.2 18.1 8 3 -9 65.59 6.1 8 3 9 52.29 18.4 8 -3 -9 82.29 7.4 -8 3 -9 83.89 8 8 3 9 67.79 9.2 -8 3 -9 76.39 7.5 -8 -3 9 75.29 6.4 8 -3 -9 89.79 27.6 -8 -3 9 78.79 23.9 9 -3 9 478.45 28.9 -9 -3 -9 487.35 28.5 -9 3 9 457.65 30.3 9 3 -9 482.05 28.3 -9 3 9 493.85 28.5 -9 -3 9 378.66 54.19 -9 -3 9 468.55 28.1 -9 3 -9 449.06 29.1 9 3 9 450.95 28.8 9 -3 -9 461.45 28.8 -9 3 -9 468.15 28.9 -10 3 9 203.98 13.6 10 -3 9 194.88 14.4 10 3 -9 199.98 13.3 -10 -3 -9 191.48 13.7 -10 3 9 177.88 19.9 -10 -3 9 193.58 16.5 -10 3 -9 203.98 14.8 10 -3 -9 197.98 14.4 10 3 9 177.88 14.4 -10 3 -9 188.98 14.3 -11 -3 -9 22.8 5.2 11 -3 9 26.2 6.2 -11 3 9 25.5 4.7 -11 3 9 23.2 6.8 11 3 -9 28.4 6.8 -11 -3 9 31.9 7.5 11 3 9 37.6 8.7 -11 3 -9 31.1 6.5 11 -3 -9 23.7 5.7 -11 3 -9 31.5 8.2 -12 -3 -9 34.9 8.5 -12 3 9 49.8 13.3 12 3 -9 38.3 7.6 12 -3 9 55.09 10.3 -12 3 -9 62.49 10.7 12 3 9 49.99 9.4 -12 -3 9 50.89 12.9 12 -3 -9 51.59 9.9 -13 -3 -9 43.8 9.8 -13 3 9 38.7 9.4 13 -3 9 59.89 11 13 3 -9 43.6 8.7 13 -3 -9 52.69 10.8 -13 3 -9 57.29 11 -13 -3 9 65.09 14.5 13 3 9 63.19 11 14 3 -9 6.5 5.5 -14 3 -9 6.7 7.7 -14 -3 9 4.8 8.3 14 -3 -9 9.5 6.9 14 3 9 -8 7.7 15 -3 9 3.4 8.3 15 -3 -9 8.1 7.5 15 3 9 13.5 8.1 -15 3 -9 1.4 8.1 16 -3 9 -6.1 8.8 16 -3 -9 1.4 8 16 3 9 -0.2 8.1 -16 3 -9 -4.7 9 17 -3 9 20.4 9.6 17 3 9 4.3 8.3 -17 3 -9 32.4 10.5 17 -3 -9 9.2 8.5 0 4 -9 39.9 4.4 0 -4 -9 41.2 14.3 0 4 9 38.2 4 0 4 -9 36.3 5.9 0 4 -9 27.5 14.3 0 -4 9 72.29 18.7 0 -4 -9 36.4 4 0 4 9 42.2 3.8 0 4 9 50.29 17 0 -4 9 44 4.3 -1 4 9 24.3 3.5 -1 -4 -9 38.2 15.4 -1 4 9 29.1 3.6 1 4 -9 34.5 20 1 -4 9 23.1 3.5 -1 -4 -9 26.2 3.3 1 -4 9 23.6 13.7 -1 4 9 21.8 12.9 1 4 -9 32.8 4.1 1 -4 -9 -12.1 19.1 1 4 9 0.3 11.3 -1 4 -9 11.3 13.6 -1 -4 9 2.5 13.8 -2 4 9 543.45 32.1 -2 -4 -9 547.65 31.5 2 -4 9 518.05 31.7 -2 -4 -9 520.95 47.2 -2 4 9 558.54 51.19 2 4 -9 520.35 32 2 -4 9 563.04 50.89 2 4 -9 523.15 47.7 2 -4 9 539.85 31.3 -2 4 9 541.55 31.7 -2 4 -9 541.45 31.9 -2 4 -9 518.15 32.8 2 -4 -9 545.15 31.9 -2 -4 9 533.35 31.7 -2 -4 9 532.85 48.6 2 4 9 555.74 31.2 -2 4 -9 520.35 49.7 2 4 9 480.05 52.09 2 -4 -9 521.65 48.7 2 4 9 568.04 31.2 2 4 9 527.25 31.5 -3 -4 -9 385.56 24.6 -3 4 9 399.76 24.9 -3 -4 -9 389.56 39.5 3 4 -9 436.76 41.8 3 4 -9 383.86 24.2 3 -4 9 391.36 43.9 3 -4 9 385.16 24.8 3 4 -9 381.86 25.2 -3 4 9 359.36 43.8 3 -4 9 393.96 24.6 -3 4 9 386.46 25.3 3 4 9 489.95 24.6 3 -4 -9 491.75 45.4 3 4 9 452.15 41.2 -3 4 -9 503.05 46.3 -3 -4 9 500.95 44.2 -3 4 -9 490.85 25.3 4 4 -9 950.2 55.99 -4 4 9 1064.19 83.19 -4 4 9 952.4 56.29 4 4 -9 955.1 55.09 4 -4 9 969.5 55.39 -4 4 9 984.6 55.69 4 4 -9 872.71 70.49 4 -4 9 937.21 74.79 -4 -4 -9 980.7 55.39 -4 -4 -9 933.71 69.59 4 -4 9 917.31 55.49 4 4 9 933.61 69.79 4 4 9 941.71 55.09 -4 4 -9 950.8 55.89 -4 4 -9 990.5 56.09 -4 -4 9 932.01 55.49 -4 -4 9 1013.3 73.99 -4 4 -9 884.21 73.59 4 -4 -9 939.11 74.19 5 -4 9 96.89 8 -5 4 9 95.89 9.4 -5 4 9 98.09 8.3 5 -4 9 111.39 33.6 5 -4 9 95.89 7.9 -5 -4 -9 81.39 24.5 -5 4 9 108.39 32.5 5 4 -9 100.39 8.8 -5 -4 -9 96.59 7.6 5 4 -9 99.99 27.8 5 4 -9 98.29 7.2 -5 4 -9 167.08 33.8 5 4 9 143.19 28.2 5 4 9 127.69 8.3 5 -4 -9 163.08 33.4 -5 4 -9 138.29 9.1 -5 4 -9 132.19 8.9 -5 -4 9 140.59 30.9 5 -4 -9 134.69 8.5 5 4 9 129.69 7.5 -5 -4 9 133.99 8.1 6 -4 9 63.99 22.6 -6 4 9 71.59 23.2 6 4 -9 88.79 28.7 -6 4 9 89.69 9.1 6 4 -9 88.79 6.6 -6 -4 -9 97.19 7.1 6 -4 9 99.39 7.7 6 4 -9 87.99 8.5 -6 4 9 102.49 7.6 6 -4 9 83.39 8 6 -4 -9 96.29 7.8 6 -4 -9 105.99 34.3 -6 -4 9 98.49 7.2 6 4 9 99.79 7.6 6 4 9 121.79 27.9 -6 -4 9 88.89 23.3 -6 4 -9 103.89 8.4 -6 4 -9 102.19 8.3 -6 4 -9 129.49 35.4 -7 4 9 14.8 4.6 7 4 -9 16.2 3.5 7 -4 9 12 3.5 7 -4 9 21.2 23.4 -7 4 9 19.1 5 -7 -4 -9 27.5 16.3 7 -4 9 18.8 3.5 -7 4 9 63.99 26.9 7 4 -9 12.8 17.2 -7 -4 -9 18.3 3.1 7 -4 9 -8.5 20.3 -7 -4 9 25.1 21.3 7 4 9 44.5 17 7 -4 -9 69.99 23.1 -7 4 -9 34.1 5.9 -7 -4 9 25 4.4 8 -4 9 919.71 52.49 -8 4 9 885.51 54.69 -8 4 9 967.9 98.19 8 -4 9 872.71 55.19 8 4 -9 945.11 52.99 8 4 -9 914.21 71.09 -8 -4 -9 814.92 67.99 -8 -4 -9 919.41 53.19 -8 4 9 949.9 53.39 -8 -4 9 906.41 75.29 8 -4 -9 899.21 54.09 8 4 9 1036.6 80.19 -8 4 -9 890.51 53.79 8 4 9 861.71 53.49 -8 -4 9 899.31 53.09 9 -4 9 6.9 4.3 -9 -4 -9 9.3 3.5 9 4 -9 10.6 3 -9 4 9 7.2 5.6 -9 4 9 7.3 3.5 9 4 9 9.2 4.4 -9 4 -9 5.9 4.1 -9 -4 9 -2 25.2 -9 4 -9 4.2 4.5 9 -4 -9 13 4.4 -9 -4 9 11.5 3 -10 4 9 50.39 7.1 10 -4 9 51.69 8.2 -10 4 9 47.4 10.2 -10 -4 -9 52.69 6.8 10 4 -9 46.8 6.3 -10 4 -9 35.7 8.6 10 4 9 45 8 10 -4 -9 34.4 8.1 -10 4 -9 39.1 8.3 -11 4 9 100.69 9.6 11 4 -9 96.59 8.7 -11 4 9 110.29 13.5 -11 -4 -9 95.79 9.4 11 -4 9 95.29 10.8 -11 -4 9 96.99 13.2 11 -4 -9 62.99 10.6 11 4 9 84.79 10.5 -11 4 -9 79.79 11 -11 4 -9 77.79 10.5 -12 4 9 52.99 13.1 12 -4 9 54.29 10.3 -12 -4 -9 43.9 11 12 4 -9 48.9 7.4 -12 4 -9 26.5 7.3 -12 -4 9 13.5 7.8 12 -4 -9 20.9 6.5 12 4 9 24.8 6.6 -13 4 9 24.4 8.8 13 -4 9 23.6 7.3 13 4 -9 22.2 5.4 13 4 9 26.2 7.4 13 -4 -9 28.5 7.5 -13 4 -9 28 7.7 -13 -4 9 24.9 8.6 14 -4 9 15.7 8.4 -14 4 -9 13.5 8.1 14 -4 -9 20.9 7.5 -14 -4 9 18 8.8 15 -4 9 3.2 8.5 15 4 9 14.9 7.8 15 -4 -9 6.7 7.6 -15 4 -9 3.4 8.1 16 -4 9 7.5 9.2 16 -4 -9 1.2 8 -16 4 -9 10.2 9.7 16 4 9 -3.7 7.6 17 -4 9 9.1 9.9 -17 4 -9 2.1 10 17 -4 -9 16.9 8.6 17 4 9 -18.2 8.1 0 5 -9 1278.17 74.29 0 -5 9 1268.07 74.09 0 5 -9 1300.77 91.79 0 -5 9 1269.57 92.19 0 5 9 1251.27 91.29 0 -5 -9 1273.97 74.09 0 5 9 1251.77 73.99 0 -5 -9 1281.07 90.69 0 5 -9 1290.37 74.79 0 5 9 1296.37 73.99 -1 5 9 2052.39 112.89 1 5 -9 2097.69 130.79 -1 -5 -9 1937.81 112.59 -1 5 9 1908.51 112.69 -1 -5 -9 1977.9 128.79 1 -5 9 1935.41 112.29 1 -5 9 1963.5 112.79 -1 5 9 1930.11 130.69 1 5 -9 1938.81 112.99 1 -5 9 2012 131.19 -1 5 -9 1912.21 112.89 1 5 9 1912.41 112.39 1 5 9 1982.1 129.89 1 -5 -9 1907.11 112.79 -1 5 -9 1961.5 113.39 1 -5 -9 1903.31 129.59 -1 -5 9 1952.4 129.89 -1 -5 9 1941.51 112.79 1 5 9 1853.01 112.59 -1 5 -9 1991.2 130.79 2 -5 9 528.65 30.6 -2 5 9 489.75 50.59 -2 -5 -9 542.45 47.7 2 -5 9 516.85 31 2 -5 9 525.55 51.79 2 5 -9 571.44 49.3 -2 -5 -9 524.65 30.7 2 5 -9 499.85 31.2 -2 5 9 561.34 31.4 -2 5 9 521.95 31 -2 5 -9 522.55 31.6 -2 5 -9 484.85 49.5 2 5 9 552.44 30.4 2 5 9 510.55 30.3 2 5 9 510.35 30.7 -2 -5 9 516.05 49.3 2 -5 -9 518.25 31.2 2 -5 -9 556.94 50.79 -2 5 -9 518.15 31.2 2 5 9 488.75 47.7 -2 -5 9 518.65 31 3 5 -9 191.08 12.2 3 5 -9 195.38 10.7 -3 5 9 194.98 12.4 -3 5 9 178.98 11.7 -3 5 9 212.88 35.7 3 5 -9 183.48 29.6 -3 -5 -9 193.68 11.2 3 -5 9 193.38 11.2 3 -5 9 185.68 11.7 -3 -5 -9 207.48 30.5 3 -5 9 146.49 44.8 -3 5 -9 144.99 11.7 3 -5 -9 156.28 32.2 -3 5 -9 140.69 12.2 3 5 9 126.69 28.2 -3 -5 9 212.38 32.6 -3 5 -9 125.09 31.9 4 5 -9 447.26 25.6 4 -5 9 446.36 26.1 4 -5 9 442.86 26.3 4 5 -9 439.46 26.8 4 5 -9 486.05 44.5 -4 5 9 354.66 47.3 -4 -5 -9 436.36 26 -4 -5 -9 445.46 42.6 4 -5 9 471.35 49.9 -4 5 9 457.35 27.1 -4 5 9 462.75 26.5 -4 -5 9 421.76 46.6 4 5 9 431.46 25.8 -4 -5 9 436.26 26.3 4 5 9 403.06 43.2 -4 5 -9 422.06 26.7 -4 5 -9 431.06 27 4 -5 -9 469.95 48.3 -4 5 -9 426.66 48.2 5 -5 9 612.34 35.9 5 -5 9 618.84 35.9 -5 5 9 632.84 60.79 5 5 -9 612.94 36.6 -5 -5 -9 601.14 35.6 5 -5 9 664.43 60.79 -5 5 9 628.04 36.1 5 5 -9 617.94 35.4 -5 5 9 614.14 37 5 5 -9 612.24 53.99 -5 -5 9 637.64 56.59 -5 5 -9 542.75 58.19 5 -5 -9 577.84 36.1 -5 5 -9 600.24 36.6 5 5 9 592.54 36 -5 -5 9 602.84 35.9 5 5 9 635.34 52.49 -5 5 -9 596.64 36.4 5 -5 -9 598.94 58.29 6 -5 9 601.64 35.8 6 -5 9 621.34 62.79 6 5 -9 632.14 36.8 6 5 -9 600.44 35.5 6 -5 9 602.34 36 -6 5 9 557.64 60.79 -6 5 9 576.84 37.1 -6 5 9 604.54 36.1 -6 -5 -9 581.84 35.6 6 5 -9 600.24 54.99 6 5 9 641.34 52.59 6 -5 -9 624.74 61.19 -6 -5 9 640.74 58.29 6 5 9 619.34 36.1 -6 5 -9 624.94 36.7 6 -5 -9 613.74 36.3 -6 5 -9 576.64 36.4 -6 -5 9 638.04 35.9 -7 -5 -9 86.89 27.6 -7 5 9 87.99 7.9 7 5 -9 84.29 21.7 7 -5 9 56.99 26.1 7 5 -9 93.59 6.9 7 -5 9 93.19 8.2 -7 -5 -9 84.19 7.3 -7 5 9 166.18 51.89 7 -5 9 91.09 7.2 7 -5 9 83.09 25.1 -7 5 9 82.49 10.1 -7 5 -9 104.89 9.2 -7 -5 9 119.19 7.7 7 5 9 109.39 30.5 7 5 9 111.99 8.4 -7 -5 9 111.29 26.7 7 -5 -9 112.69 8.6 -7 5 -9 119.59 9.1 8 -5 9 107.89 12.7 8 5 -9 110.89 7.7 -8 -5 -9 107.39 8.1 8 -5 9 108.29 7.4 -8 5 9 124.39 9.1 -8 5 9 108.59 11.3 8 5 -9 150.88 36.9 8 5 9 95.09 9 -8 5 -9 104.69 9.9 -8 -5 9 96.79 8.3 -8 5 -9 102.89 9.8 8 -5 -9 103.89 9.4 -8 -5 9 121.59 28.8 -9 5 9 19.2 5.8 -9 5 9 19.4 4.2 -9 -5 -9 18.2 3.8 9 5 -9 27.6 4.6 9 -5 9 21.3 4.9 -9 5 -9 37.4 7.7 -9 5 -9 22.6 5.4 9 -5 -9 26.8 5.1 9 5 9 29.7 6.5 -10 5 9 128.89 10.9 -10 5 9 138.19 14 10 -5 9 127.59 11.5 -10 -5 -9 128.49 10.1 10 5 -9 136.09 9.7 -10 5 -9 121.29 12.2 10 -5 -9 130.19 12 10 5 9 140.49 11.4 -10 5 -9 127.39 12.2 -11 5 9 93.89 11.2 11 5 -9 97.89 10.5 11 -5 9 105.99 11.4 -11 5 9 134.59 14.2 -11 5 -9 115.29 12.2 11 -5 -9 112.19 11.5 11 5 9 114.09 11 -11 5 -9 107.69 12.1 -11 -5 9 122.09 14.5 12 -5 9 76.49 10.9 -12 5 9 57.39 13.4 -12 5 -9 61.79 11 12 5 9 55.89 9.9 12 -5 -9 73.79 10.6 -12 -5 9 50.09 13.8 -13 5 9 17.7 8.7 13 -5 9 0.8 6.9 -13 -5 9 25.7 8.9 13 5 9 20.7 6.8 -13 5 -9 11.5 7.3 13 -5 -9 18.6 7.1 14 -5 9 55.79 12.6 14 5 9 48.5 10.9 -14 -5 9 60.09 17.6 14 -5 -9 36.8 12.3 15 -5 9 21.1 9 15 5 9 21.2 8 15 -5 -9 10.8 8 -15 5 -9 2.7 8.5 16 -5 9 1.6 9.1 -16 5 -9 11.5 9.7 16 5 9 5.4 8.1 16 -5 -9 5.5 8.4 17 -5 9 -9.6 10 -17 5 -9 2.8 10 17 5 9 -2.1 8.6 17 -5 -9 14.7 8.9 0 -6 9 3390.36 208.48 0 -6 9 3258.17 189.58 0 6 9 3268.67 189.38 0 -6 -9 3303.47 207.38 0 -6 -9 3150.78 189.38 0 6 -9 3474.75 208.88 0 6 9 3308.17 208.68 0 6 -9 3293.07 189.68 0 6 9 3166.98 189.58 0 6 -9 3321.57 190.28 1 6 -9 122.49 31 1 -6 9 137.69 33.9 -1 6 9 119.09 32 1 -6 -9 173.18 11.2 -1 -6 9 170.48 34 -1 -6 9 178.18 11.3 -1 6 -9 119.99 31.8 1 6 9 166.28 39.6 -1 6 -9 180.18 12.2 1 6 9 178.38 10.6 1 -6 -9 178.28 32.4 -1 6 -9 167.28 11.4 1 6 9 171.98 11 2 6 -9 297.27 38.6 2 -6 9 205.48 40.4 2 6 -9 296.07 18.4 -2 6 9 295.87 18 -2 -6 -9 249.58 36.2 2 -6 9 312.57 17.5 -2 6 9 278.47 40.7 2 -6 9 305.27 18.2 -2 6 -9 314.27 18.9 2 6 9 295.47 17.7 -2 -6 9 290.97 38.8 -2 6 -9 278.37 39.8 -2 6 -9 301.67 19.2 -2 -6 9 294.27 18.1 2 6 9 291.47 17.2 2 6 9 213.68 36.8 2 -6 -9 256.47 39.2 -3 6 9 159.08 10.7 -3 -6 -9 180.78 30.2 -3 6 9 155.78 11.3 3 -6 9 165.18 10.8 3 -6 9 180.28 38.1 -3 -6 -9 154.98 10 3 -6 9 155.58 10 3 6 -9 162.78 32.2 3 6 -9 146.29 11 -3 6 9 107.19 35.5 -3 6 -9 164.08 11.6 3 6 9 164.08 10.1 -3 -6 9 153.68 32.7 3 -6 -9 116.59 33.1 -3 6 -9 165.58 11.1 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6 -10 920.71 55.69 1 -6 -10 917.11 75.49 -1 -6 10 965.9 54.99 -1 -6 10 960.9 76.29 -1 6 -10 955.3 76.99 1 6 10 946.71 54.59 1 -6 -10 941.21 54.99 1 6 10 1023.4 76.99 -2 6 10 2059.59 111.39 -2 -6 -10 1942.91 110.69 2 -6 10 1971 111.09 2 6 -10 1974.1 111.29 2 -6 10 1942.91 133.39 2 6 -10 1963.2 131.09 -2 6 10 2041.7 134.09 2 -6 10 1963.1 110.49 -2 -6 -10 1919.91 129.39 2 6 -10 1969 110.19 -2 6 10 1911.71 110.99 2 6 10 1843.72 110.69 -2 -6 10 1836.22 130.29 -2 6 -10 1894.01 111.69 2 6 10 1815.02 110.29 -2 6 -10 1841.12 111.19 -2 -6 10 1862.51 110.99 -2 6 -10 1842.42 131.59 2 6 10 1894.51 110.39 2 6 10 1914.71 130.19 2 -6 -10 1839.92 131.29 -3 -6 -10 464.45 27.5 -3 6 10 467.05 28 3 6 -10 481.85 49.99 3 -6 10 466.35 27.5 3 -6 10 483.15 56.79 -3 6 10 478.55 28.6 3 6 -10 466.35 27 -3 -6 -10 448.76 46.8 3 -6 10 457.05 28 3 6 -10 480.25 28.5 -3 6 10 460.75 54.69 3 -6 -10 482.95 52.39 -3 6 -10 461.95 51.89 -3 -6 10 490.65 51.99 -3 -6 10 472.05 28 -3 6 -10 468.75 28.8 -3 6 -10 460.15 28.3 3 6 10 390.46 48.8 3 6 10 464.25 27.6 -4 -6 -10 266.57 15.5 4 6 -10 261.07 16.7 -4 6 10 269.67 48.3 4 -6 10 329.67 48.9 -4 6 10 273.77 16.3 -4 6 10 278.17 17.1 4 -6 10 277.67 15.7 4 6 -10 274.47 14.9 -4 -6 -10 260.67 37.6 4 -6 10 266.47 16.2 -4 -6 10 230.38 16 4 6 10 228.98 15.3 -4 -6 10 217.68 43.1 -4 6 -10 187.08 44.1 4 -6 -10 195.58 41.5 4 6 10 236.08 38.2 -4 6 -10 230.98 16.5 -4 6 -10 224.78 16.8 5 6 -10 203.98 37.2 5 6 -10 185.18 11.1 -5 6 10 189.18 13.8 5 -6 10 191.48 12.1 -5 6 10 147.39 42.2 -5 6 10 189.58 12.6 5 -6 10 255.07 49.1 5 -6 10 187.48 12.4 -5 -6 -10 178.78 11.6 5 6 -10 193.18 13.3 5 6 10 166.18 35.5 -5 -6 10 178.38 12.3 5 -6 -10 237.18 45.9 -5 -6 10 192.28 43.6 5 6 10 180.58 11.2 -5 6 -10 177.58 13.4 -5 6 -10 193.88 45.5 -5 6 -10 181.58 13 -6 -6 -10 105.39 7.8 6 6 -10 100.69 10 -6 6 10 107.69 9.2 6 -6 10 111.19 8.7 -6 6 10 156.88 47.8 6 -6 10 114.09 8.4 6 6 -10 80.79 24.2 -6 6 10 112.79 10.6 6 -6 10 109.59 32.3 6 -6 -10 169.88 45.7 -6 -6 10 168.68 43.3 6 6 10 160.38 36.3 -6 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7.9 -13 6 10 22 10.2 -13 6 -10 22.7 8.1 13 -6 -10 22.7 7.7 -13 -6 10 27.2 9.2 13 6 10 17.1 7.2 14 -6 10 92.99 13.7 14 6 10 73.89 13 14 -6 -10 75.59 13 -14 6 -10 66.09 14.8 15 -6 10 7.4 8.9 15 6 10 13.5 8.3 -15 6 -10 10.8 9.4 15 -6 -10 19.7 8.7 16 -6 10 -11.9 8.9 16 -6 -10 18.6 8.9 16 6 10 4.4 8.2 -16 6 -10 16.8 9.9 0 7 10 2606.04 147.69 0 -7 10 2590.14 169.98 0 -7 -10 2510.95 147.79 0 7 -10 2571.64 148.09 0 7 10 2592.04 169.88 0 7 -10 2515.35 168.88 0 -7 10 2527.45 147.99 0 7 10 2481.15 147.79 0 -7 -10 2673.63 169.48 0 7 -10 2558.54 148.79 -1 7 10 709.93 37.4 1 7 -10 686.13 37.6 -1 -7 -10 604.44 58.69 1 7 -10 638.44 60.79 1 -7 10 624.84 63.29 1 -7 10 655.73 37.4 -1 -7 -10 676.53 37 -1 7 10 631.94 63.69 -1 7 10 648.94 37.2 1 7 10 584.94 37 -1 7 -10 604.24 37.5 -1 -7 10 577.04 60.99 1 7 10 609.14 61.09 -1 7 -10 630.24 60.59 1 -7 -10 636.84 60.59 -1 7 -10 582.14 38.1 1 7 10 577.34 36.7 -1 -7 10 590.74 37.3 -2 -7 -10 334.47 21.3 2 -7 10 329.77 22 2 7 -10 359.46 45.8 -2 -7 -10 351.16 44.2 2 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15.6 -9 3 -22 73.79 15.1 9 -3 -22 71.19 11.8 -10 3 22 25.2 9 -10 -3 22 8.7 8.8 -10 3 -22 28.7 10.1 -11 3 22 4.5 9 -11 3 -22 -0.7 9.9 -12 3 -22 27.3 11 0 -4 22 31.1 7.1 0 4 22 37.5 7.2 0 4 -22 40.1 9.1 0 -4 -22 35 8.2 -1 4 22 9.7 6.4 1 -4 22 11.4 6.4 1 4 -22 23.2 8.2 -1 -4 -22 4.8 6.8 1 -4 -22 10.3 7.5 -1 4 -22 8.2 7.9 -1 -4 22 7.6 6.5 1 4 22 -1 5.8 -2 -4 -22 71.69 12 2 -4 22 81.29 11.8 2 4 -22 78.19 14.2 -2 4 22 84.19 12.2 -2 -4 22 85.09 12.5 2 4 22 90.49 11.2 -2 4 -22 77.49 13.7 2 -4 -22 91.19 13.6 -3 4 22 2.3 6.6 3 -4 22 6.9 6 -3 4 22 16.5 6.8 3 4 -22 -1.7 8.3 -3 -4 -22 -6.4 6.6 -3 -4 22 -1.7 6.7 -3 4 -22 4.5 7.8 3 -4 -22 12 8.1 3 4 22 1.3 5.3 -4 -4 -22 16.1 6.9 4 -4 22 23.1 6.5 -4 4 22 21.4 7.4 -4 4 22 14.2 7.6 4 4 -22 23.3 9.7 -4 -4 22 24.7 7.6 -4 4 -22 23.9 8.5 4 4 22 23.6 5.6 4 -4 -22 7.5 8.8 5 4 -22 52.19 10.7 -5 4 22 66.19 12.8 5 -4 22 45.1 7.4 -5 -4 -22 76.59 11.8 -5 4 22 48.9 13.5 -5 -4 22 68.69 12.7 5 4 22 56.79 8.9 -5 4 -22 52.69 13.4 -6 -4 -22 30.8 7.4 -6 4 22 29.2 8.3 6 4 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12.4 3 5 22 46.9 9.9 -4 5 22 14.5 7.5 4 -5 22 7.7 6.4 -4 5 22 6.4 6.8 4 5 -22 16.3 9.3 -4 -5 -22 7 6.5 -4 5 -22 13.3 8.6 4 5 22 18 5.4 -4 -5 22 10.1 7.2 5 5 -22 78.59 15.3 5 -5 22 88.89 11.7 -5 5 22 63.49 13.8 -5 5 22 89.39 13.7 -5 -5 -22 106.69 12.5 -5 5 -22 94.69 14 -5 -5 22 75.09 13.6 5 5 22 91.79 9.9 -6 5 22 38.1 8.4 6 5 -22 14.4 10 6 -5 22 22.4 6.1 -6 5 22 21.1 8.6 -6 5 -22 18 9 -6 -5 22 25.3 8.1 6 -5 -22 25.3 7 -7 5 22 59.99 12.1 7 5 -22 82.39 17.5 7 -5 22 70.19 10.8 -7 5 -22 113.29 15.8 7 -5 -22 100.89 12.6 -7 -5 22 106.89 13.8 -8 5 22 10.9 7.8 -8 5 -22 17.3 9.6 -8 -5 22 -0.7 7.4 8 -5 -22 10.4 6.6 -9 5 22 103.99 15.6 -9 5 -22 75.39 15.9 9 -5 -22 80.09 13 -9 -5 22 73.09 14.7 -10 5 22 14.2 8.3 -10 -5 22 14.4 12 -10 5 -22 1.1 10 10 -5 -22 2.3 7.5 -11 5 22 11 8.9 -11 5 -22 9.7 10.3 11 -5 -22 4.8 8 -12 5 22 6.7 9.8 -12 5 -22 -4.8 12.3 0 6 22 59.39 11 0 -6 22 64.89 12.2 0 -6 -22 58.29 11.8 0 6 -22 55.69 13.7 1 6 -22 78.29 13.9 1 -6 22 77.69 12.5 -1 6 22 94.99 12.3 -1 -6 -22 57.99 11.9 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11.5 -9 11 22 -14.7 8.7 9 -11 -22 3.4 9 -9 11 -22 -14.7 10.6 0 12 -22 48.4 11.2 0 12 22 61.39 12.6 0 -12 22 63.69 14.7 1 12 -22 42.2 11 -1 12 22 50.49 12.8 1 -12 22 58.69 14.8 1 12 22 43.8 8.5 -1 -12 22 56.39 14.5 -1 12 -22 69.79 15 2 -12 22 23.5 8.8 -2 12 22 25.8 8.2 2 12 -22 3.8 9.3 -2 -12 22 27.7 9.3 -2 12 -22 36.1 10.7 3 -12 22 76.49 14.3 3 12 -22 53.79 11.6 -3 12 22 71.69 14.4 -3 -12 22 78.79 14.9 -3 12 -22 72.79 15.9 4 -12 22 -0.8 7.8 4 12 -22 -9.4 9.9 -4 12 22 -10.4 7.9 -4 12 -22 4 10.2 -4 -12 22 12.5 8.1 5 -12 22 -0.8 7.7 5 12 -22 6 9.6 -5 12 22 4.8 8.3 5 -12 -22 -3.2 8.5 -5 -12 22 -10.7 8.1 -5 12 -22 -8.7 10 6 -12 22 8.2 7.6 6 12 -22 -2.3 10.1 -6 12 22 20.7 9.1 -6 12 -22 17.5 11 6 -12 -22 26.6 9.5 -6 -12 22 8.4 8.7 -7 12 22 15.1 9.2 7 -12 22 -6.4 7.7 7 12 -22 11.9 10.8 -7 -12 22 23.3 9.2 7 -12 -22 14.2 9.3 -7 12 -22 0.1 10.9 -8 12 22 13 9.2 8 -12 -22 4.8 9.1 -8 -12 22 9 9.2 -8 12 -22 8.7 11.6 -9 12 22 14.3 9.4 9 -12 -22 7.9 9.4 -9 12 -22 0.3 11.3 0 13 22 43.2 8.3 0 -13 22 43.6 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14.8 2 14 -22 88.29 15.5 2 -14 22 112.39 15.6 2 14 22 66.39 12.2 -2 -14 22 57.69 11 -2 14 -22 54.89 12.3 3 14 -22 2.6 10 3 -14 22 -4.4 8.7 -3 14 22 2.7 8.1 -3 -14 22 4.9 8.2 -3 14 -22 4 10 4 -14 22 11.3 8.6 4 14 -22 -3.1 9.7 -4 14 22 3.4 8.7 -4 14 -22 22.9 11.1 -4 -14 22 16.4 9.3 -5 14 22 22.4 9.2 5 14 -22 20.8 10.5 5 -14 22 7.7 8.1 -5 -14 22 14.7 8.9 -5 14 -22 17.1 11.7 5 -14 -22 10 9.5 6 -14 22 21.7 8.5 6 14 -22 1.8 10.2 -6 14 22 9.5 9.2 -6 14 -22 5.1 11 -6 -14 22 27 9.1 6 -14 -22 36.5 10.3 7 -14 22 13 8.2 -7 14 22 11.8 9.6 -7 14 -22 -3.8 11.3 -7 -14 22 16.5 9.3 7 -14 -22 9 10 0 -15 22 5.3 9.2 0 15 -22 20.9 10.3 -1 15 22 28.7 8.1 1 15 -22 27.7 10.6 1 -15 22 11.9 9.3 -1 15 -22 18.2 10.8 1 15 22 39.4 7.6 -1 -15 22 24.2 10.1 2 15 -22 15.6 9.9 -2 15 22 11.4 8 2 -15 22 24.2 9.8 -2 -15 22 11.5 8.9 -2 15 -22 7.3 10.5 3 -15 22 10.7 9 3 15 -22 17.6 10.5 -3 15 22 0.4 8.4 -3 15 -22 6.6 9.8 -3 -15 22 18.2 9.4 -4 15 22 17 9.2 4 15 -22 -7 9.4 4 -15 22 21.4 9.5 -4 15 -22 10.7 11 -4 -15 22 11.9 9.1 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10.9 2 -1 -28 24 11.9 2 1 28 -4.1 7.9 -2 1 -28 8.9 10.8 -2 -1 28 4.2 9 3 -1 28 3.6 7.6 3 1 -28 18.8 12.3 -3 -1 -28 19.6 10.8 -3 1 28 -9.8 9.2 -3 -1 28 2.3 9.3 3 -1 -28 15.8 11.8 -3 1 -28 -1.8 10.5 3 1 28 2.8 7.7 4 1 -28 19.6 12.9 4 -1 28 0.1 7.3 -4 -1 -28 38.4 11.2 -4 1 28 26.3 10 4 -1 -28 3.2 11.9 -4 1 -28 22.6 11 4 1 28 10.5 7.4 -4 -1 28 -6.3 9.2 -5 1 28 14.5 10 -5 -1 -28 -3.5 10 5 1 -28 17 12.8 -5 -1 28 6.7 9.6 -5 1 -28 7.9 10.7 -6 1 28 28.9 10.2 -6 -1 -28 57.99 14 -6 1 -28 51.99 12.2 -6 -1 28 48.8 11 0 2 -28 60.29 13 0 2 28 37 9.5 0 -2 -28 75.39 17.3 0 -2 28 54.19 10.7 -1 2 28 2.5 8.7 1 -2 28 -1.3 8.3 1 2 -28 -5.1 11.4 -1 -2 -28 13.4 11.1 1 -2 -28 -6.6 10.5 -1 2 -28 11.8 11.4 -1 -2 28 -7.7 8.9 1 2 28 1.3 8.4 -2 -2 -28 41.6 11.1 -2 2 28 16.4 9.4 2 -2 28 14.2 8.7 2 2 -28 23.8 12.4 -2 -2 28 14.3 9.5 -2 2 -28 28.8 11.6 2 -2 -28 42.8 12.2 2 2 28 35.1 9 -3 -2 -28 48.8 11.5 3 -2 28 42.8 9.3 3 2 -28 53.59 13.4 -3 2 28 45.1 10.4 -3 -2 28 61.79 15.7 3 -2 -28 41.4 13.4 3 2 28 47.6 8.8 -3 2 -28 59.19 12.6 4 -2 28 -11.1 7.2 -4 -2 -28 13.6 10.4 -4 2 28 7.4 9.5 4 2 -28 12 12.1 -4 2 -28 -5.5 10.6 -4 -2 28 7.9 9.5 -5 -2 -28 24 11.7 5 2 -28 -5.2 12 -5 2 28 26.3 9.9 -5 -2 28 14.4 9.3 -6 2 28 3.3 9.6 -6 -2 28 -13.3 8.9 -6 2 -28 13.5 10.5 0 3 28 8.8 8.9 0 -3 28 3.6 8.9 0 3 -28 -0.7 11.4 0 -3 -28 9.9 10.5 -1 3 28 42.2 10 1 3 -28 53.09 13.2 1 -3 28 43.4 9.9 -1 -3 -28 55.79 12.1 1 -3 -28 25.6 11.4 -1 -3 28 46.6 10.5 1 3 28 71.09 15.2 -1 3 -28 46.2 12.4 2 -3 28 12.4 8.7 2 3 -28 18.1 12.7 -2 3 28 21.2 9.7 -2 -3 -28 20.8 11.2 -2 3 -28 7.4 11 2 -3 -28 9.7 11.6 2 3 28 15.3 8 -2 -3 28 14.6 9.5 -3 3 28 14.8 9.7 3 -3 28 14.7 8.4 3 3 -28 -0.7 11.2 -3 -3 -28 17.6 10.6 -3 3 -28 7.3 10.8 3 -3 -28 12.6 12.2 3 3 28 -6.5 7.3 -3 -3 28 -0.8 9.4 4 3 -28 21.1 13.3 -4 3 28 34.4 10.5 -4 -3 -28 31.4 12 -4 -3 28 10.6 9.9 -4 3 -28 25.5 11.2 -5 3 28 18.5 10 5 3 -28 19 13.4 -5 -3 28 8.4 10 -5 3 -28 28.4 11.2 -6 3 28 1.6 9.6 -6 3 -28 1.8 10.9 -6 -3 28 11.1 10 0 4 28 -0.3 8.3 0 -4 -28 -3.5 10.2 0 4 -28 0.9 11.5 0 -4 28 6.7 8.9 -1 4 28 18.9 9.3 -1 -4 -28 39.7 11.3 1 4 -28 28.7 12.3 1 -4 28 65.79 15 -1 4 -28 35.7 12.1 1 4 28 31.7 9.2 -1 -4 28 27 10.1 1 -4 -28 20.1 11.8 -2 4 28 -17.1 8.5 2 4 -28 6.3 12.6 2 -4 28 -1.3 8.6 -2 -4 -28 1.9 10.7 2 -4 -28 5.8 11.4 2 4 28 -6.5 7.5 -2 -4 28 10.2 9.4 -2 4 -28 1.3 11.1 3 4 -28 20.6 12.9 -3 4 28 9.9 9.7 3 -4 28 16.2 8.6 -3 -4 28 47.4 10.5 -3 4 -28 22.9 11.5 3 4 28 25.6 7.9 4 -4 28 24.4 8.5 4 4 -28 3.1 12.9 -4 4 28 23.6 10.1 -4 4 -28 34.1 11.7 -4 -4 28 19 10.1 -5 4 28 2.6 9.6 5 4 -28 -7.3 12.6 -5 -4 28 7.2 9.6 -5 4 -28 -19.7 10.6 -6 4 28 35.6 11.8 6 4 -28 58.09 15.1 -6 -4 28 17.9 10.7 -6 4 -28 32.1 11.8 0 -5 28 -3.2 8.5 0 5 -28 15.6 11.3 0 -5 -28 -3 10.9 0 5 28 6.2 8.5 -1 5 28 13.3 9.4 1 5 -28 42 13.2 1 -5 28 18.2 9.3 -1 -5 -28 19.1 11.1 1 5 28 28 8.7 -1 5 -28 18.1 11.7 -1 -5 28 17 9.5 1 -5 -28 27.8 11.7 2 5 -28 6.8 12.3 -2 5 28 13.8 9.5 2 -5 28 -11.1 8.3 -2 -5 28 7.9 9.2 2 5 28 23.1 8.1 -2 5 -28 9.3 11.4 -3 5 28 21 10.3 3 5 -28 38.2 13.6 3 -5 28 36.6 9 -3 5 -28 27.2 11.7 -3 -5 28 31.5 10.1 3 5 28 28.9 8.3 -4 5 28 10.1 9.8 4 -5 28 13.4 8.2 4 5 -28 6.3 12.8 -4 5 -28 -2.8 10.5 4 -5 -28 10.4 7.9 -4 -5 28 -4.1 9.3 5 5 -28 -5.7 12.2 -5 5 28 6 10.4 5 -5 28 8.4 8.1 -5 -5 28 15.1 10 -5 5 -28 11.3 11.6 0 -6 -28 33.8 11.7 0 6 -28 17.5 11.8 0 -6 28 8.8 8.9 0 6 28 -0.8 8.4 1 6 -28 17.4 12.3 -1 6 28 16.4 8.9 1 -6 28 10.9 8.8 -1 -6 28 13.2 9.2 1 6 28 15 8.4 -1 6 -28 3.2 11.3 -2 6 28 44.9 10.5 2 -6 28 56.79 14.8 2 6 -28 62.49 14.3 -2 -6 28 55.09 10.9 2 6 28 65.69 13.6 -2 6 -28 46.2 12.9 -3 6 28 9.3 9.7 3 6 -28 21 13 3 -6 28 7.2 8.6 -3 -6 28 8.4 9.2 -3 6 -28 18 11.4 -4 6 28 34.1 10.8 4 6 -28 33.8 13.4 4 -6 28 57.39 13.8 -4 6 -28 19.5 11.4 4 -6 -28 19.7 8.9 -4 -6 28 9.4 9.6 -5 6 28 40.2 11.3 5 -6 28 36.4 9.4 5 6 -28 42.1 14 5 -6 -28 42.6 9.7 -5 6 -28 16.9 11.5 -5 -6 28 24 10 0 7 28 40.8 9.5 0 7 -28 22.3 12.3 0 -7 28 31.6 9.7 1 7 -28 -8.7 11.9 -1 7 28 -3.3 8.8 1 -7 28 7.7 9 -1 -7 28 1.2 8.9 1 7 28 10.8 8.2 -1 7 -28 4.5 11.8 2 7 -28 -1.3 12.5 -2 7 28 -0.5 9.1 2 -7 28 11.4 8.7 -2 -7 28 -2.7 8.8 -2 7 -28 8.9 11.5 2 7 28 6.9 7.7 3 -7 28 14.1 8.8 3 7 -28 33.7 13.6 -3 7 28 25.3 10.1 -3 7 -28 21 11.8 -3 -7 28 18.4 9.3 -4 7 28 0.5 10 4 -7 28 -8.5 8.1 4 7 -28 0.8 12.4 -4 -7 28 12.7 9.4 4 -7 -28 -16.6 8.2 -4 7 -28 11.2 11.2 5 -7 28 0.7 9.4 5 -7 -28 17.8 12.5 0 8 28 9 8.5 0 8 -28 7.5 11.8 0 -8 28 -0.7 9.1 1 8 -28 -7.4 12.2 1 -8 28 17.3 9.4 -1 8 28 3.6 8.8 -1 -8 28 8.9 9.4 1 8 28 15.6 8.5 -1 8 -28 10.8 12.3 2 8 -28 6.6 12.2 -2 8 28 -6.1 8.6 2 -8 28 7.5 8.8 -2 8 -28 9.7 11.9 -2 -8 28 -3.3 9.5 2 8 28 -8.1 7.7 3 -8 28 59.29 14.9 -3 8 28 46 10.7 3 8 -28 17.3 13.4 -3 -8 28 41 10.9 -3 8 -28 35.5 12.7 4 -8 28 15.1 10.4 4 8 -28 21.6 19.2 4 -8 -28 -3.8 10.9 -4 -8 28 2.6 11.4 0 -9 28 5.7 9.1 0 9 28 -2.2 8.3 0 9 -28 3.1 12.2 -1 9 28 16.4 9.2 1 -9 28 -1 9 1 9 -28 21.3 12.7 -1 9 -28 9.1 12.3 1 9 28 17 8.1 -1 -9 28 13.2 9.7 2 -9 28 15.3 9.2 -2 9 28 -3.4 9.3 2 9 -28 8.8 12.3 -2 9 -28 -0.6 12.2 -2 -9 28 5.3 10 3 -9 28 -10.8 10.2 1 10 28 6.3 9.8 0 0 29 1.7 8.5 0 0 -29 0 11.7 1 0 -29 8.5 11.5 -1 0 29 13.2 9.6 -1 0 -29 25.7 12 1 0 29 8.5 8.9 -2 0 -29 2 11 -2 0 29 11.7 9.6 2 0 -29 3.5 12.1 2 0 29 -1.1 8.1 -3 0 -29 4.7 10.8 3 0 29 1.5 8.2 -3 0 29 20.8 9.8 3 0 -29 -7.1 12 -4 0 -29 20.4 11.6 4 0 -29 8.6 13 -4 0 29 15.7 10.1 -5 0 -29 18.3 12.7 -5 0 29 28.1 13.2 0 1 -29 27.7 12.3 0 -1 -29 32.6 12.3 0 1 29 28.3 9.2 0 -1 29 18.3 9.5 1 1 -29 8.4 12.1 -1 1 29 4.5 9.2 1 -1 29 8 8.8 -1 -1 -29 17.6 12 1 -1 -29 31.2 12.4 -1 1 -29 -20.7 10.8 -1 -1 29 -1.3 9.2 1 1 29 3.2 8.5 -2 1 29 54.69 11.2 -2 -1 -29 51.69 12.4 2 -1 29 28.2 9.1 2 1 -29 49.8 13.3 2 1 29 57.19 14.4 -2 1 -29 21 11.6 -2 -1 29 26.2 10.2 2 -1 -29 46 12.8 3 -1 29 0.9 7.8 -3 -1 -29 32.3 11.5 3 1 -29 15.1 12.5 -3 1 29 18.8 10.2 -3 1 -29 13 11.1 -3 -1 29 4.3 9.8 3 -1 -29 19.7 13.4 3 1 29 14.6 8.4 -4 -1 -29 12.6 11.4 -4 1 29 -1.5 9.6 4 1 -29 3.5 13.1 4 -1 29 9.6 8.6 -4 1 -29 12.4 11.2 -4 -1 29 2.6 9.8 -5 -1 -29 -0.6 12.3 -5 1 29 -15.8 13.3 -5 -1 29 -24.2 11.8 -5 1 -29 -0.3 12.5 0 2 29 -0.8 9 0 2 -29 7 11.7 0 -2 -29 8.9 11.1 0 -2 29 1.2 8.7 1 2 -29 27.4 13 1 -2 29 19.9 9.5 -1 -2 -29 51.39 12.7 -1 2 29 39.6 10 -1 2 -29 23.3 12.2 1 2 29 16.7 9.2 -1 -2 29 29.4 9.9 1 -2 -29 24.3 12.1 2 -2 29 -6.9 8.5 -2 2 29 -0.2 9.2 2 2 -29 -7.2 11.7 -2 -2 -29 10.8 11.6 2 -2 -29 19.6 12.3 -2 -2 29 10.2 9.7 2 2 29 -5.3 7.8 -2 2 -29 7.9 11.2 3 2 -29 19 16.5 3 -2 29 12.5 8.3 -3 -2 -29 27 11.4 -3 2 29 -1.1 9.5 -3 2 -29 28.1 11.8 3 -2 -29 19.2 12.9 3 2 29 5.1 8.3 -3 -2 29 23.2 10.1 4 -2 29 37.4 8.7 4 2 -29 2.3 13.1 -4 2 29 8.9 10.4 -4 -2 -29 31.3 11.8 -4 -2 29 13.6 9.5 -4 2 -29 29 12 0 -3 -29 26.6 11.8 0 3 29 21 9.3 0 -3 29 14.6 9.6 0 3 -29 16.3 12.2 -1 -3 -29 0.8 10.9 1 3 -29 48.8 13.6 1 -3 29 34.5 9.4 -1 3 29 29.3 10 -1 -3 29 31.5 10.2 -1 3 -29 37.9 12.9 1 3 29 30.9 9.1 1 -3 -29 91.19 18.1 -2 -3 -29 36.5 12.2 -2 3 29 37.6 10.2 2 3 -29 30.3 13 2 -3 29 15.9 9 2 3 29 19.8 8.9 2 -3 -29 24.8 12.3 -2 3 -29 44.3 12.4 -2 -3 29 22.6 10.1 -3 3 29 23.5 10.4 3 3 -29 21.1 12.9 3 -3 29 20.9 8.8 -3 -3 -29 32.3 12.1 3 3 29 21.7 8.2 -3 3 -29 27.1 12.1 -3 -3 29 20.2 10.2 -4 3 29 -5.4 9.9 4 3 -29 24.2 13.3 4 -3 29 8 8.1 -4 3 -29 18.5 11.9 -4 -3 29 5.3 9.7 0 -4 29 13.1 9.4 0 4 -29 23.8 13 0 4 29 1.5 9 0 -4 -29 17.8 11.7 -1 -4 -29 0.3 10.9 1 4 -29 32.1 12.7 1 -4 29 7.7 9.2 -1 4 29 8 9.1 1 -4 -29 -27.6 10.9 1 4 29 -2.4 8.2 -1 4 -29 15.8 12.3 -1 -4 29 2.1 9.5 -2 -4 -29 9.1 13.7 -2 4 29 1.1 9.3 2 -4 29 12.5 9 2 4 -29 -3.2 12.2 2 4 29 17.4 8.3 -2 4 -29 11.2 11.5 -2 -4 29 3.9 9.8 3 -4 29 12.5 8.8 3 4 -29 11.3 12.5 -3 4 29 1.3 9.5 -3 4 -29 5.9 11.4 -3 -4 29 6.4 10.2 4 4 -29 9.6 14.3 -4 4 29 23.2 12.3 4 -4 29 6.2 8.4 -4 4 -29 31.4 13.1 -4 -4 29 -7.4 11.1 0 -5 29 13.4 9.6 0 5 -29 -13.6 12 0 5 29 10.3 8.9 0 -5 -29 -3.2 11.8 1 -5 29 16.7 9.1 1 5 -29 -9.8 12.2 -1 5 29 2.1 8.8 -1 -5 29 16.5 9.9 -1 5 -29 21.9 12.6 1 5 29 15.3 8.6 -2 5 29 -5.1 9 2 5 -29 5.3 13.3 2 -5 29 -10.8 8.7 -2 5 -29 -5.9 11.2 2 5 29 -1.5 7.9 -2 -5 29 15.6 9.9 3 -5 29 43.2 9.8 3 5 -29 46 14 -3 5 29 67.49 16.2 -3 -5 29 56.69 11.6 -3 5 -29 49.3 13.3 4 -5 29 10.4 12.6 0 -6 29 -2.2 9 0 6 -29 2.1 12.4 0 6 29 10.6 9.2 1 6 -29 5 12.9 -1 6 29 14.9 9.4 1 -6 29 9 9.4 -1 6 -29 23 12.4 1 6 29 37.4 9.1 -1 -6 29 25.1 10 -2 6 29 -5.5 9.1 2 6 -29 13.5 17.6 2 -6 29 -2.2 9 -2 -6 29 7.4 12.6 -2 6 -29 33.6 12.8 2 6 29 3 7.7 3 -6 29 27 12.4 -3 6 -29 1.7 16.1 0 7 -29 -6.7 13.9 0 7 29 -1.6 8.9 0 -7 29 -6.1 10 1 7 -29 43.3 18.3 1 -7 29 37.9 11.5 -1 7 29 28.1 11.4 -1 7 -29 35.9 16.8 1 7 29 34.3 9.4 -1 -7 29 37.6 12.9 0 0 30 18.6 9.5 0 0 -30 22 12.6 1 0 -30 7.1 13.2 -1 0 30 25.7 10.6 1 0 30 19 9.3 -1 0 -30 7.1 12.6 2 0 -30 20.4 17.9 -2 0 -30 16.2 14.6 -2 0 30 -5.2 12.8 2 0 30 7 9.7 0 1 -30 -8.7 11.9 0 -1 30 -5.4 8.8 0 1 30 -4.4 9.2 0 -1 -30 -3.5 11.1 -1 -1 -30 4.9 12.5 1 -1 30 6.3 9.5 1 1 -30 0.2 12.5 -1 1 30 1.9 10 1 -1 -30 6.1 12.2 -1 -1 30 11.9 10.2 -1 1 -30 26.3 13 1 1 30 14 9.7 2 1 -30 29.7 19.5 2 -1 30 2.4 10.3 -2 -1 -30 17 16 2 -1 -30 9.8 18.3 -2 1 -30 25.5 17.7 2 1 30 13.7 12.6 0 2 -30 -1.1 13.9 0 -2 -30 18.8 12.9 0 -2 30 -11.4 9.2 0 2 30 11.4 10.2 1 -2 30 79.39 19.3 1 2 -30 52.39 17.9 -1 2 30 92.29 19.5 -1 -2 -30 42.1 13.7 1 -2 -30 61.89 14.9 -1 -2 30 33.6 12.2 -1 2 -30 50.09 15.2 1 2 30 49.1 10.6 2 -2 30 2 12.4 -2 -2 -30 15.4 18.1 2 2 30 11.4 10.5 0 3 -30 46.4 20.9 0 -3 30 11.5 11.8 0 -3 -30 42.5 15.3 -1 -3 -30 22.7 15.2 1 3 30 27 12.1 1 -3 -30 11.7 17 #===END data_NiPhBr _audit_creation_date 2017-04-27 _audit_creation_method ; Olex2 1.2 (compiled 2016.02.19 svn.r3266 for OlexSys, GUI svn.r5155) ; _publ_contact_author_address ? _publ_contact_author_email ? _publ_contact_author_name '' _publ_contact_author_phone ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ; ? ; _chemical_formula_moiety 'C51 H43 Br N2 Ni O2, C4 H8 O' _chemical_formula_sum 'C55 H51 Br N2 Ni O3' _chemical_formula_weight 926.60 _chemical_absolute_configuration syn _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Br' 'Br' -0.6763 1.2805 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Ni' 'Ni' -3.0029 0.5091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system 'orthorhombic' _space_group_IT_number 19 _space_group_name_H-M_alt 'P 21 21 21' _space_group_name_Hall 'P 2ac 2ab' loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 'x, y, z' 2 '-x+1/2, -y, z+1/2' 3 '-x, y+1/2, -z+1/2' 4 'x+1/2, -y+1/2, -z' _cell_length_a 9.7540(5) _cell_length_b 17.1117(16) _cell_length_c 26.830(3) _cell_angle_alpha 90.00 _cell_angle_beta 90.00 _cell_angle_gamma 90.00 _cell_volume 4478.2(7) _cell_formula_units_Z 4 _cell_measurement_reflns_used 9778 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 72.331 _cell_measurement_theta_min 3.062 _exptl_absorpt_coefficient_mu 2.036 _exptl_absorpt_correction_T_max 0.7536 _exptl_absorpt_correction_T_min 0.6315 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0893 before and 0.0729 after correction. The Ratio of minimum to maximum transmission is 0.8380. The \l/2 correction factor is Not present. ; _exptl_crystal_colour orange _exptl_crystal_colour_primary orange _exptl_crystal_density_diffrn 1.374 _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_description chip _exptl_crystal_F_000 1928 _exptl_crystal_preparation ? _exptl_crystal_size_max 0.14 _exptl_crystal_size_mid 0.08 _exptl_crystal_size_min 0.05 _exptl_special_details ; ? ; _diffrn_reflns_av_R_equivalents 0.0475 _diffrn_reflns_av_unetI/netI 0.0415 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -21 _diffrn_reflns_limit_l_max 29 _diffrn_reflns_limit_l_min -33 _diffrn_reflns_number 32200 _diffrn_reflns_theta_full 72.77 _diffrn_reflns_theta_max 72.77 _diffrn_reflns_theta_min 3.06 _diffrn_ambient_temperature 100(2) _diffrn_detector_area_resol_mean ? _diffrn_measured_fraction_theta_full 0.989 _diffrn_measured_fraction_theta_max 0.989 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_source 'fine-focus sealed tube' _diffrn_special_details ? _diffrn_standards_decay_% ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_number 0 _reflns_number_gt 7993 _reflns_number_total 8614 _reflns_threshold_expression >2sigma(I) _computing_cell_refinement ? _computing_data_collection ? _computing_data_reduction ? _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'XT (Sheldrick, 2015)' _refine_diff_density_max 1.552 _refine_diff_density_min -0.603 _refine_diff_density_rms 0.081 _refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881' _refine_ls_abs_structure_Flack 0.00(2) _refine_ls_extinction_coef ? _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.029 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 562 _refine_ls_number_reflns 8614 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0501 _refine_ls_R_factor_gt 0.0452 _refine_ls_restrained_S_all 1.029 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0520P)^2^+7.8010P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1112 _refine_ls_wR_factor_ref 0.1144 _refine_special_details ? _olex2_refinement_description ; 1. Twinned data refinement Scales: 0.943(17) 0.057(17) 2. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 3.a Ternary CH refined with riding coordinates: C9(H9), C33(H33) 3.b Secondary CH2 refined with riding coordinates: C52(H52A,H52B), C53(H53A,H53B), C54(H54A,H54B), C55(H55A,H55B) 3.c Aromatic/amide H refined with riding coordinates: C2(H2), C3(H3), C4(H4), C5(H5), C6(H6), C11(H11), C12(H12), C13(H13), C14(H14), C15(H15), C17(H17), C18(H18), C19(H19), C20(H20), C21(H21), C23(H23), C24(H24), C25(H25), C26(H26), C27(H27), C35(H35), C36(H36), C37(H37), C38(H38), C39(H39), C41(H41), C42(H42), C43(H43), C44(H44), C45(H45), C47(H47), C48(H48), C49(H49), C50(H50), C51(H51) 3.d Idealised Me refined as rotating group: C29(H29A,H29B,H29C), C30(H30A,H30B,H30C) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symetry_multiplicity _atom_site_calc_flag _atom_site_disorder_assembly _atom_site_disorder_group _atom_site_refinement_flags_posn Br1 Br 0.79394(4) 0.51853(2) 0.414579(17) 0.02492(10) Uani 1 1 d . . . Ni1 Ni 0.62691(6) 0.42362(3) 0.40731(2) 0.01619(14) Uani 1 1 d . . . O1 O 0.2735(3) 0.52125(14) 0.46930(9) 0.0187(5) Uani 1 1 d . . . O2 O 0.2885(3) 0.29157(13) 0.37096(9) 0.0153(5) Uani 1 1 d . . . N1 N 0.4807(3) 0.48507(18) 0.44100(10) 0.0149(6) Uani 1 1 d . . . N2 N 0.4900(3) 0.35213(17) 0.38365(11) 0.0164(6) Uani 1 1 d . . . C1 C 0.7684(4) 0.3549(2) 0.38536(14) 0.0194(8) Uani 1 1 d . . . C2 C 0.8274(4) 0.3573(2) 0.33830(14) 0.0219(8) Uani 1 1 d . . . H2 H 0.8065 0.3990 0.3162 0.026 Uiso 1 1 calc . . R C3 C 0.9178(4) 0.2982(3) 0.32327(16) 0.0296(10) Uani 1 1 d . . . H3 H 0.9556 0.2987 0.2906 0.036 Uiso 1 1 calc . . R C4 C 0.9518(5) 0.2387(2) 0.35637(17) 0.0303(10) Uani 1 1 d . . . H4 H 1.0125 0.1984 0.3462 0.036 Uiso 1 1 calc . . R C5 C 0.8987(4) 0.2382(2) 0.40299(18) 0.0322(10) Uani 1 1 d . . . H5 H 0.9253 0.1986 0.4259 0.039 Uiso 1 1 calc . . R C6 C 0.8047(4) 0.2957(2) 0.41760(15) 0.0257(8) Uani 1 1 d . . . H6 H 0.7656 0.2938 0.4500 0.031 Uiso 1 1 calc . . R C7 C 0.3546(4) 0.46810(19) 0.44612(13) 0.0149(7) Uani 1 1 d . . . C8 C 0.3541(4) 0.59480(19) 0.46658(13) 0.0164(7) Uani 1 1 d . . . C9 C 0.5011(4) 0.5618(2) 0.46743(13) 0.0161(7) Uani 1 1 d . . . H9 H 0.5637 0.5962 0.4477 0.019 Uiso 1 1 calc . . R C10 C 0.5595(4) 0.5484(2) 0.51909(14) 0.0195(8) Uani 1 1 d . . . C11 C 0.5199(4) 0.4868(3) 0.54950(14) 0.0257(8) Uani 1 1 d . . . H11 H 0.4561 0.4493 0.5375 0.031 Uiso 1 1 calc . . R C12 C 0.5727(5) 0.4798(3) 0.59710(15) 0.0307(9) Uani 1 1 d . . . H12 H 0.5433 0.4380 0.6178 0.037 Uiso 1 1 calc . . R C13 C 0.6677(5) 0.5328(3) 0.61479(16) 0.0328(10) Uani 1 1 d . . . H13 H 0.7054 0.5269 0.6472 0.039 Uiso 1 1 calc . . R C14 C 0.7074(5) 0.5947(3) 0.58475(16) 0.0336(9) Uani 1 1 d . . . H14 H 0.7713 0.6319 0.5970 0.040 Uiso 1 1 calc . . R C15 C 0.6552(4) 0.6026(2) 0.53738(16) 0.0274(9) Uani 1 1 d . . . H15 H 0.6840 0.6449 0.5170 0.033 Uiso 1 1 calc . . R C16 C 0.3129(4) 0.63124(19) 0.41657(14) 0.0188(7) Uani 1 1 d . . . C17 C 0.3925(4) 0.6248(2) 0.37401(14) 0.0231(8) Uani 1 1 d . . . H17 H 0.4807 0.6015 0.3758 0.028 Uiso 1 1 calc . . R C18 C 0.3437(5) 0.6524(3) 0.32888(16) 0.0290(9) Uani 1 1 d . . . H18 H 0.3992 0.6484 0.2999 0.035 Uiso 1 1 calc . . R C19 C 0.2147(5) 0.6858(3) 0.32559(16) 0.0327(9) Uani 1 1 d . . . H19 H 0.1805 0.7031 0.2943 0.039 Uiso 1 1 calc . . R C20 C 0.1356(4) 0.6937(3) 0.36839(15) 0.0298(9) Uani 1 1 d . . . H20 H 0.0482 0.7181 0.3667 0.036 Uiso 1 1 calc . . R C21 C 0.1838(4) 0.6661(2) 0.41323(16) 0.0266(8) Uani 1 1 d . . . H21 H 0.1287 0.6709 0.4423 0.032 Uiso 1 1 calc . . R C22 C 0.3156(4) 0.6466(2) 0.51016(13) 0.0178(7) Uani 1 1 d . . . C23 C 0.3722(4) 0.7218(2) 0.51233(15) 0.0246(8) Uani 1 1 d . . . H23 H 0.4363 0.7379 0.4877 0.030 Uiso 1 1 calc . . R C24 C 0.3354(4) 0.7724(2) 0.54994(16) 0.0275(9) Uani 1 1 d . . . H24 H 0.3738 0.8234 0.5510 0.033 Uiso 1 1 calc . . R C25 C 0.2429(4) 0.7493(2) 0.58613(17) 0.0321(10) Uani 1 1 d . . . H25 H 0.2162 0.7846 0.6117 0.038 Uiso 1 1 calc . . R C26 C 0.1899(5) 0.6749(3) 0.58490(17) 0.0365(10) Uani 1 1 d . . . H26 H 0.1276 0.6585 0.6101 0.044 Uiso 1 1 calc . . R C27 C 0.2266(5) 0.6234(2) 0.54710(15) 0.0294(9) Uani 1 1 d . . . H27 H 0.1901 0.5719 0.5468 0.035 Uiso 1 1 calc . . R C28 C 0.2777(4) 0.3962(2) 0.42946(13) 0.0175(7) Uani 1 1 d . . . C29 C 0.1449(4) 0.4220(3) 0.40315(18) 0.0348(10) Uani 1 1 d . . . H29A H 0.0860 0.4497 0.4269 0.052 Uiso 1 1 calc . . GR H29B H 0.0965 0.3760 0.3904 0.052 Uiso 1 1 calc . . GR H29C H 0.1676 0.4569 0.3754 0.052 Uiso 1 1 calc . . GR C30 C 0.2433(5) 0.3454(3) 0.47583(16) 0.0354(11) Uani 1 1 d . . . H30A H 0.3284 0.3250 0.4903 0.053 Uiso 1 1 calc . . GR H30B H 0.1843 0.3018 0.4658 0.053 Uiso 1 1 calc . . GR H30C H 0.1956 0.3775 0.5006 0.053 Uiso 1 1 calc . . GR C31 C 0.3618(4) 0.3478(2) 0.39446(12) 0.0140(7) Uani 1 1 d . . . C32 C 0.3892(4) 0.2401(2) 0.34658(13) 0.0150(7) Uani 1 1 d . . . C33 C 0.5122(4) 0.2976(2) 0.34074(13) 0.0159(7) Uani 1 1 d . . . H33 H 0.6003 0.2687 0.3454 0.019 Uiso 1 1 calc . . R C34 C 0.5175(4) 0.3445(2) 0.29268(14) 0.0179(7) Uani 1 1 d . . . C35 C 0.4606(4) 0.4188(2) 0.28783(15) 0.0238(8) Uani 1 1 d . . . H35 H 0.4181 0.4433 0.3156 0.029 Uiso 1 1 calc . . R C36 C 0.4665(5) 0.4569(3) 0.24195(16) 0.0308(10) Uani 1 1 d . . . H36 H 0.4290 0.5079 0.2388 0.037 Uiso 1 1 calc . . R C37 C 0.5257(5) 0.4217(3) 0.20126(16) 0.0306(9) Uani 1 1 d . . . H37 H 0.5274 0.4478 0.1700 0.037 Uiso 1 1 calc . . R C38 C 0.5824(5) 0.3485(3) 0.20598(15) 0.0313(10) Uani 1 1 d . . . H38 H 0.6238 0.3242 0.1779 0.038 Uiso 1 1 calc . . R C39 C 0.5795(4) 0.3102(2) 0.25137(14) 0.0257(9) Uani 1 1 d . . . H39 H 0.6203 0.2600 0.2544 0.031 Uiso 1 1 calc . . R C40 C 0.3236(4) 0.2096(2) 0.29896(13) 0.0178(7) Uani 1 1 d . . . C41 C 0.2425(4) 0.2585(2) 0.26987(14) 0.0198(8) Uani 1 1 d . . . H41 H 0.2259 0.3107 0.2804 0.024 Uiso 1 1 calc . . R C42 C 0.1856(4) 0.2318(2) 0.22578(15) 0.0246(8) Uani 1 1 d . . . H42 H 0.1302 0.2658 0.2063 0.030 Uiso 1 1 calc . . R C43 C 0.2087(5) 0.1559(2) 0.20977(15) 0.0275(8) Uani 1 1 d . . . H43 H 0.1690 0.1375 0.1796 0.033 Uiso 1 1 calc . . R C44 C 0.2901(5) 0.1076(2) 0.23826(15) 0.0305(9) Uani 1 1 d . . . H44 H 0.3081 0.0559 0.2272 0.037 Uiso 1 1 calc . . R C45 C 0.3462(4) 0.1335(2) 0.28292(15) 0.0250(9) Uani 1 1 d . . . H45 H 0.4001 0.0990 0.3025 0.030 Uiso 1 1 calc . . R C46 C 0.4252(4) 0.1753(2) 0.38363(14) 0.0179(7) Uani 1 1 d . . . C47 C 0.5472(4) 0.1334(2) 0.37888(15) 0.0221(8) Uani 1 1 d . . . H47 H 0.6110 0.1472 0.3536 0.026 Uiso 1 1 calc . . R C48 C 0.5761(4) 0.0715(2) 0.41078(17) 0.0286(9) Uani 1 1 d . . . H48 H 0.6582 0.0424 0.4067 0.034 Uiso 1 1 calc . . R C49 C 0.4849(5) 0.0523(2) 0.44866(16) 0.0300(9) Uani 1 1 d . . . H49 H 0.5053 0.0104 0.4707 0.036 Uiso 1 1 calc . . R C50 C 0.3654(5) 0.0937(2) 0.45424(15) 0.0299(9) Uani 1 1 d . . . H50 H 0.3038 0.0809 0.4804 0.036 Uiso 1 1 calc . . R C51 C 0.3339(4) 0.1550(2) 0.42122(15) 0.0253(8) Uani 1 1 d . . . H51 H 0.2499 0.1826 0.4246 0.030 Uiso 1 1 calc . . R O00I O 0.3166(4) 0.4770(2) 0.68007(14) 0.0553(10) Uani 1 1 d . . . C52 C 0.3586(6) 0.5573(3) 0.6878(2) 0.0482(13) Uani 1 1 d . . . H52A H 0.2783 0.5904 0.6957 0.058 Uiso 1 1 calc . . R H52B H 0.4036 0.5781 0.6575 0.058 Uiso 1 1 calc . . R C53 C 0.4565(7) 0.5562(4) 0.7303(3) 0.0627(17) Uani 1 1 d . . . H53A H 0.4495 0.6050 0.7500 0.075 Uiso 1 1 calc . . R H53B H 0.5519 0.5504 0.7183 0.075 Uiso 1 1 calc . . R C54 C 0.4147(9) 0.4871(5) 0.7609(3) 0.088(2) Uani 1 1 d . . . H54A H 0.4933 0.4649 0.7794 0.105 Uiso 1 1 calc . . R H54B H 0.3404 0.5005 0.7845 0.105 Uiso 1 1 calc . . R C55 C 0.3661(10) 0.4332(4) 0.7213(2) 0.084(3) Uani 1 1 d . . . H55A H 0.4424 0.3991 0.7104 0.101 Uiso 1 1 calc . . R H55B H 0.2919 0.3996 0.7345 0.101 Uiso 1 1 calc . . R loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Br1 0.02031(17) 0.01575(17) 0.0387(2) -0.00421(17) 0.00357(17) -0.00216(15) Ni1 0.0164(3) 0.0134(3) 0.0188(3) -0.0034(2) -0.0008(3) 0.0002(2) O1 0.0211(13) 0.0102(11) 0.0248(13) -0.0055(11) 0.0034(10) -0.0013(11) O2 0.0163(11) 0.0124(11) 0.0172(12) -0.0039(9) 0.0013(10) -0.0014(10) N1 0.0191(14) 0.0107(13) 0.0147(14) -0.0021(12) -0.0019(11) -0.0028(12) N2 0.0210(16) 0.0146(15) 0.0135(15) -0.0028(12) -0.0001(12) 0.0026(12) C1 0.0159(18) 0.0223(18) 0.0201(18) -0.0027(15) -0.0016(14) -0.0025(14) C2 0.0222(19) 0.0223(19) 0.0212(19) -0.0005(15) -0.0028(15) -0.0032(15) C3 0.025(2) 0.038(2) 0.026(2) -0.0119(19) 0.0052(17) 0.0009(18) C4 0.029(2) 0.020(2) 0.042(3) -0.0101(18) 0.0037(19) 0.0046(17) C5 0.029(2) 0.023(2) 0.045(3) 0.0003(18) 0.001(2) 0.0030(17) C6 0.0261(19) 0.0265(19) 0.0245(19) -0.0031(17) 0.0008(18) 0.0010(16) C7 0.0185(17) 0.0125(17) 0.0137(16) -0.0019(13) 0.0009(13) 0.0027(13) C8 0.0229(18) 0.0077(16) 0.0186(17) -0.0025(13) 0.0037(14) -0.0024(14) C9 0.0218(18) 0.0088(16) 0.0176(17) -0.0055(13) -0.0012(14) 0.0012(13) C10 0.0211(18) 0.0189(17) 0.0184(19) -0.0071(15) -0.0008(15) 0.0016(14) C11 0.036(2) 0.0228(19) 0.0185(19) 0.0001(17) -0.0011(16) -0.0006(18) C12 0.042(2) 0.029(2) 0.021(2) 0.0036(18) -0.0038(17) -0.0021(19) C13 0.036(2) 0.041(3) 0.022(2) -0.0033(18) -0.0063(17) 0.0045(19) C14 0.034(2) 0.038(2) 0.029(2) -0.0112(19) -0.008(2) -0.0055(19) C15 0.032(2) 0.023(2) 0.027(2) -0.0020(16) -0.0052(17) -0.0065(17) C16 0.0231(18) 0.0150(15) 0.0182(17) -0.0013(15) -0.0027(16) -0.0005(13) C17 0.024(2) 0.0209(19) 0.024(2) 0.0028(15) 0.0025(16) -0.0001(16) C18 0.035(2) 0.031(2) 0.020(2) 0.0054(17) 0.0042(17) 0.0019(18) C19 0.041(2) 0.034(2) 0.023(2) 0.0055(17) -0.005(2) 0.004(2) C20 0.026(2) 0.037(2) 0.027(2) 0.0015(18) -0.0053(17) 0.0033(19) C21 0.0221(18) 0.035(2) 0.0223(19) 0.0000(18) 0.0019(17) 0.0023(16) C22 0.0250(19) 0.0116(16) 0.0169(17) -0.0059(14) -0.0031(15) 0.0031(14) C23 0.029(2) 0.0158(18) 0.029(2) -0.0035(15) -0.0020(17) 0.0020(16) C24 0.028(2) 0.0197(19) 0.035(2) -0.0093(17) -0.0081(17) 0.0063(15) C25 0.045(2) 0.028(2) 0.0234(19) -0.0109(19) -0.0036(19) 0.0155(18) C26 0.053(3) 0.033(2) 0.023(2) -0.0001(19) 0.012(2) 0.006(2) C27 0.046(3) 0.0190(18) 0.023(2) -0.0008(16) 0.0074(19) 0.0018(18) C28 0.0208(18) 0.0121(15) 0.0198(17) -0.0055(13) 0.0030(14) -0.0073(14) C29 0.026(2) 0.030(2) 0.048(3) -0.019(2) -0.0060(19) 0.0022(17) C30 0.057(3) 0.023(2) 0.026(2) -0.0050(18) 0.022(2) -0.014(2) C31 0.0172(17) 0.0117(15) 0.0131(16) -0.0008(13) -0.0024(13) -0.0008(14) C32 0.0176(17) 0.0119(16) 0.0154(16) -0.0029(13) 0.0013(14) -0.0014(14) C33 0.0203(17) 0.0148(17) 0.0125(17) -0.0034(14) -0.0005(14) -0.0010(14) C34 0.0195(18) 0.0143(17) 0.0200(19) -0.0008(14) 0.0003(14) -0.0035(14) C35 0.029(2) 0.0182(19) 0.024(2) 0.0025(16) 0.0002(16) -0.0006(16) C36 0.040(3) 0.024(2) 0.028(2) 0.0038(17) -0.0008(19) -0.0034(18) C37 0.037(2) 0.031(2) 0.024(2) 0.0099(18) 0.0020(18) -0.0096(19) C38 0.041(3) 0.037(2) 0.0158(19) 0.0018(17) 0.0055(18) -0.004(2) C39 0.034(2) 0.024(2) 0.019(2) -0.0022(16) 0.0038(16) -0.0003(17) C40 0.0206(19) 0.0181(18) 0.0148(17) -0.0019(14) -0.0009(14) -0.0031(14) C41 0.0224(19) 0.0156(17) 0.0213(18) -0.0036(15) -0.0006(14) 0.0019(14) C42 0.027(2) 0.0235(19) 0.0235(19) 0.0038(16) -0.0053(16) 0.0005(16) C43 0.036(2) 0.028(2) 0.0185(18) -0.0046(16) -0.0065(18) -0.002(2) C44 0.047(3) 0.0217(19) 0.023(2) -0.0102(16) -0.006(2) 0.001(2) C45 0.034(2) 0.0172(18) 0.024(2) -0.0025(15) -0.0069(17) 0.0046(16) C46 0.0236(18) 0.0130(17) 0.0170(18) -0.0022(14) -0.0038(15) -0.0026(14) C47 0.026(2) 0.0207(19) 0.0199(19) -0.0040(16) -0.0013(15) -0.0013(15) C48 0.032(2) 0.0211(18) 0.033(2) 0.0002(19) -0.0089(19) 0.0047(16) C49 0.040(2) 0.023(2) 0.027(2) 0.0048(17) -0.0113(19) -0.0055(18) C50 0.046(3) 0.023(2) 0.0209(19) 0.0047(16) 0.0005(19) -0.0068(19) C51 0.031(2) 0.0175(17) 0.027(2) -0.0002(16) 0.0013(16) -0.0035(15) O00I 0.075(3) 0.049(2) 0.041(2) -0.0132(18) 0.0051(19) -0.007(2) C52 0.054(3) 0.036(3) 0.055(3) -0.003(2) 0.005(3) 0.004(3) C53 0.060(4) 0.060(4) 0.068(4) -0.020(3) -0.007(3) -0.002(3) C54 0.098(6) 0.093(6) 0.072(5) -0.009(5) -0.016(4) 0.030(5) C55 0.157(8) 0.047(4) 0.049(4) 0.005(3) 0.015(4) 0.023(5) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Br1 Ni1 2.3087(7) . ? Ni1 N1 1.989(3) . ? Ni1 N2 1.919(3) . ? Ni1 C1 1.906(4) . ? O1 C7 1.356(4) . ? O1 C8 1.486(4) . ? O2 C31 1.354(4) . ? O2 C32 1.472(4) . ? N1 C7 1.271(5) . ? N1 C9 1.506(4) . ? N2 C31 1.286(5) . ? N2 C33 1.497(4) . ? C1 C2 1.388(5) . ? C1 C6 1.379(6) . ? C2 H2 0.9500 . ? C2 C3 1.400(6) . ? C3 H3 0.9500 . ? C3 C4 1.391(7) . ? C4 H4 0.9500 . ? C4 C5 1.354(7) . ? C5 H5 0.9500 . ? C5 C6 1.400(6) . ? C6 H6 0.9500 . ? C7 C28 1.509(5) . ? C8 C9 1.541(5) . ? C8 C16 1.533(5) . ? C8 C22 1.515(5) . ? C9 H9 1.0000 . ? C9 C10 1.516(5) . ? C10 C11 1.388(6) . ? C10 C15 1.404(5) . ? C11 H11 0.9500 . ? C11 C12 1.382(6) . ? C12 H12 0.9500 . ? C12 C13 1.381(6) . ? C13 H13 0.9500 . ? C13 C14 1.387(7) . ? C14 H14 0.9500 . ? C14 C15 1.376(6) . ? C15 H15 0.9500 . ? C16 C17 1.385(5) . ? C16 C21 1.397(5) . ? C17 H17 0.9500 . ? C17 C18 1.384(6) . ? C18 H18 0.9500 . ? C18 C19 1.384(6) . ? C19 H19 0.9500 . ? C19 C20 1.390(6) . ? C20 H20 0.9500 . ? C20 C21 1.375(6) . ? C21 H21 0.9500 . ? C22 C23 1.401(5) . ? C22 C27 1.376(6) . ? C23 H23 0.9500 . ? C23 C24 1.378(6) . ? C24 H24 0.9500 . ? C24 C25 1.383(6) . ? C25 H25 0.9500 . ? C25 C26 1.375(6) . ? C26 H26 0.9500 . ? C26 C27 1.391(6) . ? C27 H27 0.9500 . ? C28 C29 1.540(6) . ? C28 C30 1.554(5) . ? C28 C31 1.497(5) . ? C29 H29A 0.9800 . ? C29 H29B 0.9800 . ? C29 H29C 0.9800 . ? C30 H30A 0.9800 . ? C30 H30B 0.9800 . ? C30 H30C 0.9800 . ? C32 C33 1.559(5) . ? C32 C40 1.521(5) . ? C32 C46 1.531(5) . ? C33 H33 1.0000 . ? C33 C34 1.519(5) . ? C34 C35 1.394(5) . ? C34 C39 1.393(5) . ? C35 H35 0.9500 . ? C35 C36 1.394(6) . ? C36 H36 0.9500 . ? C36 C37 1.374(6) . ? C37 H37 0.9500 . ? C37 C38 1.374(6) . ? C38 H38 0.9500 . ? C38 C39 1.384(6) . ? C39 H39 0.9500 . ? C40 C41 1.390(5) . ? C40 C45 1.390(5) . ? C41 H41 0.9500 . ? C41 C42 1.384(5) . ? C42 H42 0.9500 . ? C42 C43 1.385(6) . ? C43 H43 0.9500 . ? C43 C44 1.378(6) . ? C44 H44 0.9500 . ? C44 C45 1.389(6) . ? C45 H45 0.9500 . ? C46 C47 1.395(5) . ? C46 C51 1.390(5) . ? C47 H47 0.9500 . ? C47 C48 1.390(6) . ? C48 H48 0.9500 . ? C48 C49 1.390(6) . ? C49 H49 0.9500 . ? C49 C50 1.372(7) . ? C50 H50 0.9500 . ? C50 C51 1.407(6) . ? C51 H51 0.9500 . ? O00I C52 1.449(6) . ? O00I C55 1.419(8) . ? C52 H52A 0.9900 . ? C52 H52B 0.9900 . ? C52 C53 1.488(9) . ? C53 H53A 0.9900 . ? C53 H53B 0.9900 . ? C53 C54 1.496(11) . ? C54 H54A 0.9900 . ? C54 H54B 0.9900 . ? C54 C55 1.485(11) . ? C55 H55A 0.9900 . ? C55 H55B 0.9900 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 Ni1 Br1 95.49(9) . . ? N2 Ni1 Br1 165.34(10) . . ? N2 Ni1 N1 89.33(12) . . ? C1 Ni1 Br1 87.07(11) . . ? C1 Ni1 N1 170.23(15) . . ? C1 Ni1 N2 90.49(14) . . ? C7 O1 C8 103.7(3) . . ? C31 O2 C32 106.2(3) . . ? C7 N1 Ni1 128.5(2) . . ? C7 N1 C9 106.1(3) . . ? C9 N1 Ni1 125.5(2) . . ? C31 N2 Ni1 129.7(3) . . ? C31 N2 C33 106.1(3) . . ? C33 N2 Ni1 123.4(2) . . ? C2 C1 Ni1 124.3(3) . . ? C6 C1 Ni1 116.5(3) . . ? C6 C1 C2 119.0(4) . . ? C1 C2 H2 119.9 . . ? C1 C2 C3 120.1(4) . . ? C3 C2 H2 119.9 . . ? C2 C3 H3 120.2 . . ? C4 C3 C2 119.6(4) . . ? C4 C3 H3 120.2 . . ? C3 C4 H4 119.9 . . ? C5 C4 C3 120.3(4) . . ? C5 C4 H4 119.9 . . ? C4 C5 H5 119.9 . . ? C4 C5 C6 120.3(4) . . ? C6 C5 H5 119.9 . . ? C1 C6 C5 120.6(4) . . ? C1 C6 H6 119.7 . . ? C5 C6 H6 119.7 . . ? O1 C7 C28 113.1(3) . . ? N1 C7 O1 117.4(3) . . ? N1 C7 C28 129.4(3) . . ? O1 C8 C9 100.5(3) . . ? O1 C8 C16 104.4(3) . . ? O1 C8 C22 109.1(3) . . ? C16 C8 C9 113.9(3) . . ? C22 C8 C9 115.7(3) . . ? C22 C8 C16 111.8(3) . . ? N1 C9 C8 100.9(3) . . ? N1 C9 H9 110.2 . . ? N1 C9 C10 110.4(3) . . ? C8 C9 H9 110.2 . . ? C10 C9 C8 114.7(3) . . ? C10 C9 H9 110.2 . . ? C11 C10 C9 123.2(3) . . ? C11 C10 C15 118.8(4) . . ? C15 C10 C9 118.0(4) . . ? C10 C11 H11 119.8 . . ? C12 C11 C10 120.4(4) . . ? C12 C11 H11 119.8 . . ? C11 C12 H12 119.7 . . ? C13 C12 C11 120.7(4) . . ? C13 C12 H12 119.7 . . ? C12 C13 H13 120.3 . . ? C12 C13 C14 119.3(4) . . ? C14 C13 H13 120.3 . . ? C13 C14 H14 119.7 . . ? C15 C14 C13 120.6(4) . . ? C15 C14 H14 119.7 . . ? C10 C15 H15 119.9 . . ? C14 C15 C10 120.3(4) . . ? C14 C15 H15 119.9 . . ? C17 C16 C8 122.9(3) . . ? C17 C16 C21 119.1(4) . . ? C21 C16 C8 117.8(3) . . ? C16 C17 H17 120.0 . . ? C18 C17 C16 120.1(4) . . ? C18 C17 H17 120.0 . . ? C17 C18 H18 119.7 . . ? C17 C18 C19 120.6(4) . . ? C19 C18 H18 119.7 . . ? C18 C19 H19 120.3 . . ? C18 C19 C20 119.5(4) . . ? C20 C19 H19 120.3 . . ? C19 C20 H20 120.0 . . ? C21 C20 C19 120.0(4) . . ? C21 C20 H20 120.0 . . ? C16 C21 H21 119.6 . . ? C20 C21 C16 120.8(4) . . ? C20 C21 H21 119.6 . . ? C23 C22 C8 118.1(3) . . ? C27 C22 C8 122.9(3) . . ? C27 C22 C23 119.0(3) . . ? C22 C23 H23 119.8 . . ? C24 C23 C22 120.3(4) . . ? C24 C23 H23 119.8 . . ? C23 C24 H24 119.8 . . ? C23 C24 C25 120.3(4) . . ? C25 C24 H24 119.8 . . ? C24 C25 H25 120.2 . . ? C26 C25 C24 119.5(4) . . ? C26 C25 H25 120.2 . . ? C25 C26 H26 119.7 . . ? C25 C26 C27 120.5(4) . . ? C27 C26 H26 119.7 . . ? C22 C27 C26 120.3(4) . . ? C22 C27 H27 119.9 . . ? C26 C27 H27 119.9 . . ? C7 C28 C29 108.6(3) . . ? C7 C28 C30 109.0(3) . . ? C29 C28 C30 110.3(4) . . ? C31 C28 C7 111.4(3) . . ? C31 C28 C29 109.4(3) . . ? C31 C28 C30 108.1(3) . . ? C28 C29 H29A 109.5 . . ? C28 C29 H29B 109.5 . . ? C28 C29 H29C 109.5 . . ? H29A C29 H29B 109.5 . . ? H29A C29 H29C 109.5 . . ? H29B C29 H29C 109.5 . . ? C28 C30 H30A 109.5 . . ? C28 C30 H30B 109.5 . . ? C28 C30 H30C 109.5 . . ? H30A C30 H30B 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? O2 C31 C28 113.3(3) . . ? N2 C31 O2 116.7(3) . . ? N2 C31 C28 130.0(3) . . ? O2 C32 C33 100.4(3) . . ? O2 C32 C40 107.3(3) . . ? O2 C32 C46 107.3(3) . . ? C40 C32 C33 117.1(3) . . ? C40 C32 C46 113.2(3) . . ? C46 C32 C33 110.3(3) . . ? N2 C33 C32 101.8(3) . . ? N2 C33 H33 109.7 . . ? N2 C33 C34 109.2(3) . . ? C32 C33 H33 109.7 . . ? C34 C33 C32 116.4(3) . . ? C34 C33 H33 109.7 . . ? C35 C34 C33 123.2(3) . . ? C39 C34 C33 117.9(3) . . ? C39 C34 C35 118.9(4) . . ? C34 C35 H35 120.2 . . ? C34 C35 C36 119.5(4) . . ? C36 C35 H35 120.2 . . ? C35 C36 H36 119.5 . . ? C37 C36 C35 120.9(4) . . ? C37 C36 H36 119.5 . . ? C36 C37 H37 120.2 . . ? C36 C37 C38 119.7(4) . . ? C38 C37 H37 120.2 . . ? C37 C38 H38 119.8 . . ? C37 C38 C39 120.3(4) . . ? C39 C38 H38 119.8 . . ? C34 C39 H39 119.7 . . ? C38 C39 C34 120.6(4) . . ? C38 C39 H39 119.7 . . ? C41 C40 C32 120.3(3) . . ? C45 C40 C32 121.0(3) . . ? C45 C40 C41 118.7(3) . . ? C40 C41 H41 119.7 . . ? C42 C41 C40 120.6(3) . . ? C42 C41 H41 119.7 . . ? C41 C42 H42 119.7 . . ? C41 C42 C43 120.6(4) . . ? C43 C42 H42 119.7 . . ? C42 C43 H43 120.5 . . ? C44 C43 C42 118.9(4) . . ? C44 C43 H43 120.5 . . ? C43 C44 H44 119.5 . . ? C43 C44 C45 121.0(4) . . ? C45 C44 H44 119.5 . . ? C40 C45 H45 119.9 . . ? C44 C45 C40 120.2(4) . . ? C44 C45 H45 119.9 . . ? C47 C46 C32 120.6(3) . . ? C51 C46 C32 120.3(3) . . ? C51 C46 C47 119.0(4) . . ? C46 C47 H47 119.7 . . ? C48 C47 C46 120.5(4) . . ? C48 C47 H47 119.7 . . ? C47 C48 H48 120.0 . . ? C49 C48 C47 120.1(4) . . ? C49 C48 H48 120.0 . . ? C48 C49 H49 120.0 . . ? C50 C49 C48 120.1(4) . . ? C50 C49 H49 120.0 . . ? C49 C50 H50 119.9 . . ? C49 C50 C51 120.1(4) . . ? C51 C50 H50 119.9 . . ? C46 C51 C50 120.2(4) . . ? C46 C51 H51 119.9 . . ? C50 C51 H51 119.9 . . ? C55 O00I C52 107.1(5) . . ? O00I C52 H52A 110.5 . . ? O00I C52 H52B 110.5 . . ? O00I C52 C53 106.2(5) . . ? H52A C52 H52B 108.7 . . ? C53 C52 H52A 110.5 . . ? C53 C52 H52B 110.5 . . ? C52 C53 H53A 110.8 . . ? C52 C53 H53B 110.8 . . ? C52 C53 C54 104.8(6) . . ? H53A C53 H53B 108.9 . . ? C54 C53 H53A 110.8 . . ? C54 C53 H53B 110.8 . . ? C53 C54 H54A 111.6 . . ? C53 C54 H54B 111.6 . . ? H54A C54 H54B 109.4 . . ? C55 C54 C53 100.7(6) . . ? C55 C54 H54A 111.6 . . ? C55 C54 H54B 111.6 . . ? O00I C55 C54 109.7(6) . . ? O00I C55 H55A 109.7 . . ? O00I C55 H55B 109.7 . . ? C54 C55 H55A 109.7 . . ? C54 C55 H55B 109.7 . . ? H55A C55 H55B 108.2 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Br1 Ni1 N1 C7 173.8(3) . . . . ? Br1 Ni1 N1 C9 -8.3(3) . . . . ? Br1 Ni1 N2 C31 -117.5(4) . . . . ? Br1 Ni1 N2 C33 51.4(5) . . . . ? Br1 Ni1 C1 C2 -75.5(3) . . . . ? Br1 Ni1 C1 C6 110.0(3) . . . . ? Ni1 N1 C7 O1 -177.8(2) . . . . ? Ni1 N1 C7 C28 1.5(6) . . . . ? Ni1 N1 C9 C8 158.5(2) . . . . ? Ni1 N1 C9 C10 -79.7(3) . . . . ? Ni1 N2 C31 O2 178.7(2) . . . . ? Ni1 N2 C31 C28 -0.9(6) . . . . ? Ni1 N2 C33 C32 165.7(2) . . . . ? Ni1 N2 C33 C34 -70.7(3) . . . . ? Ni1 C1 C2 C3 -171.6(3) . . . . ? Ni1 C1 C6 C5 174.2(3) . . . . ? O1 C7 C28 C29 46.6(4) . . . . ? O1 C7 C28 C30 -73.6(4) . . . . ? O1 C7 C28 C31 167.2(3) . . . . ? O1 C8 C9 N1 31.9(3) . . . . ? O1 C8 C9 C10 -86.8(3) . . . . ? O1 C8 C16 C17 -99.5(4) . . . . ? O1 C8 C16 C21 74.6(4) . . . . ? O1 C8 C22 C23 -175.0(3) . . . . ? O1 C8 C22 C27 4.3(5) . . . . ? O2 C32 C33 N2 28.3(3) . . . . ? O2 C32 C33 C34 -90.3(3) . . . . ? O2 C32 C40 C41 39.1(4) . . . . ? O2 C32 C40 C45 -142.6(3) . . . . ? O2 C32 C46 C47 -158.7(3) . . . . ? O2 C32 C46 C51 24.2(4) . . . . ? N1 Ni1 N2 C31 -8.0(3) . . . . ? N1 Ni1 N2 C33 160.9(3) . . . . ? N1 Ni1 C1 C2 179.0(7) . . . . ? N1 Ni1 C1 C6 4.5(10) . . . . ? N1 C7 C28 C29 -132.6(4) . . . . ? N1 C7 C28 C30 107.2(4) . . . . ? N1 C7 C28 C31 -12.0(5) . . . . ? N1 C9 C10 C11 -38.6(5) . . . . ? N1 C9 C10 C15 143.5(3) . . . . ? N2 Ni1 N1 C7 7.7(3) . . . . ? N2 Ni1 N1 C9 -174.4(3) . . . . ? N2 Ni1 C1 C2 90.1(3) . . . . ? N2 Ni1 C1 C6 -84.4(3) . . . . ? N2 C33 C34 C35 -21.8(5) . . . . ? N2 C33 C34 C39 159.8(3) . . . . ? C1 Ni1 N1 C7 -81.4(9) . . . . ? C1 Ni1 N1 C9 96.5(9) . . . . ? C1 Ni1 N2 C31 162.3(3) . . . . ? C1 Ni1 N2 C33 -28.9(3) . . . . ? C1 C2 C3 C4 -2.3(6) . . . . ? C2 C1 C6 C5 -0.6(6) . . . . ? C2 C3 C4 C5 -0.4(6) . . . . ? C3 C4 C5 C6 2.6(7) . . . . ? C4 C5 C6 C1 -2.1(6) . . . . ? C6 C1 C2 C3 2.8(6) . . . . ? C7 O1 C8 C9 -30.4(3) . . . . ? C7 O1 C8 C16 87.9(3) . . . . ? C7 O1 C8 C22 -152.4(3) . . . . ? C7 N1 C9 C8 -23.2(3) . . . . ? C7 N1 C9 C10 98.5(3) . . . . ? C7 C28 C31 O2 -167.7(3) . . . . ? C7 C28 C31 N2 11.9(5) . . . . ? C8 O1 C7 N1 18.0(4) . . . . ? C8 O1 C7 C28 -161.3(3) . . . . ? C8 C9 C10 C11 74.6(5) . . . . ? C8 C9 C10 C15 -103.4(4) . . . . ? C8 C16 C17 C18 173.7(4) . . . . ? C8 C16 C21 C20 -174.2(4) . . . . ? C8 C22 C23 C24 177.0(4) . . . . ? C8 C22 C27 C26 -176.9(4) . . . . ? C9 N1 C7 O1 4.0(4) . . . . ? C9 N1 C7 C28 -176.8(3) . . . . ? C9 C8 C16 C17 9.1(5) . . . . ? C9 C8 C16 C21 -176.8(3) . . . . ? C9 C8 C22 C23 72.7(4) . . . . ? C9 C8 C22 C27 -108.1(4) . . . . ? C9 C10 C11 C12 -177.2(4) . . . . ? C9 C10 C15 C14 177.6(4) . . . . ? C10 C11 C12 C13 -1.4(7) . . . . ? C11 C10 C15 C14 -0.5(6) . . . . ? C11 C12 C13 C14 1.6(7) . . . . ? C12 C13 C14 C15 -1.3(7) . . . . ? C13 C14 C15 C10 0.7(7) . . . . ? C15 C10 C11 C12 0.8(6) . . . . ? C16 C8 C9 N1 -79.2(3) . . . . ? C16 C8 C9 C10 162.2(3) . . . . ? C16 C8 C22 C23 -60.0(4) . . . . ? C16 C8 C22 C27 119.2(4) . . . . ? C16 C17 C18 C19 -0.8(6) . . . . ? C17 C16 C21 C20 0.2(6) . . . . ? C17 C18 C19 C20 2.0(7) . . . . ? C18 C19 C20 C21 -2.1(7) . . . . ? C19 C20 C21 C16 1.1(7) . . . . ? C21 C16 C17 C18 -0.3(6) . . . . ? C22 C8 C9 N1 149.1(3) . . . . ? C22 C8 C9 C10 30.5(4) . . . . ? C22 C8 C16 C17 142.7(4) . . . . ? C22 C8 C16 C21 -43.2(4) . . . . ? C22 C23 C24 C25 0.5(6) . . . . ? C23 C22 C27 C26 2.4(6) . . . . ? C23 C24 C25 C26 1.3(6) . . . . ? C24 C25 C26 C27 -1.2(7) . . . . ? C25 C26 C27 C22 -0.7(7) . . . . ? C27 C22 C23 C24 -2.3(6) . . . . ? C29 C28 C31 O2 -47.5(4) . . . . ? C29 C28 C31 N2 132.1(4) . . . . ? C30 C28 C31 O2 72.6(4) . . . . ? C30 C28 C31 N2 -107.8(4) . . . . ? C31 O2 C32 C33 -24.7(3) . . . . ? C31 O2 C32 C40 -147.6(3) . . . . ? C31 O2 C32 C46 90.5(3) . . . . ? C31 N2 C33 C32 -23.2(3) . . . . ? C31 N2 C33 C34 100.4(3) . . . . ? C32 O2 C31 N2 11.7(4) . . . . ? C32 O2 C31 C28 -168.7(3) . . . . ? C32 C33 C34 C35 92.7(4) . . . . ? C32 C33 C34 C39 -85.7(4) . . . . ? C32 C40 C41 C42 178.2(3) . . . . ? C32 C40 C45 C44 -177.3(4) . . . . ? C32 C46 C47 C48 -176.3(3) . . . . ? C32 C46 C51 C50 178.0(3) . . . . ? C33 N2 C31 O2 8.3(4) . . . . ? C33 N2 C31 C28 -171.3(3) . . . . ? C33 C32 C40 C41 -72.8(4) . . . . ? C33 C32 C40 C45 105.5(4) . . . . ? C33 C32 C46 C47 -50.2(4) . . . . ? C33 C32 C46 C51 132.7(3) . . . . ? C33 C34 C35 C36 -178.1(4) . . . . ? C33 C34 C39 C38 177.2(4) . . . . ? C34 C35 C36 C37 1.0(7) . . . . ? C35 C34 C39 C38 -1.2(6) . . . . ? C35 C36 C37 C38 -1.3(7) . . . . ? C36 C37 C38 C39 0.3(7) . . . . ? C37 C38 C39 C34 1.0(7) . . . . ? C39 C34 C35 C36 0.2(6) . . . . ? C40 C32 C33 N2 144.1(3) . . . . ? C40 C32 C33 C34 25.5(4) . . . . ? C40 C32 C46 C47 83.1(4) . . . . ? C40 C32 C46 C51 -94.0(4) . . . . ? C40 C41 C42 C43 -0.1(6) . . . . ? C41 C40 C45 C44 1.0(6) . . . . ? C41 C42 C43 C44 -0.5(6) . . . . ? C42 C43 C44 C45 1.4(7) . . . . ? C43 C44 C45 C40 -1.6(7) . . . . ? C45 C40 C41 C42 -0.1(6) . . . . ? C46 C32 C33 N2 -84.7(3) . . . . ? C46 C32 C33 C34 156.7(3) . . . . ? C46 C32 C40 C41 157.3(3) . . . . ? C46 C32 C40 C45 -24.4(5) . . . . ? C46 C47 C48 C49 -1.7(6) . . . . ? C47 C46 C51 C50 0.8(6) . . . . ? C47 C48 C49 C50 0.8(6) . . . . ? C48 C49 C50 C51 0.9(6) . . . . ? C49 C50 C51 C46 -1.7(6) . . . . ? C51 C46 C47 C48 0.9(6) . . . . ? O00I C52 C53 C54 -27.9(7) . . . . ? C52 O00I C55 C54 11.8(8) . . . . ? C52 C53 C54 C55 33.3(8) . . . . ? C53 C54 C55 O00I -28.3(9) . . . . ? C55 O00I C52 C53 10.2(7) . . . . ? _iucr_refine_instructions_details ; TITL cu_p17216_0m_a.res in P2(1)2(1)2(1) REM Old TITL cu_p17216_0m in P222 #16 REM SHELXT solution in P2(1)2(1)2(1) REM R1 0.098, Rweak 0.029, Alpha 0.005, Orientation as input REM Flack x = 0.057 ( 0.007 ) from Parsons' quotients REM Formula found by SHELXT: C55 N O4 Ni Br CELL 1.54184 9.754 17.1117 26.8304 90 90 90 ZERR 4 0.0005 0.0016 0.0031 0 0 0 LATT -1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H Br N Ni O UNIT 220 204 4 8 4 12 L.S. 10 PLAN 20 SIZE 0.05 0.08 0.14 TEMP -173(2) BOND $H LIST 6 MORE -1 CONF fmap 2 acta TWIN -1 0 0 0 -1 0 0 0 -1 2 REM REM REM WGHT 0.052000 7.801000 BASF 0.05667 FVAR 0.27890 BR1 3 0.793943 0.518526 0.414579 11.00000 0.02031 0.01575 = 0.03869 -0.00421 0.00357 -0.00216 NI1 5 0.626910 0.423620 0.407306 11.00000 0.01643 0.01336 = 0.01878 -0.00338 -0.00077 0.00017 O1 6 0.273511 0.521252 0.469297 11.00000 0.02110 0.01020 = 0.02477 -0.00547 0.00345 -0.00132 O2 6 0.288548 0.291565 0.370963 11.00000 0.01632 0.01237 = 0.01718 -0.00395 0.00130 -0.00144 N1 4 0.480694 0.485067 0.440998 11.00000 0.01912 0.01069 = 0.01475 -0.00205 -0.00192 -0.00281 N2 4 0.489998 0.352127 0.383650 11.00000 0.02099 0.01461 = 0.01346 -0.00278 -0.00012 0.00256 C1 1 0.768406 0.354925 0.385361 11.00000 0.01590 0.02229 = 0.02006 -0.00273 -0.00162 -0.00246 C2 1 0.827423 0.357258 0.338301 11.00000 0.02219 0.02232 = 0.02120 -0.00045 -0.00275 -0.00322 AFIX 43 H2 2 0.806461 0.399017 0.316248 11.00000 -1.20000 AFIX 0 C3 1 0.917773 0.298202 0.323265 11.00000 0.02486 0.03760 = 0.02636 -0.01189 0.00520 0.00087 AFIX 43 H3 2 0.955621 0.298743 0.290642 11.00000 -1.20000 AFIX 0 C4 1 0.951774 0.238749 0.356374 11.00000 0.02920 0.02004 = 0.04170 -0.01012 0.00369 0.00460 AFIX 43 H4 2 1.012524 0.198371 0.346236 11.00000 -1.20000 AFIX 0 C5 1 0.898671 0.238173 0.402986 11.00000 0.02924 0.02282 = 0.04450 0.00026 0.00054 0.00304 AFIX 43 H5 2 0.925256 0.198622 0.425877 11.00000 -1.20000 AFIX 0 C6 1 0.804696 0.295651 0.417596 11.00000 0.02613 0.02646 = 0.02449 -0.00313 0.00077 0.00096 AFIX 43 H6 2 0.765593 0.293796 0.450003 11.00000 -1.20000 AFIX 0 C7 1 0.354584 0.468097 0.446117 11.00000 0.01847 0.01248 = 0.01374 -0.00190 0.00093 0.00270 C8 1 0.354115 0.594800 0.466582 11.00000 0.02294 0.00767 = 0.01859 -0.00245 0.00369 -0.00243 C9 1 0.501146 0.561825 0.467435 11.00000 0.02184 0.00885 = 0.01757 -0.00549 -0.00121 0.00123 AFIX 13 H9 2 0.563718 0.596224 0.447676 11.00000 -1.20000 AFIX 0 C10 1 0.559529 0.548411 0.519088 11.00000 0.02107 0.01889 = 0.01843 -0.00709 -0.00082 0.00162 C11 1 0.519907 0.486822 0.549497 11.00000 0.03592 0.02276 = 0.01849 0.00010 -0.00113 -0.00064 AFIX 43 H11 2 0.456124 0.449295 0.537530 11.00000 -1.20000 AFIX 0 C12 1 0.572701 0.479752 0.597098 11.00000 0.04239 0.02887 = 0.02092 0.00361 -0.00376 -0.00214 AFIX 43 H12 2 0.543335 0.437998 0.617849 11.00000 -1.20000 AFIX 0 C13 1 0.667672 0.532759 0.614786 11.00000 0.03572 0.04100 = 0.02182 -0.00334 -0.00633 0.00449 AFIX 43 H13 2 0.705392 0.526872 0.647214 11.00000 -1.20000 AFIX 0 C14 1 0.707449 0.594672 0.584747 11.00000 0.03361 0.03844 = 0.02876 -0.01125 -0.00809 -0.00551 AFIX 43 H14 2 0.771318 0.631946 0.596972 11.00000 -1.20000 AFIX 0 C15 1 0.655191 0.602581 0.537376 11.00000 0.03191 0.02320 = 0.02711 -0.00203 -0.00521 -0.00649 AFIX 43 H15 2 0.683969 0.644875 0.516965 11.00000 -1.20000 AFIX 0 C16 1 0.312936 0.631244 0.416571 11.00000 0.02314 0.01495 = 0.01818 -0.00132 -0.00271 -0.00053 C17 1 0.392519 0.624825 0.374005 11.00000 0.02417 0.02091 = 0.02418 0.00277 0.00254 -0.00005 AFIX 43 H17 2 0.480727 0.601452 0.375786 11.00000 -1.20000 AFIX 0 C18 1 0.343663 0.652427 0.328879 11.00000 0.03550 0.03106 = 0.02039 0.00542 0.00420 0.00192 AFIX 43 H18 2 0.399163 0.648443 0.299894 11.00000 -1.20000 AFIX 0 C19 1 0.214671 0.685786 0.325594 11.00000 0.04149 0.03368 = 0.02294 0.00549 -0.00476 0.00445 AFIX 43 H19 2 0.180490 0.703132 0.294339 11.00000 -1.20000 AFIX 0 C20 1 0.135566 0.693697 0.368392 11.00000 0.02562 0.03699 = 0.02686 0.00153 -0.00528 0.00334 AFIX 43 H20 2 0.048232 0.718123 0.366666 11.00000 -1.20000 AFIX 0 C21 1 0.183800 0.666148 0.413226 11.00000 0.02213 0.03533 = 0.02228 -0.00004 0.00191 0.00227 AFIX 43 H21 2 0.128676 0.670904 0.442259 11.00000 -1.20000 AFIX 0 C22 1 0.315558 0.646649 0.510157 11.00000 0.02498 0.01159 = 0.01693 -0.00586 -0.00309 0.00312 C23 1 0.372218 0.721776 0.512327 11.00000 0.02918 0.01582 = 0.02885 -0.00354 -0.00196 0.00196 AFIX 43 H23 2 0.436332 0.737906 0.487738 11.00000 -1.20000 AFIX 0 C24 1 0.335431 0.772396 0.549943 11.00000 0.02809 0.01968 = 0.03461 -0.00930 -0.00815 0.00628 AFIX 43 H24 2 0.373798 0.823396 0.551034 11.00000 -1.20000 AFIX 0 C25 1 0.242895 0.749324 0.586134 11.00000 0.04483 0.02793 = 0.02340 -0.01087 -0.00361 0.01546 AFIX 43 H25 2 0.216179 0.784649 0.611665 11.00000 -1.20000 AFIX 0 C26 1 0.189854 0.674900 0.584897 11.00000 0.05317 0.03320 = 0.02313 -0.00008 0.01233 0.00646 AFIX 43 H26 2 0.127626 0.658548 0.610059 11.00000 -1.20000 AFIX 0 C27 1 0.226579 0.623381 0.547105 11.00000 0.04648 0.01897 = 0.02286 -0.00084 0.00741 0.00175 AFIX 43 H27 2 0.190100 0.571907 0.546786 11.00000 -1.20000 AFIX 0 C28 1 0.277652 0.396174 0.429458 11.00000 0.02077 0.01209 = 0.01976 -0.00552 0.00299 -0.00734 C29 1 0.144857 0.422047 0.403147 11.00000 0.02648 0.03036 = 0.04760 -0.01861 -0.00601 0.00223 AFIX 137 H29A 2 0.085955 0.449669 0.426923 11.00000 -1.50000 H29B 2 0.096544 0.375990 0.390389 11.00000 -1.50000 H29C 2 0.167575 0.456947 0.375390 11.00000 -1.50000 AFIX 0 C30 1 0.243314 0.345421 0.475831 11.00000 0.05695 0.02311 = 0.02627 -0.00502 0.02176 -0.01394 AFIX 137 H30A 2 0.328361 0.324972 0.490256 11.00000 -1.50000 H30B 2 0.184292 0.301801 0.465841 11.00000 -1.50000 H30C 2 0.195631 0.377480 0.500642 11.00000 -1.50000 AFIX 0 C31 1 0.361804 0.347761 0.394457 11.00000 0.01718 0.01174 = 0.01313 -0.00076 -0.00238 -0.00079 C32 1 0.389226 0.240146 0.346581 11.00000 0.01758 0.01189 = 0.01542 -0.00289 0.00129 -0.00135 C33 1 0.512163 0.297614 0.340741 11.00000 0.02034 0.01481 = 0.01247 -0.00342 -0.00045 -0.00098 AFIX 13 H33 2 0.600341 0.268697 0.345366 11.00000 -1.20000 AFIX 0 C34 1 0.517501 0.344478 0.292678 11.00000 0.01953 0.01429 = 0.02001 -0.00079 0.00033 -0.00347 C35 1 0.460590 0.418803 0.287826 11.00000 0.02878 0.01822 = 0.02431 0.00252 0.00022 -0.00065 AFIX 43 H35 2 0.418107 0.443327 0.315584 11.00000 -1.20000 AFIX 0 C36 1 0.466456 0.456898 0.241945 11.00000 0.04024 0.02444 = 0.02777 0.00377 -0.00083 -0.00342 AFIX 43 H36 2 0.428980 0.507898 0.238764 11.00000 -1.20000 AFIX 0 C37 1 0.525701 0.421694 0.201255 11.00000 0.03687 0.03054 = 0.02428 0.00985 0.00200 -0.00956 AFIX 43 H37 2 0.527449 0.447799 0.170012 11.00000 -1.20000 AFIX 0 C38 1 0.582408 0.348544 0.205978 11.00000 0.04123 0.03696 = 0.01581 0.00184 0.00547 -0.00437 AFIX 43 H38 2 0.623783 0.324194 0.177937 11.00000 -1.20000 AFIX 0 C39 1 0.579548 0.310176 0.251369 11.00000 0.03423 0.02363 = 0.01936 -0.00217 0.00385 -0.00032 AFIX 43 H39 2 0.620291 0.259971 0.254377 11.00000 -1.20000 AFIX 0 C40 1 0.323594 0.209644 0.298961 11.00000 0.02063 0.01808 = 0.01477 -0.00192 -0.00089 -0.00307 C41 1 0.242485 0.258467 0.269870 11.00000 0.02236 0.01561 = 0.02133 -0.00360 -0.00061 0.00186 AFIX 43 H41 2 0.225945 0.310651 0.280350 11.00000 -1.20000 AFIX 0 C42 1 0.185614 0.231759 0.225784 11.00000 0.02683 0.02346 = 0.02346 0.00379 -0.00531 0.00046 AFIX 43 H42 2 0.130245 0.265750 0.206328 11.00000 -1.20000 AFIX 0 C43 1 0.208664 0.155939 0.209765 11.00000 0.03627 0.02769 = 0.01851 -0.00457 -0.00646 -0.00234 AFIX 43 H43 2 0.169006 0.137549 0.179628 11.00000 -1.20000 AFIX 0 C44 1 0.290063 0.107632 0.238264 11.00000 0.04703 0.02165 = 0.02274 -0.01022 -0.00589 0.00054 AFIX 43 H44 2 0.308086 0.055894 0.227219 11.00000 -1.20000 AFIX 0 C45 1 0.346180 0.133473 0.282919 11.00000 0.03370 0.01720 = 0.02409 -0.00249 -0.00687 0.00458 AFIX 43 H45 2 0.400139 0.098989 0.302546 11.00000 -1.20000 AFIX 0 C46 1 0.425233 0.175295 0.383631 11.00000 0.02360 0.01300 = 0.01695 -0.00215 -0.00383 -0.00260 C47 1 0.547204 0.133386 0.378879 11.00000 0.02560 0.02073 = 0.01989 -0.00400 -0.00126 -0.00134 AFIX 43 H47 2 0.611040 0.147228 0.353636 11.00000 -1.20000 AFIX 0 C48 1 0.576094 0.071529 0.410783 11.00000 0.03152 0.02114 = 0.03304 0.00020 -0.00894 0.00469 AFIX 43 H48 2 0.658230 0.042389 0.406698 11.00000 -1.20000 AFIX 0 C49 1 0.484908 0.052275 0.448659 11.00000 0.03950 0.02343 = 0.02714 0.00483 -0.01134 -0.00546 AFIX 43 H49 2 0.505346 0.010421 0.470704 11.00000 -1.20000 AFIX 0 C50 1 0.365378 0.093679 0.454235 11.00000 0.04598 0.02269 = 0.02093 0.00470 0.00054 -0.00684 AFIX 43 H50 2 0.303785 0.080913 0.480427 11.00000 -1.20000 AFIX 0 C51 1 0.333898 0.155016 0.421216 11.00000 0.03109 0.01750 = 0.02720 -0.00018 0.00129 -0.00348 AFIX 43 H51 2 0.249943 0.182642 0.424634 11.00000 -1.20000 AFIX 0 O00I 6 0.316641 0.477001 0.680075 11.00000 0.07524 0.04948 = 0.04124 -0.01323 0.00507 -0.00673 C52 1 0.358629 0.557308 0.687753 11.00000 0.05387 0.03626 = 0.05457 -0.00324 0.00476 0.00397 AFIX 23 H52A 2 0.278321 0.590445 0.695658 11.00000 -1.20000 H52B 2 0.403592 0.578143 0.657459 11.00000 -1.20000 AFIX 0 C53 1 0.456502 0.556246 0.730312 11.00000 0.05995 0.06007 = 0.06822 -0.02009 -0.00673 -0.00222 AFIX 23 H53A 2 0.449500 0.605007 0.750008 11.00000 -1.20000 H53B 2 0.551941 0.550421 0.718318 11.00000 -1.20000 AFIX 0 C54 1 0.414692 0.487126 0.760878 11.00000 0.09800 0.09268 = 0.07239 -0.00899 -0.01636 0.02959 AFIX 23 H54A 2 0.493257 0.464892 0.779443 11.00000 -1.20000 H54B 2 0.340420 0.500474 0.784542 11.00000 -1.20000 AFIX 0 C55 1 0.366066 0.433222 0.721253 11.00000 0.15724 0.04683 = 0.04854 0.00547 0.01528 0.02259 AFIX 23 H55A 2 0.442353 0.399081 0.710379 11.00000 -1.20000 H55B 2 0.291883 0.399624 0.734483 11.00000 -1.20000 HKLF 4 REM cu_p17216_0m_a.res in P2(1)2(1)2(1) REM R1 = 0.0452 for 7993 Fo > 4sig(Fo) and 0.0501 for all 8614 data REM 562 parameters refined using 0 restraints END WGHT 0.0518 7.8723 REM Highest difference peak 1.552, deepest hole -0.603, 1-sigma level 0.081 Q1 1 0.5933 0.3227 0.4866 11.00000 0.05 1.55 Q2 1 0.7725 0.5167 0.3798 11.00000 0.05 1.51 Q3 1 0.6887 0.5218 0.4126 11.00000 0.05 0.78 Q4 1 0.8943 0.5220 0.4150 11.00000 0.05 0.72 Q5 1 0.4778 0.4694 0.7322 11.00000 0.05 0.71 Q6 1 0.7894 0.5166 0.4557 11.00000 0.05 0.67 Q7 1 0.7245 0.4330 0.4050 11.00000 0.05 0.60 Q8 1 0.6311 0.4217 0.4466 11.00000 0.05 0.53 Q9 1 0.5274 0.4258 0.4089 11.00000 0.05 0.52 Q10 1 0.6299 0.4231 0.3685 11.00000 0.05 0.48 Q11 1 0.7182 0.4576 0.4434 11.00000 0.05 0.38 Q12 1 0.5867 0.3188 0.3372 11.00000 0.05 0.33 Q13 1 0.5039 0.4792 0.4834 11.00000 0.05 0.33 Q14 1 0.7193 0.5777 0.4456 11.00000 0.05 0.32 Q15 1 0.5973 0.6381 0.4869 11.00000 0.05 0.31 Q16 1 -0.0131 0.3211 0.4834 11.00000 0.05 0.31 Q17 1 1.1031 0.1792 0.3091 11.00000 0.05 0.30 Q18 1 0.6820 0.3622 0.3779 11.00000 0.05 0.29 Q19 1 0.5649 0.5480 0.4871 11.00000 0.05 0.28 Q20 1 0.7483 0.5795 0.3797 11.00000 0.05 0.27 REM The information below was added by Olex2. REM REM R1 = 0.0452 for 7993 Fo > 4sig(Fo) and 0.0501 for all 32255 data REM n/a parameters refined using n/a restraints REM Highest difference peak 1.55, deepest hole -0.60 REM Mean Shift 0, Max Shift 0.001. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0501 REM R1_gt = 0.0452 REM wR_ref = 0.1144 REM GOOF = 1.029 REM Shift_max = 0.001 REM Shift_mean = 0 REM Reflections_all = 32255 REM Reflections_gt = 7993 REM Parameters = n/a REM Hole = -0.60 REM Peak = 1.55 REM Flack = 0.00(2) ; _olex2_date_sample_data_collection 2017-04-26 _olex2_date_sample_submission 2017-04-22 _olex2_submission_original_sample_id HLY-I-252 _olex2_submission_special_instructions 'No special instructions were received' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma 1 0 0 -0.6 1 1 0 0 -0.6 1.3 -1 0 0 0.3 1.2 2 0 0 2753.22 137.79 -2 0 0 3082.59 138.59 2 0 0 3114.99 138.69 5 0 0 3.1 8.9 5 0 0 1.6 3.9 -5 0 0 5.5 3.1 -6 0 0 544.35 26.6 -6 0 0 531.75 28.2 7 0 0 11.5 7.6 8 0 0 8.6 4 8 0 0 16.1 9.3 8 0 0 7.5 3.3 -8 0 0 4 4.9 -8 0 0 4.4 3.7 -9 0 0 -3 4.3 9 0 0 -9 11.4 9 0 0 -5.3 3.9 -10 0 0 115.79 9.5 10 0 0 113.39 9.5 10 0 0 161.08 37.2 11 0 0 2.1 3.3 -11 0 0 5.8 3.2 1 -1 0 280.57 14.1 -1 -1 0 298.97 14.6 -1 1 0 302.37 14.4 1 1 0 282.27 14.2 1 1 0 302.37 14.6 1 -1 0 300.37 14.4 -2 1 0 201.98 11 2 -1 0 206.88 11.3 2 -1 0 177.88 10.4 2 1 0 192.38 11.4 -2 -1 0 182.38 11.1 3 1 0 131.19 8.3 3 -1 0 99.19 7.9 3 -1 0 114.99 9.5 3 1 0 118.69 9.8 -3 1 0 121.19 9.3 4 1 0 247.98 14.3 4 -1 0 251.17 17.1 4 1 0 251.07 17.1 -4 -1 0 244.78 16.1 -4 1 0 247.58 15.9 4 -1 0 236.08 14.2 5 -1 0 33.5 8.1 5 1 0 33.5 7.8 -5 1 0 24 7.9 5 -1 0 22.7 8.1 5 1 0 24.8 9.5 -5 -1 0 18.8 3.9 5 1 0 28.3 4.6 6 -1 0 240.78 17.6 -6 -1 0 292.47 14.3 -6 -1 0 288.87 16 6 1 0 232.78 14.8 -6 1 0 229.68 25.7 -6 -1 0 243.48 13.9 -6 1 0 238.88 14.2 8 -1 0 14.9 9.3 8 1 0 16.3 3.6 -8 1 0 16.1 4.1 8 1 0 19.9 9.5 -8 1 0 28.4 5.8 8 -1 0 11.1 3.5 -8 -1 0 17.3 4.7 8 -1 0 10.4 4 -9 -1 0 162.28 13.1 -9 1 0 139.89 11.9 9 1 0 148.99 11.7 9 -1 0 116.39 17.8 9 -1 0 129.19 11.8 9 1 0 139.09 22.7 -10 -1 0 5.4 4.2 10 1 0 5.5 4.2 10 -1 0 7.6 4.1 -10 1 0 3.4 3.6 11 -1 0 151.48 9.8 -11 -1 0 143.39 9.5 -11 1 0 155.58 9.5 11 1 0 150.88 9.9 -12 -1 0 3.7 3.7 12 -1 0 2.3 5.5 0 2 0 1536.75 71.49 1 2 0 12.6 2.8 1 -2 0 8.2 1.9 -1 2 0 5.9 1.8 1 -2 0 9.1 1.8 1 2 0 7 1.8 2 -2 0 330.07 18 -2 2 0 363.86 18.6 2 2 0 388.86 19.2 2 2 0 349.47 18.1 2 -2 0 373.76 18.8 -2 -2 0 376.66 19 3 2 0 450.45 22.5 -3 -2 0 463.45 23.9 3 -2 0 414.86 22.4 3 2 0 447.36 23.9 -3 2 0 459.95 23.4 3 -2 0 451.35 23.7 4 -2 0 208.38 15.4 -4 2 0 201.88 14.3 4 2 0 216.08 13 -4 -2 0 219.48 15.1 4 2 0 208.08 18.3 4 -2 0 209.78 12.9 5 2 0 13.5 9.6 5 -2 0 40.8 8.2 5 -2 0 26.7 9 6 -2 0 195.78 15.8 -6 2 0 156.08 11.6 6 2 0 202.28 14.1 -6 2 0 167.28 23.7 -6 2 0 169.08 10.5 6 -2 0 193.28 11.2 -6 -2 0 152.98 10.2 -6 -2 0 167.68 10.7 -7 -2 0 9.4 4 -7 2 0 6.5 3.2 7 2 0 5.2 2.8 -7 -2 0 9.2 3.6 7 2 0 4.7 6.7 -7 2 0 4.5 4.8 7 -2 0 0.7 7.5 7 -2 0 3.9 2.8 7 -2 0 8.8 3.2 8 -2 0 16 10.5 8 2 0 18.9 8.6 9 -2 0 218.18 19.2 9 -2 0 268.97 28.9 9 2 0 243.28 23.9 10 2 0 44.9 7 -10 2 0 34.6 6.7 -10 -2 0 41.1 7 10 -2 0 42.2 7.2 -11 -2 0 37 5.7 11 2 0 30.4 6.3 11 -2 0 41.3 6 -11 2 0 43.2 5.4 0 3 0 1.1 1.7 1 -3 0 685.43 35.2 1 -3 0 777.82 35.7 1 3 0 768.72 35.3 -1 3 0 765.82 35.6 -2 3 0 1045.3 48.8 2 3 0 971.4 48.2 2 3 0 1052.09 49.4 2 -3 0 1062.29 49 2 -3 0 990.7 48.3 3 -3 0 721.43 35.9 3 -3 0 753.12 37.1 -3 3 0 754.32 36.8 3 3 0 737.73 35.9 -4 3 0 85.59 9.6 4 3 0 83.59 12.5 4 -3 0 66.99 8.1 4 -3 0 67.59 11.3 4 3 0 94.99 8.3 -5 3 0 10.5 6.3 -5 -3 0 5.5 3.4 5 3 0 12.4 4.8 5 3 0 -7.3 10.5 5 -3 0 7 4.8 -5 -3 0 8.4 2.5 5 -3 0 12.7 10 -6 -3 0 99.89 7.3 -6 -3 0 87.09 11.4 -6 -3 0 104.79 8 6 -3 0 118.29 7.7 6 3 0 116.39 11.8 -6 3 0 94.59 17 6 -3 0 100.09 13.8 -6 3 0 110.59 7.8 7 3 0 16.9 7 7 -3 0 17.9 4.2 -7 -3 0 20.2 4 -7 3 0 17.5 3.9 7 -3 0 9.4 3.3 -7 -3 0 17.5 3.9 7 -3 0 19.2 9.6 7 3 0 13 3.2 -7 -3 0 14.9 4.2 -8 -3 0 131.89 10.7 -8 -3 0 138.49 10.5 8 -3 0 124.99 21.8 -8 3 0 146.19 10.7 8 -3 0 139.59 10.8 8 3 0 159.38 17.5 -9 -3 0 81.99 9 -9 3 0 86.39 9 9 3 0 83.39 9.4 -9 -3 0 72.39 9.4 9 -3 0 81.19 9.3 9 3 0 57.79 12.7 10 -3 0 79.79 7.9 10 3 0 65.89 7.6 -10 3 0 66.99 7.2 -10 -3 0 66.69 7.8 -10 -3 0 60.09 10.8 11 -3 0 182.58 11 -11 -3 0 187.18 10.8 11 3 0 165.78 13.8 -11 3 0 180.68 10.6 0 4 0 49.2 5.2 1 -4 0 95.09 6.8 1 -4 0 99.09 7.1 1 4 0 100.39 6.6 -1 4 0 97.29 7.1 2 4 0 7.9 2.7 -2 4 0 0 2.7 2 -4 0 0.6 2.7 2 -4 0 2.4 2.9 2 4 0 6.6 3.8 3 -4 0 190.58 13.1 3 4 0 180.58 11.3 -3 4 0 192.48 12.1 3 4 0 182.18 13.5 3 -4 0 182.38 11.7 4 -4 0 590.24 31.3 4 4 0 616.34 28.6 -4 4 0 573.64 30.1 4 -4 0 560.64 28.6 -4 4 0 471.65 26.8 4 4 0 535.95 31.6 -5 -4 0 96.49 6.9 -5 -4 0 89.69 6.1 5 -4 0 89.39 6.7 -5 4 0 82.19 6.5 5 -4 0 82.39 10.8 5 4 0 86.29 9.7 5 -4 0 61.29 14 -5 -4 0 98.39 8.2 5 4 0 89.09 6.6 5 -4 0 79.99 7.2 -5 4 0 88.39 14.7 -6 -4 0 101.09 8.3 -6 -4 0 93.09 6.6 6 4 0 100.09 11.4 -6 -4 0 98.59 7.4 -6 4 0 80.59 7.1 6 -4 0 92.29 7.2 6 -4 0 88.99 7.9 6 -4 0 96.79 14 7 -4 0 12.8 10.1 7 -4 0 13.2 3.8 -7 -4 0 9 4.3 -8 -4 0 106.99 9.4 -8 4 0 121.59 9.7 -8 -4 0 122.99 10.2 8 4 0 104.49 17.2 8 -4 0 111.49 9.8 8 -4 0 124.19 23.9 -9 -4 0 42.8 7.9 -9 4 0 40.8 7.3 9 -4 0 37.3 7.5 9 4 0 19.5 12.3 9 -4 0 46.1 18.8 10 -4 0 154.88 10.8 10 4 0 159.08 10.9 -10 4 0 171.98 10.4 -10 -4 0 137.09 11.9 -10 -4 0 167.88 11.2 -11 4 0 19.7 3.3 11 4 0 20 4.3 -11 -4 0 23.7 4.1 11 -4 0 27.7 5.6 0 5 0 0.7 2.6 -1 5 0 32.3 5.3 1 -5 0 27.1 5.2 1 -5 0 25.2 5.4 2 -5 0 316.77 17 2 5 0 300.77 15.9 2 -5 0 280.27 16.3 -2 5 0 317.17 16.6 2 5 0 298.27 17.4 -4 -5 0 865.71 41.8 4 5 0 792.52 47 -4 5 0 908.91 45.1 4 -5 0 901.11 44 4 -5 0 904.41 46.4 -4 -5 0 859.61 42 4 5 0 949.01 43.7 -4 -5 0 876.81 42.7 4 -5 0 911.21 42.4 -4 5 0 890.51 42 4 -5 0 890.91 42 5 -5 0 302.47 15.8 5 -5 0 327.57 20 -5 -5 0 306.07 17 5 5 0 320.87 18.7 5 -5 0 310.17 30.7 5 5 0 318.17 15.9 5 -5 0 308.37 16.5 -5 -5 0 311.67 15.6 -5 5 0 292.07 15.9 -5 5 0 262.47 23.3 -5 -5 0 317.87 16 -6 -5 0 17.1 4.2 6 -5 0 14.1 3.3 -6 -5 0 16.6 2.9 6 5 0 12.8 6.2 6 5 0 16.6 3.7 6 -5 0 10.8 9.8 6 -5 0 14.6 3.8 -6 5 0 13.7 3.3 -6 -5 0 16.2 3.5 7 -5 0 162.08 10.6 7 5 0 193.18 16.6 -7 -5 0 167.18 10.2 7 -5 0 213.28 23.1 -7 5 0 143.69 10.8 -7 -5 0 172.78 12.1 -7 -5 0 155.58 10.8 7 -5 0 155.58 12 8 -5 0 40.9 7.4 8 -5 0 18.9 16 -8 5 0 41.3 6.8 8 5 0 39 9.8 -8 -5 0 49.7 7.4 -8 -5 0 43.5 8.4 -9 -5 0 374.56 19.6 9 5 0 350.66 28.1 9 -5 0 260.47 46.9 -9 5 0 355.96 19.3 -9 -5 0 381.46 20.2 9 5 0 361.36 19.9 9 -5 0 381.86 20.1 -10 -5 0 56.09 8.2 10 5 0 53.29 7 -10 5 0 75.89 6.9 10 -5 0 75.19 7.6 -10 -5 0 56.19 7.6 -11 -5 0 1.9 3.2 -11 5 0 5.1 3.3 11 -5 0 -2.8 3.9 11 5 0 4.6 4.6 0 6 0 244.68 14 1 -6 0 850.31 43.1 -1 6 0 953.1 43.8 2 -6 0 531.65 28.8 2 -6 0 597.74 29.7 2 6 0 568.64 30.1 -2 6 0 588.94 29.2 2 6 0 590.64 28.4 3 -6 0 1195.78 59.09 -3 -6 0 1158.48 56.09 -3 -6 0 1229.88 56.29 3 -6 0 1181.78 57.79 3 6 0 1249.07 57.49 -3 6 0 1189.88 58.39 -4 6 0 985.4 46.9 4 -6 0 963.4 47.3 4 -6 0 943.11 46.9 4 -6 0 996.1 52.39 -4 -6 0 996 46.7 4 6 0 1095.89 48.8 -4 -6 0 1040.4 47 4 -6 0 950.4 49.1 -4 -6 0 953.6 47.8 -4 6 0 1025.4 50.49 4 6 0 986.9 53.99 5 -6 0 312.57 16.9 5 6 0 323.07 19.2 5 -6 0 326.67 16.4 5 6 0 290.07 17.6 -5 6 0 295.87 16.4 5 -6 0 348.87 21.9 -5 -6 0 320.47 17.8 6 -6 0 48.7 5.9 6 -6 0 45.6 6.9 -6 -6 0 51.69 7.7 6 -6 0 62.79 15.3 -6 -6 0 49.3 6.5 -6 6 0 47.6 6 -6 -6 0 42.3 5.6 6 6 0 41.8 7.9 -7 -6 0 45.2 8.5 7 -6 0 20.9 14.1 -7 -6 0 49.2 6.7 -7 6 0 55.39 7 -7 -6 0 49.9 6.2 7 6 0 40.2 9.1 7 -6 0 60.19 7.3 -8 -6 0 467.05 24 8 -6 0 480.05 24.6 -8 -6 0 492.35 25.1 -8 -6 0 460.25 24.1 -8 6 0 453.85 24 8 -6 0 428.36 42.9 9 -6 0 15.6 4.5 -9 -6 0 16.8 4.4 -9 -6 0 18.3 4.6 9 6 0 7.4 11.9 9 6 0 18.7 4.8 -10 -6 0 203.18 12.8 10 6 0 203.48 12.9 -10 -6 0 181.18 12.6 10 -6 0 220.08 12.7 -10 6 0 222.98 11.8 11 -6 0 10.4 3.4 -11 -6 0 1.6 3.7 0 7 0 -4.2 3.2 -1 7 0 2.1 3.4 1 7 0 -3.1 3.9 1 -7 0 2.3 4.1 2 -7 0 46 10.2 2 -7 0 53.79 9.1 2 7 0 45.6 6.7 -3 7 0 303.67 16 3 7 0 362.76 18 3 7 0 298.27 22.4 3 -7 0 304.07 19.6 -3 7 0 327.67 19.6 3 -7 0 306.57 21.6 -3 -7 0 311.57 15.9 3 -7 0 321.87 19 -3 -7 0 318.97 16.2 -4 7 0 38.9 9.2 4 -7 0 55.69 6.9 4 -7 0 43.8 8.5 4 7 0 46.9 10.2 4 -7 0 54.49 6.1 -4 -7 0 42.2 5.4 -4 -7 0 48.3 4.9 4 -7 0 48.5 12.6 -4 -7 0 36.3 6.1 -4 7 0 36.4 5 -5 7 0 150.18 9.4 -5 -7 0 164.48 12.3 -5 -7 0 168.78 9.5 5 -7 0 151.88 19.6 -5 -7 0 158.78 9.7 5 7 0 171.08 13.5 6 7 0 306.77 20.2 6 -7 0 285.57 16.4 -6 -7 0 293.97 16.1 -6 7 0 283.77 15.8 6 -7 0 345.37 26.6 -6 -7 0 279.77 15.4 -6 -7 0 304.47 17.2 7 -7 0 24.9 4.9 -7 7 0 26.2 4.4 7 -7 0 32.8 16.5 7 7 0 46.9 9.6 -7 -7 0 29.9 6.2 -7 -7 0 32.5 5.6 -7 -7 0 38.5 5.8 -8 -7 0 334.07 19 8 -7 0 354.16 18.5 8 7 0 302.27 24.4 -8 -7 0 321.37 18 -8 -7 0 320.67 17.4 -8 7 0 332.37 18 9 -7 0 93.89 9.2 9 7 0 94.59 9.4 9 7 0 74.99 15.9 -9 7 0 98.19 8.4 -9 -7 0 107.69 9.6 -9 -7 0 107.79 8.7 -10 -7 0 71.69 8.7 -10 -7 0 59.69 7.7 10 -7 0 82.89 7.5 -10 7 0 73.59 6.9 11 -7 0 -4.2 3.2 -11 -7 0 1.3 3.6 0 8 0 41.4 8.4 1 -8 0 158.68 20.1 -1 8 0 188.68 13.4 1 8 0 210.08 14.3 -2 8 0 1190.28 54.89 -2 -8 0 1064.19 52.09 -2 -8 0 1113.49 52.19 2 -8 0 1110.49 54.49 -2 8 0 1103.49 52.09 2 8 0 1093.09 56.19 -3 -8 0 67.69 5.4 3 -8 0 54.69 10.6 3 -8 0 78.59 13.5 -3 8 0 73.09 5.6 3 8 0 74.69 9 -3 8 0 63.29 12.8 3 -8 0 54.89 8 -3 -8 0 63.19 5.8 4 -8 0 377.96 26.5 -4 -8 0 388.96 22.3 4 8 0 425.76 22.5 -4 8 0 395.36 19.8 4 -8 0 404.26 20.7 -5 -8 0 241.08 12.8 5 -8 0 226.38 13.3 -5 8 0 219.48 12.3 5 8 0 229.18 16.3 -5 -8 0 222.38 12.3 5 -8 0 184.08 24.2 6 -8 0 13.2 4 -6 -8 0 12.9 3.1 -6 8 0 10.1 3.3 6 8 0 17.5 7.5 -7 8 0 77.39 7.7 -7 -8 0 90.59 7.9 7 8 0 64.89 11.3 -7 -8 0 79.49 6.9 -7 -8 0 62.79 9.9 7 -8 0 80.89 8.4 -8 -8 0 64.09 7.7 -8 -8 0 90.29 8 8 -8 0 81.09 8.9 -8 -8 0 66.79 9.9 -8 8 0 79.29 7.9 8 8 0 82.89 9.2 8 8 0 109.19 19.5 9 8 0 53.19 9.2 -9 8 0 48.1 6.5 -9 -8 0 40 8.2 -9 -8 0 51.49 6.8 9 -8 0 51.99 7.3 10 -8 0 27.9 4.4 -10 -8 0 32 6.9 11 -8 0 11.5 3.5 -11 -8 0 8.8 4.9 0 -9 0 0.7 3.2 0 9 0 -0.7 2.2 0 9 0 -1.1 5.9 1 -9 0 175.88 15.6 1 9 0 163.88 16.7 1 -9 0 165.18 10.8 -1 9 0 193.28 14.8 -1 -9 0 189.78 10.3 -1 9 0 168.18 9.7 -2 -9 0 3.7 2.7 -2 9 0 13.8 6.9 2 -9 0 2.8 7.4 2 9 0 1.1 8.4 -2 -9 0 4.5 2.5 3 -9 0 161.48 18.5 -3 9 0 143.79 8.6 3 -9 0 144.19 10 -3 -9 0 147.69 9 -3 -9 0 154.68 8.7 4 -9 0 599.54 30 -4 -9 0 636.94 29.8 -4 9 0 612.04 29.4 -4 -9 0 542.15 31.4 4 9 0 640.84 32.4 -4 -9 0 622.04 29.5 -5 -9 0 120.29 11.9 5 -9 0 101.39 8.7 -5 -9 0 97.09 8.1 -5 -9 0 111.09 7.6 5 9 0 109.39 12.9 -5 9 0 93.29 7.4 -6 9 0 1314.67 63.89 -6 -9 0 1372.66 63.89 6 -9 0 1393.46 64.59 6 9 0 1335.47 67.09 -6 -9 0 1337.07 65.09 -6 -9 0 1376.66 64.29 7 9 0 136.59 28 -7 -9 0 155.18 9.9 -7 -9 0 158.38 13.3 7 -9 0 158.08 11.4 -7 -9 0 156.88 10.8 -7 9 0 163.28 10.3 8 -9 0 481.85 23.8 -8 9 0 487.15 22.8 8 9 0 424.66 23.8 -8 -9 0 454.05 24.3 8 9 0 387.56 32.7 -8 -9 0 451.25 23.2 -8 -9 0 435.76 22.5 -9 9 0 48.4 6.7 -9 -9 0 51.69 6.6 9 -9 0 42.7 6.9 -10 -9 0 21.3 4.3 10 -9 0 16 4.1 0 -10 0 78.09 6.8 0 10 0 77.49 15.6 1 -10 0 3.6 8.5 1 -10 0 15.1 3.5 -1 10 0 -8.4 9.1 -1 10 0 7.5 2.4 1 10 0 12.9 9.7 -1 -10 0 6.6 2.7 -2 10 0 194.28 10.8 -2 -10 0 211.28 11 2 10 0 185.78 24.3 -2 -10 0 217.38 11.3 2 -10 0 185.38 11.9 -3 -10 0 30.3 5.2 3 -10 0 38.8 4.8 -3 -10 0 36.9 4.8 -4 -10 0 0.3 2.6 4 -10 0 9.7 3.8 -4 -10 0 4.4 2.4 -4 10 0 4.4 2.5 -5 10 0 473.75 23.8 -5 -10 0 467.35 26.7 -5 -10 0 495.65 24 -5 -10 0 489.25 24.4 5 -10 0 476.45 24.7 -6 -10 0 14.2 3.9 6 -10 0 15 4.3 -6 -10 0 10.6 3.3 -6 -10 0 9 6.3 -7 -10 0 385.56 21 -7 -10 0 333.97 20.1 7 -10 0 348.67 22.8 -8 -10 0 23.9 4.4 -8 -10 0 29.6 6.5 -8 -10 0 23.4 4.1 8 -10 0 39.3 7.5 9 -10 0 5.1 3.9 -9 -10 0 1.4 3.4 10 -10 0 54.69 6.5 -10 -10 0 63.69 7 0 -11 0 2.9 2.9 1 -11 0 134.29 9.5 -1 11 0 137.39 8.6 -1 -11 0 158.48 9.2 -2 11 0 97.59 6.8 2 -11 0 122.39 8.8 -2 -11 0 105.99 7.4 -2 -11 0 90.39 7 3 -11 0 107.19 8.9 -3 -11 0 119.59 7.7 -3 11 0 115.89 7.5 -3 -11 0 106.59 7.9 -4 -11 0 11.6 3 -4 11 0 11.8 2.9 4 -11 0 17 4.4 -4 -11 0 14.6 3.7 5 -11 0 2.2 4.1 -5 -11 0 6.8 3.5 -5 -11 0 5.5 3 -5 -11 0 2.4 8.1 -5 11 0 7.8 3.1 -6 -11 0 342.37 18.7 6 -11 0 351.36 19.2 -6 -11 0 329.57 21.1 -6 11 0 371.66 18.1 -6 -11 0 334.07 18.1 -7 -11 0 18.2 6.9 7 -11 0 21.7 5.1 -7 -11 0 25.9 4.6 -7 11 0 22.8 3.9 -7 -11 0 28 6 -8 -11 0 75.59 7.2 -8 -11 0 78.69 7.4 -8 -11 0 65.39 11.7 8 -11 0 94.69 8.3 9 -11 0 4.4 3.8 -9 -11 0 -8.5 5.8 -9 -11 0 5.5 3.4 -10 -11 0 -7.4 4.8 10 -11 0 4.9 4.3 0 -12 0 329.97 17.3 -1 -12 0 98.49 7.9 1 -12 0 110.49 8.5 -2 -12 0 1.7 2.6 2 -12 0 3.6 3.7 -2 12 0 -0.4 2.5 -2 -12 0 0.5 2.7 -3 12 0 79.39 6.4 -3 -12 0 79.39 6.7 -3 -12 0 84.49 7.4 3 -12 0 85.79 8.2 -4 -12 0 91.59 8.1 4 -12 0 112.19 9.6 -4 -12 0 84.59 7.4 -4 12 0 99.39 7.1 -5 -12 0 461.25 23.1 -5 -12 0 447.06 23.5 -5 12 0 442.76 22.5 5 -12 0 476.55 23.9 -7 -12 0 220.58 12.5 7 -12 0 230.38 13.7 -7 -12 0 217.48 17.9 -7 -12 0 221.48 13.2 -8 -12 0 72.49 6.9 -8 -12 0 71.99 7.3 8 -12 0 77.89 8 -9 -12 0 24.7 4.5 9 -12 0 38 7.1 -9 -12 0 35.9 8.2 0 -13 0 0.9 3.4 1 -13 0 139.59 9.7 -1 -13 0 126.19 9.2 -2 -13 0 0.7 3 2 -13 0 2.3 3.8 -2 -13 0 4.7 2.9 -3 -13 0 -0.2 2.9 3 -13 0 6.2 4 -3 -13 0 2.8 3.3 -4 -13 0 263.87 14.3 -4 13 0 228.58 13.2 4 -13 0 249.28 14.8 -4 -13 0 254.17 14 5 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7.1 2 -19 2 103.29 9 2 -19 2 110.69 7.2 -2 -19 2 102.29 7.2 -2 -19 2 109.39 8.6 2 -19 -2 115.39 7.5 3 -19 2 78.29 9.1 3 -19 2 81.49 6.7 -3 -19 -2 67.09 8 -3 -19 -2 72.19 6.3 3 -19 -2 75.39 6.4 -3 -19 2 82.79 6.7 -3 -19 2 75.19 5.7 4 -19 2 32.6 4.5 -4 -19 -2 30.6 4.4 4 -19 -2 28.4 5 -4 -19 2 35.6 4.5 -4 -19 2 37.1 5.4 5 -19 2 14.1 2.8 -5 -19 -2 21.7 4.5 5 -19 -2 20 4.7 0 -20 2 67.99 8.1 0 -20 -2 62.79 5.7 0 -20 2 66.09 5.5 1 -20 2 154.78 9 1 -20 2 155.28 11.3 -1 -20 -2 152.88 9 -1 -20 2 164.28 9 -1 -20 2 146.19 10.2 1 -20 -2 167.38 9.2 2 -20 2 6.8 2.4 -2 -20 -2 4.5 2.5 2 -20 -2 7.3 2.9 -2 -20 2 1.7 3.8 -3 -20 -2 9.4 2.7 3 -20 2 7.3 2.5 -3 -20 2 8.1 3.8 3 -20 -2 3.6 2.9 -3 -20 2 9.2 2.6 0 -21 -2 130.09 7.7 0 -21 2 124.89 7.6 -1 -21 -2 6.8 2.8 -1 -21 2 8.7 2.6 0 0 3 0.6 1.1 0 0 3 0.4 0.9 0 0 -3 0.6 1.1 0 0 -3 1.7 1.2 1 0 3 409.96 19.7 1 0 3 404.96 19.2 1 0 -3 365.16 19 -1 0 -3 421.76 19.7 2 0 -3 747.73 36.9 -2 0 -3 796.62 37.8 2 0 3 750.52 37 2 0 -3 837.72 37.7 2 0 3 768.12 37.9 -3 0 -3 35.3 6.7 3 0 3 33.1 5.3 3 0 -3 29.9 6.7 3 0 3 31.2 7.1 3 0 -3 33.1 5.6 4 0 3 35.6 8 -4 0 -3 35.5 6.4 4 0 3 30.9 6.3 4 0 -3 27.6 6.7 4 0 -3 26.4 6.4 5 0 3 504.05 34.4 5 0 3 579.24 27 5 0 -3 536.55 26.9 5 0 -3 551.34 34.1 5 0 -3 563.54 29.2 -5 0 -3 585.04 32.4 -5 0 -3 551.44 27.6 -5 0 3 559.74 27.3 -5 0 -3 565.04 26.9 -5 0 -3 563.14 27.4 5 0 3 579.84 29.1 -6 0 3 74.69 7.4 -6 0 -3 48.6 9.9 6 0 -3 68.19 6.5 -6 0 -3 74.99 6.8 -6 0 3 59.69 8.3 6 0 -3 29.8 21.3 -6 0 -3 58.39 6.4 6 0 3 73.99 10.8 6 0 -3 66.29 11.4 7 0 3 736.23 39.7 7 0 -3 721.03 40.2 -7 0 -3 770.02 36.7 7 0 3 749.42 36.4 -7 0 -3 743.03 36.4 -7 0 3 700.43 36.5 -7 0 3 767.62 36.4 7 0 -3 743.73 35.8 8 0 -3 17 3.7 -8 0 -3 22.1 5.1 -8 0 3 16.5 4.3 8 0 3 13.1 4.6 8 0 -3 12.1 10.8 -8 0 -3 22 4.9 8 0 3 7.9 9.1 9 0 3 -1.3 11.5 9 0 -3 40 15.2 -9 0 3 5.5 6.6 10 0 3 47.5 7.1 -10 0 -3 40.3 7 10 0 -3 35.3 7.2 -10 0 3 41.6 6.7 -11 0 -3 33.6 5.6 -11 0 3 33.2 5.1 -12 0 -3 3.8 4.7 0 1 -3 2541.75 117.49 0 -1 3 2370.36 117.19 0 -1 -3 2760.12 116.99 0 1 3 2489.85 116.99 -1 -1 -3 225.78 11 1 1 -3 196.78 10.6 1 -1 3 194.18 10.6 1 -1 3 206.38 11.3 1 -1 -3 217.18 10.5 1 1 3 214.68 10.4 1 -1 -3 182.28 10.2 -1 1 -3 205.18 11.2 1 1 3 233.48 11.1 -2 -1 -3 1895.21 85.29 2 1 -3 1727.03 84.39 2 -1 3 1775.02 84.49 -2 1 3 1890.31 84.79 2 -1 3 1809.92 85.29 2 1 -3 1892.11 85.29 -2 1 -3 1899.61 85.39 2 1 3 1740.83 84.29 2 1 3 1806.22 85.29 2 -1 -3 1852.81 84.79 2 -1 -3 1676.93 85.19 3 -1 3 12.4 3.8 3 1 -3 12.6 3.3 -3 1 3 8.1 3.4 3 1 -3 13.1 4.2 -3 -1 -3 13.1 4 3 -1 3 9.3 3 -3 1 -3 12.5 3.6 3 1 3 12.3 3.3 3 -1 -3 14 3.7 3 1 3 11.1 4.3 3 -1 -3 13 3.3 -4 1 3 834.12 41.3 4 1 -3 806.92 39.9 -4 -1 -3 830.02 41.8 4 -1 3 816.92 39.9 4 -1 3 823.72 42.4 -4 1 -3 808.92 41.6 4 1 3 822.02 42.5 4 -1 -3 798.82 41.7 4 -1 -3 773.52 39.8 4 1 3 849.41 39.9 -5 -1 -3 85.79 6.1 5 1 -3 72.39 12 5 1 -3 77.99 6.1 -5 -1 -3 89.29 7.9 5 -1 3 70.79 12.1 5 -1 3 81.69 9.2 -5 -1 -3 55.69 12.6 -5 -1 -3 82.99 6.6 5 -1 3 84.69 6.2 5 1 -3 86.89 9.2 -5 1 3 70.69 6.7 5 -1 -3 78.69 9.9 -5 -1 3 80.99 7.5 5 1 3 79.79 17.4 -5 1 -3 95.69 13.2 5 1 3 73.89 6.2 5 1 3 77.59 9.1 -5 1 -3 82.69 7 -5 -1 3 88.09 6.9 5 -1 -3 79.49 6.4 -5 1 -3 75.49 7.2 5 -1 -3 84.29 17.4 6 1 -3 2011.4 92.59 6 -1 3 1999.2 93.09 -6 1 3 1962.2 92.99 -6 -1 -3 1768.52 99.99 -6 1 3 2088.19 92.99 -6 -1 -3 2042.8 94.79 -6 -1 -3 2006.9 92.49 6 -1 3 2088.69 93.09 6 -1 3 2142.29 95.39 6 1 3 2078.89 92.69 6 -1 -3 1997.5 93.99 6 1 3 2066.39 95.09 -6 1 -3 2006.9 94.59 -6 1 -3 1897.11 92.39 -6 -1 3 1995 92.79 -6 1 -3 2071.79 93.09 -6 1 -3 1779.12 99.39 6 -1 -3 1690.73 103.69 -6 -1 3 1962 93.09 6 -1 -3 2068.99 95.49 7 1 -3 32 5.9 7 -1 3 43.4 6.7 -7 -1 -3 33.6 6.9 7 -1 3 55.29 12.7 -7 -1 -3 46.6 7.6 -7 1 3 41.3 6.4 -7 -1 -3 49.9 6.9 -7 1 -3 51.69 7.4 7 1 3 51.29 6.8 -7 1 -3 40.7 7.5 7 1 3 51.49 11.6 -7 -1 3 40.1 7.8 -7 -1 3 53.59 6.7 7 -1 -3 61.49 14.4 7 -1 -3 39.9 5.9 -8 -1 -3 298.67 16.7 8 1 -3 258.97 23.9 8 -1 3 291.37 16.3 -8 -1 -3 279.17 16.3 -8 1 3 281.47 16 8 1 -3 293.07 15.4 8 -1 3 267.37 22.5 -8 1 -3 300.77 16.6 -8 -1 3 261.17 16 -8 -1 3 252.87 17 8 1 3 276.07 16.3 8 1 3 273.87 22 -8 1 -3 267.27 16.3 8 -1 -3 300.07 25.9 8 -1 -3 279.77 15.5 9 1 -3 10.8 13.5 9 -1 3 20.3 10.9 9 1 3 0.7 11 9 -1 -3 2.2 15.9 10 1 -3 -1 3.9 -10 -1 -3 11.9 4.1 10 -1 3 7.2 4 -10 -1 3 0.5 3.5 10 1 3 4.6 4.1 10 -1 -3 4.5 4.1 -10 1 -3 2.2 3.5 11 -1 3 4 3.3 11 1 -3 12.1 3.8 -11 -1 -3 10.4 3.5 -11 1 3 6.6 3 -11 -1 3 8.8 3.2 11 -1 -3 11.5 3.8 -11 1 -3 7.1 3.3 11 1 3 7.1 3.6 -12 -1 -3 3.3 4.4 12 -1 -3 12.3 5 0 -2 3 234.38 12.3 1 -2 3 384.86 20.1 1 -2 3 395.66 20.7 -1 -2 -3 441.46 20.4 1 2 -3 373.86 20 1 2 3 407.66 19.7 -1 2 -3 412.16 20.7 1 2 3 448.86 20.4 1 -2 -3 445.46 19.6 -2 -2 -3 2695.23 122.79 2 -2 3 2619.94 122.89 2 2 -3 2742.13 122.99 2 2 -3 2443.96 121.89 2 -2 3 2511.95 121.99 -2 2 3 2682.93 122.09 2 2 3 2528.35 121.79 -2 2 -3 2732.53 122.89 2 -2 -3 2533.05 121.59 2 2 3 2698.23 122.79 2 -2 -3 2743.13 122.19 -3 -2 -3 140.49 10.4 -3 2 3 142.79 9.4 3 2 -3 143.29 11 3 -2 3 134.19 11 3 2 -3 136.99 9.2 3 -2 3 128.19 8.9 -3 2 -3 119.59 10 3 2 3 129.49 8.8 3 -2 -3 134.49 9.9 3 -2 -3 111.79 8.8 4 -2 3 99.29 12.4 4 2 -3 109.89 9.2 4 2 -3 120.19 13 -4 2 3 108.69 10.1 -4 -2 -3 98.39 10.9 4 -2 3 116.09 9.1 4 -2 -3 113.69 11.8 4 2 3 116.89 9.1 -4 2 -3 119.79 10.8 4 2 3 110.89 12.9 4 -2 -3 100.89 9.2 -5 -2 -3 1121.49 51.39 5 2 -3 1129.69 53.19 -5 -2 -3 1127.59 51.89 5 -2 3 1005.1 57.59 5 2 -3 1062.39 57.89 -5 2 3 1036.5 51.19 -5 -2 -3 1095.99 56.29 5 2 -3 1103.99 50.99 5 -2 3 1109.49 52.99 -5 2 3 1030.1 55.09 5 -2 3 1091.39 51.39 -5 -2 -3 1059.29 50.89 5 -2 3 1168.88 51.19 -5 2 -3 1025.2 55.59 5 2 3 1152.98 51.09 -5 2 -3 1080.19 51.49 -5 -2 3 1103.69 51.29 5 -2 -3 1076.49 53.19 5 2 3 1039.3 58.09 5 2 3 1151.98 53.09 5 -2 -3 1010.4 50.99 -5 -2 3 1120.89 51.49 5 -2 -3 1047.5 56.99 -5 2 -3 1093.19 51.49 6 -2 3 17.8 3.5 -6 -2 -3 22.5 3.6 -6 -2 -3 21.8 14 6 2 -3 24.6 6.5 6 2 -3 33.7 5 -6 -2 -3 24.8 5.7 6 -2 3 27.7 6.6 -6 -2 -3 20 3.2 -6 2 -3 35 5.8 6 -2 -3 27 7.6 -6 2 -3 35.6 6.5 -6 -2 3 30.9 5.9 -6 2 -3 29.1 14.2 -6 -2 3 25.5 4 6 2 3 41.6 9.3 -7 -2 -3 765.62 37.6 7 -2 3 818.32 42.4 -7 -2 -3 734.73 38.1 -7 -2 -3 783.72 38.7 -7 2 3 776.62 38.1 7 -2 3 785.62 38.4 7 2 -3 753.62 37.8 7 2 -3 784.62 42.2 7 2 3 797.72 41.3 -7 2 -3 813.12 38.5 -7 2 -3 792.42 38.5 7 2 3 776.92 38.4 7 -2 -3 783.92 43.4 -7 -2 3 762.72 38.1 -7 -2 3 803.22 38.6 7 -2 -3 834.62 38 -8 -2 -3 234.58 14.6 8 -2 3 262.87 22.3 8 2 -3 247.48 13.8 -8 -2 -3 241.28 15 8 -2 3 245.08 14.8 -8 2 3 252.77 14.4 8 2 -3 261.97 22 -8 -2 3 241.98 14.5 -8 -2 3 207.78 14.7 8 2 3 247.48 14.8 -8 2 -3 246.88 14.9 8 -2 -3 232.78 13.9 8 2 3 249.48 20.2 9 2 -3 2.2 13.9 -9 -2 -3 19.9 5.3 -9 -2 -3 23.7 5.5 9 -2 3 4.9 11.8 -9 2 3 26.2 5 9 -2 3 29.1 7.3 9 2 3 44.8 9.2 9 2 3 46.6 11.8 9 -2 -3 6.3 18.2 9 -2 -3 24.9 5.3 -10 2 3 7.3 3.4 -10 -2 -3 12 4.8 10 -2 3 10.6 4 -10 -2 -3 1.4 3.8 10 2 -3 5 3.9 -10 2 -3 10.8 3.9 -10 -2 3 12.1 3.8 10 2 3 4.2 4.2 10 -2 -3 8 4.1 11 2 -3 11.9 3.7 -11 -2 -3 11.8 3.7 11 -2 3 14.2 3.5 -11 2 -3 13.6 3.3 11 -2 -3 16.1 3.8 11 2 3 5.7 6 0 3 -3 171.68 10.2 1 -3 3 164.58 10.3 -1 -3 -3 181.68 9.7 1 -3 3 156.08 9.6 1 3 -3 165.78 9.6 -1 3 -3 175.48 10.6 1 3 3 175.68 9.7 -2 3 3 273.27 14.7 -2 -3 -3 290.87 15.8 2 3 -3 290.27 15.2 2 -3 3 257.87 15 2 -3 3 278.37 16.3 2 3 -3 286.17 16.3 2 3 3 315.67 16 2 -3 -3 297.57 14.9 -2 3 -3 282.67 16 2 3 3 316.37 14.8 2 -3 -3 268.27 14.8 3 -3 3 1136.79 57.39 3 3 -3 1172.68 60.19 -3 -3 -3 1159.18 58.69 -3 3 3 1220.98 57.79 3 -3 3 1159.78 58.99 3 3 -3 1129.39 57.39 3 -3 -3 1334.07 58.29 -3 3 -3 1280.77 58.79 3 3 3 1269.47 58.99 3 3 3 1283.07 57.39 3 -3 -3 1168.88 57.19 4 -3 3 184.28 16.5 -4 3 3 216.18 13.8 -4 -3 -3 190.68 14.9 4 -3 3 184.68 11.2 4 -3 3 196.38 12.6 4 3 -3 200.88 12.8 4 3 -3 183.18 16.6 -4 3 -3 192.28 14.6 4 -3 -3 207.38 15.3 4 3 3 212.08 12.6 -4 -3 3 206.38 11.7 4 -3 -3 178.48 18.2 5 3 -3 117.69 11 5 -3 3 137.29 11.3 -5 3 3 121.19 14.8 5 -3 3 93.89 21.4 5 -3 3 119.19 8.4 -5 -3 -3 97.59 16.3 5 -3 3 131.49 7.8 -5 -3 -3 111.09 7.4 -5 -3 -3 115.09 8 -5 3 3 122.49 7.7 5 3 -3 128.99 23.1 -5 -3 -3 128.49 9.6 5 3 -3 127.59 7.7 5 -3 -3 120.99 12.3 -5 -3 3 119.89 7.9 5 -3 -3 117.29 7.9 5 3 3 107.29 10.3 -5 3 -3 121.29 8.8 5 3 3 103.49 8.1 -5 -3 3 115.59 7.9 -5 3 -3 112.19 8 -5 3 -3 136.59 15.9 -5 -3 3 116.89 8.6 5 -3 -3 144.79 21.9 6 -3 3 334.87 20.1 -6 -3 -3 315.77 16.3 -6 3 3 292.97 15.8 6 3 -3 315.77 19.9 6 3 -3 315.17 15.8 6 -3 3 311.57 16.4 -6 -3 -3 299.37 15.5 -6 -3 3 304.57 16.4 6 3 3 305.37 19 -6 3 -3 286.07 16.4 -6 -3 3 280.27 16.7 -6 -3 3 313.27 17.5 -6 3 -3 279.97 30.8 6 -3 -3 295.77 22 6 -3 -3 286.27 15.7 -6 3 -3 305.87 16.4 -7 -3 -3 69.49 6.8 -7 3 3 92.39 7.4 7 3 -3 89.89 7.2 7 -3 3 97.49 15.4 -7 -3 -3 93.79 9 7 -3 3 97.89 8 -7 -3 -3 83.29 8.1 7 3 -3 89.49 14 7 3 3 74.09 12.6 -7 -3 3 70.49 8.2 -7 -3 3 80.49 8 7 -3 -3 79.19 7.3 -7 3 -3 83.89 8.3 7 -3 -3 108.19 18.8 7 3 3 77.19 7.9 -8 -3 -3 126.69 10.3 8 3 -3 73.69 17.5 8 -3 3 104.09 9.4 8 -3 3 115.29 19.7 -8 -3 -3 126.69 11.2 8 3 -3 115.89 8.5 -8 -3 -3 116.09 9.6 -8 3 3 106.49 9 8 -3 -3 103.79 8.5 8 3 3 117.59 9.7 -8 -3 3 108.19 9.8 -8 3 -3 106.89 9.7 8 -3 -3 147.99 24.8 -8 -3 3 110.39 9.7 8 -3 -3 102.59 9.4 9 -3 3 123.29 10.2 9 -3 3 147.59 26 9 3 -3 106.59 16.9 -9 -3 -3 99.99 10.4 -9 3 3 116.39 9.3 -9 -3 -3 111.49 10.1 -9 3 -3 129.09 10.1 9 -3 -3 133.09 10.4 9 3 3 115.79 10.1 -9 -3 3 104.69 11.7 -9 -3 3 130.09 10.2 9 3 3 111.99 20.2 10 -3 3 12.2 3.9 10 3 -3 5.4 4 -10 -3 -3 6.9 4.4 -10 -3 -3 5.7 4.5 -10 -3 3 15.4 4.2 10 3 3 5.8 4.1 -10 3 -3 11.3 3.7 10 -3 -3 13.9 4.1 11 3 -3 11.6 4.6 11 -3 3 9.4 3.4 -11 3 3 9.1 3.4 -11 -3 -3 6.2 3.2 11 3 3 11.4 4.2 -11 -3 3 13.4 3.4 -11 3 -3 7 3.1 11 -3 -3 10 3.4 0 4 3 2.6 2.2 0 4 3 1.2 1.6 0 4 -3 2.7 2.6 1 -4 3 1037.6 49.5 1 4 -3 1026.7 48.6 1 4 3 1066.09 48.8 -1 4 -3 982.3 49.3 2 -4 3 77.89 7.1 2 -4 3 89.29 8.8 2 4 3 82.59 8 -2 4 -3 103.99 8.4 2 4 3 95.89 6.6 2 -4 -3 96.19 8 2 -4 -3 103.89 7 3 -4 3 575.14 30 -3 4 3 598.64 30.1 3 -4 3 589.74 31.9 3 4 -3 610.74 30.1 3 4 -3 607.44 32.2 3 4 3 623.04 29.7 3 -4 -3 633.54 30.7 -3 4 -3 606.14 31.4 3 -4 -3 592.84 30.1 4 4 -3 1642.64 77.79 4 -4 3 1642.74 77.79 4 4 -3 1576.54 76.09 -4 4 3 1675.93 78.59 4 -4 3 1598.24 76.49 -4 -4 -3 1588.84 76.29 4 -4 3 1632.94 80.59 4 4 -3 1592.04 80.79 -4 -4 3 1611.24 76.59 4 4 3 1736.53 77.59 -4 4 -3 1696.83 79.79 4 -4 -3 1681.33 79.39 4 -4 -3 1596.34 77.69 -4 -4 3 1642.84 76.29 -5 -4 -3 91.89 9.2 5 -4 3 93.19 7.4 -5 4 3 113.19 14.9 -5 -4 -3 81.59 6.3 5 -4 3 101.99 10.9 5 -4 3 83.39 16.2 5 4 -3 96.59 10.3 -5 -4 -3 92.59 7.2 -5 4 3 92.79 6.4 5 4 -3 96.39 6.6 -5 -4 3 87.29 6.8 -5 4 -3 71.99 16.6 -5 4 -3 86.49 7 -5 -4 3 88.89 6.5 5 -4 -3 84.39 7 5 -4 -3 82.19 12.9 -5 -4 3 93.09 7.8 5 -4 -3 89.29 13.6 -6 -4 -3 10.3 2.8 6 -4 3 26.1 6.6 6 4 -3 16 3 -6 4 3 18.1 3.2 6 -4 3 14.8 3.7 -6 -4 -3 10.2 5.9 -6 -4 -3 16.3 3.7 6 4 -3 24 6.5 6 -4 -3 -3.2 9 -6 -4 3 18.7 3.4 -6 -4 3 9.2 3.1 -6 -4 3 14.4 3.8 -6 4 -3 0.9 15.3 -6 4 -3 14.6 3.4 6 -4 -3 13.3 3 6 4 3 15.5 5.7 -7 -4 -3 135.99 9.3 7 -4 3 138.49 10.3 7 4 -3 132.59 9.2 7 -4 3 158.88 18 -7 4 3 133.59 9.6 -7 -4 -3 151.18 11.3 7 4 -3 124.09 16.2 -7 -4 -3 139.29 10.2 -7 -4 3 162.58 10.2 -7 -4 3 165.68 11 7 -4 -3 145.09 9.6 7 -4 -3 144.89 10.2 7 4 3 156.08 15.2 7 -4 -3 142.39 26.1 -7 4 -3 155.48 10.6 -8 4 3 157.28 10.9 8 4 -3 154.48 19.1 -8 -4 -3 148.29 11.9 8 4 -3 159.48 10.2 8 -4 3 189.68 23.5 8 -4 3 167.68 11.5 -8 -4 -3 169.58 10.5 -8 -4 -3 177.08 11.4 8 -4 -3 146.89 30.1 8 -4 -3 167.38 11.5 -8 -4 3 157.08 11.7 -8 4 -3 169.18 11.7 8 4 3 136.49 17.8 8 4 3 167.88 11.5 8 -4 -3 137.09 10.5 -8 -4 3 154.98 11.1 -9 -4 -3 52.59 8.2 -9 4 3 61.79 7.3 -9 -4 -3 51.59 8.9 9 4 -3 60.79 14.5 9 -4 3 87.39 18.4 9 -4 3 61.09 8.2 9 4 3 68.19 8.4 9 4 3 41.8 12.2 -9 -4 3 63.89 9.3 -9 4 -3 62.69 8 -9 -4 3 61.19 8.1 9 -4 -3 59.99 8.5 -10 -4 -3 82.19 8.7 10 -4 3 104.89 8.6 -10 4 3 98.59 7.6 10 4 -3 85.59 8.2 -10 -4 -3 85.89 8.9 10 4 3 79.29 8.6 -10 4 -3 83.49 7.6 10 -4 -3 88.09 8.3 -10 -4 3 86.89 8 -11 4 3 1.1 3.7 -11 -4 -3 6.4 3.8 11 -4 3 2.4 4.2 11 4 -3 3.5 3.7 11 4 3 9.5 5.3 -11 4 -3 5.4 4.1 11 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7.3 -5 -2 -4 73.49 8.8 -5 -2 -4 92.99 15.1 5 -2 4 91.99 7.4 5 2 -4 97.09 10.2 -5 2 4 97.19 7 -5 -2 -4 81.59 6.4 5 2 -4 105.99 20.6 5 2 -4 102.99 6.7 -5 2 -4 102.99 7.6 5 -2 -4 100.29 11.5 5 2 4 106.19 10.1 5 -2 -4 100.69 7.4 -5 2 -4 95.89 7.6 -5 -2 4 106.99 7.4 -5 -2 4 97.79 7.4 5 2 4 93.59 16.4 -5 2 -4 99.69 14.7 6 -2 4 15.4 5.8 -6 -2 -4 21 3.9 6 -2 4 16.3 3.8 -6 -2 -4 28.6 5.7 -6 -2 -4 1.4 17.7 -6 2 4 25.1 5 -6 2 -4 14.8 3.8 6 2 4 12 3.7 -6 2 -4 10.4 4.6 -6 2 -4 19.3 15.5 6 2 4 20.6 5.8 6 -2 -4 16.4 7.3 -7 2 4 136.69 10 7 2 -4 168.48 9.9 7 -2 4 142.09 16.3 -7 -2 -4 157.68 10.8 7 2 -4 162.88 17.1 -7 -2 -4 138.99 9.6 7 -2 4 148.39 10.5 -7 -2 -4 155.28 11.3 -7 2 -4 168.38 11.1 -7 -2 4 178.98 10.9 7 2 4 167.28 11 7 2 4 180.58 15 7 -2 -4 156.18 10 -7 2 -4 155.58 11 -7 -2 4 155.48 10.9 7 -2 -4 127.59 18.9 8 -2 4 17.8 4.3 -8 -2 -4 11.2 4.5 8 -2 4 30.8 9.6 8 2 -4 20.5 9.7 -8 2 4 21.6 4.3 -8 -2 -4 19.1 4.7 8 2 4 13.9 4.5 8 -2 -4 15.2 3.9 -8 -2 4 21.7 4.7 -8 -2 4 21.8 5.4 8 2 4 22.3 8 8 -2 -4 21.3 13.6 -8 2 -4 17.7 4.9 9 -2 4 155.48 23.1 -9 -2 -4 168.58 12.5 -9 2 4 198.38 12.1 9 -2 4 186.38 12.6 -9 -2 -4 160.88 12.3 9 2 -4 176.78 11.3 9 2 -4 169.58 25.9 9 2 4 158.08 21.2 9 -2 -4 161.28 34.9 9 -2 -4 186.38 12.6 9 2 4 175.28 12.2 -9 2 -4 194.48 12.8 9 -2 -4 192.58 11.5 -9 -2 4 170.08 12.2 10 2 -4 33.2 6.6 -10 2 4 38.8 6.2 -10 -2 -4 34.9 5.5 -10 -2 -4 34 5.4 10 -2 4 43.2 6.8 -10 -2 4 47 6.5 10 2 4 30.5 5 10 -2 -4 39.5 7 -10 2 -4 45.5 6.8 11 2 -4 119.49 8.7 11 -2 4 129.39 8.5 -11 2 4 106.69 10.8 -11 -2 -4 120.49 8.5 11 2 4 112.49 9 11 -2 -4 117.99 8.6 -11 2 -4 120.29 8.2 -11 -2 4 120.29 8.1 0 3 -4 3676.93 162.38 0 -3 4 3318.57 161.58 1 -3 4 2699.73 131.09 1 -3 4 2667.63 130.39 1 3 -4 2670.33 130.39 -1 -3 -4 3084.79 130.59 -1 3 -4 2844.32 131.19 1 3 4 2922.81 130.49 2 -3 4 4879.31 222.98 2 -3 4 4524.95 221.68 -2 -3 -4 4878.51 222.48 2 3 -4 4448.75 221.68 2 -3 -4 4645.74 221.28 2 3 4 4750.02 221.28 2 3 4 4901.81 222.48 2 -3 -4 5282.47 221.68 -2 3 -4 4876.81 222.78 3 -3 4 883.81 43.5 3 -3 4 887.41 41.6 -3 3 4 940.11 41.8 -3 -3 -4 870.71 42.9 3 3 -4 878.71 47.9 3 3 -4 828.52 41.5 3 3 4 819.12 42.9 3 3 4 823.62 41.2 3 -3 -4 881.81 42 -3 3 -4 844.02 42.9 3 -3 -4 798.32 41.2 4 -3 4 194.48 12.3 4 -3 4 206.78 17.1 4 3 -4 198.88 17.1 -4 3 4 198.78 13.4 -4 -3 -4 199.18 14.7 4 3 -4 189.68 12.6 4 -3 -4 162.08 12.8 4 -3 -4 157.68 14.4 4 3 4 185.78 12.1 -4 3 -4 176.98 14.4 -4 -3 4 188.58 10.9 5 3 -4 26.3 12.2 5 3 -4 31.5 4.8 -5 -3 -4 43.5 5.6 -5 3 4 31.3 4.7 5 3 -4 25.6 5.9 5 -3 4 52.49 8.8 -5 -3 -4 34.6 4.5 -5 -3 -4 33.5 9.4 -5 -3 -4 23.4 4.9 5 -3 4 48 14 5 -3 4 30 5.6 -5 -3 4 47.5 6.9 5 -3 -4 25 6.4 5 -3 -4 40.8 5.6 -5 -3 4 40.4 5.5 -5 3 -4 17.4 8.5 5 3 4 44.5 8.1 5 -3 -4 42.4 11.1 -5 -3 4 44.1 6 -5 3 -4 34.1 5.6 -6 3 4 66.79 6.3 6 3 -4 97.59 6.6 6 -3 4 88.09 12 6 3 -4 100.39 12.2 -6 -3 -4 82.39 6.4 -6 -3 -4 69.09 7.2 6 -3 4 81.79 7.2 -6 -3 4 86.79 8.1 -6 3 -4 81.59 7.3 -6 3 -4 66.59 8.1 6 -3 -4 80.49 6.7 6 -3 -4 72.39 10.9 6 3 4 86.29 10.7 -6 -3 4 94.59 7.6 7 -3 4 40.3 8.9 -7 -3 -4 52.29 8.1 7 -3 4 36.5 6.5 -7 -3 -4 34.5 6.7 -7 -3 -4 35.3 5.4 -7 3 4 42.5 6 7 -3 -4 28.5 11.4 -7 3 -4 41.7 6.9 7 3 4 55.09 12.1 -7 -3 4 51.39 7.1 7 -3 -4 33.3 6 7 3 4 38.2 5.2 8 -3 4 31.6 5.6 8 3 -4 51.39 6.3 -8 3 4 42.1 6.6 8 -3 4 36.1 10.5 8 3 -4 41.4 10.5 -8 -3 -4 47 7.5 -8 -3 -4 42.1 7.2 -8 -3 -4 38.7 8.1 -8 -3 4 45.9 7.5 8 3 4 37.2 7.4 8 -3 -4 36.2 6.5 8 -3 -4 28.8 16.7 8 3 4 24.9 8.8 -8 3 -4 46.7 7.9 8 -3 -4 37 7.3 -8 -3 4 59.09 8.5 -9 -3 -4 99.09 9.7 9 -3 4 98.79 9.4 9 -3 4 69.59 16.6 9 3 -4 98.99 8.5 -9 3 4 117.69 9.3 -9 -3 -4 108.39 10.3 -9 3 -4 119.59 9.9 9 -3 -4 126.29 10.2 -9 -3 4 106.49 9.5 9 3 4 101.39 9.4 9 -3 -4 112.89 8.8 -10 -3 -4 136.19 10.8 10 3 -4 150.08 10.5 -10 -3 -4 151.28 11.1 10 -3 4 164.58 10.6 -10 3 4 157.48 9.8 -10 3 -4 146.89 10.1 -10 -3 4 145.09 10.2 10 -3 -4 152.68 10.6 10 3 4 130.29 10.5 -11 3 4 82.49 7.1 11 3 -4 93.69 8.8 11 -3 4 100.49 7.9 11 3 4 82.09 8.5 11 -3 -4 83.19 7.3 -11 -3 4 80.09 6.8 -11 3 -4 82.49 6.9 0 4 -4 1.7 2.6 1 4 -4 1744.53 78.29 1 4 -4 1642.14 77.09 1 -4 4 1643.54 78.09 1 -4 4 1534.05 76.99 1 4 4 1700.83 77.09 -1 4 -4 1620.34 77.89 2 4 -4 1132.99 54.69 2 -4 4 1157.38 56.09 -2 4 4 1198.28 54.09 2 -4 4 1142.29 54.69 -2 -4 -4 1182.58 55.39 -2 4 -4 1150.68 55.79 2 4 4 1134.49 53.99 2 -4 -4 1004.5 54.59 2 4 4 1194.48 55.49 2 -4 -4 1236.78 54.29 -3 -4 -4 1054.29 50.19 -3 4 4 1048.6 48.7 3 4 -4 1064.09 50.99 3 -4 4 987.1 50.69 3 4 -4 1025.5 48.7 3 -4 -4 1011.8 48.9 -3 4 -4 982.8 49.99 3 -4 -4 888.21 48.4 3 4 4 1051.49 52.89 3 4 4 1003.1 48.2 -4 -4 -4 236.38 17.6 4 -4 4 239.18 19.8 4 -4 4 244.68 13.2 -4 4 4 244.38 15.7 4 -4 4 260.17 15 -4 -4 -4 244.18 13 -4 -4 -4 223.88 12.5 4 4 -4 248.88 12.6 4 4 -4 246.38 15.1 4 4 -4 256.37 21.7 4 4 4 257.17 14.5 -4 4 -4 243.88 17.4 4 -4 -4 222.78 16.9 -4 -4 4 238.58 13.3 -4 -4 4 234.68 12.9 4 -4 -4 241.98 17.2 4 4 4 231.58 19.6 5 -4 4 119.69 11.3 5 -4 4 110.89 8.1 -5 -4 -4 109.89 10.4 -5 -4 -4 113.39 7.7 5 -4 4 157.48 26.7 -5 4 4 102.39 16.6 -5 4 4 113.09 7.2 5 4 -4 131.29 11.4 -5 -4 -4 111.39 7.2 5 -4 -4 97.39 14.3 -5 4 -4 109.79 17.5 5 4 4 127.09 10.6 5 -4 -4 102.19 8 5 -4 -4 108.79 14.4 -5 -4 4 115.59 7.7 -5 -4 4 108.69 8.2 -5 -4 4 94.49 7.4 -5 4 -4 111.19 8 -6 4 4 4.2 2.6 -6 -4 -4 -2.3 4.1 6 4 -4 3.1 2.4 -6 -4 -4 -1.9 2.4 -6 -4 -4 1.6 2.8 6 -4 4 6.3 5.9 6 -4 4 -1.8 2.9 6 4 -4 -4.5 5.7 -6 -4 4 7.1 3.8 -6 4 -4 0.6 16.2 6 4 4 7.2 5.4 6 -4 -4 2.2 9.8 -6 -4 4 5.3 3.5 -6 -4 4 6.2 3 -6 4 -4 1.5 3.1 6 -4 -4 6 2.6 7 -4 4 64.99 15.6 -7 -4 -4 55.09 6.4 7 4 -4 90.29 14.2 -7 4 4 63.99 6.8 -7 -4 -4 66.59 9.1 -7 -4 -4 60.49 8.9 7 -4 4 73.79 7.5 7 4 -4 69.59 6.6 -7 -4 4 65.49 7.2 -7 -4 4 64.89 7.5 -7 4 -4 56.59 8.4 7 4 4 43.8 7.6 7 -4 -4 65.19 14.1 7 4 4 61.09 12.6 7 -4 -4 64.09 6.8 8 4 -4 106.09 18.6 -8 -4 -4 130.69 10.9 -8 -4 -4 126.39 9.6 -8 4 4 104.79 8.9 8 4 -4 121.19 8.4 -8 -4 -4 118.69 8.6 8 -4 4 103.99 21 8 -4 4 114.69 9.4 8 4 4 91.89 16.4 8 4 4 92.99 9.3 8 -4 -4 81.79 9.1 -8 4 -4 95.79 9.5 -8 -4 4 85.69 9.4 -8 -4 4 108.09 9.6 8 -4 -4 91.39 8.4 -9 4 4 164.38 11 9 -4 4 164.18 11.8 9 -4 4 160.28 28.6 9 4 -4 186.18 24.6 -9 -4 -4 162.88 12.6 -9 -4 -4 161.98 11.6 -9 -4 4 171.88 12.7 -9 -4 4 174.48 11.7 9 4 4 177.28 22.7 -9 4 -4 168.48 11.7 9 -4 -4 173.18 12.1 9 4 4 147.49 11.5 -10 4 4 190.48 11.1 10 -4 4 178.28 11.5 -10 -4 -4 171.08 11.9 10 4 -4 190.28 11.8 -10 -4 -4 174.18 12.2 -10 4 -4 192.48 11.5 10 -4 -4 201.88 12.2 -10 -4 4 178.58 11.6 10 4 4 196.48 12.2 11 4 -4 42.1 6.3 -11 -4 -4 39.6 6.2 11 -4 4 36.1 6 -11 4 -4 42.9 5.4 -11 -4 4 34.1 6.4 11 -4 -4 45.1 6.3 0 5 -4 108.79 9.1 1 5 -4 159.48 11.3 1 5 -4 140.29 9.9 1 -5 4 142.79 10.8 1 -5 4 149.88 10 1 5 4 165.78 9.5 -1 5 -4 152.88 10.8 2 -5 4 1302.57 67.29 2 5 -4 1434.76 66.09 2 -5 4 1333.27 65.99 2 -5 -4 1459.75 65.39 2 5 4 1438.26 65.19 -2 5 -4 1379.76 67.19 2 5 4 1415.26 66.79 3 5 -4 89.29 12.7 3 -5 4 84.49 7.2 3 -5 4 87.39 8.7 3 5 -4 105.29 8.8 -3 5 4 96.29 7.9 3 5 4 100.69 7.6 -3 5 -4 74.99 9.8 3 -5 -4 86.29 9 3 -5 -4 82.39 11.1 -4 5 4 244.78 15 4 5 -4 235.38 14.4 -4 -5 -4 224.78 12.1 -4 -5 -4 212.48 11.6 4 -5 4 228.58 21.6 4 5 -4 219.98 21.7 4 5 -4 224.78 11.6 4 -5 4 214.38 12.1 -4 5 4 205.08 11.5 4 -5 4 230.98 14.4 4 -5 -4 200.58 17.4 4 5 4 182.68 20.4 -4 -5 4 222.68 11.8 -4 -5 4 215.78 11.6 -4 5 -4 196.48 17.3 4 5 4 248.38 13.9 -4 -5 4 191.48 15.6 -4 5 -4 209.58 12.1 -5 -5 -4 320.47 16.2 5 -5 4 311.47 16.7 5 -5 4 293.67 36.5 5 5 -4 315.77 19.3 -5 5 4 311.17 16.1 -5 -5 -4 320.57 16.6 5 5 -4 307.17 16 -5 -5 -4 308.97 18.4 5 -5 4 349.57 20.2 -5 -5 4 305.27 16.9 -5 5 -4 298.67 25.8 -5 -5 4 317.67 16.3 5 -5 -4 303.37 22.7 -5 5 -4 325.87 16.9 5 5 4 336.77 18.7 -5 -5 4 323.17 16.1 5 -5 -4 308.97 16.4 -6 -5 -4 37.4 5.1 6 5 -4 46.4 5.8 6 -5 4 54.39 6.4 -6 -5 -4 30.7 5.8 6 -5 4 58.99 12.7 -6 -5 -4 41.8 6.2 -6 5 4 41.6 5.4 6 5 -4 42.7 8 6 5 4 44.9 10.2 6 -5 -4 25.2 11.4 -6 5 -4 45.3 6.5 -6 -5 4 52.89 7.1 -6 -5 4 32.6 6.5 -6 -5 4 42.3 5.9 6 -5 -4 56.39 6.1 7 5 -4 27.5 5.4 7 5 -4 24.2 8.7 -7 5 4 30.8 6 7 -5 4 23.6 4.6 -7 -5 -4 29.6 6.1 -7 -5 -4 24.7 4.4 -7 -5 4 24.8 4.5 -7 5 -4 28 4.7 -7 -5 4 35.8 7.2 7 -5 -4 35.2 6 7 5 4 20 5.3 7 5 4 15.6 7.8 7 -5 -4 34.3 5 8 5 -4 192.98 21.1 -8 -5 -4 244.68 13.1 8 -5 4 222.88 26.9 8 5 -4 233.08 13.3 -8 -5 -4 226.78 15.1 8 -5 4 221.48 14 -8 5 4 228.68 13.5 -8 -5 -4 212.48 13.8 -8 -5 4 246.48 14.8 -8 5 -4 231.38 14.2 8 -5 -4 230.98 13.6 -8 -5 4 225.88 13.7 8 -5 -4 223.38 14.2 8 5 4 240.38 14.3 8 5 4 246.38 20.8 -9 -5 -4 91.59 9.3 9 -5 4 103.39 9.5 -9 5 4 100.39 8.3 9 -5 4 106.49 18.4 9 5 -4 72.19 16.5 -9 -5 -4 93.69 10.6 9 5 4 148.89 21.8 -9 -5 4 116.29 10.1 9 -5 -4 109.79 9.7 9 5 4 108.99 9.7 -9 -5 4 120.29 9.2 -9 5 -4 105.89 9.2 10 5 -4 55.59 7.2 -10 -5 -4 51.59 8 -10 5 4 59.79 6.8 10 -5 4 58.49 6.8 -10 -5 -4 53.99 7.1 -10 -5 4 64.79 7 -10 5 -4 63.89 6.8 10 5 4 64.79 8.6 10 -5 -4 64.19 7.6 11 5 -4 26.9 4.4 11 -5 4 32.5 5.3 -11 -5 4 27.7 5.2 -11 5 -4 34.5 4.9 11 -5 -4 31.5 6.4 0 6 4 306.17 15.7 0 6 -4 313.47 18.2 0 6 4 317.47 15.8 1 -6 4 164.08 13 1 6 -4 188.68 13.1 1 -6 4 156.88 11.5 1 6 4 203.08 11.3 -1 6 -4 209.28 13 2 -6 4 125.79 12.6 2 -6 4 122.99 10.2 2 6 -4 143.39 10.1 2 6 4 164.88 8.7 2 6 4 143.89 10.9 -2 6 -4 148.19 11.6 2 -6 -4 125.99 13.4 -3 -6 -4 431.46 22 3 6 -4 461.15 28.1 -3 -6 -4 445.46 22.4 3 -6 4 458.15 22.4 3 6 -4 487.65 24.2 3 -6 4 461.25 27.4 3 -6 4 468.95 24.2 -3 -6 4 398.96 22.7 -3 6 -4 444.76 22.7 3 6 4 448.96 26.6 3 6 4 474.05 23.3 -3 6 -4 434.76 25.8 -3 -6 4 446.36 21.9 3 -6 -4 457.65 24.2 4 -6 4 188.78 23.5 4 -6 4 184.38 14 -4 6 4 191.98 14.8 -4 -6 -4 185.48 10.9 4 6 -4 196.38 13.6 4 6 -4 169.98 10.4 4 -6 4 176.78 11.2 -4 6 4 162.88 10.3 -4 -6 -4 170.58 10.4 4 -6 -4 229.58 18.1 -4 6 -4 179.28 18.3 -4 -6 4 222.78 11.9 -4 -6 4 220.38 10.6 4 -6 -4 174.28 12.9 -4 6 -4 207.58 11 -4 -6 4 215.28 10.8 5 -6 4 99.09 33.8 -5 -6 -4 59.09 10.3 -5 -6 -4 46.8 6.3 5 -6 4 51.69 8.2 -5 -6 -4 52.39 5.2 -5 6 4 49.5 5.5 5 -6 4 58.29 6.4 5 6 -4 52.29 10.1 5 6 -4 62.69 5.8 -5 6 -4 64.69 6.4 -5 -6 4 69.09 10.8 5 -6 -4 51.69 7.8 -5 -6 4 68.59 5.9 -5 -6 4 61.79 6.1 5 -6 -4 69.89 6.9 6 -6 4 151.28 17.5 -6 -6 -4 154.78 9.5 6 -6 4 162.68 10.3 6 6 -4 175.68 15 -6 6 4 166.88 9.6 -6 -6 -4 176.78 10.4 -6 -6 -4 145.89 12.2 6 6 -4 166.08 9.6 -6 -6 4 142.79 9.5 6 -6 -4 140.59 9.7 6 6 4 138.59 10.7 -6 -6 4 136.69 10.5 6 6 4 154.68 14 6 -6 -4 150.68 10.9 -6 6 -4 142.29 10.2 -6 -6 4 155.98 9.9 -7 -6 -4 170.18 12.8 7 6 -4 164.68 10 7 -6 4 175.08 21.4 7 -6 4 145.99 10.6 -7 -6 -4 154.48 9.5 -7 6 4 154.28 9.9 -7 -6 -4 151.48 10.6 7 6 -4 159.38 17.1 7 -6 -4 140.39 9.9 7 6 4 161.08 16.2 7 6 4 148.19 10.9 7 -6 -4 123.89 11.1 -7 -6 4 138.79 10.2 -7 6 -4 146.39 10.7 -7 -6 4 137.99 10.8 -8 -6 -4 190.38 13.8 -8 6 4 200.68 11.7 8 6 -4 161.78 21.6 8 -6 4 183.68 12.4 8 -6 4 200.78 38.5 -8 -6 -4 192.18 12.6 -8 -6 -4 179.48 11.4 -8 -6 4 198.68 13.3 -8 -6 4 203.38 12.3 8 -6 -4 198.58 12.1 8 6 4 180.78 12.9 -8 6 -4 203.98 12.6 8 6 4 192.78 24.5 8 -6 -4 194.78 12.7 -9 6 4 288.17 15.3 9 -6 4 295.87 16.2 9 6 -4 254.37 27.5 -9 -6 -4 263.77 16 -9 -6 -4 292.97 17.1 9 -6 4 307.97 40.8 9 -6 -4 283.47 16.3 9 6 4 265.67 26.9 -9 6 -4 293.47 16 -9 -6 4 268.27 16.1 9 6 4 257.87 16.4 -9 -6 4 272.67 16 -10 -6 -4 41.4 7.7 10 6 -4 55.99 7.1 10 -6 4 49.5 6.6 -10 -6 -4 51.99 6.7 10 -6 -4 54.49 7.4 -10 -6 4 66.79 7 -10 6 -4 63.99 6.1 -11 -6 -4 24.5 4.1 11 -6 4 27.3 5.1 -11 6 -4 24 3.7 11 -6 -4 33.5 6.2 -11 -6 4 22.8 3.5 0 7 4 0.8 2.7 0 7 -4 1.3 3.9 0 7 4 5.4 2.8 1 -7 4 210.68 14.4 1 7 -4 263.27 16.4 1 7 4 234.88 14 -1 7 -4 232.58 15.6 -1 -7 4 225.58 12.5 1 7 4 254.67 14 2 -7 4 112.49 14.5 2 -7 4 130.29 8 2 -7 4 122.89 10.5 2 7 -4 149.09 13.1 2 7 -4 135.49 10.2 -2 -7 4 101.59 7.4 -2 7 -4 121.69 11.8 -2 7 -4 99.59 7.4 3 -7 4 845.02 41.2 3 -7 4 774.42 39.1 3 7 -4 876.81 41 -3 -7 -4 761.42 38.7 -3 -7 -4 831.72 39.1 -3 7 4 764.62 40 3 -7 4 753.42 44.6 3 7 -4 756.62 45.4 -3 -7 4 859.51 38.9 -3 7 -4 823.52 43.4 -3 -7 4 861.41 38.8 3 7 4 792.22 43.9 3 7 4 918.21 39.8 3 -7 -4 883.61 41.1 -3 -7 4 806.02 39.5 -3 7 -4 803.22 39 -4 7 4 385.36 19 4 -7 4 397.76 34.7 4 -7 4 417.46 23.2 4 7 -4 411.26 22.5 -4 -7 -4 389.46 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7.5 -5 -3 9 78.19 7 5 3 9 90.89 9.5 -6 3 9 215.98 12 -6 -3 -9 218.78 12.3 6 3 -9 230.58 18.9 6 -3 9 217.78 13 6 -3 9 215.58 16.9 -6 -3 -9 228.58 13.2 -6 -3 -9 214.18 14.8 6 3 -9 213.68 12.3 6 3 9 215.98 13.5 -6 -3 9 230.08 12.9 -6 -3 9 207.98 13.7 6 -3 -9 223.18 12.4 -6 3 -9 224.08 12.4 6 3 9 197.88 15.7 -6 3 -9 234.68 13.6 7 -3 9 32.4 8.1 7 -3 9 21.3 4.6 -7 -3 -9 12.1 4.9 7 3 -9 13.8 10.9 -7 3 9 21.1 3.6 7 3 -9 31.9 5.9 -7 -3 -9 18.4 3.5 -7 3 -9 10.9 4.4 -7 -3 9 19.5 4.1 7 -3 -9 14.7 3.4 7 3 9 18 7.1 -8 -3 -9 107.29 9.9 -8 -3 -9 123.69 12 8 -3 9 122.49 19.7 -8 -3 -9 98.59 8.3 8 3 -9 116.89 8.8 -8 3 9 120.29 8.8 8 -3 9 121.69 9.5 8 3 9 121.19 10.2 8 -3 -9 130.39 9.4 -8 3 -9 141.49 10.7 8 3 9 108.19 17.1 -8 -3 9 124.69 9.8 9 3 -9 102.09 7.6 9 -3 9 111.49 23.2 9 -3 9 81.19 8.4 -9 -3 -9 72.39 8.6 9 3 -9 54.69 22.3 -9 3 9 75.19 7.7 -9 -3 -9 89.49 10.1 -9 -3 9 99.69 8 9 3 9 77.79 9.2 -9 3 -9 101.59 9 9 3 9 116.09 24.3 9 -3 -9 80.89 7.8 9 -3 -9 98.29 9.2 -10 -3 -9 9.8 4.7 10 -3 9 9.1 3.9 -10 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4 -9 73.89 11.3 -5 4 9 241.58 14.1 -5 -4 -9 272.77 14.5 5 -4 9 263.87 14.9 -5 -4 -9 295.07 15.2 5 4 -9 279.77 14.5 -5 -4 -9 243.58 18.1 5 -4 9 281.37 18.1 5 4 -9 290.77 19 5 4 9 300.97 17.1 -5 4 -9 220.48 30.2 5 -4 -9 241.28 15.2 -5 -4 9 292.17 15.1 -5 4 -9 291.27 14.6 -5 4 -9 300.27 15.7 5 4 9 304.97 16.8 -5 -4 9 291.47 15.1 -6 -4 -9 27.9 4.6 6 -4 9 25.5 4.1 -6 4 9 29.5 4.9 6 -4 9 28 8.1 6 4 -9 23.3 3.5 6 4 -9 33.9 8.6 -6 -4 -9 19.9 5.9 -6 -4 -9 23.8 5.1 6 4 9 17.2 6.2 6 4 9 27.2 5.2 -6 -4 9 31 4.6 6 -4 -9 32.1 4.3 -6 -4 9 27.4 4.6 -6 4 -9 40.5 6.9 -7 -4 -9 190.78 12.5 7 4 -9 172.18 21.7 7 -4 9 190.68 12.1 -7 4 9 188.78 11.1 7 -4 9 180.18 18.4 -7 -4 -9 176.98 11.1 7 4 -9 176.78 11.2 -7 -4 -9 179.98 14.5 -7 4 -9 211.88 12.9 7 -4 -9 194.98 11.4 -7 -4 9 186.78 11.9 7 4 9 196.98 13 7 4 9 185.78 16.4 -7 -4 9 173.18 13.1 -8 4 9 281.97 15.2 -8 -4 -9 288.37 16.5 8 4 -9 288.47 15.3 8 -4 9 263.47 24.9 -8 -4 -9 298.27 18.2 8 4 -9 266.07 28.3 8 -4 9 276.87 15.9 -8 -4 -9 294.77 15.2 -8 4 -9 237.58 18.4 -8 -4 9 263.77 16 8 -4 -9 278.47 15.6 8 4 9 273.87 16.7 8 4 9 273.27 23.4 -9 4 9 88.39 8 -9 -4 -9 95.89 9 9 4 -9 81.49 19.9 -9 -4 -9 100.39 8.8 9 -4 9 82.59 17.7 9 -4 9 77.79 8 9 4 -9 102.49 7.8 -9 4 -9 93.39 9.2 9 -4 -9 98.49 9.5 9 -4 -9 86.49 7.8 -9 -4 9 105.89 8.5 9 4 9 88.89 16.9 -10 -4 -9 4.2 3.7 -10 -4 -9 6.6 4.2 -10 4 -9 7.6 3.4 -10 -4 9 13 3.3 10 -4 -9 4.8 4 11 -4 9 12.4 3.6 11 4 -9 14.8 3.7 -11 -4 -9 22.7 5.4 11 -4 -9 9.6 4.3 -11 -4 9 10.1 3.1 -11 4 -9 10.8 3.1 0 -5 9 512.75 26.1 0 5 -9 511.05 28.4 1 -5 9 296.17 16.6 1 -5 9 312.47 20 -1 -5 9 318.77 16.8 -1 5 -9 280.27 19.3 -1 5 -9 255.07 17.8 -1 -5 9 308.47 15.5 2 -5 9 987.2 53.59 2 5 -9 1059.39 49.7 2 5 -9 1058.19 50.89 2 5 -9 970.8 49.4 2 -5 9 997.3 48.9 2 -5 9 1036.9 50.39 2 5 -9 1005.4 52.89 -2 -5 9 1059.39 48.8 -2 5 -9 1064.79 52.89 -2 -5 9 1045.1 49.1 -2 5 -9 1063.89 49.3 -2 5 -9 1057.59 48.8 2 5 9 1092.99 51.09 3 -5 9 443.16 23.3 -3 -5 -9 384.26 21 3 5 -9 431.56 27.7 -3 -5 -9 401.16 21.5 3 5 -9 417.36 23.5 -3 -5 -9 417.56 25.3 3 -5 9 433.96 21.3 3 5 -9 374.46 30.2 3 -5 9 404.66 29.4 3 5 -9 404.36 20.9 3 5 9 427.26 26.7 -3 -5 9 445.66 21.4 -3 5 -9 464.85 27.2 -3 5 -9 458.85 21.7 -3 5 -9 473.25 21.1 -3 -5 9 439.26 21.1 4 -5 9 170.28 12.7 -4 -5 -9 150.38 8.8 -4 -5 -9 171.18 9.8 -4 -5 -9 156.58 20.3 4 -5 9 165.38 9.3 -4 -5 9 135.09 9.2 -4 -5 9 137.29 9.3 4 5 9 149.09 10.5 -4 5 -9 124.19 9.6 5 -5 9 276.47 18 -5 -5 -9 256.17 13.8 5 5 -9 252.37 13.8 -5 -5 -9 252.67 14.4 5 5 -9 271.17 19 -5 5 9 261.87 13.5 5 -5 9 267.97 14.4 5 5 9 251.97 16.3 -5 5 -9 256.67 14.3 5 -5 -9 234.28 15.2 -5 -5 9 257.67 14 -5 -5 9 253.17 14.4 -5 5 -9 277.37 14.8 6 -5 9 41.2 6.5 -6 -5 -9 43.3 7.2 -6 -5 -9 33.2 5.7 6 5 -9 43.6 6 -6 5 9 44.6 6.1 6 5 -9 45.2 9.5 6 -5 9 54.29 12.3 -6 -5 -9 55.49 8.1 -6 5 -9 57.19 7.6 -6 -5 9 57.99 7.3 -6 -5 9 47.7 6.6 6 5 9 50.49 11.3 7 5 -9 94.29 18.6 7 -5 9 71.09 7.9 7 5 -9 80.99 7.3 -7 -5 -9 73.99 7.1 -7 5 9 78.89 7.2 -7 -5 -9 81.49 8.3 -7 -5 -9 74.09 12.3 -7 -5 9 88.29 8.8 7 5 9 97.09 15.7 7 5 9 60.69 10.2 7 -5 -9 67.79 7.5 -7 -5 9 75.59 8 -7 5 -9 81.69 9 8 -5 9 16.8 6 -8 5 9 14 4.5 8 -5 9 15.2 12.1 -8 -5 -9 12.8 7.5 8 5 -9 30.1 12.7 -8 -5 9 15.2 6.2 8 -5 -9 16.9 7 8 5 9 11.8 10.6 -9 -5 -9 95.99 8 -9 -5 -9 105.69 10.7 9 5 -9 93.49 7.7 9 5 -9 62.29 28.2 9 -5 9 95.19 8.2 -9 -5 -9 81.29 8.4 9 -5 9 104.19 20.1 -9 5 -9 95.59 8.7 9 -5 -9 86.39 7.7 9 -5 -9 80.99 9.3 -9 -5 9 73.89 7.9 10 -5 9 38.8 6 -10 -5 -9 40.4 8.2 -10 -5 -9 46.8 6.4 10 -5 -9 41.3 7.5 -10 5 -9 42.1 6 -10 -5 9 50.29 6 11 5 -9 5.6 3.7 11 -5 9 5.2 3.3 -11 -5 9 0 3 -11 5 -9 4.4 2.7 0 -6 9 263.57 13.7 0 6 -9 261.17 13.5 0 -6 9 278.37 15.8 0 6 -9 262.67 14.3 0 6 -9 257.07 18.5 1 6 -9 218.38 16.6 1 -6 9 201.28 13.1 1 6 -9 209.28 10.9 1 -6 9 199.58 11 1 6 -9 183.88 11.7 -1 6 -9 213.48 11 -1 -6 9 184.18 10.9 -1 -6 9 205.98 13.1 -1 6 -9 185.68 16.4 -1 6 -9 212.18 11.7 -1 -6 9 206.38 11.8 -1 -6 9 202.78 10.8 2 -6 9 130.89 8.1 2 6 -9 145.59 7.9 2 6 -9 147.99 15.8 2 -6 9 133.29 10.7 2 -6 9 133.19 18.1 2 6 -9 146.29 9 -2 -6 9 120.29 8.5 -2 -6 9 130.49 8 -2 -6 9 122.89 7.7 -2 6 -9 112.39 14.2 -2 6 -9 116.79 8.4 -2 6 -9 111.19 7.8 3 6 -9 257.97 16.1 -3 -6 -9 255.87 13.4 -3 -6 -9 223.28 12.6 3 -6 9 252.07 12.7 3 6 -9 249.28 12.4 3 -6 9 215.58 27.3 3 6 -9 230.58 22.1 3 -6 9 268.37 15.6 3 6 -9 197.98 28 3 6 9 199.18 20.8 -3 -6 9 217.98 12.8 -3 -6 9 220.08 12.3 -3 -6 9 215.78 12.3 -3 6 -9 227.68 12.4 -3 6 -9 216.78 20.5 -3 6 -9 226.78 13 -4 -6 -9 80.09 6.2 4 -6 9 74.79 10.2 4 6 -9 76.69 6.1 4 -6 9 87.79 6.7 4 6 -9 91.29 11.3 -4 -6 -9 76.79 7.1 -4 -6 9 64.29 7.1 -4 -6 9 67.39 6.9 -4 6 -9 75.49 15.3 -4 6 -9 81.79 7.2 -4 -6 9 69.69 7.5 -4 6 -9 76.29 7.3 5 6 -9 98.69 6.8 -5 -6 -9 94.89 7.7 -5 -6 -9 88.19 6.9 5 6 -9 85.09 13.4 5 -6 9 108.59 12.4 5 -6 9 83.89 7.3 -5 -6 9 82.19 7.8 -5 -6 9 82.09 7.3 -5 6 -9 69.49 7.8 5 6 9 92.79 10.2 6 6 -9 47.7 10.7 -6 -6 -9 51.69 7.3 6 -6 9 46.6 6.8 6 6 -9 60.49 6 -6 -6 -9 52.19 6.1 6 -6 9 49.1 9.3 -6 -6 9 50.19 7 6 6 9 67.69 13.5 6 -6 -9 52.79 7.3 -6 6 -9 49.3 7.4 -6 -6 9 63.59 6.9 -7 -6 -9 213.08 12.3 7 -6 9 238.08 21.5 -7 -6 -9 206.98 17.8 7 -6 9 230.28 13.3 7 6 -9 184.38 22.2 -7 -6 -9 211.68 13.4 7 6 -9 213.98 12.4 -7 -6 9 223.88 13.3 7 -6 -9 221.28 12.8 7 6 9 230.38 18.9 -7 6 -9 201.58 13.4 -7 -6 9 196.98 12.9 7 -6 -9 177.88 14.1 -8 -6 -9 125.89 10.2 -8 -6 -9 119.99 9 8 -6 9 125.19 9.9 -8 -6 -9 122.09 14.5 8 6 -9 124.39 9.2 8 6 -9 118.39 23.3 8 -6 -9 128.49 9.5 8 6 9 119.59 23.1 8 -6 -9 147.29 11.2 -8 -6 9 133.49 10.2 -8 6 -9 135.39 10.4 -8 -6 9 133.39 11.5 -9 -6 -9 58.99 7.3 -9 -6 -9 54.39 6.8 9 6 -9 66.09 8.1 9 -6 9 57.79 7.2 -9 -6 -9 88.19 12.2 -9 -6 9 66.29 7.2 9 -6 -9 70.99 7 -9 6 -9 66.79 7.2 9 -6 -9 68.39 9.2 10 6 -9 67.49 6.9 10 -6 9 83.79 6.8 -10 -6 -9 59.19 6.7 -10 -6 -9 69.59 10.8 -10 -6 9 77.39 6.7 -10 6 -9 81.69 6.5 10 -6 -9 70.59 8.9 -11 6 -9 34 5.1 -11 -6 9 24.3 5.2 0 -7 9 186.28 12.8 0 -7 9 162.08 9.8 0 7 -9 170.78 17 0 7 -9 180.58 9.9 0 -7 9 180.58 11 0 7 -9 174.18 10.5 1 7 -9 750.02 40.5 1 7 -9 779.42 34.7 1 -7 9 760.92 37 1 7 -9 741.93 35.2 1 -7 9 725.33 34.8 -1 7 -9 697.13 35.1 -1 -7 9 718.13 34.6 -1 7 -9 698.13 40.1 -1 7 -9 697.33 34.6 -1 -7 9 722.63 34.8 -1 -7 9 757.82 37 -1 -7 9 706.83 35.3 2 7 -9 262.97 23.5 2 -7 9 280.17 27.4 2 -7 9 284.57 15 2 -7 9 285.27 17.5 2 7 -9 292.47 14.8 -2 7 -9 290.37 15 -2 -7 9 294.67 15.4 -2 7 -9 293.37 15.3 -2 -7 9 288.77 14.8 -2 -7 9 298.47 14.6 -2 7 -9 311.17 22.4 2 7 9 267.57 19.4 -3 -7 -9 131.09 8.4 3 7 -9 123.89 12.5 3 7 -9 138.79 7.9 -3 -7 -9 128.59 9.3 3 7 -9 102.69 22.3 3 -7 9 122.79 9.3 -3 -7 9 119.69 8.4 -3 7 -9 152.88 20.8 -3 7 -9 109.09 8.5 -3 -7 9 126.79 7.8 -3 -7 9 124.39 7.9 4 -7 9 467.45 25.4 4 7 -9 443.66 21.5 4 7 -9 437.96 25.6 -4 -7 -9 440.26 22.1 4 -7 9 432.16 21.9 -4 -7 -9 419.76 21.5 -4 7 -9 436.76 22.2 -4 -7 9 425.16 22.1 -4 -7 9 440.56 21.5 -4 -7 9 420.16 21.6 -4 7 -9 372.46 38.6 5 -7 9 28.7 7.9 5 -7 9 20.1 3.7 -5 -7 -9 21.2 3.4 -5 -7 -9 21.7 3.9 5 7 -9 21.2 8.5 5 7 -9 25.3 5.1 -5 -7 9 24.9 3.9 -5 7 -9 27.5 4.4 -5 -7 9 34.1 6.2 -6 -7 -9 38.3 5.2 6 -7 9 29 9.9 6 7 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9 73.69 7.5 -1 -8 9 97.49 10 -1 -8 9 71.99 6 2 8 -9 560.84 26 2 -8 9 565.54 26.7 2 8 -9 536.85 36.3 -2 -8 -9 497.25 27.8 2 -8 9 554.94 33.7 -2 -8 9 542.05 26.7 -2 8 -9 498.55 34.8 -2 8 -9 550.24 26.6 -2 -8 9 539.45 26.2 2 8 9 495.25 30.6 -2 -8 9 546.75 25.9 3 -8 9 211.68 11.3 -3 -8 -9 178.58 11.2 3 -8 9 204.38 15.5 -3 -8 -9 191.88 12.1 3 8 -9 183.28 11.1 -3 -8 9 197.68 11.6 -3 -8 9 192.28 11 -3 -8 9 191.68 12 -3 8 -9 200.98 11.5 -3 8 -9 184.88 29.1 4 8 -9 6.9 2.5 -4 -8 -9 2.9 2.8 4 -8 9 3.1 6.2 4 8 -9 7 7.1 4 -8 9 2.1 3 -4 -8 -9 3.6 3.3 -4 8 -9 -1 3.1 -4 -8 9 4.3 2.8 -4 -8 9 2.2 2.7 5 8 -9 56.89 11.3 5 8 -9 62.09 6.2 5 -8 9 65.39 6.7 -5 -8 -9 49.8 6.3 -5 -8 -9 45.2 7.1 5 -8 9 64.79 14.3 -5 -8 9 70.59 7.6 -5 -8 9 63.09 6.9 -5 8 -9 65.69 7.1 -5 -8 9 79.49 7.5 6 8 -9 128.29 9.2 6 8 -9 121.39 18.7 6 -8 9 162.28 19.2 -6 -8 -9 142.69 9.3 6 -8 9 129.59 9.7 -6 -8 -9 128.39 9.9 -6 -8 9 122.19 9.7 -6 8 -9 134.39 10.1 -6 -8 9 147.29 10.5 6 -8 -9 129.29 10.3 7 -8 9 6.4 3.8 7 8 -9 15.1 12 7 8 -9 21.2 4.8 -7 -8 -9 15.1 3.6 7 -8 9 10.6 12.7 -7 -8 -9 20.7 5 7 -8 -9 22 9.2 -7 -8 9 19 4.5 -7 -8 9 12.3 4.3 7 -8 -9 8 3.7 -7 8 -9 9.2 4.4 -8 -8 -9 35.1 5.5 -8 -8 -9 27.2 4.9 8 -8 9 40.5 6.4 8 8 -9 42.2 17.2 8 -8 9 14.3 19.8 -8 -8 9 32.5 6.8 -8 8 -9 39.5 6.8 8 -8 -9 29.5 4.5 8 -8 -9 27.7 6.4 -8 -8 9 30.9 5.3 -9 -8 -9 51.89 6.7 9 -8 9 53.19 6.3 -9 -8 -9 44.6 6 -9 8 -9 50.39 6.1 9 -8 -9 55.79 7.5 -9 -8 9 55.29 6.4 -10 -8 -9 28.1 5.6 10 8 -9 23.8 4.4 10 -8 9 20.2 3.5 -10 -8 9 25.7 3.9 -10 8 -9 32.1 4.8 0 -9 9 299.97 16.3 0 -9 9 297.67 18.9 0 9 -9 283.17 28.6 0 -9 9 277.87 15.4 1 -9 9 897.71 42.9 1 -9 9 964.2 46 1 -9 9 902.41 43.7 1 9 -9 879.11 52.59 1 9 -9 847.42 42.6 1 9 -9 946.91 43.4 -1 -9 9 900.21 42.9 -1 -9 9 886.01 43.4 -1 9 -9 882.01 43.1 -1 9 -9 829.82 52.29 -1 -9 9 937.91 42.9 -1 -9 9 939.81 46 2 9 -9 143.59 9.1 2 9 -9 136.79 30.9 2 -9 9 147.29 9 -2 -9 -9 153.28 16.3 2 -9 9 156.48 13.8 -2 -9 9 140.59 9 -2 -9 9 145.19 8.7 -2 9 -9 137.39 9.4 -2 -9 9 160.08 13.1 -2 9 -9 149.29 28.9 -3 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10 -9 1396.36 64.89 0 10 -9 1230.38 76.49 1 10 -9 38.1 5.9 1 -10 9 50.09 8.6 1 -10 9 49.2 11.5 1 -10 9 56.39 5.6 1 10 -9 36.6 20.4 -1 -10 9 41.2 5.2 -1 -10 9 47.8 8.5 -1 10 -9 32.1 19.4 -1 10 -9 53.29 5.8 -1 -10 9 52.49 5.6 -1 -10 9 63.79 11.2 2 -10 9 221.58 13 2 -10 9 258.77 18.4 -2 -10 9 247.38 17.8 -2 10 -9 233.88 13.3 -2 -10 9 230.08 13 -2 -10 9 239.98 12.8 -2 -10 9 232.08 14 -3 -10 -9 139.29 9.2 3 -10 9 143.99 16.3 3 -10 9 140.99 9.3 -3 -10 -9 142.09 10.3 -3 -10 9 135.89 10 -3 -10 9 141.09 8.8 -3 10 -9 137.79 9.6 -3 -10 9 127.99 8.9 -4 -10 -9 17.4 4.1 4 -10 9 14.1 3.3 4 -10 9 10.1 9.4 -4 -10 -9 13 3.3 -4 10 -9 17.7 3.7 -4 -10 9 24.2 4.8 -4 -10 9 13.5 3.6 -4 -10 9 15.9 3.7 5 -10 9 107.69 21.7 -5 -10 -9 146.49 9.4 5 -10 9 128.39 9.6 -5 -10 -9 143.89 10.1 -5 -10 9 144.09 9.5 -5 -10 9 137.09 10.8 -5 -10 9 124.39 9.5 -5 10 -9 127.69 10 -6 -10 -9 101.79 8.4 6 -10 9 121.19 23.8 -6 -10 -9 102.39 8.9 6 -10 9 91.89 8.6 -6 -10 9 100.89 9.6 -6 -10 9 101.69 8.5 -6 10 -9 119.29 9.3 6 -10 -9 101.29 9.7 7 -10 9 172.28 11.7 -7 -10 -9 183.78 12.1 7 -10 9 183.08 34.3 -7 -10 -9 187.58 11.3 -7 -10 9 192.58 12.3 -7 -10 9 199.28 11.7 -7 10 -9 183.18 12 -8 -10 -9 28.3 4.9 8 -10 9 29.2 4.5 -8 -10 -9 31.4 6.2 -8 10 -9 20.4 4 -8 -10 9 16.1 4.2 -9 -10 -9 -0.5 3.2 9 -10 9 4.8 3.2 -9 -10 -9 1.2 3.1 -9 -10 9 2.5 3.2 -9 10 -9 8.7 3 -10 -10 -9 38.8 4.4 10 -10 9 43.1 5.3 -10 -10 9 49.4 5.5 0 11 -9 608.84 30.4 0 -11 9 611.64 31.4 0 -11 9 601.04 30.1 0 -11 9 644.04 34.5 1 -11 9 650.93 31.3 1 -11 9 651.93 35.9 1 -11 9 660.53 32.7 -1 -11 9 627.94 31 -1 -11 9 615.54 32.2 -1 -11 9 642.04 35.8 -1 11 -9 622.94 31.5 -1 -11 9 658.03 31.3 2 -11 9 34.2 8.3 2 -11 9 22.7 3.9 -2 -11 -9 16.1 4.2 2 -11 9 18.9 5.9 -2 -11 9 21.6 4.8 -2 -11 9 24.2 4.9 -2 -11 9 17.4 3.3 -2 11 -9 26.6 4.2 -2 -11 9 10.1 7.9 3 -11 9 13.2 3.6 -3 -11 -9 14.1 4.5 -3 -11 -9 15.5 3.5 3 -11 9 4.3 9.7 -3 -11 9 16 3.2 -3 -11 9 15.3 3.3 -3 -11 9 15.6 4.6 -3 11 -9 28.7 5.9 -3 -11 9 20.2 7.8 4 -11 9 3.6 3.7 -4 -11 -9 8.4 4.1 4 -11 9 4 10.7 -4 -11 -9 9 3.2 -4 11 -9 16 4.2 -4 -11 9 11.8 3.3 -4 -11 9 11.1 4.5 -4 -11 9 3.6 3.3 -5 -11 -9 8.5 3.3 -5 -11 -9 5.1 3.9 5 -11 9 -16.7 14.4 5 -11 9 4.6 3.5 -5 11 -9 7.7 3.8 -5 -11 9 3.5 3.3 -5 -11 9 8.3 3.5 6 -11 9 174.78 30.9 6 -11 9 136.29 10 -6 -11 -9 150.58 9.9 -6 -11 -9 135.79 10.1 -6 -11 9 140.99 10 -6 -11 9 144.89 11.2 -6 11 -9 150.38 10.3 -7 -11 -9 6.7 3.8 -7 -11 -9 12.6 3.1 7 -11 9 10.5 3.6 -7 -11 9 22.6 13.6 -7 -11 9 3.7 3.9 -7 11 -9 9.7 3.6 -7 -11 9 10.9 3.7 -8 -11 -9 130.99 9.1 8 -11 9 129.89 9 -8 -11 -9 132.29 8.3 -8 -11 9 132.49 9.7 -8 -11 9 122.99 9.4 -8 11 -9 125.79 8.7 -9 -11 -9 3.7 3 -9 -11 -9 6.7 3.8 9 -11 9 8.5 2.9 -9 -11 9 1.1 3.5 -9 11 -9 10.2 3.1 0 -12 9 209.78 12.1 0 -12 9 196.58 19.4 0 12 -9 203.18 12.4 0 -12 9 216.88 15.1 0 -12 9 209.18 11.9 1 -12 9 111.59 8.3 1 -12 9 91.09 17.2 1 -12 9 116.19 13.1 -1 -12 9 116.49 17.2 -1 -12 9 111.59 7.7 -1 -12 9 111.59 8 -1 -12 9 106.79 10.8 -1 12 -9 94.59 8.3 2 -12 9 13.1 3.8 2 -12 9 21.8 8.1 -2 -12 -9 11.6 4 2 -12 9 7.2 9.4 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-13 9 661.13 33.6 -1 -13 9 673.43 31.7 -1 -13 9 684.13 32 2 -13 9 118.09 22.3 -2 -13 -9 129.69 9.9 2 -13 9 119.19 9.2 -2 -13 9 140.69 9.4 -2 -13 9 153.18 12 -2 13 -9 131.59 9.5 -2 -13 9 138.99 19.8 -2 -13 9 141.59 9 3 -13 9 231.78 13.8 -3 -13 -9 212.18 14.7 -3 -13 -9 226.78 13.5 3 -13 9 245.78 28.5 -3 -13 9 240.58 23.3 -3 13 -9 237.18 13.8 -3 -13 9 233.78 13.3 -3 -13 9 240.18 13.6 -3 -13 9 272.47 16 -4 -13 -9 7.7 5.1 -4 -13 -9 -3.5 6.2 4 -13 9 24.3 16.4 4 -13 9 4 5.5 -4 -13 9 9.5 4.3 -4 -13 9 12.9 6.5 -4 -13 9 -13.3 11.2 -4 -13 9 2.4 5 -4 13 -9 6.6 5.4 5 -13 9 90.49 24.7 5 -13 9 52.49 6.7 -5 -13 -9 54.69 6.6 -5 -13 -9 48.3 7.3 -5 -13 9 55.69 6.8 -5 -13 9 47.2 8.6 -5 -13 9 42 7.1 -5 13 -9 57.49 6.6 -5 -13 9 36.8 13.9 -6 -13 -9 99.69 7.5 -6 -13 -9 89.09 8.1 6 -13 9 85.89 7.7 -6 13 -9 91.89 7.6 -6 -13 9 90.69 9.5 -6 -13 9 92.79 7.7 7 -13 9 105.89 8.4 -7 -13 -9 111.99 7.6 -7 -13 -9 126.09 8.9 -7 13 -9 125.69 8.2 -7 -13 9 120.49 9.5 -7 -13 9 123.09 8.4 8 -13 9 8.7 3.1 -8 -13 -9 11.8 3.4 -8 -13 -9 9 2.6 -8 13 -9 14.7 3.5 -8 -13 9 12.3 4.3 0 -14 9 34.7 12.4 0 -14 9 22.9 3.9 0 -14 9 29.1 8.9 0 -14 9 26.1 4.1 -1 -14 -9 135.49 10.7 1 -14 9 134.09 9.8 1 -14 9 136.69 26.1 -1 -14 9 137.69 22.7 -1 -14 9 165.98 14.5 -1 -14 9 153.18 9.9 -1 14 -9 138.79 10 -1 -14 9 155.88 9.7 2 -14 9 149.39 35.7 2 -14 9 215.68 12.6 -2 -14 -9 233.28 12.8 -2 -14 9 181.68 25.6 -2 -14 9 218.58 12.2 -2 14 -9 204.28 12.5 -2 -14 9 205.88 12.2 -2 -14 9 174.48 16 3 -14 9 58.79 21.9 -3 -14 -9 96.69 10.2 3 -14 9 91.69 10.1 -3 -14 -9 99.29 8.7 -3 -14 9 96.39 17.6 -3 -14 9 64.89 12.4 -3 -14 9 85.39 10.1 -3 -14 9 105.49 9.8 4 -14 9 46.7 6.5 -4 -14 -9 55.79 8 4 -14 9 73.59 29.1 -4 -14 -9 50.69 6.6 -4 -14 9 41.8 6.3 -4 14 -9 35.1 6.2 -4 -14 9 33.3 6.2 -4 -14 9 29.4 6 -4 -14 9 31.4 15.9 5 -14 9 38.5 6.2 -5 -14 -9 41.8 6.1 -5 -14 -9 43.1 7.3 -5 -14 9 33.2 6.9 -5 -14 9 65.09 17.6 -5 -14 9 59.09 8.6 -5 -14 9 37.8 6.1 -5 14 -9 46.4 6 -6 -14 -9 18.4 3.3 -6 -14 -9 19.6 4.3 6 -14 9 17.8 3.8 -6 -14 9 21.9 3.9 -6 14 -9 25.2 3.9 -6 -14 9 24.3 5.3 -7 -14 -9 11.3 2.7 -7 -14 -9 16.8 4.9 7 -14 9 8.8 3.1 -7 -14 9 7.5 3.6 -7 -14 9 6.5 4.7 -7 14 -9 13.8 3.2 -8 -14 -9 44.9 4.8 -8 -14 -9 50.69 6.4 8 -14 9 27.8 4.4 -8 -14 9 34 6.4 0 -15 9 7 3.7 0 -15 9 -14.6 15.6 1 -15 9 93.89 18.8 1 -15 9 71.29 7.2 -1 -15 -9 53.19 6.1 1 -15 9 66.29 6.7 -1 -15 9 62.39 6.8 -1 -15 9 79.59 16.3 -1 -15 9 61.19 6.6 2 -15 9 53.69 23.7 -2 -15 -9 33.6 4.7 2 -15 9 34.1 6.1 -2 -15 9 30 5.7 -2 -15 9 30.4 8.7 -2 -15 9 66.69 17.9 -2 -15 9 37.8 6.2 -3 -15 -9 269.57 15.2 -3 -15 -9 262.67 17 3 -15 9 290.87 15.6 -3 -15 9 283.17 15.4 -3 -15 9 230.28 42.2 -3 -15 9 322.97 15.3 -3 -15 9 264.77 18.2 -3 15 -9 277.77 15.4 4 -15 9 7.2 3.4 -4 -15 -9 10.8 3.3 -4 -15 -9 21.2 5.1 -4 -15 9 15.7 3.8 -4 -15 9 8.7 6.2 -4 15 -9 14.4 3.7 -4 -15 9 11.7 3.4 -5 -15 -9 11.9 3.3 -5 -15 -9 13 4.2 5 -15 9 9 3.4 -5 -15 9 17.5 6.4 -5 15 -9 16.5 3.5 -5 -15 9 12.4 3.3 6 -15 9 -1 2.9 -6 -15 -9 -0.1 3.7 -6 -15 -9 3.4 2.6 -6 -15 9 -2.4 2.7 -7 -15 -9 74.89 5.4 -7 -15 -9 73.39 7.1 7 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133.79 16.6 6 -6 -14 149.59 11.2 -6 -6 14 158.08 15.5 -6 6 -14 163.08 11.4 -6 -6 14 144.29 10 -7 -6 -14 102.69 9.5 7 -6 14 80.29 13.7 7 -6 14 91.59 8.2 7 6 -14 124.09 21.7 7 6 -14 93.19 7.7 -7 -6 -14 100.29 7.7 7 -6 -14 84.39 8.4 -7 -6 14 62.39 13.5 -7 -6 14 79.79 8.2 -7 6 -14 89.89 9.1 -8 -6 -14 56.69 6.2 8 -6 14 59.09 6.9 8 6 -14 51.59 6.3 -8 -6 -14 50.89 7.6 -8 -6 14 61.29 6.5 -8 6 -14 60.99 7.5 8 -6 -14 50.39 6.9 -9 -6 -14 99.29 8.1 9 -6 14 94.49 7.8 9 6 -14 96.19 8.5 -9 -6 -14 102.19 8.5 -9 -6 14 95.29 7.2 -9 6 -14 87.19 7.7 9 -6 -14 101.49 7.6 -10 6 -14 78.49 6.7 -10 -6 14 91.09 6.8 0 -7 14 1.2 3.1 0 7 -14 2.1 4.1 0 -7 14 2.4 5 0 7 -14 0.3 2.3 0 -7 14 0.3 2.9 0 -7 14 0.9 2.4 1 -7 14 277.67 14.5 1 7 -14 290.37 14.4 1 -7 14 271.07 17.6 1 7 -14 263.07 16.6 1 -7 14 283.37 14.2 -1 -7 14 272.67 15.1 -1 7 -14 266.57 15.4 -1 7 -14 261.57 14.2 -1 -7 14 265.17 17.5 -1 -7 14 262.17 14.4 2 -7 14 251.87 14.1 2 7 -14 271.57 14 2 -7 14 253.17 17.3 -2 -7 14 259.57 17.1 -2 7 -14 253.57 13.8 -2 -7 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147.09 10.1 8 -7 14 255.97 14.2 -8 -7 -14 267.87 13.8 8 7 -14 233.18 13.8 -8 -7 -14 263.37 14.8 -8 7 -14 244.08 14.6 8 -7 -14 244.18 14.4 -8 -7 14 252.67 14.2 -9 -7 -14 0.8 3.2 -9 -7 -14 7.8 3.5 9 -7 14 5.2 3.4 -9 7 -14 5.4 3.4 -9 -7 14 0.2 2.8 9 -7 -14 5.5 3.3 10 7 -14 20 3.9 -10 7 -14 19.1 3.2 -10 -7 14 17.3 3.4 0 8 -14 127.59 8.5 0 -8 14 131.99 9.3 0 8 -14 130.59 9.6 0 -8 14 140.59 12.9 0 -8 14 146.29 8.6 0 -8 14 135.89 8.8 1 -8 14 34.1 6.6 1 -8 14 43.4 5.3 1 8 -14 42.3 5.3 1 8 -14 33.7 6.7 1 -8 14 42 5.2 -1 -8 14 41.8 5.5 -1 -8 14 42 9.9 -1 8 -14 41.1 5.2 -1 8 -14 52.49 7 -1 -8 14 35.4 6.5 2 -8 14 1.1 2.6 2 -8 14 -5.6 5.1 2 8 -14 3.3 2.6 -2 8 -14 3.1 3.7 -2 8 -14 3.6 2.8 -2 -8 14 3.5 5.7 -2 -8 14 3.5 2.7 -2 -8 14 6.2 3.3 -3 -8 -14 175.78 12.5 3 -8 14 156.68 15.4 3 8 -14 179.28 10.4 -3 -8 -14 166.88 10.9 3 -8 14 163.08 10.7 -3 8 -14 191.08 11.9 -3 8 -14 160.18 10.6 -3 -8 14 182.08 10.5 -3 -8 14 179.08 11.2 -3 -8 14 182.98 15.4 4 -8 14 74.99 13.9 4 -8 14 68.79 7.1 -4 -8 -14 65.09 8.6 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66.99 8 0 9 -15 80.79 6.8 1 -9 15 716.33 38.8 1 -9 15 709.33 34.7 1 9 -15 728.33 34.9 1 -9 15 742.23 35.3 1 9 -15 751.32 36 1 -9 15 739.33 35.9 -1 -9 15 676.63 36.8 -1 -9 15 710.83 35.2 -1 -9 15 756.82 35.8 -1 9 -15 694.93 34.8 -1 9 -15 733.23 35.8 -1 -9 15 734.23 39.1 2 -9 15 31.8 5.9 2 -9 15 56.39 12.2 2 -9 15 40.9 5.8 2 9 -15 28.8 5.5 -2 -9 15 43.9 5.7 -2 -9 15 39.4 8.1 -2 -9 15 48.1 6.8 -2 9 -15 45.6 6.8 -2 9 -15 49.3 7 3 -9 15 94.19 7.9 3 9 -15 99.89 7.4 3 -9 15 96.89 14.6 -3 -9 -15 103.99 11.6 -3 -9 -15 91.29 8.6 -3 -9 15 87.09 7.5 -3 -9 15 96.79 14.1 -3 9 -15 105.09 9.1 -3 -9 15 104.29 8.6 4 -9 15 187.08 19.5 -4 -9 -15 201.58 12 -4 -9 -15 178.38 13.2 4 9 -15 198.78 11.6 4 -9 15 199.58 12 -4 -9 15 192.28 11.9 -4 9 -15 213.48 13.2 -4 -9 15 196.28 12.8 -4 -9 15 207.18 18.1 5 9 -15 33.4 6.6 5 -9 15 14.6 10.6 -5 -9 -15 40.8 7 -5 -9 -15 32.8 6 5 -9 15 28.9 4.7 -5 -9 15 35.3 9.9 -5 -9 15 45.9 7.8 -5 -9 15 38.7 7.4 6 9 -15 26.3 4 -6 -9 -15 33 5.4 -6 -9 -15 27.9 5.6 6 -9 15 25.8 13 6 -9 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122.89 10.6 1 -6 22 127.49 9.8 -1 -6 22 142.09 9.7 -1 6 -22 124.19 14.1 -1 6 -22 126.59 9.3 2 6 -22 50.39 7.2 2 -6 22 38.7 6.6 2 -6 22 74.39 14.7 -2 -6 -22 42.9 7.8 -2 6 -22 60.29 6.6 -2 6 -22 64.09 11.6 -2 -6 22 62.09 7 3 -6 22 185.28 18.9 3 -6 22 215.68 13.7 3 6 -22 222.78 13.1 -3 -6 -22 223.98 13.3 -3 -6 22 240.68 13.4 -3 6 -22 227.58 16.1 -3 6 -22 225.58 12.9 -4 -6 -22 71.69 7.6 4 -6 22 116.29 18.6 4 6 -22 87.59 7.6 -4 -6 22 91.39 7.7 -4 6 -22 79.59 10.6 -4 6 -22 75.09 7.5 5 6 -22 44.7 6 -5 -6 -22 38.4 6.2 -5 -6 22 38.4 5.7 -5 6 -22 38.1 6.5 -5 6 -22 44.4 9 6 6 -22 10.4 2.9 -6 -6 -22 10.3 3.1 6 -6 -22 12.9 5.7 -6 6 -22 14.1 4.7 -6 -6 22 13.2 3.2 -7 -6 -22 13.5 3 -7 -6 22 14.7 3.3 7 -6 -22 12.4 4.2 -7 6 -22 21.1 5.1 -8 -6 -22 95.19 7 0 7 -22 2.7 3.2 0 7 -22 0.1 6.2 0 -7 22 18.7 8 0 -7 22 3.7 3.4 1 -7 22 1.7 8.3 1 -7 22 15.8 4.3 1 7 -22 13.9 3.7 -1 7 -22 12.5 3.5 -1 -7 22 6.3 8.8 -1 -7 22 12.6 4.1 -1 7 -22 16.4 7 -2 -7 -22 107.79 9.9 2 -7 22 121.49 10.8 2 7 -22 131.59 9.6 2 -7 22 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12.8 -4 -8 22 196.08 11.6 5 8 -22 92.89 7 -5 -8 -22 102.09 7.5 5 -8 22 98.49 8.1 -5 -8 22 89.29 7.4 -5 8 -22 87.19 8.9 6 8 -22 30.2 5.3 6 -8 22 38.7 5.6 -6 -8 -22 41.8 5.2 -6 -8 22 38.6 5.1 -6 8 -22 48 7.6 7 -8 22 114.09 7.4 -7 8 -22 85.19 8.2 -7 -8 22 98.59 6.9 0 -9 22 37.1 10.7 0 9 -22 33 5.9 0 -9 22 45.1 6.9 1 9 -22 56.49 6.3 1 -9 22 48.7 7.3 1 -9 22 39.2 8.2 -1 -9 22 65.59 6.7 -1 -9 22 47.2 11.6 -1 9 -22 46.8 6.5 -1 9 -22 73.29 9.6 -2 -9 -22 44 5.5 2 -9 22 24.8 11.9 2 -9 22 61.29 7.9 2 -9 22 44.4 7 2 9 -22 47.7 6 -2 9 -22 34.1 4.7 -2 9 -22 60.49 8.9 -2 -9 22 27.4 18 3 -9 22 7.1 14.7 3 -9 22 1.3 4.2 3 -9 22 -2.3 3.1 -3 9 -22 -4.4 4.2 -3 -9 22 -0.8 3.1 4 -9 22 82.09 7.5 4 9 -22 67.09 6.6 4 -9 22 85.89 8.7 -4 -9 -22 74.49 7.3 -4 -9 22 78.69 7.1 -4 9 -22 92.29 8.7 5 -9 22 4.7 3.1 -5 -9 -22 3.1 3 5 9 -22 1.6 3.3 -5 9 -22 7.3 4.1 -6 -9 -22 147.19 9.4 6 -9 22 128.29 11.3 -6 -9 22 144.79 9.6 -6 9 -22 133.69 9.8 7 -9 22 35.4 5.5 -7 9 -22 36.1 4.7 -7 -9 22 32 5.1 0 10 -22 63.29 7.6 0 -10 22 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9.7 3.1 -2 0 -23 10 3.4 -3 0 -23 96.49 8.4 3 0 -23 119.19 9 4 0 -23 106.49 8.6 -4 0 -23 94.89 8.2 -5 0 -23 6.8 3.2 5 0 -23 8 3.3 -6 0 -23 207.28 11.5 6 0 -23 184.38 11.5 -7 0 -23 1.4 3 7 0 -23 5.7 2.8 8 0 -23 30.7 4.8 0 1 -23 121.99 9 0 -1 -23 120.09 9 0 -1 23 115.79 8.1 1 1 -23 29.2 4.3 1 -1 23 30.8 5.4 -1 -1 -23 26 4.3 -1 -1 23 26.5 3.6 1 -1 -23 24 4.2 1 1 23 24.1 3.5 -1 1 -23 20.3 4.2 -2 -1 -23 251.87 14.4 2 1 -23 259.97 14.7 2 -1 23 264.47 14.3 2 1 23 262.57 13.7 -2 1 -23 247.68 14.4 2 -1 -23 259.07 14.9 -2 -1 23 233.78 13.5 -3 -1 -23 65.89 6.8 3 1 -23 57.59 7.5 3 -1 -23 71.49 8.1 -3 -1 23 48.7 6.6 -3 1 -23 48.5 6.9 -4 -1 -23 145.49 10.2 4 1 -23 158.58 10.6 -4 1 -23 157.08 10.3 4 -1 -23 148.39 10.4 5 1 -23 211.98 12.5 -5 -1 -23 207.18 12.3 5 -1 -23 187.68 12.4 -5 1 -23 221.08 12.4 6 1 -23 4.6 3.1 -6 -1 -23 -1.7 2.8 -6 1 -23 -2.1 2.8 6 -1 -23 0.4 2.8 7 1 -23 154.38 9.2 -7 -1 -23 148.69 9.5 7 -1 -23 147.39 9.3 -7 1 -23 140.79 11.7 8 1 -23 4 2.5 8 -1 -23 3.4 2.8 0 2 -23 37.2 6.4 0 -2 23 38.1 5.9 0 -2 -23 38.7 6.6 1 -2 23 196.88 11.8 1 2 -23 200.58 12.2 -1 -2 -23 194.08 12.1 -1 2 -23 200.08 12.2 1 -2 -23 202.58 12.3 -1 -2 23 194.88 11.4 2 -2 23 70.09 7 2 2 -23 57.29 7.2 -2 -2 -23 51.69 7 -2 -2 23 66.19 6.2 2 -2 -23 67.99 8.1 -2 2 -23 73.89 7.2 2 2 23 56.19 6.2 3 2 -23 89.59 8.2 -3 -2 -23 82.69 7.8 3 2 23 79.49 7.4 -3 2 -23 90.89 7.9 -3 -2 23 84.59 7.1 3 -2 -23 90.09 9.3 4 2 -23 212.98 12.1 -4 -2 -23 201.38 11.7 -4 2 -23 188.58 11.6 -4 -2 23 167.08 10.9 4 -2 -23 172.18 12 -5 -2 -23 42.5 6.3 5 2 -23 56.09 6.7 5 -2 -23 45.5 7 -5 2 -23 44.5 6.1 -6 -2 -23 93.39 7.4 6 2 -23 90.59 7.4 -6 2 -23 88.69 7.2 6 -2 -23 91.69 7.8 7 2 -23 17.9 3.3 -7 -2 -23 11.6 3.3 -7 2 -23 11 4.4 7 -2 -23 10.2 3.9 8 2 -23 33 5 8 -2 -23 25.4 4.9 0 3 -23 123.39 9.3 0 -3 23 129.09 9 0 -3 -23 125.49 9.6 -1 -3 -23 2.5 3.4 1 -3 23 2.5 3.1 1 3 -23 5.5 3.4 -1 3 -23 1.2 3.3 1 -3 -23 2.4 4.1 2 -3 23 97.59 8.1 -2 -3 -23 80.69 7.8 2 3 -23 95.89 8.3 2 -3 -23 93.69 9.4 -2 -3 23 79.89 7.5 -2 3 -23 98.59 8.1 -3 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29 9.8 2.6 1 7 -29 7.1 2.7 -1 -7 -29 5.9 4.7 -1 7 -29 3.1 3 -1 -7 29 1.6 3 -2 -7 -29 66.79 7.6 2 -7 29 69.59 5.5 2 7 -29 63.89 5.8 3 7 -29 38.4 5.5 3 -7 29 37.2 4.8 0 -8 29 1.4 2.6 1 -8 29 32.8 4.3 -1 -8 29 26.9 5 2 -8 29 34 4.5 3 -8 29 16.8 3.1 0 -9 29 57.49 5.3 1 -9 29 4.8 2.6 2 -9 29 29.1 4.6 0 0 -30 237.58 13 -1 0 -30 18 3.2 1 0 -30 16.7 3.2 -2 0 -30 33.6 4.8 2 0 -30 25 4.9 3 0 -30 13.4 3 4 0 -30 14.9 2.9 -4 0 -30 25 4.3 5 0 -30 29.6 6.1 0 1 -30 106.59 7.3 0 -1 -30 98.69 7.4 -1 -1 -30 85.89 6.7 1 1 -30 78.69 6.5 -1 1 -30 91.99 6.7 1 -1 -30 89.59 6.6 2 1 -30 14.3 3 -2 -1 -30 13 3 -2 1 -30 16.5 3 2 -1 -30 12.2 4.3 3 -1 -30 21.9 3.3 4 1 -30 16.2 2.9 -4 -1 -30 22.9 3.1 4 -1 -30 14.3 3.1 -4 1 -30 23.4 4.3 -5 -1 -30 5.7 3.7 5 1 -30 3 2.5 0 -2 -30 17.4 3.3 0 2 -30 19.3 3.1 1 2 -30 23.7 3.6 -1 -2 -30 24.5 5 -1 2 -30 25.2 4.5 1 -2 -30 29.7 5 2 2 -30 62.99 5.6 -2 -2 -30 68.99 5.8 -2 2 -30 61.49 5.6 2 -2 -30 66.39 6 -3 -2 -30 0.4 2.4 3 2 -30 1.2 2.8 3 -2 -30 -0.3 2.9 -3 2 -30 2.8 2.6 4 2 -30 10.4 2.6 -4 -2 -30 9.7 2.5 -4 2 -30 5.6 2.6 4 -2 -30 6.6 3.1 5 2 -30 12.2 3.2 0 3 -30 17.2 3.1 -1 -3 -30 33.6 6.9 1 3 -30 27.6 4.6 1 -3 -30 37.1 5.5 -1 3 -30 32.1 4.6 2 3 -30 30.9 4.4 -2 -3 -30 31.4 5.6 -2 3 -30 34.6 4.6 3 3 -30 66.29 5.5 -3 -3 -30 61.49 5.6 -3 3 -30 55.99 5.4 -4 -3 -30 13.6 2.8 4 3 -30 12.6 2.7 -4 3 -30 13.1 3.1 0 -4 -30 21.3 3.7 0 4 -30 24.4 4.6 1 4 -30 5.3 2.4 -1 -4 -30 7.7 3 -1 4 -30 3 2.5 1 -4 -30 -0.4 3.1 -2 -4 -30 24.9 3.6 -2 4 -30 30.7 4.6 -3 -4 -30 65.89 5.4 3 4 -30 49.1 5.4 3 -4 -30 50.19 7 -3 4 -30 60.79 5.4 -4 -4 -30 9.7 2.6 4 4 -30 12.3 2.7 0 -5 -30 -2.8 3.7 -1 -5 -30 153.98 9.1 1 5 -30 128.79 10.6 1 -5 -30 120.79 10.1 -1 5 -30 135.19 8.3 2 5 -30 7.1 2.6 -2 -5 -30 3.5 3 -2 5 -30 1.2 2.6 -3 -5 -30 34.2 5.5 3 5 -30 26 4.5 -4 -5 -30 97.69 7 4 5 -30 90.89 6.5 0 6 -30 99.09 6.8 0 -6 -30 113.39 10.5 -1 -6 -30 18.4 4.1 1 6 -30 23.3 4.6 -1 6 -30 13.2 2.9 2 6 -30 24 4.5 -2 -6 -30 32.4 5.9 3 6 -30 27.3 3.4 -3 -6 -30 33.7 5.4 0 7 -30 2.7 3.8 1 7 -30 -0.4 3.2 1 0 -31 38.1 5.1 2 0 -31 77.69 6.2 -2 0 -31 83.29 6.1 -3 0 -31 18.5 2.8 4 0 -31 -0.7 2.7 -4 0 -31 0.1 2.4 0 1 -31 15.4 4 0 -1 -31 12.8 3 -1 -1 -31 40 5.1 1 1 -31 44.5 6.8 1 -1 -31 39.7 5 2 1 -31 48.4 5.1 -2 -1 -31 55.19 5.4 2 -1 -31 64.99 5.6 -2 1 -31 63.59 5.4 3 1 -31 38.4 4.5 -3 -1 -31 29.9 4.5 -3 1 -31 32.1 4.4 3 -1 -31 25.6 5.2 -4 -1 -31 -0.1 2.4 -4 1 -31 0.6 4.3 0 -2 -31 2.6 2.6 -1 -2 -31 0.5 2.5 1 2 -31 3.5 2.9 1 -2 -31 1.6 2.7 -1 2 -31 2.7 3.2 -2 -2 -31 7.1 2.6 2 2 -31 7.8 2.5 -2 2 -31 11.6 2.6 2 -2 -31 6.7 2.9 -3 -2 -31 30.1 4.5 3 2 -31 20.8 4.2 -3 2 -31 20.1 4.2 3 -2 -31 30.8 5.6 -4 -2 -31 28.6 4.4 4 2 -31 33.4 4.7 0 3 -31 8.8 2.8 0 -3 -31 8.2 2.9 -1 -3 -31 13.4 3 1 3 -31 13.5 2.8 -1 3 -31 12.9 2.8 1 -3 -31 12.9 3.3 -2 -3 -31 30.9 4.7 2 3 -31 21.8 3.2 -2 3 -31 21.9 4.2 2 -3 -31 30.9 5.7 3 3 -31 10.6 2.6 -3 -3 -31 8.9 2.6 -3 3 -31 7.5 2.6 -4 -3 -31 24.7 5.1 0 -4 -31 -3.7 3 0 4 -31 2.2 2.4 -1 -4 -31 101.89 7.8 1 4 -31 107.79 7 1 -4 -31 112.99 9.2 -1 4 -31 119.19 7.1 2 4 -31 11.1 2.6 -2 -4 -31 9.6 2.9 -2 4 -31 9.2 2.8 3 4 -31 10.4 2.6 -3 -4 -31 8.3 2.8 0 5 -31 23.3 4.3 -1 -5 -31 3.1 3.3 1 5 -31 0.9 2.5 -1 5 -31 7.2 2.6 -2 -5 -31 41.3 5.8 2 5 -31 39.7 4.7 0 6 -31 13.1 3.6 1 6 -31 19.3 3.4 0 0 -32 -3.2 2.3 -1 0 -32 81.59 5.8 1 0 -32 81.69 6.1 2 0 -32 9.3 2.8 -3 0 -32 53.89 5 0 1 -32 55.49 5.1 0 -1 -32 48.1 5.1 1 1 -32 3.9 2.2 -1 1 -32 4.8 2.4 1 -1 -32 3.3 2.7 2 1 -32 47.2 5.1 -2 -1 -32 52.49 4.7 -2 1 -32 51.29 4.7 2 -1 -32 37.6 5.3 -3 -1 -32 9.4 2.6 3 1 -32 9.7 2.8 -3 1 -32 13.7 3 0 2 -32 20.4 4.2 -1 -2 -32 12.5 2.7 1 2 -32 14.8 2.6 1 -2 -32 10 3 -1 2 -32 11.8 2.6 -2 -2 -32 17.5 2.8 2 2 -32 14.3 2.8 -2 2 -32 11.3 2.6 2 -2 -32 7.8 4.3 -3 -2 -32 24.9 4 3 2 -32 21.9 3.4 0 -3 -32 10.8 3.1 -1 -3 -32 46.7 5.1 1 3 -32 41.5 4.7 -1 3 -32 36.7 4.6 1 -3 -32 36 5.8 2 3 -32 77.99 5.9 -2 -3 -32 84.09 6.2 -2 3 -32 87.69 6.2 0 4 -32 0.4 2.5 1 4 -32 24.7 4.6 -1 4 -32 39.6 4.7 2 4 -32 -1.6 2.6 0 0 -33 -3.2 2.4 1 0 -33 2.8 3.4 -1 0 -33 -1.2 2.5 0 1 -33 3.2 2.5 0 -1 -33 0.1 3.4 1 1 -33 10.4 2.9 -1 -1 -33 11.7 3.8 -1 1 -33 12.8 2.7 0 2 -33 10 2.5 loop_ _twin_individual_id _twin_individual_mass_fraction_refined 1 0.943(17) 2 0.057(17)