data_UMEX406_2 _publ_contact_author_name ; Yasuhide Inokuma ; _publ_contact_author_address ; Division of Applied Chemistry, Faculty of Engineering, Hokkaido University, Kita 13 Nishi 8 Kita-ku, Sapporo, Hokkaido 060-8628, (Japan). Institute for Chemical Reaction Design and Discovery(WPI-ICRD), Hokkaido University, Kita 21, Nishi 10, Kita-ku, Sapporo 001-0021, (Japan) ; _publ_contact_author_email 'inokuma@eng.hokudai.ac.jp' _publ_contact_author_fax +81-11-706-6557 _publ_contact_author_phone +81-11-706-6556 _publ_requested_journal 'The Journal of Organic Chemistry' _publ_section_title ; Two-Step Transformation of Aliphatic Polyketones into Highly Pi-Conjugated Polyimines ; loop_ _publ_author_name _publ_author_address 'Yumehiro Manabe' ; Division of Applied Chemistry, Faculty of Engineering, Hokkaido University, Kita 13 Nishi 8 Kita-ku, Sapporo, Hokkaido 060-8628, (Japan). ; 'Mitsuharu Uesaka' ; Division of Applied Chemistry, Faculty of Engineering, Hokkaido University, Kita 13 Nishi 8 Kita-ku, Sapporo, Hokkaido 060-8628, (Japan). ; 'Tomoki Yoneda' ; Division of Applied Chemistry, Faculty of Engineering, Hokkaido University, Kita 13 Nishi 8 Kita-ku, Sapporo, Hokkaido 060-8628, (Japan). ; 'Yasuhide Inokuma ' ; Division of Applied Chemistry, Faculty of Engineering, Hokkaido University, Kita 13 Nishi 8 Kita-ku, Sapporo, Hokkaido 060-8628, (Japan). Institute for Chemical Reaction Design and Discovery(WPI-ICRD), Hokkaido University, Kita 21, Nishi 10, Kita-ku, Sapporo 001-0021, (Japan) ; _publ_section_abstract ; ; _publ_section_references ; Sheldrick, G. M. (2008). Acta Cryst. A64, 112-122. SHELXT Version 2018/2 Sheldrick, G.M. (2015) SHELXL Version 2018/3, Acta Cryst. C71, 3-8. ; _audit_creation_method 'SHELXL-2018/3' _shelx_SHELXL_version_number '2018/3' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C14 H20 N4' _chemical_formula_sum 'C14 H20 N4' _chemical_formula_weight 244.34 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/n' _space_group_name_Hall '-P 2yn' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 6.1286(4) _cell_length_b 12.4667(8) _cell_length_c 9.5271(8) _cell_angle_alpha 90 _cell_angle_beta 104.044(8) _cell_angle_gamma 90 _cell_volume 706.15(9) _cell_formula_units_Z 2 _cell_measurement_temperature 123(2) _cell_measurement_reflns_used 2413 _cell_measurement_theta_min 3.2780 _cell_measurement_theta_max 28.4990 _exptl_crystal_description 'plate' _exptl_crystal_colour 'brown' _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_density_diffrn 1.149 _exptl_crystal_F_000 264 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.450 _exptl_crystal_size_mid 0.310 _exptl_crystal_size_min 0.090 _exptl_absorpt_coefficient_mu 0.071 _shelx_estimated_absorpt_T_min 0.969 _shelx_estimated_absorpt_T_max 0.994 _exptl_absorpt_correction_T_min 0.43754 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.43a (Rigaku Oxford Diffraction, 2018) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 123(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'Rotating-anode X-ray tube (dual wavelength)' _diffrn_source_type 'Rigaku (Mo) X-ray DW Source' _diffrn_radiation_probe x-ray _diffrn_radiation_monochromator mirror _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB AFC11 (RCD3): quarter-chi single' _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 5932 _diffrn_reflns_av_unetI/netI 0.0280 _diffrn_reflns_av_R_equivalents 0.0324 _diffrn_reflns_limit_h_min -6 _diffrn_reflns_limit_h_max 7 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_l_min -11 _diffrn_reflns_limit_l_max 11 _diffrn_reflns_theta_min 2.743 _diffrn_reflns_theta_max 25.990 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.989 _diffrn_measured_fraction_theta_full 0.994 _diffrn_reflns_Laue_measured_fraction_max 0.989 _diffrn_reflns_Laue_measured_fraction_full 0.994 _diffrn_reflns_point_group_measured_fraction_max 0.989 _diffrn_reflns_point_group_measured_fraction_full 0.994 _reflns_number_total 1381 _reflns_number_gt 1149 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'CrysAlisPro 1.171.39.43a (Rigaku OD, 2018)' _computing_cell_refinement 'CrysAlisPro 1.171.39.43a (Rigaku OD, 2018)' _computing_data_reduction 'CrysAlisPro 1.171.39.43a (Rigaku OD, 2018)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0485P)^2^+0.2053P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 1381 _refine_ls_number_parameters 85 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0548 _refine_ls_R_factor_gt 0.0439 _refine_ls_wR_factor_ref 0.1106 _refine_ls_wR_factor_gt 0.1046 _refine_ls_goodness_of_fit_ref 1.100 _refine_ls_restrained_S_all 1.100 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group N2 N 0.6525(2) 0.58927(9) 0.74986(13) 0.0314(3) Uani 1 1 d . . . . . N1 N 0.7409(2) 0.54555(10) 0.63483(14) 0.0333(3) Uani 1 1 d . . . . . C3 C 0.6729(2) 0.40384(11) 0.77782(15) 0.0237(3) Uani 1 1 d . . . . . C4 C 0.6117(2) 0.51127(10) 0.82906(15) 0.0243(3) Uani 1 1 d . . . . . C2 C 0.7494(2) 0.44280(11) 0.64864(15) 0.0267(3) Uani 1 1 d . . . . . C5 C 0.5217(2) 0.53566(11) 0.95262(15) 0.0262(3) Uani 1 1 d . . . . . H10 H 0.490547 0.608824 0.967774 0.031 Uiso 1 1 calc R U . . . C6 C 0.4741(2) 0.32596(12) 0.73262(16) 0.0309(4) Uani 1 1 d . . . . . H1 H 0.411956 0.310712 0.816074 0.046 Uiso 1 1 calc R U . . . H2 H 0.525957 0.259025 0.697559 0.046 Uiso 1 1 calc R U . . . H3 H 0.357590 0.358442 0.655389 0.046 Uiso 1 1 calc R U . . . C7 C 0.8702(2) 0.35224(12) 0.88773(16) 0.0337(4) Uani 1 1 d . . . . . H4 H 0.995730 0.403074 0.912028 0.051 Uiso 1 1 calc R U . . . H5 H 0.918471 0.287302 0.845735 0.051 Uiso 1 1 calc R U . . . H6 H 0.822405 0.333425 0.975582 0.051 Uiso 1 1 calc R U . . . C1 C 0.8239(3) 0.37064(13) 0.54490(17) 0.0352(4) Uani 1 1 d . . . . . H7 H 0.691900 0.339130 0.478486 0.053 Uiso 1 1 calc R U . . . H8 H 0.918186 0.313349 0.598289 0.053 Uiso 1 1 calc R U . . . H9 H 0.910523 0.411920 0.489594 0.053 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 N2 0.0416(7) 0.0260(7) 0.0291(7) 0.0005(5) 0.0135(6) -0.0015(5) N1 0.0412(7) 0.0325(7) 0.0296(7) -0.0011(5) 0.0154(6) -0.0053(6) C3 0.0261(7) 0.0217(7) 0.0224(7) -0.0017(5) 0.0041(6) -0.0006(5) C4 0.0249(6) 0.0231(7) 0.0235(7) 0.0002(6) 0.0033(6) -0.0017(5) C2 0.0239(7) 0.0301(8) 0.0255(8) -0.0028(6) 0.0049(6) -0.0035(6) C5 0.0303(7) 0.0210(7) 0.0266(8) -0.0024(5) 0.0055(6) -0.0006(6) C6 0.0341(8) 0.0293(8) 0.0299(8) -0.0045(6) 0.0086(6) -0.0079(6) C7 0.0360(8) 0.0326(8) 0.0292(8) -0.0015(6) 0.0011(7) 0.0084(6) C1 0.0337(8) 0.0410(9) 0.0330(9) -0.0080(7) 0.0121(7) -0.0029(7) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag N2 C4 1.2919(18) . ? N2 N1 1.4421(17) . ? N1 C2 1.2875(19) . ? C3 C2 1.5003(19) . ? C3 C4 1.5038(19) . ? C3 C6 1.5352(19) . ? C3 C7 1.5358(19) . ? C4 C5 1.449(2) . ? C2 C1 1.488(2) . ? C5 C5 1.339(3) 3_667 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C4 N2 N1 108.73(11) . . ? C2 N1 N2 108.16(11) . . ? C2 C3 C4 97.47(11) . . ? C2 C3 C6 111.06(11) . . ? C4 C3 C6 114.27(11) . . ? C2 C3 C7 110.10(11) . . ? C4 C3 C7 111.64(12) . . ? C6 C3 C7 111.49(12) . . ? N2 C4 C5 118.85(13) . . ? N2 C4 C3 112.46(13) . . ? C5 C4 C3 128.67(12) . . ? N1 C2 C1 123.03(13) . . ? N1 C2 C3 113.15(12) . . ? C1 C2 C3 123.82(13) . . ? C5 C5 C4 125.85(17) 3_667 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C4 N2 N1 C2 0.22(16) . . . . ? N1 N2 C4 C5 179.85(12) . . . . ? N1 N2 C4 C3 1.12(16) . . . . ? C2 C3 C4 N2 -1.78(14) . . . . ? C6 C3 C4 N2 -118.96(14) . . . . ? C7 C3 C4 N2 113.36(14) . . . . ? C2 C3 C4 C5 179.64(13) . . . . ? C6 C3 C4 C5 62.46(19) . . . . ? C7 C3 C4 C5 -65.22(18) . . . . ? N2 N1 C2 C1 177.47(12) . . . . ? N2 N1 C2 C3 -1.47(16) . . . . ? C4 C3 C2 N1 1.94(15) . . . . ? C6 C3 C2 N1 121.60(13) . . . . ? C7 C3 C2 N1 -114.42(14) . . . . ? C4 C3 C2 C1 -176.99(13) . . . . ? C6 C3 C2 C1 -57.34(17) . . . . ? C7 C3 C2 C1 66.65(17) . . . . ? N2 C4 C5 C5 -177.51(17) . . . 3_667 ? C3 C4 C5 C5 1.0(3) . . . 3_667 ? _refine_diff_density_max 0.252 _refine_diff_density_min -0.129 _refine_diff_density_rms 0.036 _shelx_res_file ; TITL umex406_2_a.res in P2(1)/n UMEX406_2.res created by SHELXL-2018/3 at 19:20:57 on 06-Mar-2019 REM Yadorkari-X generated CELL 0.71073 6.1286 12.4667 9.5271 90.0000 104.0440 90.0000 ZERR 2.0 0.0004 0.0008 0.0008 0.0000 0.0080 0.0000 LATT 1 SYMM 1/2-X, 1/2+Y, 1/2-Z REM SPGR P21/n monoclinic SFAC C H N UNIT 28 40 8 SIZE 0.45 0.31 0.09 TEMP -150.0 L.S. 10 FMAP 2 PLAN -20 ACTA CONF LIST 4 OMIT -10.000000 52.000000 list 4 fmap 2 WGHT 0.048500 0.205300 FVAR 0.86091 N2 3 0.652534 0.589268 0.749862 11.00000 0.04157 0.02598 = 0.02906 0.00045 0.01349 -0.00146 N1 3 0.740921 0.545551 0.634825 11.00000 0.04122 0.03249 = 0.02956 -0.00110 0.01535 -0.00526 C3 1 0.672868 0.403837 0.777819 11.00000 0.02606 0.02172 = 0.02240 -0.00166 0.00407 -0.00063 C4 1 0.611740 0.511270 0.829062 11.00000 0.02493 0.02314 = 0.02348 0.00015 0.00333 -0.00167 C2 1 0.749416 0.442800 0.648642 11.00000 0.02392 0.03011 = 0.02548 -0.00279 0.00488 -0.00350 C5 1 0.521664 0.535661 0.952621 11.00000 0.03032 0.02099 = 0.02664 -0.00236 0.00551 -0.00056 AFIX 43 H10 2 0.490547 0.608824 0.967774 11.00000 -1.20000 AFIX 0 C6 1 0.474123 0.325963 0.732624 11.00000 0.03405 0.02932 = 0.02991 -0.00449 0.00864 -0.00791 AFIX 137 H1 2 0.411956 0.310712 0.816074 11.00000 -1.50000 H2 2 0.525957 0.259025 0.697559 11.00000 -1.50000 H3 2 0.357590 0.358442 0.655389 11.00000 -1.50000 AFIX 0 C7 1 0.870223 0.352242 0.887735 11.00000 0.03595 0.03255 = 0.02919 -0.00150 0.00105 0.00840 AFIX 137 H4 2 0.995730 0.403074 0.912028 11.00000 -1.50000 H5 2 0.918471 0.287302 0.845735 11.00000 -1.50000 H6 2 0.822405 0.333425 0.975582 11.00000 -1.50000 AFIX 0 C1 1 0.823856 0.370645 0.544904 11.00000 0.03366 0.04097 = 0.03300 -0.00802 0.01206 -0.00293 AFIX 137 H7 2 0.691900 0.339130 0.478486 11.00000 -1.50000 H8 2 0.918186 0.313349 0.598289 11.00000 -1.50000 H9 2 0.910523 0.411920 0.489594 11.00000 -1.50000 AFIX 0 HKLF 4 1 1 0 0 0 1 0 0 0 1 REM umex406_2_a.res in P2(1)/n REM wR2 = 0.1106, GooF = S = 1.100, Restrained GooF = 1.100 for all data REM R1 = 0.0439 for 1149 Fo > 4sig(Fo) and 0.0548 for all 1381 data REM 85 parameters refined using 0 restraints END WGHT 0.0485 0.2053 REM Highest difference peak 0.252, deepest hole -0.129, 1-sigma level 0.036 Q1 1 0.7194 0.4151 0.7171 11.00000 0.05 0.25 Q2 1 0.6420 0.4524 0.8098 11.00000 0.05 0.24 Q3 1 0.5933 0.3666 0.7589 11.00000 0.05 0.24 Q4 1 0.7472 0.3812 0.8332 11.00000 0.05 0.21 Q5 1 0.7811 0.4071 0.6008 11.00000 0.05 0.18 Q6 1 0.5642 0.5120 0.8862 11.00000 0.05 0.17 Q7 1 0.6690 0.5446 0.8217 11.00000 0.05 0.15 Q8 1 0.4254 0.4995 0.9708 11.00000 0.05 0.15 Q9 1 0.5741 0.5398 0.7763 11.00000 0.05 0.14 Q10 1 0.6869 0.4839 0.6144 11.00000 0.05 0.14 Q11 1 0.9628 0.3244 0.8284 11.00000 0.05 0.13 Q12 1 0.7815 0.4097 0.4348 11.00000 0.05 0.13 Q13 1 0.7444 0.5951 0.5620 11.00000 0.05 0.13 Q14 1 0.9662 0.3701 0.5221 11.00000 0.05 0.12 Q15 1 0.8292 0.4914 0.6719 11.00000 0.05 0.12 Q16 1 0.7537 0.2979 0.5341 11.00000 0.05 0.12 Q17 1 0.4712 0.2746 0.8327 11.00000 0.05 0.11 Q18 1 0.6000 0.6219 0.9763 11.00000 0.05 0.10 Q19 1 0.6899 0.5797 0.6930 11.00000 0.05 0.10 Q20 1 0.5920 0.6610 0.7243 11.00000 0.05 0.09 ; _shelx_res_checksum 6964 _shelx_hkl_file ; 0 -1 1 -0.12 0.09 0 -1 1 -0.18 0.26 0 1 1 -0.20 0.29 0 -1 -1 -0.03 0.12 0 -1 2 16.86 0.80 0 -1 2 15.96 1.04 0 -1 2 17.31 1.11 0 1 2 13.83 1.00 0 -1 3 28.13 1.44 0 1 3 26.19 1.43 0 -1 3 29.19 1.51 0 -1 -3 28.17 1.47 0 -1 3 30.84 1.24 0 -1 -4 16.30 1.30 0 -1 4 20.04 1.42 0 -1 4 16.89 1.33 0 -1 4 20.75 1.08 0 1 4 17.73 1.34 0 1 5 70.42 3.01 0 -1 5 75.54 3.17 0 -1 -5 73.84 3.21 0 -1 5 70.01 3.02 0 -1 5 75.15 2.82 0 -1 -6 107.83 4.55 0 -1 6 111.55 4.06 0 -1 6 110.11 4.27 0 1 6 108.92 4.26 0 -1 6 111.92 4.45 0 1 7 144.73 5.52 0 -1 7 152.85 5.58 0 -1 7 143.63 5.34 0 -1 7 152.37 5.82 0 -1 8 21.45 2.37 0 -1 8 22.73 1.77 0 -1 8 28.03 2.26 0 1 8 29.61 2.26 0 -1 9 -3.95 2.21 0 -1 9 1.61 1.27 0 -1 10 1.67 1.41 0 -1 10 0.99 2.28 0 -1 11 17.20 2.04 0 -2 0 2672.97 85.52 0 2 0 2882.67 85.51 0 -2 1 919.73 28.86 0 2 -1 925.50 28.86 0 2 1 978.09 28.84 0 -2 -1 958.20 28.85 0 -2 1 920.11 28.84 0 2 1 911.00 28.84 0 -2 2 23.58 1.19 0 -2 -2 26.38 1.20 0 2 2 26.12 1.18 0 2 -2 26.46 1.08 0 2 2 23.78 1.15 0 -2 2 24.66 1.05 0 2 3 70.45 2.76 0 -2 3 74.73 2.61 0 2 3 73.69 2.74 0 -2 3 69.62 2.72 0 -2 -3 78.56 2.82 0 2 4 107.49 4.02 0 -2 4 110.29 4.19 0 2 4 109.43 4.05 0 -2 4 106.10 4.03 0 -2 -4 116.30 4.17 0 -2 4 114.10 3.87 0 -2 5 0.64 0.61 0 -2 -5 0.06 0.92 0 2 5 -0.40 1.03 0 2 5 -0.69 1.07 0 -2 5 0.58 1.10 0 -2 5 0.49 1.06 0 -2 6 84.07 3.75 0 -2 6 87.65 3.60 0 -2 6 88.52 3.40 0 2 6 87.10 3.57 0 -2 -6 92.28 3.86 0 2 6 86.39 3.65 0 2 7 1.58 1.42 0 -2 7 1.97 1.44 0 -2 -7 0.62 1.45 0 -2 7 0.82 0.92 0 -2 7 0.78 1.48 0 2 7 0.34 1.44 0 -2 8 3.44 1.86 0 2 8 3.14 1.66 0 2 8 2.00 1.67 0 -2 8 0.76 1.15 0 -2 8 1.96 1.71 0 -2 9 3.17 1.38 0 2 9 -1.14 2.04 0 -2 9 -0.95 2.07 0 2 10 64.95 3.23 0 -2 10 68.43 3.39 0 2 10 61.41 3.78 0 -2 10 70.18 4.02 0 -2 11 14.52 2.04 0 2 11 17.26 2.05 0 -3 0 0.30 0.34 0 3 0 0.13 0.34 0 3 -1 52.03 1.83 0 -3 1 52.47 1.73 0 3 1 49.87 1.78 0 -3 1 49.40 1.79 0 -3 -1 49.55 1.77 0 3 1 53.08 1.73 0 3 2 -0.02 0.48 0 -3 -2 0.07 0.46 0 -3 2 -0.23 0.36 0 -3 2 -0.25 0.55 0 3 2 -0.33 0.52 0 3 -2 0.42 0.43 0 3 3 259.01 8.20 0 3 3 255.34 8.21 0 -3 3 251.09 8.15 0 3 -3 253.22 8.14 0 -3 3 244.89 8.19 0 -3 -3 257.47 8.31 0 -3 4 103.69 3.84 0 3 4 105.09 3.84 0 -3 4 104.75 4.05 0 3 4 98.69 3.81 0 -3 -4 112.31 4.01 0 -3 4 108.23 3.74 0 -3 5 242.21 8.39 0 3 5 232.10 8.12 0 -3 5 232.95 8.11 0 3 5 245.82 8.20 0 -3 -5 246.96 8.38 0 -3 5 257.23 8.08 0 -3 6 24.96 2.05 0 -3 6 25.82 1.82 0 3 6 29.49 1.84 0 -3 -6 27.22 1.99 0 3 6 29.47 1.87 0 -3 6 25.96 1.58 0 3 7 105.52 4.34 0 -3 7 110.66 4.25 0 3 7 108.24 4.44 0 -3 7 112.41 4.39 0 -3 -7 111.79 4.80 0 -3 7 110.70 4.70 0 -3 -8 148.37 6.15 0 3 8 151.74 5.62 0 -3 8 143.16 5.50 0 3 8 144.05 5.73 0 -3 8 148.29 5.65 0 -3 8 143.98 5.95 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2.75 0 -4 8 52.12 3.25 0 4 8 48.13 2.86 0 -4 8 44.22 2.88 0 -4 8 46.19 2.57 0 -4 -8 51.64 3.24 0 -4 8 55.41 2.89 0 4 8 53.96 2.78 0 4 9 32.89 2.68 0 -4 9 32.16 2.77 0 -4 -9 34.51 2.97 0 -4 9 38.67 2.35 0 -4 10 -0.09 2.30 0 -4 10 1.36 1.49 0 4 10 2.57 2.21 0 4 11 1.43 1.54 0 -4 11 0.56 1.69 0 5 0 -0.13 0.41 0 -5 0 0.18 0.36 0 5 1 156.02 4.80 0 -5 1 149.60 4.99 0 5 1 150.61 4.98 0 -5 1 156.61 4.79 0 5 1 153.20 4.80 0 -5 -1 150.63 4.98 0 -5 1 152.02 4.79 0 5 -1 149.38 5.02 0 -5 2 49.69 1.94 0 5 2 50.07 1.91 0 5 -2 50.64 1.96 0 -5 2 49.45 1.82 0 5 2 51.70 1.84 0 -5 -2 50.58 1.94 0 -5 3 4.82 0.73 0 5 3 4.45 0.71 0 5 3 5.24 0.74 0 5 -3 4.30 0.71 0 -5 -3 4.78 0.82 0 -5 3 3.65 0.63 0 5 -4 4.00 0.77 0 5 4 5.39 0.91 0 -5 4 3.76 0.84 0 5 4 3.37 0.81 0 -5 -4 3.57 0.97 0 -5 4 3.50 0.73 0 5 5 0.08 0.86 0 -5 5 2.81 1.01 0 -5 5 0.17 0.70 0 5 5 2.29 1.03 0 -5 -5 -0.12 1.00 0 -5 6 7.81 1.29 0 -5 6 6.35 1.06 0 -5 6 4.40 1.61 0 -5 -6 5.23 1.37 0 5 6 3.83 1.19 0 5 6 7.39 1.28 0 -5 7 46.05 2.44 0 5 7 42.30 2.39 0 5 7 47.31 2.43 0 -5 7 47.27 3.00 0 5 7 35.27 2.40 0 -5 7 42.71 2.32 0 -5 -7 41.92 2.76 0 -5 7 39.44 2.48 0 -5 8 13.12 1.83 0 -5 -8 10.49 2.08 0 5 8 9.92 1.90 0 -5 8 9.34 1.55 0 5 8 13.95 1.76 0 -5 -9 136.19 5.95 0 5 9 121.17 5.25 0 -5 9 131.45 5.22 0 -5 9 130.51 5.41 0 -5 10 12.29 2.58 0 5 10 10.50 2.40 0 -5 10 9.21 1.78 0 -5 11 13.87 2.13 0 -6 0 0.62 0.47 0 6 0 0.64 0.53 0 -6 1 137.82 4.85 0 -6 -1 152.18 4.87 0 6 -1 144.35 4.90 0 6 1 160.11 4.93 0 -6 2 130.81 4.28 0 -6 2 132.62 4.49 0 -6 2 132.38 4.30 0 6 2 130.93 4.31 0 6 -2 132.57 4.50 0 6 2 141.63 4.48 0 -6 -2 133.41 4.49 0 6 2 131.99 4.30 0 -6 3 309.98 9.86 0 -6 3 325.77 10.04 0 -6 3 293.80 9.87 0 6 3 319.33 9.97 0 6 -3 320.72 10.02 0 -6 -3 326.03 10.12 0 6 3 291.92 9.87 0 6 3 313.43 9.87 0 6 -4 97.40 3.38 0 6 4 90.58 3.34 0 -6 -4 87.83 3.57 0 6 4 94.59 3.32 0 -6 4 88.78 3.30 0 -6 4 86.78 3.37 0 -6 4 88.37 3.28 0 -6 -5 19.68 1.67 0 6 5 23.07 1.46 0 -6 5 18.31 1.47 0 -6 5 20.55 1.40 0 6 5 20.16 1.47 0 -6 5 23.07 1.44 0 6 5 21.11 1.45 0 6 6 21.62 1.63 0 -6 6 18.40 1.74 0 -6 -6 22.20 1.98 0 6 6 22.08 1.65 0 -6 6 21.31 2.27 0 -6 6 23.03 1.68 0 6 6 21.82 1.74 0 -6 6 22.10 1.57 0 -6 7 20.52 2.43 0 6 7 18.05 1.89 0 -6 7 20.48 1.72 0 6 7 24.60 1.87 0 -6 7 24.36 1.85 0 6 7 20.02 1.77 0 -6 7 18.23 1.89 0 -6 -7 18.17 2.13 0 6 8 27.45 2.09 0 -6 8 20.61 1.83 0 6 8 19.43 2.15 0 -6 -8 23.30 2.47 0 -6 8 27.98 2.09 0 -6 8 23.34 2.21 0 -6 9 3.57 1.49 0 -6 9 4.65 2.10 0 6 9 3.01 1.98 0 -6 -9 2.27 2.08 0 -6 10 5.49 1.74 0 6 10 8.57 2.33 0 -6 10 6.39 2.49 0 -6 -10 5.66 2.49 0 7 0 0.07 0.56 0 -7 0 -0.07 0.50 0 -7 -1 73.73 2.59 0 7 -1 70.43 2.62 0 -7 1 70.46 2.60 0 7 1 70.89 2.58 0 7 2 10.52 0.61 0 -7 2 8.77 0.61 0 7 2 9.50 0.62 0 7 2 10.61 0.85 0 7 -2 9.04 0.84 0 -7 2 10.63 0.59 0 -7 2 9.77 0.82 0 -7 -2 10.55 0.86 0 7 3 228.47 7.62 0 -7 3 242.22 7.80 0 -7 -3 229.13 7.86 0 -7 3 227.34 7.60 0 7 3 247.00 7.76 0 7 -3 245.54 7.80 0 -7 3 241.89 7.59 0 7 3 237.81 7.60 0 -7 -4 23.83 1.63 0 -7 4 21.41 1.38 0 -7 4 24.85 1.41 0 7 4 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135.82 4.31 -2 -2 2 144.85 4.40 -2 2 2 137.32 4.39 -2 -2 2 136.35 4.11 2 -2 -2 137.08 4.30 -2 2 1 33.53 1.61 -2 -2 1 37.05 1.63 2 -2 -1 35.21 1.41 -2 -2 1 34.10 1.21 2 2 -1 37.56 1.51 2 -2 -1 34.30 1.49 -2 2 1 33.17 1.41 2 2 -1 36.06 1.21 -2 -2 0 495.94 14.47 -2 2 0 451.83 14.17 2 2 0 452.09 13.95 -2 2 0 458.56 14.41 2 -2 0 453.30 14.31 2 2 0 459.71 14.32 -2 -2 0 459.31 13.96 -2 -2 -1 5.43 0.52 -2 2 -1 5.49 0.72 2 2 1 5.92 0.52 2 2 1 6.02 0.90 2 -2 1 6.29 0.90 2 -2 1 6.38 0.67 2 2 2 1125.65 35.10 2 -2 2 1130.44 35.07 -2 2 -2 1141.04 35.09 2 2 2 1118.69 34.92 2 2 3 159.19 5.34 2 2 3 159.39 5.60 -2 2 -3 163.19 5.50 2 -2 3 156.45 5.47 2 2 4 0.53 1.02 -2 2 -4 0.79 0.83 2 2 4 0.81 0.62 2 -2 4 1.06 0.70 2 2 5 87.53 3.74 2 2 5 88.87 3.39 2 -2 5 88.46 3.51 2 -2 6 -1.06 1.58 2 2 6 -0.80 1.47 2 -2 6 0.18 1.03 2 2 6 0.41 0.93 2 2 7 6.83 1.82 2 -2 7 4.86 1.32 2 2 7 3.69 1.16 2 2 8 33.24 2.16 2 -2 8 33.51 2.26 2 2 9 0.92 1.40 2 -2 9 0.85 1.45 2 2 10 -0.77 1.58 2 -2 10 1.41 1.74 -2 -3 11 35.90 2.71 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868.36 27.19 2 3 -3 869.40 27.19 -2 -3 3 866.31 27.06 -2 -3 2 37.72 1.53 2 3 -2 32.55 1.29 -2 -3 2 33.63 1.18 -2 3 2 31.22 1.46 -2 3 2 31.92 1.47 2 3 -2 33.86 1.39 2 -3 -2 32.43 1.39 -2 3 1 74.64 2.88 -2 -3 1 92.07 3.11 -2 3 1 81.79 3.05 2 3 -1 84.60 2.95 2 -3 -1 83.98 2.96 2 -3 0 321.16 10.25 -2 3 0 293.76 10.14 2 3 0 322.65 10.26 2 3 0 323.02 9.86 2 3 1 1253.35 36.18 2 3 1 1144.05 36.27 2 3 1 1181.50 36.62 2 -3 1 1170.07 36.63 -2 3 -2 0.17 0.72 2 3 2 0.51 0.71 2 3 2 0.20 0.45 -2 3 -3 0.55 0.78 2 3 3 1.23 0.54 2 3 3 2.37 0.87 2 3 4 1.72 1.05 -2 3 -4 0.35 0.85 2 3 4 -0.10 0.61 -2 3 -5 3.43 1.08 2 3 5 5.45 1.32 2 3 5 3.38 0.83 2 3 6 23.03 2.07 2 3 6 22.27 1.56 2 3 7 10.91 1.93 2 3 7 12.70 1.41 2 3 8 18.02 1.77 2 3 9 4.47 1.50 2 3 10 31.48 2.50 -2 -4 11 1.47 2.00 -2 4 11 0.87 1.99 -2 -4 11 2.13 1.49 -2 -4 10 4.84 1.80 -2 4 10 4.27 1.83 -2 -4 10 5.84 1.40 -2 -4 9 9.77 1.70 -2 4 9 11.03 1.77 -2 -4 9 12.04 1.42 -2 -4 8 46.00 2.72 2 -4 -8 43.37 2.90 -2 -4 8 48.69 2.42 -2 4 8 51.01 2.48 -2 -4 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5 4 22.84 1.27 2 5 5 67.34 3.03 2 5 5 65.91 2.72 2 -5 5 66.27 2.97 -2 5 -5 67.13 2.97 2 5 6 0.69 1.43 2 5 6 0.64 0.95 2 -5 6 0.07 1.19 -2 5 -6 1.75 1.29 2 5 7 72.56 3.23 2 -5 7 74.35 3.47 2 5 7 76.38 3.62 2 5 8 20.77 1.84 2 -5 8 22.45 2.06 2 5 9 5.63 1.56 2 -5 9 7.57 1.82 2 5 10 5.57 1.75 -2 -6 11 17.51 2.06 2 -6 -10 1.70 2.26 -2 -6 10 2.99 1.43 -2 -6 9 29.61 2.02 2 -6 -9 28.96 2.77 -2 -6 8 0.75 1.38 -2 6 8 0.05 1.37 -2 -6 8 3.10 1.66 -2 -6 8 3.44 1.20 2 -6 -8 4.19 1.86 2 6 -7 -1.80 1.72 2 -6 -7 -1.67 1.63 -2 -6 7 -1.11 1.24 -2 6 7 -0.27 1.25 -2 6 7 1.19 1.32 2 -6 -7 1.45 1.61 -2 -6 7 0.94 1.46 -2 -6 7 1.75 1.02 -2 -6 6 26.89 1.91 -2 -6 6 27.99 1.58 2 -6 -6 27.14 2.07 -2 6 6 29.62 1.78 2 6 -6 27.05 1.97 2 -6 -6 28.38 2.00 -2 -6 6 26.58 1.61 -2 6 6 27.88 1.66 -2 -6 5 81.80 3.37 -2 -6 5 89.79 3.20 2 -6 -5 83.00 3.53 -2 6 5 91.48 3.41 2 6 -5 88.76 3.43 -2 6 5 89.14 3.21 2 -6 -5 79.82 3.37 -2 -6 5 85.62 3.19 -2 -6 4 74.95 2.91 -2 -6 4 77.32 2.77 2 6 -4 80.12 2.93 2 -6 -4 73.28 2.87 -2 6 4 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1.21 2 6 6 1.67 1.02 2 6 7 38.18 2.19 2 -6 7 37.19 2.41 2 6 7 42.12 2.50 2 6 8 68.02 3.22 2 -6 8 70.52 3.52 2 -6 9 13.32 2.08 2 6 9 13.92 1.78 2 6 10 51.17 3.05 -2 -7 11 10.38 1.87 -2 -7 10 25.23 2.17 2 -7 -10 29.84 3.17 2 -7 -9 16.92 2.55 -2 -7 9 13.44 1.68 -2 -7 8 -2.54 1.45 -2 7 8 -3.09 1.50 -2 -7 8 -0.67 1.70 2 -7 -8 0.10 1.79 -2 -7 8 -0.65 1.16 2 -7 -7 165.83 6.44 -2 -7 7 157.67 6.04 -2 -7 7 167.45 5.84 -2 -7 7 165.20 5.77 -2 7 7 159.62 5.78 -2 -7 6 21.97 1.38 2 -7 -6 19.72 1.93 -2 -7 6 16.79 1.64 -2 -7 6 17.97 1.35 -2 7 6 21.56 1.41 2 7 -6 13.55 1.78 2 -7 -6 13.85 1.70 -2 7 6 19.98 1.61 -2 7 5 174.52 5.97 -2 -7 5 165.80 5.91 -2 -7 5 173.09 5.76 -2 7 5 171.52 5.73 -2 -7 5 163.83 5.70 2 7 -5 166.30 5.99 2 -7 -5 168.51 5.98 2 -7 -5 170.31 6.15 -2 -7 4 13.74 1.13 2 -7 -4 13.67 1.25 -2 7 4 11.32 1.02 -2 -7 4 11.56 1.01 2 -7 -4 13.27 1.11 -2 -7 4 12.52 0.91 2 7 -4 14.13 1.15 -2 7 4 14.65 1.27 -2 -7 3 66.79 2.35 -2 -7 3 64.60 2.47 2 -7 -3 63.59 2.50 2 -7 -3 70.14 2.79 2 7 -3 69.02 2.54 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62.19 2.45 -3 -3 2 60.61 2.11 3 -3 -2 63.49 2.50 3 3 -2 65.80 2.51 3 3 -2 63.96 2.19 3 3 -1 0.09 0.32 3 3 -1 0.20 0.67 3 -3 -1 0.43 0.64 -3 -3 1 0.15 0.35 -3 3 1 0.10 0.68 -3 -3 1 -0.99 0.95 -3 3 1 -0.36 0.95 3 -3 -1 -0.46 0.64 3 -3 0 178.40 6.03 3 3 0 177.90 5.71 -3 -3 0 183.45 5.74 -3 3 0 181.28 6.07 3 3 0 179.90 6.25 3 -3 0 172.63 6.25 -3 -3 -1 2.08 0.50 -3 3 -1 1.36 0.75 3 3 1 1.93 0.47 3 -3 1 1.79 0.71 3 3 1 2.02 0.99 3 -3 1 0.84 0.92 3 3 2 178.36 6.37 -3 3 -2 190.79 6.44 3 3 2 185.13 6.17 3 -3 2 194.74 6.46 3 3 2 198.18 6.87 3 -3 2 188.48 6.84 3 3 3 1.47 1.06 -3 3 -3 2.81 0.93 3 3 3 3.18 0.70 3 -3 3 3.41 0.87 3 3 4 7.10 1.45 -3 3 -4 7.88 1.25 3 3 4 7.69 0.98 3 -3 4 6.60 1.06 3 3 5 0.44 0.94 3 3 5 2.72 1.50 -3 3 -5 1.14 1.24 3 -3 5 0.54 1.06 3 3 6 0.70 1.64 3 3 6 0.40 1.09 3 -3 6 -0.27 1.19 3 -3 7 10.64 1.56 3 3 7 8.24 1.49 3 3 8 14.65 1.78 3 -3 8 15.76 1.91 3 -3 9 4.12 1.73 3 3 9 4.68 1.68 -3 -4 12 3.05 1.53 -3 -4 11 23.94 1.97 3 -4 -10 -2.99 2.37 3 4 -10 -3.86 2.36 3 -4 -10 0.26 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4 -3 144.07 4.78 3 -4 -3 135.53 4.77 3 4 -2 51.55 1.78 -3 4 2 48.99 2.11 -3 -4 2 51.80 2.33 -3 4 2 47.84 2.29 3 -4 -2 52.13 2.14 3 -4 -2 51.25 2.12 -3 -4 2 48.54 1.68 3 4 -2 55.46 2.13 -3 -4 1 9.10 0.44 3 -4 -1 11.15 0.93 3 4 -1 13.20 0.99 3 -4 -1 10.75 0.95 -3 4 1 10.92 0.99 3 4 -1 10.16 0.47 -3 -4 1 9.77 1.28 -3 4 1 8.82 1.22 3 4 0 20.38 1.01 -3 4 0 23.93 1.38 3 4 0 23.93 0.88 3 -4 0 20.59 1.29 3 4 0 23.91 1.42 3 -4 0 20.70 1.42 3 -4 1 44.21 2.31 3 4 1 46.04 1.87 -3 4 -1 43.12 2.07 3 4 1 46.83 1.69 3 -4 1 45.53 2.06 3 4 1 49.81 2.35 3 4 2 39.85 1.77 3 4 2 36.41 1.53 3 -4 2 35.34 1.84 3 4 2 38.11 2.16 -3 4 -2 34.64 1.86 3 -4 2 32.67 2.16 3 4 3 12.19 0.94 -3 4 -3 9.76 1.22 3 -4 3 13.66 1.21 3 4 3 10.44 1.23 3 4 4 34.30 2.10 3 4 4 35.40 1.75 3 -4 4 33.10 1.96 -3 4 -4 32.86 2.02 3 4 5 30.55 1.77 3 4 5 31.64 2.25 -3 4 -5 31.42 2.05 3 -4 5 30.04 1.98 3 4 6 0.15 1.72 3 -4 6 1.47 1.24 3 4 6 0.73 1.08 3 4 7 0.33 1.25 3 -4 7 0.93 1.33 3 4 8 1.48 1.45 3 -4 8 1.80 1.57 3 4 9 3.55 1.63 3 -4 9 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-5 -7 1.04 1.77 4 -5 -7 -0.08 1.50 4 5 -7 5.76 1.50 4 -5 -7 6.27 1.51 -4 -5 7 0.06 1.39 -4 5 7 1.15 1.36 4 5 -6 69.00 3.05 4 -5 -6 69.47 3.06 4 5 -6 66.78 3.12 4 -5 -6 68.22 3.18 -4 5 6 65.82 3.00 -4 -5 6 66.12 3.07 -4 5 6 63.55 3.09 -4 -5 6 64.81 2.54 4 -5 -6 62.13 3.15 4 5 -5 28.92 1.78 4 -5 -5 27.93 1.78 4 5 -5 24.69 1.68 4 5 -5 27.60 1.90 4 -5 -5 25.10 1.91 -4 5 5 24.61 1.80 -4 -5 5 27.27 1.85 -4 5 5 26.19 1.84 -4 -5 5 26.97 1.28 4 -5 -5 28.49 1.90 4 5 -4 8.37 1.19 4 -5 -4 5.97 1.13 4 -5 -4 10.52 1.29 -4 -5 4 8.80 1.40 -4 5 4 9.57 1.37 4 5 -4 8.32 1.00 -4 5 4 11.82 1.38 -4 -5 4 8.51 0.69 4 5 -3 119.34 4.07 -4 -5 3 118.01 3.92 -4 5 3 119.67 4.45 -4 -5 3 133.54 4.85 -4 5 3 125.55 4.80 4 -5 -3 123.09 4.52 4 5 -3 129.59 4.46 4 -5 -3 132.88 4.48 4 -5 -2 17.92 1.35 4 5 -2 20.05 1.39 4 -5 -2 17.69 1.39 -4 5 2 16.94 1.41 -4 -5 2 19.05 1.80 -4 5 2 16.16 1.78 -4 5 1 79.22 3.20 -4 -5 1 85.18 3.74 -4 5 1 73.40 3.62 4 -5 -1 74.29 3.11 4 5 -1 73.89 3.16 4 -5 -1 78.10 3.22 4 5 0 10.38 1.24 4 -5 0 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176.36 5.93 4 6 -6 178.68 6.38 4 -6 -6 180.13 6.37 4 6 -6 183.87 6.44 4 -6 -6 177.40 6.41 -4 -6 6 181.97 6.42 -4 6 6 181.86 6.46 -4 -6 6 171.05 5.85 4 -6 -6 168.71 6.55 -4 -6 5 2.87 0.65 4 -6 -5 2.40 1.28 4 6 -5 6.30 1.32 4 -6 -5 3.96 1.25 -4 -6 5 2.12 1.19 -4 6 5 2.73 1.31 4 6 -5 2.48 1.43 -4 -6 5 3.25 0.72 4 -6 -5 4.65 1.48 -4 6 5 2.44 1.27 4 6 -4 354.41 11.31 4 -6 -4 342.92 11.29 -4 -6 4 336.62 10.82 -4 6 4 359.37 11.45 -4 -6 4 355.29 10.81 -4 -6 4 346.52 11.54 -4 6 4 326.11 11.53 4 -6 -4 334.34 11.44 -4 -6 3 -0.39 1.34 -4 6 3 -0.74 1.37 4 -6 -3 1.50 1.02 -4 6 3 0.64 1.05 4 6 -3 1.40 0.87 4 -6 -3 1.55 0.86 -4 6 2 75.58 3.17 -4 -6 2 76.75 3.47 -4 6 2 72.26 3.45 4 -6 -2 72.81 3.10 4 6 -2 77.42 3.05 4 -6 -2 70.89 2.99 4 6 -1 10.44 1.25 4 -6 -1 9.55 1.23 -4 6 1 12.97 1.44 4 -6 -1 13.79 1.32 4 6 0 10.10 1.23 4 -6 0 8.11 1.23 -4 6 0 6.64 1.24 4 -6 0 9.07 1.36 4 6 1 6.31 1.29 4 -6 1 4.76 1.29 4 6 1 5.38 0.74 4 6 1 6.78 0.52 -4 6 -1 5.01 1.27 4 -6 1 8.00 1.24 4 6 2 0.49 1.39 4 -6 2 0.33 1.43 4 6 2 1.62 0.95 -4 6 -2 2.62 1.31 4 6 2 1.17 0.59 4 -6 2 3.71 1.17 4 6 3 8.67 1.26 4 6 3 7.25 0.90 4 -6 3 6.71 1.41 4 6 3 6.06 1.70 4 -6 3 7.86 1.82 4 6 4 61.80 2.95 4 6 4 68.46 2.69 4 -6 4 58.16 3.05 4 6 4 61.01 3.50 4 -6 4 56.89 3.53 4 6 5 21.86 1.62 4 -6 5 20.11 1.97 4 6 5 18.37 2.44 4 -6 5 13.97 2.46 4 6 6 10.95 1.59 4 -6 6 11.42 1.83 4 -6 6 12.47 2.61 4 6 7 0.79 1.49 4 7 -10 7.29 2.78 4 -7 -10 9.83 2.73 4 7 -9 12.96 2.45 4 -7 -9 8.28 2.27 -4 -7 8 1.60 1.11 4 7 -8 1.47 1.75 4 -7 -8 1.75 1.77 4 -7 -7 0.06 1.82 -4 -7 7 2.40 1.02 4 7 -7 5.10 1.57 4 -7 -7 1.49 1.47 4 7 -7 -0.25 1.86 -4 -7 6 13.97 1.54 -4 7 6 12.45 1.57 4 7 -6 13.10 1.66 4 -7 -6 11.41 1.63 -4 -7 6 10.14 1.09 4 7 -6 13.81 1.95 4 -7 -6 13.58 1.91 -4 -7 5 8.95 0.71 -4 -7 5 8.78 0.85 -4 -7 5 8.70 1.45 -4 7 5 10.46 1.50 4 7 -5 10.73 1.45 4 -7 -5 10.45 1.42 4 7 -5 10.84 1.64 4 -7 -5 7.90 1.58 4 7 -4 72.17 2.93 4 -7 -4 67.25 2.88 4 -7 -4 69.21 2.95 -4 -7 4 70.61 3.19 -4 7 4 64.55 3.18 -4 7 3 0.90 1.41 4 7 -3 2.16 0.93 -4 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3 26.38 2.19 4 -9 -2 2.85 1.29 4 9 -2 1.87 0.94 4 -9 -2 2.92 0.91 4 -9 -1 9.15 1.46 4 9 -1 8.24 1.15 4 -9 -1 8.05 1.11 4 9 0 -1.64 1.16 4 -9 0 -0.15 1.09 4 -9 0 2.06 1.33 4 9 1 8.23 1.25 4 -9 1 9.76 1.36 4 -9 1 12.06 1.65 4 9 2 1.36 1.19 4 -9 2 0.83 1.33 4 -9 2 -0.81 1.25 4 9 3 8.32 1.61 4 -9 3 4.89 1.69 4 -9 3 8.99 1.46 4 -9 4 38.18 2.51 4 9 4 39.38 2.63 4 -9 4 37.89 2.95 4 -9 5 16.78 2.05 4 9 5 13.76 1.93 4 -9 5 13.67 2.36 4 9 6 2.41 1.80 4 -9 6 1.96 2.44 4 9 7 11.38 2.26 4 -10 -8 17.19 2.71 4 -10 -7 14.26 2.25 4 10 -7 14.33 2.15 4 -10 -7 14.23 2.13 4 -10 -6 1.58 1.65 4 10 -6 6.63 1.66 4 -10 -6 4.21 1.59 4 10 -5 42.37 2.35 4 -10 -5 45.09 2.31 4 -10 -4 0.43 1.40 4 10 -4 4.02 1.30 4 -10 -4 3.65 1.27 4 10 -4 2.25 1.49 4 -10 -3 3.72 1.34 4 10 -3 3.93 1.33 4 10 -3 5.38 1.19 4 -10 -3 3.61 1.13 4 -10 -2 47.19 2.59 4 10 -2 45.27 2.19 4 -10 -2 45.97 2.16 4 -10 -1 91.28 3.79 4 10 -1 91.06 3.34 4 -10 0 86.80 3.88 4 10 0 94.37 3.61 4 -10 0 88.48 3.56 4 10 1 0.44 1.05 4 -10 1 0.80 1.08 4 -10 1 -1.14 1.40 4 -10 2 5.59 1.38 4 -10 2 3.25 1.60 4 10 3 1.02 1.39 4 -10 3 0.08 1.52 4 -10 3 2.95 1.57 4 10 4 1.26 1.63 4 -10 4 0.56 1.86 4 -10 4 2.64 1.51 4 -10 5 16.72 2.10 4 10 5 8.72 1.93 4 -11 -7 30.09 2.84 4 -11 -6 9.42 2.03 4 -11 -5 11.84 1.94 4 -11 -4 5.50 1.59 4 -11 -3 46.61 2.69 4 -11 -2 29.76 2.17 4 -11 -1 36.67 2.40 4 -11 0 3.41 1.50 4 -11 1 26.05 2.11 4 -11 2 15.97 2.15 4 -11 3 -0.25 1.65 4 -11 4 19.95 2.14 4 -12 -6 3.35 2.04 4 -12 -5 3.75 1.82 4 -12 -4 4.31 1.73 4 -12 -3 0.15 1.51 4 -12 -2 0.90 1.47 4 -12 -1 6.69 1.66 4 -12 0 59.25 3.17 4 -12 1 13.17 1.92 4 -12 2 1.12 1.72 4 -12 3 1.43 1.93 4 -13 -4 13.31 2.18 4 -13 -3 1.62 1.66 4 -13 -2 12.22 1.83 4 -13 -1 7.57 1.78 4 -13 0 29.91 2.46 4 -13 1 13.83 2.05 5 0 -11 25.64 3.34 5 0 -10 4.70 2.33 5 0 -9 2.97 2.07 5 0 -8 -1.82 1.95 5 0 -7 111.03 4.82 -5 0 7 113.58 4.28 5 0 -6 1.13 1.44 -5 0 6 2.75 1.15 -5 0 5 176.18 5.87 5 0 -5 155.58 5.91 5 0 -4 -0.27 0.97 -5 0 4 -0.23 0.89 -5 0 3 21.31 1.37 5 0 -3 18.57 1.32 5 0 -2 0.15 0.81 -5 0 2 0.66 0.89 -5 0 1 121.25 4.37 5 0 -1 121.55 4.33 -5 0 0 -0.84 0.97 5 0 0 -0.77 0.97 -5 0 -1 3.44 1.11 5 0 1 3.83 0.92 -5 0 -2 -1.06 1.14 5 0 2 -0.10 0.94 -5 0 -3 208.47 7.14 5 0 3 202.07 7.15 -5 0 -4 1.52 1.27 5 0 4 -0.12 1.20 5 0 5 110.09 4.47 5 0 6 0.52 1.43 5 0 7 3.45 1.65 5 -1 -11 2.54 2.71 5 1 -11 1.79 2.64 5 -1 -10 5.94 2.42 5 1 -10 5.38 2.40 5 -1 -10 6.81 2.29 5 1 -9 6.86 2.17 5 1 -9 11.76 2.11 5 -1 -9 8.09 1.98 5 -1 -8 23.26 2.48 5 1 -8 26.26 2.41 5 -1 -8 29.03 2.41 5 1 -8 26.78 2.36 -5 -1 8 28.91 1.88 5 1 -7 34.96 2.60 5 1 -7 39.00 2.53 5 -1 -7 43.62 2.57 -5 1 7 41.53 2.22 -5 -1 7 38.20 2.07 5 -1 -7 37.69 2.61 5 1 -6 229.81 8.08 5 1 -6 221.09 7.97 5 -1 -6 232.16 8.00 5 -1 -6 233.01 8.06 -5 1 6 230.19 7.79 -5 -1 6 231.73 7.70 5 -1 -6 223.67 8.06 5 1 -5 -2.54 1.47 5 -1 -5 -3.94 1.47 -5 -1 5 0.45 1.44 -5 1 5 0.90 1.46 5 -1 -5 0.16 1.11 5 1 -5 2.06 1.16 -5 1 5 0.70 1.19 -5 -1 5 0.99 1.02 -5 -1 4 41.20 1.90 -5 1 4 42.43 2.04 -5 -1 4 40.96 2.59 -5 1 4 41.33 2.61 5 -1 -4 43.90 2.15 5 1 -4 43.89 2.24 5 -1 -4 45.37 2.26 5 1 -4 40.45 2.03 -5 -1 3 4.23 1.65 -5 1 3 4.66 1.70 5 -1 -3 5.19 0.97 5 1 -3 2.98 0.88 5 1 -3 3.06 1.10 5 -1 -3 4.41 1.17 -5 -1 3 4.69 0.91 -5 1 3 3.29 1.03 -5 -1 2 96.21 3.55 -5 1 2 103.09 3.72 -5 -1 2 100.06 4.47 -5 1 2 97.52 4.48 5 -1 -2 92.10 3.62 5 1 -2 93.29 3.51 5 1 -2 95.87 4.00 5 -1 -2 104.15 4.07 5 1 -1 11.88 1.02 5 1 -1 10.93 1.42 5 -1 -1 12.83 1.45 -5 -1 1 8.43 1.04 -5 1 1 10.00 1.18 -5 -1 1 12.22 2.13 -5 1 1 11.03 2.09 5 -1 -1 10.40 1.12 5 1 0 11.26 1.60 5 -1 0 13.54 1.64 -5 -1 0 14.29 1.20 -5 1 0 13.23 1.33 5 -1 0 16.25 1.39 5 1 0 14.29 1.22 -5 -1 -1 25.96 1.58 -5 1 -1 28.62 1.76 5 1 1 24.61 1.44 5 -1 1 25.56 1.57 5 1 1 25.44 2.20 5 -1 1 25.98 2.18 -5 -1 -2 74.93 2.98 -5 1 -2 66.19 3.04 5 1 2 69.75 2.90 5 -1 2 71.68 3.03 5 1 2 70.99 3.76 5 -1 2 74.38 3.78 -5 -1 -3 35.72 2.04 -5 1 -3 35.66 2.15 5 1 3 38.05 2.07 5 -1 3 36.79 2.13 5 1 3 43.13 3.06 5 -1 3 40.55 2.98 5 1 4 75.07 3.32 5 -1 4 78.29 3.45 5 1 4 80.42 4.39 5 -1 4 76.36 4.39 5 1 5 3.88 1.35 5 -1 5 2.73 1.39 5 1 5 3.23 2.51 5 -1 5 2.75 2.46 5 1 6 0.58 1.40 5 -1 6 3.01 1.57 5 1 6 -1.38 2.81 5 -1 6 1.16 2.72 5 1 7 8.38 1.81 5 -1 7 6.24 1.82 5 2 -11 11.16 2.87 5 -2 -10 3.62 2.36 5 2 -10 -2.29 2.23 5 2 -10 1.47 2.22 5 -2 -10 0.95 2.20 5 -2 -9 7.47 2.28 5 2 -9 8.27 2.21 5 2 -9 10.90 2.10 5 -2 -9 11.65 2.08 -5 -2 8 1.45 1.15 5 -2 -8 2.14 1.85 5 2 -8 3.19 1.83 5 2 -8 5.95 1.85 5 -2 -8 2.87 1.75 5 2 -7 28.45 2.30 5 2 -7 28.62 2.15 5 -2 -7 26.12 2.17 -5 -2 7 26.33 1.68 5 -2 -7 26.45 2.28 5 2 -6 4.78 1.42 5 -2 -6 5.47 1.40 5 2 -6 7.00 1.74 5 -2 -6 6.36 1.74 5 -2 -6 5.37 1.40 5 2 -6 2.61 1.46 -5 2 6 3.50 1.24 -5 -2 6 5.72 1.03 5 2 -5 19.25 1.75 5 -2 -5 21.94 1.82 -5 -2 5 22.11 1.98 -5 2 5 24.90 2.05 5 2 -5 21.18 1.69 -5 -2 5 22.65 1.46 5 -2 -5 22.72 1.71 -5 2 5 20.81 1.68 -5 -2 4 1.26 1.52 -5 2 4 -0.71 1.49 5 -2 -4 0.85 0.99 5 2 -4 1.25 0.97 -5 -2 4 0.24 0.75 -5 2 4 1.34 1.03 5 2 -4 2.05 1.07 5 -2 -4 1.28 1.03 -5 -2 3 3.96 1.62 -5 2 3 2.66 1.62 5 -2 -3 2.89 0.99 5 2 -3 3.16 0.86 5 2 -3 2.32 1.03 5 -2 -3 3.72 1.08 -5 -2 3 3.00 0.83 -5 2 3 2.41 1.04 5 -2 -2 1.02 0.89 5 2 -2 0.37 0.72 5 2 -2 -0.58 1.16 5 -2 -2 -0.90 1.15 -5 -2 2 0.83 0.78 -5 2 2 1.41 1.05 -5 -2 2 2.48 1.74 -5 2 2 0.82 1.77 5 2 -1 14.00 1.52 5 -2 -1 13.48 1.47 -5 -2 1 11.23 1.03 5 2 -1 13.24 1.02 -5 2 1 12.54 1.34 -5 -2 1 13.46 2.17 -5 2 1 9.66 2.03 5 -2 -1 11.55 1.22 -5 -2 0 44.85 2.02 -5 2 0 43.62 2.27 5 -2 0 48.59 2.35 5 2 0 45.50 2.01 5 2 0 47.85 2.62 5 -2 0 45.24 2.60 5 2 1 11.91 1.72 5 -2 1 10.19 1.70 -5 -2 -1 10.97 1.14 -5 2 -1 11.75 1.38 5 2 1 11.79 1.04 5 -2 1 11.82 1.24 -5 -2 -2 41.11 1.97 -5 2 -2 38.50 2.21 5 2 2 37.91 1.89 5 -2 2 36.11 2.09 5 2 2 37.04 2.77 5 -2 2 35.66 2.71 -5 2 -3 115.60 4.47 5 2 3 111.29 4.23 5 -2 3 111.59 4.41 5 2 3 116.73 5.22 5 -2 3 108.08 5.14 5 2 4 1.11 1.72 5 2 4 -0.22 1.13 5 -2 4 -0.07 1.23 5 2 4 0.13 2.04 5 -2 4 1.12 1.94 5 2 5 3.74 1.31 5 -2 5 3.59 1.44 5 2 5 4.76 2.43 5 -2 5 5.21 2.37 5 2 6 10.86 1.65 5 -2 6 9.16 1.74 5 2 6 9.43 2.99 5 -2 6 10.41 2.95 5 2 7 9.88 1.85 5 -2 7 9.57 1.91 5 2 8 0.27 1.86 5 3 -11 4.58 2.73 5 -3 -10 6.01 2.53 5 3 -10 2.68 2.34 5 3 -10 4.57 2.34 5 -3 -10 2.23 2.29 5 -3 -9 13.15 2.51 5 3 -9 14.08 2.37 5 3 -9 20.03 2.32 5 -3 -9 19.75 2.32 -5 -3 8 2.41 1.13 5 -3 -8 -1.09 1.77 5 3 -8 1.60 1.76 5 3 -8 2.94 1.83 5 -3 -8 2.65 1.80 -5 -3 7 0.52 1.00 5 -3 -7 2.32 1.60 5 3 -7 5.60 1.62 5 -3 -7 2.72 1.58 5 3 -7 2.18 1.59 5 3 -6 1.56 1.36 5 -3 -6 0.67 1.35 5 -3 -6 3.99 1.42 5 3 -6 1.64 1.63 5 -3 -6 2.96 1.69 5 3 -6 2.61 1.38 -5 3 6 2.47 1.28 -5 -3 6 2.31 0.94 5 3 -5 28.44 1.95 5 -3 -5 26.22 1.96 5 3 -5 31.66 1.93 -5 3 5 32.55 1.96 -5 -3 5 30.74 1.60 -5 -3 5 27.62 2.18 -5 3 5 27.05 2.24 5 -3 -5 28.25 1.98 -5 -3 4 9.99 1.74 -5 3 4 10.71 1.77 5 -3 -4 10.30 1.30 5 3 -4 11.33 1.22 -5 -3 4 10.18 0.91 -5 3 4 10.12 1.22 5 3 -4 12.15 1.32 5 -3 -4 13.45 1.35 -5 -3 3 2.50 1.67 -5 3 3 3.30 1.73 5 -3 -3 3.42 1.05 5 3 -3 2.06 0.85 5 3 -3 2.54 1.15 5 -3 -3 1.89 1.09 -5 -3 3 3.47 0.76 -5 3 3 2.30 1.12 -5 -3 2 132.78 4.73 -5 3 2 138.01 5.14 -5 -3 2 156.09 5.91 -5 3 2 145.58 5.83 5 -3 -2 147.12 5.12 5 3 -2 145.47 5.35 5 -3 -2 142.68 5.34 5 3 -2 139.64 4.74 5 3 -1 0.34 0.65 5 3 -1 1.03 1.11 5 -3 -1 2.92 1.28 -5 -3 1 -0.49 0.77 -5 3 1 0.31 1.09 5 -3 -1 0.54 0.99 5 3 0 16.71 1.76 5 -3 0 17.63 1.77 -5 -3 0 16.50 1.14 5 3 0 16.25 1.12 -5 3 0 15.32 1.50 5 -3 0 17.25 1.58 5 3 1 4.83 1.48 5 -3 1 4.77 1.55 -5 -3 -1 5.90 0.94 -5 3 -1 6.00 1.31 5 3 1 5.41 0.85 5 -3 1 5.52 1.16 5 3 2 21.55 2.20 5 -3 2 21.08 2.27 -5 3 -2 23.20 1.83 5 3 2 22.09 1.37 5 -3 2 20.62 1.61 5 3 3 39.01 2.51 5 3 3 40.75 2.06 5 -3 3 41.96 2.32 5 3 3 41.35 2.96 5 -3 3 36.69 2.90 5 3 4 27.29 1.79 5 3 4 27.05 2.33 5 -3 4 24.20 1.99 5 3 4 25.94 2.73 5 -3 4 30.76 2.84 5 3 5 1.98 1.25 5 -3 5 0.08 1.43 5 3 5 -0.44 2.28 5 -3 5 -0.28 2.25 5 3 6 1.58 1.45 5 -3 6 1.32 1.61 5 3 6 -1.50 2.64 5 -3 6 -0.77 2.64 5 3 7 9.63 1.85 5 -4 -10 -0.13 2.51 5 4 -10 3.45 2.38 5 -4 -10 1.72 2.31 5 -4 -9 22.97 2.75 5 4 -9 20.97 2.53 5 4 -9 24.22 2.50 5 -4 -9 25.81 2.60 5 -4 -8 2.01 1.83 5 4 -8 -1.45 1.76 5 4 -8 4.04 1.81 5 -4 -8 0.31 1.73 5 -4 -7 10.45 1.84 5 4 -7 16.31 1.91 5 -4 -7 13.99 1.86 5 4 -7 9.84 1.79 5 -4 -6 4.19 1.47 5 4 -6 6.38 1.49 5 -4 -6 5.97 1.49 5 4 -6 6.70 1.77 5 -4 -6 5.36 1.76 5 4 -6 5.16 1.45 -5 -4 6 3.88 0.93 5 4 -5 74.09 3.35 5 -4 -5 73.85 3.37 5 4 -5 78.40 3.24 -5 4 5 83.39 3.39 -5 -4 5 78.67 2.92 -5 -4 5 79.57 3.66 -5 4 5 81.07 3.73 5 -4 -5 71.86 3.39 -5 -4 4 15.93 1.95 -5 4 4 16.44 1.97 5 -4 -4 17.19 1.54 5 4 -4 14.09 1.32 -5 -4 4 14.43 0.97 -5 4 4 15.44 1.45 5 4 -4 17.95 1.49 5 -4 -4 15.31 1.43 -5 -4 3 19.55 1.09 -5 4 3 23.96 1.69 5 -4 -3 21.18 1.60 5 4 -3 22.20 1.64 5 -4 -3 21.90 1.69 5 4 -3 23.21 1.31 -5 -4 3 23.91 2.19 -5 4 3 22.94 2.26 -5 -4 2 23.30 1.14 -5 4 2 23.89 1.73 5 -4 -2 22.37 1.61 5 4 -2 24.87 1.80 5 -4 -2 22.74 1.78 5 4 -2 17.97 1.13 -5 -4 2 26.55 2.38 -5 4 2 23.58 2.43 -5 -4 1 179.40 5.74 -5 4 1 177.30 6.28 5 -4 -1 170.10 6.20 5 4 -1 189.49 6.50 5 -4 -1 177.18 6.45 5 4 -1 168.63 5.67 5 4 0 19.29 1.84 5 -4 0 18.94 1.81 -5 -4 0 21.87 1.23 5 4 0 21.37 1.12 -5 4 0 20.45 1.75 5 -4 0 20.29 1.72 5 4 1 14.09 1.79 5 -4 1 11.55 1.77 5 4 1 14.68 1.03 -5 4 -1 17.15 1.64 5 -4 1 14.16 1.45 5 4 2 26.16 2.34 5 -4 2 22.68 2.37 5 4 2 23.60 1.87 5 4 2 25.25 1.40 5 -4 2 24.27 1.76 5 4 3 28.46 2.15 5 4 3 26.98 1.62 5 -4 3 25.20 1.91 5 4 3 30.84 2.66 5 -4 3 26.79 2.55 5 4 4 23.82 1.65 5 -4 4 22.74 1.95 5 4 4 20.32 2.61 5 -4 4 19.66 2.58 5 4 5 10.88 1.48 5 -4 5 11.32 1.79 5 4 5 14.32 2.75 5 -4 5 15.28 2.62 5 4 6 2.63 1.48 5 -4 6 1.37 1.59 5 4 6 4.84 2.81 5 -4 6 1.19 2.49 5 5 -10 27.99 3.00 5 -5 -10 20.67 2.92 5 -5 -9 7.90 2.33 5 5 -9 10.21 2.19 5 -5 -9 7.70 2.15 5 -5 -8 20.46 2.48 5 5 -8 23.71 2.26 5 -5 -8 24.72 2.29 5 5 -7 51.24 2.85 5 5 -7 51.35 2.85 5 -5 -7 53.13 2.90 5 -5 -7 49.91 3.03 5 5 -6 33.15 2.16 5 5 -6 34.00 2.26 5 -5 -6 36.61 2.29 5 5 -6 33.65 2.37 5 -5 -6 32.05 2.40 5 -5 -6 31.10 2.28 5 5 -5 38.68 2.27 5 -5 -5 39.08 2.30 5 5 -5 40.67 2.10 -5 -5 5 42.46 2.57 -5 5 5 39.45 2.59 5 -5 -5 35.57 2.32 -5 -5 4 12.29 1.92 -5 5 4 12.18 1.90 5 -5 -4 14.57 1.50 5 5 -4 12.99 1.20 -5 -5 4 11.96 0.84 -5 5 4 11.89 1.38 5 5 -4 17.31 1.46 5 -5 -4 16.61 1.46 5 5 -3 16.84 1.09 5 -5 -3 15.80 1.49 -5 -5 3 16.58 0.89 5 -5 -3 16.63 1.54 5 5 -3 18.82 1.55 -5 5 3 19.29 1.66 -5 -5 3 20.33 2.16 -5 5 3 20.28 2.20 -5 -5 2 22.07 0.99 -5 5 2 23.73 1.79 5 -5 -2 24.09 1.70 5 5 -2 23.91 1.78 5 -5 -2 21.13 1.74 -5 -5 2 23.33 2.31 -5 5 2 18.48 2.30 5 5 -2 19.21 1.07 5 5 -1 11.29 1.56 5 -5 -1 9.82 1.53 -5 5 1 12.68 1.51 5 5 -1 12.25 0.75 5 5 0 4.37 0.61 5 5 0 5.82 1.41 5 -5 0 4.37 1.39 5 5 0 3.74 1.04 -5 5 0 3.09 1.31 5 -5 0 3.79 1.27 5 5 1 0.92 1.42 5 -5 1 1.95 1.48 5 5 1 0.81 1.16 5 -5 1 0.13 1.13 5 5 1 0.49 0.69 5 5 2 25.44 2.23 5 -5 2 23.24 2.27 5 5 2 21.40 1.27 5 -5 2 20.58 1.71 5 5 3 1.85 1.84 5 -5 3 1.21 1.77 5 5 3 -0.41 0.91 5 -5 3 0.91 1.28 5 5 4 0.28 1.03 5 -5 4 -0.68 1.38 5 5 4 2.81 2.00 5 -5 4 2.04 2.04 5 -5 5 8.79 1.77 5 5 5 8.20 2.41 5 -5 5 4.09 2.23 5 -5 6 0.27 1.62 5 5 6 -0.15 2.61 5 -5 6 0.43 2.47 5 6 -10 3.70 2.58 5 -6 -10 3.41 2.51 5 -6 -9 2.18 2.31 5 6 -9 5.50 2.18 5 6 -8 7.05 1.92 5 -6 -8 9.51 1.93 5 -6 -7 17.40 2.09 5 6 -7 18.47 2.06 5 -6 -7 15.53 1.98 5 -6 -6 11.92 1.82 5 6 -6 18.18 1.90 5 -6 -6 17.17 1.85 5 6 -6 18.26 2.09 5 -6 -6 16.95 2.09 5 6 -5 142.47 5.29 5 -6 -5 143.57 5.28 -5 -6 5 140.76 5.62 -5 6 5 133.06 5.62 5 -6 -5 145.21 5.50 -5 -6 4 39.54 2.63 -5 6 4 32.21 2.61 5 -6 -4 34.55 2.17 5 6 -4 33.66 2.08 5 -6 -4 34.29 2.11 -5 -6 3 109.45 4.74 -5 6 3 107.52 4.79 5 -6 -3 103.77 4.27 5 6 -3 112.73 4.22 5 -6 -3 105.56 4.16 5 -6 -2 8.40 1.37 5 6 -2 8.65 1.37 5 -6 -2 7.44 1.35 -5 -6 2 10.54 2.09 -5 6 2 3.74 1.99 5 6 -1 -3.05 1.43 5 -6 -1 -1.79 1.38 5 -6 -1 -0.06 1.19 5 6 0 1.62 0.33 5 6 0 3.12 1.35 5 -6 0 4.17 1.36 5 -6 0 2.26 1.27 5 6 1 2.28 1.40 5 -6 1 2.91 1.47 5 -6 1 1.86 1.37 5 6 1 1.77 0.57 5 6 2 3.95 1.61 5 -6 2 4.04 1.71 5 -6 2 7.09 1.42 5 6 3 0.85 1.78 5 -6 3 -0.11 1.81 5 -6 3 2.29 1.32 5 -6 4 7.77 1.66 5 6 4 8.83 2.25 5 -6 4 6.02 2.19 5 -6 5 0.94 1.62 5 6 5 1.56 2.24 5 -6 5 -1.16 2.23 5 6 6 18.66 2.98 5 -6 6 13.80 2.89 5 7 -9 30.93 2.91 5 -7 -9 28.27 2.83 5 -7 -8 1.82 2.02 5 7 -8 5.70 1.87 5 -7 -8 4.09 1.86 5 -7 -7 3.06 1.76 5 7 -7 5.88 1.82 5 -7 -7 3.82 1.77 5 -7 -6 12.17 1.87 5 7 -6 20.40 1.92 5 -7 -6 20.03 1.90 5 7 -6 17.70 2.16 5 -7 -6 17.73 2.08 5 7 -5 3.60 1.68 5 -7 -5 1.11 1.43 5 7 -5 1.78 1.30 5 -7 -5 2.52 1.33 5 -7 -5 1.93 1.62 -5 7 4 -0.18 1.78 5 7 -4 -2.30 1.36 5 -7 -4 -2.90 1.35 5 -7 -4 -0.33 1.28 -5 -7 4 -0.09 1.65 -5 -7 3 41.62 2.84 -5 7 3 43.16 2.94 5 -7 -3 38.75 2.37 5 7 -3 44.21 2.26 5 -7 -3 44.45 2.27 5 -7 -2 0.45 1.25 5 7 -2 0.63 1.16 5 -7 -2 -0.90 1.16 5 -7 -1 2.77 1.34 5 7 -1 -0.77 1.37 5 -7 -1 -0.32 1.30 5 7 0 23.96 1.88 5 -7 0 26.61 1.98 5 -7 0 20.95 1.83 5 7 1 7.58 1.55 5 -7 1 8.28 1.68 5 -7 1 11.62 1.72 5 7 2 15.96 1.95 5 -7 2 11.64 1.93 5 -7 2 15.48 1.73 5 7 3 4.43 1.84 5 -7 3 3.44 1.95 5 -7 3 5.55 1.49 5 7 4 4.29 2.01 5 -7 4 5.01 2.18 5 -7 4 8.18 1.70 5 -7 5 13.37 1.98 5 7 5 11.76 2.46 5 -7 5 13.45 2.60 5 7 6 0.27 2.49 5 -7 6 2.36 2.57 5 8 -9 37.04 3.27 5 -8 -9 36.61 3.19 5 8 -8 11.24 2.11 5 -8 -8 11.63 2.12 5 -8 -7 7.13 2.04 5 8 -7 11.29 1.92 5 -8 -6 0.76 1.61 5 8 -6 2.07 1.61 5 -8 -6 2.70 1.58 5 8 -5 39.95 2.35 5 -8 -5 35.13 2.25 5 8 -5 39.48 2.50 5 -8 -5 38.81 2.45 5 8 -4 -0.81 1.33 5 -8 -4 0.16 1.32 5 -8 -4 1.91 1.41 -5 -8 4 1.89 1.75 -5 8 4 4.58 1.92 -5 -8 3 69.75 3.60 -5 8 3 60.65 3.56 5 -8 -3 63.99 3.15 5 8 -3 69.18 2.93 5 -8 -3 63.39 2.86 5 -8 -2 0.21 1.30 5 8 -2 -0.94 1.21 5 -8 -2 -1.23 1.18 5 -8 -1 31.59 2.16 5 8 -1 29.92 2.02 5 -8 -1 27.12 1.98 5 -8 0 53.14 2.89 5 8 0 57.71 2.87 5 -8 0 55.97 2.90 5 8 1 5.16 1.44 5 -8 1 5.26 1.52 5 8 2 2.62 1.52 5 -8 2 2.90 1.70 5 -8 2 3.13 1.55 5 8 3 12.59 1.98 5 -8 3 10.17 2.09 5 -8 3 13.62 1.79 5 8 4 1.61 1.87 5 -8 4 1.03 2.07 5 8 5 6.90 2.31 5 -8 5 5.24 2.41 5 8 6 45.29 3.48 5 -8 6 45.41 3.78 5 9 -9 3.41 2.48 5 -9 -9 2.39 2.44 5 9 -8 19.39 2.45 5 -9 -8 15.70 2.31 5 9 -7 7.49 1.86 5 -9 -7 6.50 1.78 5 9 -6 35.67 2.45 5 -9 -6 33.76 2.37 5 9 -5 25.17 2.04 5 -9 -5 24.03 1.98 5 9 -5 25.25 2.15 5 -9 -4 0.10 1.50 5 9 -4 -0.42 1.36 5 -9 -4 0.86 1.30 -5 9 4 -0.09 1.87 5 9 -3 -1.04 1.34 5 -9 -3 -0.71 1.33 -5 9 3 3.24 2.01 5 9 -2 25.41 1.75 5 -9 -2 24.51 1.72 5 9 -1 0.99 1.27 5 -9 -1 -0.11 1.20 5 9 0 32.22 2.18 5 -9 0 30.50 2.15 5 9 1 1.51 1.31 5 -9 1 3.79 1.45 5 9 2 13.56 1.72 5 -9 2 12.10 1.90 5 9 3 8.31 1.76 5 -9 3 4.67 1.88 5 9 4 1.29 1.83 5 -9 4 0.65 2.11 5 9 5 48.84 3.39 5 -9 5 53.12 3.87 5 -10 -6 -0.85 1.96 5 10 -6 4.62 1.82 5 -10 -5 1.05 1.73 5 10 -5 2.63 1.58 5 -10 -5 3.07 1.56 5 -10 -4 2.40 1.65 5 10 -4 3.50 1.45 5 -10 -4 4.16 1.40 5 10 -3 4.83 1.40 5 -10 -3 6.87 1.39 5 -10 -3 7.02 1.65 5 -10 -2 0.77 1.53 5 10 -2 1.92 1.19 5 -10 -2 3.97 1.20 5 -10 -1 20.34 1.63 5 10 -1 22.95 1.72 5 10 0 7.87 1.50 5 -10 0 7.60 1.49 5 -10 0 9.78 1.82 5 -10 1 77.58 3.94 5 10 1 87.63 3.74 5 -10 1 84.09 3.78 5 10 2 21.33 1.98 5 -10 2 21.92 2.43 5 -11 -5 23.10 2.48 5 -11 -4 54.05 3.22 5 -11 -3 19.45 2.13 5 -11 -2 26.08 2.25 5 -11 -1 7.55 1.77 5 -11 0 1.45 1.72 5 -11 1 -0.70 1.72 6 0 -10 37.31 3.55 6 0 -9 2.60 2.29 6 0 -8 2.54 2.01 6 0 -7 0.34 1.70 -6 0 6 222.50 7.65 6 0 -6 223.08 7.94 6 0 -5 -1.04 1.25 -6 0 5 -0.04 1.06 -6 0 4 95.58 3.70 6 0 -4 94.69 3.79 6 0 -3 1.00 1.06 -6 0 3 0.60 1.12 6 0 -2 3.78 1.06 -6 0 2 5.86 1.16 6 0 -1 0.77 1.01 -6 0 1 -0.19 1.09 -6 0 0 26.85 1.80 6 0 0 28.91 1.76 -6 0 -1 0.63 1.16 6 0 1 -0.92 1.18 -6 0 -2 0.83 1.21 6 0 2 2.44 1.17 6 0 3 1.36 1.26 6 0 4 199.75 7.19 6 0 5 -0.45 1.55 6 0 6 28.27 2.49 6 -1 -10 5.70 2.75 6 1 -10 2.07 2.50 6 -1 -9 5.15 2.37 6 1 -9 2.07 2.21 6 -1 -9 2.53 2.11 6 -1 -8 -0.69 1.98 6 1 -8 2.72 1.90 6 -1 -8 3.97 1.92 6 1 -8 -2.69 2.02 6 1 -7 16.44 2.06 6 -1 -7 18.64 2.12 6 -1 -7 17.93 2.15 6 1 -7 13.88 2.04 6 1 -6 3.23 1.61 6 -1 -6 4.57 1.69 6 -1 -6 6.79 1.59 6 1 -6 6.05 1.61 -6 -1 6 5.55 1.19 6 1 -5 3.26 1.38 6 -1 -5 5.10 1.44 6 -1 -5 1.38 1.32 6 1 -5 4.96 1.32 -6 -1 5 1.87 1.00 -6 1 5 2.04 1.08 -6 -1 4 35.17 1.90 -6 1 4 36.09 2.03 6 -1 -4 34.62 2.10 6 1 -4 35.48 2.25 6 -1 -4 41.67 2.33 6 1 -4 32.56 1.97 -6 -1 3 104.56 3.94 -6 1 3 108.96 4.11 6 -1 -3 103.60 4.05 6 1 -3 105.38 4.41 6 -1 -3 111.58 4.47 6 1 -3 103.51 3.95 6 -1 -2 0.10 1.03 6 1 -2 -0.87 0.94 6 1 -2 -1.97 1.54 6 -1 -2 -2.67 1.53 -6 -1 2 0.42 0.99 -6 1 2 0.05 1.10 -6 -1 1 37.33 1.96 -6 1 1 37.22 2.10 6 -1 -1 38.96 2.04 6 1 -1 32.57 1.86 6 1 -1 37.77 2.50 6 -1 -1 37.17 2.48 6 1 0 1.65 1.53 6 -1 0 0.83 1.46 -6 -1 0 0.32 1.05 -6 1 0 0.93 1.22 6 -1 0 1.53 1.15 6 1 0 0.74 1.01 6 1 1 1.51 1.65 6 -1 1 2.51 1.61 -6 -1 -1 4.74 1.18 -6 1 -1 4.56 1.34 6 -1 1 3.02 1.23 6 1 1 2.37 1.16 6 -1 2 1.22 1.75 -6 -1 -2 -0.10 1.16 6 1 2 1.43 1.06 6 -1 2 -0.06 1.12 6 1 3 1.02 2.09 6 -1 3 2.27 2.11 6 1 3 2.09 1.23 6 -1 3 -0.38 1.23 6 -1 4 0.70 2.26 6 1 4 2.34 1.41 6 -1 4 1.25 1.42 6 1 5 0.58 1.55 6 -1 5 -0.08 1.50 6 1 6 1.54 1.76 6 -1 6 0.17 1.78 6 -2 -10 -0.66 2.60 6 -2 -9 3.26 2.40 6 2 -9 8.81 2.32 6 2 -9 6.91 2.30 6 -2 -9 6.39 2.31 6 -2 -8 8.30 2.20 6 2 -8 9.46 2.07 6 -2 -8 9.60 2.12 6 2 -8 10.66 2.13 6 2 -7 1.28 1.74 6 -2 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4.50 6 -2 4 69.11 4.43 6 2 5 12.91 1.88 6 -2 5 10.43 1.87 6 -3 -9 20.14 2.86 6 3 -9 25.95 2.74 6 -3 -9 27.05 2.70 6 -3 -8 1.66 2.05 6 3 -8 3.47 1.95 6 -3 -8 3.08 1.95 6 3 -8 2.12 1.91 6 3 -7 3.92 1.75 6 -3 -7 6.04 1.81 6 -3 -7 1.56 1.74 6 3 -7 2.91 1.71 6 3 -6 0.83 1.54 6 -3 -6 2.03 1.59 6 -3 -6 2.79 1.56 6 3 -6 1.17 1.50 6 3 -5 56.44 2.77 6 -3 -5 57.21 2.94 6 3 -5 55.98 2.98 6 -3 -5 60.74 3.04 6 -3 -4 24.91 1.89 6 3 -4 29.63 2.06 6 -3 -4 27.46 2.01 6 3 -4 28.39 1.74 6 -3 -3 3.98 1.19 6 3 -3 3.44 1.02 6 3 -3 4.96 1.47 6 -3 -3 5.05 1.45 6 -3 -2 15.63 1.49 6 3 -2 10.88 1.11 6 3 -2 11.37 1.74 6 -3 -2 12.11 1.74 -6 3 2 13.65 1.58 6 3 -1 25.45 2.11 6 -3 -1 22.90 2.10 6 -3 -1 24.13 1.81 6 3 -1 24.01 1.37 6 3 0 2.81 1.62 6 -3 0 1.18 1.45 6 -3 0 1.71 1.23 6 3 0 1.72 0.86 6 3 1 13.65 1.98 6 -3 1 10.30 1.93 6 -3 1 11.44 1.63 6 3 1 9.56 1.22 6 3 2 20.63 2.37 6 -3 2 17.67 2.42 6 3 2 20.95 1.45 6 -3 2 20.85 1.81 6 3 3 0.25 2.00 6 -3 3 0.74 2.01 6 3 3 1.95 1.15 6 -3 3 1.15 1.36 6 3 4 32.74 3.24 6 -3 4 27.96 3.19 6 -3 4 27.97 2.21 6 -3 5 19.01 2.09 6 -4 -9 17.13 2.79 6 4 -9 25.64 2.70 6 -4 -9 20.78 2.58 6 -4 -8 5.14 2.14 6 4 -8 6.99 2.07 6 -4 -8 6.52 2.11 6 -4 -7 7.03 1.87 6 4 -7 7.86 1.91 6 -4 -7 11.39 1.94 6 4 -6 -1.11 1.54 6 -4 -6 -0.69 1.57 6 -4 -6 1.23 1.52 6 4 -5 7.16 1.67 6 -4 -5 9.49 1.70 6 -4 -5 8.67 1.61 6 4 -4 21.24 1.63 6 -4 -4 24.03 1.88 6 4 -4 27.04 1.96 6 -4 -4 24.91 1.91 6 -4 -3 2.28 1.23 6 4 -3 1.45 0.93 6 4 -3 1.54 1.34 6 -4 -3 0.49 1.32 6 -4 -2 76.83 3.30 6 4 -2 81.57 3.57 6 -4 -2 79.85 3.55 6 -4 -1 15.29 1.62 6 4 -1 17.04 1.98 6 -4 -1 16.04 1.95 6 4 -1 15.04 1.09 6 -4 0 76.60 3.34 6 4 0 67.31 2.72 6 4 0 81.39 3.72 6 -4 0 78.72 3.74 6 4 1 1.38 1.66 6 -4 1 0.79 1.61 6 -4 1 -1.47 1.48 6 4 2 3.28 1.83 6 -4 2 1.09 1.84 6 -4 2 4.82 1.48 6 4 3 -0.73 1.96 6 -4 3 0.12 2.03 6 -4 3 0.64 1.37 6 4 4 2.92 2.48 6 -4 4 1.88 2.36 6 -4 4 2.29 1.58 6 -5 -8 3.39 2.12 6 5 -8 5.81 2.11 6 -5 -8 4.13 2.11 6 5 -7 11.90 2.02 6 -5 -7 9.46 1.94 6 5 -6 4.76 1.67 6 -5 -6 3.31 1.60 6 -5 -6 3.54 1.68 6 5 -5 48.39 2.71 6 -5 -5 42.59 2.65 6 -5 -5 45.64 2.70 6 -5 -4 4.46 1.41 6 5 -4 5.50 1.41 6 -5 -4 4.82 1.42 6 -5 -3 10.65 1.51 6 5 -3 8.19 1.46 6 -5 -3 10.65 1.61 6 -5 -2 10.00 1.52 6 5 -2 11.79 1.74 6 -5 -2 9.23 1.66 6 -5 -1 12.78 1.59 6 5 -1 11.91 1.81 6 -5 -1 10.92 1.89 6 5 0 3.97 1.54 6 -5 0 3.93 1.58 6 -5 0 2.96 1.39 6 5 1 4.16 1.73 6 -5 1 5.10 1.76 6 -5 1 4.48 1.70 6 5 2 23.77 2.39 6 -5 2 20.52 2.43 6 -5 2 21.51 1.98 6 -5 3 34.24 3.05 6 -5 3 30.60 2.35 6 5 3 39.58 3.09 6 5 4 25.79 3.00 6 -5 4 24.59 2.98 6 -5 4 25.94 2.18 6 -6 -8 1.08 2.11 6 6 -8 3.07 2.15 6 -6 -8 5.76 2.16 6 -6 -7 9.88 2.05 6 6 -7 11.87 2.06 6 -6 -7 10.80 2.05 6 -6 -6 7.40 1.82 6 6 -6 8.91 1.84 6 -6 -6 7.46 1.77 6 6 -5 7.88 1.72 6 -6 -5 6.62 1.68 6 -6 -5 8.97 1.72 6 -6 -4 43.35 2.64 6 6 -4 48.63 2.59 6 -6 -4 50.01 2.64 6 -6 -3 30.00 2.14 6 6 -3 32.86 2.15 6 -6 -3 27.84 2.11 6 -6 -2 18.80 1.80 6 6 -2 16.57 1.85 6 -6 -2 12.74 1.79 6 -6 -1 17.42 1.79 6 6 -1 16.31 1.94 6 6 0 4.27 1.58 6 -6 0 5.22 1.69 6 -6 0 1.91 1.40 6 6 1 4.43 1.72 6 -6 1 3.48 1.72 6 -6 1 1.70 1.54 6 6 2 21.40 2.37 6 -6 2 19.20 2.45 6 -6 2 18.00 2.05 6 6 3 -0.57 1.99 6 -6 3 1.23 1.58 6 6 4 6.42 2.43 6 -6 4 1.54 2.30 6 7 -8 5.54 2.29 6 -7 -8 3.47 2.17 6 -7 -7 7.17 2.11 6 7 -7 13.91 2.14 6 -7 -7 12.11 2.10 6 -7 -6 2.90 1.82 6 7 -6 4.12 1.80 6 -7 -6 4.26 1.78 6 7 -5 3.25 1.62 6 -7 -5 3.66 1.60 6 -7 -5 6.48 1.75 6 7 -4 11.09 1.60 6 -7 -4 10.60 1.64 6 -7 -4 11.32 1.71 6 -7 -3 6.47 1.52 6 7 -3 5.81 1.46 6 -7 -3 5.08 1.42 6 -7 -2 1.92 1.45 6 7 -2 2.22 1.43 6 -7 -2 -0.07 1.41 6 -7 -1 9.87 1.71 6 7 -1 9.53 1.75 6 -7 -1 7.72 1.75 6 7 0 15.12 1.94 6 -7 0 10.01 1.88 6 -7 0 14.84 1.89 6 7 1 24.86 2.30 6 -7 1 25.41 2.43 6 -7 1 25.46 2.28 6 7 2 6.53 1.95 6 -7 2 5.29 1.98 6 -7 2 4.88 1.85 6 7 3 19.95 2.50 6 -7 3 16.31 2.52 6 7 4 13.81 2.57 6 -7 4 12.70 2.65 6 8 -8 6.64 2.22 6 -8 -8 8.32 2.24 6 8 -7 9.62 2.16 6 -8 -7 6.49 2.03 6 8 -6 28.35 2.40 6 -8 -6 26.28 2.31 6 8 -5 8.32 1.79 6 -8 -5 7.04 1.70 6 -8 -5 8.32 1.89 6 -8 -4 35.05 2.49 6 8 -4 35.94 2.43 6 -8 -4 33.88 2.38 6 -8 -3 13.87 1.90 6 8 -3 16.75 1.72 6 -8 -3 14.81 1.67 6 -8 -2 9.60 1.73 6 8 -2 5.18 1.51 6 -8 -2 7.32 1.53 6 -8 -1 3.76 1.69 6 8 -1 2.81 1.59 6 -8 -1 1.58 1.51 6 8 0 4.78 1.72 6 -8 0 4.51 1.80 6 -8 0 3.31 1.74 6 8 1 2.83 1.68 6 -8 1 3.55 1.77 6 -8 1 -1.22 1.69 6 8 2 3.75 1.86 6 -8 2 6.22 2.02 6 8 3 12.58 2.24 6 -8 3 10.60 2.38 6 9 -7 12.83 2.31 6 -9 -7 13.30 2.31 6 9 -6 6.61 2.02 6 -9 -6 2.91 1.90 6 9 -5 1.77 1.74 6 -9 -5 1.73 1.67 6 9 -4 31.85 2.32 6 -9 -4 29.41 2.30 6 -9 -4 29.90 2.45 6 9 -3 49.57 2.57 6 -9 -3 47.62 2.53 6 -9 -2 20.14 2.16 6 9 -2 20.96 1.92 6 -9 -2 19.15 1.87 6 -9 -1 10.59 1.90 6 9 -1 11.57 1.78 6 -9 -1 11.79 1.80 6 -9 0 -1.22 1.71 6 9 0 -1.50 1.73 6 -9 0 -1.19 1.75 6 -9 1 32.78 2.61 6 9 1 35.93 2.55 6 9 2 5.13 1.85 6 -9 2 5.01 1.99 6 9 3 2.18 1.92 7 0 -8 -0.70 2.14 7 0 -7 5.86 2.03 7 0 -6 3.56 1.68 7 0 -5 105.73 4.36 7 0 -4 0.35 1.33 7 0 -3 2.42 1.23 7 0 -2 -0.10 1.16 7 0 -1 24.07 1.77 7 0 0 0.17 1.20 7 0 1 8.42 1.54 7 0 2 1.50 1.55 7 0 3 0.80 1.48 7 -1 -9 6.16 2.64 7 -1 -8 -0.31 2.16 7 1 -7 -0.17 1.87 7 -1 -7 -2.00 1.88 7 -1 -7 1.17 1.86 7 -1 -6 1.46 1.61 7 1 -6 3.23 1.70 7 -1 -5 4.37 1.56 7 1 -5 7.08 1.56 7 1 -5 8.27 1.69 7 -1 -5 10.02 1.77 7 -1 -4 34.40 2.23 7 1 -4 37.04 2.42 7 -1 -4 37.26 2.45 7 -1 -3 18.17 1.71 7 1 -3 16.24 1.59 7 1 -3 16.89 2.01 7 -1 -3 20.91 2.06 7 -1 -2 19.83 1.72 7 1 -2 18.66 1.55 7 1 -2 18.57 2.20 7 -1 -2 17.67 2.21 7 -1 -1 5.49 1.36 7 1 -1 7.12 1.28 7 1 -1 3.75 1.84 7 -1 -1 4.85 1.90 7 1 0 5.19 1.31 7 1 0 8.62 2.04 7 -1 0 5.68 1.93 7 -1 0 3.81 1.36 7 -1 1 2.71 1.91 7 -1 1 2.88 1.43 7 -1 2 0.80 1.57 7 -1 3 1.69 1.46 7 -1 4 5.39 1.66 7 -2 -9 -0.48 2.53 7 -2 -8 5.67 2.39 7 2 -7 5.93 2.06 7 -2 -7 4.19 2.03 7 -2 -7 4.21 1.98 7 2 -6 1.30 1.85 7 -2 -6 3.34 1.89 7 -2 -6 6.74 1.81 7 2 -5 90.36 3.95 7 -2 -5 90.85 3.95 7 -2 -4 1.31 1.46 7 2 -4 0.16 1.49 7 -2 -4 1.28 1.45 7 -2 -3 1.27 1.31 7 2 -3 3.13 1.64 7 -2 -3 2.12 1.58 7 -2 -2 2.29 1.29 7 2 -2 -0.46 1.72 7 -2 -2 -1.29 1.70 7 -2 -1 19.17 1.76 7 2 -1 14.68 2.18 7 -2 -1 17.61 2.27 7 2 0 2.30 1.79 7 -2 0 1.15 1.81 7 -2 0 0.58 1.34 7 2 1 1.58 1.93 7 -2 1 2.26 1.94 7 -2 1 -1.23 1.49 7 -2 2 8.56 1.81 7 -2 3 6.23 1.70 7 -3 -8 28.43 3.08 7 3 -7 2.42 2.01 7 -3 -7 0.59 1.98 7 -3 -7 2.61 1.90 7 3 -6 0.57 1.88 7 -3 -6 3.08 1.83 7 -3 -6 4.37 1.78 7 3 -5 1.51 1.58 7 -3 -5 3.74 1.72 7 -3 -5 1.49 1.66 7 3 -4 59.38 3.06 7 -3 -4 63.70 3.16 7 -3 -3 12.32 1.67 7 3 -3 10.44 1.81 7 -3 -3 10.57 1.83 7 -3 -2 2.07 1.40 7 3 -2 -0.55 1.71 7 -3 -2 -2.57 1.85 7 -3 -1 12.41 1.64 7 3 -1 9.42 2.06 7 -3 -1 10.57 2.13 7 3 0 5.41 1.93 7 -3 0 2.84 1.89 7 -3 0 1.58 1.46 7 3 1 1.92 1.96 7 -3 1 0.23 1.93 7 -3 1 -0.73 1.51 7 -3 2 17.05 2.10 7 -3 3 14.82 1.98 7 -4 -7 17.36 2.40 7 4 -6 2.83 1.95 7 -4 -6 2.35 1.93 7 -4 -6 2.54 1.79 7 4 -5 2.32 1.71 7 -4 -5 1.60 1.86 7 -4 -5 4.62 1.71 7 -4 -4 1.93 1.51 7 4 -4 3.49 1.64 7 -4 -4 0.72 1.52 7 -4 -3 3.28 1.45 7 4 -3 2.74 1.68 7 -4 -3 1.74 1.59 7 -4 -2 15.52 1.81 7 4 -2 14.28 2.06 7 -4 -2 17.65 2.16 7 4 -1 34.22 2.76 7 -4 -1 37.37 2.33 7 4 0 7.69 1.96 7 -4 0 2.83 1.89 7 -4 0 1.90 1.50 7 4 1 3.89 2.00 7 -4 1 5.69 2.09 7 -4 1 -0.08 1.61 7 -4 2 14.55 2.19 7 -5 -7 1.49 2.08 7 5 -6 0.16 1.93 7 -5 -6 2.71 1.91 7 -5 -6 1.68 1.92 7 5 -5 2.23 1.89 7 -5 -5 3.19 1.88 7 -5 -4 45.51 2.83 7 5 -4 52.40 2.89 7 -5 -4 47.67 2.85 7 -5 -3 1.31 1.55 7 5 -3 -0.98 1.57 7 -5 -3 0.33 1.61 7 -5 -2 7.38 1.70 7 5 -2 5.69 1.82 7 -5 -2 10.56 2.02 7 -5 -1 3.75 1.57 7 5 -1 1.05 1.87 7 -5 -1 1.16 1.92 7 5 0 1.64 1.94 7 -5 0 -0.93 1.94 7 -5 0 2.40 1.60 7 5 1 4.81 2.07 7 -5 1 3.65 2.07 7 -5 1 2.01 1.67 7 6 -6 2.07 1.99 7 -6 -6 0.08 1.88 7 6 -5 10.42 2.08 7 -6 -5 7.04 2.02 7 -6 -5 12.42 2.10 7 6 -4 21.15 2.08 7 -6 -4 23.25 2.16 7 -6 -3 16.34 2.07 7 6 -3 20.36 2.10 7 -6 -2 8.92 1.77 7 6 -2 6.04 1.86 7 -6 -1 20.86 2.16 7 6 -1 20.17 2.37 7 -6 -1 20.98 2.41 7 6 0 10.04 2.24 7 -6 0 5.83 2.15 7 7 -5 -0.16 1.92 7 -7 -5 -2.72 2.00 7 7 -4 8.69 1.80 7 -7 -4 10.70 1.91 7 -7 -3 9.38 1.90 7 7 -3 15.39 1.95 7 -7 -3 11.96 1.93 7 -7 -2 47.61 2.96 7 7 -2 48.29 2.99 7 -7 -2 50.14 3.03 7 7 -1 -0.64 1.95 7 -7 -1 -0.74 1.98 7 7 0 5.50 2.10 7 -7 0 2.61 2.10 7 8 -5 -1.47 1.94 7 -8 -5 -1.51 1.95 7 8 -4 11.68 2.10 7 -8 -4 6.79 1.99 7 8 -3 3.63 1.73 7 -8 -3 2.14 1.69 7 8 -2 3.96 1.80 7 -8 -2 7.31 1.89 7 8 -1 2.99 1.93 7 -8 -1 6.50 1.99 7 8 0 7.12 2.12 7 -8 0 5.15 2.15 8 -2 -3 1.24 1.65 8 -3 -6 2.34 2.07 8 -3 -5 1.82 1.88 8 -3 -4 3.50 1.86 8 -3 -3 2.19 1.65 8 -3 -2 7.28 1.77 8 -3 -1 5.24 1.76 8 -3 0 1.60 1.72 8 -4 -3 1.78 1.76 0 0 0 0.00 0.00 TITL UMEX406_2 in P2(1)/n REM P2(1)/n (#14 in standard setting) CELL 0.71073 6.128602 12.466699 9.527078 90.0000 104.0440 90.0000 ZERR 2.00 0.000416 0.000800 0.000813 0.0000 0.0078 0.0000 LATT 1 SYMM -x+1/2, y+1/2,-z+1/2 SFAC C H N UNIT 28.00 40.00 8.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 30770