data_mono_p_a _audit_creation_date 2019-05-19 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _shelx_SHELXL_version_number '2014/7' _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_name '' _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C21 H23 Cl N2 O4 S' _chemical_formula_sum 'C21 H23 Cl N2 O4 S' _chemical_formula_weight 434.92 _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'monoclinic' _space_group_IT_number 14 _space_group_name_H-M_alt 'P 1 21/c 1' _space_group_name_Hall '-P 2ybc' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 9.0240(9) _cell_length_b 13.3762(13) _cell_length_c 18.311(2) _cell_angle_alpha 90 _cell_angle_beta 103.731(3) _cell_angle_gamma 90 _cell_volume 2147.2(4) _cell_formula_units_Z 4 _cell_measurement_reflns_used 46529 _cell_measurement_temperature 273.0(2) _cell_measurement_theta_max 24.995 _cell_measurement_theta_min 2.323 _shelx_estimated_absorpt_T_max 0.942 _shelx_estimated_absorpt_T_min 0.920 _exptl_absorpt_coefficient_mu 0.305 _exptl_absorpt_correction_T_max 0.7461 _exptl_absorpt_correction_T_min 0.6434 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1707 before and 0.0740 after correction. The Ratio of minimum to maximum transmission is 0.8624. The \l/2 correction factor is Not present.' _exptl_absorpt_special_details ? _exptl_crystal_colour 'clear light yellow' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier light _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 1.345 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description block _exptl_crystal_F_000 912 _exptl_crystal_size_max 0.28 _exptl_crystal_size_mid 0.25 _exptl_crystal_size_min 0.2 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0213 _diffrn_reflns_av_unetI/netI 0.0088 _diffrn_reflns_Laue_measured_fraction_full 0.980 _diffrn_reflns_Laue_measured_fraction_max 0.980 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_number 46529 _diffrn_reflns_point_group_measured_fraction_full 0.980 _diffrn_reflns_point_group_measured_fraction_max 0.980 _diffrn_reflns_theta_full 24.995 _diffrn_reflns_theta_max 24.995 _diffrn_reflns_theta_min 2.323 _diffrn_ambient_temperature 273.0(2) _diffrn_detector_area_resol_mean ? _diffrn_measured_fraction_theta_full 0.980 _diffrn_measured_fraction_theta_max 0.980 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\ w scan' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_source ? _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 3518 _reflns_number_total 3705 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement ? _computing_data_collection ? _computing_data_reduction ? _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _refine_diff_density_max 0.396 _refine_diff_density_min -0.415 _refine_diff_density_rms 0.033 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.037 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 267 _refine_ls_number_reflns 3705 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0421 _refine_ls_R_factor_gt 0.0405 _refine_ls_restrained_S_all 1.037 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0482P)^2^+1.0630P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1042 _refine_ls_wR_factor_ref 0.1057 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Secondary CH2 refined with riding coordinates: C10(H10A,H10B) 2.b Aromatic/amide H refined with riding coordinates: C2(H2), C3(H3), C15(H15), C14(H14), C6(H6), C12(H12) 2.c Idealised Me refined as rotating group: C17(H17A,H17B,H17C), C9(H9A,H9B,H9C), C20(H20A,H20B,H20C), C21(H21A,H21B, H21C), C19(H19A,H19B,H19C) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary ? _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cl1 Cl 0.78637(7) 0.91056(5) 0.43317(4) 0.0748(2) Uani 1 1 d . . . . . S2 S 0.59351(5) 0.45692(4) 0.72133(2) 0.04692(16) Uani 1 1 d . . . . . O1 O 0.84812(15) 0.52861(9) 0.55942(8) 0.0488(3) Uani 1 1 d . . . . . O2 O 0.95736(15) 0.50980(12) 0.72270(9) 0.0662(4) Uani 1 1 d . . . . . O4 O 0.66433(17) 0.53756(13) 0.76770(8) 0.0671(4) Uani 1 1 d . . . . . N1 N 0.96554(17) 0.68126(13) 0.71292(8) 0.0502(4) Uani 1 1 d . . . . . N2 N 0.61393(15) 0.47880(10) 0.63439(8) 0.0388(3) Uani 1 1 d . . . . . O3 O 0.64100(18) 0.35689(12) 0.74003(8) 0.0659(4) Uani 1 1 d . . . . . C2 C 0.9248(2) 0.89718(14) 0.58153(13) 0.0548(5) Uani 1 1 d . . . . . H2 H 0.9523 0.9636 0.5777 0.066 Uiso 1 1 calc R . . . . C3 C 0.9721(2) 0.84758(15) 0.64948(12) 0.0538(5) Uani 1 1 d . . . . . H3 H 1.0320 0.8794 0.6914 0.065 Uiso 1 1 calc R . . . . C4 C 0.92758(18) 0.74964(14) 0.65298(9) 0.0425(4) Uani 1 1 d . . . . . C5 C 0.83784(18) 0.70197(13) 0.59048(9) 0.0393(4) Uani 1 1 d . . . . . C7 C 0.80911(19) 0.59699(12) 0.61138(9) 0.0396(4) Uani 1 1 d . . . . . C16 C 0.78628(19) 0.43397(13) 0.55616(10) 0.0412(4) Uani 1 1 d . . . . . C15 C 0.8412(2) 0.36646(15) 0.51194(12) 0.0558(5) Uani 1 1 d . . . . . H15 H 0.9172 0.3859 0.4884 0.067 Uiso 1 1 calc R . . . . C14 C 0.7846(2) 0.27115(16) 0.50249(13) 0.0589(5) Uani 1 1 d . . . . . H14 H 0.8225 0.2266 0.4724 0.071 Uiso 1 1 calc R . . . . C13 C 0.6717(2) 0.24005(14) 0.53715(11) 0.0495(4) Uani 1 1 d . . . . . C17 C 0.6100(3) 0.13472(17) 0.52729(16) 0.0749(7) Uani 1 1 d . . . . . H17A H 0.5444 0.1236 0.5608 0.112 Uiso 1 1 calc GR . . . . H17B H 0.6931 0.0881 0.5384 0.112 Uiso 1 1 calc GR . . . . H17C H 0.5531 0.1255 0.4763 0.112 Uiso 1 1 calc GR . . . . C9 C 1.0617(3) 0.7044(2) 0.78699(12) 0.0718(7) Uani 1 1 d . . . . . H9A H 1.0760 0.6451 0.8174 0.108 Uiso 1 1 calc GR . . . . H9B H 1.0134 0.7549 0.8105 0.108 Uiso 1 1 calc GR . . . . H9C H 1.1589 0.7283 0.7817 0.108 Uiso 1 1 calc GR . . . . C8 C 0.91842(19) 0.58727(15) 0.68981(10) 0.0464(4) Uani 1 1 d . . . . . C1 C 0.8380(2) 0.84932(14) 0.51981(11) 0.0503(4) Uani 1 1 d . . . . . C6 C 0.7920(2) 0.75108(14) 0.52344(10) 0.0458(4) Uani 1 1 d . . . . . H6 H 0.7317 0.7195 0.4816 0.055 Uiso 1 1 calc R . . . . C10 C 0.64247(18) 0.58161(13) 0.61454(10) 0.0401(4) Uani 1 1 d . . . . . H10A H 0.6180 0.6268 0.6514 0.048 Uiso 1 1 calc R . . . . H10B H 0.5764 0.5977 0.5660 0.048 Uiso 1 1 calc R . . . . C11 C 0.67286(18) 0.40555(12) 0.59186(9) 0.0367(4) Uani 1 1 d . . . . . C12 C 0.61701(19) 0.30832(13) 0.58122(10) 0.0417(4) Uani 1 1 d . . . . . H12 H 0.5406 0.2886 0.6044 0.050 Uiso 1 1 calc R . . . . C18 C 0.3898(2) 0.46791(19) 0.71556(12) 0.0633(6) Uani 1 1 d . . . . . C20 C 0.3736(4) 0.4455(3) 0.79506(18) 0.1074(11) Uani 1 1 d . . . . . H20A H 0.2678 0.4476 0.7961 0.161 Uiso 1 1 calc GR . . . . H20B H 0.4289 0.4945 0.8292 0.161 Uiso 1 1 calc GR . . . . H20C H 0.4140 0.3802 0.8099 0.161 Uiso 1 1 calc GR . . . . C21 C 0.3030(3) 0.3940(3) 0.65920(19) 0.0982(11) Uani 1 1 d . . . . . H21A H 0.1958 0.4003 0.6563 0.147 Uiso 1 1 calc GR . . . . H21B H 0.3356 0.3274 0.6747 0.147 Uiso 1 1 calc GR . . . . H21C H 0.3222 0.4072 0.6108 0.147 Uiso 1 1 calc GR . . . . C19 C 0.3397(3) 0.5744(2) 0.69248(19) 0.0917(9) Uani 1 1 d . . . . . H19A H 0.3516 0.5868 0.6426 0.137 Uiso 1 1 calc GR . . . . H19B H 0.4013 0.6206 0.7268 0.137 Uiso 1 1 calc GR . . . . H19C H 0.2345 0.5827 0.6935 0.137 Uiso 1 1 calc GR . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cl1 0.0815(4) 0.0697(4) 0.0732(4) 0.0292(3) 0.0185(3) -0.0046(3) S2 0.0390(2) 0.0692(3) 0.0341(2) -0.0063(2) 0.01180(18) -0.0079(2) O1 0.0528(7) 0.0429(7) 0.0599(8) -0.0049(6) 0.0318(6) -0.0064(5) O2 0.0456(7) 0.0753(10) 0.0743(10) 0.0328(8) 0.0072(7) 0.0034(7) O4 0.0582(8) 0.0993(12) 0.0435(7) -0.0245(7) 0.0118(6) -0.0227(8) N1 0.0414(8) 0.0675(10) 0.0386(8) -0.0013(7) 0.0030(6) -0.0026(7) N2 0.0361(7) 0.0448(8) 0.0384(7) -0.0045(6) 0.0148(6) -0.0020(6) O3 0.0741(10) 0.0765(10) 0.0504(8) 0.0156(7) 0.0212(7) 0.0046(8) C2 0.0529(11) 0.0400(10) 0.0747(14) -0.0059(9) 0.0213(10) -0.0051(8) C3 0.0474(10) 0.0529(11) 0.0604(12) -0.0217(9) 0.0113(9) -0.0067(8) C4 0.0362(8) 0.0506(10) 0.0407(9) -0.0068(7) 0.0093(7) 0.0010(7) C5 0.0365(8) 0.0413(9) 0.0400(9) -0.0036(7) 0.0089(7) -0.0024(7) C7 0.0376(8) 0.0418(9) 0.0400(9) -0.0008(7) 0.0103(7) -0.0011(7) C16 0.0411(9) 0.0413(9) 0.0445(9) -0.0007(7) 0.0165(7) -0.0001(7) C15 0.0594(12) 0.0537(11) 0.0649(12) -0.0054(9) 0.0357(10) 0.0007(9) C14 0.0642(12) 0.0523(11) 0.0671(13) -0.0125(10) 0.0293(10) 0.0062(9) C13 0.0505(10) 0.0426(10) 0.0541(11) -0.0035(8) 0.0098(8) 0.0016(8) C17 0.0799(16) 0.0498(12) 0.0972(18) -0.0147(12) 0.0251(14) -0.0076(11) C9 0.0600(13) 0.1063(19) 0.0414(11) -0.0082(11) -0.0036(9) -0.0017(12) C8 0.0302(8) 0.0616(12) 0.0481(10) 0.0113(9) 0.0106(7) 0.0017(8) C1 0.0501(10) 0.0460(10) 0.0566(11) 0.0070(9) 0.0164(9) -0.0010(8) C6 0.0460(9) 0.0479(10) 0.0415(9) -0.0022(8) 0.0068(7) -0.0051(8) C10 0.0354(8) 0.0439(9) 0.0406(9) -0.0041(7) 0.0081(7) 0.0019(7) C11 0.0335(8) 0.0437(9) 0.0333(8) -0.0009(7) 0.0085(6) 0.0018(7) C12 0.0366(8) 0.0464(10) 0.0421(9) 0.0013(7) 0.0089(7) -0.0033(7) C18 0.0423(10) 0.0971(17) 0.0582(12) -0.0232(11) 0.0270(9) -0.0168(10) C20 0.094(2) 0.166(3) 0.0831(19) -0.016(2) 0.0628(17) -0.026(2) C21 0.0492(13) 0.137(3) 0.115(2) -0.056(2) 0.0315(14) -0.0341(15) C19 0.0526(13) 0.111(2) 0.120(2) -0.0161(18) 0.0375(15) 0.0133(14) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cl1 C1 1.748(2) . ? S2 O4 1.4266(15) . ? S2 N2 1.6714(14) . ? S2 O3 1.4218(17) . ? S2 C18 1.822(2) . ? O1 C7 1.423(2) . ? O1 C16 1.379(2) . ? O2 C8 1.208(2) . ? N1 C4 1.407(2) . ? N1 C9 1.459(2) . ? N1 C8 1.362(3) . ? N2 C10 1.461(2) . ? N2 C11 1.430(2) . ? C2 H2 0.9300 . ? C2 C3 1.385(3) . ? C2 C1 1.371(3) . ? C3 H3 0.9300 . ? C3 C4 1.376(3) . ? C4 C5 1.390(2) . ? C5 C7 1.494(2) . ? C5 C6 1.367(2) . ? C7 C8 1.543(2) . ? C7 C10 1.532(2) . ? C16 C15 1.381(3) . ? C16 C11 1.392(2) . ? C15 H15 0.9300 . ? C15 C14 1.369(3) . ? C14 H14 0.9300 . ? C14 C13 1.386(3) . ? C13 C17 1.510(3) . ? C13 C12 1.385(3) . ? C17 H17A 0.9600 . ? C17 H17B 0.9600 . ? C17 H17C 0.9600 . ? C9 H9A 0.9600 . ? C9 H9B 0.9600 . ? C9 H9C 0.9600 . ? C1 C6 1.384(3) . ? C6 H6 0.9300 . ? C10 H10A 0.9700 . ? C10 H10B 0.9700 . ? C11 C12 1.392(2) . ? C12 H12 0.9300 . ? C18 C20 1.527(3) . ? C18 C21 1.508(3) . ? C18 C19 1.523(4) . ? C20 H20A 0.9600 . ? C20 H20B 0.9600 . ? C20 H20C 0.9600 . ? C21 H21A 0.9600 . ? C21 H21B 0.9600 . ? C21 H21C 0.9600 . ? C19 H19A 0.9600 . ? C19 H19B 0.9600 . ? C19 H19C 0.9600 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O4 S2 N2 107.43(8) . . ? O4 S2 C18 106.07(10) . . ? N2 S2 C18 105.57(9) . . ? O3 S2 O4 120.09(10) . . ? O3 S2 N2 107.40(8) . . ? O3 S2 C18 109.40(11) . . ? C16 O1 C7 117.20(13) . . ? C4 N1 C9 124.63(18) . . ? C8 N1 C4 110.94(15) . . ? C8 N1 C9 123.86(18) . . ? C10 N2 S2 117.88(11) . . ? C11 N2 S2 122.55(12) . . ? C11 N2 C10 113.53(13) . . ? C3 C2 H2 119.6 . . ? C1 C2 H2 119.6 . . ? C1 C2 C3 120.71(18) . . ? C2 C3 H3 121.1 . . ? C4 C3 C2 117.82(17) . . ? C4 C3 H3 121.1 . . ? C3 C4 N1 129.45(17) . . ? C3 C4 C5 121.19(17) . . ? C5 C4 N1 109.29(16) . . ? C4 C5 C7 108.83(15) . . ? C6 C5 C4 120.79(17) . . ? C6 C5 C7 130.37(16) . . ? O1 C7 C5 110.32(13) . . ? O1 C7 C8 111.30(14) . . ? O1 C7 C10 109.86(13) . . ? C5 C7 C8 101.90(14) . . ? C5 C7 C10 111.55(14) . . ? C10 C7 C8 111.71(14) . . ? O1 C16 C15 115.33(15) . . ? O1 C16 C11 124.45(15) . . ? C15 C16 C11 120.19(17) . . ? C16 C15 H15 119.7 . . ? C14 C15 C16 120.54(18) . . ? C14 C15 H15 119.7 . . ? C15 C14 H14 119.5 . . ? C15 C14 C13 120.95(18) . . ? C13 C14 H14 119.5 . . ? C14 C13 C17 121.04(18) . . ? C12 C13 C14 118.12(17) . . ? C12 C13 C17 120.84(18) . . ? C13 C17 H17A 109.5 . . ? C13 C17 H17B 109.5 . . ? C13 C17 H17C 109.5 . . ? H17A C17 H17B 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? N1 C9 H9A 109.5 . . ? N1 C9 H9B 109.5 . . ? N1 C9 H9C 109.5 . . ? H9A C9 H9B 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? O2 C8 N1 127.19(18) . . ? O2 C8 C7 125.62(18) . . ? N1 C8 C7 107.15(15) . . ? C2 C1 Cl1 120.42(15) . . ? C2 C1 C6 121.51(18) . . ? C6 C1 Cl1 118.05(15) . . ? C5 C6 C1 117.97(17) . . ? C5 C6 H6 121.0 . . ? C1 C6 H6 121.0 . . ? N2 C10 C7 111.61(13) . . ? N2 C10 H10A 109.3 . . ? N2 C10 H10B 109.3 . . ? C7 C10 H10A 109.3 . . ? C7 C10 H10B 109.3 . . ? H10A C10 H10B 108.0 . . ? C16 C11 N2 118.58(15) . . ? C12 C11 N2 123.18(14) . . ? C12 C11 C16 118.15(15) . . ? C13 C12 C11 122.04(16) . . ? C13 C12 H12 119.0 . . ? C11 C12 H12 119.0 . . ? C20 C18 S2 104.61(19) . . ? C21 C18 S2 109.88(15) . . ? C21 C18 C20 111.8(2) . . ? C21 C18 C19 110.6(2) . . ? C19 C18 S2 108.70(15) . . ? C19 C18 C20 111.0(2) . . ? C18 C20 H20A 109.5 . . ? C18 C20 H20B 109.5 . . ? C18 C20 H20C 109.5 . . ? H20A C20 H20B 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? C18 C21 H21A 109.5 . . ? C18 C21 H21B 109.5 . . ? C18 C21 H21C 109.5 . . ? H21A C21 H21B 109.5 . . ? H21A C21 H21C 109.5 . . ? H21B C21 H21C 109.5 . . ? C18 C19 H19A 109.5 . . ? C18 C19 H19B 109.5 . . ? C18 C19 H19C 109.5 . . ? H19A C19 H19B 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Cl1 C1 C6 C5 177.30(14) . . . . ? S2 N2 C10 C7 105.41(14) . . . . ? S2 N2 C11 C16 -132.23(14) . . . . ? S2 N2 C11 C12 51.1(2) . . . . ? O1 C7 C8 O2 -46.8(2) . . . . ? O1 C7 C8 N1 131.11(15) . . . . ? O1 C7 C10 N2 56.89(18) . . . . ? O1 C16 C15 C14 -177.87(19) . . . . ? O1 C16 C11 N2 0.7(3) . . . . ? O1 C16 C11 C12 177.55(16) . . . . ? O4 S2 N2 C10 -21.58(14) . . . . ? O4 S2 N2 C11 129.26(14) . . . . ? O4 S2 C18 C20 -67.3(2) . . . . ? O4 S2 C18 C21 172.4(2) . . . . ? O4 S2 C18 C19 51.32(19) . . . . ? N1 C4 C5 C7 2.61(19) . . . . ? N1 C4 C5 C6 -176.71(16) . . . . ? N2 S2 C18 C20 178.83(19) . . . . ? N2 S2 C18 C21 58.6(2) . . . . ? N2 S2 C18 C19 -62.50(18) . . . . ? N2 C11 C12 C13 177.21(16) . . . . ? O3 S2 N2 C10 -152.05(12) . . . . ? O3 S2 N2 C11 -1.21(15) . . . . ? O3 S2 C18 C20 63.5(2) . . . . ? O3 S2 C18 C21 -56.7(2) . . . . ? O3 S2 C18 C19 -177.80(17) . . . . ? C2 C3 C4 N1 176.35(17) . . . . ? C2 C3 C4 C5 -0.1(3) . . . . ? C2 C1 C6 C5 -1.1(3) . . . . ? C3 C2 C1 Cl1 -176.95(15) . . . . ? C3 C2 C1 C6 1.4(3) . . . . ? C3 C4 C5 C7 179.73(16) . . . . ? C3 C4 C5 C6 0.4(3) . . . . ? C4 N1 C8 O2 164.95(18) . . . . ? C4 N1 C8 C7 -12.93(19) . . . . ? C4 C5 C7 O1 -127.89(15) . . . . ? C4 C5 C7 C8 -9.60(17) . . . . ? C4 C5 C7 C10 109.72(16) . . . . ? C4 C5 C6 C1 0.2(3) . . . . ? C5 C7 C8 O2 -164.39(17) . . . . ? C5 C7 C8 N1 13.53(17) . . . . ? C5 C7 C10 N2 179.55(13) . . . . ? C7 O1 C16 C15 -172.46(16) . . . . ? C7 O1 C16 C11 9.6(3) . . . . ? C7 C5 C6 C1 -178.98(17) . . . . ? C16 O1 C7 C5 -160.44(14) . . . . ? C16 O1 C7 C8 87.21(18) . . . . ? C16 O1 C7 C10 -37.1(2) . . . . ? C16 C15 C14 C13 -0.2(3) . . . . ? C16 C11 C12 C13 0.5(3) . . . . ? C15 C16 C11 N2 -177.18(17) . . . . ? C15 C16 C11 C12 -0.3(3) . . . . ? C15 C14 C13 C17 -179.5(2) . . . . ? C15 C14 C13 C12 0.4(3) . . . . ? C14 C13 C12 C11 -0.6(3) . . . . ? C17 C13 C12 C11 179.37(19) . . . . ? C9 N1 C4 C3 1.7(3) . . . . ? C9 N1 C4 C5 178.46(18) . . . . ? C9 N1 C8 O2 -6.8(3) . . . . ? C9 N1 C8 C7 175.37(17) . . . . ? C8 N1 C4 C3 -169.97(18) . . . . ? C8 N1 C4 C5 6.8(2) . . . . ? C8 C7 C10 N2 -67.14(18) . . . . ? C1 C2 C3 C4 -0.7(3) . . . . ? C6 C5 C7 O1 51.4(2) . . . . ? C6 C5 C7 C8 169.64(18) . . . . ? C6 C5 C7 C10 -71.0(2) . . . . ? C10 N2 C11 C16 19.8(2) . . . . ? C10 N2 C11 C12 -156.90(15) . . . . ? C10 C7 C8 O2 76.4(2) . . . . ? C10 C7 C8 N1 -105.68(16) . . . . ? C11 N2 C10 C7 -47.98(18) . . . . ? C11 C16 C15 C14 0.2(3) . . . . ? C18 S2 N2 C10 91.29(14) . . . . ? C18 S2 N2 C11 -117.87(14) . . . . ? loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma 1 0 0 333.97 7.4 1 0 0 292.57 7.1 1 0 0 291.67 6.9 1 0 0 290.37 7.1 -1 0 0 315.57 7.9 -1 0 0 327.37 7.1 -1 0 0 310.77 7.5 -1 0 0 335.17 7.9 6 0 0 242.08 8.8 6 0 0 244.28 9.9 6 0 0 247.58 8.3 -6 0 0 233.28 8.5 6 0 0 236.68 8.9 -6 0 0 234.88 11.5 -6 0 0 230.88 8.7 7 0 0 3498.55 74.19 7 0 0 3430.36 77.09 -7 0 0 3416.56 74.79 7 0 0 3441.06 75.29 -7 0 0 3411.96 80.59 -7 0 0 3465.05 75.09 -8 0 0 570.14 21.8 8 0 0 576.04 19.2 8 0 0 582.44 17.6 -8 0 0 592.14 17.4 -8 0 0 555.44 16.9 8 0 0 572.34 16.3 -9 0 0 447.96 19.9 -9 0 0 446.56 15 9 0 0 449.06 17.1 9 0 0 457.05 15.7 -9 0 0 436.96 14.8 9 0 0 449.76 14.2 10 0 0 114.59 7.7 10 0 0 96.99 6.4 10 0 0 109.79 8.5 -10 0 0 108.69 10.5 -10 0 0 100.69 7 11 0 0 257.77 10.7 -11 0 0 257.87 11.3 -11 0 0 262.67 17 -12 0 0 26.6 4.9 -12 0 0 20.1 7 -1 -1 0 976.9 21.2 1 -1 0 972.3 21 -1 -1 0 986.1 21.1 -1 -1 0 970.6 20.2 1 -1 0 989 20.7 -1 -1 0 1084.09 21.1 1 -1 0 956.4 21.1 -1 -1 0 1013.9 21.1 -1 -1 0 1010.2 20.3 1 -1 0 963.1 21.5 1 -1 0 988.4 20.8 1 1 0 983.2 21.2 -1 1 0 955.7 20.7 -1 1 0 975.2 20.7 1 1 0 987.1 20.3 1 1 0 971.6 21 1 1 0 962.6 21.2 -1 1 0 953.1 21.5 -1 1 0 960.5 21 3 -1 0 704.53 15.7 3 -1 0 678.43 14.6 3 -1 0 688.43 16.9 -3 -1 0 686.53 17.4 -3 -1 0 690.53 18.4 -3 -1 0 681.93 15.1 -3 -1 0 696.53 18.1 -3 -1 0 713.23 16.6 3 -1 0 690.93 18.7 3 -1 0 651.33 16.3 -3 -1 0 722.43 16 -3 -1 0 736.43 16.2 3 -1 0 664.43 16.7 3 -1 0 704.33 17.1 -3 -1 0 698.83 16.5 -3 1 0 705.43 17 3 1 0 761.22 16.8 3 1 0 686.83 17.2 -3 1 0 701.93 17.1 3 1 0 722.13 16.2 3 1 0 683.63 16.1 -3 1 0 719.23 16.4 -3 1 0 692.83 18.7 -3 1 0 701.03 16.8 4 -1 0 5.3 1.6 4 -1 0 9.3 2.2 4 -1 0 7.7 1.9 -4 -1 0 4.6 2.2 4 -1 0 5.7 2.1 -4 -1 0 5 0.9 -4 -1 0 8.8 2.2 4 -1 0 2.1 1.5 -4 -1 0 2.5 1.5 -4 -1 0 7.5 1.5 -4 -1 0 6.1 2.2 -4 1 0 7.6 1.9 -4 1 0 12.4 1.9 -4 1 0 3.9 2.1 4 1 0 4.4 2.2 -4 1 0 7.7 2 4 1 0 7.1 1.5 4 1 0 8.8 1.5 -4 1 0 9.9 2.3 4 1 0 5 2 4 1 0 4.7 1.6 -5 -1 0 1338.57 30.1 5 -1 0 1309.07 31.2 5 -1 0 1352.96 29.4 -5 -1 0 1293.47 27.5 -5 -1 0 1312.77 33.9 -5 -1 0 1283.97 33.4 -5 -1 0 1338.07 30.6 5 -1 0 1350.36 30.6 5 -1 0 1320.27 31.7 -5 -1 0 1338.97 30 -5 1 0 1296.27 30.2 -5 1 0 1347.27 31.2 5 1 0 1299.17 30.1 -5 1 0 1286.37 34.2 5 1 0 1339.57 30.5 5 1 0 1278.07 31.8 5 1 0 1313.17 30.2 6 -1 0 110.99 6.4 6 -1 0 108.09 4.8 -6 -1 0 101.89 5.3 -6 -1 0 99.79 7.4 -6 -1 0 107.59 7.2 -6 -1 0 104.09 5.5 6 -1 0 113.19 5.8 6 -1 0 94.59 5.9 -6 -1 0 102.79 5.2 -6 1 0 97.69 5.1 6 1 0 103.49 5.5 -6 1 0 99.49 7.5 6 1 0 104.29 5.5 6 1 0 92.49 6.1 -6 1 0 94.89 5.5 7 -1 0 689.63 20.6 -7 -1 0 705.13 23.4 7 -1 0 703.03 19.9 7 -1 0 690.43 19 -7 -1 0 688.83 18.4 -7 -1 0 700.23 18.5 7 -1 0 676.13 17.6 7 1 0 670.33 20.6 -7 1 0 702.63 19.7 -7 1 0 669.03 23.3 7 1 0 651.33 18.6 -7 1 0 657.33 19.1 7 1 0 703.63 18.8 8 -1 0 5.4 2.9 -8 -1 0 14 3.1 8 -1 0 6.8 2.4 8 -1 0 8.5 3 8 -1 0 5.7 3 -8 -1 0 5.8 2.1 -8 -1 0 9.5 4.2 -8 1 0 8.8 2.7 -8 1 0 10.2 3.3 8 1 0 7.4 2.7 8 1 0 3.2 3.1 8 1 0 7.4 2.5 -8 1 0 4.9 3.8 -9 -1 0 1.2 2.2 -9 -1 0 5.9 2.3 9 -1 0 4.9 3.3 9 -1 0 3.5 2 9 -1 0 5.6 2.8 -9 -1 0 1 3.2 -9 1 0 6.7 2.9 9 1 0 7.6 3 -9 1 0 1.5 3.6 9 1 0 5.2 2.7 9 1 0 5.3 3.6 -9 1 0 7.4 3 -10 -1 0 33.5 4.4 10 -1 0 37.4 4.3 10 -1 0 37.3 5.7 10 -1 0 30.1 5.7 -10 -1 0 35.9 7.1 -10 1 0 40.2 7.8 10 1 0 40.4 5 -10 1 0 32.5 5.1 10 1 0 41.1 5.3 10 1 0 42.6 6.8 -11 -1 0 4 2.8 -11 -1 0 4.5 4.2 11 -1 0 4.6 3.9 -11 1 0 1 4.1 -11 1 0 -2 2.8 11 1 0 1.2 3.2 -12 -1 0 23.5 4.1 -12 -1 0 28.5 7.4 -12 1 0 33.9 12.5 -12 1 0 24.6 4.8 2 -2 0 139.89 4.4 2 -2 0 141.79 5.5 -2 -2 0 133.19 4.9 -2 -2 0 142.39 3.7 -2 -2 0 133.39 4.7 2 -2 0 130.59 4.7 -2 -2 0 140.39 3.6 2 -2 0 132.59 4.3 -2 -2 0 132.99 4.1 -2 -2 0 136.09 4.7 -2 -2 0 137.29 4.7 2 -2 0 132.29 4.8 2 2 0 140.29 4.8 -2 2 0 133.89 4.3 2 2 0 142.49 5.1 -2 2 0 135.29 4.8 -2 2 0 134.89 4.8 2 2 0 135.09 4.9 2 2 0 134.29 3.7 -2 2 0 119.69 5.2 -3 -2 0 2792.92 56.19 -3 -2 0 2750.32 56.19 -3 -2 0 2694.43 57.49 3 -2 0 2714.73 57.79 -3 -2 0 2736.33 58.19 3 -2 0 2755.02 57.09 -3 -2 0 2754.72 58.99 -3 -2 0 2720.23 57.29 3 -2 0 2665.73 57.39 3 -2 0 2730.23 59.69 -3 -2 0 2763.32 55.89 3 -2 0 2691.23 57.99 -3 -2 0 2774.82 58.39 3 -2 0 2685.43 55.69 3 2 0 2543.85 58.49 3 2 0 2689.23 57.89 3 2 0 2551.84 55.99 -3 2 0 2692.63 59.59 3 2 0 2648.64 57.59 -3 2 0 2680.03 57.39 3 2 0 2620.34 56.09 3 2 0 2687.13 58.99 -3 2 0 2727.03 56.89 -3 2 0 2783.92 57.99 -4 -2 0 5238.78 110.09 4 -2 0 5064.09 111.49 4 -2 0 5125.39 105.59 -4 -2 0 5396.36 107.09 4 -2 0 5275.57 107.99 -4 -2 0 5192.98 108.39 4 -2 0 5071.49 108.99 -4 -2 0 5133.39 109.49 -4 -2 0 5230.98 108.29 -4 -2 0 5210.18 106.39 4 -2 0 5080.59 108.69 4 -2 0 5164.68 108.69 4 2 0 5071.69 107.09 -4 2 0 5100.49 108.69 -4 2 0 5215.18 107.69 -4 2 0 5291.07 108.79 4 2 0 5199.58 106.99 4 2 0 5304.97 111.29 -4 2 0 5042 111.29 4 2 0 5259.67 109.29 -4 2 0 5349.56 109.09 4 2 0 5271.07 108.59 -5 -2 0 1805.12 39.2 5 -2 0 1875.91 41.6 -5 -2 0 1872.21 40.3 -5 -2 0 1895.11 40.6 5 -2 0 1842.92 42.6 5 -2 0 1949.01 40 -5 -2 0 1828.02 44 -5 -2 0 1842.62 41.8 5 -2 0 1874.71 42.7 -5 -2 0 1871.91 44.9 -5 2 0 1859.01 41.3 5 2 0 1765.32 40.6 -5 2 0 1916.71 45.9 5 2 0 1877.51 42 -5 2 0 1883.91 42.3 5 2 0 1853.31 40.6 -5 2 0 1821.22 42.6 -5 2 0 1828.42 42.5 5 2 0 1861.71 43.1 -6 -2 0 396.56 14.5 6 -2 0 380.86 13.2 6 -2 0 406.46 13.4 -6 -2 0 399.06 11.4 -6 -2 0 401.56 15.3 -6 -2 0 376.46 9.6 6 -2 0 410.66 12.5 -6 -2 0 414.06 11.3 6 -2 0 395.56 10.7 -6 -2 0 389.26 12.5 6 2 0 396.06 13.7 6 2 0 393.26 11.6 -6 2 0 385.76 13.2 -6 2 0 387.56 15.6 -6 2 0 416.46 13 -6 2 0 381.96 11.9 6 2 0 393.96 12.6 -7 -2 0 31.2 3.2 7 -2 0 32.2 2.9 7 -2 0 29.2 4 7 -2 0 27.8 4.4 -7 -2 0 26.5 5 7 -2 0 31.9 4.8 7 2 0 34.6 4 -7 2 0 31.6 4.1 7 2 0 24 4.1 -7 2 0 29.3 5.3 -7 2 0 27 4 7 2 0 30.1 3.6 8 -2 0 77.49 4.5 -8 -2 0 80.19 4.9 -8 -2 0 80.89 7.9 8 -2 0 70.59 5.6 8 -2 0 75.49 6.3 8 -2 0 84.09 6.6 -8 -2 0 87.09 5 -8 2 0 76.69 6.3 8 2 0 68.89 6.2 8 2 0 77.79 5.8 8 2 0 79.79 5.4 -8 2 0 86.69 8.7 -8 2 0 70.39 5.7 -9 -2 0 35.5 4 9 -2 0 33.9 5.2 -9 -2 0 34.3 3.9 9 -2 0 37.1 4.9 -9 -2 0 34.3 6.5 9 -2 0 39.7 5.7 9 -2 0 33.5 3.6 -9 2 0 32.5 4.8 9 2 0 42.6 4.8 -9 2 0 45.9 5.8 9 2 0 30.2 4.6 -9 2 0 27 6.2 9 2 0 38.3 6.2 -10 -2 0 168.58 12.7 -10 -2 0 129.59 7 10 -2 0 158.58 9.7 10 -2 0 136.79 6.5 10 -2 0 146.49 9.9 -10 2 0 146.09 12.6 10 2 0 158.78 9 -10 2 0 147.39 9.2 10 2 0 145.59 8.1 -11 -2 0 101.39 11.2 11 -2 0 84.29 8.8 -11 -2 0 96.59 6.1 11 -2 0 102.79 8.8 11 2 0 91.89 7.6 -11 2 0 90.29 8.1 -11 2 0 100.39 11 -12 -2 0 -0.3 5.4 -12 -2 0 6.2 2.5 -12 2 0 4 3.5 0 -3 0 0.8 0.6 0 -3 0 0.6 0.5 0 -3 0 1.2 0.6 0 -3 0 0.3 0.5 0 3 0 0.5 0.5 0 3 0 0.4 0.5 0 3 0 1 0.6 3 -3 0 1293.07 30.2 -3 -3 0 1275.87 29.6 -3 -3 0 1352.56 27.8 3 -3 0 1316.67 29.2 3 -3 0 1299.57 29.1 3 -3 0 1299.77 29.9 -3 -3 0 1298.47 27.5 -3 -3 0 1305.27 30.3 -3 -3 0 1259.77 28.5 -3 -3 0 1298.67 29.8 3 -3 0 1302.87 31.4 -3 -3 0 1270.27 29.9 3 -3 0 1301.27 28.2 3 3 0 1251.87 27.7 -3 3 0 1309.87 30.1 -3 3 0 1286.47 29 3 3 0 1322.07 30 3 3 0 1293.57 30.5 3 3 0 1305.17 30.4 -3 3 0 1307.67 31.4 -3 3 0 1302.97 28.8 -3 3 0 1311.07 30 3 3 0 1322.67 29.8 -4 -3 0 277.17 7.3 4 -3 0 263.47 7.1 4 -3 0 277.57 8.8 4 -3 0 275.77 8.5 4 -3 0 271.57 9.4 -4 -3 0 268.57 9.9 -4 -3 0 254.77 9.3 -4 -3 0 267.97 8.9 4 -3 0 255.47 8.9 4 -3 0 263.27 10.6 -4 -3 0 267.77 7 -4 -3 0 261.37 8.6 -4 -3 0 267.57 7.6 -4 -3 0 260.67 9.2 4 3 0 263.57 9 -4 3 0 268.57 8.2 4 3 0 259.77 7.4 4 3 0 255.57 9.1 -4 3 0 258.77 9 4 3 0 257.47 9.7 4 3 0 251.17 10 -4 3 0 266.77 8.6 -4 3 0 261.37 10.5 -4 3 0 261.97 9.3 4 3 0 246.38 7.1 -5 -3 0 24.1 2.1 5 -3 0 17.9 1.8 5 -3 0 19.5 3.4 -5 -3 0 15.2 2.6 -5 -3 0 19.7 3.4 -5 -3 0 18.4 2 5 -3 0 17.5 1.6 5 -3 0 14.2 2.7 5 -3 0 21.2 2.9 -5 -3 0 17.8 3.4 -5 -3 0 17.3 1.9 -5 -3 0 18.2 2.8 5 3 0 17.6 3 -5 3 0 12.3 3 -5 3 0 21.1 2.7 -5 3 0 17.7 2.9 5 3 0 18.8 2.2 5 3 0 18.3 2 -5 3 0 20.4 3.7 -5 3 0 15.9 2.8 5 3 0 21.9 3.4 6 -3 0 196.08 8.9 -6 -3 0 185.28 9.9 -6 -3 0 178.08 6 -6 -3 0 182.38 6.3 -6 -3 0 174.38 8.9 6 -3 0 197.68 8.6 6 -3 0 201.08 8.1 -6 -3 0 198.98 6.8 6 -3 0 206.98 6.2 -6 3 0 187.48 8.4 -6 3 0 194.38 8.8 -6 3 0 186.48 7.5 6 3 0 205.98 8.6 -6 3 0 185.58 10.4 6 3 0 188.18 8.8 6 3 0 199.08 6.9 7 -3 0 287.87 8.4 -7 -3 0 274.07 7.8 -7 -3 0 290.17 13.5 7 -3 0 274.67 11.3 7 -3 0 295.07 11.9 7 -3 0 290.77 10.8 -7 -3 0 290.77 8.9 -7 3 0 296.57 14.4 7 3 0 292.07 11.2 -7 3 0 287.27 11.2 7 3 0 289.37 12 -7 3 0 299.47 12 7 3 0 290.37 9.5 -8 -3 0 517.65 14.7 -8 -3 0 546.65 12.3 8 -3 0 529.35 13.8 -8 -3 0 536.45 20.6 8 -3 0 528.95 17.9 8 -3 0 537.75 18.2 8 -3 0 549.54 16.8 -8 -3 0 535.55 14.5 -8 3 0 535.65 18.1 -8 3 0 473.35 18.7 8 3 0 551.24 15.4 -8 3 0 523.15 21.2 8 3 0 528.25 18.4 8 3 0 528.25 17.2 9 -3 0 12.6 4.2 9 -3 0 11.2 4.1 9 -3 0 5.3 3.1 -9 -3 0 10 2.6 -9 -3 0 13 2.6 9 -3 0 7.5 2 -9 -3 0 9 4.4 9 3 0 12.4 3.7 -9 3 0 13.6 5 -9 3 0 13.5 3.9 9 3 0 6.1 2.6 10 -3 0 67.89 6.7 10 -3 0 75.99 8.1 -10 -3 0 66.79 4.7 -10 -3 0 81.69 9.5 10 -3 0 67.29 7.4 10 -3 0 70.89 4.2 -10 3 0 54.39 8.8 10 3 0 73.59 5.6 -10 3 0 71.99 7.3 10 3 0 72.59 6.8 11 -3 0 -0.3 3.8 -11 -3 0 4.1 2.2 -11 -3 0 4.7 4.5 11 -3 0 -7.8 4.5 -11 3 0 0.6 3.6 -11 3 0 5.4 5.6 11 3 0 6.6 3.8 -12 -3 0 41.2 3.7 -12 -3 0 35.5 7.9 -12 3 0 48.7 6.8 0 -4 0 556.94 13.3 0 -4 0 562.14 13.5 0 -4 0 555.64 13.7 0 -4 0 546.35 13.5 0 4 0 538.35 11.7 0 4 0 573.24 13.5 0 4 0 570.14 13.4 0 4 0 555.14 13.8 0 4 0 544.85 13.4 1 -4 0 36.5 2.2 -1 -4 0 42.7 1.6 -1 -4 0 45.2 2 -1 -4 0 33.1 2 1 -4 0 35.7 1.5 1 -4 0 39.1 2.6 1 -4 0 33.4 2.3 -1 -4 0 43.1 2.7 1 -4 0 37.2 2.2 -1 -4 0 38.4 2.3 -1 -4 0 39.3 2.1 1 4 0 35.5 2.3 1 4 0 43.3 2.1 -1 4 0 35.2 2.5 -1 4 0 35.4 2.5 -1 4 0 39.4 2.2 -1 4 0 38.8 2.2 1 4 0 35.1 1.6 -1 4 0 34.1 2.1 -2 -4 0 1626.04 34.4 2 -4 0 1546.35 35.4 -2 -4 0 1603.84 35 2 -4 0 1586.34 34 2 -4 0 1578.54 35.8 -2 -4 0 1640.54 33.6 2 -4 0 1575.74 34.8 2 -4 0 1595.54 35.9 -2 -4 0 1578.14 35.7 -2 -4 0 1712.13 33.5 -2 -4 0 1602.34 34.5 2 -4 0 1589.04 33.9 2 4 0 1520.95 33.5 -2 4 0 1631.44 35.8 2 4 0 1614.54 35.9 -2 4 0 1605.24 34.6 2 4 0 1570.34 34.7 2 4 0 1464.95 35 -2 4 0 1604.14 36 2 4 0 1542.35 33.5 -2 4 0 1578.84 33.6 -2 4 0 1612.14 35.7 -3 -4 0 95.19 3.1 -3 -4 0 92.59 3.2 -3 -4 0 86.29 4.4 3 -4 0 95.29 4.3 3 -4 0 91.89 4 3 -4 0 89.39 3.3 3 -4 0 89.69 4.9 -3 -4 0 92.99 4.7 3 -4 0 90.39 4.8 -3 -4 0 91.99 4.2 3 -4 0 92.79 5.2 -3 -4 0 89.59 4.2 -3 -4 0 98.19 4.8 -3 4 0 95.59 4.9 -3 4 0 89.59 3.8 -3 4 0 95.49 5.4 3 4 0 97.79 4.9 3 4 0 94.29 4.5 3 4 0 89.69 4.8 -3 4 0 95.99 5 -3 4 0 97.89 4.2 3 4 0 95.69 4.9 3 4 0 93.79 3.2 -4 -4 0 50.89 3.1 4 -4 0 51.89 3.4 -4 -4 0 50.29 2.3 -4 -4 0 50.09 3.8 -4 -4 0 51.19 2.5 -4 -4 0 53.09 4.1 4 -4 0 48.1 2.4 4 -4 0 51.99 3.5 4 -4 0 53.29 4.2 4 -4 0 49 2.8 -4 -4 0 52.19 3.6 -4 -4 0 52.09 3.8 4 -4 0 51.99 4.5 4 4 0 52.19 2.6 -4 4 0 48.8 4.6 4 4 0 48.9 4.1 4 4 0 48.7 3.8 4 4 0 52.29 4.2 -4 4 0 42.4 3.8 -4 4 0 47 3.2 -4 4 0 44 4 4 4 0 49.1 3.9 -4 4 0 47.5 3.1 -5 -4 0 92.59 3.9 -5 -4 0 87.19 6 5 -4 0 102.69 6.3 -5 -4 0 92.89 6.3 5 -4 0 86.69 5.3 5 -4 0 87.89 5.1 5 -4 0 89.39 3.9 -5 -4 0 94.49 3.6 -5 -4 0 89.79 5.6 -5 -4 0 99.39 4.5 -5 4 0 99.79 5.9 5 4 0 98.39 5.9 5 4 0 96.19 7.8 5 4 0 106.39 6.1 -5 4 0 96.39 5.3 -5 4 0 79.69 5.8 -5 4 0 98.69 4.9 5 4 0 83.59 3.9 -5 4 0 87.79 6.8 5 4 0 98.99 4 6 -4 0 658.93 15.2 6 -4 0 660.83 18.9 -6 -4 0 684.03 16.3 6 -4 0 664.43 20.1 6 -4 0 641.54 15.2 -6 -4 0 640.34 19.5 -6 -4 0 725.13 21.6 -6 -4 0 647.14 15.7 -6 -4 0 643.14 16.5 6 -4 0 661.83 18.3 6 -4 0 661.53 15.5 -6 4 0 658.73 22.1 -6 4 0 679.93 20.1 6 4 0 689.83 19.6 6 4 0 637.74 16.2 -6 4 0 644.64 19.3 6 4 0 659.93 19.5 7 -4 0 103.69 7.4 -7 -4 0 87.19 4.1 -7 -4 0 96.09 7.9 7 -4 0 84.99 3.8 7 -4 0 90.49 6.3 7 -4 0 101.09 6.3 -7 -4 0 87.59 4.3 7 4 0 87.59 4.7 -7 4 0 87.59 8.6 -7 4 0 95.39 7.1 7 4 0 91.09 6.7 7 4 0 93.99 6.7 -8 -4 0 8.4 4.2 8 -4 0 4.2 1.6 8 -4 0 5 3.1 8 -4 0 0.8 2.9 -8 -4 0 4.8 2 -8 -4 0 4.5 1.7 -8 -4 0 7.9 1.6 -8 -4 0 8.8 2 8 -4 0 6.9 4 -8 4 0 3.1 3.3 8 4 0 5.2 2.3 -8 4 0 3 4.2 8 4 0 4 3 9 -4 0 97.19 4.1 9 -4 0 99.59 8 9 -4 0 116.89 7.7 -9 -4 0 106.89 9.9 9 -4 0 116.79 9 -9 -4 0 93.89 5 -9 -4 0 91.09 5.1 9 4 0 108.99 6 -9 4 0 119.79 11.2 9 4 0 110.29 8 -9 4 0 102.69 8.5 -10 -4 0 12.4 2.4 10 -4 0 14.2 4.2 10 -4 0 10.2 4.4 -10 -4 0 8.1 5 10 -4 0 8.2 5 10 4 0 8.6 4.2 -10 4 0 9.6 5.4 -10 4 0 15 4.9 -11 -4 0 103.79 11.4 11 -4 0 122.49 10.1 11 -4 0 109.89 9.3 -11 -4 0 105.69 5 11 -4 0 113.49 8.3 -11 4 0 119.99 12.9 11 4 0 102.69 8.6 -11 4 0 115.19 9.6 -12 -4 0 -0.8 4.9 12 4 0 -5.1 4.1 -12 4 0 1.2 3.9 0 -5 0 7.5 1.5 0 -5 0 10.9 1.7 0 5 0 7.4 1.5 0 5 0 8 1.6 0 5 0 8.9 1.6 -1 -5 0 1510.45 30.4 -1 -5 0 1462.45 32.8 -1 -5 0 1490.45 32.2 1 -5 0 1431.46 32.5 -1 -5 0 1511.35 32 -1 -5 0 1462.15 33.4 -1 -5 0 1397.96 31.8 1 -5 0 1475.75 30.8 1 -5 0 1481.45 32.8 1 -5 0 1482.25 33 1 -5 0 1510.25 33.5 1 5 0 1478.45 33.6 -1 5 0 1495.75 32.2 -1 5 0 1454.65 32.5 1 5 0 1487.85 32.1 -1 5 0 1468.45 32.7 -1 5 0 1494.15 33.3 1 5 0 1437.36 32 -1 5 0 1473.05 33.1 1 5 0 1485.45 32.8 1 5 0 1479.25 30.7 2 -5 0 797.82 18 2 -5 0 800.52 20.4 -2 -5 0 809.72 19.1 -2 -5 0 798.02 19.3 -2 -5 0 804.62 20.4 2 -5 0 774.82 19.9 2 -5 0 804.92 19.5 2 -5 0 798.02 18.7 -2 -5 0 809.12 19.6 -2 -5 0 812.72 18.2 -2 -5 0 835.32 18.1 -2 -5 0 823.42 18.3 -2 5 0 800.82 20.3 -2 5 0 797.72 20 -2 5 0 818.22 18.7 -2 5 0 820.72 20.3 2 5 0 771.92 20.3 2 5 0 792.72 18.7 -2 5 0 811.32 19.2 2 5 0 795.32 18.2 2 5 0 806.52 19.8 2 5 0 802.82 18.1 -3 -5 0 22 3 -3 -5 0 26 2.7 -3 -5 0 22.3 1.8 3 -5 0 30.7 3.3 3 -5 0 27.6 3.4 -3 -5 0 22.3 2.4 -3 -5 0 30.8 3.5 3 -5 0 20.6 3.1 -3 -5 0 19.4 2.4 3 -5 0 21.5 2.2 -3 -5 0 21.8 1.8 3 -5 0 19.5 1.9 -3 5 0 21.6 3.2 -3 5 0 20.2 3 -3 5 0 22.1 2.9 3 5 0 22.2 2.7 3 5 0 27.4 3.4 3 5 0 21.8 1.8 3 5 0 21.4 3 -3 5 0 23.8 2.1 -3 5 0 22 2.4 4 -5 0 217.78 9.1 4 -5 0 219.08 8 -4 -5 0 232.68 6.1 4 -5 0 214.08 9.6 -4 -5 0 224.08 6.2 -4 -5 0 222.68 7.9 4 -5 0 207.18 7.4 4 -5 0 214.38 7.3 -4 -5 0 208.98 7.6 4 -5 0 209.68 6.3 -4 -5 0 204.38 8.3 -4 5 0 202.08 7.1 4 5 0 220.48 8.9 4 5 0 218.78 8.9 -4 5 0 216.48 7.6 -4 5 0 218.08 8.8 -4 5 0 214.98 9.7 4 5 0 221.18 9 -4 5 0 212.98 9 4 5 0 222.28 6.4 -5 -5 0 712.83 16.3 5 -5 0 717.93 21 -5 -5 0 722.33 18.4 -5 -5 0 695.93 19.3 5 -5 0 734.13 16.6 -5 -5 0 748.43 20.8 5 -5 0 703.73 19 5 -5 0 717.43 17.6 -5 -5 0 738.73 16.7 5 -5 0 730.53 19.3 5 5 0 707.63 20.5 -5 5 0 702.33 20.8 5 5 0 666.13 16.9 5 5 0 730.23 21.2 -5 5 0 705.93 18.6 5 5 0 710.03 21.3 -5 5 0 740.53 22.6 -5 5 0 713.83 18.8 -6 -5 0 7.3 2.1 6 -5 0 7.1 2.7 -6 -5 0 7.6 3 -6 -5 0 9.3 1.8 -6 -5 0 4 1.4 6 -5 0 3.7 2.6 6 -5 0 7.5 3.5 6 -5 0 6.3 1.4 6 -5 0 7.5 1.8 6 -5 0 5.7 1.7 -6 -5 0 6 2.9 6 5 0 7.3 3.3 -6 5 0 8.2 3.4 -6 5 0 8 3.6 -7 -5 0 2.9 3.1 7 -5 0 6.3 1.4 7 -5 0 0.5 1.2 7 -5 0 5.3 2.8 7 -5 0 3.5 1.4 -7 -5 0 0.8 1.4 7 -5 0 12 3.3 7 -5 0 -0.3 1.2 -7 -5 0 3.8 1.7 7 -5 0 1.9 3.1 -7 5 0 4.9 3.6 7 5 0 -0.9 1.3 -7 5 0 2.6 3.2 7 5 0 2.5 2.9 -8 -5 0 509.25 12.9 8 -5 0 492.15 17 -8 -5 0 501.05 19.5 -8 -5 0 459.85 13.3 8 -5 0 505.65 16.5 -8 -5 0 472.55 12.4 8 -5 0 513.15 18.7 -8 5 0 501.75 20.9 8 5 0 520.55 18 8 5 0 482.35 13.6 -8 5 0 507.55 18.5 -9 -5 0 96.69 4.6 -9 -5 0 113.59 10 9 -5 0 119.19 9.5 9 -5 0 99.69 7.9 -9 -5 0 99.49 4.9 9 -5 0 120.49 8 -9 -5 0 99.09 4.4 9 5 0 105.49 5.7 -9 5 0 110.09 9.2 -9 5 0 97.09 10.3 9 5 0 115.59 8.9 -10 -5 0 273.87 7.9 10 -5 0 291.07 12.7 10 -5 0 285.87 13.7 -10 -5 0 304.77 16.5 10 -5 0 282.57 14.6 -10 5 0 286.77 14.5 -10 5 0 275.07 17.7 10 5 0 293.27 14 11 -5 0 41.3 5.9 11 -5 0 30.4 6.3 11 -5 0 36.9 6.6 -11 -5 0 36.2 7.8 -11 5 0 40.7 7 -11 5 0 39 8.8 11 5 0 32.5 5.8 -12 -5 0 6.3 5.3 12 5 0 8.6 5 -1 -6 0 69.09 3.9 -1 -6 0 70.99 4.4 -1 -6 0 71.99 4.1 -1 -6 0 71.59 3.6 1 -6 0 85.69 4.5 1 -6 0 71.99 4.6 1 -6 0 64.79 3.9 -1 -6 0 78.29 3.5 1 -6 0 76.09 4.3 1 6 0 83.89 3.9 -1 6 0 67.59 3.8 1 6 0 68.19 4.5 -1 6 0 70.19 4.3 -1 6 0 69.69 3.6 -1 6 0 69.39 4.1 -1 6 0 71.79 4.5 1 6 0 72.49 3.8 1 6 0 78.09 4.4 -3 -6 0 807.02 20.3 3 -6 0 789.72 18.7 -3 -6 0 770.12 19.4 3 -6 0 796.12 20.2 -3 -6 0 776.82 20.3 3 -6 0 790.52 18.6 -3 -6 0 844.92 18.1 -3 -6 0 789.72 18.1 -3 -6 0 799.22 19.1 3 -6 0 777.12 20.8 3 -6 0 801.72 21.5 3 6 0 762.32 21.2 -3 6 0 778.52 18 -3 6 0 782.92 21.2 3 6 0 798.82 18.2 -3 6 0 782.42 21.1 -3 6 0 800.92 19.6 -3 6 0 785.82 21.3 3 6 0 772.52 18.1 3 6 0 777.32 19.8 3 6 0 792.92 20.8 -4 -6 0 428.26 10.5 -4 -6 0 448.16 10.7 4 -6 0 422.26 14.3 4 -6 0 422.66 12.9 -4 -6 0 389.96 12.5 -4 -6 0 417.56 12.3 4 -6 0 422.26 11 4 -6 0 425.86 12 4 -6 0 425.86 12.4 -4 -6 0 437.66 12.9 4 6 0 409.36 10.7 -4 6 0 429.46 11.6 4 6 0 430.86 13.6 -4 6 0 432.76 12.4 4 6 0 421.96 14.1 -4 6 0 411.16 14.1 4 6 0 433.16 14.1 -4 6 0 433.06 14.9 -5 -6 0 61.69 4.7 5 -6 0 48.5 4.5 -5 -6 0 68.69 3.3 5 -6 0 68.59 3.4 5 -6 0 63.09 4.7 5 -6 0 73.69 5.3 -5 -6 0 65.49 3.1 -5 -6 0 64.69 5.8 5 -6 0 65.99 6.7 -5 -6 0 69.29 4.9 -5 6 0 57.09 6.6 5 6 0 57.69 5.7 -5 6 0 61.79 4.3 5 6 0 64.09 5.9 5 6 0 60.49 6 5 6 0 62.99 3.5 -5 6 0 59.99 6.2 6 -6 0 155.08 7.9 6 -6 0 147.09 7.3 -6 -6 0 139.39 8.6 6 -6 0 141.29 5.9 6 -6 0 131.99 6 -6 -6 0 139.49 4.6 -6 -6 0 130.39 6.7 6 -6 0 133.49 4.7 -6 -6 0 136.29 7.3 6 -6 0 138.69 9.2 -6 -6 0 142.69 5 6 6 0 146.69 8.8 -6 6 0 140.09 9.9 -6 6 0 139.69 9.1 7 -6 0 2482.15 55.89 -7 -6 0 2388.96 50.59 7 -6 0 2577.14 59.09 7 -6 0 2387.46 51.89 7 -6 0 2378.06 50.39 7 -6 0 2382.26 50.39 -7 -6 0 2510.15 58.79 -7 -6 0 2295.37 54.89 7 -6 0 2407.86 55.79 7 -6 0 2400.76 52.09 -7 6 0 2459.75 58.49 -7 6 0 2394.06 60.89 7 6 0 2468.25 57.89 -8 -6 0 524.75 12.6 8 -6 0 546.55 12.8 -8 -6 0 566.74 12.9 -8 -6 0 582.54 20.9 8 -6 0 538.75 20.3 -8 -6 0 509.75 15.2 8 -6 0 553.64 18 8 -6 0 551.94 18.1 -8 6 0 551.24 20.3 -8 6 0 566.64 22.5 8 6 0 561.34 19.7 9 -6 0 636.44 20.3 -9 -6 0 630.94 23.5 9 -6 0 635.14 23.1 -9 -6 0 623.94 17.2 9 -6 0 609.74 20.6 9 6 0 632.74 22 -9 6 0 608.64 25.1 -9 6 0 667.93 23.1 -10 -6 0 90.19 10 10 -6 0 104.69 8.5 10 -6 0 124.19 8.5 10 -6 0 112.79 10.3 -10 6 0 105.19 10 10 6 0 92.49 9.2 -10 6 0 105.49 11.5 11 -6 0 28.5 5.9 11 -6 0 33.1 5.7 11 -6 0 27.9 6.8 -11 -6 0 25.7 6.7 -11 6 0 26.9 8.2 11 6 0 24.3 5.6 -11 6 0 28 6.6 0 -7 0 7.8 2.1 0 -7 0 9.1 2.1 0 -7 0 11.7 2.1 0 7 0 6.8 1.9 0 7 0 9.2 2.2 0 7 0 4.5 2.1 0 7 0 7.4 1.9 0 7 0 7.5 1.8 -1 -7 0 551.74 13.5 1 -7 0 524.25 14.6 -1 -7 0 573.04 14.5 1 -7 0 546.15 14.9 -1 -7 0 524.85 13.8 -1 -7 0 508.35 14.6 1 -7 0 552.54 15 -1 -7 0 524.05 15.3 -1 7 0 526.75 14.5 1 7 0 543.45 15 1 7 0 521.95 15.5 -1 7 0 551.84 15.3 -1 7 0 547.25 13.4 -1 7 0 533.55 16.2 1 7 0 525.95 14.2 -1 7 0 553.44 14.9 1 7 0 497.65 13.9 2 -7 0 51.19 2.5 2 -7 0 47.6 4.2 2 -7 0 43.3 3.5 -2 -7 0 49.99 3.2 -2 -7 0 53.99 3 2 -7 0 53.79 4 -2 -7 0 54.89 2.5 -2 -7 0 52.39 3.2 -2 -7 0 48.9 3.7 2 -7 0 46.8 3.2 2 7 0 47.4 3 -2 7 0 48.9 3.5 -2 7 0 49.99 3.4 2 7 0 44.3 4.2 2 7 0 51.49 2.5 2 7 0 51.89 3.1 -2 7 0 52.39 3.6 -2 7 0 48.9 4.2 2 7 0 42.2 3.8 3 -7 0 326.17 9.1 3 -7 0 320.27 9.7 3 -7 0 329.07 12.1 -3 -7 0 337.37 9.2 -3 -7 0 344.77 9 3 -7 0 327.57 10.9 -3 -7 0 327.77 10.8 -3 -7 0 341.37 9.3 -3 -7 0 340.97 10.4 -3 -7 0 331.57 10.9 3 7 0 337.67 9.3 3 7 0 332.57 11.5 -3 7 0 329.07 11.4 3 7 0 318.57 9.9 -3 7 0 333.47 12 3 7 0 304.57 9 3 7 0 328.17 12 4 -7 0 1753.02 40 4 -7 0 1743.53 38.6 4 -7 0 1762.12 42.5 -4 -7 0 1729.73 39.4 4 -7 0 1704.83 38 -4 -7 0 1792.82 39.5 -4 -7 0 1763.42 37.3 -4 -7 0 1800.82 37.4 4 -7 0 1750.12 40.5 -4 7 0 1754.22 42.3 4 7 0 1752.42 41.8 -4 7 0 1759.82 42.5 4 7 0 1607.84 37.5 4 7 0 1761.72 42.3 4 7 0 1722.73 40.5 4 7 0 1645.84 37.4 -4 7 0 1698.83 37.8 5 -7 0 1540.95 34.7 -5 -7 0 1598.54 37.9 5 -7 0 1607.74 40.3 -5 -7 0 1651.63 34.3 5 -7 0 1612.04 36.9 5 -7 0 1600.04 38.1 5 -7 0 1574.04 36.5 -5 -7 0 1580.14 37 -5 -7 0 1585.34 33.9 5 7 0 1555.34 39 5 7 0 1550.24 39.6 -5 7 0 1604.04 40.2 5 7 0 1621.64 40 -5 7 0 1594.24 40.9 -5 7 0 1520.85 35.8 6 -7 0 797.32 20.9 -6 -7 0 807.72 18 -6 -7 0 847.12 23.7 6 -7 0 820.02 21.9 6 -7 0 801.32 24.9 -6 -7 0 842.52 18.4 6 -7 0 824.62 22.8 6 -7 0 794.92 20.5 6 -7 0 797.52 18.7 -6 7 0 828.22 25 -6 7 0 782.62 25.8 6 7 0 830.82 24.7 6 7 0 811.32 24.7 7 -7 0 1285.27 30.1 7 -7 0 1305.37 33.4 7 -7 0 1318.67 36.3 -7 -7 0 1367.66 35.4 7 -7 0 1318.87 32.8 7 -7 0 1269.27 30.3 -7 7 0 1307.07 38 7 7 0 1277.67 29.2 7 7 0 1324.27 35.7 -7 7 0 1256.77 35.8 8 -7 0 30.3 6.2 8 -7 0 20.9 4.5 -8 -7 0 20.5 5.1 8 -7 0 17.1 4 8 -7 0 19.3 2.6 8 -7 0 25.9 2.9 8 7 0 27.7 5.6 8 7 0 25.3 2.8 -8 7 0 21.2 5.5 -8 7 0 13.2 4.7 9 -7 0 933.61 27.4 9 -7 0 1004.1 31 9 -7 0 948.11 27.4 -9 -7 0 954.8 25 -9 -7 0 942.01 30.2 9 7 0 984.6 29.9 -9 7 0 929.71 30.3 -9 7 0 954.7 33.3 10 -7 0 108.39 8.4 10 -7 0 106.69 10.3 -10 -7 0 87.99 9.6 10 -7 0 119.89 8.5 -10 7 0 103.59 10.1 -10 7 0 110.39 12 10 7 0 112.89 10 11 -7 0 56.49 7 -11 -7 0 39.2 7.6 11 -7 0 62.49 9.1 -11 7 0 43.9 8.8 -11 7 0 51.49 8.3 11 7 0 43.6 7.1 0 -8 0 112.99 5.9 0 -8 0 112.49 6 0 -8 0 114.09 5.6 0 8 0 117.49 6.4 0 8 0 114.19 6.2 0 8 0 114.19 6 1 -8 0 561.04 15.9 1 -8 0 542.45 15.8 -1 -8 0 543.05 15.9 -1 -8 0 573.84 15.1 -1 -8 0 561.74 15.5 1 -8 0 578.74 16.2 -1 -8 0 577.34 14.5 1 8 0 582.04 16.3 -1 8 0 571.94 16.6 1 8 0 571.04 17.1 -1 8 0 586.24 14 -1 8 0 582.94 16.2 1 8 0 571.64 15.5 -2 -8 0 0.4 1.7 2 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888.01 23 8 1 -3 888.41 22.8 -8 1 3 882.21 22.1 8 1 -3 899.31 26.5 -8 1 3 912.21 24 -7 -1 3 31.6 5.6 -7 -1 3 36.1 3.3 7 -1 -3 34.6 4.2 -7 -1 3 39.1 3.1 7 -1 -3 35.1 4.9 7 -1 -3 36.7 2.7 -7 -1 3 36.3 3.2 -7 1 3 31.7 5.6 -7 1 3 32.3 3.5 -7 1 3 35.3 3.1 7 1 -3 34.9 3.5 7 1 -3 47.6 5.8 7 1 -3 29.3 3.3 -7 1 3 35 4.1 -6 -1 3 95.49 4.4 -6 -1 3 102.69 4.5 6 -1 -3 98.09 4.3 -6 -1 3 97.79 4.2 -6 -1 3 96.09 4.6 -6 -1 3 70.79 6.8 6 -1 -3 94.29 3.8 6 -1 -3 92.29 5.3 6 -1 -3 87.59 6 6 1 -3 103.69 4.9 -6 1 3 90.29 4.1 -6 1 3 90.59 4.8 -6 1 3 100.49 5.3 6 1 -3 92.29 4.6 -6 1 3 86.59 7.4 6 1 -3 85.89 6.1 -5 -1 3 398.26 8.7 -5 -1 3 387.16 10.1 -5 -1 3 371.66 14 5 -1 -3 379.86 11.3 5 -1 -3 389.96 12.5 -5 -1 3 370.96 10.1 -5 -1 3 359.46 10.4 5 -1 -3 368.56 9.8 -5 -1 3 374.66 13.9 -5 -1 3 384.56 9.8 5 -1 -3 377.56 10.8 5 -1 -3 383.06 9.3 5 1 -3 357.76 9.9 -5 1 3 383.86 10.9 -5 1 3 387.86 14.4 -5 1 3 355.26 14.6 5 1 -3 368.66 12.4 5 1 -3 386.26 10.3 -5 1 3 378.96 9.8 -5 1 3 368.16 11.1 5 1 -3 376.76 10.6 -3 -1 3 1867.91 41.5 -3 -1 3 1862.21 40.3 3 -1 -3 1956.3 39.4 -3 -1 3 1864.61 39.3 -3 -1 3 1860.21 43.4 3 -1 -3 1902.41 39 3 -1 -3 1912.01 40.7 -3 -1 3 1894.51 42.9 -3 -1 3 1946.91 39.8 3 -1 -3 1915.61 41.7 -3 -1 3 1983.2 39.2 3 -1 -3 1831.82 40.3 3 1 -3 1853.31 39.3 -3 1 3 1948.21 39.3 -3 1 3 1893.11 38.9 3 1 -3 1874.91 40.4 3 1 -3 1863.51 39.6 -3 1 3 1863.91 40.5 3 1 -3 1882.21 41.7 3 1 -3 1863.11 43.8 -3 1 3 1924.61 39 -3 1 3 1839.42 41.2 -3 1 3 1916.51 40.5 2 -1 -3 1924.41 40.1 -2 -1 3 1846.32 41.5 -2 -1 3 1967 39.4 2 -1 -3 1952.6 39.7 2 -1 -3 1921.11 39.1 2 -1 -3 1725.43 39.3 -2 -1 3 1863.61 39.6 -2 -1 3 1867.51 38.4 2 -1 -3 1577.64 37.9 -2 -1 3 1902.01 40.1 -2 -1 3 1914.21 38.5 -2 -1 3 1917.01 38.4 2 1 -3 1889.01 41.9 2 1 -3 1857.31 39.6 -2 1 3 1969 39.6 2 1 -3 1827.02 38.4 2 1 -3 1872.71 39.3 -2 1 3 1858.41 39.8 2 1 -3 1838.32 40.1 -2 1 3 1939.41 39.1 -2 1 3 1829.72 39.5 -1 -1 3 1173.48 25 1 -1 -3 1172.28 24.5 -1 -1 3 1178.28 24.6 -1 -1 3 1193.28 25.4 1 -1 -3 1222.78 25.3 1 -1 -3 1173.28 25.2 -1 -1 3 1198.28 24.7 1 -1 -3 1213.98 25.3 -1 -1 3 1190.98 24.7 -1 -1 3 1122.69 25.2 -1 -1 3 1150.48 26.2 -1 -1 3 1205.68 25.5 -1 1 3 1124.19 26.5 1 1 -3 1213.38 24.7 -1 1 3 1199.78 25.3 1 1 -3 1169.68 24.7 1 1 -3 1138.19 24.6 1 1 -3 1180.18 25.2 1 1 -3 1170.78 26.5 -1 1 3 1198.98 25.3 1 1 -3 1169.78 25.4 -1 1 3 1125.89 25.7 -1 1 3 1159.38 25.2 -2 -1 -3 1962.9 43.6 -2 -1 -3 1979 42.3 2 -1 3 2026.1 43.4 -2 -1 -3 1959 42.7 2 -1 3 1954.8 43.2 2 -1 3 2009.2 42.3 -2 -1 -3 1965.3 42.8 -2 -1 -3 2034.4 43.3 2 -1 3 2020.2 43.3 -2 1 -3 2014 43.1 -2 1 -3 1996.7 42.3 2 1 3 1954 42.8 2 1 3 2008.5 43.3 -2 1 -3 1980.2 43.3 2 1 3 1984.3 42.7 -2 1 -3 1985.4 42.5 -2 1 -3 2025.1 43.4 2 1 3 2007.7 42.4 -2 1 -3 2008.6 43.9 4 -1 3 1378.06 32.7 4 -1 3 1410.06 30.3 -4 -1 -3 1409.26 32.2 4 -1 3 1371.76 32.7 -4 -1 -3 1397.56 30.5 -4 -1 -3 1404.56 31.9 -4 -1 -3 1376.96 32.5 4 -1 3 1397.76 32.6 -4 -1 -3 1412.06 33 4 -1 3 1343.47 34.9 -4 -1 -3 1416.66 34.3 4 1 3 1423.66 32.8 -4 1 -3 1373.16 30.3 -4 1 -3 1382.76 32.4 4 1 3 1428.96 32.5 4 1 3 1334.77 34.6 4 1 3 1401.96 30.6 -4 1 -3 1361.76 32.6 -4 1 -3 1363.86 32.4 4 1 3 1430.66 32.1 -4 1 -3 1394.46 32.7 4 1 3 1331.77 32 -4 1 -3 1410.56 34.5 -5 -1 -3 4194.48 89.59 -5 -1 -3 4268.27 95.09 -5 -1 -3 4371.46 91.89 5 -1 3 4410.06 92.89 -5 -1 -3 4288.37 92.09 5 -1 3 4442.26 92.89 5 -1 3 4347.27 89.39 5 1 3 4360.66 92.89 -5 1 -3 4372.66 92.89 5 1 3 4429.06 92.49 5 1 3 4282.67 89.69 5 1 3 4279.47 91.89 -5 1 -3 4203.98 89.39 -5 1 -3 4303.67 92.89 -5 1 -3 4297.47 95.39 -6 -1 -3 844.52 25 -6 -1 -3 778.32 23.3 -6 -1 -3 811.32 21.4 6 -1 3 795.02 18.3 6 -1 3 853.71 22.6 -6 -1 -3 778.22 21.5 6 -1 3 839.32 21.2 -6 -1 -3 786.52 18.7 6 -1 3 796.42 22.3 6 1 3 810.12 21.8 6 1 3 805.22 18.7 6 1 3 746.43 21.9 -6 1 -3 775.32 18.3 -6 1 -3 820.52 22.3 6 1 3 817.52 21.6 -6 1 -3 796.02 22.3 -6 1 -3 833.72 25.1 -7 -1 -3 196.98 11.3 -7 -1 -3 186.18 6 7 -1 3 194.88 8.5 7 -1 3 194.38 9.5 7 -1 3 212.98 9.7 -7 -1 -3 218.48 9.1 -7 -1 -3 196.88 8.9 7 -1 3 189.18 5.4 -7 1 -3 208.98 11.8 -7 1 -3 203.78 9.4 7 1 3 211.28 9.2 -7 1 -3 206.68 9.6 7 1 3 204.28 9.1 -8 -1 -3 449.36 15.4 8 -1 3 452.05 16.2 8 -1 3 448.56 16.2 -8 -1 -3 461.35 15.2 8 -1 3 477.35 14.9 -8 -1 -3 477.85 19.4 8 1 3 498.95 16 -8 1 -3 467.55 19.4 -8 1 -3 447.76 16 -8 1 -3 442.16 15.9 8 1 3 463.95 15.6 9 -1 3 328.97 14.2 9 -1 3 342.27 12.5 -9 -1 -3 343.27 12.9 -9 -1 -3 377.66 17.8 9 -1 3 356.46 14.4 9 1 3 352.36 13.7 -9 1 -3 336.77 13.8 -9 1 -3 327.87 16.9 9 1 3 322.97 13.1 -10 -1 -3 214.38 14.5 10 -1 3 202.28 9.8 10 -1 3 195.58 11.3 -10 -1 -3 220.68 10.4 -10 1 -3 202.48 11 -10 1 -3 216.88 14.7 10 1 3 198.38 10.6 10 1 3 214.88 11 -11 -1 -3 33.2 7.8 11 -1 3 35.6 7.8 11 -1 3 26.7 5.2 -11 -1 -3 28 4.9 -11 1 -3 29.4 5.7 11 1 3 25.2 4.9 -11 1 -3 31.1 8.1 -12 -1 -3 3 3.1 -12 1 -3 -5.4 2.9 -12 -2 3 -0.6 1.6 12 -2 -3 -4 3.3 -12 -2 3 -4.5 4.4 -12 2 3 -5.1 5 12 2 -3 2 4 -12 2 3 -1.8 2.8 -11 -2 3 9.1 2.3 11 -2 -3 8.3 4.5 -11 -2 3 12.3 5.9 11 -2 -3 12.4 4.5 -11 2 3 6 5.5 11 2 -3 19 4 11 2 -3 14.3 5.1 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3171.18 66.29 1 -3 4 94.99 4.3 -1 -3 -4 83.69 4.1 1 -3 4 92.59 4.4 -1 -3 -4 92.49 3.9 1 -3 4 96.99 4.4 -1 -3 -4 93.49 4.2 1 -3 4 87.69 4 -1 -3 -4 83.49 4 -1 -3 -4 88.59 3.9 1 -3 4 95.49 4.3 1 3 4 90.79 4.3 -1 3 -4 93.09 4.3 -1 3 -4 89.39 3.9 -1 3 -4 99.29 4.2 1 3 4 86.89 4.2 1 3 4 94.49 4.1 1 3 4 91.49 3.9 -1 3 -4 87.99 4.4 -1 3 -4 89.99 4.2 -1 3 -4 88.09 4.2 1 3 4 81.29 3.7 -2 -3 -4 2379.96 51.99 -2 -3 -4 2355.16 52.49 2 -3 4 2439.86 52.09 -2 -3 -4 2456.35 52.29 2 -3 4 2355.06 52.79 2 -3 4 2394.96 53.29 2 -3 4 2441.06 52.69 2 -3 4 2397.86 52.89 -2 -3 -4 2487.25 51.79 -2 -3 -4 2471.55 51.69 2 3 4 2240.78 52.39 -2 3 -4 2365.36 51.89 -2 3 -4 2400.46 50.69 -2 3 -4 2445.46 52.89 2 3 4 2449.35 51.59 -2 3 -4 2423.06 52.69 2 3 4 2418.66 52.09 -2 3 -4 2435.06 52.39 2 3 4 2478.45 53.09 -2 3 -4 2467.35 53.19 2 3 4 2361.76 51.59 3 -3 4 2045.4 46.1 -3 -3 -4 2088.19 44.8 -3 -3 -4 2043.4 42.2 3 -3 4 2031.7 45.7 -3 -3 -4 2016.5 44.3 -3 -3 -4 2019.3 45.5 -3 -3 -4 2064.59 45.8 3 -3 4 2092.89 44.5 -3 -3 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4.6 -6 3 -4 46.9 5.5 6 3 4 64.19 4.9 6 3 4 56.79 5.5 -6 3 -4 45.4 5.8 6 3 4 50.19 3.9 -7 -3 -4 206.68 9 -7 -3 -4 212.08 8.7 7 -3 4 200.88 10.2 -7 -3 -4 202.38 9.2 7 -3 4 204.48 8.6 7 -3 4 199.78 10.5 7 -3 4 203.28 6.7 -7 -3 -4 222.98 11.5 -7 -3 -4 187.78 7.3 -7 3 -4 188.88 10.2 7 3 4 209.08 8.9 -7 3 -4 211.58 11.9 7 3 4 219.28 10.3 8 -3 4 192.28 10.7 -8 -3 -4 171.18 6.5 8 -3 4 164.18 8 -8 -3 -4 178.68 8.4 8 -3 4 155.28 5 8 -3 4 168.68 9.9 -8 -3 -4 172.08 11.3 -8 -3 -4 179.18 8.7 -8 3 -4 164.78 11.4 -8 3 -4 170.38 10.1 8 3 4 177.68 8.7 8 3 4 168.88 9.5 9 -3 4 440.66 17.1 9 -3 4 416.06 14.3 -9 -3 -4 428.76 14.5 9 -3 4 457.85 17.9 -9 -3 -4 437.96 19.4 -9 3 -4 441.16 20.4 9 3 4 438.86 15.3 9 3 4 436.46 16.8 -9 3 -4 404.16 17 10 -3 4 11.8 4.3 -10 -3 -4 3.8 2.9 10 -3 4 3 3.1 -10 -3 -4 3.8 4.9 10 -3 4 12.5 4.9 -10 3 -4 3 3.9 -10 3 -4 3.7 5 10 3 4 12.1 4.3 10 3 4 9.5 6.8 -11 -3 -4 48.4 5.7 -11 -3 -4 48.2 8.9 11 -3 4 82.09 8.6 11 -3 4 49.7 7.4 11 3 4 38.4 6.5 -11 3 -4 52.29 7.4 -11 3 -4 29.2 8.1 -12 -4 4 -0.6 5.2 12 -4 -4 11.9 4.7 12 4 -4 9.8 4.7 12 4 -4 10.3 6.4 -12 4 4 10.4 6.7 -12 4 4 5 4.1 11 -4 -4 170.48 11.6 11 -4 -4 175.78 11.2 -11 -4 4 175.18 13.8 -11 4 4 159.28 10.6 11 4 -4 170.98 10 11 4 -4 174.98 12.2 -11 4 4 173.98 15 10 -4 -4 33.2 5.9 10 -4 -4 39.1 6.6 -10 -4 4 25.1 6.4 10 4 -4 27.8 6.2 10 4 -4 35.3 5.4 -10 4 4 32.9 5.9 -10 4 4 28.6 7.2 9 -4 -4 59.09 6.8 9 -4 -4 55.29 7.1 -9 -4 4 52.99 7.9 9 -4 -4 59.89 4.7 -9 4 4 57.99 3.9 -9 4 4 53.79 6.3 9 4 -4 60.99 3.5 9 4 -4 59.89 6.7 9 4 -4 65.19 6.2 -9 4 4 45 7.8 -8 -4 4 32.2 2.6 8 -4 -4 25.4 4.5 8 -4 -4 34.2 5.2 -8 -4 4 34.6 6.4 -8 -4 4 33.6 3 8 -4 -4 33.5 3.6 -8 4 4 33.7 3.1 8 4 -4 33.4 4.9 -8 4 4 37.6 5.2 -8 4 4 34.1 5.1 8 4 -4 34.7 2.6 8 4 -4 38 6 -8 4 4 29.6 6.1 -7 -4 4 166.88 6.4 -7 -4 4 164.08 10.4 7 -4 -4 180.48 9.1 -7 -4 4 172.08 6.2 7 -4 -4 169.18 6.7 -7 -4 4 157.68 8.2 7 -4 -4 170.58 8.8 7 4 -4 177.18 5.1 -7 4 4 175.38 6.2 -7 4 4 166.18 11.5 -7 4 4 190.48 9.2 7 4 -4 157.48 4.9 -7 4 4 173.38 8.4 7 4 -4 163.38 8.2 7 4 -4 176.48 9.5 6 -4 -4 -0.3 1.9 -6 -4 4 1.6 1.6 -6 -4 4 0.2 2.3 6 -4 -4 1.7 1 6 -4 -4 0.4 1.4 6 -4 -4 0 2.2 -6 -4 4 3.7 1.7 6 4 -4 5.9 3.7 -6 4 4 4.5 2.5 6 4 -4 -0.2 0.7 6 4 -4 1.7 2 -6 4 4 -1 2.5 -6 4 4 0.1 1.2 -6 4 4 2.3 2 6 4 -4 -0.6 1.9 6 4 -4 1.2 0.6 5 -4 -4 795.72 21.4 5 -4 -4 793.92 18.8 -5 -4 4 810.02 22.8 5 -4 -4 800.72 21.5 5 -4 -4 822.52 18.7 -5 -4 4 762.72 21 -5 -4 4 825.62 19.9 -5 -4 4 805.22 19.4 -5 4 4 785.52 21.4 5 4 -4 802.02 21.8 -5 4 4 790.52 24.2 5 4 -4 770.62 21.1 -5 4 4 789.32 18.3 -5 4 4 791.82 21 5 4 -4 806.62 24.5 4 -4 -4 6071.29 124.79 4 -4 -4 6064.49 125.29 4 -4 -4 6041.5 127.49 4 -4 -4 6131.89 127.19 -4 -4 4 6001.3 127.09 -4 -4 4 6212.48 126.39 -4 -4 4 6025.9 127.39 -4 -4 4 6123.39 128.99 -4 -4 4 6206.58 128.49 4 4 -4 6050.19 127.39 -4 4 4 6137.99 130.29 4 4 -4 6174.58 127.59 -4 4 4 6087.29 124.39 -4 4 4 6112.19 127.09 -4 4 4 5921.61 126.19 4 4 -4 6045.8 130.59 -4 4 4 5867.21 127.29 3 -4 -4 6394.36 136.29 -3 -4 4 6503.65 136.79 -3 -4 4 6642.83 136.19 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468.55 10.3 3 -4 4 472.35 13.2 3 -4 4 466.45 14.4 3 -4 4 465.55 14.9 -3 -4 -4 461.05 13.1 -3 -4 -4 474.05 13.7 -3 -4 -4 472.95 15.4 3 -4 4 464.95 14.2 -3 4 -4 475.25 14.4 -3 4 -4 456.45 12.1 3 4 4 483.75 12.7 3 4 4 485.45 14.5 -3 4 -4 457.45 14.5 -3 4 -4 446.76 13.5 3 4 4 477.15 13.4 3 4 4 436.46 12.6 -3 4 -4 469.85 12.9 -3 4 -4 449.76 14.1 3 4 4 461.55 14.2 4 -4 4 77.09 4.5 -4 -4 -4 76.19 4.4 -4 -4 -4 76.09 4.5 4 -4 4 86.69 5.6 -4 -4 -4 79.39 3.2 -4 -4 -4 79.19 4.5 4 -4 4 78.19 5.8 -4 -4 -4 79.59 5.4 4 4 4 76.69 4.7 -4 4 -4 78.59 5.8 4 4 4 72.39 5.4 4 4 4 84.39 4.5 -4 4 -4 81.19 5.9 -4 4 -4 77.19 4.3 5 -4 4 12.1 2.5 -5 -4 -4 19.4 3.2 -5 -4 -4 19.2 2.8 -5 -4 -4 18.6 3.9 -5 -4 -4 20.3 2.9 5 -4 4 19.1 4 5 -4 4 13.9 3.6 -5 -4 -4 23.4 3.2 -5 4 -4 16.9 3.8 -5 4 -4 16.4 3.2 5 4 4 23.2 3.2 -5 4 -4 22.4 4.5 5 4 4 12.6 3.6 5 4 4 22.7 3.3 6 -4 4 13.4 3.7 6 -4 4 17.7 4.6 -6 -4 -4 10.6 2.4 -6 -4 -4 15.2 3 -6 -4 -4 13.8 2.9 6 -4 4 7.9 2.2 -6 -4 -4 15.9 4 -6 -4 -4 10.5 2.7 6 4 4 12.6 2.9 6 4 4 12 3.6 -6 4 -4 11.8 4 -6 4 -4 16.6 4.3 -7 -4 -4 24.8 4.1 7 -4 4 20.8 2.8 7 -4 4 23.2 4.6 -7 -4 -4 24.5 3.7 -7 -4 -4 22.9 3.5 -7 -4 -4 23.6 4.9 7 -4 4 20.8 5.1 -7 -4 -4 17.2 2.9 -7 4 -4 22.9 5.1 7 4 4 26.5 3.9 7 4 4 23.6 4.7 -7 4 -4 25 5.2 -8 -4 -4 636.54 22.6 8 -4 4 609.54 17.6 8 -4 4 624.64 20.7 -8 -4 -4 581.34 16.3 -8 -4 -4 597.54 18.3 -8 -4 -4 617.94 18.6 -8 -4 -4 606.04 17.6 8 -4 4 641.54 21.8 8 -4 4 572.94 14.5 -8 4 -4 617.64 23.6 8 4 4 614.34 18.2 8 4 4 629.94 20.9 -8 4 -4 622.04 21.5 9 -4 4 277.57 13.3 9 -4 4 262.77 10.4 -9 -4 -4 272.87 15.1 -9 -4 -4 264.87 10.5 9 -4 4 272.87 14.1 9 4 4 294.67 13.9 -9 4 -4 273.27 13.9 -9 4 -4 272.27 16.1 9 4 4 280.27 11.4 -10 -4 -4 54.29 8.5 -10 -4 -4 61.99 5.5 10 -4 4 81.39 8.8 10 -4 4 62.09 8 10 -4 4 55.69 5.6 -10 4 -4 52.19 9 -10 4 -4 50.29 7.3 10 4 4 75.89 8.2 11 -4 4 21.1 6.1 11 -4 4 21.6 5.7 -11 -4 -4 16.4 3.8 -11 -4 -4 19.9 6.6 -11 4 -4 10.9 6.4 -11 4 -4 27.9 6.1 11 4 4 17.8 5.1 12 -5 -4 6.6 4.7 -12 -5 4 9.3 5.6 12 5 -4 10.8 5.3 -12 5 4 18.7 5.1 -11 -5 4 -4 3.5 11 -5 -4 4.4 4.5 11 -5 -4 9.2 4.4 -11 -5 4 4.8 3 11 5 -4 0.2 3.8 -11 5 4 3.4 3.7 11 5 -4 5.7 4.3 -11 5 4 -6 4.9 -10 -5 4 32 4.7 -10 -5 4 33.9 7 10 -5 -4 37.7 6.3 10 -5 -4 25.6 6.1 10 -5 -4 32.6 4.3 -10 5 4 23.5 6.6 10 5 -4 30.5 6.5 10 5 -4 32.4 5.8 -10 5 4 30.4 5.9 -9 -5 4 22.6 2.8 -9 -5 4 14.1 4.9 9 -5 -4 17.6 3.4 -9 -5 4 20.4 2.4 9 -5 -4 17 4.7 9 -5 -4 16.7 4.8 -9 5 4 27.1 6.5 -9 5 4 25.4 5.4 9 5 -4 15.6 5.2 9 5 -4 16.1 4.3 9 5 -4 18.3 2 -8 -5 4 22.6 3.6 8 -5 -4 24.8 5.6 -8 -5 4 23.8 3.2 8 -5 -4 31.9 5.3 8 -5 -4 25.6 3.5 -8 -5 4 18.3 5.1 -8 -5 4 15.1 2.6 8 5 -4 26.3 4.9 -8 5 4 17.3 4.8 8 5 -4 27.6 1.7 -8 5 4 22 6 -8 5 4 24.6 3 8 5 -4 17.1 4.8 7 -5 -4 1808.82 40.8 -7 -5 4 1843.72 46.6 -7 -5 4 1848.92 41.4 7 -5 -4 1802.42 44.2 7 -5 -4 1751.82 38.5 7 -5 -4 1826.82 44.7 -7 -5 4 1827.22 41 -7 -5 4 1743.53 40.3 7 -5 -4 1802.12 38.6 7 5 -4 1864.41 44.1 -7 5 4 1742.33 39.8 -7 5 4 1810.22 44.4 -7 5 4 1785.22 48.5 7 5 -4 1845.32 45 7 5 -4 1818.32 48.5 6 -5 -4 -2.7 2.2 -6 -5 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14.9 10 -4 -7 337.37 14.6 -10 -4 7 310.27 17.3 10 4 -7 309.97 15.5 -10 4 7 302.67 18.2 -10 4 7 298.97 13.6 10 4 -7 299.67 12.8 -9 -4 7 326.17 16.6 -9 -4 7 278.37 8.3 -9 -4 7 288.47 10.1 -9 -4 7 293.77 8.7 9 -4 -7 309.77 13.4 -9 -4 7 300.77 9.6 9 -4 -7 287.37 13.7 -9 4 7 270.17 11.8 -9 4 7 315.07 13.2 -9 4 7 302.57 17.1 9 4 -7 299.97 12.2 9 4 -7 295.17 14.2 -8 -4 7 46.4 7.2 8 -4 -7 65.69 6.5 -8 -4 7 47.4 3.7 -8 -4 7 57.59 4 8 -4 -7 55.39 6.3 -8 -4 7 62.79 4.3 -8 4 7 63.89 6.2 -8 4 7 60.19 2.5 8 4 -7 60.39 7.4 -8 4 7 48 7.8 8 4 -7 54.09 5.6 -8 4 7 46 5.1 7 -4 -7 958.1 22.2 -7 -4 7 956 23.8 7 -4 -7 986.1 27.6 7 -4 -7 951.2 20.9 -7 -4 7 966.8 23.4 -7 -4 7 955.4 29.5 -7 -4 7 958.5 22.8 7 4 -7 998.6 26.1 -7 4 7 901.01 25.3 -7 4 7 974.2 31.5 7 4 -7 973.8 32 7 4 -7 921.01 27.3 -7 4 7 992.4 26.5 6 -4 -7 971.6 26 6 -4 -7 914.11 22 6 -4 -7 914.01 20.1 -6 -4 7 935.81 21.7 6 -4 -7 897.91 24.8 -6 -4 7 907.41 27.1 -6 -4 7 930.91 23.2 -6 4 7 878.01 24 6 4 -7 912.81 29.6 -6 4 7 899.71 24.6 6 4 -7 943.31 25.8 6 4 -7 926.51 24.4 -6 4 7 909.41 28.7 5 -4 -7 408.76 13.2 5 -4 -7 391.16 9.5 -5 -4 7 389.56 10.8 -5 -4 7 397.66 12.3 5 -4 -7 395.16 11.5 5 -4 -7 409.96 13.6 -5 -4 7 403.66 14.6 5 4 -7 383.96 12.8 -5 4 7 383.66 12.9 -5 4 7 375.46 12.5 -5 4 7 394.56 11.4 5 4 -7 389.66 16.3 5 4 -7 394.06 13.3 4 -4 -7 316.67 10.9 4 -4 -7 316.97 10.9 -4 -4 7 314.97 10.4 4 -4 -7 332.47 10.1 -4 -4 7 316.77 9.1 -4 -4 7 314.47 12.1 4 -4 -7 319.27 8.1 -4 -4 7 321.87 10.6 -4 4 7 312.57 10.5 -4 4 7 309.47 10.7 4 4 -7 319.37 10.9 -4 4 7 319.07 8.1 4 4 -7 321.37 11 4 4 -7 294.67 7.6 4 4 -7 321.57 7.7 4 4 -7 315.37 13.5 -4 4 7 328.37 10 3 -4 -7 1617.64 36.8 -3 -4 7 1618.74 35.5 -3 -4 7 1624.24 37.3 3 -4 -7 1608.94 36.5 3 -4 -7 1629.14 34.4 -3 -4 7 1680.63 34.2 -3 -4 7 1622.04 33.8 -3 -4 7 1569.64 36 -3 -4 7 1544.15 35.9 3 -4 -7 1635.04 37.3 -3 -4 7 1622.84 37.5 3 4 -7 1565.24 36.9 3 4 -7 1603.64 40.4 3 4 -7 1634.94 37.4 -3 4 7 1523.15 37.5 -3 4 7 1554.64 36.7 3 4 -7 1509.45 34.2 -3 4 7 1623.54 36.6 3 4 -7 1594.04 35.2 3 4 -7 1627.44 36.7 -3 4 7 1656.13 37.2 -2 -4 7 199.98 7.9 2 -4 -7 204.58 7.7 -2 -4 7 192.38 8 2 -4 -7 200.78 7.6 2 -4 -7 197.48 7.3 -2 -4 7 205.98 6.4 -2 -4 7 189.18 6.4 -2 -4 7 189.58 7.7 -2 -4 7 212.48 7 -2 -4 7 193.88 6.2 -2 -4 7 188.28 5.9 -2 4 7 184.88 7.4 -2 4 7 192.28 7.5 -2 4 7 189.08 7.3 2 4 -7 177.08 8.6 2 4 -7 193.08 6.5 2 4 -7 193.18 7.6 2 4 -7 183.58 6.1 2 4 -7 190.88 6.7 2 4 -7 194.98 6.3 -2 4 7 181.98 7.2 0 -4 -7 232.18 8.1 0 -4 7 239.88 8.6 0 -4 -7 230.48 8.1 0 -4 7 229.88 8.2 0 -4 7 237.78 8.5 0 -4 -7 235.68 8.6 0 -4 -7 245.88 8.2 0 -4 -7 237.98 8.4 0 -4 7 234.48 8.4 0 -4 7 232.18 8.9 0 -4 7 243.18 8 0 -4 7 236.68 8.7 0 4 7 236.58 8.3 0 4 7 231.38 8.2 0 4 -7 242.08 7.8 0 4 7 237.28 7.9 0 4 -7 217.18 8 0 4 -7 230.48 8.1 0 4 -7 227.28 8.9 0 4 -7 251.47 8.5 0 4 7 236.28 8.4 0 4 7 246.48 8.8 0 4 -7 233.88 8.7 -1 -4 -7 3753.52 78.19 -1 -4 -7 3615.24 78.69 1 -4 7 3703.33 79.19 1 -4 7 3669.93 78.79 -1 -4 -7 3682.43 78.39 1 -4 7 3647.33 78.49 1 -4 7 3681.63 79.09 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4 -7 22.5 4.6 -4 4 -7 13.9 2.7 4 4 7 15.9 3.1 4 4 7 12.6 3.3 -5 -4 -7 378.96 13.6 5 -4 7 395.66 15 5 -4 7 388.16 12.9 5 -4 7 388.76 15.1 -5 -4 -7 416.06 13.4 -5 -4 -7 410.16 15.1 5 4 7 383.86 13.1 5 4 7 402.36 15.2 -5 4 -7 388.86 15.2 5 4 7 383.66 13.1 -5 4 -7 401.66 15.5 -6 -4 -7 868.61 26.3 6 -4 7 854.61 22.7 6 -4 7 890.41 26.5 -6 -4 -7 866.61 24.6 -6 -4 -7 866.51 23.7 6 -4 7 873.91 26.1 6 4 7 871.81 23.5 6 4 7 902.51 26.4 -6 4 -7 835.42 26.2 -6 4 -7 882.11 27.2 6 4 7 897.31 24 7 -4 7 -0.4 2 -7 -4 -7 1 3 7 -4 7 -1 3.3 -7 -4 -7 -0.3 2.3 -7 -4 -7 0.6 2.5 7 -4 7 1.7 3.3 -7 4 -7 -1.3 3.2 7 4 7 1.2 2.4 -7 4 -7 0.4 4 7 4 7 -0.6 2.7 7 4 7 1.5 3.4 8 -4 7 63.89 8.1 8 -4 7 64.89 8.3 -8 -4 -7 46.8 7.2 -8 -4 -7 67.29 6.2 8 -4 7 60.69 4.7 8 4 7 69.79 6.6 -8 4 -7 64.29 8.4 -8 4 -7 60.09 8.7 8 4 7 65.89 7.7 9 -4 7 10 3.9 -9 -4 -7 19.4 4.4 9 -4 7 19.7 5.4 9 -4 7 19.4 5.6 -9 -4 -7 1 4.5 9 4 7 14.7 4.6 -9 4 -7 8.4 5.7 9 4 7 14.6 4.4 -9 4 -7 14.4 5 10 -4 7 77.99 9.1 10 -4 7 79.99 8.8 -10 -4 -7 82.39 7 10 -4 7 71.19 7.3 -10 -4 -7 58.49 9.3 10 4 7 75.49 8.5 -10 4 -7 59.59 8.3 -10 4 -7 78.39 11.1 -12 -5 7 8 5.7 12 -5 -7 16.8 5.6 12 5 -7 10.7 4.9 -12 5 7 7 4.1 11 -5 -7 20.7 6.5 11 -5 -7 9.6 5.2 -11 -5 7 10 5.4 11 5 -7 14.8 4.5 -11 5 7 15.8 5 11 5 -7 12.3 5.7 -11 5 7 10.6 6.1 10 -5 -7 4.9 4 -10 -5 7 2.7 4.4 -10 -5 7 4.4 2.5 10 -5 -7 8.5 4.5 -10 5 7 2.3 5.3 10 5 -7 3.1 3.5 10 5 -7 6.5 4.9 -10 5 7 9.9 3.9 9 -5 -7 92.69 7.9 9 -5 -7 82.89 7.7 -9 -5 7 66.79 4.5 -9 -5 7 77.69 8.6 -9 -5 7 80.69 5 -9 5 7 97.19 10.5 -9 5 7 68.69 3.2 -9 5 7 66.69 7.1 9 5 -7 79.69 7 9 5 -7 77.19 7.5 8 -5 -7 37.3 5.8 -8 -5 7 40.6 3.8 8 -5 -7 43.4 6.2 -8 -5 7 40.9 4.1 8 -5 -7 43.2 2.8 -8 -5 7 45.3 6.9 8 -5 -7 32.7 2.7 8 5 -7 41.5 5.3 -8 5 7 37.2 6.7 -8 5 7 36.8 2.4 -8 5 7 33.1 5.2 8 5 -7 42.9 6.7 -7 -5 7 266.07 13.4 7 -5 -7 266.37 7.7 -7 -5 7 276.77 10.1 -7 -5 7 260.57 8.9 7 -5 -7 254.87 8.5 7 -5 -7 269.07 12.1 -7 5 7 268.37 11.6 -7 5 7 270.87 14.9 7 5 -7 248.78 14.8 7 5 -7 284.87 11.5 7 5 -7 271.87 12.3 6 -5 -7 -0.3 1.7 -6 -5 7 1.4 2.6 6 -5 -7 2.2 1.2 -6 -5 7 2.4 2.1 6 -5 -7 -0.7 2.3 6 -5 -7 0.6 2.2 -6 -5 7 3.2 1.8 -6 5 7 3.1 2.6 -6 5 7 1.7 2.3 -6 5 7 2.9 3.4 6 5 -7 2.8 2.3 6 5 -7 -0.5 3.1 6 5 -7 2.9 2.8 -5 -5 7 108.09 5.9 5 -5 -7 117.89 6.6 5 -5 -7 107.49 4.2 -5 -5 7 111.39 5 -5 -5 7 111.29 7.1 5 -5 -7 111.29 6.8 5 -5 -7 111.09 5.4 5 5 -7 122.69 6.8 -5 5 7 99.49 6.1 5 5 -7 120.39 8.8 -5 5 7 111.19 6.6 -5 5 7 108.69 5.4 5 5 -7 107.19 6.5 -4 -5 7 35 3.6 4 -5 -7 31.1 3.1 4 -5 -7 32.7 2.4 -4 -5 7 35.1 2.8 4 -5 -7 35.4 3.6 -4 -5 7 37.8 3.3 4 -5 -7 32.5 4 4 5 -7 32.4 1.6 4 5 -7 30.1 3.5 4 5 -7 37.8 3.6 -4 5 7 36.3 3.8 4 5 -7 42.8 6.4 -4 5 7 36.3 3.6 4 5 -7 31.9 1.6 -4 5 7 38.1 3.3 -4 5 7 35.3 2.1 3 -5 -7 1918.01 43.3 3 -5 -7 1951.5 44.3 -3 -5 7 1891.91 42 -3 -5 7 1939.91 42.5 3 -5 -7 1903.31 43.4 -3 -5 7 1838.62 42.3 -3 -5 7 1954 40.1 3 -5 -7 1905.31 41.2 -3 -5 7 1980.3 40.5 -3 -5 7 1979 44.4 3 5 -7 1889.31 42.1 -3 5 7 1942.51 43.5 -3 5 7 1915.11 43.7 -3 5 7 1871.01 44.3 -3 5 7 1907.01 41.5 3 5 -7 1920.41 44.4 3 5 -7 1929.91 47.2 -3 5 7 1910.01 44.1 3 5 -7 1965.2 43.2 3 5 -7 1852.31 40.7 -2 -5 7 877.91 23.1 -2 -5 7 922.81 21.9 -2 -5 7 893.61 20.6 2 -5 -7 888.61 22.6 2 -5 -7 900.31 20.9 2 -5 -7 882.41 22.8 -2 -5 7 883.11 20.7 -2 -5 7 890.71 20.4 -2 -5 7 898.31 20.5 2 -5 -7 885.71 22.3 -2 5 7 873.21 21.9 2 5 -7 848.82 20.7 -2 5 7 884.21 22.7 2 5 -7 884.41 21.2 -2 5 7 888.21 22.7 2 5 -7 902.21 21.5 2 5 -7 894.61 20.9 2 5 -7 900.21 24.9 -2 5 7 886.71 21.4 -2 5 7 895.61 22.5 2 5 -7 827.62 22.6 1 -5 -7 1998.9 45 1 -5 -7 2104.29 45.8 1 -5 -7 2045.1 45.7 1 -5 -7 1992.7 45.7 -1 -5 7 2077.29 48 -1 -5 7 2003.3 46.3 -1 -5 7 2075.69 48 -1 -5 7 2017.7 45.1 -1 -5 7 2076.29 43.8 -1 -5 7 1994.1 44.4 -1 -5 7 2019.9 44.2 -1 5 7 2022.6 45.9 1 5 -7 1935.71 44.3 1 5 -7 2005.7 43.1 -1 5 7 2015 44.5 -1 5 7 2055.99 45.1 -1 5 7 1936.21 45.1 1 5 -7 1982 47.6 1 5 -7 1965.2 44.5 1 5 -7 2045.6 44.6 -1 5 7 2001.2 45.4 1 5 -7 2013.3 47.1 1 5 -7 1998.6 43.7 0 -5 -7 6629.44 136.79 0 -5 7 6681.23 138.29 0 -5 7 6742.73 137.19 0 -5 7 6581.34 137.39 0 -5 7 6551.64 135.89 0 -5 7 6738.53 136.89 0 -5 -7 6520.25 137.19 0 -5 7 6580.64 139.09 0 5 -7 6659.23 137.29 0 5 -7 5996.1 137.19 0 5 7 6726.63 137.69 0 5 7 6576.84 137.89 0 5 7 6614.24 137.09 0 5 -7 6453.95 133.99 0 5 7 6585.74 136.59 0 5 -7 6470.85 136.69 -1 -5 -7 924.41 24.3 1 -5 7 982.2 25.7 -1 -5 -7 1007.4 24.9 1 -5 7 989.2 24.8 1 -5 7 1014.4 25.5 -1 -5 -7 1026.1 24.4 1 -5 7 1004.6 25.6 1 -5 7 1022.7 25.5 1 5 7 1026.5 25.9 1 5 7 977.5 22.5 1 5 7 969.7 24.7 1 5 7 1002.9 25.6 -1 5 -7 1023 25.8 -1 5 -7 1007.9 25.7 1 5 7 1077.69 25 -1 5 -7 1010.8 24.2 2 -5 7 460.95 14.7 2 -5 7 468.05 14.9 2 -5 7 462.25 14.8 -2 -5 -7 444.76 13.7 2 -5 7 467.35 14.9 -2 -5 -7 491.95 14.2 2 -5 7 461.25 14.6 -2 -5 -7 473.25 13.9 2 5 7 462.55 15.1 -2 5 -7 477.55 14.8 2 5 7 482.55 13.9 2 5 7 440.06 14.1 2 5 7 475.35 14.7 -2 5 -7 477.35 14 -2 5 -7 459.95 11.7 -2 5 -7 481.45 15.2 -3 -5 -7 22.2 3.3 -3 -5 -7 20.2 3.1 3 -5 7 22.1 4.1 -3 -5 -7 24.8 4 3 -5 7 38.5 4.2 3 -5 7 25.5 3.8 3 5 7 21.2 3.3 3 5 7 19.4 3.8 -3 5 -7 21.9 2.5 3 5 7 15.7 3.1 -3 5 -7 23.9 4.2 -3 5 -7 25.9 4.6 -3 5 -7 23.8 3.8 4 -5 7 7.6 3.3 -4 -5 -7 16.4 3.9 4 -5 7 7.2 2.8 4 -5 7 9.6 3.6 -4 -5 -7 14.1 3.1 -4 -5 -7 16.1 3.2 4 5 7 13.7 3 -4 5 -7 13.4 2.5 -4 5 -7 10.8 3.3 4 5 7 7.4 2.9 -4 5 -7 6.1 3.7 4 5 7 10.4 3.4 5 -5 7 1799.72 42.3 -5 -5 -7 1725.23 42.8 -5 -5 -7 1799.92 42.2 -5 -5 -7 1867.81 44.6 5 -5 7 1734.03 45 5 -5 7 1779.12 44.7 5 5 7 1785.92 42.2 -5 5 -7 1819.12 45.2 5 5 7 1821.32 45.2 5 5 7 1882.91 43.1 -5 5 -7 1756.82 45.2 6 -5 7 0 3.9 6 -5 7 3.1 3.5 -6 -5 -7 0.4 2.1 -6 -5 -7 3.6 3.6 6 -5 7 -1.5 2.2 -6 -5 -7 -0.8 2.2 -6 5 -7 -2.8 3.1 6 5 7 3.8 2.7 -6 5 -7 0.4 3.3 6 5 7 -1.6 3.1 6 5 7 0.6 2.7 -7 -5 -7 7.2 4.3 -7 -5 -7 14.3 3.4 7 -5 7 10.3 4.6 7 -5 7 17.4 4.9 7 -5 7 10 2.9 -7 -5 -7 12.2 3.5 7 5 7 9.8 4.2 -7 5 -7 14.4 4.7 -7 5 -7 4.4 4.2 7 5 7 10.9 3.6 8 -5 7 27 6.2 -8 -5 -7 32.3 5 8 -5 7 30.9 3.9 -8 -5 -7 21.3 5.4 8 -5 7 29.9 5.8 8 5 7 27.2 4.7 8 5 7 36.7 6.6 -8 5 -7 27.4 5.7 -8 5 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3 4 -9 3987.1 84.59 -3 4 9 3973 84.79 -2 -4 9 1747.63 39.3 2 -4 -9 1702.63 38.7 -2 -4 9 1795.52 39.3 2 -4 -9 1763.02 40.7 -2 -4 9 1742.33 39.5 -2 -4 9 1793.92 41.4 -2 -4 9 1796.52 38.7 2 4 -9 1759.22 39 -2 4 9 1712.63 40.2 -2 4 9 1802.22 41 2 4 -9 1760.02 39.3 2 4 -9 1757.12 43.5 -2 4 9 1707.33 42.5 2 4 -9 1735.13 39 2 4 -9 1667.43 38.8 -2 4 9 1819.42 40.7 1 -4 -9 1271.77 30.1 -1 -4 9 1320.07 30.2 1 -4 -9 1300.57 31.2 1 -4 -9 1285.27 31.4 -1 -4 9 1340.27 30.9 -1 -4 9 1298.37 30 -1 -4 9 1292.47 31.9 -1 -4 9 1297.67 30.6 -1 4 9 1287.67 31.6 -1 4 9 1258.47 31.5 1 4 -9 1288.17 30 1 4 -9 1259.97 29.1 1 4 -9 1266.57 30.1 1 4 -9 1303.07 30.4 -1 4 9 1287.57 31 -1 4 9 1304.17 31.1 1 4 -9 1267.47 32.9 0 -4 9 533.75 16.2 0 -4 -9 506.45 15.2 0 -4 9 531.15 15 0 -4 9 519.25 15.4 0 -4 9 546.05 15.5 0 -4 9 524.35 15 0 -4 -9 511.15 14.9 0 -4 -9 510.05 14.9 0 -4 -9 518.15 15 0 4 -9 520.85 14.5 0 4 -9 544.95 16.4 0 4 9 520.65 15.8 0 4 -9 536.45 15.4 0 4 9 514.05 14.1 0 4 9 527.45 15.2 1 -4 9 274.07 10.3 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5 -4 9 -1.3 3.3 -5 4 -9 1.5 3.3 5 4 9 -2.8 2.7 5 4 9 -0.1 2.7 -5 4 -9 -2 3.4 -5 4 -9 9 4 5 4 9 2.6 3.4 6 -4 9 85.69 8.2 6 -4 9 78.09 7.7 -6 -4 -9 75.69 6.5 6 -4 9 85.19 6.2 -6 -4 -9 79.99 7.8 -6 4 -9 81.99 8.4 6 4 9 72.99 7.7 -6 4 -9 78.09 8 6 4 9 89.49 6.8 6 4 9 84.39 6.8 -7 -4 -9 -2.4 3.3 -7 -4 -9 0 2.8 7 -4 9 0.3 2.3 7 -4 9 -5.7 3.2 7 -4 9 -6.1 3 7 4 9 3.8 2.8 7 4 9 0.2 3.5 -7 4 -9 -3.5 3.7 7 4 9 -2.4 2.5 -7 4 -9 -0.4 3.3 -8 -4 -9 251.47 11.7 -8 -4 -9 262.47 15.1 8 -4 9 246.38 10.1 8 -4 9 272.57 14.3 8 -4 9 243.78 14 8 4 9 254.97 13.7 -8 4 -9 245.08 15 8 4 9 265.17 12.3 -8 4 -9 237.78 13.6 8 4 9 260.47 10.9 9 -4 9 18.7 6.3 -9 -4 -9 11.8 5.7 -9 -4 -9 21.6 4.8 9 -4 9 23.9 6.6 9 -4 9 10.6 4.4 -9 4 -9 16.6 5.9 9 4 9 20.8 6 -9 4 -9 9 5.9 9 4 9 13.6 4.6 10 -4 9 7.1 4.9 10 -4 9 22.1 6 -10 -4 -9 1.1 5.8 -10 -4 -9 15 4.5 10 -4 9 18.8 6.1 10 4 9 16.3 5.6 -12 -5 9 -3.9 4.5 12 -5 -9 5 4.4 -12 5 9 6.2 4.3 11 -5 -9 150.88 11.2 -11 -5 9 144.69 13.1 11 -5 -9 137.09 11.2 11 5 -9 147.09 9.3 -11 5 9 142.19 14.8 11 5 -9 144.49 11.9 -11 5 9 145.59 10.4 -10 -5 9 4 2.2 10 -5 -9 9.7 4.6 10 -5 -9 5.6 4.2 -10 -5 9 7.5 4.7 -10 5 9 7.1 5.7 10 5 -9 4.2 3.4 10 5 -9 1.8 4.9 -10 5 9 1.3 3.5 9 -5 -9 16.9 2 -9 -5 9 18.5 2.9 9 -5 -9 23.7 4.9 -9 -5 9 18.4 3.3 9 -5 -9 27.6 5.5 -9 -5 9 22.2 5.4 9 5 -9 18.3 4.3 -9 5 9 13.7 5.5 9 5 -9 22.6 5.3 -9 5 9 20.9 4.9 -8 -5 9 181.48 8.1 -8 -5 9 162.88 6.9 -8 -5 9 172.58 11.6 -8 -5 9 165.78 6.7 8 -5 -9 163.18 10.3 8 -5 -9 166.48 6.7 8 5 -9 167.48 13.3 -8 5 9 186.38 10 8 5 -9 186.58 9.6 8 5 -9 178.78 10.6 -8 5 9 166.58 13 -7 -5 9 318.07 11.5 -7 -5 9 302.47 14.5 7 -5 -9 292.47 10 7 -5 -9 294.27 13 -7 -5 9 299.57 9.5 7 -5 -9 307.97 12.8 7 5 -9 291.57 12.9 7 5 -9 304.57 12.3 -7 5 9 296.47 12.5 7 5 -9 308.87 16.9 -7 5 9 287.87 15.6 6 -5 -9 610.54 17.3 6 -5 -9 625.54 14.1 -6 -5 9 643.34 21.4 -6 -5 9 621.04 16.3 6 -5 -9 636.44 19.7 6 -5 -9 615.14 19.7 -6 -5 9 627.14 18.4 6 5 -9 603.44 19 -6 5 9 630.14 17.3 6 5 -9 648.14 24.5 -6 5 9 626.84 19.4 6 5 -9 644.34 20 -5 -5 9 140.39 7.3 5 -5 -9 135.39 7.5 -5 -5 9 138.19 5.8 5 -5 -9 139.49 4.6 5 -5 -9 136.79 7.6 5 5 -9 129.69 7.4 5 5 -9 133.89 4.1 5 5 -9 145.59 7.6 5 5 -9 145.99 10.4 5 5 -9 123.19 4 -5 5 9 140.79 4.6 -5 5 9 144.59 6.9 -5 5 9 140.19 7.6 4 -5 -9 142.29 4.9 -4 -5 9 147.79 4.5 -4 -5 9 133.69 7.2 -4 -5 9 141.19 4.2 -4 -5 9 145.59 6.5 -4 -5 9 144.89 6.1 4 -5 -9 139.19 7.1 4 -5 -9 137.39 7.4 4 5 -9 134.19 6.9 -4 5 9 132.29 7.2 4 5 -9 140.89 5.7 -4 5 9 143.09 6.8 4 5 -9 141.19 9.7 -4 5 9 142.09 5.4 4 5 -9 136.49 4.8 -3 -5 9 1999.1 44.7 3 -5 -9 2099.29 46 -3 -5 9 2061.39 43.4 3 -5 -9 1982.6 43.2 -3 -5 9 1985.4 46.8 -3 -5 9 2046.5 42.8 -3 -5 9 1950.6 44 -3 -5 9 1958.2 44.1 3 -5 -9 2041.2 46.5 3 5 -9 2045 45.3 3 5 -9 1909.11 43.3 -3 5 9 2005 44.3 -3 5 9 2025.5 46.4 3 5 -9 1948.8 49.9 3 5 -9 1965.9 44 -3 5 9 2002.7 46 3 5 -9 1970.5 43.3 -2 -5 9 2735.43 60.89 2 -5 -9 2669.93 60.09 -2 -5 9 2721.13 58.99 2 -5 -9 2537.95 57.89 -2 -5 9 2680.63 57.99 -2 -5 9 2703.33 57.49 -2 -5 9 2739.93 58.19 2 5 -9 2676.03 57.99 -2 5 9 2737.93 60.09 2 5 -9 2624.74 58.19 2 5 -9 2662.03 57.99 -2 5 9 2759.82 60.29 -2 5 9 2585.14 61.89 -2 5 9 2734.13 58.79 2 5 -9 2705.73 62.99 -1 -5 9 165.78 8.1 -1 -5 9 162.48 6.9 -1 -5 9 161.88 6.7 -1 -5 9 159.78 6.8 1 -5 -9 152.88 7.5 1 -5 -9 167.78 6.9 1 -5 -9 174.68 7.7 -1 -5 9 165.78 7.3 -1 5 9 162.58 7.7 -1 5 9 157.48 7.7 -1 5 9 165.98 7.5 1 5 -9 148.99 8.4 -1 5 9 162.78 7.2 1 5 -9 163.88 5.9 1 5 -9 173.38 7.1 1 5 -9 151.78 6.5 0 -5 -9 185.48 7.8 0 -5 9 172.68 8.5 0 -5 9 180.88 8 0 -5 9 171.08 7.8 0 -5 -9 183.48 8 0 -5 9 175.28 7.6 0 -5 9 176.38 7.3 0 5 -9 183.68 5.9 0 5 9 172.38 7 0 5 9 177.58 7.9 0 5 -9 176.28 8.7 0 5 9 171.48 8 0 5 9 182.18 8.3 0 5 -9 179.58 7.2 0 5 -9 177.98 7.9 1 -5 9 98.99 6.1 1 -5 9 97.99 5.8 1 -5 9 112.59 6.4 -1 -5 -9 101.39 6.6 1 -5 9 99.69 6.1 -1 -5 -9 105.29 6.2 -1 -5 -9 105.99 6.1 1 -5 9 102.29 6.3 -1 5 -9 100.99 6.5 1 5 9 102.99 6 -1 5 -9 99.09 6.3 1 5 9 95.09 6.2 1 5 9 101.29 3.6 -1 5 -9 95.59 6.1 1 5 9 98.19 6.4 2 -5 9 1133.19 28.6 2 -5 9 1069.39 28.3 -2 -5 -9 1013.2 27 -2 -5 -9 1130.69 27.8 -2 -5 -9 1073.29 27.5 2 -5 9 1042.8 28.4 2 5 9 1080.09 28.3 -2 5 -9 1071.89 28.1 2 5 9 1083.89 27.3 -2 5 -9 1084.89 28.8 -2 5 -9 1060.69 27.3 2 5 9 1067.59 28.8 3 -5 9 45 5.1 3 -5 9 32.2 4.4 -3 -5 -9 45.9 6.1 -3 -5 -9 39.8 4.4 3 -5 9 39.9 5.5 -3 -5 -9 45 5.3 -3 5 -9 44 5.7 -3 5 -9 42.5 3.4 -3 5 -9 36.2 5.1 3 5 9 35.6 5 -3 5 -9 49.4 6.2 3 5 9 47.2 5.2 3 5 9 44 4.7 4 -5 9 73.79 6.1 -4 -5 -9 83.09 7.2 4 -5 9 75.79 7.3 -4 -5 -9 74.89 6 4 -5 9 67.59 6.4 -4 5 -9 80.89 7.1 4 5 9 85.09 6.6 -4 5 -9 82.79 7.5 4 5 9 81.49 7.4 -4 5 -9 76.99 5.3 4 5 9 80.59 6.2 -4 5 -9 82.99 7.4 5 -5 9 106.39 7.1 5 -5 9 96.69 8.5 -5 -5 -9 97.39 8.5 -5 -5 -9 96.39 6.9 5 -5 9 91.99 8 -5 5 -9 99.69 7.7 5 5 9 88.29 8.2 -5 5 -9 96.09 8.4 5 5 9 98.99 7.3 5 5 9 91.19 6.8 -5 5 -9 104.19 8 -6 -5 -9 55.19 5.8 -6 -5 -9 49.9 7 6 -5 9 58.49 7.2 6 -5 9 49.5 5.2 6 -5 9 49.99 7.2 -6 5 -9 43.4 6.8 6 5 9 50.29 5.9 6 5 9 53.89 7.3 6 5 9 52.39 6.1 -6 5 -9 53.59 7.5 -7 -5 -9 81.19 9 7 -5 9 79.89 8.2 7 -5 9 91.69 9.1 7 -5 9 88.49 6.5 -7 -5 -9 86.69 6.9 -7 5 -9 73.69 8.1 -7 5 -9 91.89 9.4 7 5 9 88.09 8.5 7 5 9 87.99 7 7 5 9 85.79 6.9 -8 -5 -9 42.4 5.9 8 -5 9 55.59 5.4 8 -5 9 50.39 8 -8 -5 -9 39.8 7.2 8 -5 9 57.89 8 8 5 9 50.29 7.5 8 5 9 60.89 7.1 -8 5 -9 53.69 7.9 -8 5 -9 35.6 7.1 9 -5 9 102.29 8.5 -9 -5 -9 114.79 11.7 9 -5 9 112.09 10.5 -9 -5 -9 123.49 8.4 9 -5 9 129.79 11.3 -9 5 -9 114.79 12 9 5 9 120.99 10.8 -9 5 -9 132.99 11 10 -5 9 12.1 5.2 -10 -5 -9 -1.3 5.3 -10 -5 -9 6.6 3.7 10 -5 9 10.6 5.4 10 5 9 7.8 5.3 12 -6 -9 8 5.3 -12 -6 9 -2.6 4.7 -12 6 9 4.6 4.2 11 -6 -9 9.6 4.9 -11 -6 9 3.5 4.6 11 -6 -9 17.8 5 11 6 -9 2.4 3.7 -11 6 9 6.7 6.3 -11 6 9 6.3 4.2 11 6 -9 3.3 4.7 -10 -6 9 30.4 3.9 10 -6 -9 37 6.4 -10 -6 9 33.4 6.6 10 -6 -9 34.1 6.5 -10 -6 9 30.9 4.1 -10 6 9 26.9 7.9 10 6 -9 28.6 5.2 10 6 -9 32.3 6.4 -10 6 9 30.1 6.2 -9 -6 9 201.58 12.9 9 -6 -9 190.68 11.5 9 -6 -9 185.38 11.5 -9 -6 9 171.88 8.3 -9 -6 9 169.68 7.5 9 6 -9 192.88 11.7 9 6 -9 189.58 10.5 -9 6 9 186.78 11 -9 6 9 191.28 14.4 8 -6 -9 40.8 4 8 -6 -9 31 5.7 -8 -6 9 35.4 4.6 -8 -6 9 33.8 3.6 -8 -6 9 30.6 6 8 6 -9 40.8 5.7 8 6 -9 30.7 5.5 -8 6 9 31.3 5.2 8 6 -9 38.1 9 -8 6 9 31 6.6 7 -6 -9 81.09 5.2 -7 -6 9 79.59 6 -7 -6 9 78.49 4.8 7 -6 -9 80.69 3.3 -7 -6 9 77.89 7.6 7 -6 -9 70.29 6.9 7 -6 -9 88.69 7.4 7 6 -9 79.99 9.6 7 6 -9 86.69 7.3 -7 6 9 83.19 9.1 7 6 -9 84.69 6.7 -7 6 9 76.49 6.8 -6 -6 9 62.29 6.2 -6 -6 9 66.39 5.8 -6 -6 9 56.79 4.3 6 -6 -9 55.79 6 6 -6 -9 54.79 3.1 6 -6 -9 70.89 6.5 6 6 -9 63.69 8.3 6 6 -9 74.69 6.2 -6 6 9 47.9 5.4 5 -6 -9 222.38 10 5 -6 -9 208.78 6.8 -5 -6 9 225.08 9.8 -5 -6 9 235.58 8.4 5 -6 -9 221.78 10.4 5 6 -9 225.18 10.2 5 6 -9 220.78 5.5 5 6 -9 191.18 5.3 -5 6 9 224.58 9 5 6 -9 213.48 9.5 -5 6 9 206.48 9.9 5 6 -9 210.78 12.5 -5 6 9 214.58 6.3 -4 -6 9 766.62 20.1 -4 -6 9 784.22 20.4 -4 -6 9 833.82 17.4 4 -6 -9 807.82 19 4 -6 -9 795.62 22.7 -4 -6 9 762.42 17 -4 -6 9 814.62 22.6 4 -6 -9 816.72 22.1 -4 6 9 771.62 19.1 4 6 -9 806.72 21.5 -4 6 9 776.12 22.3 4 6 -9 781.22 26 -4 6 9 812.22 21.7 4 6 -9 785.42 18.2 4 6 -9 740.03 18.2 3 -6 -9 85.49 6 3 -6 -9 86.49 4.4 -3 -6 9 76.89 3.7 -3 -6 9 91.89 5.2 -3 -6 9 89.99 4 -3 -6 9 66.39 4.4 -3 -6 9 76.89 4.3 3 -6 -9 81.39 5.2 -3 -6 9 99.19 6.3 3 6 -9 88.79 4.3 3 6 -9 82.59 7.5 3 6 -9 98.69 5.3 -3 6 9 93.89 5.9 -3 6 9 93.49 4.9 -3 6 9 93.69 6.2 -2 -6 9 314.17 10.8 -2 -6 9 300.17 9.6 -2 -6 9 304.97 11.9 -2 -6 9 315.87 9.6 2 -6 -9 326.27 11.7 -2 -6 9 310.07 9.7 2 6 -9 302.37 9.6 -2 6 9 316.77 10.5 -2 6 9 292.17 11.3 2 6 -9 289.37 12.9 2 6 -9 305.67 9.9 -2 6 9 303.17 11.2 -1 -6 9 728.63 19.3 -1 -6 9 714.53 21.3 -1 -6 9 753.32 20.4 -1 -6 9 704.73 19.4 1 -6 -9 730.23 20.6 -1 -6 9 764.22 19 1 -6 -9 752.02 20.9 -1 6 9 745.03 21.1 1 6 -9 735.63 19.7 -1 6 9 761.32 20.7 -1 6 9 732.43 21.1 1 6 -9 740.43 22.3 1 6 -9 739.93 17.8 1 6 -9 733.53 18.8 -1 6 9 745.23 20.3 0 -6 9 258.57 9.9 0 -6 9 248.28 10.7 0 -6 -9 268.57 10.3 0 -6 9 251.77 9.2 0 -6 9 264.57 9.9 0 -6 9 262.07 10.3 0 -6 -9 258.07 9.9 0 6 -9 261.57 10.1 0 6 9 269.77 10.5 0 6 -9 267.37 9 0 6 9 248.08 10.4 0 6 9 258.07 10.1 0 6 -9 257.57 11 0 6 9 256.67 9.4 0 6 -9 261.87 7.5 1 -6 9 77.49 6.2 1 -6 9 72.79 5.4 1 -6 9 78.59 5.8 1 -6 9 73.79 5.7 -1 -6 -9 70.09 5.5 1 -6 9 64.49 5 -1 -6 -9 71.59 5.4 1 6 9 72.89 5.4 1 6 9 72.19 5.7 -1 6 -9 65.49 6 1 6 9 66.79 3.4 -1 6 -9 73.29 5.9 -1 6 -9 74.99 5.7 1 6 9 67.59 5.5 2 -6 9 1262.67 32.5 -2 -6 -9 1200.48 30.9 2 -6 9 1230.18 32.5 -2 -6 -9 1261.97 31.5 2 -6 9 1294.37 32.6 -2 6 -9 1222.28 28 2 6 9 1284.87 33.2 2 6 9 1279.47 32.6 -2 6 -9 1271.27 32.9 2 6 9 1232.28 31.1 -2 6 -9 1238.68 32.3 -2 6 -9 1273.87 31.1 -3 -6 -9 376.46 15.2 -3 -6 -9 394.76 13.7 -3 -6 -9 414.76 14.4 3 -6 9 409.06 15.2 3 -6 9 403.96 14.5 3 -6 9 392.56 15 -3 6 -9 381.66 11.3 3 6 9 394.66 13.6 -3 6 -9 411.46 14.3 3 6 9 408.76 14.6 -3 6 -9 389.56 15.2 3 6 9 429.76 15.7 -3 6 -9 396.96 14.7 -4 -6 -9 476.15 15.8 -4 -6 -9 508.05 17 4 -6 9 465.35 17.5 4 -6 9 454.65 16.1 4 -6 9 504.35 17.9 -4 6 -9 442.46 13.6 -4 6 -9 503.05 17.1 -4 6 -9 483.65 17.9 4 6 9 474.85 16.6 4 6 9 495.45 18 4 6 9 482.85 15.8 -4 6 -9 460.35 16.7 5 -6 9 -2.3 3.3 -5 -6 -9 -1.4 3.5 -5 -6 -9 0.2 2.4 5 -6 9 -0.8 3.5 5 -6 9 6.4 3 -5 6 -9 6.2 4.2 5 6 9 -0.5 3.4 -5 6 -9 4.6 3.5 -5 6 -9 -5.1 3.9 5 6 9 0.8 2.9 5 6 9 2 3.2 -6 -6 -9 21 5.1 6 -6 9 26.9 4.4 -6 -6 -9 32.7 4.9 6 -6 9 31.9 6.4 6 -6 9 26.5 5.8 6 6 9 29.9 5.9 6 6 9 27.7 4.8 -6 6 -9 23.3 5.6 6 6 9 24.5 4.7 -6 6 -9 22.8 5.6 -7 -6 -9 167.78 11.8 -7 -6 -9 183.98 9.6 7 -6 9 184.68 9.3 7 -6 9 173.38 11.5 7 -6 9 183.88 12.1 -7 6 -9 179.58 12 -7 6 -9 195.48 12.5 7 6 9 186.08 9.7 7 6 9 176.08 11.8 -8 -6 -9 50.59 8.2 8 -6 9 44.9 8.1 8 -6 9 44.3 7.7 -8 -6 -9 47.1 6.1 8 -6 9 50.39 5.4 -8 6 -9 43.1 7.7 -8 6 -9 43.4 7.8 8 6 9 40.8 7.2 8 6 9 45.9 6.2 -9 -6 -9 12.9 6.4 9 -6 9 29.2 6.8 9 -6 9 30.1 6.4 -9 -6 -9 26.8 4.6 -9 6 -9 18.5 6.8 -9 6 -9 22 6.3 9 6 9 18 5.5 -10 -6 -9 7.2 10.7 -10 -6 -9 13.8 4.3 10 -6 9 20.7 5.9 10 -6 9 13.6 5.8 10 6 9 19.3 6.4 11 -7 -9 6.9 5.1 -11 -7 9 3.6 4.6 11 -7 -9 2 4 11 7 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53.89 8.9 -8 6 -12 63.19 8.8 8 6 12 58.59 9.1 -8 6 -12 49.1 7.7 8 6 12 69.79 8.2 -8 6 -12 53.99 8.9 9 -6 12 13.3 5.9 -9 6 -12 4.6 5 11 -7 -12 102.19 10.7 11 -7 -12 122.49 11.6 -11 -7 12 108.29 11.7 -11 7 12 90.89 14.7 11 7 -12 117.69 10.8 -11 7 12 90.69 9.4 10 -7 -12 122.19 10.8 10 -7 -12 127.09 10.5 -10 -7 12 134.29 11.7 -10 -7 12 106.09 7.6 10 7 -12 124.79 10.6 -10 7 12 119.69 10.1 -10 7 12 117.99 13.1 -9 -7 12 143.59 11.6 9 -7 -12 139.49 10.4 -9 -7 12 129.39 6.5 9 -7 -12 146.09 10.8 -9 -7 12 138.79 8.5 9 7 -12 127.89 13.8 9 7 -12 137.99 10.4 -9 7 12 125.69 12.7 -9 7 12 134.59 10.1 -8 -7 12 84.39 8.8 8 -7 -12 73.79 7.8 -8 -7 12 73.09 5.2 -8 -7 12 76.19 6.8 8 -7 -12 91.59 8.3 -8 7 12 62.99 9.7 8 7 -12 87.49 13.4 8 7 -12 72.69 7.5 -8 7 12 71.49 7.4 -7 -7 12 48.7 6.9 -7 -7 12 43.5 4.3 7 -7 -12 46.6 6.8 -7 -7 12 47.5 6 7 -7 -12 49.3 7 7 7 -12 57.59 10.6 -7 7 12 42.7 6.2 7 7 -12 45 6.3 6 -7 -12 330.67 9.4 -6 -7 12 338.77 13.9 6 -7 -12 335.37 9.6 6 -7 -12 347.07 14.8 -6 -7 12 339.77 11.8 6 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12 45.5 5.9 -2 7 12 34.6 4.8 2 7 -12 33.4 3.8 -1 -7 12 1224.18 31.3 -1 -7 12 1216.38 32.2 -1 -7 12 1212.88 33.5 1 -7 -12 1256.27 32.9 -1 -7 12 1275.97 31 1 -7 -12 1259.47 33.1 -1 7 12 1208.78 32.3 1 7 -12 1230.08 31.5 -1 7 12 1197.38 32.9 1 7 -12 1232.68 30.5 -1 7 12 1179.78 31.9 1 7 -12 1218.48 35.1 1 7 -12 1245.88 28.8 -1 7 12 1253.37 32.4 0 -7 12 60.59 5.8 0 -7 12 56.29 6.4 0 -7 12 64.89 5.8 0 -7 -12 57.49 6.3 0 -7 -12 53.69 6.1 0 -7 12 58.79 6.2 0 7 -12 55.89 6 0 7 12 54.29 6.2 0 7 -12 53.89 6.4 0 7 12 45.4 6 0 7 12 64.89 6.4 0 7 -12 59.29 5.3 0 7 12 52.09 4.5 0 7 -12 56.59 3.7 1 -7 12 1171.28 31.4 -1 -7 -12 1177.28 30.6 1 -7 12 1160.88 32.6 -1 -7 -12 1140.49 31.3 1 -7 12 1197.48 32.5 -1 7 -12 1128.79 32.8 1 7 12 1166.98 32.4 1 7 12 1184.88 31.3 -1 7 -12 1139.89 26.6 1 7 12 1182.68 32.6 -1 7 -12 1201.48 32.1 -1 7 -12 1187.18 29.7 2 -7 12 424.06 16.3 -2 -7 -12 420.16 15.2 -2 -7 -12 417.46 15.6 2 -7 12 442.26 16.9 2 -7 12 428.66 16.8 2 7 12 446.56 16.9 -2 7 -12 448.26 17 -2 7 -12 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5.6 -9 -1 14 56.19 4.3 -9 1 14 50.09 9.3 -9 1 14 48.3 4.8 -9 1 14 49.99 5.1 9 1 -14 56.69 8.6 9 1 -14 42.9 4.8 8 -1 -14 150.88 10.3 -8 -1 14 143.39 6.4 -8 -1 14 152.48 7.9 -8 -1 14 154.68 6.9 8 -1 -14 147.39 8.2 -8 1 14 135.59 6.7 -8 1 14 139.49 7.1 -8 1 14 143.09 7.8 8 1 -14 147.79 7.4 -8 1 14 139.19 7.5 8 1 -14 159.68 10.8 7 -1 -14 46.2 5 7 -1 -14 52.89 6.9 -7 -1 14 51.69 5.4 -7 -1 14 59.29 4.2 -7 -1 14 49.7 4.4 -7 1 14 53.99 4.6 -7 1 14 61.89 5.5 7 1 -14 49.6 4.7 7 1 -14 64.29 6.7 -7 1 14 60.39 5.3 6 -1 -14 4.1 2.7 6 -1 -14 6.5 3.8 -6 -1 14 6.3 3.2 -6 -1 14 6.6 2.4 -6 -1 14 2.8 2 6 1 -14 4.8 2.2 6 1 -14 5.2 3.3 -6 1 14 7.2 2.9 6 1 -14 3.3 5 -6 1 14 5.7 2.5 -6 1 14 -0.4 2.5 -5 -1 14 27 3.6 -5 -1 14 36.2 4.3 5 -1 -14 32.6 4.5 -5 -1 14 36 4.9 -5 -1 14 31.9 2.5 5 -1 -14 33.9 5.3 -5 1 14 32.1 4.7 5 1 -14 28.6 5 5 1 -14 33.9 2.2 5 1 -14 35.8 4.3 -5 1 14 25.7 4.1 -5 1 14 39.5 4.7 5 1 -14 33.2 7.8 4 -1 -14 1929.21 42.9 -4 -1 14 1969.9 45.8 -4 -1 14 1998.4 43.7 4 -1 -14 1969.5 47.7 -4 -1 14 2020.9 45.7 4 -1 -14 2010.2 53.19 -4 -1 14 2033.5 47.8 4 -1 -14 2002.6 46.5 4 1 -14 2013.5 45.8 4 1 -14 1923.61 43.1 -4 1 14 1951.2 46.1 -4 1 14 2024.7 46.6 4 1 -14 2004.9 47.7 -4 1 14 2046.7 47.8 4 1 -14 1939.81 53.09 -3 -1 14 826.22 21 -3 -1 14 817.62 22 3 -1 -14 831.32 27.2 3 -1 -14 820.82 20.5 -3 -1 14 801.42 22.3 3 -1 -14 859.21 23.2 -3 -1 14 827.72 23.9 3 -1 -14 832.82 22.7 -3 1 14 821.82 20.6 -3 1 14 831.12 23.7 3 1 -14 798.82 27 3 1 -14 819.82 22.2 -3 1 14 850.71 22.7 3 1 -14 848.52 23 -3 1 14 811.52 22.5 3 1 -14 787.22 20.4 -2 -1 14 6.5 2.7 2 -1 -14 2.5 3 -2 -1 14 4 2.3 -2 -1 14 5.5 2.6 2 -1 -14 7.7 2.3 2 -1 -14 9 2.9 -2 -1 14 4.3 3.2 2 -1 -14 11.2 4.4 -2 1 14 5 2.4 -2 1 14 5.7 3.2 2 1 -14 8 2.8 2 1 -14 0.6 2.8 2 1 -14 6.7 2.9 2 1 -14 3.8 3.5 -2 1 14 11.8 3 1 -1 -14 1080.29 30.6 -1 -1 14 1075.89 29.5 1 -1 -14 1021 28.2 1 -1 -14 1037.1 29 -1 -1 14 1133.99 28.3 -1 -1 14 1125.59 28.2 -1 1 14 1090.39 27.8 1 1 -14 1101.49 29.1 1 1 -14 1125.99 31.5 -1 1 14 1109.39 29.6 1 1 -14 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4 -1 5 14 22.2 4 1 5 -14 25.7 4.3 1 5 -14 13.5 5.6 0 -5 -14 24.1 5.2 0 -5 -14 25.7 4.9 0 -5 14 25.6 4.8 0 -5 14 19.9 4.8 0 -5 14 23.2 4.6 0 5 -14 19.2 5.6 0 5 14 22.6 4.8 0 5 14 25.1 3.3 0 5 14 24.4 5.4 0 5 -14 35.1 5.4 0 5 -14 20.2 4.1 -1 -5 -14 529.15 18.3 -1 -5 -14 535.65 18.2 1 -5 14 563.14 19.6 1 -5 14 533.65 18.1 1 -5 14 532.45 18.9 1 5 14 572.34 19.5 -1 5 -14 545.15 18.7 -1 5 -14 551.84 17.7 -1 5 -14 566.54 19.9 1 5 14 559.14 18.4 1 5 14 529.95 13 2 -5 14 483.65 18.2 2 -5 14 521.25 18.8 -2 -5 -14 516.65 18 2 -5 14 513.45 18.1 -2 -5 -14 506.35 17.9 -2 5 -14 509.15 17.8 2 5 14 526.15 18.8 -2 5 -14 513.05 18.7 -2 5 -14 524.95 18.7 2 5 14 509.35 17.9 -3 -5 -14 77.99 8.1 3 -5 14 73.59 7.5 3 -5 14 91.89 8.1 -3 -5 -14 75.49 7.3 3 -5 14 77.09 7.6 3 5 14 88.39 7.8 3 5 14 77.79 8 3 5 14 83.59 7.8 -3 5 -14 73.99 7.4 -3 5 -14 86.19 8.1 -3 5 -14 82.69 8.5 4 -5 14 19.9 5 4 -5 14 18.3 5.1 -4 -5 -14 11.3 3.9 -4 -5 -14 16.6 5.5 4 -5 14 14.3 5 4 5 14 12.3 5.1 -4 5 -14 18.9 5.8 -4 5 -14 21.6 5.9 4 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3.1 4.7 -8 7 14 9.6 4.2 8 7 -14 13.9 7.4 -7 -7 14 143.39 10.7 7 -7 -14 172.58 11 -7 -7 14 159.08 9.9 -7 -7 14 156.68 7.5 7 -7 -14 149.88 10.5 -7 7 14 169.78 10.6 7 7 -14 152.78 14 -7 7 14 151.38 8.9 7 7 -14 154.28 9.8 6 -7 -14 32.7 2.6 6 -7 -14 34.3 2.9 -6 -7 14 33.6 4.5 -6 -7 14 29.1 5.5 6 -7 -14 30.4 5.6 6 -7 -14 29.8 5.6 6 7 -14 33.4 5.4 -6 7 14 34.4 3.4 -6 7 14 30.1 4.8 -6 7 14 40.6 6.4 6 7 -14 34 2.9 6 7 -14 31.3 8.3 -5 -7 14 196.68 6.6 5 -7 -14 212.18 10.9 -5 -7 14 183.08 6.3 5 -7 -14 205.08 7.1 -5 -7 14 180.48 8.9 -5 -7 14 200.78 11.2 5 -7 -14 199.48 11.2 5 -7 -14 207.88 7.7 5 7 -14 193.28 7.3 5 7 -14 205.58 10.2 5 7 -14 193.48 14.3 -5 7 14 194.38 8.3 -5 7 14 211.88 10.7 -5 7 14 199.08 11 -4 -7 14 297.37 13.8 4 -7 -14 302.87 10.1 -4 -7 14 311.17 10.2 -4 -7 14 305.27 12 4 -7 -14 307.47 13.8 4 -7 -14 321.27 13.2 -4 -7 14 302.57 9.8 4 7 -14 325.67 12.3 -4 7 14 300.47 11.5 4 7 -14 287.97 16.8 4 7 -14 300.37 10.4 -4 7 14 295.27 13.4 -4 7 14 329.27 13.6 3 -7 -14 170.88 10.2 -3 -7 14 190.28 8.2 -3 -7 14 190.18 7.9 -3 -7 14 183.88 10.8 -3 -7 14 182.48 9.2 3 7 -14 192.08 8.7 -3 7 14 177.28 10.1 3 7 -14 170.58 12.6 -3 7 14 198.18 10.5 -3 7 14 180.88 8.9 3 7 -14 179.48 8.1 -2 -7 14 274.97 11.1 -2 -7 14 300.67 12.3 2 -7 -14 272.37 12.7 -2 -7 14 256.27 13.2 -2 -7 14 280.87 10.7 -2 7 14 278.87 12.7 2 7 -14 264.17 14.8 2 7 -14 283.17 11.1 2 7 -14 287.17 10.4 -2 7 14 283.97 12.1 -2 7 14 282.17 12.9 -1 -7 14 46 5.2 1 -7 -14 43.6 5.9 -1 -7 14 36.3 6.4 1 -7 -14 59.09 7.4 -1 -7 14 38.4 5.6 -1 -7 14 40 5.2 1 7 -14 44.6 4.1 -1 7 14 38.2 5.8 1 7 -14 45.4 7.4 1 7 -14 49.1 5.8 -1 7 14 46.1 5.9 -1 7 14 47.8 5.2 1 7 -14 38.3 5 -1 7 14 48.9 6.7 0 -7 -14 85.09 7.5 0 -7 -14 72.59 7 0 -7 14 85.59 8.1 0 -7 14 81.39 6.8 0 -7 14 91.19 7.2 0 7 14 99.39 8.1 0 7 14 86.99 5.1 0 7 -14 83.89 8.3 0 7 14 78.39 7.3 0 7 14 86.19 7.5 0 7 -14 75.39 6.5 0 7 -14 92.19 7.5 0 7 -14 81.99 4.9 -1 -7 -14 594.54 19.7 1 -7 14 563.34 20.9 -1 -7 -14 618.14 20.5 1 -7 14 595.24 20 1 -7 14 611.34 20.8 1 7 14 588.94 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112.49 9.2 -6 7 -14 98.89 9.2 6 7 14 97.59 8.9 6 7 14 98.59 9.2 -6 7 -14 88.59 11.3 6 7 14 77.69 10.4 -6 7 -14 86.29 10.9 7 -7 14 49.5 7.1 -7 -7 -14 68.89 8.1 7 -7 14 51.29 9 -7 -7 -14 40.1 8.3 7 -7 14 71.69 9.7 7 7 14 60.19 9.1 -7 7 -14 75.79 8.7 7 7 14 75.09 8.7 -7 7 -14 57.99 9 -7 7 -14 41.4 8.8 7 7 14 65.79 8.5 -10 -8 14 23.3 5.4 -10 -8 14 20.3 6.5 10 -8 -14 22.7 6.4 -10 8 14 21.9 5.9 10 8 -14 21.1 6 10 8 -14 25.9 9.9 -10 8 14 23.1 8.2 9 -8 -14 -4.5 4.1 -9 -8 14 0.8 3.8 -9 -8 14 4.3 3.2 9 -8 -14 -9.1 3.4 -9 8 14 1.3 5.6 -9 8 14 1 4.1 9 8 -14 9.4 7.7 9 8 -14 2 3.7 -8 -8 14 47.6 4.9 8 -8 -14 56.69 8.1 8 -8 -14 50.29 8 -8 -8 14 48.7 6.6 -8 -8 14 37.8 7 8 8 -14 47.3 7.1 -8 8 14 58.19 8.3 -8 8 14 42.9 8.6 8 8 -14 51.79 11.1 7 -8 -14 66.99 8.3 -7 -8 14 57.19 7.3 -7 -8 14 65.19 6.9 7 -8 -14 50.79 7.7 -7 -8 14 53.09 5.3 7 8 -14 75.69 12.6 -7 8 14 57.49 7.6 7 8 -14 67.89 7.2 -7 8 14 67.19 6.4 6 -8 -14 1.1 3.7 -6 -8 14 2.9 3.6 6 -8 -14 2 1.7 -6 -8 14 7.6 3 6 -8 -14 -2.1 2.4 6 8 -14 -2.8 1.3 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8.9 -5 1 25 83.59 9.7 5 1 -25 105.29 10.3 -5 1 25 80.59 10.7 -4 -1 25 51.09 7.4 4 -1 -25 41.5 7.5 4 -1 -25 39.7 7.9 -4 -1 25 49.4 8.5 4 1 -25 48.9 10.8 -4 1 25 41.2 7.7 -4 1 25 38.4 6.8 4 1 -25 43.8 7.5 4 1 -25 41.8 7.5 3 -1 -25 4.8 4.9 3 -1 -25 0.5 4.2 -3 -1 25 -0.2 4.5 -3 -1 25 1.4 4.3 -3 -1 25 -1.9 3 3 1 -25 -5.8 4.3 -3 1 25 1.7 4.3 -3 1 25 3.5 5.2 3 1 -25 -0.9 3.9 3 1 -25 2.4 5.8 2 -1 -25 22.8 6.3 -2 -1 25 16.8 6.5 2 -1 -25 24.7 6.6 -2 -1 25 23.3 5.3 -2 -1 25 20.1 6.4 2 1 -25 22.8 6.1 2 1 -25 17.8 6.6 -2 1 25 25.7 10 -2 1 25 16.6 7.1 2 1 -25 22.9 7.3 1 -1 -25 87.09 9.9 1 -1 -25 81.89 9.2 -1 -1 25 97.79 9.3 1 1 -25 145.59 18.5 1 1 -25 94.69 10.3 1 1 -25 84.89 8.9 1 1 -25 109.59 10.1 0 -1 25 142.69 11.3 0 -1 -25 153.38 12.5 0 1 -25 141.69 11.9 -6 -2 25 21 5 6 -2 -25 -2.3 8.5 -6 -2 25 14.5 5.8 6 2 -25 16.3 5.7 -6 2 25 16.5 5.6 -5 -2 25 -1.3 4.5 -5 -2 25 7.6 4 5 -2 -25 -3.5 5.1 5 2 -25 1.1 4.3 5 2 -25 3 5.9 -5 2 25 3.4 5.3 -4 -2 25 11.1 5.5 4 -2 -25 13.7 5.4 -4 -2 25 11 4.7 4 -2 -25 5.3 5.3 4 2 -25 14.7 5.3 -4 2 25 8 8.3 4 2 -25 -6.6 4.4 -4 2 25 2.8 4.9 4 2 -25 22.6 8.4 -3 -2 25 9.4 4.6 3 -2 -25 1.4 4.2 -3 -2 25 4.5 3.5 -3 -2 25 5.8 5.7 3 -2 -25 3.3 4.7 3 2 -25 6.4 6.3 3 2 -25 4 4.4 -3 2 25 7.7 5 3 2 -25 2.9 4.3 2 -2 -25 42.1 7.5 -2 -2 25 35.2 9 2 -2 -25 39 7.5 -2 -2 25 41.2 6.7 2 2 -25 34.8 6.5 2 2 -25 55.79 11.3 2 2 -25 28.2 6.6 1 -2 -25 21.3 6.9 -1 -2 25 20.6 5.7 1 2 -25 41.2 9.9 1 2 -25 24.9 7.2 1 2 -25 23.2 5.9 1 2 -25 23.4 6.5 0 -2 25 42 7.9 0 -2 -25 38.4 8.5 0 2 -25 31.4 6.8 0 2 -25 36.9 7.1 6 -3 -25 19.9 7 -6 -3 25 23 4.9 6 3 -25 21.5 6.5 -6 3 25 10.4 5.6 -5 -3 25 146.79 13.9 5 -3 -25 146.19 12.1 -5 -3 25 170.88 10.7 -5 3 25 159.38 12.6 5 3 -25 177.18 16.4 5 3 -25 162.98 11.9 -4 -3 25 154.28 10.7 4 -3 -25 167.38 12.4 -4 -3 25 202.48 21.5 -4 3 25 169.18 14.6 4 3 -25 166.78 11.7 4 3 -25 163.18 15 3 -3 -25 2 4.4 3 -3 -25 -5.7 3.9 -3 -3 25 2.4 3.4 -3 -3 25 0.7 3.7 -3 3 25 4.1 7.9 3 3 -25 -4.6 4 3 3 -25 2.5 4.3 3 3 -25 7.7 7.2 2 -3 -25 13.1 5.7 2 -3 -25 9.5 5.8 -2 -3 25 9.7 4.8 2 3 -25 15.6 5.4 2 3 -25 11.5 5.9 2 3 -25 21.4 7.2 -1 -3 25 63.99 8.6 1 -3 -25 80.79 10.4 1 3 -25 118.39 12.4 1 3 -25 100.89 11.7 1 3 -25 81.29 8.8 1 3 -25 73.39 9.9 0 -3 25 147.59 11.7 0 -3 -25 153.18 12.7 0 3 -25 158.88 12.4 0 3 -25 112.69 9.9 0 3 -25 150.78 12.3 5 -4 -25 -8.9 4.4 -5 -4 25 -1 2.9 5 4 -25 4.2 5.1 5 4 -25 5.8 6.5 -4 -4 25 30.5 6.3 4 -4 -25 35.5 7.6 -4 -4 25 39 8.3 4 4 -25 51.19 11.2 4 4 -25 35.2 6.9 3 -4 -25 14.3 6.2 -3 -4 25 15.8 4.5 -3 -4 25 9.3 5.7 3 4 -25 13.2 5.3 3 4 -25 17.6 5.9 3 4 -25 26.1 8.5 2 -4 -25 40.2 8.3 -2 -4 25 45.8 7.2 2 4 -25 33.7 7.3 2 4 -25 66.59 11.5 2 4 -25 42.8 6.8 1 -4 -25 5.8 5 -1 -4 25 9.1 4.9 1 4 -25 8.3 5.6 1 4 -25 -0.9 3.9 1 4 -25 20 7.6 1 4 -25 10.4 6.2 4 -5 -25 62.09 9.1 -4 -5 25 64.89 7.7 -4 -5 25 69.19 11.5 4 5 -25 81.79 14 4 5 -25 82.59 9 -3 -5 25 7.8 4.2 3 -5 -25 -6.8 4.3 3 5 -25 9.8 6.3 3 5 -25 3.9 4.5 2 -5 -25 54.59 9.1 -2 -5 25 42.5 7.2 2 5 -25 45.1 10.4 2 5 -25 40.6 7.9 2 5 -25 47.8 7.2 4 0 -26 -2.7 4.6 3 0 -26 158.38 16.9 3 0 -26 174.68 12.6 2 0 -26 17.7 6 2 0 -26 22.3 6.8 4 -1 -26 9.3 5.1 4 1 -26 23.4 7.3 4 1 -26 15.7 6.1 3 -1 -26 -2.9 4.3 3 1 -26 11.6 6.2 3 1 -26 -9.5 3.9 3 1 -26 3.5 4.1 2 -1 -26 7.6 5.2 -2 -1 26 4.8 4 2 1 -26 8.6 5.6 2 1 -26 0.1 4.5 2 1 -26 1.8 4 4 -2 -26 8 5.6 4 2 -26 11 5 3 -2 -26 47 8.3 -3 -2 26 54.29 7.2 3 2 -26 64.99 12 3 2 -26 38 7.1 3 2 -26 57.49 8.4 _iucr_refine_instructions_details ; mono_p_a.res created by SHELXL-2014/7 TITL Mono_p_a.res in P2(1)/c CELL 0.71073 9.024 13.3762 18.3115 90 103.731 90 ZERR 4 0.0009 0.0013 0.002 0 0.003 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H Cl N O S UNIT 84 92 4 8 16 4 L.S. 10 PLAN -5 0 0 SIZE 0.2 0.25 0.28 TEMP 0 HTAB BOND $H CONF CONF HTAB fmap 2 acta OMIT -2 50 OMIT 6 0 0 OMIT 1 6 2 OMIT -3 4 6 OMIT 3 3 5 REM REM REM WGHT 0.048200 1.063000 FVAR 1.40736 CL1 3 0.786371 0.910558 0.433171 11.00000 0.08146 0.06966 = 0.07324 0.02920 0.01846 -0.00460 S2 6 0.593512 0.456923 0.721332 11.00000 0.03901 0.06923 = 0.03410 -0.00634 0.01180 -0.00795 O1 5 0.848125 0.528608 0.559415 11.00000 0.05282 0.04288 = 0.05991 -0.00495 0.03175 -0.00637 O2 5 0.957360 0.509801 0.722697 11.00000 0.04560 0.07528 = 0.07432 0.03276 0.00720 0.00339 O4 5 0.664326 0.537561 0.767705 11.00000 0.05823 0.09933 = 0.04345 -0.02446 0.01178 -0.02271 N1 4 0.965541 0.681261 0.712916 11.00000 0.04136 0.06752 = 0.03859 -0.00128 0.00299 -0.00255 N2 4 0.613935 0.478799 0.634387 11.00000 0.03613 0.04482 = 0.03842 -0.00449 0.01485 -0.00203 O3 5 0.640996 0.356893 0.740032 11.00000 0.07410 0.07651 = 0.05043 0.01564 0.02116 0.00457 C2 1 0.924815 0.897177 0.581531 11.00000 0.05287 0.03998 = 0.07474 -0.00595 0.02130 -0.00513 AFIX 43 H2 2 0.952251 0.963647 0.577720 11.00000 -1.20000 AFIX 0 C3 1 0.972101 0.847578 0.649476 11.00000 0.04744 0.05293 = 0.06035 -0.02175 0.01131 -0.00674 AFIX 43 H3 2 1.031980 0.879414 0.691364 11.00000 -1.20000 AFIX 0 C4 1 0.927579 0.749644 0.652977 11.00000 0.03618 0.05058 = 0.04075 -0.00685 0.00930 0.00099 C5 1 0.837840 0.701967 0.590478 11.00000 0.03645 0.04134 = 0.04002 -0.00355 0.00887 -0.00238 C7 1 0.809111 0.596988 0.611381 11.00000 0.03757 0.04176 = 0.04001 -0.00082 0.01026 -0.00110 C16 1 0.786277 0.433973 0.556160 11.00000 0.04112 0.04134 = 0.04445 -0.00066 0.01653 -0.00006 C15 1 0.841184 0.366459 0.511938 11.00000 0.05943 0.05370 = 0.06486 -0.00540 0.03571 0.00066 AFIX 43 H15 2 0.917209 0.385906 0.488381 11.00000 -1.20000 AFIX 0 C14 1 0.784621 0.271146 0.502495 11.00000 0.06422 0.05228 = 0.06710 -0.01247 0.02933 0.00616 AFIX 43 H14 2 0.822511 0.226617 0.472396 11.00000 -1.20000 AFIX 0 C13 1 0.671688 0.240053 0.537148 11.00000 0.05054 0.04258 = 0.05412 -0.00353 0.00977 0.00162 C17 1 0.609966 0.134715 0.527288 11.00000 0.07993 0.04979 = 0.09718 -0.01474 0.02514 -0.00760 AFIX 137 H17A 2 0.544389 0.123643 0.560819 11.00000 -1.50000 H17B 2 0.693149 0.088076 0.538436 11.00000 -1.50000 H17C 2 0.553120 0.125461 0.476341 11.00000 -1.50000 AFIX 0 C9 1 1.061709 0.704365 0.786987 11.00000 0.06000 0.10628 = 0.04141 -0.00824 -0.00356 -0.00167 AFIX 137 H9A 2 1.076038 0.645108 0.817433 11.00000 -1.50000 H9B 2 1.013425 0.754887 0.810532 11.00000 -1.50000 H9C 2 1.158929 0.728300 0.781724 11.00000 -1.50000 AFIX 0 C8 1 0.918424 0.587271 0.689808 11.00000 0.03016 0.06164 = 0.04807 0.01128 0.01055 0.00172 C1 1 0.837969 0.849322 0.519809 11.00000 0.05005 0.04598 = 0.05661 0.00698 0.01638 -0.00102 C6 1 0.791965 0.751079 0.523444 11.00000 0.04604 0.04788 = 0.04151 -0.00215 0.00677 -0.00506 AFIX 43 H6 2 0.731693 0.719466 0.481557 11.00000 -1.20000 AFIX 0 C10 1 0.642474 0.581606 0.614542 11.00000 0.03537 0.04395 = 0.04065 -0.00414 0.00811 0.00188 AFIX 23 H10A 2 0.617974 0.626782 0.651419 11.00000 -1.20000 H10B 2 0.576425 0.597678 0.565969 11.00000 -1.20000 AFIX 0 C11 1 0.672857 0.405546 0.591858 11.00000 0.03347 0.04373 = 0.03332 -0.00087 0.00848 0.00179 C12 1 0.617012 0.308318 0.581223 11.00000 0.03656 0.04639 = 0.04206 0.00135 0.00891 -0.00330 AFIX 43 H12 2 0.540607 0.288577 0.604434 11.00000 -1.20000 AFIX 0 C18 1 0.389808 0.467908 0.715558 11.00000 0.04227 0.09706 = 0.05821 -0.02315 0.02703 -0.01678 C20 1 0.373638 0.445481 0.795059 11.00000 0.09393 0.16615 = 0.08308 -0.01614 0.06282 -0.02605 AFIX 137 H20A 2 0.267806 0.447562 0.796070 11.00000 -1.50000 H20B 2 0.428915 0.494547 0.829159 11.00000 -1.50000 H20C 2 0.414028 0.380234 0.809932 11.00000 -1.50000 AFIX 0 C21 1 0.302970 0.393974 0.659202 11.00000 0.04922 0.13651 = 0.11506 -0.05609 0.03155 -0.03408 AFIX 137 H21A 2 0.195754 0.400317 0.656285 11.00000 -1.50000 H21B 2 0.335649 0.327361 0.674686 11.00000 -1.50000 H21C 2 0.322214 0.407169 0.610751 11.00000 -1.50000 AFIX 0 C19 1 0.339661 0.574363 0.692484 11.00000 0.05257 0.11096 = 0.12003 -0.01607 0.03755 0.01327 AFIX 137 H19A 2 0.351578 0.586819 0.642563 11.00000 -1.50000 H19B 2 0.401276 0.620637 0.726818 11.00000 -1.50000 H19C 2 0.234526 0.582726 0.693527 11.00000 -1.50000 AFIX 0 HKLF 4 REM Mono_p_a.res in P2(1)/c REM R1 = 0.0405 for 3518 Fo > 4sig(Fo) and 0.0421 for all 3705 data REM 267 parameters refined using 0 restraints END WGHT 0.0482 1.0630 REM Instructions for potential hydrogen bonds EQIV $1 -x+2, -y+2, -z+1 HTAB C2 Cl1_$1 EQIV $2 -x+2, y+1/2, -z+3/2 HTAB C3 O2_$2 HTAB C9 O3_$2 REM Highest difference peak 0.396, deepest hole -0.415, 1-sigma level 0.033 Q1 1 0.8316 0.9297 0.4776 11.00000 0.05 0.40 Q2 1 0.8639 0.5943 0.6497 11.00000 0.05 0.22 Q3 1 0.4854 0.4661 0.7169 11.00000 0.05 0.21 Q4 1 0.7331 0.5844 0.6125 11.00000 0.05 0.21 Q5 1 0.6548 0.0986 0.4843 11.00000 0.05 0.19 REM The information below was added by Olex2. REM REM R1 = 0.0405 for 3518 Fo > 4sig(Fo) and 0.0421 for all 69742 data REM n/a parameters refined using n/a restraints REM Highest difference peak 0.40, deepest hole -0.41 REM Mean Shift 0, Max Shift 0.001. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0421 REM R1_gt = 0.0405 REM wR_ref = 0.1057 REM GOOF = 1.037 REM Shift_max = 0.001 REM Shift_mean = 0 REM Reflections_all = 69742 REM Reflections_gt = 3518 REM Parameters = n/a REM Hole = -0.41 REM Peak = 0.40 REM Flack = n/a ; _olex2_submission_special_instructions 'No special instructions were received'