 
data_shelx
 
_audit_creation_method            SHELXL-2014
_chemical_name_systematic
;
 ?
;
_chemical_name_common             Ag-stellerite
_chemical_melting_point           ?
_chemical_formula_moiety          ?
_chemical_formula_sum
 'Ag14.57 O144 Si72' 
_chemical_formula_weight          5898.15

loop_
 _atom_type_symbol
 _atom_type_description
 _atom_type_scat_dispersion_real
 _atom_type_scat_dispersion_imag
 _atom_type_scat_source
 'O'  'O'   0.0106   0.0060
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Ag'  'Ag'  -0.8971   1.1015
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Si'  'Si'   0.0817   0.0704
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 
_space_group_crystal_system       orthorhombic
_space_group_IT_number            36
_space_group_name_H-M_alt         'A 21 m a'
_space_group_name_Hall            ?
 
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
 
loop_
 _space_group_symop_operation_xyz
 'x, y, z'
 'x+1/2, y, -z'
 'x+1/2, -y, -z'
 'x, -y, z'
 'x, y+1/2, z+1/2'
 'x+1/2, y+1/2, -z+1/2'
 'x+1/2, -y+1/2, -z+1/2'
 'x, -y+1/2, z+1/2'
 
_cell_length_a                    13.5218(12)
_cell_length_b                    17.1991(16)
_cell_length_c                    16.1640(16)
_cell_angle_alpha                 90
_cell_angle_beta                  90
_cell_angle_gamma                 90
_cell_volume                      3759.1(6)
_cell_formula_units_Z             1
_cell_measurement_temperature     573(2)
_cell_measurement_reflns_used     3267 
_cell_measurement_theta_min       2.3 
_cell_measurement_theta_max       22.7 
 
_exptl_crystal_description        'fragment' 
_exptl_crystal_colour             'grey-white' 
_exptl_crystal_density_meas       ? 
_exptl_crystal_density_method     ?              
_exptl_crystal_density_diffrn     2.605          
_exptl_crystal_F_000              2845
_exptl_transmission_factor_min    ?                                             
_exptl_transmission_factor_max    ?                                             
_exptl_crystal_size_max           0.120 
_exptl_crystal_size_mid           0.100 
_exptl_crystal_size_min           0.08 
_exptl_absorpt_coefficient_mu     2.563
_shelx_estimated_absorpt_T_min    ? 
_shelx_estimated_absorpt_T_max    ? 
_exptl_absorpt_correction_type    'multi-scan' 
_exptl_absorpt_correction_T_min   0.5395 
_exptl_absorpt_correction_T_max   0.7454 
_exptl_absorpt_process_details    ? 
 
_exptl_special_details
;
 ?
;
 
_diffrn_ambient_temperature       573(2)
_diffrn_radiation_wavelength      0.71073
_diffrn_radiation_type            MoK\a
_diffrn_source                    'fine-focus sealed tube'                       
_diffrn_measurement_device_type   'APEX II SMART' 
_diffrn_measurement_method        ? 
_diffrn_detector_area_resol_mean  ? 
_diffrn_reflns_number             25618
_diffrn_reflns_av_unetI/netI      0.0747
_diffrn_reflns_av_R_equivalents   0.1322
_diffrn_reflns_limit_h_min        -16
_diffrn_reflns_limit_h_max        16
_diffrn_reflns_limit_k_min        -21
_diffrn_reflns_limit_k_max        21
_diffrn_reflns_limit_l_min        -19
_diffrn_reflns_limit_l_max        20
_diffrn_reflns_theta_min          1.729
_diffrn_reflns_theta_max          26.369
_diffrn_reflns_theta_full         25.242
_diffrn_measured_fraction_theta_max   0.997
_diffrn_measured_fraction_theta_full  0.997
_diffrn_reflns_Laue_measured_fraction_max    0.997
_diffrn_reflns_Laue_measured_fraction_full   0.997
_diffrn_reflns_point_group_measured_fraction_max   0.995
_diffrn_reflns_point_group_measured_fraction_full  0.995
_reflns_number_total              3965
_reflns_number_gt                 2652
_reflns_threshold_expression      'I > 2σ(I)'
_reflns_Friedel_coverage          0.910
_reflns_Friedel_fraction_max      0.993
_reflns_Friedel_fraction_full     0.992
 
_reflns_special_details
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
 
_computing_data_collection        ?
_computing_cell_refinement        ?
_computing_data_reduction         ?
_computing_structure_solution     ?
_computing_structure_refinement   'SHELXL-2014 (Sheldrick, 2014)'
_computing_molecular_graphics     ?
_computing_publication_material   ?
 
_refine_special_details
;
 ?
;
_refine_ls_structure_factor_coef  Fsqd
_refine_ls_matrix_type            full
_refine_ls_weighting_scheme       calc
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.2000P)²] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary      direct
_atom_sites_solution_secondary    difmap
_atom_sites_solution_hydrogens    .
_refine_ls_hydrogen_treatment     undef
_refine_ls_extinction_method      SHELXL
_refine_ls_extinction_coef        0.012(2)
_refine_ls_extinction_expression
 'Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^'
_refine_ls_abs_structure_details
;
 Flack x determined using 1007 quotients [(I+)-(I-)]/[(I+)+(I-)]
 (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259).
;
_refine_ls_abs_structure_Flack    0.23(4)
_chemical_absolute_configuration  ?
_refine_ls_number_reflns          3965
_refine_ls_number_parameters      280
_refine_ls_number_restraints      1
_refine_ls_R_factor_all           0.1503
_refine_ls_R_factor_gt            0.1162
_refine_ls_wR_factor_ref          0.3343
_refine_ls_wR_factor_gt           0.2991
_refine_ls_goodness_of_fit_ref    1.233
_refine_ls_restrained_S_all       1.233
_refine_ls_shift/su_max           0.002
_refine_ls_shift/su_mean          0.000
 
loop_
 _atom_site_label
 _atom_site_type_symbol
 _atom_site_fract_x
 _atom_site_fract_y
 _atom_site_fract_z
 _atom_site_U_iso_or_equiv
 _atom_site_adp_type
 _atom_site_occupancy
 _atom_site_site_symmetry_order  
 _atom_site_calc_flag
 _atom_site_refinement_flags_posn
 _atom_site_refinement_flags_adp
 _atom_site_refinement_flags_occupancy
 _atom_site_disorder_assembly
 _atom_site_disorder_group
T1 Si 0.4466(5) 0.6818(5) 0.9578(4) 0.0533(18) Uani 0.789(11) 1 d . . P . .
T1D Si 0.427(3) 0.720(2) 0.894(2) 0.068(9) Uiso 0.211(11) 1 d . . P . .
T1A Si 0.6238(5) 0.5895(4) 0.1961(4) 0.0568(17) Uani 1 1 d . . . . .
T2 Si 0.5834(5) 0.8203(3) 0.0091(5) 0.0569(15) Uani 1 1 d . . . . .
T2A Si 0.5411(5) 0.5896(3) 0.8046(4) 0.0527(16) Uani 1 1 d . . . . .
T3 Si 0.917(3) 0.594(3) 0.873(3) 0.039(9) Uiso 0.106(6) 1 d . . P . .
T3N Si 0.9337(6) 0.6675(6) 0.8527(6) 0.063(2) Uani 0.789(11) 1 d . . P . .
T3ND Si 0.935(2) 0.6940(17) 0.7843(19) 0.012(6) Uiso 0.106(6) 1 d . . P . .
T3A Si 0.4410(5) 0.1454(5) 0.1422(5) 0.0479(18) Uani 0.789(11) 1 d . . P . .
T3AD Si 0.428(4) 0.089(3) 0.132(3) 0.090(12) Uiso 0.211(11) 1 d . . P . .
T4 Si 0.7324(6) 0.6939(5) 0.7881(5) 0.060(2) Uani 0.865(18) 1 d . . P . .
T4D Si 0.7267(18) 0.6720(15) 0.8554(16) 0.019(9) Uiso 0.135(18) 1 d . . P . .
T4A Si 0.7155(4) 0.8582(4) 0.8656(4) 0.0534(16) Uani 1 1 d . . . . .
T5 Si 0.7375(6) 0.7763(5) 0.6157(5) 0.0545(18) Uani 0.789(11) 1 d . . P . .
T5D Si 0.222(2) 0.6895(19) 0.9619(17) 0.0545(18) Uani 0.211(11) 1 d . . P . .
O2 O 0.6415(14) 0.8767(10) -0.0578(13) 0.075(5) Uani 1 1 d . . . . .
O3 O 0.569(3) 0.5000 0.822(3) 0.111(11) Uiso 1 2 d S . P . .
O4 O 0.771(2) 0.7284(16) 0.6974(15) 0.087(7) Uani 0.865(18) 1 d . . P . .
O5 O 0.7052(15) 0.7681(12) 0.8436(12) 0.073(5) Uiso 1 1 d . . . . .
O6 O 0.5126(14) 0.7658(12) -0.0403(13) 0.075(5) Uiso 1 1 d . . . . .
O7 O 0.617(2) 0.5000 0.164(2) 0.083(7) Uiso 1 2 d S . P . .
O8 O 0.6818(16) 0.9104(12) 0.7866(13) 0.078(5) Uiso 1 1 d . . . . .
O9 O 0.670(4) 0.767(3) 0.047(4) 0.089(16) Uiso 0.5 1 d . . P . .
O9A O 0.657(4) 0.718(3) 0.574(4) 0.093(16) Uiso 0.5 1 d . . P . .
O11 O 0.6417(15) 0.6372(13) 0.7804(13) 0.077(5) Uiso 1 1 d . . . . .
O12 O 0.688(2) 0.6374(17) 0.1345(17) 0.109(8) Uiso 1 1 d . . . . .
O13 O 0.495(2) 0.6222(16) 0.8907(16) 0.102(7) Uiso 1 1 d . . . . .
O14 O 0.4613(15) 0.5990(12) 0.7338(13) 0.078(5) Uiso 1 1 d . . . . .
O15 O 0.8288(16) 0.8828(10) 0.8877(11) 0.076(4) Uiso 1 1 d . . . . .
O16 O 0.334(2) 0.7050(14) 0.9386(16) 0.106(6) Uiso 1 1 d . . . . .
O17 O 0.4520(17) 0.6397(14) 1.0519(15) 0.069(6) Uiso 0.789(11) 1 d . . P . .
O18 O 0.5122(18) 0.6252(17) 0.2033(16) 0.099(7) Uiso 1 1 d . . . . .
O19 O 0.8242(18) 0.6437(11) 0.8238(12) 0.080(4) Uiso 1 1 d . . . . .
O20 O 0.5188(13) 0.8799(11) 0.0678(12) 0.070(5) Uiso 1 1 d . . . . .
OD1 O 1.008(3) 0.726(3) 0.691(3) 0.019(9) Uiso 0.211(11) 1 d . . P . .
OD4 O 0.710(5) 0.657(4) -0.046(4) 0.022(16) Uiso 0.135(18) 1 d . . P . .
OD3 O 0.9488(15) 0.7582(12) 0.8459(13) 0.078(5) Uiso 1 1 d . . . . .
Ag1 Ag 0.8294(7) 0.5000 0.275(2) 0.043(4) Uiso 0.35(4) 2 d S . . . .
Ag1B Ag 0.838(3) 0.5000 0.307(5) 0.071(13) Uiso 0.11(3) 2 d S . . . .
Ag1A Ag 0.8278(10) 0.5000 0.246(2) 0.058(5) Uiso 0.27(4) 2 d S . . . .
Ag1C Ag 0.846(10) 0.5000 0.175(8) 0.08(6) Uiso 0.025(16) 2 d S . . . .
Ag2 Ag 0.553(3) 0.0000 0.039(2) 0.045(14) Uiso 0.084(19) 2 d S . . . .
Ag2A Ag 0.794(5) 0.5000 0.108(5) 0.120 Uiso 0.072(13) 2 d S U . . .
Ag2B Ag 0.622(2) 1.0000 -0.0204(17) 0.111(12) Uiso 0.26(3) 2 d S . . . .
Ag2C Ag 0.604(2) 1.0000 0.0321(18) 0.061(12) Uiso 0.13(2) 2 d S . . . .
Ag2D Ag 0.511(6) 1.0000 -0.007(4) 0.16(3) Uiso 0.14(4) 2 d S . . . .
Ag2E Ag 0.573(2) 1.0000 -0.068(2) 0.147(15) Uiso 0.25(3) 2 d S . . . .
Ag2F Ag 0.5711(16) 1.0000 -0.0071(15) 0.053(9) Uiso 0.17(3) 2 d S . . . .
Ag3 Ag 0.761(7) 0.5000 0.772(11) 0.120 Uiso 0.06(2) 2 d S U . . .
Ag3A Ag 0.773(2) 0.5000 0.812(3) 0.076(15) Uiso 0.13(3) 2 d S . . . .
Ag4 Ag 0.999(3) 0.5000 -0.0217(17) 0.102(14) Uiso 0.18(3) 2 d S . . . .
Ag4A Ag 1.048(3) 0.5000 -0.0064(18) 0.112(15) Uiso 0.23(5) 2 d S . . . .
Ag4B Ag 1.073(4) 0.459(4) -0.015(3) 0.07(2) Uiso 0.044(14) 1 d . . . . .
AgO1 Ag 0.9691(14) 0.6980(13) 0.6754(9) 0.112(7) Uiso 0.28(2) 1 d . . . . .
AgO2 Ag 0.848(6) 0.5000 0.806(4) 0.150 Uiso 0.099(15) 2 d S U . . .
AgO3 Ag 0.9405(13) 0.6627(12) 0.6597(10) 0.093(7) Uiso 0.203(19) 1 d . . . . .
 
 
_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
 
loop_
 _geom_bond_atom_site_label_1
 _geom_bond_atom_site_label_2
 _geom_bond_distance
 _geom_bond_site_symmetry_2
 _geom_bond_publ_flag
T1 T1D 1.25(4) . ?
T1 O16 1.60(3) . ?
T1 O13 1.63(3) . ?
T1 O17 1.69(3) . ?
T1 O6 1.70(2) 1_556 ?
T1 AgO1 3.002(16) 7_466 ?
T1 Ag4B 3.10(5) 3_466 ?
T1D O16 1.46(5) . ?
T1D O6 1.75(4) 1_556 ?
T1D AgO1 1.89(4) 7_466 ?
T1D O13 1.92(5) . ?
T1D OD1 1.99(6) 7_466 ?
T1D AgO3 2.20(4) 7_466 ?
T1D T5 2.56(4) 7_466 ?
T1A O12 1.56(3) . ?
T1A O7 1.628(12) . ?
T1A O18 1.63(3) . ?
T1A O8 1.66(2) 8_564 ?
T2 O6 1.56(2) . ?
T2 O9A 1.59(6) 8_564 ?
T2 O9 1.62(6) . ?
T2 O20 1.65(2) . ?
T2 O2 1.652(18) . ?
T2 Ag2F 3.106(6) . ?
T2A O14 1.58(2) . ?
T2A O3 1.613(14) . ?
T2A O13 1.62(3) . ?
T2A O11 1.64(2) . ?
T2A Ag1C 3.07(11) 2_456 ?
T3 T3N 1.33(5) . ?
T3 O17 1.53(5) 2_557 ?
T3 O19 1.71(5) . ?
T3 O18 1.86(5) 2_556 ?
T3 AgO2 2.15(7) . ?
T3 T3ND 2.26(5) . ?
T3 Ag4 2.60(5) 1_556 ?
T3 Ag3A 2.71(5) . ?
T3 Ag4B 2.93(7) 4_566 ?
T3 Ag4A 3.09(6) 1_556 ?
T3 Ag3 3.11(14) . ?
T3N T3ND 1.20(3) . ?
T3N O18 1.57(3) 2_556 ?
T3N OD3 1.58(2) . ?
T3N O19 1.61(3) . ?
T3N O17 1.63(3) 2_557 ?
T3N T4D 2.80(2) . ?
T3N AgO1 2.952(16) . ?
T3ND OD3 1.50(4) . ?
T3ND O18 1.59(4) 2_556 ?
T3ND AgO1 1.82(3) . ?
T3ND O19 1.85(4) . ?
T3ND OD1 1.88(5) . ?
T3ND AgO3 2.09(4) . ?
T3ND T4 2.74(3) . ?
T3A T3AD 1.01(5) . ?
T3A O20 1.66(2) 4_565 ?
T3A O15 1.66(2) 3_466 ?
T3A OD3 1.67(2) 3_466 ?
T3A O14 1.70(2) 5_544 ?
T3A Ag1B 2.98(4) 6_445 ?
T3AD O15 1.46(5) 3_466 ?
T3AD O20 1.70(5) 4_565 ?
T3AD O14 1.72(6) 5_544 ?
T3AD Ag1B 2.19(8) 6_445 ?
T3AD Ag1 2.52(6) 6_445 ?
T3AD Ag2 2.73(6) . ?
T3AD Ag1A 2.83(6) 6_445 ?
T3AD Ag2D 2.93(8) 1_545 ?
T4 T4D 1.15(3) . ?
T4 O11 1.57(2) . ?
T4 O5 1.60(2) . ?
T4 O19 1.62(2) . ?
T4 O4 1.67(3) . ?
T4D O19 1.49(3) . ?
T4D OD4 1.63(7) 1_556 ?
T4D O5 1.69(3) . ?
T4D O11 1.78(3) . ?
T4D Ag3A 3.10(3) . ?
T4A O5 1.60(2) . ?
T4A O2 1.624(18) 1_556 ?
T4A O8 1.63(2) . ?
T4A O15 1.63(2) . ?
T4A Ag1B 3.09(2) 5 ?
T5 T5D 1.40(3) 7_566 ?
T5 O16 1.61(3) 7_566 ?
T5 O9 1.61(6) 8_565 ?
T5 O4 1.62(2) . ?
T5 O9A 1.62(6) . ?
T5 O12 1.65(3) 8_565 ?
T5 T1D 2.56(4) 7_566 ?
T5D T5 1.40(3) 7_466 ?
T5D OD4 1.49(8) 2_456 ?
T5D O9 1.51(7) 2_456 ?
T5D O16 1.58(4) . ?
T5D O12 1.85(4) 2_456 ?
T5D O9A 1.91(7) 7_466 ?
O2 T4A 1.624(18) 1_554 ?
O2 Ag2B 2.220(19) . ?
O2 Ag2E 2.32(2) . ?
O2 Ag2F 2.46(2) . ?
O3 T2A 1.613(14) 4_565 ?
O6 T1 1.70(2) 1_554 ?
O6 T1D 1.75(4) 1_554 ?
O6 AgO1 2.35(3) 7_465 ?
O6 AgO3 2.49(3) 7_465 ?
O7 T1A 1.628(12) 4_565 ?
O7 Ag2A 2.56(8) . ?
O7 Ag4B 2.58(6) 2_455 ?
O7 Ag4B 2.58(6) 3_465 ?
O8 T1A 1.66(2) 8_565 ?
O8 Ag1 2.53(2) 5 ?
O8 Ag1A 2.59(3) 5 ?
O9 O9A 0.53(8) 8_564 ?
O9 T5D 1.51(7) 2_556 ?
O9 T5 1.61(6) 8_564 ?
O9A O9 0.53(8) 8_565 ?
O9A T2 1.59(6) 8_565 ?
O9A T5D 1.91(7) 7_566 ?
O12 T5 1.65(3) 8_564 ?
O12 T5D 1.85(4) 2_556 ?
O14 T3A 1.70(2) 5 ?
O14 T3AD 1.72(6) 5 ?
O14 Ag1 2.47(2) 2_456 ?
O14 Ag1B 2.48(3) 2_456 ?
O14 Ag1A 2.50(2) 2_456 ?
O15 T3AD 1.46(5) 3_566 ?
O15 T3A 1.66(2) 3_566 ?
O15 Ag1B 2.40(5) 5 ?
O16 T5 1.61(3) 7_466 ?
O17 T3 1.53(5) 2_457 ?
O17 T3N 1.63(3) 2_457 ?
O17 Ag4B 2.43(6) 3_466 ?
O17 Ag4 2.53(3) 2_456 ?
O18 T3N 1.57(3) 2_456 ?
O18 T3ND 1.59(4) 2_456 ?
O18 T3 1.86(5) 2_456 ?
O18 AgO1 2.40(3) 2_456 ?
O18 AgO3 2.50(3) 2_456 ?
O19 AgO2 2.51(2) . ?
O19 Ag3A 2.58(2) . ?
O20 T3A 1.66(2) 4_565 ?
O20 T3AD 1.70(5) 4_565 ?
O20 Ag2 2.17(2) 1_565 ?
O20 Ag2D 2.39(4) . ?
O20 Ag2C 2.43(3) . ?
O20 Ag2F 2.50(2) . ?
OD1 AgO1 0.76(4) . ?
OD1 AgO3 1.51(5) . ?
OD1 T1D 1.99(6) 7_566 ?
OD4 T5D 1.49(8) 2_556 ?
OD4 T4D 1.63(7) 1_554 ?
OD3 T3A 1.67(2) 3_566 ?
Ag1 Ag1B 0.53(6) . ?
Ag1 Ag1C 1.62(13) . ?
Ag1 O14 2.47(2) 2_556 ?
Ag1 O14 2.47(2) 3_566 ?
Ag1 T3AD 2.52(6) 6 ?
Ag1 T3AD 2.52(6) 7 ?
Ag1 O8 2.53(2) 5_544 ?
Ag1 O8 2.53(2) 8_564 ?
Ag1 Ag2A 2.73(9) . ?
Ag1B Ag1A 0.99(8) . ?
Ag1B Ag1C 2.13(14) . ?
Ag1B T3AD 2.19(8) 6 ?
Ag1B T3AD 2.19(8) 7 ?
Ag1B O15 2.40(5) 8_564 ?
Ag1B O15 2.40(5) 5_544 ?
Ag1B O14 2.47(3) 2_556 ?
Ag1B O14 2.47(3) 3_566 ?
Ag1B T3A 2.98(4) 6 ?
Ag1B T3A 2.98(4) 7 ?
Ag1B T4A 3.09(2) 5_544 ?
Ag1A Ag1C 1.17(13) . ?
Ag1A Ag2A 2.27(9) . ?
Ag1A O14 2.50(2) 2_556 ?
Ag1A O14 2.50(2) 3_566 ?
Ag1A O8 2.59(3) 5_544 ?
Ag1A O8 2.59(3) 8_564 ?
Ag1A T3AD 2.83(6) 6 ?
Ag1A T3AD 2.83(6) 7 ?
Ag1C Ag2A 1.29(15) . ?
Ag1C T2A 3.07(11) 2_556 ?
Ag1C T2A 3.07(11) 3_566 ?
Ag2 Ag2C 0.69(3) 1_545 ?
Ag2 Ag2F 0.78(3) 1_545 ?
Ag2 Ag2D 0.92(8) 1_545 ?
Ag2 Ag2B 1.34(4) 1_545 ?
Ag2 Ag2E 1.75(5) 1_545 ?
Ag2 O20 2.17(2) 4_565 ?
Ag2 O20 2.17(2) 1_545 ?
Ag2 T3AD 2.73(6) 4 ?
Ag2B Ag2F 0.72(3) . ?
Ag2B Ag2C 0.88(3) . ?
Ag2B Ag2E 1.01(3) . ?
Ag2B Ag2 1.34(5) 1_565 ?
Ag2B Ag2D 1.51(9) . ?
Ag2B O2 2.220(19) 4_575 ?
Ag2C Ag2 0.69(3) 1_565 ?
Ag2C Ag2F 0.77(3) . ?
Ag2C Ag2D 1.40(9) . ?
Ag2C Ag2E 1.67(5) . ?
Ag2C O20 2.43(3) 4_575 ?
Ag2D Ag2F 0.81(8) . ?
Ag2D Ag2 0.92(8) 1_565 ?
Ag2D Ag2E 1.30(7) . ?
Ag2D O20 2.39(4) 4_575 ?
Ag2D T3AD 2.93(8) 1_565 ?
Ag2D T3AD 2.93(8) 4_565 ?
Ag2E Ag2F 0.98(4) . ?
Ag2E Ag2 1.75(5) 1_565 ?
Ag2E O2 2.32(2) 4_575 ?
Ag2F Ag2 0.78(3) 1_565 ?
Ag2F O2 2.46(2) 4_575 ?
Ag2F O20 2.50(2) 4_575 ?
Ag2F T2 3.106(6) 4_575 ?
Ag3 Ag3A 0.66(14) . ?
Ag3 AgO2 1.30(16) . ?
Ag3 T3 3.11(14) 4_565 ?
Ag3A AgO2 1.03(9) . ?
Ag3A O19 2.58(2) 4_565 ?
Ag3A T3 2.71(5) 4_565 ?
Ag3A T4D 3.10(3) 4_565 ?
Ag4 Ag4A 0.71(3) . ?
Ag4 Ag4B 1.24(8) 4_565 ?
Ag4 Ag4B 1.24(8) . ?
Ag4 O17 2.53(3) 3_566 ?
Ag4 O17 2.53(3) 2_556 ?
Ag4 T3 2.60(5) 4_564 ?
Ag4 T3 2.60(5) 1_554 ?
Ag4A Ag4B 0.80(6) 4_565 ?
Ag4A Ag4B 0.80(6) . ?
Ag4A T3 3.09(6) 4_564 ?
Ag4A T3 3.09(6) 1_554 ?
Ag4B Ag4B 1.42(12) 4_565 ?
Ag4B O17 2.43(6) 3_566 ?
Ag4B O7 2.58(6) 2 ?
Ag4B T3 2.93(7) 4_564 ?
Ag4B T1 3.10(5) 3_566 ?
AgO1 AgO3 0.763(17) . ?
AgO1 T1D 1.89(4) 7_566 ?
AgO1 O6 2.35(3) 7_565 ?
AgO1 O18 2.40(3) 2_556 ?
AgO1 T1 3.001(16) 7_566 ?
AgO2 T3 2.15(7) 4_565 ?
AgO2 O19 2.51(2) 4_565 ?
AgO3 T1D 2.20(4) 7_566 ?
AgO3 O6 2.49(3) 7_565 ?
AgO3 O18 2.50(3) 2_556 ?
 
loop_
 _geom_angle_atom_site_label_1
 _geom_angle_atom_site_label_2
 _geom_angle_atom_site_label_3
 _geom_angle
 _geom_angle_site_symmetry_1
 _geom_angle_site_symmetry_3
 _geom_angle_publ_flag
T1D T1 O16 60(2) . . ?
T1D T1 O13 82.7(19) . . ?
O16 T1 O13 114.1(14) . . ?
T1D T1 O17 168(2) . . ?
O16 T1 O17 108.9(13) . . ?
O13 T1 O17 108.3(14) . . ?
T1D T1 O6 71.1(19) . 1_556 ?
O16 T1 O6 106.8(13) . 1_556 ?
O13 T1 O6 109.7(13) . 1_556 ?
O17 T1 O6 109.1(11) . 1_556 ?
T1D T1 AgO1 21.3(18) . 7_466 ?
O16 T1 AgO1 77.6(10) . 7_466 ?
O13 T1 AgO1 85.1(11) . 7_466 ?
O17 T1 AgO1 159.8(10) . 7_466 ?
O6 T1 AgO1 51.2(8) 1_556 7_466 ?
T1D T1 Ag4B 140.9(19) . 3_466 ?
O16 T1 Ag4B 140.8(15) . 3_466 ?
O13 T1 Ag4B 59.2(13) . 3_466 ?
O17 T1 Ag4B 51.1(12) . 3_466 ?
O6 T1 Ag4B 111.6(13) 1_556 3_466 ?
AgO1 T1 Ag4B 134.1(11) 7_466 3_466 ?
T1 T1D O16 72(2) . . ?
T1 T1D O6 66.4(19) . 1_556 ?
O16 T1D O6 111(3) . 1_556 ?
T1 T1D AgO1 145(3) . 7_466 ?
O16 T1D AgO1 133(3) . 7_466 ?
O6 T1D AgO1 80.0(18) 1_556 7_466 ?
T1 T1D O13 57.1(17) . . ?
O16 T1D O13 105(2) . . ?
O6 T1D O13 95(2) 1_556 . ?
AgO1 T1D O13 119(2) 7_466 . ?
T1 T1D OD1 134(3) . 7_466 ?
O16 T1D OD1 153(3) . 7_466 ?
O6 T1D OD1 81(2) 1_556 7_466 ?
AgO1 T1D OD1 22.5(13) 7_466 7_466 ?
O13 T1D OD1 97(2) . 7_466 ?
T1 T1D AgO3 142(3) . 7_466 ?
O16 T1D AgO3 115(2) . 7_466 ?
O6 T1D AgO3 77.0(16) 1_556 7_466 ?
AgO1 T1D AgO3 19.7(7) 7_466 7_466 ?
O13 T1D AgO3 139(2) . 7_466 ?
OD1 T1D AgO3 42.0(16) 7_466 7_466 ?
T1 T1D T5 106(2) . 7_466 ?
O16 T1D T5 35.3(14) . 7_466 ?
O6 T1D T5 133(2) 1_556 7_466 ?
AgO1 T1D T5 104.4(18) 7_466 7_466 ?
O13 T1D T5 120(2) . 7_466 ?
OD1 T1D T5 120(2) 7_466 7_466 ?
AgO3 T1D T5 92.2(15) 7_466 7_466 ?
O12 T1A O7 109.1(16) . . ?
O12 T1A O18 111.4(15) . . ?
O7 T1A O18 109.0(15) . . ?
O12 T1A O8 107.3(13) . 8_564 ?
O7 T1A O8 108.1(14) . 8_564 ?
O18 T1A O8 111.9(13) . 8_564 ?
O6 T2 O9A 118(2) . 8_564 ?
O6 T2 O9 108(2) . . ?
O9A T2 O9 19(3) 8_564 . ?
O6 T2 O20 110.1(11) . . ?
O9A T2 O20 102(3) 8_564 . ?
O9 T2 O20 121(2) . . ?
O6 T2 O2 108.1(12) . . ?
O9A T2 O2 112(2) 8_564 . ?
O9 T2 O2 104(2) . . ?
O20 T2 O2 105.3(8) . . ?
O6 T2 Ag2F 121.5(9) . . ?
O9A T2 Ag2F 120(2) 8_564 . ?
O9 T2 Ag2F 129(2) . . ?
O20 T2 Ag2F 53.2(8) . . ?
O2 T2 Ag2F 52.1(8) . . ?
O14 T2A O3 112.6(16) . . ?
O14 T2A O13 108.9(13) . . ?
O3 T2A O13 105.8(18) . . ?
O14 T2A O11 110.1(11) . . ?
O3 T2A O11 108.8(17) . . ?
O13 T2A O11 110.6(12) . . ?
O14 T2A Ag1C 63(3) . 2_456 ?
O3 T2A Ag1C 73(2) . 2_456 ?
O13 T2A Ag1C 76(2) . 2_456 ?
O11 T2A Ag1C 172(3) . 2_456 ?
T3N T3 O17 69(2) . 2_557 ?
T3N T3 O19 62.3(19) . . ?
O17 T3 O19 109(3) 2_557 . ?
T3N T3 O18 56.0(19) . 2_556 ?
O17 T3 O18 99(3) 2_557 2_556 ?
O19 T3 O18 93(2) . 2_556 ?
T3N T3 AgO2 132(3) . . ?
O17 T3 AgO2 157(3) 2_557 . ?
O19 T3 AgO2 80(3) . . ?
O18 T3 AgO2 101(3) 2_556 . ?
T3N T3 T3ND 25.3(14) . . ?
O17 T3 T3ND 94(2) 2_557 . ?
O19 T3 T3ND 53.5(16) . . ?
O18 T3 T3ND 44.1(15) 2_556 . ?
AgO2 T3 T3ND 108(3) . . ?
T3N T3 Ag4 133(3) . 1_556 ?
O17 T3 Ag4 70.3(19) 2_557 1_556 ?
O19 T3 Ag4 158(3) . 1_556 ?
O18 T3 Ag4 109(2) 2_556 1_556 ?
AgO2 T3 Ag4 93(2) . 1_556 ?
T3ND T3 Ag4 148(2) . 1_556 ?
T3N T3 Ag3A 127(3) . . ?
O17 T3 Ag3A 145(3) 2_557 . ?
O19 T3 Ag3A 66.9(16) . . ?
O18 T3 Ag3A 116(2) 2_556 . ?
AgO2 T3 Ag3A 21(2) . . ?
T3ND T3 Ag3A 108(2) . . ?
Ag4 T3 Ag3A 100.3(18) 1_556 . ?
T3N T3 Ag4B 108(3) . 4_566 ?
O17 T3 Ag4B 56(2) 2_557 4_566 ?
O19 T3 Ag4B 165(3) . 4_566 ?
O18 T3 Ag4B 90(2) 2_556 4_566 ?
AgO2 T3 Ag4B 113(3) . 4_566 ?
T3ND T3 Ag4B 123(2) . 4_566 ?
Ag4 T3 Ag4B 25.0(17) 1_556 4_566 ?
Ag3A T3 Ag4B 124(2) . 4_566 ?
T3N T3 Ag4A 123(3) . 1_556 ?
O17 T3 Ag4A 65.6(18) 2_557 1_556 ?
O19 T3 Ag4A 167(2) . 1_556 ?
O18 T3 Ag4A 100(2) 2_556 1_556 ?
AgO2 T3 Ag4A 100(2) . 1_556 ?
T3ND T3 Ag4A 137(2) . 1_556 ?
Ag4 T3 Ag4A 10.3(7) 1_556 1_556 ?
Ag3A T3 Ag4A 109.5(16) . 1_556 ?
Ag4B T3 Ag4A 15.0(13) 4_566 1_556 ?
T3N T3 Ag3 119(3) . . ?
O17 T3 Ag3 154(3) 2_557 . ?
O19 T3 Ag3 62(2) . . ?
O18 T3 Ag3 106(3) 2_556 . ?
AgO2 T3 Ag3 20(2) . . ?
T3ND T3 Ag3 98(3) . . ?
Ag4 T3 Ag3 108(2) 1_556 . ?
Ag3A T3 Ag3 10(2) . . ?
Ag4B T3 Ag3 131(2) 4_566 . ?
Ag4A T3 Ag3 117(2) 1_556 . ?
T3ND T3N T3 126(3) . . ?
T3ND T3N O18 68.4(18) . 2_556 ?
T3 T3N O18 79(2) . 2_556 ?
T3ND T3N OD3 63.7(17) . . ?
T3 T3N OD3 170(2) . . ?
O18 T3N OD3 109.3(14) 2_556 . ?
T3ND T3N O19 81.1(17) . . ?
T3 T3N O19 71(2) . . ?
O18 T3N O19 109.8(13) 2_556 . ?
OD3 T3N O19 110.5(11) . . ?
T3ND T3N O17 168.9(18) . 2_557 ?
T3 T3N O17 61(2) . 2_557 ?
O18 T3N O17 107.9(14) 2_556 2_557 ?
OD3 T3N O17 109.5(13) . 2_557 ?
O19 T3N O17 109.8(12) . 2_557 ?
T3ND T3N T4D 91.3(16) . . ?
T3 T3N T4D 81(2) . . ?
O18 T3N T4D 134.2(12) 2_556 . ?
OD3 T3N T4D 95.9(11) . . ?
O19 T3N T4D 24.5(9) . . ?
O17 T3N T4D 98.3(11) 2_557 . ?
T3ND T3N AgO1 14.6(14) . . ?
T3 T3N AgO1 116(2) . . ?
O18 T3N AgO1 54.1(10) 2_556 . ?
OD3 T3N AgO1 74.7(10) . . ?
O19 T3N AgO1 85.0(9) . . ?
O17 T3N AgO1 160.7(10) 2_557 . ?
T4D T3N AgO1 99.9(7) . . ?
T3N T3ND OD3 70.7(18) . . ?
T3N T3ND O18 67.1(17) . 2_556 ?
OD3 T3ND O18 113(2) . 2_556 ?
T3N T3ND AgO1 156(2) . . ?
OD3 T3ND AgO1 126(2) . . ?
O18 T3ND AgO1 89.2(17) 2_556 . ?
T3N T3ND O19 59.1(15) . . ?
OD3 T3ND O19 102.3(19) . . ?
O18 T3ND O19 98.1(19) 2_556 . ?
AgO1 T3ND O19 123.8(19) . . ?
T3N T3ND OD1 150(3) . . ?
OD3 T3ND OD1 104(2) . . ?
O18 T3ND OD1 89(2) 2_556 . ?
AgO1 T3ND OD1 23.7(14) . . ?
O19 T3ND OD1 147(3) . . ?
T3N T3ND AgO3 143(2) . . ?
OD3 T3ND AgO3 146(2) . . ?
O18 T3ND AgO3 84.7(16) 2_556 . ?
AgO1 T3ND AgO3 21.1(7) . . ?
O19 T3ND AgO3 103.9(16) . . ?
OD1 T3ND AgO3 44.5(17) . . ?
T3N T3ND T3 28.5(15) . . ?
OD3 T3ND T3 99(2) . . ?
O18 T3ND T3 54.7(17) 2_556 . ?
AgO1 T3ND T3 132(2) . . ?
O19 T3ND T3 48.0(14) . . ?
OD1 T3ND T3 142(2) . . ?
AgO3 T3ND T3 114.7(19) . . ?
T3N T3ND T4 87.7(16) . . ?
OD3 T3ND T4 96.1(16) . . ?
O18 T3ND T4 130.6(19) 2_556 . ?
AgO1 T3ND T4 105.8(15) . . ?
O19 T3ND T4 34.8(8) . . ?
OD1 T3ND T4 123(2) . . ?
AgO3 T3ND T4 93.2(12) . . ?
T3 T3ND T4 82.7(15) . . ?
T3AD T3A O20 75(3) . 4_565 ?
T3AD T3A O15 61(3) . 3_466 ?
O20 T3A O15 106.9(10) 4_565 3_466 ?
T3AD T3A OD3 173(3) . 3_466 ?
O20 T3A OD3 107.7(11) 4_565 3_466 ?
O15 T3A OD3 112.4(10) 3_466 3_466 ?
T3AD T3A O14 73(3) . 5_544 ?
O20 T3A O14 113.9(10) 4_565 5_544 ?
O15 T3A O14 105.2(10) 3_466 5_544 ?
OD3 T3A O14 110.8(11) 3_466 5_544 ?
T3AD T3A Ag1B 32(3) . 6_445 ?
O20 T3A Ag1B 106.1(15) 4_565 6_445 ?
O15 T3A Ag1B 53.7(10) 3_466 6_445 ?
OD3 T3A Ag1B 146.1(15) 3_466 6_445 ?
O14 T3A Ag1B 56.1(14) 5_544 6_445 ?
T3A T3AD O15 83(3) . 3_466 ?
T3A T3AD O20 70(3) . 4_565 ?
O15 T3AD O20 115(3) 3_466 4_565 ?
T3A T3AD O14 72(3) . 5_544 ?
O15 T3AD O14 115(3) 3_466 5_544 ?
O20 T3AD O14 111(3) 4_565 5_544 ?
T3A T3AD Ag1B 134(4) . 6_445 ?
O15 T3AD Ag1B 80(2) 3_466 6_445 ?
O20 T3AD Ag1B 154(3) 4_565 6_445 ?
O14 T3AD Ag1B 78(3) 5_544 6_445 ?
T3A T3AD Ag1 125(4) . 6_445 ?
O15 T3AD Ag1 81(2) 3_466 6_445 ?
O20 T3AD Ag1 160(3) 4_565 6_445 ?
O14 T3AD Ag1 68.2(19) 5_544 6_445 ?
Ag1B T3AD Ag1 10.1(15) 6_445 6_445 ?
T3A T3AD Ag2 121(4) . . ?
O15 T3AD Ag2 129(3) 3_466 . ?
O20 T3AD Ag2 52.5(16) 4_565 . ?
O14 T3AD Ag2 115(2) 5_544 . ?
Ag1B T3AD Ag2 102(2) 6_445 . ?
Ag1 T3AD Ag2 108.7(19) 6_445 . ?
T3A T3AD Ag1A 119(4) . 6_445 ?
O15 T3AD Ag1A 84(2) 3_466 6_445 ?
O20 T3AD Ag1A 160(3) 4_565 6_445 ?
O14 T3AD Ag1A 61.0(17) 5_544 6_445 ?
Ag1B T3AD Ag1A 17.4(18) 6_445 6_445 ?
Ag1 T3AD Ag1A 7.3(4) 6_445 6_445 ?
Ag2 T3AD Ag1A 112.3(18) . 6_445 ?
T3A T3AD Ag2D 124(4) . 1_545 ?
O15 T3AD Ag2D 111(3) 3_466 1_545 ?
O20 T3AD Ag2D 54.6(19) 4_565 1_545 ?
O14 T3AD Ag2D 133(3) 5_544 1_545 ?
Ag1B T3AD Ag2D 101(3) 6_445 1_545 ?
Ag1 T3AD Ag2D 110(2) 6_445 1_545 ?
Ag2 T3AD Ag2D 18.3(16) . 1_545 ?
Ag1A T3AD Ag2D 116(2) 6_445 1_545 ?
T4D T4 O11 79.7(15) . . ?
T4D T4 O5 73.5(15) . . ?
O11 T4 O5 111.1(12) . . ?
T4D T4 O19 62.7(15) . . ?
O11 T4 O19 107.2(11) . . ?
O5 T4 O19 113.7(11) . . ?
T4D T4 O4 165.4(17) . . ?
O11 T4 O4 113.2(12) . . ?
O5 T4 O4 106.3(13) . . ?
O19 T4 O4 105.4(13) . . ?
T4D T4 T3ND 95.1(15) . . ?
O11 T4 T3ND 141.1(11) . . ?
O5 T4 T3ND 104.0(11) . . ?
O19 T4 T3ND 40.7(10) . . ?
O4 T4 T3ND 70.6(12) . . ?
T4 T4D O19 74.0(16) . . ?
T4 T4D OD4 170(3) . 1_556 ?
O19 T4D OD4 114(3) . 1_556 ?
T4 T4D O5 65.6(15) . . ?
O19 T4D O5 115.6(19) . . ?
OD4 T4D O5 104(3) 1_556 . ?
T4 T4D O11 60.6(13) . . ?
O19 T4D O11 103.1(18) . . ?
OD4 T4D O11 121(3) 1_556 . ?
O5 T4D O11 98.1(16) . . ?
T4 T4D T3N 85.8(14) . . ?
O19 T4D T3N 26.4(10) . . ?
OD4 T4D T3N 99(3) 1_556 . ?
O5 T4D T3N 101.4(14) . . ?
O11 T4D T3N 128.8(14) . . ?
T4 T4D Ag3A 94.7(17) . . ?
O19 T4D Ag3A 55.6(13) . . ?
OD4 T4D Ag3A 95(3) 1_556 . ?
O5 T4D Ag3A 160.2(18) . . ?
O11 T4D Ag3A 69.6(13) . . ?
T3N T4D Ag3A 76.7(9) . . ?
O5 T4A O2 107.9(11) . 1_556 ?
O5 T4A O8 109.7(11) . . ?
O2 T4A O8 108.5(11) 1_556 . ?
O5 T4A O15 112.5(11) . . ?
O2 T4A O15 111.2(11) 1_556 . ?
O8 T4A O15 107.0(10) . . ?
O5 T4A Ag1B 138.0(12) . 5 ?
O2 T4A Ag1B 114.1(12) 1_556 5 ?
O8 T4A Ag1B 58.3(16) . 5 ?
O15 T4A Ag1B 50.2(14) . 5 ?
T5D T5 O16 63.1(16) 7_566 7_566 ?
T5D T5 O9 60(3) 7_566 8_565 ?
O16 T5 O9 100(2) 7_566 8_565 ?
T5D T5 O4 169.8(17) 7_566 . ?
O16 T5 O4 108.7(15) 7_566 . ?
O9 T5 O4 119(3) 8_565 . ?
T5D T5 O9A 78(3) 7_566 . ?
O16 T5 O9A 116(2) 7_566 . ?
O9 T5 O9A 19(3) 8_565 . ?
O4 T5 O9A 102(3) . . ?
T5D T5 O12 74.2(16) 7_566 8_565 ?
O16 T5 O12 104.3(14) 7_566 8_565 ?
O9 T5 O12 108(2) 8_565 8_565 ?
O4 T5 O12 114.7(15) . 8_565 ?
O9A T5 O12 111(2) . 8_565 ?
T5D T5 T1D 94.6(16) 7_566 7_566 ?
O16 T5 T1D 31.7(13) 7_566 7_566 ?
O9 T5 T1D 122(2) 8_565 7_566 ?
O4 T5 T1D 77.6(14) . 7_566 ?
O9A T5 T1D 131(2) . 7_566 ?
O12 T5 T1D 113.0(14) 8_565 7_566 ?
T5 T5D OD4 177(4) 7_466 2_456 ?
T5 T5D O9 67(3) 7_466 2_456 ?
OD4 T5D O9 112(4) 2_456 2_456 ?
T5 T5D O16 64.9(15) 7_466 . ?
OD4 T5D O16 113(3) 2_456 . ?
O9 T5D O16 106(3) 2_456 . ?
T5 T5D O12 59.2(14) 7_466 2_456 ?
OD4 T5D O12 124(3) 2_456 2_456 ?
O9 T5D O12 103(3) 2_456 2_456 ?
O16 T5D O12 96.8(19) . 2_456 ?
T5 T5D O9A 56(2) 7_466 7_466 ?
OD4 T5D O9A 123(4) 2_456 7_466 ?
O9 T5D O9A 12(3) 2_456 7_466 ?
O16 T5D O9A 103(3) . 7_466 ?
O12 T5D O9A 92(2) 2_456 7_466 ?
T4A O2 T2 132.6(11) 1_554 . ?
T4A O2 Ag2B 117.9(12) 1_554 . ?
T2 O2 Ag2B 109.0(12) . . ?
T4A O2 Ag2E 111.8(12) 1_554 . ?
T2 O2 Ag2E 113.3(11) . . ?
Ag2B O2 Ag2E 25.6(9) . . ?
T4A O2 Ag2F 131.3(11) 1_554 . ?
T2 O2 Ag2F 96.0(9) . . ?
Ag2B O2 Ag2F 16.7(7) . . ?
Ag2E O2 Ag2F 23.5(9) . . ?
T2A O3 T2A 146(3) . 4_565 ?
T5 O4 T4 144(2) . . ?
T4A O5 T4 151.4(15) . . ?
T4A O5 T4D 155.5(17) . . ?
T4 O5 T4D 40.9(10) . . ?
T2 O6 T1 147.4(14) . 1_554 ?
T2 O6 T1D 169(2) . 1_554 ?
T1 O6 T1D 42.5(14) 1_554 1_554 ?
T2 O6 AgO1 118.1(12) . 7_465 ?
T1 O6 AgO1 94.5(10) 1_554 7_465 ?
T1D O6 AgO1 52.6(14) 1_554 7_465 ?
T2 O6 AgO3 109.9(12) . 7_465 ?
T1 O6 AgO3 101.6(10) 1_554 7_465 ?
T1D O6 AgO3 59.6(14) 1_554 7_465 ?
AgO1 O6 AgO3 17.9(4) 7_465 7_465 ?
T1A O7 T1A 142(2) . 4_565 ?
T1A O7 Ag2A 93.3(13) . . ?
T1A O7 Ag2A 93.3(13) 4_565 . ?
T1A O7 Ag4B 125.0(19) . 2_455 ?
T1A O7 Ag4B 92.9(16) 4_565 2_455 ?
Ag2A O7 Ag4B 84(2) . 2_455 ?
T1A O7 Ag4B 92.9(16) . 3_465 ?
T1A O7 Ag4B 125.0(19) 4_565 3_465 ?
Ag2A O7 Ag4B 84(2) . 3_465 ?
Ag4B O7 Ag4B 32(3) 2_455 3_465 ?
T4A O8 T1A 145.6(14) . 8_565 ?
T4A O8 Ag1 100.1(12) . 5 ?
T1A O8 Ag1 107.7(13) 8_565 5 ?
T4A O8 Ag1A 108.3(12) . 5 ?
T1A O8 Ag1A 97.8(12) 8_565 5 ?
Ag1 O8 Ag1A 10.2(5) 5 5 ?
O9A O9 T5D 132(10) 8_564 2_556 ?
O9A O9 T5 82(10) 8_564 8_564 ?
T5D O9 T5 53(2) 2_556 8_564 ?
O9A O9 T2 78(10) 8_564 . ?
T5D O9 T2 143(4) 2_556 . ?
T5 O9 T2 159(5) 8_564 . ?
O9 O9A T2 83(10) 8_565 8_565 ?
O9 O9A T5 79(10) 8_565 . ?
T2 O9A T5 162(5) 8_565 . ?
O9 O9A T5D 36(10) 8_565 7_566 ?
T2 O9A T5D 116(4) 8_565 7_566 ?
T5 O9A T5D 45.9(19) . 7_566 ?
T4 O11 T2A 160.1(15) . . ?
T4 O11 T4D 39.7(10) . . ?
T2A O11 T4D 122.9(16) . . ?
T1A O12 T5 145(2) . 8_564 ?
T1A O12 T5D 158(2) . 2_556 ?
T5 O12 T5D 46.6(12) 8_564 2_556 ?
T2A O13 T1 160.3(19) . . ?
T2A O13 T1D 120.8(19) . . ?
T1 O13 T1D 40.2(13) . . ?
T2A O14 T3A 141.9(14) . 5 ?
T2A O14 T3AD 150(2) . 5 ?
T3A O14 T3AD 34.3(17) 5 5 ?
T2A O14 Ag1 117.5(13) . 2_456 ?
T3A O14 Ag1 99.2(12) 5 2_456 ?
T3AD O14 Ag1 72(2) 5 2_456 ?
T2A O14 Ag1B 125.7(17) . 2_456 ?
T3A O14 Ag1B 89.0(19) 5 2_456 ?
T3AD O14 Ag1B 60(3) 5 2_456 ?
Ag1 O14 Ag1B 12.4(14) 2_456 2_456 ?
T2A O14 Ag1A 109.2(13) . 2_456 ?
T3A O14 Ag1A 108.4(13) 5 2_456 ?
T3AD O14 Ag1A 82(2) 5 2_456 ?
Ag1 O14 Ag1A 10.6(5) 2_456 2_456 ?
Ag1B O14 Ag1A 23.0(18) 2_456 2_456 ?
T3AD O15 T4A 154(2) 3_566 . ?
T3AD O15 T3A 37(2) 3_566 3_566 ?
T4A O15 T3A 135.8(12) . 3_566 ?
T3AD O15 Ag1B 64(2) 3_566 5 ?
T4A O15 Ag1B 98.4(16) . 5 ?
T3A O15 Ag1B 92.4(12) 3_566 5 ?
T1D O16 T5D 164(3) . . ?
T1D O16 T1 47.9(18) . . ?
T5D O16 T1 145(2) . . ?
T1D O16 T5 113(2) . 7_466 ?
T5D O16 T5 52.1(15) . 7_466 ?
T1 O16 T5 158.1(19) . 7_466 ?
T3 O17 T3N 49.6(19) 2_457 2_457 ?
T3 O17 T1 158(2) 2_457 . ?
T3N O17 T1 136.1(16) 2_457 . ?
T3 O17 Ag4B 93(2) 2_457 3_466 ?
T3N O17 Ag4B 122.4(17) 2_457 3_466 ?
T1 O17 Ag4B 96.2(16) . 3_466 ?
T3 O17 Ag4 75(2) 2_457 2_456 ?
T3N O17 Ag4 119.8(14) 2_457 2_456 ?
T1 O17 Ag4 104.2(13) . 2_456 ?
Ag4B O17 Ag4 29(2) 3_466 2_456 ?
T3N O18 T3ND 44.5(14) 2_456 2_456 ?
T3N O18 T1A 139.1(18) 2_456 . ?
T3ND O18 T1A 153(2) 2_456 . ?
T3N O18 T3 44.6(16) 2_456 2_456 ?
T3ND O18 T3 81(2) 2_456 2_456 ?
T1A O18 T3 119(2) . 2_456 ?
T3N O18 AgO1 93.8(13) 2_456 2_456 ?
T3ND O18 AgO1 49.4(14) 2_456 2_456 ?
T1A O18 AgO1 118.7(14) . 2_456 ?
T3 O18 AgO1 121.5(19) 2_456 2_456 ?
T3N O18 AgO3 97.4(13) 2_456 2_456 ?
T3ND O18 AgO3 56.1(14) 2_456 2_456 ?
T1A O18 AgO3 121.2(14) . 2_456 ?
T3 O18 AgO3 112.9(18) 2_456 2_456 ?
AgO1 O18 AgO3 17.8(5) 2_456 2_456 ?
T4D O19 T3N 129.1(16) . . ?
T4D O19 T4 43.3(12) . . ?
T3N O19 T4 132.5(13) . . ?
T4D O19 T3 131(2) . . ?
T3N O19 T3 47.2(16) . . ?
T4 O19 T3 173(2) . . ?
T4D O19 T3ND 133.1(18) . . ?
T3N O19 T3ND 39.7(12) . . ?
T4 O19 T3ND 104.5(13) . . ?
T3 O19 T3ND 79(2) . . ?
T4D O19 AgO2 118(2) . . ?
T3N O19 AgO2 99(2) . . ?
T4 O19 AgO2 126(2) . . ?
T3 O19 AgO2 57(2) . . ?
T3ND O19 AgO2 108(2) . . ?
T4D O19 Ag3A 95.7(16) . . ?
T3N O19 Ag3A 121.1(13) . . ?
T4 O19 Ag3A 106.1(14) . . ?
T3 O19 Ag3A 75.5(18) . . ?
T3ND O19 Ag3A 130.0(15) . . ?
AgO2 O19 Ag3A 23.3(19) . . ?
T2 O20 T3A 126.2(13) . 4_565 ?
T2 O20 T3AD 159(2) . 4_565 ?
T3A O20 T3AD 34.9(18) 4_565 4_565 ?
T2 O20 Ag2 110.8(14) . 1_565 ?
T3A O20 Ag2 122.9(14) 4_565 1_565 ?
T3AD O20 Ag2 89(2) 4_565 1_565 ?
T2 O20 Ag2D 105.7(18) . . ?
T3A O20 Ag2D 124(2) 4_565 . ?
T3AD O20 Ag2D 90(3) 4_565 . ?
Ag2 O20 Ag2D 22.7(18) 1_565 . ?
T2 O20 Ag2C 98.2(11) . . ?
T3A O20 Ag2C 134.1(13) 4_565 . ?
T3AD O20 Ag2C 102(2) 4_565 . ?
Ag2 O20 Ag2C 16.0(7) 1_565 . ?
Ag2D O20 Ag2C 34(2) . . ?
T2 O20 Ag2F 94.9(10) . . ?
T3A O20 Ag2F 138.6(12) 4_565 . ?
T3AD O20 Ag2F 104(2) 4_565 . ?
Ag2 O20 Ag2F 17.5(8) 1_565 . ?
Ag2D O20 Ag2F 18.9(19) . . ?
Ag2C O20 Ag2F 18.0(6) . . ?
AgO1 OD1 AgO3 7(2) . . ?
AgO1 OD1 T3ND 74(3) . . ?
AgO3 OD1 T3ND 75(2) . . ?
AgO1 OD1 T1D 72(4) . 7_566 ?
AgO3 OD1 T1D 77(2) . 7_566 ?
T3ND OD1 T1D 114(3) . 7_566 ?
T5D OD4 T4D 145(5) 2_556 1_554 ?
T3ND OD3 T3N 45.7(14) . . ?
T3ND OD3 T3A 143.1(19) . 3_566 ?
T3N OD3 T3A 164.7(15) . 3_566 ?
Ag1B Ag1 Ag1C 160(6) . . ?
Ag1B Ag1 O14 84(3) . 2_556 ?
Ag1C Ag1 O14 81(3) . 2_556 ?
Ag1B Ag1 O14 84(3) . 3_566 ?
Ag1C Ag1 O14 81(3) . 3_566 ?
O14 Ag1 O14 87.2(10) 2_556 3_566 ?
Ag1B Ag1 T3AD 46(3) . 6 ?
Ag1C Ag1 T3AD 121(3) . 6 ?
O14 Ag1 T3AD 40.2(13) 2_556 6 ?
O14 Ag1 T3AD 93.9(14) 3_566 6 ?
Ag1B Ag1 T3AD 46(3) . 7 ?
Ag1C Ag1 T3AD 121(3) . 7 ?
O14 Ag1 T3AD 93.9(14) 2_556 7 ?
O14 Ag1 T3AD 40.2(13) 3_566 7 ?
T3AD Ag1 T3AD 74(2) 6 7 ?
Ag1B Ag1 O8 95(4) . 5_544 ?
Ag1C Ag1 O8 101(4) . 5_544 ?
O14 Ag1 O8 173.9(8) 2_556 5_544 ?
O14 Ag1 O8 98.9(7) 3_566 5_544 ?
T3AD Ag1 O8 137.5(19) 6 5_544 ?
T3AD Ag1 O8 90.1(13) 7 5_544 ?
Ag1B Ag1 O8 95(4) . 8_564 ?
Ag1C Ag1 O8 101(4) . 8_564 ?
O14 Ag1 O8 98.9(7) 2_556 8_564 ?
O14 Ag1 O8 173.9(8) 3_566 8_564 ?
T3AD Ag1 O8 90.1(13) 6 8_564 ?
T3AD Ag1 O8 137.5(19) 7 8_564 ?
O8 Ag1 O8 75.1(10) 5_544 8_564 ?
Ag1B Ag1 Ag2A 178(5) . . ?
Ag1C Ag1 Ag2A 18(5) . . ?
O14 Ag1 Ag2A 94.1(15) 2_556 . ?
O14 Ag1 Ag2A 94.1(15) 3_566 . ?
T3AD Ag1 Ag2A 132.9(16) 6 . ?
T3AD Ag1 Ag2A 132.9(16) 7 . ?
O8 Ag1 Ag2A 86.5(16) 5_544 . ?
O8 Ag1 Ag2A 86.5(15) 8_564 . ?
Ag1 Ag1B Ag1A 4(3) . . ?
Ag1 Ag1B Ag1C 15(5) . . ?
Ag1A Ag1B Ag1C 11(4) . . ?
Ag1 Ag1B T3AD 124(3) . 6 ?
Ag1A Ag1B T3AD 121(2) . 6 ?
Ag1C Ag1B T3AD 115(3) . 6 ?
Ag1 Ag1B T3AD 124(3) . 7 ?
Ag1A Ag1B T3AD 121(2) . 7 ?
Ag1C Ag1B T3AD 115(3) . 7 ?
T3AD Ag1B T3AD 88(4) 6 7 ?
Ag1 Ag1B O15 121(2) . 8_564 ?
Ag1A Ag1B O15 122.1(19) . 8_564 ?
Ag1C Ag1B O15 123.0(17) . 8_564 ?
T3AD Ag1B O15 36.7(15) 6 8_564 ?
T3AD Ag1B O15 111(4) 7 8_564 ?
Ag1 Ag1B O15 121(2) . 5_544 ?
Ag1A Ag1B O15 122.1(19) . 5_544 ?
Ag1C Ag1B O15 123.0(17) . 5_544 ?
T3AD Ag1B O15 111(4) 6 5_544 ?
T3AD Ag1B O15 36.7(15) 7 5_544 ?
O15 Ag1B O15 114(3) 8_564 5_544 ?
Ag1 Ag1B O14 83(3) . 2_556 ?
Ag1A Ag1B O14 80(2) . 2_556 ?
Ag1C Ag1B O14 73(3) . 2_556 ?
T3AD Ag1B O14 42.6(15) 6 2_556 ?
T3AD Ag1B O14 103(2) 7 2_556 ?
O15 Ag1B O14 66.5(9) 8_564 2_556 ?
O15 Ag1B O14 139(3) 5_544 2_556 ?
Ag1 Ag1B O14 83(3) . 3_566 ?
Ag1A Ag1B O14 80(2) . 3_566 ?
Ag1C Ag1B O14 73(3) . 3_566 ?
T3AD Ag1B O14 103(2) 6 3_566 ?
T3AD Ag1B O14 42.6(15) 7 3_566 ?
O15 Ag1B O14 139(3) 8_564 3_566 ?
O15 Ag1B O14 66.5(9) 5_544 3_566 ?
O14 Ag1B O14 86.9(14) 2_556 3_566 ?
Ag1 Ag1B T3A 112(2) . 6 ?
Ag1A Ag1B T3A 109.6(15) . 6 ?
Ag1C Ag1B T3A 105(2) . 6 ?
T3AD Ag1B T3A 14.0(14) 6 6 ?
T3AD Ag1B T3A 101(3) 7 6 ?
O15 Ag1B T3A 33.9(7) 8_564 6 ?
O15 Ag1B T3A 125(3) 5_544 6 ?
O14 Ag1B T3A 34.9(7) 2_556 6 ?
O14 Ag1B T3A 109.5(15) 3_566 6 ?
Ag1 Ag1B T3A 112(2) . 7 ?
Ag1A Ag1B T3A 109.6(15) . 7 ?
Ag1C Ag1B T3A 105(2) . 7 ?
T3AD Ag1B T3A 101(3) 6 7 ?
T3AD Ag1B T3A 14.0(14) 7 7 ?
O15 Ag1B T3A 125(3) 8_564 7 ?
O15 Ag1B T3A 33.9(7) 5_544 7 ?
O14 Ag1B T3A 109.5(15) 2_556 7 ?
O14 Ag1B T3A 34.9(7) 3_566 7 ?
T3A Ag1B T3A 114(2) 6 7 ?
Ag1 Ag1B T4A 101(3) . 5_544 ?
Ag1A Ag1B T4A 103(2) . 5_544 ?
Ag1C Ag1B T4A 110(3) . 5_544 ?
T3AD Ag1B T4A 135(4) 6 5_544 ?
T3AD Ag1B T4A 67.1(15) 7 5_544 ?
O15 Ag1B T4A 118(2) 8_564 5_544 ?
O15 Ag1B T4A 31.4(6) 5_544 5_544 ?
O14 Ag1B T4A 169.8(19) 2_556 5_544 ?
O14 Ag1B T4A 84.3(5) 3_566 5_544 ?
T3A Ag1B T4A 146(3) 6 5_544 ?
T3A Ag1B T4A 60.3(5) 7 5_544 ?
Ag1B Ag1A Ag1C 160(7) . . ?
Ag1B Ag1A Ag2A 176(3) . . ?
Ag1C Ag1A Ag2A 24(7) . . ?
Ag1B Ag1A O14 77.0(16) . 2_556 ?
Ag1C Ag1A O14 89(5) . 2_556 ?
Ag2A Ag1A O14 105.7(17) . 2_556 ?
Ag1B Ag1A O14 77.0(16) . 3_566 ?
Ag1C Ag1A O14 89(5) . 3_566 ?
Ag2A Ag1A O14 105.7(17) . 3_566 ?
O14 Ag1A O14 85.7(10) 2_556 3_566 ?
Ag1B Ag1A O8 81(2) . 5_544 ?
Ag1C Ag1A O8 114(5) . 5_544 ?
Ag2A Ag1A O8 95.6(17) . 5_544 ?
O14 Ag1A O8 157.2(18) 2_556 5_544 ?
O14 Ag1A O8 96.4(8) 3_566 5_544 ?
Ag1B Ag1A O8 81(2) . 8_564 ?
Ag1C Ag1A O8 114(5) . 8_564 ?
Ag2A Ag1A O8 95.6(17) . 8_564 ?
O14 Ag1A O8 96.4(7) 2_556 8_564 ?
O14 Ag1A O8 157.2(18) 3_566 8_564 ?
O8 Ag1A O8 73.1(11) 5_544 8_564 ?
Ag1B Ag1A T3AD 41.1(16) . 6 ?
Ag1C Ag1A T3AD 125(5) . 6 ?
Ag2A Ag1A T3AD 140.9(16) . 6 ?
O14 Ag1A T3AD 36.8(12) 2_556 6 ?
O14 Ag1A T3AD 86.0(13) 3_566 6 ?
O8 Ag1A T3AD 120.5(18) 5_544 6 ?
O8 Ag1A T3AD 82.4(13) 8_564 6 ?
Ag1B Ag1A T3AD 41.1(16) . 7 ?
Ag1C Ag1A T3AD 125(5) . 7 ?
Ag2A Ag1A T3AD 140.9(16) . 7 ?
O14 Ag1A T3AD 86.0(13) 2_556 7 ?
O14 Ag1A T3AD 36.8(12) 3_566 7 ?
O8 Ag1A T3AD 82.4(13) 5_544 7 ?
O8 Ag1A T3AD 120.5(18) 8_564 7 ?
T3AD Ag1A T3AD 65(2) 6 7 ?
Ag1A Ag1C Ag2A 135(10) . . ?
Ag1A Ag1C Ag1 4(2) . . ?
Ag2A Ag1C Ag1 139(10) . . ?
Ag1A Ag1C Ag1B 9(3) . . ?
Ag2A Ag1C Ag1B 144(10) . . ?
Ag1 Ag1C Ag1B 4.9(16) . . ?
Ag1A Ag1C T2A 94(6) . 2_556 ?
Ag2A Ag1C T2A 124(7) . 2_556 ?
Ag1 Ag1C T2A 91(5) . 2_556 ?
Ag1B Ag1C T2A 87(4) . 2_556 ?
Ag1A Ag1C T2A 94(6) . 3_566 ?
Ag2A Ag1C T2A 124(7) . 3_566 ?
Ag1 Ag1C T2A 91(5) . 3_566 ?
Ag1B Ag1C T2A 87(4) . 3_566 ?
T2A Ag1C T2A 60(2) 2_556 3_566 ?
Ag2C Ag2 Ag2F 63(4) 1_545 1_545 ?
Ag2C Ag2 Ag2D 119(6) 1_545 1_545 ?
Ag2F Ag2 Ag2D 56(5) 1_545 1_545 ?
Ag2C Ag2 Ag2B 37(3) 1_545 1_545 ?
Ag2F Ag2 Ag2B 26(2) 1_545 1_545 ?
Ag2D Ag2 Ag2B 82(5) 1_545 1_545 ?
Ag2C Ag2 Ag2E 72(3) 1_545 1_545 ?
Ag2F Ag2 Ag2E 9.2(19) 1_545 1_545 ?
Ag2D Ag2 Ag2E 47(5) 1_545 1_545 ?
Ag2B Ag2 Ag2E 35.2(14) 1_545 1_545 ?
Ag2C Ag2 O20 104.2(12) 1_545 4_565 ?
Ag2F Ag2 O20 105.8(11) 1_545 4_565 ?
Ag2D Ag2 O20 92.4(19) 1_545 4_565 ?
Ag2B Ag2 O20 107.7(11) 1_545 4_565 ?
Ag2E Ag2 O20 104.3(11) 1_545 4_565 ?
Ag2C Ag2 O20 104.2(12) 1_545 1_545 ?
Ag2F Ag2 O20 105.8(11) 1_545 1_545 ?
Ag2D Ag2 O20 92.4(19) 1_545 1_545 ?
Ag2B Ag2 O20 107.7(11) 1_545 1_545 ?
Ag2E Ag2 O20 104.3(11) 1_545 1_545 ?
O20 Ag2 O20 145(2) 4_565 1_545 ?
Ag2C Ag2 T3AD 134(3) 1_545 . ?
Ag2F Ag2 T3AD 136(2) 1_545 . ?
Ag2D Ag2 T3AD 93(4) 1_545 . ?
Ag2B Ag2 T3AD 145.9(12) 1_545 . ?
Ag2E Ag2 T3AD 130.0(18) 1_545 . ?
O20 Ag2 T3AD 38.5(13) 4_565 . ?
O20 Ag2 T3AD 106.2(18) 1_545 . ?
Ag2C Ag2 T3AD 134(3) 1_545 4 ?
Ag2F Ag2 T3AD 136(2) 1_545 4 ?
Ag2D Ag2 T3AD 93(4) 1_545 4 ?
Ag2B Ag2 T3AD 145.9(12) 1_545 4 ?
Ag2E Ag2 T3AD 130.0(18) 1_545 4 ?
O20 Ag2 T3AD 106.2(18) 4_565 4 ?
O20 Ag2 T3AD 38.5(13) 1_545 4 ?
T3AD Ag2 T3AD 68(2) . 4 ?
Ag1C Ag2A Ag1A 21(6) . . ?
Ag1C Ag2A O7 102(7) . . ?
Ag1A Ag2A O7 81(2) . . ?
Ag1C Ag2A Ag1 23(6) . . ?
Ag1A Ag2A Ag1 1.5(6) . . ?
O7 Ag2A Ag1 79(2) . . ?
Ag1C Ag2A Ag1B 22(6) . . ?
Ag1A Ag2A Ag1B 1.1(9) . . ?
O7 Ag2A Ag1B 80(2) . . ?
Ag1 Ag2A Ag1B 0.3(8) . . ?
Ag2F Ag2B Ag2C 56(3) . . ?
Ag2F Ag2B Ag2E 67(3) . . ?
Ag2C Ag2B Ag2E 123(4) . . ?
Ag2F Ag2B Ag2 28(2) . 1_565 ?
Ag2C Ag2B Ag2 28(2) . 1_565 ?
Ag2E Ag2B Ag2 95(3) . 1_565 ?
Ag2F Ag2B Ag2D 9(3) . . ?
Ag2C Ag2B Ag2D 65(4) . . ?
Ag2E Ag2B Ag2D 58(3) . . ?
Ag2 Ag2B Ag2D 37(3) 1_565 . ?
Ag2F Ag2B O2 101.2(11) . . ?
Ag2C Ag2B O2 107.1(8) . . ?
Ag2E Ag2B O2 82.6(11) . . ?
Ag2 Ag2B O2 106.1(9) 1_565 . ?
Ag2D Ag2B O2 99.1(12) . . ?
Ag2F Ag2B O2 101.2(11) . 4_575 ?
Ag2C Ag2B O2 107.1(8) . 4_575 ?
Ag2E Ag2B O2 82.6(11) . 4_575 ?
Ag2 Ag2B O2 106.1(9) 1_565 4_575 ?
Ag2D Ag2B O2 99.1(12) . 4_575 ?
O2 Ag2B O2 145.4(17) . 4_575 ?
Ag2 Ag2C Ag2F 64(3) 1_565 . ?
Ag2 Ag2C Ag2B 115(4) 1_565 . ?
Ag2F Ag2C Ag2B 51(2) . . ?
Ag2 Ag2C Ag2D 36(4) 1_565 . ?
Ag2F Ag2C Ag2D 29(3) . . ?
Ag2B Ag2C Ag2D 80(4) . . ?
Ag2 Ag2C Ag2E 85(3) 1_565 . ?
Ag2F Ag2C Ag2E 20.6(18) . . ?
Ag2B Ag2C Ag2E 30(2) . . ?
Ag2D Ag2C Ag2E 49(3) . . ?
Ag2 Ag2C O20 59.8(10) 1_565 4_575 ?
Ag2F Ag2C O20 85.7(16) . 4_575 ?
Ag2B Ag2C O20 111.0(14) . 4_575 ?
Ag2D Ag2C O20 71.6(17) . 4_575 ?
Ag2E Ag2C O20 96.5(12) . 4_575 ?
Ag2 Ag2C O20 59.8(10) 1_565 . ?
Ag2F Ag2C O20 85.7(16) . . ?
Ag2B Ag2C O20 111.0(14) . . ?
Ag2D Ag2C O20 71.6(17) . . ?
Ag2E Ag2C O20 96.5(12) . . ?
O20 Ag2C O20 116.2(16) 4_575 . ?
Ag2F Ag2D Ag2 53(5) . 1_565 ?
Ag2F Ag2D Ag2E 49(4) . . ?
Ag2 Ag2D Ag2E 102(7) 1_565 . ?
Ag2F Ag2D Ag2C 27(3) . . ?
Ag2 Ag2D Ag2C 26(3) 1_565 . ?
Ag2E Ag2D Ag2C 76(5) . . ?
Ag2F Ag2D Ag2B 8(3) . . ?
Ag2 Ag2D Ag2B 61(5) 1_565 . ?
Ag2E Ag2D Ag2B 41(3) . . ?
Ag2C Ag2D Ag2B 35(2) . . ?
Ag2F Ag2D O20 88(3) . 4_575 ?
Ag2 Ag2D O20 65(2) 1_565 4_575 ?
Ag2E Ag2D O20 111(3) . 4_575 ?
Ag2C Ag2D O20 75(2) . 4_575 ?
Ag2B Ag2D O20 92(3) . 4_575 ?
Ag2F Ag2D O20 88(3) . . ?
Ag2 Ag2D O20 65(2) 1_565 . ?
Ag2E Ag2D O20 111(3) . . ?
Ag2C Ag2D O20 75(2) . . ?
Ag2B Ag2D O20 92(3) . . ?
O20 Ag2D O20 119(3) 4_575 . ?
Ag2F Ag2D T3AD 113(5) . 1_565 ?
Ag2 Ag2D T3AD 68(4) 1_565 1_565 ?
Ag2E Ag2D T3AD 146(2) . 1_565 ?
Ag2C Ag2D T3AD 90(3) . 1_565 ?
Ag2B Ag2D T3AD 120(3) . 1_565 ?
O20 Ag2D T3AD 35.4(14) 4_575 1_565 ?
O20 Ag2D T3AD 95(2) . 1_565 ?
Ag2F Ag2D T3AD 113(5) . 4_565 ?
Ag2 Ag2D T3AD 68(4) 1_565 4_565 ?
Ag2E Ag2D T3AD 146(2) . 4_565 ?
Ag2C Ag2D T3AD 90(3) . 4_565 ?
Ag2B Ag2D T3AD 120(3) . 4_565 ?
O20 Ag2D T3AD 95(2) 4_575 4_565 ?
O20 Ag2D T3AD 35.4(14) . 4_565 ?
T3AD Ag2D T3AD 63(2) 1_565 4_565 ?
Ag2F Ag2E Ag2B 42(2) . . ?
Ag2F Ag2E Ag2D 38(4) . . ?
Ag2B Ag2E Ag2D 81(5) . . ?
Ag2F Ag2E Ag2C 16.0(15) . . ?
Ag2B Ag2E Ag2C 26(2) . . ?
Ag2D Ag2E Ag2C 54(4) . . ?
Ag2F Ag2E Ag2 7.3(16) . 1_565 ?
Ag2B Ag2E Ag2 50(3) . 1_565 ?
Ag2D Ag2E Ag2 31(4) . 1_565 ?
Ag2C Ag2E Ag2 23.3(11) . 1_565 ?
Ag2F Ag2E O2 86.7(14) . 4_575 ?
Ag2B Ag2E O2 71.8(11) . 4_575 ?
Ag2D Ag2E O2 101.7(17) . 4_575 ?
Ag2C Ag2E O2 80.4(12) . 4_575 ?
Ag2 Ag2E O2 89.6(13) 1_565 4_575 ?
Ag2F Ag2E O2 86.7(14) . . ?
Ag2B Ag2E O2 71.8(11) . . ?
Ag2D Ag2E O2 101.7(17) . . ?
Ag2C Ag2E O2 80.4(12) . . ?
Ag2 Ag2E O2 89.6(13) 1_565 . ?
O2 Ag2E O2 132.4(18) 4_575 . ?
Ag2B Ag2F Ag2C 73(3) . . ?
Ag2B Ag2F Ag2 126(4) . 1_565 ?
Ag2C Ag2F Ag2 53(2) . 1_565 ?
Ag2B Ag2F Ag2D 163(6) . . ?
Ag2C Ag2F Ag2D 124(6) . . ?
Ag2 Ag2F Ag2D 71(5) 1_565 . ?
Ag2B Ag2F Ag2E 71(3) . . ?
Ag2C Ag2F Ag2E 143(3) . . ?
Ag2 Ag2F Ag2E 164(3) 1_565 . ?
Ag2D Ag2F Ag2E 92(5) . . ?
Ag2B Ag2F O2 62.1(9) . . ?
Ag2C Ag2F O2 93.0(14) . . ?
Ag2 Ag2F O2 115.9(10) 1_565 . ?
Ag2D Ag2F O2 113.0(19) . . ?
Ag2E Ag2F O2 69.8(11) . . ?
Ag2B Ag2F O2 62.1(9) . 4_575 ?
Ag2C Ag2F O2 93.0(14) . 4_575 ?
Ag2 Ag2F O2 115.9(10) 1_565 4_575 ?
Ag2D Ag2F O2 113.0(19) . 4_575 ?
Ag2E Ag2F O2 69.8(11) . 4_575 ?
O2 Ag2F O2 118.7(12) . 4_575 ?
Ag2B Ag2F O20 114.5(12) . 4_575 ?
Ag2C Ag2F O20 76.3(14) . 4_575 ?
Ag2 Ag2F O20 56.7(8) 1_565 4_575 ?
Ag2D Ag2F O20 73(3) . 4_575 ?
Ag2E Ag2F O20 119.6(9) . 4_575 ?
O2 Ag2F O20 169.3(13) . 4_575 ?
O2 Ag2F O20 63.8(5) 4_575 4_575 ?
Ag2B Ag2F O20 114.5(12) . . ?
Ag2C Ag2F O20 76.3(14) . . ?
Ag2 Ag2F O20 56.7(8) 1_565 . ?
Ag2D Ag2F O20 73(3) . . ?
Ag2E Ag2F O20 119.6(9) . . ?
O2 Ag2F O20 63.8(5) . . ?
O2 Ag2F O20 169.3(13) 4_575 . ?
O20 Ag2F O20 111.7(13) 4_575 . ?
Ag2B Ag2F T2 88.5(5) . 4_575 ?
Ag2C Ag2F T2 84.3(4) . 4_575 ?
Ag2 Ag2F T2 86.4(5) 1_565 4_575 ?
Ag2D Ag2F T2 93.0(6) . 4_575 ?
Ag2E Ag2F T2 94.7(5) . 4_575 ?
O2 Ag2F T2 149.7(10) . 4_575 ?
O2 Ag2F T2 31.9(4) 4_575 4_575 ?
O20 Ag2F T2 31.9(5) 4_575 4_575 ?
O20 Ag2F T2 142.9(10) . 4_575 ?
Ag2B Ag2F T2 88.5(5) . . ?
Ag2C Ag2F T2 84.3(4) . . ?
Ag2 Ag2F T2 86.4(5) 1_565 . ?
Ag2D Ag2F T2 93.0(6) . . ?
Ag2E Ag2F T2 94.7(5) . . ?
O2 Ag2F T2 31.9(4) . . ?
O2 Ag2F T2 149.7(10) 4_575 . ?
O20 Ag2F T2 142.9(10) 4_575 . ?
O20 Ag2F T2 31.9(5) . . ?
T2 Ag2F T2 168.6(9) 4_575 . ?
Ag3A Ag3 AgO2 51(9) . . ?
Ag3A Ag3 T3 48(6) . . ?
AgO2 Ag3 T3 34(3) . . ?
Ag3A Ag3 T3 48(6) . 4_565 ?
AgO2 Ag3 T3 34(3) . 4_565 ?
T3 Ag3 T3 62(3) . 4_565 ?
Ag3 Ag3A AgO2 99(10) . . ?
Ag3 Ag3A O19 98(3) . 4_565 ?
AgO2 Ag3A O19 74.8(10) . 4_565 ?
Ag3 Ag3A O19 98(3) . . ?
AgO2 Ag3A O19 74.8(10) . . ?
O19 Ag3A O19 147.3(17) 4_565 . ?
Ag3 Ag3A T3 122(7) . . ?
AgO2 Ag3A T3 47(3) . . ?
O19 Ag3A T3 110.3(16) 4_565 . ?
O19 Ag3A T3 37.7(11) . . ?
Ag3 Ag3A T3 122(7) . 4_565 ?
AgO2 Ag3A T3 47(3) . 4_565 ?
O19 Ag3A T3 37.7(11) 4_565 4_565 ?
O19 Ag3A T3 110.3(16) . 4_565 ?
T3 Ag3A T3 73(2) . 4_565 ?
Ag3 Ag3A T4D 100(3) . 4_565 ?
AgO2 Ag3A T4D 102.7(13) . 4_565 ?
O19 Ag3A T4D 28.6(7) 4_565 4_565 ?
O19 Ag3A T4D 162(2) . 4_565 ?
T3 Ag3A T4D 128.7(18) . 4_565 ?
T3 Ag3A T4D 59.7(11) 4_565 4_565 ?
Ag3 Ag3A T4D 100(3) . . ?
AgO2 Ag3A T4D 102.7(13) . . ?
O19 Ag3A T4D 162(2) 4_565 . ?
O19 Ag3A T4D 28.6(7) . . ?
T3 Ag3A T4D 59.7(11) . . ?
T3 Ag3A T4D 128.7(18) 4_565 . ?
T4D Ag3A T4D 144.7(16) 4_565 . ?
Ag4A Ag4 Ag4B 38(3) . 4_565 ?
Ag4A Ag4 Ag4B 38(3) . . ?
Ag4B Ag4 Ag4B 70(6) 4_565 . ?
Ag4A Ag4 O17 107.4(12) . 3_566 ?
Ag4B Ag4 O17 140(3) 4_565 3_566 ?
Ag4B Ag4 O17 71(3) . 3_566 ?
Ag4A Ag4 O17 107.4(12) . 2_556 ?
Ag4B Ag4 O17 71(3) 4_565 2_556 ?
Ag4B Ag4 O17 140(3) . 2_556 ?
O17 Ag4 O17 143(2) 3_566 2_556 ?
Ag4A Ag4 T3 129(3) . 4_564 ?
Ag4B Ag4 T3 139(3) 4_565 4_564 ?
Ag4B Ag4 T3 93(3) . 4_564 ?
O17 Ag4 T3 34.8(12) 3_566 4_564 ?
O17 Ag4 T3 110.8(19) 2_556 4_564 ?
Ag4A Ag4 T3 129(3) . 1_554 ?
Ag4B Ag4 T3 93(3) 4_565 1_554 ?
Ag4B Ag4 T3 139(3) . 1_554 ?
O17 Ag4 T3 110.8(19) 3_566 1_554 ?
O17 Ag4 T3 34.8(12) 2_556 1_554 ?
T3 Ag4 T3 77(2) 4_564 1_554 ?
Ag4 Ag4A Ag4B 110(5) . 4_565 ?
Ag4 Ag4A Ag4B 110(5) . . ?
Ag4B Ag4A Ag4B 125(9) 4_565 . ?
Ag4 Ag4A T3 41(2) . 4_564 ?
Ag4B Ag4A T3 126(5) 4_565 4_564 ?
Ag4B Ag4A T3 71(5) . 4_564 ?
Ag4 Ag4A T3 41(2) . 1_554 ?
Ag4B Ag4A T3 71(5) 4_565 1_554 ?
Ag4B Ag4A T3 126(5) . 1_554 ?
T3 Ag4A T3 62.7(18) 4_564 1_554 ?
Ag4A Ag4B Ag4 33(3) . . ?
Ag4A Ag4B Ag4B 27(5) . 4_565 ?
Ag4 Ag4B Ag4B 55(3) . 4_565 ?
Ag4A Ag4B O17 112(5) . 3_566 ?
Ag4 Ag4B O17 80(3) . 3_566 ?
Ag4B Ag4B O17 134.2(15) 4_565 3_566 ?
Ag4A Ag4B O7 91(5) . 2 ?
Ag4 Ag4B O7 87(3) . 2 ?
Ag4B Ag4B O7 74.0(14) 4_565 2 ?
O17 Ag4B O7 96.9(18) 3_566 2 ?
Ag4A Ag4B T3 94(5) . 4_564 ?
Ag4 Ag4B T3 62(3) . 4_564 ?
Ag4B Ag4B T3 107.8(15) 4_565 4_564 ?
O17 Ag4B T3 31.6(12) 3_566 4_564 ?
O7 Ag4B T3 70.9(16) 2 4_564 ?
Ag4A Ag4B T1 114(5) . 3_566 ?
Ag4 Ag4B T1 91(3) . 3_566 ?
Ag4B Ag4B T1 141.2(11) 4_565 3_566 ?
O17 Ag4B T1 32.7(9) 3_566 3_566 ?
O7 Ag4B T1 128.4(19) 2 3_566 ?
T3 Ag4B T1 63.2(13) 4_564 3_566 ?
OD1 AgO1 AgO3 167(4) . . ?
OD1 AgO1 T3ND 83(4) . . ?
AgO3 AgO1 T3ND 100(2) . . ?
OD1 AgO1 T1D 86(4) . 7_566 ?
AgO3 AgO1 T1D 104(2) . 7_566 ?
T3ND AgO1 T1D 121.9(17) . 7_566 ?
OD1 AgO1 O6 88(4) . 7_565 ?
AgO3 AgO1 O6 91.6(18) . 7_565 ?
T3ND AgO1 O6 166.7(16) . 7_565 ?
T1D AgO1 O6 47.4(13) 7_566 7_565 ?
OD1 AgO1 O18 84(4) . 2_556 ?
AgO3 AgO1 O18 88.9(19) . 2_556 ?
T3ND AgO1 O18 41.4(12) . 2_556 ?
T1D AgO1 O18 161.6(17) 7_566 2_556 ?
O6 AgO1 O18 147.0(10) 7_565 2_556 ?
OD1 AgO1 T3N 84(3) . . ?
AgO3 AgO1 T3N 95.8(17) . . ?
T3ND AgO1 T3N 9.5(10) . . ?
T1D AgO1 T3N 131.4(14) 7_566 . ?
O6 AgO1 T3N 172.5(12) 7_565 . ?
O18 AgO1 T3N 32.1(7) 2_556 . ?
OD1 AgO1 T1 82(3) . 7_566 ?
AgO3 AgO1 T1 104.9(17) . 7_566 ?
T3ND AgO1 T1 134.0(12) . 7_566 ?
T1D AgO1 T1 13.9(12) 7_566 7_566 ?
O6 AgO1 T1 34.3(6) 7_565 7_566 ?
O18 AgO1 T1 166.2(13) 2_556 7_566 ?
T3N AgO1 T1 143.4(7) . 7_566 ?
Ag3A AgO2 Ag3 30(5) . . ?
Ag3A AgO2 T3 112(4) . 4_565 ?
Ag3 AgO2 T3 127(3) . 4_565 ?
Ag3A AgO2 T3 112(4) . . ?
Ag3 AgO2 T3 127(3) . . ?
T3 AgO2 T3 97(4) 4_565 . ?
Ag3A AgO2 O19 82(2) . 4_565 ?
Ag3 AgO2 O19 86(2) . 4_565 ?
T3 AgO2 O19 42.2(13) 4_565 4_565 ?
T3 AgO2 O19 137(3) . 4_565 ?
Ag3A AgO2 O19 82(2) . . ?
Ag3 AgO2 O19 86(2) . . ?
T3 AgO2 O19 137(3) 4_565 . ?
T3 AgO2 O19 42.2(13) . . ?
O19 AgO2 O19 160(4) 4_565 . ?
AgO1 AgO3 OD1 7(2) . . ?
AgO1 AgO3 T3ND 59.3(18) . . ?
OD1 AgO3 T3ND 60.5(19) . . ?
AgO1 AgO3 T1D 56.5(19) . 7_566 ?
OD1 AgO3 T1D 61(2) . 7_566 ?
T3ND AgO3 T1D 98.3(16) . 7_566 ?
AgO1 AgO3 O6 70.6(17) . 7_565 ?
OD1 AgO3 O6 70.6(18) . 7_565 ?
T3ND AgO3 O6 129.4(15) . 7_565 ?
T1D AgO3 O6 43.4(11) 7_566 7_565 ?
AgO1 AgO3 O18 73.3(18) . 2_556 ?
OD1 AgO3 O18 69.9(18) . 2_556 ?
T3ND AgO3 O18 39.2(11) . 2_556 ?
T1D AgO3 O18 128.3(16) 7_566 2_556 ?
O6 AgO3 O18 131.5(12) 7_565 2_556 ?
 
_refine_diff_density_max    1.283
_refine_diff_density_min   -0.962
_refine_diff_density_rms    0.287

_shelxl_version_number 2014-1



