data_mht-iii-53 # start Validation Reply Form _vrf_PLAT975_mht-iii-53 ; PROBLEM: Check Calcd Resid. Dens. 0.55A From N2_2 2.10 eA-3 RESPONSE: There is underlying disorder of the organic molecules. This disorder is indicated by the large and very anisotropic thermal ellispoids. The complexity and the degree of this disorder prohibited building a model that could reproduce these effects This residual is probably unresolved disorder. ; _vrf_PLAT241_mht-iii-53 ; PROBLEM: High MainMol Ueq as Compared to Neighbors of C8_3 Check RESPONSE: A qualitative examination of the thermal ellipsoids of this sample suggests underlying disorder associated with packing defects in the crystal. The complexity and the degree of this disorder prohibited building a model that could reproduce these effects. ; _vrf_PLAT430_mht-iii-53 ; PROBLEM: Short Inter D...A Contact O2_2 ..O1_4 . 2.78 Ang. RESPONSE: This is a real contact in the crystal. The nitro groups interact with each other in many modes; described in the paper. ; # end Validation Reply Form _audit_creation_date 2018-10-20 _audit_creation_method ; Olex2 1.2-alpha (compiled 2018.07.26 svn.r3523 for OlexSys, GUI svn.r5532) ; _shelx_SHELXL_version_number '2018/3' _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_name '' _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _publ_section_references ; Bruker (2013). SAINT-Plus V8.34A Bruker AXS Inc., Madison, Wisconsin, USA. Bruker (2016). APEX2 Version 2016.5-1. Bruker AXS Inc., Madison, Wisconsin, USA. Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Krause, L., Herbst-Irmer, R., Sheldrick, G. M., and Stalke, D., J. Appl. Cryst. (2015). 48, 1907-1913. Palatinus, L. & Chapuis, G. (2007). J. Appl. Cryst., 40, 786-790; Palatinus, L. & van der Lee, A. (2008). J. Appl. Cryst. 41, 975-984; Palatinus, L., Prathapa, S. J. & van Smaalen, S. (2012). J. Appl. Cryst. 45, 575-580 Petricek,V., Dusek,M. & Palatinus,L.(2006). Jana2006. The crystallographic computing system. Institute of Physics, Praha, Czech Republic. Rigaku Oxford Diffraction, (2015), CrysAlisPro Software system, version 1.171.39.20a, Rigaku Corporation, Oxford, UK. Sheldrick, G.M. (2015). Acta Cryst. (2015). A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. (2015). C71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. Spek, A. L. (2015). Acta Cryst. C71, 9-18. Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety '(I4 Pb), 2(C8 H11 N2 O2)' _chemical_formula_sum 'C16 H22 I4 N4 O4 Pb' _chemical_formula_weight 1049.16 _chemical_melting_point ? _chemical_oxdiff_formula 'C180 I32 N12 O8 Pb8 ' loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'I' 'I' -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Pb' 'Pb' -3.3944 10.1111 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'monoclinic' _space_group_IT_number 14 _space_group_name_H-M_alt 'P 1 21/c 1' _space_group_name_Hall '-P 2ybc' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 21.0976(4) _cell_length_b 19.8255(3) _cell_length_c 12.6149(2) _cell_angle_alpha 90 _cell_angle_beta 98.2252(17) _cell_angle_gamma 90 _cell_volume 5222.17(16) _cell_formula_units_Z 8 _cell_measurement_reflns_used 32454 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 33.7420 _cell_measurement_theta_min 1.9140 _shelx_estimated_absorpt_T_max ? _shelx_estimated_absorpt_T_min ? _exptl_absorpt_coefficient_mu 11.218 _exptl_absorpt_correction_T_max 0.908 _exptl_absorpt_correction_T_min 0.408 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.43c (Rigaku Oxford Diffraction, 2018) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _exptl_crystal_colour orange _exptl_crystal_colour_primary orange _exptl_crystal_density_diffrn 2.669 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description plate _exptl_crystal_F_000 3776 loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 1 -4 -5 0.0476 -1 4 5 0.0476 0 -5 2 0.0438 0 5 -2 0.0438 1 0 0 0.0095 -1 0 0 0.0095 0 -5 -1 0.0488 0 5 1 0.0488 _exptl_crystal_recrystallization_method 'The material was recrystallised from --- by as supplied' _exptl_crystal_size_max 0.099 _exptl_crystal_size_mid 0.088 _exptl_crystal_size_min 0.019 loop_ _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z 1.0066 -3.9919 -4.9978 0.0079 0.0035 0.3151 -1.0066 3.9919 4.9978 -0.0079 -0.0035 -0.3151 0.0126 -5.0048 1.9973 0.1969 0.0749 -0.0252 -0.0126 5.0048 -1.9973 -0.1969 -0.0749 0.0252 1.0009 0.0013 -0.0006 0.0145 -0.0308 -0.0007 -1.0009 -0.0013 0.0006 -0.0145 0.0308 0.0007 0.0106 -5.0000 -1.0004 0.1223 0.0632 0.1275 -0.0106 5.0000 1.0004 -0.1223 -0.0632 -0.1275 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0476 _diffrn_reflns_av_unetI/netI 0.0348 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 29 _diffrn_reflns_limit_h_min -29 _diffrn_reflns_limit_k_max 27 _diffrn_reflns_limit_k_min -27 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_number 90640 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 29.575 _diffrn_reflns_theta_min 1.928 _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100(2) _diffrn_detector HyPix _diffrn_detector_area_resol_mean ? _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -2.00 80.00 0.50 25.00 -- 15.69 38.00 -60.00 164 2 \w 57.00 85.00 0.50 25.00 -- 15.69 0.00 -30.00 56 3 \w 4.00 34.00 0.50 25.00 -- 15.69 57.00-150.00 60 4 \w -34.00 -1.00 0.50 25.00 -- 15.69 0.00 -30.00 66 5 \w -24.00 5.00 0.50 25.00 -- 15.69 -57.00-120.00 58 6 \w -56.00 34.00 0.50 25.00 -- 15.69 -57.00-150.00 180 7 \w -24.00 59.00 0.50 25.00 -- -15.84 38.00-180.00 166 8 \w -59.00 34.00 0.50 25.00 -- 15.69 -38.00 -60.00 186 9 \w -86.00 -32.00 0.50 25.00 -- -15.84 -57.00 60.00 108 10 \w -89.00 -21.00 0.50 25.00 -- -15.84 -57.00-180.00 136 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy, Dualflex, HyPix' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0144901000 _diffrn_orient_matrix_UB_12 -0.0293935000 _diffrn_orient_matrix_UB_13 0.0248131000 _diffrn_orient_matrix_UB_21 -0.0307133000 _diffrn_orient_matrix_UB_22 -0.0134875000 _diffrn_orient_matrix_UB_23 0.0038903000 _diffrn_orient_matrix_UB_31 -0.0007337000 _diffrn_orient_matrix_UB_32 -0.0153028000 _diffrn_orient_matrix_UB_33 -0.0509651000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_current 1.0 _diffrn_source_type 'PhotonJet (Mo) X-ray Source' _diffrn_source_voltage 50 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 11561 _reflns_number_total 14658 _reflns_odcompleteness_completeness 99.98 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 30.44 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'CrysAlisPro 1.171.39.43c (Rigaku OD, 2018)' _computing_data_collection 'CrysAlisPro 1.171.39.43c (Rigaku OD, 2018)' _computing_data_reduction 'CrysAlisPro 1.171.39.43c (Rigaku OD, 2018)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _refine_diff_density_max 3.260 _refine_diff_density_min -2.533 _refine_diff_density_rms 0.238 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.025 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 555 _refine_ls_number_reflns 14658 _refine_ls_number_restraints 603 _refine_ls_R_factor_all 0.0704 _refine_ls_R_factor_gt 0.0521 _refine_ls_restrained_S_all 1.032 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0421P)^2^+85.4699P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1129 _refine_ls_wR_factor_ref 0.1208 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups, All N(H,H,H) groups 2. Restrained distances N2_4-C8_4 1.48 with sigma of 0.005 C8_1-C7_1 1.52 with sigma of 0.005 N1_3-C1_3 1.47 with sigma of 0.005 Pb1-I2B \\sim Pb1-I2A with sigma of 0.005 Pb2-I4A \\sim Pb2-I4B with sigma of 0.002 O2_4-N1_4 \\sim O1_4-N1_4 with sigma of 0.002 C6_2-C1_2 \\sim C2_2-C1_2 with sigma of 0.002 C3_2-C2_2 \\sim C6_2-C5_2 with sigma of 0.002 C5_2-C4_2 \\sim C4_2-C3_2 with sigma of 0.002 3. Restrained planarity C2_3, C1_3, C6_3, C5_3, C4_3, C3_3, N1_3 with sigma of 0.002 4. Uiso/Uaniso restraints and constraints I4A \\sim I4B: within 2A with sigma of 0.004 and sigma for terminal atoms of 0.008 I7B \\sim I7A: within 2A with sigma of 0.004 and sigma for terminal atoms of 0.008 Uanis(I7B) \\sim Ueq: with sigma of 0.002 and sigma for terminal atoms of 0.004 Uanis(C6_4) \\sim Ueq: with sigma of 0.002 and sigma for terminal atoms of 0.004 Uanis(C1_2) \\sim Ueq: with sigma of 0.002 and sigma for terminal atoms of 0.004 Uanis(C1_1) \\sim Ueq: with sigma of 0.002 and sigma for terminal atoms of 0.004 Uanis(C1_3) \\sim Ueq: with sigma of 0.002 and sigma for terminal atoms of 0.004 Uanis(I8A) = Uanis(I8B) Uanis(I2A) = Uanis(I2B) 5. Rigid body (RIGU) restrains Pb2, I4A with sigma for 1-2 distances of 0.0002 and sigma for 1-3 distances of 0.0002 O1_4, N1_4, O2_4, C1_4, C2_4, C6_4, C3_4, C5_4, C4_4, C7_4, C8_4, N2_4 with sigma for 1-2 distances of 0.0001 and sigma for 1-3 distances of 0.0001 C7_2, O1_2, N1_2, O2_2, C1_2, C2_2, C6_2, C3_2, C5_2, C4_2, C8_2, N2_2 with sigma for 1-2 distances of 0.0001 and sigma for 1-3 distances of 0.0001 C7_1, O1_1, N1_1, O2_1, C1_1, C2_1, C6_1, C3_1, C5_1, C4_1, C8_1, N2_1 with sigma for 1-2 distances of 0.0001 and sigma for 1-3 distances of 0.0001 C1_3, O1_3, N1_3, O2_3, C2_3, C6_3, C3_3, C5_3, C4_3, C7_3, C8_3, N2_3 with sigma for 1-2 distances of 0.0001 and sigma for 1-3 distances of 0.0001 6. Same fragment restrains {O1_2, O2_2, N1_2, N2_2, C1_2, C2_2, C3_2, C4_2, C5_2, C6_2, C7_2, C8_2} {O1_3, O2_3, N1_3, N2_3, C1_3, C2_3, C3_3, C4_3, C5_3, C6_3, C7_3, C8_3} {O1_4, O2_4, N1_4, N2_4, C1_4, C2_4, C3_4, C4_4, C5_4, C6_4, C7_4, C8_4} as {O1_1, O2_1, N1_1, N2_1, C1_1, C2_1, C3_1, C4_1, C5_1, C6_1, C7_1, C8_1} sigma for 1-2: 0.002 1-3: 0.004 7. Others Sof(I8B)=Sof(I4A)=Sof(I7B)=Sof(I2B)=1-FVAR(1) Sof(I2A)=Sof(I8A)=Sof(I7A)=Sof(I4B)=FVAR(1) 8.a Secondary CH2 refined with riding coordinates: C7(H7A,H7B), C8(H8A,H8B), C7(H7A,H7B), C8(H8A,H8B), C7(H7A,H7B), C8(H8A,H8B), C7(H7A,H7B), C8(H8A,H8B) 8.b Aromatic/amide H refined with riding coordinates: C2(H2), C3(H3), C5(H5), C6(H6), C2(H2), C3(H3), C5(H5), C6(H6), C2(H2), C3(H3), C5(H5), C6(H6), C2(H2), C3(H3), C5(H5), C6(H6) 8.c Idealised Me refined as rotating group: N2(H2A,H2B,H2C), N2(H2A,H2B,H2C), N2(H2A,H2B,H2C), N2(H2A,H2B,H2C) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group I1 I 0.62079(3) 0.59502(3) 0.99335(5) 0.04032(15) Uani 1 1 d . . . . . I8B I 0.81514(8) 0.16864(8) 0.53886(15) 0.0389(2) Uani 0.4076(13) 1 d . . . A 2 I3 I 0.47827(3) 0.47757(4) 0.74536(4) 0.04070(15) Uani 1 1 d . . . . . I5 I 0.56080(3) 0.35279(3) 0.49787(6) 0.04766(17) Uani 1 1 d . . . . . I6 I 0.78379(4) 0.37647(3) 0.50661(6) 0.0540(2) Uani 1 1 d . . . . . Pb1 Pb 0.500000 0.500000 1.000000 0.02431(9) Uani 1 2 d DS T P . . Pb2 Pb 0.500000 0.500000 0.500000 0.02238(9) Uani 1 2 d DS TU P . . Pb3 Pb 0.69303(2) 0.25864(2) 0.52252(2) 0.02703(7) Uani 1 1 d . . . . . I2A I 0.41670(8) 0.63569(7) 0.98525(15) 0.0348(3) Uani 0.5924(13) 1 d D . . A 1 I4A I 0.64063(9) 0.5509(2) 0.5705(3) 0.0408(8) Uani 0.4076(13) 1 d D U . A 1 I7B I 0.67603(14) 0.27640(13) 0.7732(2) 0.0445(5) Uani 0.4076(13) 1 d . U . A 2 I8A I 0.79559(5) 0.15395(6) 0.58059(10) 0.0389(2) Uani 0.5924(13) 1 d . . . A 1 I7A I 0.69130(11) 0.25220(8) 0.77454(13) 0.0487(4) Uani 0.5924(13) 1 d . U . A 1 I2B I 0.40070(12) 0.62166(11) 0.9621(2) 0.0348(3) Uani 0.4076(13) 1 d D . . A 2 I4B I 0.63170(7) 0.56370(14) 0.59626(18) 0.0343(4) Uani 0.5924(13) 1 d D U . A 2 O1_1 O 0.8387(5) 0.6923(6) 0.9924(8) 0.099(3) Uani 1 1 d D U . . . O2_1 O 0.8057(4) 0.7692(5) 1.0914(6) 0.077(2) Uani 1 1 d D U . . . N1_1 N 0.8008(4) 0.7333(4) 1.0142(6) 0.0623(16) Uani 1 1 d D U . . . N2_1 N 0.5175(5) 0.6721(4) 0.7741(8) 0.0580(19) Uani 1 1 d D U . . . H2A_1 H 0.514621 0.650985 0.711296 0.070 Uiso 1 1 calc GR . . . . H2B_1 H 0.484995 0.659595 0.807578 0.070 Uiso 1 1 calc GR . . . . H2C_1 H 0.554312 0.661252 0.814050 0.070 Uiso 1 1 calc GR . . . . C1_1 C 0.7421(4) 0.7420(5) 0.9355(7) 0.0642(14) Uani 1 1 d D U . . . C2_1 C 0.6974(4) 0.7874(5) 0.9555(7) 0.0545(15) Uani 1 1 d D U . . . H2_1 H 0.703976 0.812441 1.018399 0.065 Uiso 1 1 calc R . . . . C3_1 C 0.6435(4) 0.7967(5) 0.8857(6) 0.0537(15) Uani 1 1 d D U . . . H3_1 H 0.612907 0.827502 0.901360 0.064 Uiso 1 1 calc R . . . . C4_1 C 0.6334(4) 0.7600(4) 0.7889(6) 0.0547(11) Uani 1 1 d D U . . . C5_1 C 0.6815(4) 0.7136(5) 0.7710(7) 0.0557(16) Uani 1 1 d D U . . . H5_1 H 0.676601 0.688127 0.708395 0.067 Uiso 1 1 calc R . . . . C6_1 C 0.7343(4) 0.7058(5) 0.8436(7) 0.0604(18) Uani 1 1 d D U . . . H6_1 H 0.765770 0.675295 0.830528 0.072 Uiso 1 1 calc R . . . . C7_1 C 0.5747(4) 0.7692(5) 0.7139(6) 0.0581(11) Uani 1 1 d D U . . . H7A_1 H 0.578504 0.744441 0.648781 0.070 Uiso 1 1 calc R . . . . H7B_1 H 0.570336 0.816643 0.695310 0.070 Uiso 1 1 calc R . . . . C8_1 C 0.5150(4) 0.7463(4) 0.7562(9) 0.0571(15) Uani 1 1 d D U . . . H8A_1 H 0.511501 0.769262 0.823080 0.069 Uiso 1 1 calc R . . . . H8B_1 H 0.477566 0.757665 0.705273 0.069 Uiso 1 1 calc R . . . . O1_2 O 1.0292(5) 0.6067(9) 0.9098(10) 0.155(5) Uani 1 1 d D U . . . O2_2 O 0.9991(6) 0.6464(9) 0.7520(10) 0.153(4) Uani 1 1 d D U . . . N1_2 N 0.9908(5) 0.6166(7) 0.8316(8) 0.120(3) Uani 1 1 d D U . . . N2_2 N 0.6514(4) 0.4414(7) 0.7926(10) 0.102(3) Uani 1 1 d D U . . . H2A_2 H 0.635159 0.462480 0.732576 0.123 Uiso 1 1 calc GR . . . . H2B_2 H 0.623052 0.442231 0.838579 0.123 Uiso 1 1 calc GR . . . . H2C_2 H 0.660086 0.398759 0.777812 0.123 Uiso 1 1 calc GR . . . . C1_2 C 0.9293(4) 0.5797(6) 0.8257(10) 0.0980(18) Uani 1 1 d D U . . . C2_2 C 0.8805(4) 0.5958(6) 0.7481(9) 0.084(2) Uani 1 1 d D U . . . H2_2 H 0.885234 0.631388 0.701886 0.101 Uiso 1 1 calc R . . . . C3_2 C 0.8252(5) 0.5607(7) 0.7370(12) 0.117(3) Uani 1 1 d D U . . . H3_2 H 0.790521 0.574637 0.687917 0.141 Uiso 1 1 calc R . . . . C4_2 C 0.8202(5) 0.5028(6) 0.8004(10) 0.117(2) Uani 1 1 d D U . . . C5_2 C 0.8683(6) 0.4938(7) 0.8893(11) 0.114(3) Uani 1 1 d D U . . . H5_2 H 0.862509 0.462620 0.942143 0.136 Uiso 1 1 calc R . . . . C6_2 C 0.9226(5) 0.5304(6) 0.8974(9) 0.092(2) Uani 1 1 d D U . . . H6_2 H 0.955761 0.521700 0.952706 0.110 Uiso 1 1 calc R . . . . C7_2 C 0.7648(4) 0.4584(6) 0.7784(11) 0.113(2) Uani 1 1 d D U . . . H7A_2 H 0.778352 0.412379 0.795053 0.136 Uiso 1 1 calc R . . . . H7B_2 H 0.748550 0.460409 0.702557 0.136 Uiso 1 1 calc R . . . . C8_2 C 0.7113(5) 0.4759(7) 0.8411(10) 0.108(3) Uani 1 1 d D U . . . H8A_2 H 0.722575 0.461715 0.914976 0.130 Uiso 1 1 calc R . . . . H8B_2 H 0.704719 0.524315 0.840192 0.130 Uiso 1 1 calc R . . . . O1_3 O 1.0357(8) 0.5588(10) 0.5821(13) 0.242(6) Uani 1 1 d D U . . . O2_3 O 1.1138(5) 0.5554(5) 0.7118(8) 0.103(3) Uani 1 1 d D U . . . N1_3 N 1.0627(4) 0.5379(5) 0.6657(8) 0.147(3) Uani 1 1 d D U . . . N2_3 N 0.8838(6) 0.2119(6) 0.8317(11) 0.102(3) Uani 1 1 d D U . . . H2A_3 H 0.856685 0.188040 0.785871 0.122 Uiso 1 1 calc GR . . . . H2B_3 H 0.865552 0.221855 0.889154 0.122 Uiso 1 1 calc GR . . . . H2C_3 H 0.919192 0.187933 0.851508 0.122 Uiso 1 1 calc GR . . . . C1_3 C 1.0343(3) 0.4778(4) 0.7108(5) 0.0919(18) Uani 1 1 d D U . . . C2_3 C 1.0654(4) 0.4494(4) 0.8011(6) 0.0742(18) Uani 1 1 d D U . . . H2_3 H 1.103887 0.467899 0.833356 0.089 Uiso 1 1 calc R . . . . C3_3 C 1.0414(4) 0.3948(4) 0.8449(7) 0.082(2) Uani 1 1 d D U . . . H3_3 H 1.063362 0.375910 0.907019 0.098 Uiso 1 1 calc R . . . . C4_3 C 0.9830(4) 0.3662(5) 0.7968(7) 0.102(3) Uani 1 1 d D U . . . C5_3 C 0.9523(5) 0.3975(5) 0.7028(8) 0.086(2) Uani 1 1 d D U . . . H5_3 H 0.913678 0.380242 0.668518 0.103 Uiso 1 1 calc R . . . . C6_3 C 0.9783(4) 0.4521(4) 0.6622(7) 0.087(3) Uani 1 1 d D U . . . H6_3 H 0.957553 0.472183 0.600161 0.105 Uiso 1 1 calc R . . . . C7_3 C 0.9545(8) 0.3106(8) 0.8492(11) 0.144(3) Uani 1 1 d D U . . . H7A_3 H 0.938531 0.327824 0.912287 0.173 Uiso 1 1 calc R . . . . H7B_3 H 0.987677 0.277832 0.872902 0.173 Uiso 1 1 calc R . . . . C8_3 C 0.9006(11) 0.2755(10) 0.7793(15) 0.196(5) Uani 1 1 d D U . . . H8A_3 H 0.863526 0.304836 0.767484 0.235 Uiso 1 1 calc R . . . . H8B_3 H 0.913541 0.265236 0.710241 0.235 Uiso 1 1 calc R . . . . O1_4 O 0.9546(7) 0.7532(7) 0.3758(13) 0.176(5) Uani 1 1 d D U . . . O2_4 O 0.9839(6) 0.6840(7) 0.5051(11) 0.148(4) Uani 1 1 d D U . . . N1_4 N 0.9484(5) 0.7040(6) 0.4289(10) 0.109(3) Uani 1 1 d D U . . . N2_4 N 0.6805(8) 0.4368(6) 0.2630(16) 0.147(6) Uani 1 1 d D U . . . H2A_4 H 0.649630 0.437195 0.206982 0.177 Uiso 1 1 calc GR . . . . H2B_4 H 0.663940 0.446771 0.322145 0.177 Uiso 1 1 calc GR . . . . H2C_4 H 0.698232 0.395988 0.269674 0.177 Uiso 1 1 calc GR . . . . C1_4 C 0.8911(5) 0.6619(5) 0.3948(8) 0.085(2) Uani 1 1 d D U . . . C2_4 C 0.8788(5) 0.6086(6) 0.4558(9) 0.093(3) Uani 1 1 d D U . . . H2_4 H 0.908171 0.596913 0.515156 0.112 Uiso 1 1 calc R . . . . C3_4 C 0.8247(5) 0.5723(6) 0.4317(9) 0.088(2) Uani 1 1 d D U . . . H3_4 H 0.816321 0.536532 0.475339 0.106 Uiso 1 1 calc R . . . . C4_4 C 0.7807(5) 0.5885(5) 0.3402(8) 0.0901(17) Uani 1 1 d D U . . . C5_4 C 0.7979(5) 0.6410(5) 0.2743(8) 0.082(2) Uani 1 1 d D U . . . H5_4 H 0.772289 0.650352 0.209643 0.099 Uiso 1 1 calc R . . . . C6_4 C 0.8511(6) 0.6777(7) 0.3046(10) 0.1026(19) Uani 1 1 d D U . . . H6_4 H 0.860513 0.714169 0.263207 0.123 Uiso 1 1 calc R . . . . C7_4 C 0.7221(5) 0.5493(5) 0.3134(10) 0.0926(17) Uani 1 1 d D U . . . H7A_4 H 0.689392 0.577969 0.274532 0.111 Uiso 1 1 calc R . . . . H7B_4 H 0.707066 0.535380 0.379166 0.111 Uiso 1 1 calc R . . . . C8_4 C 0.7301(6) 0.4876(6) 0.2467(12) 0.097(3) Uani 1 1 d D U . . . H8A_4 H 0.725973 0.499920 0.171634 0.116 Uiso 1 1 calc R . . . . H8B_4 H 0.772452 0.468568 0.267472 0.116 Uiso 1 1 calc R . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 I1 0.0499(4) 0.0349(3) 0.0403(3) -0.0060(2) 0.0203(3) -0.0107(3) I8B 0.0360(5) 0.0337(5) 0.0466(6) 0.0041(4) 0.0046(4) 0.0078(4) I3 0.0466(3) 0.0620(4) 0.0140(2) -0.0038(2) 0.0061(2) -0.0152(3) I5 0.0482(4) 0.0300(3) 0.0616(4) -0.0037(3) -0.0031(3) 0.0130(3) I6 0.0741(5) 0.0312(3) 0.0639(4) -0.0100(3) 0.0346(4) -0.0206(3) Pb1 0.0386(2) 0.01832(17) 0.01633(17) 0.00090(14) 0.00493(15) 0.00483(16) Pb2 0.0272(2) 0.02420(18) 0.01482(16) -0.00292(14) -0.00021(14) 0.00317(15) Pb3 0.03655(17) 0.02407(14) 0.01912(13) 0.00255(10) -0.00066(11) -0.00272(12) I2A 0.0407(9) 0.0195(6) 0.0428(9) 0.0051(5) 0.0008(6) 0.0063(5) I4A 0.0562(14) 0.0351(14) 0.0260(15) 0.0023(9) -0.0115(9) -0.0150(11) I7B 0.0698(12) 0.0484(12) 0.0150(7) 0.0015(9) 0.0056(7) 0.0064(10) I8A 0.0360(5) 0.0337(5) 0.0466(6) 0.0041(4) 0.0046(4) 0.0078(4) I7A 0.0946(13) 0.0381(8) 0.0136(5) 0.0009(6) 0.0082(6) 0.0008(7) I2B 0.0407(9) 0.0195(6) 0.0428(9) 0.0051(5) 0.0008(6) 0.0063(5) I4B 0.0337(6) 0.0394(11) 0.0259(10) 0.0039(6) -0.0085(5) -0.0123(6) O1_1 0.090(2) 0.112(4) 0.088(3) -0.025(3) -0.011(2) 0.031(3) O2_1 0.077(3) 0.079(4) 0.071(2) -0.004(2) 0.001(2) 0.009(3) N1_1 0.0673(17) 0.059(3) 0.0612(18) 0.0104(19) 0.0109(16) -0.0039(18) N2_1 0.065(4) 0.063(3) 0.048(5) 0.009(3) 0.012(4) -0.0119(18) C1_1 0.0688(16) 0.062(2) 0.0621(16) 0.0061(14) 0.0097(12) -0.0013(14) C2_1 0.0637(17) 0.048(3) 0.0533(17) 0.0149(19) 0.0145(15) -0.0096(18) C3_1 0.0631(17) 0.048(3) 0.0521(18) 0.0152(18) 0.0154(15) -0.0102(19) C4_1 0.0623(16) 0.051(2) 0.0530(17) 0.0135(15) 0.0154(14) -0.0096(14) C5_1 0.0623(18) 0.050(3) 0.0567(17) 0.0127(19) 0.0163(15) -0.0101(19) C6_1 0.0652(19) 0.057(3) 0.0603(17) 0.009(2) 0.0132(16) -0.005(2) C7_1 0.0628(16) 0.061(3) 0.0526(18) 0.0120(16) 0.0152(14) -0.0076(15) C8_1 0.0628(16) 0.063(3) 0.047(3) 0.008(3) 0.0129(18) -0.0114(18) O1_2 0.108(3) 0.216(12) 0.136(4) 0.057(6) -0.005(3) -0.034(5) O2_2 0.113(4) 0.205(9) 0.134(4) 0.053(4) -0.008(3) -0.039(5) N1_2 0.102(2) 0.134(5) 0.120(3) 0.021(3) 0.006(2) -0.008(3) N2_2 0.095(2) 0.117(7) 0.092(6) 0.065(4) 0.005(3) 0.021(3) C1_2 0.0943(19) 0.101(2) 0.100(2) -0.0015(17) 0.0164(15) 0.0083(15) C2_2 0.090(2) 0.081(4) 0.084(3) -0.019(3) 0.025(2) 0.019(2) C3_2 0.101(2) 0.117(4) 0.129(5) 0.026(4) 0.000(3) -0.001(2) C4_2 0.099(2) 0.118(3) 0.131(4) 0.028(3) 0.003(2) 0.002(2) C5_2 0.094(3) 0.118(5) 0.126(4) 0.025(4) 0.008(3) 0.006(3) C6_2 0.087(2) 0.095(4) 0.097(3) -0.006(3) 0.025(2) 0.019(2) C7_2 0.096(2) 0.116(3) 0.124(4) 0.028(3) 0.006(2) 0.005(2) C8_2 0.095(3) 0.115(6) 0.110(5) 0.057(5) 0.001(3) 0.024(3) O1_3 0.209(6) 0.262(7) 0.214(5) 0.139(6) -0.107(5) -0.143(6) O2_3 0.101(3) 0.112(4) 0.095(5) 0.002(4) 0.006(3) -0.012(3) N1_3 0.129(3) 0.151(4) 0.145(4) 0.050(3) -0.032(3) -0.046(3) N2_3 0.083(6) 0.138(4) 0.087(7) 0.024(5) 0.019(5) -0.013(4) C1_3 0.089(2) 0.094(2) 0.092(2) -0.0034(16) 0.0121(15) 0.0026(15) C2_3 0.075(2) 0.077(3) 0.075(2) -0.021(2) 0.027(2) 0.020(2) C3_3 0.081(3) 0.086(3) 0.082(3) -0.013(3) 0.020(2) 0.013(2) C4_3 0.096(3) 0.107(4) 0.099(4) 0.007(3) 0.004(3) -0.005(3) C5_3 0.085(3) 0.089(3) 0.085(3) -0.008(3) 0.016(3) 0.007(3) C6_3 0.086(2) 0.089(3) 0.087(3) -0.008(3) 0.016(3) 0.006(3) C7_3 0.125(5) 0.162(4) 0.131(4) 0.050(3) -0.028(3) -0.045(4) C8_3 0.199(6) 0.209(5) 0.151(6) 0.091(5) -0.071(5) -0.108(5) O1_4 0.173(5) 0.153(5) 0.179(6) 0.059(5) -0.050(5) -0.063(5) O2_4 0.147(4) 0.133(6) 0.152(5) 0.034(5) -0.026(4) -0.039(4) N1_4 0.119(3) 0.097(4) 0.111(4) -0.003(3) 0.009(3) -0.008(3) N2_4 0.149(7) 0.101(4) 0.205(14) -0.060(6) 0.073(9) -0.018(4) C1_4 0.098(2) 0.072(3) 0.089(2) -0.024(2) 0.028(2) 0.015(2) C2_4 0.105(3) 0.082(3) 0.094(3) -0.016(3) 0.020(3) 0.007(2) C3_4 0.101(3) 0.075(3) 0.090(3) -0.020(3) 0.023(2) 0.011(2) C4_4 0.101(2) 0.081(3) 0.091(3) -0.017(2) 0.023(2) 0.010(2) C5_4 0.093(2) 0.072(3) 0.088(3) -0.023(2) 0.031(2) 0.020(2) C6_4 0.109(2) 0.097(2) 0.103(2) -0.0043(16) 0.0163(15) -0.0006(16) C7_4 0.101(2) 0.079(3) 0.099(4) -0.013(2) 0.020(2) 0.011(2) C8_4 0.100(4) 0.084(3) 0.105(7) -0.020(4) 0.010(4) 0.014(3) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag I1 Pb1 3.1797(6) . ? I8B Pb3 3.1162(16) . ? I3 Pb1 3.2102(5) . ? I3 Pb2 3.2240(5) . ? I5 Pb2 3.1896(6) . ? I5 Pb3 3.3340(7) . ? I6 Pb3 3.0453(7) . ? Pb1 I2A 3.2041(14) . ? Pb1 I2A 3.2040(14) 3_667 ? Pb1 I2B 3.186(2) 3_667 ? Pb1 I2B 3.186(2) . ? Pb2 I4A 3.1398(15) . ? Pb2 I4A 3.1399(15) 3_666 ? Pb2 I4B 3.1343(10) 3_666 ? Pb2 I4B 3.1343(10) . ? Pb3 I2A 3.3535(15) 2_646 ? Pb3 I7B 3.253(3) . ? Pb3 I7B 3.190(2) 4_565 ? Pb3 I8A 3.0122(11) . ? Pb3 I7A 3.1306(17) 4_565 ? Pb3 I7A 3.1872(17) . ? Pb3 I2B 3.381(2) 2_646 ? O1_1 N1_1 1.200(5) . ? O2_1 N1_1 1.199(5) . ? N1_1 C1_1 1.482(5) . ? N2_1 C8_1 1.489(5) . ? C1_1 C2_1 1.352(6) . ? C1_1 C6_1 1.353(6) . ? C2_1 C3_1 1.348(7) . ? C3_1 C4_1 1.411(7) . ? C4_1 C5_1 1.411(7) . ? C4_1 C7_1 1.458(10) . ? C5_1 C6_1 1.348(7) . ? C7_1 C8_1 1.508(5) . ? O1_2 N1_2 1.200(5) . ? O2_2 N1_2 1.200(5) . ? N1_2 C1_2 1.482(5) . ? N2_2 C8_2 1.490(5) . ? C1_2 C2_2 1.353(6) . ? C1_2 C6_2 1.352(6) . ? C2_2 C3_2 1.349(7) . ? C3_2 C4_2 1.412(7) . ? C4_2 C5_2 1.412(7) . ? C4_2 C7_2 1.458(10) . ? C5_2 C6_2 1.348(7) . ? C7_2 C8_2 1.508(5) . ? O1_3 N1_3 1.200(5) . ? O2_3 N1_3 1.201(5) . ? N1_3 C1_3 1.482(5) . ? N2_3 C8_3 1.489(5) . ? C1_3 C2_3 1.353(6) . ? C1_3 C6_3 1.352(6) . ? C2_3 C3_3 1.347(7) . ? C3_3 C4_3 1.412(7) . ? C4_3 C5_3 1.411(7) . ? C4_3 C7_3 1.458(10) . ? C5_3 C6_3 1.348(7) . ? C7_3 C8_3 1.507(5) . ? O1_4 N1_4 1.200(5) . ? O2_4 N1_4 1.199(5) . ? N1_4 C1_4 1.482(5) . ? N2_4 C8_4 1.489(5) . ? C1_4 C2_4 1.353(6) . ? C1_4 C6_4 1.352(6) . ? C2_4 C3_4 1.348(7) . ? C3_4 C4_4 1.411(7) . ? C4_4 C5_4 1.411(7) . ? C4_4 C7_4 1.459(10) . ? C5_4 C6_4 1.347(7) . ? C7_4 C8_4 1.508(5) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Pb1 I3 Pb2 157.22(2) . . ? Pb2 I5 Pb3 147.53(3) . . ? I1 Pb1 I1 180.0 3_667 . ? I1 Pb1 I3 86.794(16) 3_667 . ? I1 Pb1 I3 93.206(16) . . ? I1 Pb1 I3 93.205(16) 3_667 3_667 ? I1 Pb1 I3 86.794(16) . 3_667 ? I1 Pb1 I2A 86.33(3) . . ? I1 Pb1 I2A 93.67(3) 3_667 . ? I1 Pb1 I2A 86.33(3) 3_667 3_667 ? I1 Pb1 I2A 93.67(3) . 3_667 ? I1 Pb1 I2B 93.43(5) . . ? I1 Pb1 I2B 93.43(5) 3_667 3_667 ? I1 Pb1 I2B 86.57(5) . 3_667 ? I1 Pb1 I2B 86.57(5) 3_667 . ? I3 Pb1 I3 180.00(2) 3_667 . ? I2A Pb1 I3 93.42(4) 3_667 3_667 ? I2A Pb1 I3 93.42(4) . . ? I2A Pb1 I3 86.58(4) 3_667 . ? I2A Pb1 I3 86.58(4) . 3_667 ? I2A Pb1 I2A 180.00(6) 3_667 . ? I2B Pb1 I3 92.40(6) 3_667 . ? I2B Pb1 I3 87.60(6) . . ? I2B Pb1 I2B 180.00(9) 3_667 . ? I3 Pb2 I3 180.0 . 3_666 ? I5 Pb2 I3 89.681(19) 3_666 3_666 ? I5 Pb2 I3 89.682(19) . . ? I5 Pb2 I3 90.318(19) . 3_666 ? I5 Pb2 I3 90.318(19) 3_666 . ? I5 Pb2 I5 180.0 3_666 . ? I4A Pb2 I3 91.76(7) 3_666 3_666 ? I4A Pb2 I3 91.77(7) . . ? I4A Pb2 I3 88.23(7) 3_666 . ? I4A Pb2 I3 88.24(7) . 3_666 ? I4A Pb2 I5 86.09(8) 3_666 3_666 ? I4A Pb2 I5 86.09(8) . . ? I4A Pb2 I5 93.91(8) 3_666 . ? I4A Pb2 I5 93.91(8) . 3_666 ? I4A Pb2 I4A 180.00(12) . 3_666 ? I4B Pb2 I3 85.62(5) . . ? I4B Pb2 I3 94.38(5) 3_666 . ? I4B Pb2 I5 92.10(5) . . ? I4B Pb2 I5 87.90(5) 3_666 . ? I4B Pb2 I4B 180.0 3_666 . ? I8B Pb3 I5 178.26(4) . . ? I8B Pb3 I7B 101.70(6) . . ? I5 Pb3 I2A 80.75(3) . 2_646 ? I5 Pb3 I2B 88.09(5) . 2_646 ? I6 Pb3 I8B 85.52(4) . . ? I6 Pb3 I5 95.16(2) . . ? I6 Pb3 I2A 173.52(3) . 2_646 ? I6 Pb3 I7B 97.98(5) . . ? I6 Pb3 I7B 94.88(5) . 4_565 ? I6 Pb3 I7A 84.51(4) . 4_565 ? I6 Pb3 I7A 101.16(4) . . ? I6 Pb3 I2B 176.65(5) . 2_646 ? I2A Pb3 I2B 8.47(4) 2_646 2_646 ? I7B Pb3 I5 93.18(6) 4_565 . ? I7B Pb3 I5 79.80(5) . . ? I7B Pb3 I7B 165.83(10) 4_565 . ? I8A Pb3 I5 166.14(3) . . ? I8A Pb3 I6 96.20(3) . . ? I8A Pb3 I2A 88.58(3) . 2_646 ? I8A Pb3 I7B 93.74(6) . 4_565 ? I8A Pb3 I7A 80.80(4) . . ? I8A Pb3 I7A 95.80(4) . 4_565 ? I8A Pb3 I2B 80.70(5) . 2_646 ? I7A Pb3 I5 93.16(4) 4_565 . ? I7A Pb3 I5 89.23(4) . . ? I7A Pb3 I2A 83.90(5) . 2_646 ? I7A Pb3 I2A 90.67(5) 4_565 2_646 ? I7A Pb3 I7B 163.50(5) . 4_565 ? I7A Pb3 I7B 10.42(4) 4_565 4_565 ? I7A Pb3 I7A 173.63(2) 4_565 . ? I7A Pb3 I2B 94.52(6) 4_565 2_646 ? I7A Pb3 I2B 79.66(6) . 2_646 ? Pb1 I2A Pb3 169.29(6) . 2_656 ? Pb3 I7B Pb3 157.28(9) 4_566 . ? Pb3 I7A Pb3 177.90(7) 4_566 . ? Pb1 I2B Pb3 167.69(9) . 2_656 ? O1_1 N1_1 C1_1 116.5(6) . . ? O2_1 N1_1 O1_1 127.3(7) . . ? O2_1 N1_1 C1_1 116.2(6) . . ? C2_1 C1_1 N1_1 119.4(5) . . ? C2_1 C1_1 C6_1 120.7(7) . . ? C6_1 C1_1 N1_1 120.0(5) . . ? C3_1 C2_1 C1_1 121.0(7) . . ? C2_1 C3_1 C4_1 120.2(7) . . ? C3_1 C4_1 C5_1 116.9(8) . . ? C3_1 C4_1 C7_1 120.4(6) . . ? C5_1 C4_1 C7_1 122.7(6) . . ? C6_1 C5_1 C4_1 120.6(7) . . ? C5_1 C6_1 C1_1 120.6(7) . . ? C4_1 C7_1 C8_1 114.0(5) . . ? N2_1 C8_1 C7_1 109.7(5) . . ? O1_2 N1_2 C1_2 116.3(6) . . ? O2_2 N1_2 O1_2 127.3(8) . . ? O2_2 N1_2 C1_2 115.7(6) . . ? C2_2 C1_2 N1_2 119.3(5) . . ? C6_2 C1_2 N1_2 119.8(5) . . ? C6_2 C1_2 C2_2 120.9(7) . . ? C3_2 C2_2 C1_2 120.7(7) . . ? C2_2 C3_2 C4_2 119.6(7) . . ? C3_2 C4_2 C5_2 116.7(8) . . ? C3_2 C4_2 C7_2 120.4(6) . . ? C5_2 C4_2 C7_2 122.7(6) . . ? C6_2 C5_2 C4_2 120.0(7) . . ? C5_2 C6_2 C1_2 120.4(7) . . ? C4_2 C7_2 C8_2 113.7(6) . . ? N2_2 C8_2 C7_2 109.5(6) . . ? O1_3 N1_3 O2_3 127.3(8) . . ? O1_3 N1_3 C1_3 116.7(6) . . ? O2_3 N1_3 C1_3 115.5(6) . . ? C2_3 C1_3 N1_3 118.9(5) . . ? C6_3 C1_3 N1_3 120.3(5) . . ? C6_3 C1_3 C2_3 120.8(7) . . ? C3_3 C2_3 C1_3 121.0(7) . . ? C2_3 C3_3 C4_3 120.1(7) . . ? C3_3 C4_3 C7_3 119.9(6) . . ? C5_3 C4_3 C3_3 117.0(8) . . ? C5_3 C4_3 C7_3 122.9(6) . . ? C6_3 C5_3 C4_3 120.5(7) . . ? C5_3 C6_3 C1_3 120.6(7) . . ? C4_3 C7_3 C8_3 114.2(5) . . ? N2_3 C8_3 C7_3 109.8(6) . . ? O1_4 N1_4 C1_4 116.5(6) . . ? O2_4 N1_4 O1_4 127.6(8) . . ? O2_4 N1_4 C1_4 115.9(6) . . ? C2_4 C1_4 N1_4 119.3(5) . . ? C6_4 C1_4 N1_4 119.8(5) . . ? C6_4 C1_4 C2_4 120.9(7) . . ? C3_4 C2_4 C1_4 120.9(7) . . ? C2_4 C3_4 C4_4 120.0(7) . . ? C3_4 C4_4 C5_4 117.1(8) . . ? C3_4 C4_4 C7_4 120.3(6) . . ? C5_4 C4_4 C7_4 122.5(6) . . ? C6_4 C5_4 C4_4 120.3(7) . . ? C5_4 C6_4 C1_4 120.5(7) . . ? C4_4 C7_4 C8_4 113.7(5) . . ? N2_4 C8_4 C7_4 109.5(6) . . ? _shelx_res_file ; TITL MHT-III-53 in P2(1)/c mht-iii-53.res created by SHELXL-2018/3 at 15:13:33 on 20-Oct-2018 REM P2(1)/c (#14 in standard setting) CELL 0.71073 21.097616 19.825465 12.614931 90 98.2252 90 ZERR 8 0.000427 0.000343 0.000197 0 0.0017 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H I N O Pb UNIT 128 176 32 32 32 8 DFIX_4 1.48 0.005 N2 C8 DFIX_1 1.52 0.005 C8 C7 DFIX_3 1.47 0.005 N1 C1 SADI 0.005 Pb1 I2B Pb1 I2A SADI 0.002 Pb2 I4A Pb2 I4B SADI_4 0.002 O2 N1 O1 N1 SADI_2 0.002 C6 C1 C2 C1 SADI_2 0.002 C3 C2 C6 C5 SADI_2 0.002 C5 C4 C4 C3 FLAT_3 0.002 C2 C1 C6 C5 C4 C3 N1 SIMU 0.004 0.008 2 I4A I4B SIMU 0.004 0.008 2 I7b I7a RIGU 0.0002 0.0002 Pb2 I4A RIGU_4 0.0001 0.0001 O1 N1 O2 C1 C2 C6 C3 C5 C4 C7 C8 N2 RIGU_2 0.0001 0.0001 C7 O1 N1 O2 C1 C2 C6 C3 C5 C4 C8 N2 RIGU_1 0.0001 0.0001 C7 O1 N1 O2 C1 C2 C6 C3 C5 C4 C8 N2 RIGU_3 0.0001 0.0001 C1 O1 N1 O2 C2 C6 C3 C5 C4 C7 C8 N2 ISOR 0.002 0.004 I7b ISOR_4 0.002 0.004 C6 ISOR_2 0.002 0.004 C1 ISOR_1 0.002 0.004 C1 ISOR_3 0.002 0.004 C1 EADP I8a I8b EADP I2A I2B SAME_4NPE 0.002 0.004 O1 > C8 L.S. 9 PLAN 20 list 4 fmap 2 acta SHEL 20 0.72 OMIT 7 0 2 OMIT 1 3 1 OMIT 8 0 2 REM REM REM WGHT 0.042100 85.469902 FVAR 0.07848 0.59237 I1 3 0.620786 0.595020 0.993346 11.00000 0.04988 0.03489 = 0.04026 -0.00602 0.02033 -0.01065 PART 2 I8B 3 0.815135 0.168638 0.538855 -21.00000 0.03596 0.03370 = 0.04660 0.00412 0.00464 0.00783 PART 0 I3 3 0.478269 0.477565 0.745357 11.00000 0.04658 0.06199 = 0.01403 -0.00382 0.00607 -0.01525 I5 3 0.560801 0.352790 0.497870 11.00000 0.04818 0.03000 = 0.06158 -0.00371 -0.00314 0.01301 I6 3 0.783789 0.376466 0.506610 11.00000 0.07409 0.03120 = 0.06387 -0.00999 0.03456 -0.02057 PB1 6 0.500000 0.500000 1.000000 10.50000 0.03855 0.01832 = 0.01633 0.00090 0.00493 0.00483 PB2 6 0.500000 0.500000 0.500000 10.50000 0.02717 0.02420 = 0.01482 -0.00292 -0.00021 0.00317 PB3 6 0.693029 0.258636 0.522521 11.00000 0.03655 0.02407 = 0.01912 0.00255 -0.00066 -0.00272 PART 1 I2A 3 0.416701 0.635689 0.985249 21.00000 0.04066 0.01947 = 0.04282 0.00515 0.00081 0.00627 I4A 3 0.640626 0.550944 0.570509 -21.00000 0.05618 0.03512 = 0.02595 0.00229 -0.01147 -0.01497 PART 0 PART 2 I7B 3 0.676029 0.276404 0.773219 -21.00000 0.06985 0.04841 = 0.01497 0.00151 0.00562 0.00644 PART 0 PART 1 I8A 3 0.795594 0.153948 0.580593 21.00000 0.03596 0.03370 = 0.04660 0.00412 0.00464 0.00783 I7A 3 0.691298 0.252197 0.774544 21.00000 0.09459 0.03807 = 0.01364 0.00087 0.00821 0.00078 PART 0 PART 2 I2B 3 0.400700 0.621660 0.962142 -21.00000 0.04066 0.01947 = 0.04282 0.00515 0.00081 0.00627 I4B 3 0.631696 0.563699 0.596264 21.00000 0.03375 0.03939 = 0.02593 0.00387 -0.00854 -0.01235 RESI 4NPE 1 PART 0 O1 5 0.838695 0.692268 0.992433 11.00000 0.08990 0.11220 = 0.08762 -0.02474 -0.01116 0.03086 O2 5 0.805660 0.769221 1.091432 11.00000 0.07726 0.07935 = 0.07098 -0.00380 0.00066 0.00943 N1 4 0.800792 0.733322 1.014164 11.00000 0.06731 0.05897 = 0.06118 0.01040 0.01090 -0.00386 N2 4 0.517474 0.672071 0.774084 11.00000 0.06474 0.06275 = 0.04775 0.00870 0.01240 -0.01187 AFIX 137 H2A 2 0.514621 0.650985 0.711296 11.00000 -1.20000 H2B 2 0.484995 0.659595 0.807578 11.00000 -1.20000 H2C 2 0.554312 0.661252 0.814050 11.00000 -1.20000 AFIX 0 C1 1 0.742132 0.742032 0.935472 11.00000 0.06884 0.06161 = 0.06209 0.00614 0.00966 -0.00126 C2 1 0.697424 0.787354 0.955490 11.00000 0.06371 0.04834 = 0.05331 0.01485 0.01452 -0.00965 AFIX 43 H2 2 0.703976 0.812441 1.018399 11.00000 -1.20000 AFIX 0 C3 1 0.643524 0.796732 0.885703 11.00000 0.06307 0.04793 = 0.05207 0.01522 0.01541 -0.01017 AFIX 43 H3 2 0.612907 0.827502 0.901360 11.00000 -1.20000 AFIX 0 C4 1 0.633408 0.759999 0.788943 11.00000 0.06230 0.05079 = 0.05304 0.01348 0.01543 -0.00961 C5 1 0.681467 0.713583 0.770956 11.00000 0.06228 0.05043 = 0.05666 0.01267 0.01630 -0.01010 AFIX 43 H5 2 0.676601 0.688127 0.708395 11.00000 -1.20000 AFIX 0 C6 1 0.734338 0.705829 0.843633 11.00000 0.06515 0.05691 = 0.06031 0.00900 0.01324 -0.00530 AFIX 43 H6 2 0.765770 0.675295 0.830528 11.00000 -1.20000 AFIX 0 C7 1 0.574734 0.769228 0.713880 11.00000 0.06281 0.06108 = 0.05257 0.01202 0.01517 -0.00757 AFIX 23 H7A 2 0.578504 0.744441 0.648781 11.00000 -1.20000 H7B 2 0.570336 0.816643 0.695310 11.00000 -1.20000 AFIX 0 C8 1 0.514955 0.746325 0.756228 11.00000 0.06277 0.06272 = 0.04741 0.00824 0.01290 -0.01137 AFIX 23 H8A 2 0.511501 0.769262 0.823080 11.00000 -1.20000 H8B 2 0.477566 0.757665 0.705273 11.00000 -1.20000 AFIX 0 RESI 4NPE 2 O1 5 1.029172 0.606725 0.909842 11.00000 0.10789 0.21613 = 0.13574 0.05721 -0.00491 -0.03399 O2 5 0.999098 0.646422 0.751966 11.00000 0.11335 0.20536 = 0.13413 0.05273 -0.00784 -0.03894 N1 4 0.990781 0.616587 0.831567 11.00000 0.10227 0.13376 = 0.11973 0.02096 0.00561 -0.00802 N2 4 0.651367 0.441364 0.792636 11.00000 0.09491 0.11713 = 0.09184 0.06512 0.00519 0.02061 AFIX 137 H2A 2 0.635159 0.462480 0.732576 11.00000 -1.20000 H2B 2 0.623052 0.442231 0.838579 11.00000 -1.20000 H2C 2 0.660086 0.398759 0.777812 11.00000 -1.20000 AFIX 0 C1 1 0.929259 0.579699 0.825728 11.00000 0.09431 0.10091 = 0.09963 -0.00146 0.01640 0.00831 C2 1 0.880528 0.595775 0.748109 11.00000 0.08971 0.08115 = 0.08427 -0.01860 0.02533 0.01877 AFIX 43 H2 2 0.885234 0.631388 0.701886 11.00000 -1.20000 AFIX 0 C3 1 0.825187 0.560726 0.737009 11.00000 0.10118 0.11654 = 0.12931 0.02593 0.00021 -0.00129 AFIX 43 H3 2 0.790521 0.574637 0.687917 11.00000 -1.20000 AFIX 0 C4 1 0.820196 0.502786 0.800368 11.00000 0.09881 0.11800 = 0.13071 0.02784 0.00297 0.00235 C5 1 0.868300 0.493782 0.889265 11.00000 0.09436 0.11809 = 0.12599 0.02465 0.00752 0.00573 AFIX 43 H5 2 0.862509 0.462620 0.942143 11.00000 -1.20000 AFIX 0 C6 1 0.922635 0.530398 0.897432 11.00000 0.08708 0.09457 = 0.09664 -0.00577 0.02484 0.01885 AFIX 43 H6 2 0.955761 0.521700 0.952706 11.00000 -1.20000 AFIX 0 C7 1 0.764780 0.458389 0.778417 11.00000 0.09601 0.11583 = 0.12442 0.02792 0.00626 0.00461 AFIX 23 H7A 2 0.778352 0.412379 0.795053 11.00000 -1.20000 H7B 2 0.748550 0.460409 0.702557 11.00000 -1.20000 AFIX 0 C8 1 0.711302 0.475883 0.841086 11.00000 0.09549 0.11450 = 0.11049 0.05680 0.00150 0.02413 AFIX 23 H8A 2 0.722575 0.461715 0.914976 11.00000 -1.20000 H8B 2 0.704719 0.524315 0.840192 11.00000 -1.20000 AFIX 0 RESI 4NPE 3 O1 5 1.035687 0.558843 0.582066 11.00000 0.20897 0.26177 = 0.21433 0.13878 -0.10739 -0.14325 O2 5 1.113800 0.555406 0.711791 11.00000 0.10118 0.11197 = 0.09478 0.00234 0.00608 -0.01207 N1 4 1.062689 0.537869 0.665745 11.00000 0.12928 0.15149 = 0.14475 0.05029 -0.03220 -0.04583 N2 4 0.883826 0.211933 0.831725 11.00000 0.08308 0.13780 = 0.08737 0.02448 0.01908 -0.01332 AFIX 137 H2A 2 0.856685 0.188040 0.785871 11.00000 -1.20000 H2B 2 0.865552 0.221855 0.889154 11.00000 -1.20000 H2C 2 0.919192 0.187933 0.851508 11.00000 -1.20000 AFIX 0 C1 1 1.034330 0.477832 0.710813 11.00000 0.08914 0.09409 = 0.09215 -0.00339 0.01211 0.00258 C2 1 1.065390 0.449434 0.801073 11.00000 0.07535 0.07686 = 0.07535 -0.02116 0.02745 0.01989 AFIX 43 H2 2 1.103887 0.467899 0.833356 11.00000 -1.20000 AFIX 0 C3 1 1.041417 0.394820 0.844915 11.00000 0.08096 0.08564 = 0.08162 -0.01286 0.02034 0.01307 AFIX 43 H3 2 1.063362 0.375910 0.907019 11.00000 -1.20000 AFIX 0 C4 1 0.983025 0.366220 0.796763 11.00000 0.09621 0.10718 = 0.09944 0.00747 0.00392 -0.00528 C5 1 0.952254 0.397466 0.702754 11.00000 0.08479 0.08851 = 0.08539 -0.00823 0.01628 0.00739 AFIX 43 H5 2 0.913678 0.380242 0.668518 11.00000 -1.20000 AFIX 0 C6 1 0.978306 0.452060 0.662178 11.00000 0.08569 0.08925 = 0.08745 -0.00755 0.01611 0.00646 AFIX 43 H6 2 0.957553 0.472183 0.600161 11.00000 -1.20000 AFIX 0 C7 1 0.954544 0.310622 0.849192 11.00000 0.12502 0.16177 = 0.13137 0.05013 -0.02776 -0.04491 AFIX 23 H7A 2 0.938531 0.327824 0.912287 11.00000 -1.20000 H7B 2 0.987677 0.277832 0.872902 11.00000 -1.20000 AFIX 0 C8 1 0.900644 0.275472 0.779252 11.00000 0.19898 0.20934 = 0.15121 0.09141 -0.07051 -0.10751 AFIX 23 H8A 2 0.863526 0.304836 0.767484 11.00000 -1.20000 H8B 2 0.913541 0.265236 0.710241 11.00000 -1.20000 AFIX 0 RESI 4NPE 4 O1 5 0.954613 0.753152 0.375841 11.00000 0.17339 0.15349 = 0.17948 0.05896 -0.04986 -0.06281 O2 5 0.983877 0.684038 0.505131 11.00000 0.14691 0.13253 = 0.15170 0.03395 -0.02595 -0.03908 N1 4 0.948359 0.704025 0.428883 11.00000 0.11911 0.09653 = 0.11050 -0.00327 0.00869 -0.00757 N2 4 0.680494 0.436779 0.263019 11.00000 0.14939 0.10105 = 0.20544 -0.05953 0.07268 -0.01797 AFIX 137 H2A 2 0.649630 0.437195 0.206982 11.00000 -1.20000 H2B 2 0.663940 0.446771 0.322145 11.00000 -1.20000 H2C 2 0.698232 0.395988 0.269674 11.00000 -1.20000 AFIX 0 C1 1 0.891056 0.661868 0.394828 11.00000 0.09807 0.07229 = 0.08863 -0.02353 0.02822 0.01512 C2 1 0.878831 0.608619 0.455809 11.00000 0.10521 0.08170 = 0.09387 -0.01596 0.02001 0.00654 AFIX 43 H2 2 0.908171 0.596913 0.515156 11.00000 -1.20000 AFIX 0 C3 1 0.824674 0.572297 0.431683 11.00000 0.10147 0.07529 = 0.08994 -0.01991 0.02327 0.01143 AFIX 43 H3 2 0.816321 0.536532 0.475339 11.00000 -1.20000 AFIX 0 C4 1 0.780652 0.588533 0.340198 11.00000 0.10075 0.08141 = 0.09085 -0.01665 0.02338 0.00982 C5 1 0.797858 0.641026 0.274318 11.00000 0.09270 0.07155 = 0.08786 -0.02256 0.03055 0.01984 AFIX 43 H5 2 0.772289 0.650352 0.209643 11.00000 -1.20000 AFIX 0 C6 1 0.851127 0.677692 0.304632 11.00000 0.10886 0.09681 = 0.10257 -0.00427 0.01632 -0.00062 AFIX 43 H6 2 0.860513 0.714169 0.263207 11.00000 -1.20000 AFIX 0 C7 1 0.722062 0.549321 0.313354 11.00000 0.10075 0.07919 = 0.09936 -0.01346 0.01964 0.01075 AFIX 23 H7A 2 0.689392 0.577969 0.274532 11.00000 -1.20000 H7B 2 0.707066 0.535380 0.379166 11.00000 -1.20000 AFIX 0 C8 1 0.730138 0.487593 0.246723 11.00000 0.09965 0.08408 = 0.10458 -0.02006 0.01041 0.01366 AFIX 23 H8A 2 0.725973 0.499920 0.171634 11.00000 -1.20000 H8B 2 0.772452 0.468568 0.267472 11.00000 -1.20000 AFIX 0 HKLF 4 REM MHT-III-53 in P2(1)/c REM wR2 = 0.1208, GooF = S = 1.025, Restrained GooF = 1.032 for all data REM R1 = 0.0521 for 11561 Fo > 4sig(Fo) and 0.0704 for all 14658 data REM 555 parameters refined using 603 restraints END WGHT 0.0421 85.4813 REM Highest difference peak 3.260, deepest hole -2.533, 1-sigma level 0.238 Q1 1 0.7367 0.4984 0.8554 11.00000 0.05 3.26 Q2 1 0.6551 0.2467 0.7634 11.00000 0.05 2.82 Q3 1 0.7194 0.4396 0.7710 11.00000 0.05 2.71 Q4 1 0.4682 0.5098 0.7418 11.00000 0.05 2.65 Q5 1 0.5480 0.3661 0.5417 11.00000 0.05 2.44 Q6 1 0.5910 0.6049 0.9651 11.00000 0.05 2.39 Q7 1 0.8023 0.5271 0.8437 11.00000 0.05 2.30 Q8 1 0.7628 0.3799 0.4653 11.00000 0.05 2.09 Q9 1 1.1130 0.4967 0.7844 11.00000 0.05 2.03 Q10 1 0.8102 0.1440 0.5411 11.00000 0.05 2.01 Q11 1 1.1616 0.4895 0.8546 11.00000 0.05 2.00 Q12 1 0.5018 0.4747 0.7418 11.00000 0.05 1.95 Q13 1 0.4315 0.6270 1.0189 11.00000 0.05 1.94 Q14 1 0.6447 0.4234 0.7609 11.00000 0.05 1.93 Q15 1 0.8966 0.2661 0.8391 11.00000 0.05 1.81 Q16 1 0.8034 0.3793 0.5190 11.00000 0.05 1.78 Q17 1 0.8236 0.1917 0.5284 11.00000 0.05 1.73 Q18 1 0.5906 0.3699 0.4990 11.00000 0.05 1.65 Q19 1 0.7505 0.5037 0.2365 11.00000 0.05 1.49 Q20 1 1.0255 0.3561 0.8436 11.00000 0.05 1.41 ; _shelx_res_checksum 90688 _shelx_hkl_file ; 2 0 0 52.3597 2.22173 5 -2 0 0 50.1403 2.40794 1 -3 0 0 1.15053 0.98534 2 -3 0 0 1.44798 1.16824 1 -3 0 0 1.27873 0.93638 7 3 0 0 1.53064 0.84159 5 -4 0 0 397.129 14.6479 7 4 0 0 380.159 14.3921 5 -4 0 0 400.895 14.7068 2 -5 0 0 77.3701 4.02655 2 -5 0 0 77.7442 3.73024 6 -5 0 0 78.2909 3.66765 5 -5 0 0 80.4124 4.03621 7 -6 0 0 1842.86 66.4336 6 -6 0 0 1857.69 66.8375 2 -6 0 0 1900.98 66.7951 7 6 0 0 1865.07 66.7272 1 -6 0 0 1880.82 66.3811 5 7 0 0 1038.33 39.0261 7 -7 0 0 1115.08 39.2832 2 -7 0 0 1086.26 38.7200 5 7 0 0 1054.23 39.0982 1 -7 0 0 1102.29 39.1930 7 -7 0 0 1064.03 38.7534 6 -8 0 0 28.4151 2.42270 5 8 0 0 30.3241 2.99672 1 -8 0 0 30.2539 2.54017 6 -8 0 0 34.7421 2.86607 7 -8 0 0 33.6588 2.90819 2 8 0 0 35.4715 3.01125 7 -9 0 0 151.849 7.35434 2 -9 0 0 155.292 6.86079 6 -9 0 0 148.202 6.75008 5 9 0 0 157.016 7.26278 7 -9 0 0 161.824 7.31891 7 9 0 0 151.364 7.23109 1 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0.97149 6 5 2 0 3.18517 0.98740 6 5 2 0 2.84872 1.45393 1 -5 2 0 1.43362 1.32575 7 -5 2 0 0.59185 1.28024 2 6 2 0 84.6975 4.00824 1 -6 2 0 76.8549 4.03948 2 -6 2 0 76.0821 3.86284 7 6 2 0 80.8155 3.63593 5 -6 -2 0 78.0621 3.48454 6 6 2 0 72.3307 3.47658 6 6 -2 0 75.6105 3.89192 7 6 -2 0 89.6003 4.06203 8 -7 2 0 2749.66 97.6083 2 -7 -2 0 2626.06 97.4196 7 7 -2 0 2792.86 97.4850 8 -7 2 0 2786.66 97.3946 7 7 2 0 2758.48 96.9841 6 7 2 0 2635.04 97.3558 1 7 2 0 2730.24 97.0611 5 -7 -2 0 2776.08 96.9099 6 7 -2 0 2824.99 97.3864 7 -8 2 0 4983.03 170.611 7 8 2 0 4900.20 170.170 5 8 2 0 4592.35 170.475 1 -8 -2 0 4644.05 170.555 7 -8 -2 0 4758.73 169.945 6 8 -2 0 4833.82 170.492 7 8 -2 0 5046.10 170.679 8 -8 2 0 4915.62 170.798 2 9 2 0 1228.60 44.1770 7 -9 -2 0 1122.10 44.1493 7 9 -2 0 1248.14 44.1677 7 -9 2 0 1235.48 44.2501 7 -9 2 0 1257.85 44.4571 2 -9 2 0 1206.45 43.7540 5 -9 -2 0 1162.33 43.4802 6 9 2 0 1157.87 44.0971 1 9 -2 0 1271.71 44.3458 8 9 2 0 1256.11 43.7852 5 10 2 0 58.3302 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18.9761 1.22709 3 -3 -3 0 17.1676 1.22697 6 -3 3 0 16.0210 1.20031 3 3 -3 0 16.9122 1.42230 8 3 3 0 18.5418 1.30036 1 -3 3 0 18.4618 1.52225 7 3 3 0 16.8024 1.17975 6 -3 3 0 19.8164 1.81669 10 4 3 0 2459.23 85.3815 6 -4 -3 0 2382.22 85.3912 6 4 3 0 2372.88 85.5268 1 -4 3 0 2419.30 85.7043 7 4 -3 0 2439.47 85.7113 8 4 -3 0 2402.89 85.4114 3 -4 3 0 2571.78 85.9982 10 -5 -3 0 1602.32 57.3163 6 5 3 0 1600.96 57.2961 6 -5 3 0 1734.01 58.1301 10 5 3 0 1666.10 57.5860 1 5 -3 0 1627.65 57.7139 8 -5 3 0 1559.03 57.6764 7 6 3 0 391.380 13.8835 1 6 -3 0 378.429 13.9445 8 -6 -3 0 368.778 13.8612 1 6 -3 0 364.259 13.8783 7 6 3 0 352.948 13.4110 6 -6 3 0 367.728 13.8880 7 -6 -3 0 355.354 13.4377 6 7 3 0 210.823 8.35535 1 7 -3 0 211.945 8.36501 7 -7 -3 0 193.325 8.33511 1 -7 -3 0 207.702 7.85809 6 7 -3 0 196.401 8.35068 8 7 3 0 199.513 7.84065 6 -7 3 0 190.999 8.26349 7 8 -3 0 7.06091 1.99747 7 8 -3 0 11.6789 1.97448 8 8 3 0 10.3309 1.55108 6 -8 3 0 12.1860 2.06014 2 -8 -3 0 9.74489 1.54803 6 8 3 0 12.0854 1.71493 5 -8 3 0 12.9754 2.07915 7 8 3 0 14.4186 2.30179 1 -8 -3 0 11.1309 2.12878 1 9 3 0 6.56919 1.86899 5 -9 3 0 5.78189 2.21650 2 9 -3 0 5.06407 2.00460 8 9 3 0 2.88859 1.56733 6 -9 3 0 5.44341 2.01066 7 9 3 0 1.91830 2.05486 1 -9 -3 0 4.01953 1.54356 6 -9 -3 0 2.25097 2.03003 1 9 3 0-0.76846 2.20204 7 9 -3 0 6.52607 2.22776 7 -10 3 0 445.258 17.4823 7 -10 3 0 448.116 17.8343 2 10 3 0 459.401 17.4697 7 10 3 0 452.315 17.0175 5 10 3 0 413.752 17.3408 1 10 -3 0 461.997 17.6493 8 -10 -3 0 444.883 16.7141 6 -10 -3 0 438.210 17.6833 1 10 -3 0 433.878 17.4230 7 -11 3 0 484.950 17.7740 5 11 3 0 414.448 17.9983 1 -11 3 0 447.660 18.4999 2 11 3 0 464.303 17.6689 5 11 -3 0 491.186 18.4136 8 11 3 0 443.708 18.0872 7 -11 -3 0 452.772 17.3322 6 -11 3 0 450.322 18.4632 10 -11 3 0 465.693 18.2445 7 11 -3 0 459.745 18.1040 7 -11 -3 0 461.258 18.3826 1 -12 -3 0 351.641 14.3358 1 -12 -3 0 325.609 13.1879 6 -12 3 0 353.446 14.4038 10 12 3 0 363.627 13.7586 5 12 -3 0 332.716 14.0525 7 -12 3 0 326.320 14.4557 2 12 -3 0 335.469 14.2528 8 -12 3 0 344.840 13.6301 5 -12 3 0 334.248 14.2069 7 12 3 0 313.040 13.9424 1 12 3 0 317.992 14.0494 7 13 3 0 5.77283 3.06459 1 13 -3 0 0.29406 2.93873 7 -13 3 0 1.45735 2.91034 2 -13 3 0 1.61068 2.83922 7 13 -3 0 1.34932 2.64747 8 13 3 0 2.74036 2.94847 7 -13 3 0 3.25916 2.14544 5 -13 3 0-0.92244 3.36591 10 -13 -3 0 3.77033 2.83762 1 -13 -3 0 1.49377 1.89760 6 13 3 0 1.44270 2.62641 5 14 -3 0 527.967 21.0839 1 14 3 0 517.403 21.1158 7 14 -3 0 477.057 21.0957 8 14 3 0 518.137 20.5842 5 -14 -3 0 508.494 20.0258 6 -14 3 0 582.966 21.4757 10 -14 3 0 538.926 21.2896 7 14 3 0 544.584 21.0344 1 -14 3 0 520.809 21.5301 2 14 -3 0 489.880 20.8943 7 -14 -3 0 568.764 21.3696 1 -15 3 0 313.951 13.5832 6 -15 -3 0 330.758 14.2077 1 -15 -3 0 314.354 13.0111 6 15 3 0 329.329 13.6139 5 15 3 0 323.833 14.1602 7 15 -3 0 307.430 14.3119 8 -15 3 0 320.265 14.5313 2 -15 3 0 311.578 14.1472 10 15 -3 0 326.956 14.0389 7 -15 3 0 308.139 14.0967 7 15 3 0 324.292 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0 915.641 32.2890 10 1 -4 0 914.152 32.5970 8 -1 -4 0 886.868 32.3002 10 -1 4 0 919.168 32.4927 10 -2 -4 0 5.22807 0.89401 1 2 4 0 4.50654 1.05210 6 2 -4 0 3.30450 1.07016 9 2 4 0 3.73187 1.09785 4 -2 4 0 5.83350 1.34134 10 -2 -4 0 3.91147 0.78411 10 2 -4 0 4.26201 1.07842 8 -3 4 0 58.7224 3.07577 7 -3 4 0 60.1942 2.71096 3 3 4 0 60.3637 2.78295 6 -3 -4 0 63.6514 3.01393 9 -3 -4 0 60.7171 2.72442 1 -3 -4 0 60.2748 2.79651 6 -3 4 0 63.8397 3.23321 10 3 4 0 60.1585 2.75143 1 3 4 0 57.8995 2.97469 4 3 -4 0 58.5272 3.03063 8 4 -4 0 1350.51 47.4290 3 -4 4 0 1307.80 47.7750 7 -4 -4 0 1329.38 47.4418 6 4 4 0 1303.42 47.4891 1 -4 -4 0 1331.34 47.5142 1 4 -4 0 1389.94 47.8067 8 4 4 0 1320.12 47.4120 6 -4 4 0 1419.55 48.0358 10 5 4 0 11545.5 411.639 6 5 -4 0 11639.5 411.689 3 5 -4 0 11684.1 412.074 7 -5 -4 0 11570.1 411.672 6 5 4 0 11602.0 411.818 1 -5 4 0 11636.5 412.072 7 -5 4 0 12666.5 412.433 10 5 -4 0 12146.7 412.123 8 -5 -4 0 11757.2 411.867 1 -6 -4 0 4217.62 146.578 1 6 4 0 4072.69 146.213 6 6 -4 0 4292.59 146.783 8 -6 4 0 4060.00 146.684 7 6 -4 0 4222.58 146.327 3 -6 4 0 4103.57 147.065 10 6 4 0 4256.24 146.540 1 6 -4 0 4145.75 146.716 7 -6 -4 0 4089.53 146.260 6 7 -4 0 94.6323 4.60320 8 7 -4 0 85.3010 4.52567 7 -7 4 0 84.2700 5.03856 10 -7 4 0 86.7547 4.49324 7 7 4 0 91.7741 3.98728 6 7 4 0 90.6413 4.45665 1 -7 -4 0 99.7159 4.55429 1 -7 -4 0 93.4980 4.06851 6 -8 4 0 14.7055 2.04341 7 8 4 0 20.1809 2.35349 1 -8 -4 0 19.9524 1.76386 6 -8 -4 0 15.6636 2.26265 1 8 -4 0 22.0139 2.27073 8 8 -4 0 19.9383 2.41236 7 8 4 0 17.9230 1.69003 6 9 4 0 801.289 30.2589 5 -9 4 0 818.594 30.6804 7 -9 -4 0 801.127 30.0316 6 9 -4 0 852.837 30.8576 8 9 4 0 846.988 30.0717 6 -9 -4 0 817.765 30.7782 1 9 -4 0 850.254 30.7207 7 9 4 0 879.571 30.7165 1 10 4 0 437.596 17.5229 7 10 4 0 448.039 16.9285 6 -10 4 0 439.449 17.5703 7 10 -4 0 469.636 17.8137 8 10 4 0 451.269 17.1676 5 10 -4 0 480.191 17.6927 7 10 4 0 449.219 17.5395 1 -10 -4 0 429.121 17.7130 1 -10 -4 0 451.743 16.8872 6 -11 4 0 583.092 22.5519 7 11 -4 0 597.308 22.5583 7 -11 -4 0 564.097 22.7068 1 11 4 0 580.154 22.4748 1 11 -4 0 615.592 22.7907 8 11 4 0 595.973 22.5225 7 -11 -4 0 578.533 21.6914 6 11 4 0 597.218 22.0309 5 11 4 0 563.107 21.7941 6 -12 -4 0 340.123 13.5608 6 -12 4 0 345.768 14.9090 10 12 4 0 369.868 14.0555 5 12 4 0 321.799 14.2805 1 12 4 0 353.852 14.4975 7 -12 4 0 320.446 14.3908 7 12 -4 0 373.510 14.7529 8 -12 -4 0 364.964 14.8364 1 12 -4 0 351.650 14.4626 7 -13 -4 0 0.70464 1.98833 6 -13 4 0 2.93563 3.45409 10 13 -4 0 5.22743 2.75489 8 13 -4 0 7.17051 2.95400 7 13 4 0 0.58171 2.90001 7 13 4 0 8.50316 3.07529 1 -13 -4 0 2.57520 2.80801 1 13 4 0 1.13926 2.50200 5 -13 4 0 3.98171 2.78639 7 -14 4 0 10.8227 4.00468 10 14 4 0 9.75679 3.38296 1 -14 4 0 3.39855 3.31743 7 14 4 0 5.16197 3.30213 7 -14 -4 0 4.70470 3.29950 1 -14 -4 0 6.37508 2.30420 6 14 -4 0 3.60043 2.99442 8 14 4 0 8.60851 2.83748 5 14 -4 0 8.11981 3.27224 7 15 -4 0 336.549 14.9286 8 -15 -4 0 347.011 14.7146 1 -15 4 0 329.758 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4 0 142.706 8.66882 9 -21 -4 0 141.104 7.39730 6 -21 4 0 125.468 8.76982 7 21 -4 0 137.546 9.31070 8 22 4 0 37.6925 5.42001 9 22 -4 0 38.2601 5.95482 8 -22 4 0 43.8229 5.80377 7 23 -4 0 1.08535 5.16117 8 23 4 0 2.15005 4.41595 9 -23 4 0 3.15612 4.90203 7 23 4 0 10.1199 5.42558 8 24 4 0-0.44087 4.67825 9 -24 4 0 0.46252 5.32522 7 24 -4 0 2.79673 5.41544 8 24 4 0 7.68541 6.05010 8 25 -4 0 29.9783 7.11656 8 25 4 0 37.8685 6.82601 8 -25 4 0 32.7188 6.42005 7 25 4 0 21.1692 5.59723 9 -26 4 0 75.6450 7.89543 7 26 4 0 76.0583 7.43883 9 26 4 0 76.7564 8.51548 8 26 -4 0 79.6895 8.35609 8 27 4 0 20.3081 6.64075 8 -27 4 0 17.0069 6.46854 7 27 -4 0 36.1006 7.22921 8 27 4 0 28.2941 5.93111 9 28 -4 0-3.77041 6.20909 8 -28 4 0 6.66005 5.96031 7 28 4 0 8.58165 6.34238 8 28 -4 0-4.89380 4.59920 9 28 4 0 13.9459 5.47908 9 29 4 0 6.29472 6.93702 8 29 -4 0 1.93749 7.14973 8 29 4 0-7.33243 5.89228 9 30 4 0 11.4786 6.07472 9 31 4 0 36.3196 7.08237 9 0 5 0 0.48434 1.04037 9 0 -5 0 1.23034 1.00661 10 0 5 0-0.43266 1.08600 10 0 -5 0-0.77159 1.12848 8 -1 5 0 269.712 10.2536 9 1 -5 0 260.995 10.3400 8 1 5 0 266.597 10.3223 9 1 5 0 265.575 10.2387 4 -1 -5 0 270.656 10.0128 10 -1 5 0 271.989 10.1996 10 1 5 0 278.437 9.99940 10 2 -5 0 16.2717 1.61096 8 -2 5 0 13.2532 1.70373 10 2 5 0 15.4056 1.61136 4 2 5 0 13.6531 1.65277 9 2 5 0 15.7578 1.52571 6 -2 -5 0 13.0454 1.19113 1 2 -5 0 15.0979 1.44554 9 -2 -5 0 12.9852 1.12158 10 3 5 0 1053.14 38.9191 4 -3 -5 0 1095.83 38.6410 1 3 5 0 1083.36 38.7493 6 -3 -5 0 1083.43 38.5039 10 -3 5 0 1093.07 38.6585 3 3 -5 0 1092.19 39.0212 8 -3 5 0 1098.69 39.0530 10 -4 -5 0 5593.41 198.567 1 -4 -5 0 5609.68 198.860 9 4 -5 0 5644.43 198.940 8 -4 5 0 5704.68 198.520 3 -4 -5 0 5614.60 198.611 6 -4 5 0 5701.21 198.978 7 4 5 0 5638.86 198.861 4 -4 5 0 5680.05 199.059 10 4 5 0 5683.01 198.572 6 4 5 0 5636.78 198.554 1 -5 -5 0 514.416 18.7966 1 5 5 0 503.791 18.6445 6 -5 5 0 512.195 19.1129 7 -5 -5 0 497.604 18.6840 6 5 5 0 499.694 18.7497 1 -5 5 0 543.641 19.4309 10 5 -5 0 520.268 18.6860 3 5 -5 0 531.816 19.1540 8 6 5 0 1904.21 66.9629 6 6 -5 0 1867.65 67.0365 3 6 -5 0 1851.27 67.4654 7 -6 5 0 1945.59 67.5234 7 -6 5 0 1929.15 67.8513 10 6 -5 0 1906.06 67.5355 8 6 5 0 1874.22 67.1647 1 -6 -5 0 1893.56 67.2468 1 -6 -5 0 1881.44 67.0246 6 -7 5 0 146.856 6.62080 7 7 -5 0 151.738 6.17801 3 7 5 0 153.888 6.45319 1 7 -5 0 152.207 6.72288 7 7 5 0 150.876 6.07406 6 -7 -5 0 146.284 6.46192 1 7 -5 0 154.371 6.74772 8 7 -5 0 140.743 6.62861 1 -7 5 0 158.347 7.30111 10 -7 -5 0 150.539 6.16451 6 -8 5 0 275.413 12.0925 10 8 -5 0 307.676 11.6631 8 8 5 0 282.336 10.8389 6 -8 5 0 290.887 11.5300 7 8 -5 0 293.737 11.5573 7 -8 -5 0 281.901 10.9411 6 8 -5 0 263.022 11.5054 1 8 -5 0 281.580 10.9859 3 8 5 0 288.775 11.3326 1 -8 -5 0 292.584 11.4312 1 9 -5 0 204.560 8.89326 8 9 5 0 215.296 8.71917 1 -9 5 0 189.078 8.71258 7 9 -5 0 216.540 8.92470 7 -9 -5 0 201.538 8.17436 6 9 5 0 197.458 8.07137 6 -9 -5 0 205.607 8.77197 1 10 5 0 218.977 9.31913 6 -10 -5 0 223.221 9.38752 6 -10 -5 0 250.799 10.2895 1 10 5 0 245.639 10.1671 7 10 -5 0 239.826 10.1675 7 10 -5 0 248.490 10.3086 8 10 5 0 252.466 10.1178 1 -10 5 0 231.957 10.0651 7 10 5 0 243.598 10.4553 9 11 5 0 22.2493 2.99464 7 11 -5 0 24.7799 3.15446 8 -11 -5 0 26.4681 3.26295 1 11 5 0 22.6436 2.36735 6 -11 -5 0 28.7796 2.47911 6 11 5 0 25.9842 2.70755 5 -11 5 0 21.1363 2.95224 7 11 -5 0 24.6791 3.10984 7 11 5 0 23.5582 3.02558 1 12 -5 0 594.810 23.1160 7 12 5 0 610.817 22.5842 5 12 5 0 567.902 22.2445 6 -12 5 0 614.800 23.1438 7 12 5 0 587.516 22.9368 1 12 5 0 606.306 23.0686 7 12 -5 0 654.717 23.4943 8 -12 -5 0 564.662 23.2401 1 -12 -5 0 581.403 22.1320 6 13 5 0 197.873 9.45936 7 13 5 0 183.399 9.55797 9 13 -5 0 206.688 9.51118 7 13 -5 0 205.837 9.63301 8 -13 5 0 190.793 9.36389 7 -13 -5 0 192.585 8.42553 6 13 5 0 197.997 8.88329 5 -13 -5 0 194.550 9.69173 1 13 5 0 199.794 9.37866 1 14 -5 0 283.317 12.4356 7 14 5 0 295.461 11.8767 5 -14 -5 0 281.748 11.3067 6 14 5 0 260.252 12.1610 1 -14 5 0 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13.7173 6.75136 8 28 -5 0 10.0762 4.68231 9 -29 -5 0 3.28046 6.77005 2 29 5 0-6.37541 6.57864 8 29 -5 0 3.95476 6.85429 8 -29 5 0 1.57188 6.25522 7 29 5 0 3.07220 5.71965 9 30 5 0-0.51876 5.94714 9 31 5 0-0.52391 6.16877 9 32 5 0 4.77137 6.34353 9 0 6 0 9.26544 1.50976 9 0 -6 0 7.09646 1.43131 8 0 -6 0 9.53728 1.37034 10 0 6 0 8.35538 1.44561 10 1 6 0 155.095 6.31556 9 1 -6 0 145.693 6.12720 10 1 -6 0 151.778 6.14933 9 1 6 0 149.839 5.90109 10 -1 6 0 149.697 6.13210 10 -1 -6 0 146.387 5.91447 10 -1 6 0 150.862 6.22010 9 1 6 0 146.426 6.17908 4 1 -6 0 147.113 6.30947 8 2 -6 0 2722.39 98.8773 10 2 6 0 2779.43 98.8429 4 -2 -6 0 2769.09 98.4819 1 2 -6 0 2907.98 99.0174 8 -2 6 0 2825.38 98.8370 10 2 -6 0 2841.77 98.7358 9 2 6 0 2775.19 98.9607 9 -2 -6 0 2770.45 98.4712 10 -3 -6 0 7390.35 261.064 10 3 6 0 7399.76 261.380 6 -3 6 0 7555.92 261.605 10 -3 6 0 7349.53 261.237 3 3 -6 0 7635.00 261.679 8 3 -6 0 7557.20 261.361 9 3 6 0 7199.55 261.703 9 3 6 0 7532.14 261.554 4 -3 -6 0 7398.10 261.178 1 -4 6 0 2062.35 72.1908 10 -4 6 0 1998.10 71.6287 3 -4 -6 0 2021.38 71.6596 1 4 6 0 2053.72 72.0205 4 4 6 0 2045.42 71.6423 1 4 -6 0 2034.69 72.1457 8 -4 -6 0 1953.96 71.9981 9 4 6 0 2034.33 71.7514 6 -5 6 0 5.02398 2.10761 10 5 6 0 4.23107 1.38618 1 -5 -6 0 6.15985 1.43463 6 5 6 0 3.44249 1.16935 6 -5 6 0 3.01665 1.54275 7 -5 -6 0 6.83496 1.38666 1 -5 6 0 5.77508 1.22930 3 5 6 0 5.65336 1.79185 4 5 -6 0 6.12085 1.56502 8 6 6 0 61.6530 3.22319 1 -6 -6 0 57.9726 3.11105 6 -6 6 0 58.6842 4.07309 10 6 -6 0 56.2296 3.00165 3 6 -6 0 62.9618 3.58571 8 -6 -6 0 58.5551 3.21262 1 6 6 0 57.4586 3.01292 6 -6 6 0 59.7621 3.62590 7 7 -6 0 211.766 8.10903 3 -7 -6 0 201.248 8.09178 6 7 6 0 203.988 7.98134 6 7 6 0 203.089 8.24561 1 7 -6 0 192.537 8.41361 1 -7 6 0 195.163 8.56743 7 -7 -6 0 199.099 8.28476 1 7 -6 0 209.152 8.66052 8 -7 6 0 204.595 9.15457 10 8 -6 0 213.536 8.09328 3 8 -6 0 187.966 8.52165 1 -8 -6 0 207.932 8.06972 6 -8 6 0 195.634 8.57737 7 8 6 0 196.242 7.90977 6 -8 6 0 206.573 9.28668 10 8 -6 0 191.063 8.56153 7 8 6 0 194.170 8.27882 1 8 -6 0 205.729 8.67666 8 -8 -6 0 191.629 8.33022 1 9 6 0 37.4792 2.53405 6 -9 -6 0 36.7448 2.98620 1 9 -6 0 42.6050 3.28580 8 9 -6 0 38.6765 3.32331 7 -9 6 0 42.5802 4.05416 10 9 -6 0 44.2852 3.40176 1 -9 -6 0 33.7260 2.59071 6 9 6 0 40.4835 3.14955 1 9 -6 0 43.6324 2.67529 3 -9 6 0 38.5462 3.17082 7 -10 -6 0 5.35482 1.78247 6 -10 6 0 7.98533 2.39982 7 10 -6 0 10.7152 2.41081 8 10 -6 0 8.69026 2.48380 7 10 6 0 4.37720 1.64115 6 10 6 0 8.25353 2.30336 1 -10 -6 0 3.66459 2.27697 1 -10 6 0 4.85294 3.08134 10 10 -6 0 9.19430 1.85000 3 -11 -6 0 2.02401 1.82052 6 11 6 0 2.78304 1.78587 6 11 -6 0 4.65626 2.80675 1 -11 6 0 1.92702 2.46171 7 -11 -6 0 4.25218 2.48031 1 11 -6 0 2.66037 2.50425 7 11 -6 0 1.49101 1.78660 3 11 -6 0 3.22083 2.36725 8 11 6 0 2.53770 2.53658 1 11 6 0 7.64732 2.62492 7 12 -6 0 662.714 26.7555 1 12 6 0 713.675 26.5970 7 12 -6 0 731.523 26.7469 7 12 6 0 697.875 26.4718 1 12 6 0 664.537 26.0502 5 12 6 0 648.932 26.9554 9 -12 -6 0 700.906 25.7386 6 12 6 0 681.437 25.7252 6 -12 -6 0 677.116 26.7876 1 -12 6 0 724.036 26.6851 7 12 -6 0 785.488 27.1913 8 13 -6 0 1426.15 57.4198 1 -13 6 0 1653.36 57.5016 7 13 6 0 1492.48 56.3711 6 -13 -6 0 1660.64 56.4490 6 13 6 0 1466.98 57.7774 9 13 -6 0 1622.04 57.4388 7 13 -6 0 1685.73 57.8669 8 13 6 0 1605.96 57.3404 7 -13 -6 0 1457.46 57.5092 1 13 6 0 1566.08 56.7795 5 13 6 0 1609.19 57.2161 1 14 6 0 355.126 14.2844 5 -14 -6 0 331.958 15.0969 1 14 -6 0 363.827 14.9468 7 14 6 0 341.028 14.6725 1 14 6 0 341.897 14.8016 7 -14 -6 0 341.302 13.7377 6 14 6 0 317.579 15.1181 9 14 6 0 336.063 13.8782 6 -14 6 0 372.931 15.0686 7 14 -6 0 364.940 15.2750 8 15 6 0 33.8441 3.94968 5 15 6 0 39.8363 4.43912 1 15 -6 0 45.6857 4.71683 7 -15 6 0 39.2560 4.67442 7 -15 -6 0 41.9195 4.77687 1 15 -6 0 38.8571 4.59862 8 -15 -6 0 43.4676 3.51846 6 15 6 0 38.2594 4.42193 9 -16 -6 0 11.5775 2.63379 6 16 -6 0 9.74479 4.00411 8 -16 6 0 9.87113 3.47262 5 -16 6 0 11.9010 3.95399 7 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51.3468 7.25369 8 -23 -6 0 35.3897 6.73301 2 23 6 0 63.9642 6.69714 9 -23 6 0 40.2306 6.52115 7 24 -6 0 18.5704 6.29036 8 -24 6 0 18.2492 5.78219 7 -24 -6 0 19.9393 6.17899 2 24 6 0 28.6155 5.88311 9 25 6 0 2.47403 5.18568 9 25 -6 0-4.30527 5.68445 8 -25 -6 0 14.1291 6.24696 2 -25 6 0 0.48841 5.29652 7 -26 6 0 6.97675 5.67815 7 26 6 0-2.53123 5.82947 9 26 6 0-0.60963 6.50115 8 -26 -6 0 13.3479 6.34272 2 26 -6 0 2.52419 6.14636 8 27 -6 0 16.0786 5.37143 3 27 -6 0 23.8798 7.18604 8 27 6 0 14.9548 5.99162 9 -27 -6 0 10.6365 6.50055 2 -27 6 0 21.7882 6.49756 7 27 6 0 17.4494 7.03299 8 28 6 0 53.4493 8.52759 8 28 -6 0 46.8777 8.15298 8 -28 6 0 45.3867 7.27321 7 -28 -6 0 52.7149 8.11894 2 28 6 0 41.9915 7.29102 9 28 -6 0 51.8225 6.45098 3 29 6 0 27.1580 7.07037 9 -29 -6 0 31.7555 7.53340 2 29 6 0 22.0545 7.42030 8 -29 6 0 21.5898 6.83746 7 29 -6 0 37.8821 8.10172 8 30 6 0 11.3256 6.23761 9 -30 6 0-1.06776 6.70261 7 31 6 0-1.63175 6.50621 9 0 7 0-0.55204 1.38649 9 0 -7 0-0.73799 1.43369 9 0 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1.60285 1 5 7 0 13.9456 1.76814 6 5 7 0 13.7620 1.69080 1 5 -7 0 9.73792 1.89325 8 5 7 0 13.9589 2.11267 4 -5 7 0 15.2441 2.17370 7 -5 7 0 10.2822 2.40510 10 -5 7 0 11.0138 1.58616 3 -6 -7 0 533.409 20.2771 6 6 -7 0 561.861 20.8471 8 6 7 0 543.056 20.6390 4 6 7 0 526.758 20.1937 6 -6 -7 0 542.812 20.2713 1 -6 7 0 573.510 20.8733 7 -6 7 0 565.949 20.1325 3 6 7 0 547.714 20.2462 1 -6 7 0 564.776 21.0602 10 7 7 0 509.999 19.5755 1 7 -7 0 527.447 20.1401 8 7 7 0 525.923 19.4191 6 -7 -7 0 504.452 19.5157 6 -7 7 0 552.111 20.5569 10 7 -7 0 551.666 19.5224 3 -7 7 0 530.848 20.1111 7 -7 -7 0 527.575 19.6525 1 -8 7 0 28.5316 3.38695 10 8 -7 0 23.4176 2.16702 3 -8 7 0 26.3014 2.77787 7 -8 -7 0 23.0699 2.25913 6 8 -7 0 28.1286 2.64225 2 8 7 0 26.4769 2.15887 6 8 7 0 21.5497 2.38754 1 8 -7 0 28.4774 2.73291 1 8 -7 0 29.7387 2.90383 8 -8 -7 0 26.3506 2.43023 1 -9 -7 0 131.114 5.98643 6 9 -7 0 146.446 6.82392 8 9 -7 0 131.330 5.96695 3 9 7 0 133.485 6.32571 1 -9 7 0 147.337 6.74669 7 -9 -7 0 127.574 6.33552 1 9 7 0 136.972 5.90668 6 -9 7 0 153.950 7.52371 10 -10 -7 0 170.789 7.63443 1 10 7 0 167.319 7.47988 1 -10 -7 0 162.339 7.02679 6 10 -7 0 164.657 7.83081 7 -10 7 0 163.744 8.48049 10 -10 7 0 167.706 7.79123 7 10 7 0 154.738 6.85511 6 10 -7 0 162.287 7.88411 8 10 -7 0 165.136 7.09490 3 -11 -7 0 118.336 5.69626 6 11 7 0 122.393 5.64959 6 -11 7 0 138.130 6.67761 7 11 -7 0 119.585 5.83799 3 11 -7 0 114.923 6.56466 1 11 -7 0 134.259 6.80046 8 11 -7 0 121.837 6.42041 2 11 7 0 130.487 7.01874 9 11 7 0 123.871 6.35181 1 11 7 0 129.372 6.61724 7 -11 7 0 113.231 7.33369 10 11 -7 0 116.069 6.54951 7 -11 -7 0 122.435 6.49223 1 12 7 0 734.182 27.1865 6 12 -7 0 734.680 28.0699 2 -12 -7 0 740.280 27.2921 6 12 -7 0 773.668 27.5017 3 12 7 0 753.523 27.9126 1 12 -7 0 728.665 28.1835 7 12 7 0 701.349 28.6632 9 -12 7 0 737.597 28.1868 7 -12 -7 0 713.922 28.1731 1 12 -7 0 731.252 28.2723 1 12 7 0 732.497 28.0901 7 12 -7 0 771.895 28.5344 8 13 7 0 52.1445 4.00397 5 13 7 0 44.9072 4.34347 7 13 -7 0 50.2098 4.55794 8 -13 7 0 59.4163 4.58500 7 13 -7 0 49.1824 4.48193 7 13 -7 0 54.7370 3.77279 3 13 7 0 49.8094 4.83440 9 13 7 0 47.5996 3.44950 6 -13 -7 0 53.3825 3.63620 6 13 7 0 57.1793 4.45020 1 13 -7 0 49.2158 4.33761 2 -13 -7 0 49.7260 4.62687 1 13 -7 0 49.6366 4.62447 1 14 -7 0 25.1083 3.90092 7 14 -7 0 36.4312 4.38163 8 14 7 0 27.8239 3.45733 5 -14 -7 0 31.8311 3.06274 6 14 7 0 37.6050 4.45201 9 14 7 0 31.9365 3.97167 1 14 7 0 31.0670 3.17937 6 -14 7 0 27.7251 3.89352 7 14 -7 0 35.8448 3.36939 3 -14 -7 0 34.5992 4.27050 1 -15 -7 0 124.465 6.29467 6 15 7 0 119.057 6.90176 5 -15 -7 0 127.215 7.85188 1 15 -7 0 133.008 7.84050 8 15 -7 0 134.316 6.66235 3 15 7 0 109.400 7.60271 9 -15 7 0 123.586 7.56120 7 15 7 0 134.543 7.29949 1 15 7 0 117.172 6.34295 6 15 -7 0 132.886 7.58333 7 16 -7 0 223.847 10.0441 3 16 7 0 224.357 10.3312 5 16 7 0 197.165 11.0735 9 16 -7 0 235.849 11.5563 8 -16 -7 0 225.464 9.61793 6 -16 7 0 225.195 11.1236 7 -16 -7 0 198.708 10.9594 1 -17 7 0 41.6853 5.41598 7 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97.1203 8.33540 7 22 -7 0 110.525 7.15309 3 23 -7 0 25.9447 4.76482 3 -23 -7 0 26.1453 6.08504 2 -23 7 0 28.9799 5.97991 7 23 -7 0 24.2506 6.43442 8 23 7 0 26.9925 5.58431 9 -23 -7 0 24.5741 5.69071 1 24 7 0 9.15697 5.41492 9 24 -7 0 4.36878 5.77140 8 -24 -7 0 1.75271 5.92133 2 24 -7 0 1.13269 4.25068 3 -24 7 0 18.3188 5.76300 7 -25 -7 0 15.6033 6.12629 2 -25 7 0 17.0040 5.71312 7 25 7 0 11.9271 5.69162 9 25 -7 0 13.0265 4.75926 3 25 -7 0 1.91810 6.25898 8 -26 -7 0-0.61912 6.04672 2 26 -7 0 1.95935 6.41569 8 26 7 0-1.58708 5.57150 9 26 -7 0 0.77569 4.43709 3 -26 7 0 5.57017 5.87838 7 27 -7 0 4.31584 4.60277 3 -27 7 0 7.20532 6.15729 7 27 7 0-7.67521 7.06569 8 27 7 0 5.91817 5.86226 9 -27 -7 0 6.34954 6.65453 2 27 -7 0 5.34790 6.54879 8 -28 7 0 7.29455 6.51711 7 -28 -7 0 1.95797 6.44917 2 28 -7 0 2.72820 7.14815 8 28 7 0 3.90525 6.54023 8 28 7 0 3.27813 5.79838 9 29 7 0 2.21560 5.83637 9 -29 7 0 8.97442 6.20623 7 30 7 0-1.67928 6.40371 9 -30 7 0 3.21788 6.46462 7 31 7 0-3.40773 6.79370 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1496.64 52.5356 10 4 -8 0 1451.54 52.1745 9 4 8 0 1436.15 52.3894 4 -4 8 0 1447.05 51.9987 3 4 -8 0 1407.70 52.5738 10 4 8 0 1462.20 52.2021 6 4 8 0 1455.85 52.6667 9 -5 -8 0 588.850 21.5870 10 5 8 0 596.219 22.2949 4 -5 -8 0 601.253 21.8447 1 5 -8 0 618.373 22.5408 8 5 8 0 603.313 21.9666 6 -5 8 0 572.834 21.7771 3 -5 8 0 605.988 22.5323 10 5 -8 0 590.478 22.0042 9 -6 -8 0 102.739 4.75084 1 6 8 0 98.2617 4.70492 1 6 8 0 114.426 5.35037 4 -6 8 0 98.7641 4.61350 3 -6 8 0 99.1568 5.36327 7 6 -8 0 96.3697 5.25200 8 -6 8 0 106.241 5.61886 10 6 8 0 105.611 4.80560 6 7 8 0 9.91471 2.31800 4 -7 -8 0 7.10946 1.82749 1 -7 8 0 7.50606 2.12941 7 -7 8 0 8.87289 2.73307 10 7 -8 0 7.64838 2.17526 8 7 8 0 7.52469 1.87758 1 7 8 0 7.79993 1.73456 6 -7 -8 0 6.15168 1.75785 6 8 -8 0 129.047 5.97413 1 -8 -8 0 118.561 5.71571 1 8 8 0 120.804 5.65618 1 -8 8 0 122.637 6.15340 7 8 -8 0 125.634 6.24971 8 8 8 0 124.921 5.45392 6 -8 -8 0 110.680 5.52985 6 -8 8 0 125.549 6.78296 10 9 8 0 6.56740 1.86098 6 -9 8 0 4.68386 3.45650 10 9 -8 0 3.96563 2.38916 8 -9 8 0 2.57859 2.33961 7 -9 -8 0 1.83579 2.02779 1 9 8 0 2.95336 2.08529 1 9 -8 0 3.05739 1.64289 3 -9 -8 0 5.96262 1.98433 6 10 8 0 1875.23 66.9114 6 -10 -8 0 1839.19 67.0526 6 10 -8 0 1957.88 68.0837 8 -10 8 0 1819.44 68.3808 10 10 -8 0 1913.23 67.0852 3 -10 8 0 1860.74 67.8449 7 10 8 0 1872.07 67.3319 1 -10 -8 0 1922.73 67.5554 1 10 -8 0 1839.68 67.6308 2 11 8 0 1922.43 68.6759 1 -11 -8 0 1942.11 68.9646 1 -11 -8 0 1942.53 68.3206 6 -11 8 0 1945.11 69.1877 7 -11 8 0 1860.23 69.8102 10 11 8 0 1854.80 68.1104 6 11 -8 0 1929.87 68.3893 3 11 -8 0 1895.32 69.0805 1 11 -8 0 1953.45 69.4222 8 11 -8 0 1878.91 68.9157 2 12 8 0 118.385 7.09926 9 -12 -8 0 115.658 5.70158 6 12 8 0 114.533 6.48814 7 12 8 0 111.252 5.55423 6 12 -8 0 116.313 6.32709 2 -12 8 0 98.7031 7.15676 10 12 -8 0 124.743 5.79830 3 12 -8 0 118.499 6.81325 8 -12 8 0 115.205 6.53161 7 12 8 0 122.387 6.33179 1 -12 -8 0 109.356 6.34089 1 12 -8 0 117.165 6.65710 1 13 8 0 2.73602 3.05374 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355.204 14.6629 1 13 9 0 331.719 13.4253 6 13 9 0 337.799 14.1596 1 13 9 0 313.802 15.2108 9 -14 -9 0 424.571 18.1515 1 14 -9 0 438.296 18.4208 8 14 9 0 433.494 16.8801 6 14 -9 0 445.509 17.1821 3 -14 -9 0 443.209 17.0813 6 14 9 0 456.530 17.7769 1 -14 9 0 422.135 18.1104 7 14 9 0 407.077 18.8464 9 15 9 0 102.057 5.52118 6 -15 -9 0 99.3989 6.87720 1 15 -9 0 100.102 5.66796 3 -15 -9 0 99.1855 5.51556 6 15 9 0 93.9217 6.09129 5 15 -9 0 124.402 7.41949 8 -15 9 0 96.5407 6.63338 7 15 9 0 92.8444 7.23699 9 16 9 0 8.64071 2.89892 6 16 9 0 4.46851 4.32988 9 -16 9 0-0.37364 3.92754 7 16 -9 0 2.62597 3.96742 8 16 -9 0 5.43286 2.91682 3 16 9 0 1.71577 3.36993 5 -16 -9 0 1.61873 4.19976 1 -17 9 0 53.7237 5.85917 7 17 9 0 58.5747 6.45942 9 17 -9 0 58.8233 4.84571 3 -17 -9 0 49.0679 5.84171 1 17 9 0 64.2134 5.31037 5 17 -9 0 61.7929 6.45153 8 18 -9 0 60.8520 4.96680 3 18 -9 0 52.8093 6.62620 8 18 9 0 51.5247 5.48612 5 -18 9 0 69.8547 6.64496 7 -18 -9 0 49.6905 5.93716 1 18 9 0 33.3750 5.89313 9 -19 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168.186 11.9694 9 -18 -14 0 108.503 8.07894 1 18 14 0 105.299 6.31785 6 -18 14 0 112.094 8.46720 7 18 14 0 106.035 9.53761 9 18 -14 0 115.614 9.14504 8 -19 -14 0 22.1441 5.43304 1 -19 14 0 6.75159 5.40255 7 19 14 0 12.6312 6.09617 9 19 -14 0 13.0369 6.12306 8 19 14 0 19.1561 4.93119 5 19 14 0 16.7316 3.82979 6 -20 14 0 7.08345 5.64197 7 20 14 0 12.1288 4.93636 5 -20 -14 0 8.74065 5.17832 1 20 14 0 15.5148 6.61438 9 20 -14 0 19.4890 6.48362 8 21 14 0 2.12703 6.06831 9 21 -14 0 7.28488 6.61865 8 -21 -14 0-0.46451 5.48268 1 21 14 0 6.93718 5.11470 5 -21 14 0 9.08216 5.98311 7 22 14 0 28.4760 8.23593 9 -22 -14 0 19.7673 5.74172 1 -22 14 0 23.1585 6.98459 7 22 -14 0 16.7953 7.21031 8 22 14 0 29.1774 6.28966 5 -23 -14 0 99.7581 8.75218 1 23 -14 0 109.127 10.5018 8 23 14 0 112.797 10.5373 9 23 14 0 97.3432 8.43425 5 -23 14 0 119.776 10.1493 7 24 -14 0 75.7992 9.60387 8 -24 -14 0 78.0284 7.90624 1 24 14 0 68.9607 9.81851 9 -24 14 0 65.3543 9.03680 7 24 14 0 62.3649 7.53197 5 25 14 0-3.59380 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88.9080 5.60368 10 3 15 0 94.7087 6.19444 9 -3 -15 0 98.5048 4.90185 1 -4 -15 0 129.263 7.27746 4 -4 15 0 133.619 7.11572 10 4 -15 0 124.610 7.72595 8 4 15 0 134.393 7.30209 6 4 15 0 130.682 7.65042 9 4 -15 0 136.842 6.93432 9 -4 -15 0 126.936 6.18671 1 -4 -15 0 134.267 6.41013 10 5 15 0 4.65087 3.01139 6 -5 -15 0 5.29001 2.27884 1 5 15 0 11.6973 3.68515 9 -5 15 0 2.97415 3.34194 10 -5 15 0 5.11100 2.76869 3 5 -15 0 1.91319 2.54759 9 5 -15 0-1.49297 3.46332 8 -5 -15 0 3.76738 2.25982 10 -6 15 0 14.6385 3.04228 3 -6 -15 0 14.6777 2.58135 10 6 15 0 16.1803 3.38083 6 6 -15 0 14.3265 3.84110 8 -6 15 0 12.0630 3.56919 10 -6 -15 0 14.1100 2.65625 1 6 -15 0 14.7844 3.05483 9 6 15 0 12.5257 3.87698 9 7 -15 0 10.7272 2.91103 9 7 15 0 13.8784 4.00600 9 -7 15 0 7.44697 3.63855 7 7 -15 0 9.20479 3.61411 8 -7 15 0 8.20454 2.69114 3 -7 -15 0 4.34879 2.36711 1 7 15 0 11.0130 3.18307 6 -7 -15 0 9.10879 2.43540 10 8 15 0 6.27805 3.03293 6 -8 15 0 0.38951 2.51518 3 -8 -15 0 3.59862 2.52098 1 -8 15 0 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231.968 10.0381 9 5 16 0 204.883 10.1779 6 5 -16 0 204.153 10.9540 8 -5 16 0 227.135 9.70738 3 5 16 0 198.846 10.7577 9 6 16 0 148.963 8.53829 9 -6 -16 0 136.624 6.56438 10 6 -16 0 125.478 7.13278 9 -6 16 0 139.422 6.91056 3 6 -16 0 125.248 8.04655 8 -6 -16 0 139.545 6.63862 1 6 16 0 136.356 7.34827 6 -7 -16 0 26.0519 2.98064 10 7 16 0 25.5688 4.64274 9 -7 -16 0 25.4612 3.07075 1 7 16 0 22.3501 3.65578 6 7 -16 0 33.2918 4.62766 8 -7 16 0 29.2097 3.40781 3 -7 16 0 30.5973 4.69065 7 7 -16 0 28.3270 3.66354 9 8 16 0 39.4496 5.25363 9 -8 16 0 38.3517 5.21875 7 8 -16 0 39.1031 5.09057 8 -8 -16 0 45.6981 3.80406 1 8 16 0 42.4116 4.19651 6 8 -16 0 37.6658 4.10822 9 -8 -16 0 35.0018 3.28693 10 -8 16 0 40.2658 3.79885 3 -9 -16 0 88.1277 5.05267 10 9 -16 0 100.513 7.26279 8 -9 16 0 92.5750 7.04489 7 -9 -16 0 101.925 5.66772 1 9 -16 0 101.164 6.06990 9 9 16 0 86.1002 5.84445 6 9 16 0 101.513 7.65886 9 -9 16 0 98.7588 5.45544 3 -10 16 0 303.067 13.9700 7 10 -16 0 286.712 12.6141 9 -10 -16 0 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20.7251 3.74443 1 1 -22 0 88.2369 7.30616 4 -1 22 0 80.0480 7.56207 6 -1 -22 0 84.3128 5.45894 1 -1 -22 0 78.5717 7.09362 4 1 22 0 73.6208 7.47151 6 -2 -22 0 191.087 9.08984 1 -2 -22 0 200.175 11.0982 4 2 22 0 189.300 11.2388 6 2 -22 0 207.858 11.3736 4 3 22 0 54.2888 6.51332 6 3 -22 0 44.4618 6.05178 4 -3 -22 0 51.2934 4.38113 1 3 22 0 46.1448 6.42760 9 4 22 0 9.54509 5.60050 9 4 22 0 3.42520 4.84812 6 -4 -22 0 5.54223 3.19179 1 4 -22 0 1.18422 5.59674 8 4 -22 0 0.47836 4.70126 4 5 22 0-0.54104 5.39302 9 5 -22 0 7.75050 5.19261 4 5 -22 0-1.18613 5.33896 8 -5 -22 0 6.16064 3.40163 1 5 22 0 8.62738 4.91684 6 6 22 0 7.21933 5.69332 9 6 -22 0 10.6993 5.99556 8 6 -22 0 8.84041 5.14224 4 6 22 0 7.49392 4.80882 6 -6 -22 0 8.88137 3.24569 1 7 -22 0 26.7815 5.49700 4 7 -22 0 19.0985 6.11218 8 7 22 0 17.0494 5.10012 6 -7 22 0 34.5707 6.52030 7 -7 -22 0 24.6323 3.72064 1 7 22 0 11.9709 5.96461 9 8 22 0 95.2414 8.72621 9 -8 -22 0 81.2243 5.32042 10 8 -22 0 81.5792 8.25467 8 8 22 0 85.0628 6.82148 6 8 -22 0 85.4952 7.59129 4 -8 22 0 90.1647 8.25026 7 -8 -22 0 81.2112 5.54181 1 9 22 0 41.3254 7.41598 9 -9 -22 0 58.9619 4.85659 1 9 -22 0 58.1586 6.68301 4 -9 22 0 61.5781 7.67269 7 9 22 0 52.7979 5.90181 6 -9 -22 0 44.0418 4.35848 10 9 -22 0 60.2859 7.85051 8 10 22 0 4.63898 4.40164 6 10 -22 0 12.1492 6.12543 8 10 22 0 3.13174 6.17620 9 10 -22 0 8.31967 5.24516 4 -10 22 0 18.0340 6.50421 7 -10 -22 0 6.25635 3.75552 1 11 22 0 32.9411 4.90133 6 11 -22 0 35.1427 6.94806 8 11 22 0 35.2022 7.41617 9 -11 22 0 32.5852 6.77645 7 -11 -22 0 29.0390 4.49504 1 -12 22 0 107.580 9.36083 7 -12 -22 0 112.676 7.14225 1 12 22 0 122.086 10.5800 9 12 -22 0 117.951 9.73505 8 12 22 0 108.511 7.14608 6 -13 22 0 105.770 9.17661 7 -13 -22 0 103.328 6.99736 1 13 -22 0 115.079 9.72691 8 13 22 0 96.5574 6.79811 6 13 22 0 111.229 10.6247 9 -14 22 0 62.1611 7.62724 7 -14 -22 0 56.7166 6.02200 1 14 22 0 52.4568 9.04935 9 14 -22 0 59.0828 8.39544 8 -15 -22 0 25.3439 5.46648 1 15 -22 0 28.5751 7.37100 8 15 22 0 32.4916 8.77684 9 -15 22 0 13.1647 6.60162 7 -16 -22 0 11.5765 5.02969 1 -16 22 0 20.4910 6.77806 7 16 22 0 27.4631 9.04251 9 16 -22 0 18.3344 7.43891 8 17 22 0 10.1210 7.95614 9 -17 22 0 16.7362 6.72888 7 18 -22 0 30.2644 7.77932 8 -18 22 0 28.8870 7.47134 7 18 22 0 37.0092 9.68390 9 -19 22 0 12.0107 6.84081 7 -20 22 0-2.32225 6.71211 7 -21 22 0-4.74427 7.49639 7 -22 22 0 12.7084 8.12396 7 0 -23 0-1.45193 4.81247 4 0 23 0 8.25107 5.68646 6 0 -23 0 8.78316 3.59337 1 -1 -23 0 80.4385 7.21833 4 1 -23 0 93.4313 7.60620 4 -1 23 0 79.3142 8.00987 6 -1 -23 0 92.2675 5.79037 1 1 23 0 75.3970 7.91510 6 2 23 0 2.89356 5.68084 6 2 -23 0 10.7742 5.22437 4 -2 -23 0 3.71476 3.38339 1 -2 -23 0 3.36916 4.81168 4 3 23 0 6.95627 5.36308 6 -3 -23 0 20.3031 3.65967 1 3 -23 0 22.2754 5.45238 4 4 23 0 6.64996 5.65161 9 -4 -23 0 12.7965 3.43181 1 4 23 0 5.35749 5.30758 6 4 -23 0 4.50133 5.24984 4 -5 -23 0 30.6989 3.93330 1 5 -23 0 19.1998 5.61536 4 5 -23 0 15.6408 6.52907 8 5 23 0 39.8880 6.07144 6 5 23 0 30.0642 6.77643 9 6 -23 0 53.3207 7.51294 8 6 23 0 46.4199 7.37915 9 -6 -23 0 54.7210 4.72117 1 6 -23 0 66.7490 6.97066 4 6 23 0 58.8335 6.42702 6 7 23 0-1.19112 5.90180 9 7 23 0-3.16181 5.02234 6 -7 23 0 7.00134 6.05298 7 7 -23 0 0.62890 6.16127 8 -7 -23 0 7.29926 3.46278 1 7 -23 0 8.32168 5.45149 4 8 23 0 9.45941 4.96166 6 -8 23 0 3.47751 6.09555 7 8 -23 0 9.44777 5.17890 4 8 23 0 11.0255 6.26104 9 8 -23 0 3.16017 5.92336 8 -8 -23 0 10.0494 3.73599 1 9 23 0 6.94717 6.29260 9 9 -23 0 11.4354 6.55568 8 9 -23 0-2.12990 5.40819 4 9 23 0-1.08414 4.71558 6 -9 23 0 7.47581 6.49481 7 -9 -23 0-1.20750 3.61074 1 -10 -23 0 15.2815 3.92325 1 10 23 0 7.60624 4.51712 6 10 -23 0 25.9143 5.95730 4 -10 23 0 14.8332 6.55972 7 10 23 0 9.79669 6.87935 9 10 -23 0 15.9667 7.15176 8 11 23 0 89.9035 9.63250 9 11 -23 0 82.5590 7.86304 4 11 -23 0 91.2341 9.09408 8 -11 23 0 86.0339 8.67218 7 -11 -23 0 78.4430 6.12347 1 11 23 0 79.4297 6.64738 6 12 23 0 27.3453 7.89135 9 -12 -23 0 31.9936 5.06692 1 -12 23 0 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-10 2 444.958 17.5878 8 -1 10 -2 448.369 17.2538 8 1 10 2 447.770 17.4261 8 -2 -10 -2 627.514 23.2435 4 2 -10 2 613.267 23.6310 8 2 10 2 623.596 23.5176 9 -2 10 -2 621.600 23.4451 10 -2 -10 -2 646.203 22.2717 1 2 -10 2 626.189 23.5479 9 2 10 2 612.077 22.3826 10 2 10 2 593.149 23.4742 8 -2 10 -2 603.817 23.3013 8 2 -10 2 600.701 23.6205 10 -3 10 -2 111.573 5.97541 10 3 10 2 120.617 5.57347 4 3 -10 2 121.183 6.05396 10 3 10 2 118.955 6.02695 8 3 -10 2 115.938 5.93834 9 -3 10 -2 122.458 5.87704 3 3 10 2 111.333 5.86507 9 3 -10 2 111.822 5.93363 8 -3 -10 -2 113.836 4.65920 1 4 10 2 133.580 6.12696 6 4 10 2 148.238 6.44839 4 -4 10 -2 132.392 6.50081 3 -4 -10 -2 138.348 5.54890 1 4 -10 2 139.313 6.83644 8 4 -10 2 145.771 6.77296 9 4 10 2 127.012 6.70325 8 4 10 2 141.192 6.92963 9 -4 10 -2 139.777 6.89527 10 5 10 2 13.3333 2.68604 9 5 10 2 12.4685 1.92140 6 5 10 2 13.2387 2.28080 4 -5 10 -2 10.1558 2.30955 3 5 10 2 14.8051 2.53227 8 -5 -10 -2 14.2826 1.65181 1 5 -10 2 11.2934 2.56637 8 -5 10 -2 14.8683 2.97709 10 -5 10 -2 15.1849 2.89973 7 -6 10 -2 70.0500 4.77233 10 -6 -10 -2 65.3880 3.53960 1 -6 10 -2 67.5202 4.85992 7 6 10 2 65.6684 3.50860 6 6 -10 2 74.0321 4.57992 8 -6 10 -2 68.1887 4.21710 3 6 10 2 64.2496 4.61815 9 6 10 2 65.2246 4.04526 4 -7 10 -2 906.947 33.4687 8 -7 10 -2 897.745 33.3091 3 7 10 2 872.157 33.3715 4 7 10 2 965.018 34.3793 9 7 -10 2 950.002 33.9287 8 -7 10 -2 897.642 34.1738 7 -7 -10 -2 928.740 32.9931 1 -7 10 -2 931.981 34.0806 10 7 10 2 888.071 32.6185 6 7 10 2 879.217 32.6302 1 -8 10 -2 2027.58 74.3145 7 8 10 2 2045.17 72.8478 1 -8 10 -2 2020.21 74.2510 10 8 10 2 2072.06 73.6026 4 -8 -10 -2 2013.94 73.2980 1 8 -10 2 2092.07 74.0902 8 -8 10 -2 2075.65 73.6476 8 8 10 2 2188.84 74.7227 9 8 10 2 2010.77 72.6287 6 9 10 2 706.030 24.5626 6 9 10 2 732.826 25.8171 4 9 10 2 730.229 26.1003 7 -9 10 -2 705.421 26.4709 7 9 10 2 716.764 25.0075 1 -9 10 -2 691.082 25.6969 8 -9 -10 -2 631.735 24.0485 10 -9 -10 -2 653.935 23.9715 10 9 -10 2 740.925 26.3154 8 9 10 2 764.201 26.9435 9 -9 10 -2 701.915 26.5434 10 -9 -10 -2 674.177 25.5430 1 10 10 2 193.926 8.15101 1 -10 -10 -2 177.215 7.15509 10 10 -10 2 183.498 9.13482 8 -10 -10 -2 182.148 8.65141 1 10 10 2 198.017 9.84229 9 10 -10 2 186.423 8.73627 3 10 10 2 195.596 7.47109 6 -10 10 -2 190.865 9.46522 7 -10 10 -2 180.441 8.71794 8 -11 -10 -2 262.139 10.5136 10 11 10 2 300.862 13.3962 9 11 10 2 281.730 10.6298 6 11 -10 2 283.595 11.9964 3 -11 10 -2 279.721 12.7671 7 11 10 2 286.464 11.4726 1 -11 -10 -2 278.128 11.9549 1 11 -10 2 266.647 12.3713 8 -12 -10 -2 97.7750 5.98580 1 -12 10 -2 97.0350 6.65074 7 12 10 2 116.161 5.78212 1 12 -10 2 97.5951 5.96711 3 -12 -10 -2 95.7910 4.59946 10 12 10 2 93.9413 4.52895 6 12 -10 2 106.463 6.64229 8 13 -10 2 6.16834 3.52354 8 -13 10 -2 4.14689 3.76621 7 13 10 2 8.80041 2.99496 1 13 10 2 8.60528 1.84692 6 13 -10 2 7.97924 3.18111 3 -13 -10 -2 7.73575 2.04598 10 -13 -10 -2 9.27272 3.21286 1 -14 10 -2 22.5107 4.27842 7 14 10 2 18.9624 3.52711 1 -14 -10 -2 20.5191 3.67515 1 14 -10 2 11.7724 3.45492 3 14 -10 2 15.9677 4.06797 8 -14 -10 -2 13.0721 2.33053 10 15 -10 2 20.4955 4.50858 8 -15 -10 -2 27.4816 4.24665 1 -15 -10 -2 28.7550 3.04954 10 15 -10 2 32.3118 4.23763 3 -15 10 -2 38.2210 5.04277 7 15 10 2 38.5640 3.90768 5 15 10 2 36.7730 4.29314 1 -16 10 -2 14.0702 4.75895 7 -16 -10 -2 15.4381 3.82717 1 16 10 2 17.0763 3.54131 5 -16 -10 -2 22.5686 2.95713 10 16 10 2 13.9838 4.86841 9 16 -10 2 14.8363 4.60393 8 16 -10 2 13.2655 3.70035 3 -17 10 -2 237.594 12.6041 7 17 -10 2 243.152 12.7195 8 17 10 2 247.777 13.2228 9 17 -10 2 251.218 11.7868 3 -17 -10 -2 235.440 11.5551 1 -17 -10 -2 243.790 10.2255 10 17 10 2 221.557 10.7640 5 -18 10 -2 384.398 18.0718 7 -18 -10 -2 391.975 17.0169 1 -18 -10 -2 397.615 15.5670 10 18 10 2 392.147 18.4892 9 18 -10 2 400.312 17.0885 3 18 10 2 369.194 16.1740 5 18 -10 2 387.198 18.1194 8 19 10 2 51.5361 5.33371 5 -19 10 -2 56.4570 7.23608 7 19 -10 2 65.9848 7.13742 8 -19 -10 -2 59.4406 4.04845 6 19 -10 2 64.2910 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104.379 4.26207 1 -3 11 -2 114.681 5.56639 3 3 -11 2 94.9376 5.62389 8 -3 11 -2 99.0861 5.67002 10 -4 11 -2 2.21774 2.24235 3 4 11 2 3.50506 1.97780 4 4 11 2 4.62602 2.60691 8 -4 -11 -2 5.03023 1.26817 1 4 11 2 3.82126 1.94276 6 4 11 2 4.36733 2.54274 9 -4 11 -2 5.40158 2.69117 10 4 -11 2 2.70402 2.41922 9 4 -11 2 8.02451 2.39716 8 5 -11 2-0.22822 2.33048 9 -5 -11 -2 2.03021 1.38335 1 -5 11 -2 1.69670 2.09555 8 -5 11 -2 0.60163 2.30418 3 5 -11 2 1.05556 2.30876 8 5 11 2-0.27468 2.38562 9 5 11 2 1.73705 2.23613 4 -5 11 -2-0.49702 2.90276 10 5 11 2 0.76231 2.39376 8 -5 11 -2 1.54811 2.75741 7 5 11 2 0.30366 1.81990 6 6 -11 2 144.655 7.69026 10 6 11 2 153.790 7.07080 4 -6 11 -2 146.650 7.07345 8 6 -11 2 133.081 7.32090 8 -6 -11 -2 145.828 6.24618 1 -6 11 -2 164.176 7.10832 3 6 11 2 150.808 7.71105 9 -6 11 -2 150.259 7.60487 10 6 11 2 139.480 7.36771 8 6 11 2 145.843 6.40456 6 -6 11 -2 149.484 7.83333 7 6 -11 2 140.276 7.23543 9 -7 11 -2 73.0316 5.39922 7 -7 11 -2 74.5439 4.54041 3 7 11 2 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102.846 5.09249 4 5 10 4 100.552 5.71149 7 -5 10 -4 101.865 6.17796 10 5 10 4 105.361 5.80141 8 5 10 4 119.604 6.34867 9 -5 10 -4 101.888 5.78626 3 5 -10 4 94.6803 5.57403 8 5 10 4 103.886 4.56074 6 6 10 4 96.3753 5.63979 8 6 10 4 91.9265 4.89467 4 -6 10 -4 94.3080 5.57213 3 -6 10 -4 94.0190 6.08073 10 6 10 4 90.9650 4.00435 6 6 10 4 91.6455 5.59020 7 -6 10 -4 107.390 6.29666 7 6 10 4 99.2218 6.16627 9 6 10 4 89.8973 3.94735 1 6 -10 4 96.7918 5.51037 8 7 10 4 2005.50 68.8436 1 7 10 4 1970.56 69.6992 4 -7 10 -4 1866.16 70.8912 7 7 10 4 1993.64 70.3448 7 -7 10 -4 1926.92 70.5678 10 7 10 4 2047.35 71.2058 9 7 -10 4 1936.42 70.2118 8 7 10 4 1882.49 68.5062 6 -7 10 -4 1996.48 69.8979 8 -8 10 -4 2057.56 68.7470 7 8 10 4 2045.34 67.3014 4 8 10 4 2040.96 68.0024 7 8 -10 4 2008.90 68.1777 3 8 10 4 2056.40 66.4531 1 8 -10 4 1911.47 68.5284 10 8 -10 4 2044.96 67.9036 8 -8 10 -4 2055.45 67.4667 8 -9 10 -4 271.358 12.8405 7 -9 10 -4 294.069 11.8855 8 9 -10 4 259.638 12.7255 10 9 -10 4 272.736 12.4400 3 9 10 4 277.440 10.9653 1 9 -10 4 276.014 12.1781 8 -10 10 -4 35.9034 4.63854 7 -10 10 -4 31.3978 3.74764 8 10 -10 4 39.2807 4.28040 3 10 -10 4 30.8829 4.63830 10 10 -10 4 32.5275 3.97726 8 10 10 4 35.0103 3.04558 1 -11 10 -4 96.6379 7.23218 7 11 -10 4 121.110 7.65002 10 11 -10 4 115.788 7.01126 3 11 -10 4 110.203 6.78116 8 11 10 4 110.775 5.75933 1 -12 10 -4 55.6190 5.82838 7 12 -10 4 60.1503 5.31871 3 12 -10 4 42.7737 5.64442 10 12 -10 4 56.9571 5.05127 8 12 10 4 56.5979 4.18410 1 13 -10 4 12.7337 3.86523 8 13 -10 4 11.1580 3.84208 3 13 10 4 16.2432 3.22000 1 -13 10 -4 6.08755 4.32950 7 -14 10 -4 21.9469 5.01526 7 -14 -10 -4 19.9390 1.58874 10 14 -10 4 21.8502 4.45244 8 14 -10 4 32.4977 4.59875 3 14 10 4 26.0256 3.71897 1 15 10 4-4.25689 2.83499 5 15 -10 4 7.01951 4.38122 3 -15 -10 -4-0.48378 1.70833 10 -15 10 -4-2.87095 4.76746 7 15 -10 4 0.41892 4.12710 8 15 10 4-3.40212 3.46294 1 16 10 4 31.6574 3.58538 5 -16 10 -4 41.8445 6.27527 7 16 -10 4 28.7296 5.27599 3 -16 -10 -4 24.9233 2.63240 10 -16 -10 -4 34.3610 5.26197 2 16 -10 4 28.8385 5.56703 8 -17 -10 -4 241.302 12.7917 2 -17 10 -4 258.201 13.8724 7 -17 -10 -4 247.960 10.1018 10 17 -10 4 265.832 13.1381 3 17 -10 4 258.564 13.3412 8 17 10 4 247.130 10.8908 5 18 10 4 185.628 11.9504 9 -18 -10 -4 210.951 11.3219 2 18 -10 4 203.198 11.4661 3 -18 -10 -4 203.895 8.58789 10 -18 10 -4 184.375 12.0976 7 18 -10 4 212.889 11.9566 8 18 10 4 192.886 9.24395 5 -19 -10 -4 2.88095 4.46718 2 19 -10 4 8.08772 4.89459 3 19 10 4 1.68210 5.16574 9 19 -10 4 0.55342 5.11534 8 19 10 4 6.10976 3.27787 5 -19 10 -4-7.16030 5.87903 7 -20 -10 -4 9.42358 5.27830 2 20 -10 4 17.7016 5.67111 8 -20 10 -4 12.6909 6.51963 7 20 10 4 25.1687 6.34218 9 20 -10 4 15.8992 5.36730 3 -21 10 -4-2.02338 6.45205 7 21 10 4 6.98638 5.60324 9 21 -10 4 6.66419 5.39268 3 -21 -10 -4 0.51257 5.24809 2 21 -10 4-1.88260 5.70479 8 -22 -10 -4 63.7303 7.22341 2 -22 10 -4 48.5711 8.46521 7 22 10 4 37.3909 7.31443 9 22 -10 4 45.1494 6.93176 3 22 -10 4 48.5787 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524.466 18.8772 1 -4 11 4 530.252 19.8978 8 -4 11 4 539.464 19.9736 10 -3 -11 4 70.8379 4.90474 4 -3 11 4 78.2525 4.65732 8 3 -11 -4 80.2672 5.00764 8 3 -11 -4 69.9637 3.96206 4 -3 11 4 79.4393 4.49911 10 -3 11 4 79.7705 4.24311 9 3 11 -4 65.2867 5.07007 6 -3 -11 4 66.8551 4.88746 9 3 -11 -4 71.9030 3.26804 1 2 -11 -4 996.289 36.0915 1 2 11 -4 1025.16 38.3048 6 2 -11 -4 998.903 37.0505 4 -2 11 4 1070.83 37.1924 10 -2 11 4 1051.58 37.3117 9 -2 11 4 1062.41 37.6387 8 2 -11 -4 1052.12 38.0683 8 -2 -11 4 1042.09 38.1850 4 1 -11 -4 257.916 10.3656 4 -1 -11 4 267.542 11.4199 4 1 -11 -4 260.471 11.3225 8 -1 11 4 249.160 10.6505 9 -1 11 4 260.679 10.2724 10 -1 11 4 252.898 10.8511 8 1 11 -4 262.316 11.5649 6 0 11 -4 40.1932 3.81271 10 0 -11 -4 40.1795 2.92427 4 0 -11 4 38.2068 3.71209 4 0 -11 4 49.6712 3.78342 8 0 11 4 38.4347 2.59632 10 0 11 4 34.6367 3.15707 9 0 11 -4 42.8824 3.89713 3 0 11 4 37.2838 3.40750 8 0 11 -4 39.3646 4.08144 6 1 -11 4 91.2519 5.63128 9 -1 11 -4 90.0264 5.64326 10 1 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41.9379 3.60889 8 5 11 4 44.0482 2.86994 6 -6 11 -4 848.693 33.6118 7 6 11 4 908.812 33.0089 8 6 11 4 871.419 32.1728 4 6 11 4 885.597 32.8063 7 -6 11 -4 839.713 33.0559 10 6 -11 4 899.122 32.9349 8 6 11 4 927.971 33.5984 9 -6 11 -4 890.684 32.7797 3 6 11 4 851.256 31.3955 6 -6 11 -4 865.065 32.4474 8 7 11 4 155.596 7.19887 4 7 11 4 159.216 8.01736 8 7 11 4 153.930 7.92590 7 7 -11 4 160.803 7.96006 8 7 11 4 166.168 8.69345 9 -7 11 -4 156.150 7.48131 8 7 11 4 149.927 6.09821 6 -7 11 -4 148.915 8.55317 7 7 11 4 150.745 6.17185 1 8 11 4 259.560 10.5161 4 8 11 4 253.452 9.48220 1 8 11 4 242.569 11.9296 9 8 11 4 233.054 8.98336 6 -8 11 -4 242.642 11.7226 7 8 -11 4 236.376 10.9740 8 -8 11 -4 243.620 10.5250 8 -9 11 -4 29.5672 4.26009 7 9 11 4 27.1094 3.29810 4 9 11 4 18.6737 1.18200 6 9 11 4 20.7668 4.51044 9 9 -11 4 19.4679 3.56856 8 9 11 4 26.0330 2.48934 1 -9 11 -4 23.2065 3.31013 8 10 11 4 189.845 10.6453 9 10 -11 4 197.055 9.77553 3 10 11 4 196.994 9.12944 4 -10 11 -4 195.653 10.3199 7 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260.375 12.5970 9 5 -16 4 280.242 12.7264 8 6 16 4 74.2427 6.23633 9 -6 16 -4 64.7399 6.71327 7 6 -16 4 66.0839 6.16110 10 6 16 4 60.9894 4.31926 6 6 -16 4 59.4450 5.70635 8 7 -16 4 58.5739 6.24449 10 7 16 4 58.5764 4.06065 6 7 -16 4 65.2569 6.00476 8 -7 16 -4 67.1837 6.45988 7 7 16 4 71.4292 6.28675 9 -8 16 -4 7.80710 4.87644 7 8 16 4-1.85209 4.49723 9 8 -16 4 12.1898 4.95126 10 8 -16 4 9.86936 4.40746 8 8 16 4 0.29355 2.22439 6 -9 16 -4 33.0689 5.62651 7 9 -16 4 32.2990 5.20977 8 9 -16 4 24.3176 5.40313 10 9 16 4 29.6247 2.77996 6 9 16 4 19.2447 5.36733 9 -10 16 -4 367.478 17.7444 7 10 16 4 377.071 14.4254 6 10 -16 4 406.099 17.4400 8 10 -16 4 391.878 18.0418 10 10 16 4 396.392 18.2271 9 11 -16 4 340.181 14.9296 8 -11 16 -4 278.510 14.9934 7 11 16 4 337.103 16.0117 9 11 16 4 294.926 11.4354 6 11 -16 4 297.733 15.4317 10 12 16 4 21.5904 2.08742 6 -12 16 -4 26.0753 6.03091 7 12 -16 4 24.3257 5.41897 8 12 16 4 27.8251 6.64570 9 -13 16 -4 42.1109 6.67850 7 13 -16 4 40.9056 6.23301 8 13 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33.8951 3.56854 6 -5 -8 5 33.6493 3.22397 4 -5 8 5 33.7415 2.69674 1 5 -8 -5 34.9040 2.30936 2 -5 8 5 29.3782 3.85154 6 -5 -8 5 34.7610 3.38983 9 5 8 -5 38.6091 3.03796 8 5 -8 -5 34.3033 2.30135 1 5 -8 -5 40.2135 3.03170 8 -5 8 5 39.0269 3.00518 8 4 -8 -5 2.38257 1.88015 8 -4 -8 5 3.32033 2.18809 4 -4 8 5 4.01026 1.57445 1 -4 8 5 1.74555 2.74318 6 4 -8 -5 2.99672 1.23268 2 -4 8 5 6.39479 1.99905 8 -4 8 5 3.70094 1.28705 9 -4 -8 5 3.92843 2.48492 9 4 8 -5 2.28155 1.75782 8 4 8 -5 3.04029 2.30635 6 4 -8 -5 4.14993 1.24992 1 3 8 -5 177.240 8.51011 6 3 -8 -5 177.685 6.88381 1 -3 8 5 182.066 7.37360 9 -3 8 5 196.000 7.08561 1 -3 -8 5 180.636 8.29725 4 -3 -8 5 186.022 8.44425 9 3 -8 -5 180.009 7.03113 4 -3 8 5 152.858 8.44577 6 -3 8 5 191.891 7.82433 8 3 8 -5 170.330 7.68159 8 3 -8 -5 177.034 7.96622 8 -2 -8 5 572.829 22.2766 9 2 -8 -5 586.375 20.8896 4 -2 -8 5 560.502 22.1842 4 -2 8 5 549.059 22.2135 6 2 -8 -5 578.841 21.9181 8 2 8 -5 578.704 22.4429 6 2 8 -5 563.973 21.5407 8 -2 8 5 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16 -5 131.754 8.00803 6 1 -16 -5 29.8841 3.41712 4 -1 -16 5 18.2311 4.56942 4 -1 -16 5 30.7860 4.59448 10 -1 16 5 30.4413 4.01346 9 -1 16 5 27.7303 2.96217 10 1 16 -5 32.7388 5.34420 6 0 -16 5-0.41781 3.94788 4 0 16 5 1.16827 2.14196 10 0 -16 5 0.39981 3.87047 10 0 16 5-2.39426 3.37263 9 0 16 -5 0.43797 4.20210 6 1 16 5 18.2889 3.94006 9 1 -16 5 16.0318 4.54299 4 1 -16 5 10.6641 4.38678 10 1 16 5 15.9736 2.16535 10 -1 16 -5 16.9709 4.88518 6 2 -16 5 1.95089 3.62951 8 2 -16 5 8.40107 4.37965 10 2 16 5 0.11740 1.37515 10 2 16 5 3.65663 3.57063 9 -2 16 -5 0.91489 4.68349 6 2 -16 5 8.95821 4.58181 4 -3 16 -5 115.732 8.51012 7 3 -16 5 113.381 7.77968 4 3 16 5 116.535 7.26204 9 3 -16 5 103.783 7.78205 10 3 -16 5 111.522 7.50322 8 -3 16 -5 122.270 8.46680 6 -4 16 -5 27.9934 5.16253 7 4 -16 5 49.0430 5.55357 4 4 -16 5 36.7391 5.62836 10 4 16 5 47.9912 5.21875 9 4 -16 5 36.4420 5.23134 8 -5 16 -5 17.8469 5.26823 7 5 -16 5 7.28265 4.73035 10 5 16 5 8.30082 4.19404 9 5 -16 5 1.96633 3.86331 8 5 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658.940 25.0289 6 4 6 7 677.647 23.7969 5 -4 6 -7 667.532 23.7145 8 -5 6 -7 324.979 14.2958 7 5 6 7 347.033 14.5684 7 -5 6 -7 330.041 14.0389 10 5 6 7 335.224 12.6828 10 5 -6 7 313.809 14.2232 10 5 -6 7 323.225 12.9077 8 -5 6 -7 341.492 14.0938 6 5 6 7 321.901 12.0513 6 5 6 7 348.688 12.5727 5 -5 6 -7 339.130 12.8634 8 -6 6 -7 7.51619 3.29772 7 6 6 7 9.03127 3.52314 7 6 6 7 8.57641 2.14661 1 6 -6 7 8.33299 3.27479 10 -6 6 -7 10.1843 3.16335 10 6 6 7 8.40270 1.92579 10 6 -6 7 5.57603 2.01932 8 -6 -6 -7 8.78491 2.07849 2 -6 6 -7 7.94523 3.10895 6 6 6 7 5.22229 1.36810 5 -6 6 -7 7.49469 2.16252 8 -7 6 -7 23.6515 3.80613 7 7 6 7 24.6045 4.28893 7 7 6 7 27.9776 2.75224 1 7 6 7 26.3095 2.39363 10 7 -6 7 30.9515 4.24233 10 7 -6 7 24.8396 2.79653 8 -7 -6 -7 23.9787 2.75780 2 -7 6 -7 24.1388 3.54775 6 -8 6 -7 43.2038 4.52227 7 8 6 7 33.3389 4.83630 7 8 6 7 41.7938 3.52215 1 8 -6 7 25.9059 4.41166 10 8 6 7 40.8779 2.83335 10 -8 -6 -7 36.5974 3.37808 2 8 -6 7 30.8275 3.16091 8 -8 6 -7 36.8859 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8 1226.75 47.6670 7 0 -8 8 1303.55 47.7952 4 0 8 8 1282.12 45.9876 1 0 -8 8 1334.88 48.4788 10 0 8 8 1324.58 46.7053 6 0 8 -8 1343.87 48.2535 6 0 8 8 1276.37 46.7051 8 0 8 -8 1322.22 46.4201 8 -1 8 -8 3.01392 3.35640 7 1 8 8 4.09783 1.44079 1 1 8 8-0.89340 3.48661 7 1 -8 8 1.42616 2.75477 4 1 8 8 3.48628 2.03639 6 -1 8 -8 7.86022 3.38957 6 1 8 8 1.42873 2.08024 8 -1 8 -8 1.47734 1.76368 8 1 -8 8 1.81404 3.60585 10 -2 8 -8 99.3607 6.44400 7 2 8 8 86.8541 6.35484 7 2 -8 8 94.7489 6.07695 4 2 8 8 99.2814 4.86592 10 2 8 8 104.536 4.33752 1 2 8 8 100.119 4.80256 6 2 -8 8 102.229 6.81588 10 2 -8 8 98.7281 5.07999 8 -2 8 -8 109.290 6.59959 6 2 8 8 104.253 5.18476 8 -2 8 -8 101.574 4.81991 8 -3 8 -8 176.138 8.89755 7 3 8 8 169.906 8.93699 7 3 8 8 156.910 6.83475 10 3 -8 8 156.385 8.92792 10 3 8 8 162.706 6.67877 6 3 -8 8 167.881 7.24602 8 3 8 8 164.456 7.34307 8 -3 8 -8 150.653 8.58520 6 -3 8 -8 157.905 6.92398 8 -4 8 -8 818.885 33.2833 7 4 8 8 909.811 33.4162 7 4 8 8 931.926 31.1454 1 4 8 8 845.984 30.8199 4 4 -8 8 869.341 33.4568 10 4 8 8 859.057 30.9588 6 4 8 8 866.924 31.2436 10 4 -8 8 812.182 31.6316 8 4 8 8 851.138 31.8341 8 -4 8 -8 880.232 33.1664 6 -4 8 -8 853.783 31.4708 8 -5 8 -8 421.179 18.0012 7 5 8 8 426.177 15.5846 4 5 8 8 462.250 18.2119 7 5 8 8 454.531 15.9323 1 5 8 8 420.568 15.7250 10 5 -8 8 401.791 17.9893 10 5 8 8 403.926 16.4670 8 5 -8 8 402.169 16.2792 8 -5 8 -8 434.502 17.8581 6 5 8 8 408.610 15.2051 6 -5 8 -8 428.560 16.1725 8 -6 8 -8 103.803 7.01428 7 6 8 8 102.251 7.14127 7 6 8 8 103.246 5.08229 1 6 -8 8 84.8851 6.85087 10 6 8 8 101.209 4.60892 10 6 8 8 99.2097 5.62366 8 6 -8 8 97.9558 5.36050 8 -6 8 -8 106.193 6.78089 6 -6 -8 -8 98.1390 4.94279 2 6 8 8 100.805 4.81215 5 -6 8 -8 98.0725 5.19997 8 -7 8 -8 23.3224 4.36066 7 7 -8 8 24.1107 4.83966 10 7 8 8 22.1980 2.17401 10 7 8 8 23.3495 3.07172 1 7 8 8 24.8676 3.38735 8 7 -8 8 16.7502 2.90594 8 -7 8 -8 24.5590 4.25568 6 -7 -8 -8 22.8236 2.84281 2 7 8 8 17.5652 2.06122 5 8 -8 8 47.1126 5.64367 3 -8 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9 120.087 7.72932 5 -3 8 9 126.369 5.87301 1 2 8 -9 104.164 6.50773 7 -2 8 9 99.4405 4.62281 1 -2 8 9 111.708 5.44161 7 -2 -8 9 97.7680 6.04455 4 -2 -8 9 102.061 6.91900 10 -2 8 9 94.4470 5.41841 6 2 8 -9 94.5841 6.52984 6 2 8 -9 99.8214 4.64666 8 -2 8 9 101.683 4.98870 8 -2 8 9 84.6390 6.32306 5 1 8 -9 23.5025 4.00700 7 -1 8 9 26.5431 3.31358 7 -1 -8 9 31.0198 3.79278 4 -1 -8 9 29.7291 4.46990 10 -1 8 9 20.3307 2.99147 6 -1 8 9 24.7501 2.20032 1 1 8 -9 23.7638 4.21924 6 1 8 -9 26.0686 2.26877 8 -1 8 9 28.0993 2.65080 8 -1 8 9 23.7162 3.85122 5 0 8 -9 11.0452 3.57150 7 0 8 9 19.4894 3.43702 7 0 -8 9 20.1520 3.31890 4 0 -8 9 17.3176 4.09662 10 0 8 9 8.89720 2.45401 6 0 8 -9 3.84968 3.65781 6 0 8 9 13.7426 2.24247 8 0 8 -9 13.0300 1.91698 8 0 8 9 13.0984 3.50686 5 0 8 9 12.5293 1.79704 1 -1 8 -9 24.8602 4.00065 7 1 8 9 25.5022 3.84807 7 1 -8 9 31.9947 3.95353 4 1 -8 9 23.0177 4.59238 10 1 8 9 24.3623 2.67849 6 -1 8 -9 29.0802 4.27249 6 1 8 9 28.4690 2.71809 8 1 8 9 26.6847 2.18387 1 -1 8 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4.38608 2.14122 1 5 -8 9 3.75722 4.22994 10 5 8 9 0.13695 2.14228 10 5 -8 9 3.12855 2.35395 8 5 8 9 3.27529 2.64792 8 -5 8 -9-3.24180 3.67957 6 5 8 9 3.54452 1.38369 6 -5 8 -9 1.26706 2.06289 8 6 8 9 44.5298 2.80091 4 -6 8 -9 43.7226 5.35866 7 6 8 9 43.2343 3.38355 1 6 8 9 42.3350 3.11657 10 6 -8 9 45.2908 5.89246 10 6 8 9 46.3373 3.94182 8 6 -8 9 44.9580 3.59549 8 -6 8 -9 43.1463 4.88115 6 6 8 9 41.6897 2.67902 5 -7 8 -9 275.251 14.1109 7 7 8 9 311.027 12.1502 1 7 -8 9 287.063 14.2922 10 7 8 9 289.382 11.6006 10 7 8 9 310.684 12.6010 8 7 -8 9 307.597 12.3406 8 -7 8 -9 294.202 13.7602 6 -8 8 -9 136.807 9.71900 7 8 8 9 168.940 7.94074 1 8 -8 9 169.708 10.1125 10 8 8 9 164.827 7.09282 10 8 8 9 178.732 8.36107 8 8 -8 9 166.711 7.96583 8 -8 8 -9 193.471 9.57203 6 -9 8 -9 2.90890 4.36427 7 9 -8 9 2.27558 4.72230 10 9 -8 9 3.01057 4.40717 3 9 8 9 3.86291 3.04337 1 9 -8 9 3.94542 2.92562 8 -9 8 -9 5.02409 4.00025 6 -10 8 -9 18.7837 5.28914 7 10 -8 9 28.8226 5.69934 10 10 -8 9 31.8781 5.34103 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56.5565 5.11606 8 5 14 9 49.2857 6.17209 9 -5 14 -9 52.0576 6.42123 6 -5 -14 -9 49.3615 3.49021 2 -6 -14 -9 3.66842 2.58123 2 -6 14 -9 8.64559 5.26467 7 6 -14 9-0.47685 5.12424 4 6 -14 9 5.46789 5.49585 10 6 14 9 4.46397 5.09413 9 6 -14 9 7.86741 3.77776 8 -6 14 -9 7.20287 5.21395 6 -7 -14 -9 40.4261 3.79313 2 -7 14 -9 47.5547 6.71149 7 7 -14 9 43.4234 6.80518 10 7 14 9 45.6815 6.49820 9 7 -14 9 54.2523 5.27814 8 -7 14 -9 44.0709 6.65648 6 -8 14 -9 118.629 8.95230 7 8 -14 9 96.2151 8.90151 10 8 14 9 90.2434 8.65770 9 8 -14 9 115.666 7.19565 8 -8 14 -9 129.308 9.26365 6 -8 -14 -9 110.658 6.20899 2 -9 14 -9 0.58177 5.89267 7 9 -14 9-8.06829 6.42324 10 9 14 9 3.62991 5.36869 9 9 -14 9 3.17391 4.05160 8 -9 14 -9-0.55063 5.45541 6 -9 -14 -9 2.40895 3.19415 2 -10 14 -9 121.273 9.68095 7 10 -14 9 116.717 9.79946 10 10 -14 9 138.736 8.21311 8 -10 14 -9 124.913 9.71128 6 -10 -14 -9 131.589 7.24162 2 11 14 9 80.9030 8.71850 9 11 -14 9 89.9562 6.92828 8 11 -14 9 81.1755 8.74217 10 -11 -14 -9 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2.68588 2 5 3 10 2.32102 1.87038 8 -6 3 -10 4.62687 2.17955 5 6 3 10 9.87681 3.33338 10 -6 3 -10 4.26120 4.41409 7 -6 -3 -10 7.05361 4.20857 7 6 -3 10 11.4838 3.90670 10 -6 -3 -10 7.10546 2.49587 6 6 -3 10 4.53602 4.51222 3 -6 3 -10 1.07454 3.46060 6 6 3 10 10.7808 2.11613 8 6 -3 10 6.08556 1.64147 8 6 -3 10 8.63978 3.13936 2 6 3 10 3.55438 2.14173 8 -7 3 -10 195.739 10.6408 7 -7 -3 -10 206.240 10.4291 7 -7 -3 -10 181.369 7.82048 6 7 -3 10 192.536 9.96079 10 7 3 10 206.208 9.06781 10 7 -3 10 198.924 10.8034 3 -7 3 -10 184.596 8.94298 6 7 -3 10 187.575 7.53681 8 7 -3 10 202.713 8.76590 2 -7 3 -10 174.176 7.37935 5 7 3 10 147.636 7.86135 8 -8 3 -10 184.673 10.4654 7 -8 -3 -10 195.009 10.2887 7 -8 -3 -10 176.776 7.31145 6 8 -3 10 169.907 9.54840 10 8 3 10 161.025 8.46226 10 8 -3 10 175.332 10.4588 3 -8 3 -10 173.281 8.61331 6 8 -3 10 171.746 7.40856 8 8 -3 10 167.692 8.37045 2 8 3 10 163.075 7.87996 8 -9 3 -10 2.61630 4.97573 7 -9 -3 -10 0.93205 4.51246 7 -9 -3 -10 3.31784 1.85150 6 9 -3 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7 17 4 -10 94.8953 8.12730 6 -17 4 10 94.2531 8.05885 1 -17 4 10 98.7108 6.67618 2 17 -4 -10 81.3955 6.62547 8 17 4 -10 83.8300 6.59111 8 -17 -4 10 96.7744 7.96163 1 -16 -4 10 101.968 8.20761 1 16 4 -10 111.782 5.61053 7 16 4 -10 114.294 8.54901 6 -16 -4 10 110.628 6.32437 9 -16 4 10 113.242 8.07402 1 -16 4 10 121.211 7.09524 2 16 -4 -10 106.281 6.97177 8 16 4 -10 97.1679 6.92568 8 15 4 -10 0.90423 2.36637 7 15 4 -10-4.68898 5.19165 6 -15 -4 10-2.15413 4.42316 1 -15 -4 10 4.52190 3.25290 9 15 -4 -10 7.85025 3.45520 8 -15 4 10 6.23640 4.49749 1 -15 4 10 1.84766 3.42557 2 15 4 -10 3.60119 3.37922 8 14 4 -10 15.2365 2.52630 7 14 4 -10 16.1635 5.14831 6 -14 -4 10 8.27529 3.40643 9 -14 -4 10 9.51942 4.52422 1 14 -4 -10 12.1222 3.65035 8 -14 4 10 19.1728 3.53489 2 -14 4 10 16.6358 4.58807 1 14 4 -10 7.91767 5.39867 5 14 4 -10 15.6426 3.49763 8 -13 4 10 38.7999 5.17937 1 13 4 -10 49.4236 6.08147 6 -13 -4 10 36.3538 4.02119 9 -13 -4 10 51.5909 5.57899 1 13 -4 -10 41.0841 4.05363 8 -13 4 10 41.9834 4.21977 2 13 4 -10 37.4780 4.08172 8 13 4 -10 26.4778 5.81838 5 -12 -4 10 297.617 13.6958 1 -12 4 10 285.037 10.8521 9 -12 -4 10 297.823 12.4204 9 -12 4 10 283.330 12.1758 2 12 -4 -10 308.123 12.3449 8 -12 4 10 315.695 13.2880 1 12 4 -10 306.818 14.9253 5 12 4 -10 249.874 12.2881 8 11 4 -10 227.605 10.6151 7 11 -4 -10 258.117 10.3176 4 11 4 -10 282.138 11.3859 4 -11 4 10 246.485 9.81818 9 -11 -4 10 259.396 11.2009 9 -11 -4 10 272.059 12.4384 1 -11 4 10 258.053 10.7277 2 11 -4 -10 273.083 10.8759 8 -11 4 10 247.448 11.6065 1 11 4 -10 256.625 13.0925 5 11 4 -10 227.805 10.8696 8 10 4 -10 144.827 6.80590 7 10 -4 -10 143.452 6.17874 4 10 4 -10 146.554 7.32309 4 -10 -4 10 123.497 7.12372 9 -10 4 10 129.041 6.00830 9 -10 -4 10 163.477 8.66038 1 10 -4 -10 142.149 6.66955 8 -10 4 10 142.950 6.56274 2 10 4 -10 151.401 9.13868 5 10 4 -10 135.952 6.78417 8 -10 4 10 133.237 7.49420 1 9 4 -10 82.1305 5.00145 7 -9 4 10 85.5532 5.68890 1 9 -4 -10 88.7494 4.26957 4 9 4 -10 87.6068 5.37550 4 -9 -4 10 87.9696 5.66433 9 -9 4 10 86.5373 4.51121 9 9 -4 -10 95.9735 4.84598 8 -9 4 10 92.7639 4.52725 2 9 4 -10 103.773 7.28969 5 9 4 -10 83.5498 4.77406 8 -9 -4 10 92.2723 6.30616 1 8 4 -10 21.6477 4.53232 5 8 4 -10 20.0458 2.86828 7 8 -4 -10 20.4538 1.89606 4 8 -4 -10 25.9416 5.07366 6 8 4 -10 21.4960 4.13193 6 -8 4 10 21.4650 3.50810 1 -8 -4 10 27.3616 3.84624 9 8 -4 -10 21.1799 2.43348 8 -8 4 10 21.9191 2.05001 2 8 4 -10 19.5401 3.08221 4 -8 -4 10 19.7290 4.10573 1 8 4 -10 21.3845 2.34031 8 7 4 -10 53.9260 4.06831 7 7 -4 -10 54.4036 5.72583 6 -7 -4 10 58.6334 5.13499 1 7 4 -10 58.4622 5.31424 6 -7 -4 10 69.7160 4.96676 9 7 4 -10 56.7623 3.14406 8 -7 4 10 51.4335 4.33727 1 7 -4 -10 63.8073 3.49547 8 7 4 -10 62.6619 3.24438 8 7 4 -10 64.2262 5.85530 5 -6 4 10 337.941 14.3974 5 6 4 -10 345.034 13.5409 7 6 -4 -10 388.591 15.4805 6 -6 4 10 349.341 13.6456 1 6 4 -10 352.758 14.6524 6 -6 -4 10 325.018 14.0427 9 6 -4 -10 340.425 12.5672 8 6 4 -10 291.184 12.0536 8 -6 -4 10 356.965 14.5826 1 6 4 -10 331.746 12.1411 8 6 4 -10 369.393 15.2262 5 -5 4 10 228.670 10.5120 5 5 4 -10 203.336 9.64980 7 -5 -4 10 224.600 10.5964 1 5 -4 -10 231.553 11.2414 6 -5 4 10 224.028 9.85778 3 5 4 -10 219.998 10.6972 6 -5 4 10 204.599 9.99754 6 -5 4 10 220.572 9.70503 1 5 4 -10 241.550 11.1642 5 4 4 -10 2.41271 3.44361 5 4 4 -10 5.37979 2.40096 7 -4 4 10-1.79259 3.08086 5 4 -4 -10 0.73285 3.51568 6 -4 4 10 1.23093 2.62401 1 -4 4 10-0.73888 2.69557 3 4 4 -10-4.53128 3.56685 6 -4 4 10-4.20378 3.14012 6 -4 -4 10-0.63191 3.37699 1 -3 4 10 5.36057 1.91606 7 3 4 -10 5.24150 3.29238 5 -3 4 10 0.46188 2.94520 5 -3 -4 10 3.78691 2.37261 4 -3 -4 10 1.87118 3.58096 10 3 -4 -10 2.08052 3.34818 6 3 4 -10-1.90402 3.35992 6 -3 4 10 3.65861 2.97833 3 -3 4 10-0.22171 3.00521 6 -3 4 10 2.19495 2.69682 1 2 4 -10 59.9123 4.81331 5 -2 4 10 53.3579 3.39487 7 -2 -4 10 51.0455 3.85493 4 -2 -4 10 41.0985 5.01665 10 2 -4 -10 44.5346 4.52223 6 -2 4 10 45.8933 3.73143 1 2 4 -10 47.5500 4.58459 6 -2 4 10 51.1010 4.03509 6 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44.2230 3.83705 5 -2 4 -10 37.1566 4.47377 7 2 -4 10 50.3838 3.99085 4 2 4 10 44.4500 3.95938 10 2 -4 10 47.4432 5.16261 10 -2 -4 -10 39.7358 3.87037 6 2 -4 10 38.1527 4.99921 3 -2 4 -10 50.9052 4.43901 6 2 4 10 43.7396 3.46726 6 2 4 10 37.6219 4.80207 3 2 4 10 37.8603 2.14712 8 -3 4 -10 125.290 6.81428 5 3 4 10 131.553 7.26949 7 -3 4 -10 141.115 7.90553 7 3 4 10 138.020 5.27930 4 -3 -4 -10 135.633 7.42114 7 3 4 10 139.760 7.08074 10 3 -4 10 136.293 6.96939 4 -3 -4 -10 140.247 6.94011 6 3 -4 10 157.643 8.43492 10 3 -4 10 139.206 8.46327 3 -3 4 -10 144.586 7.45401 6 3 4 10 128.676 5.41221 8 3 4 10 121.918 6.26470 6 -4 4 -10 212.291 9.43228 5 4 4 10 240.019 10.5818 7 -4 4 -10 214.341 10.8184 7 -4 -4 -10 217.825 10.5275 7 -4 -4 -10 213.442 9.41630 6 4 -4 10 209.155 10.7532 10 4 4 10 209.075 9.64613 10 4 -4 10 230.975 11.4177 3 -4 4 -10 230.622 10.2830 6 4 4 10 202.956 8.34872 8 4 4 10 217.388 8.94926 6 -5 4 -10 228.702 9.73861 5 5 4 10 242.086 11.3218 7 -5 4 -10 258.607 11.8938 7 -5 -4 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15.1581 7 -9 -4 -10 315.967 14.4236 7 9 -4 10 291.396 13.8168 10 9 4 10 313.365 12.5987 10 9 -4 10 286.342 14.7578 3 -9 4 -10 324.578 13.0723 6 9 -4 10 299.084 11.7940 8 -9 4 -10 265.557 10.7888 5 -10 4 -10 160.372 10.1344 7 -10 -4 -10 161.143 9.51402 7 10 -4 10 139.487 9.00049 10 10 4 10 147.564 7.75674 10 -10 4 -10 167.387 8.31411 6 10 -4 10 146.272 7.17598 8 10 4 10 143.745 7.61274 8 -11 4 -10 23.2206 6.02093 7 -11 -4 -10 15.5265 4.88228 7 11 -4 10 25.1454 4.98012 10 11 4 10 22.8553 3.97943 10 -11 4 -10 27.7751 4.11896 6 11 -4 10 26.1694 3.48067 8 11 4 10 27.4275 3.84475 8 -12 4 -10 54.3068 7.25708 7 -12 -4 -10 58.2804 6.56640 7 12 -4 10 56.9609 6.45105 10 12 4 10 52.2369 4.90201 10 -12 4 -10 64.0883 5.32771 6 12 -4 10 50.0840 4.61884 8 12 4 10 60.4211 5.00306 8 -13 4 -10 153.240 11.2213 7 -13 -4 -10 154.152 10.3686 7 13 -4 10 151.819 9.77182 10 -13 4 -10 168.936 8.77666 6 13 -4 10 150.227 8.19913 8 13 4 10 162.748 8.55128 8 -14 4 -10 224.011 13.3580 7 -14 -4 -10 210.445 12.3023 7 14 -4 10 212.308 11.6531 10 14 -4 10 196.810 13.2790 3 -14 4 -10 214.983 10.5300 6 14 -4 10 212.458 10.3961 8 14 4 10 202.287 10.3594 8 -15 4 -10 140.035 11.2687 7 -15 -4 -10 152.380 10.6944 7 15 -4 10 152.093 9.93220 10 15 -4 10 163.889 12.0366 3 -15 4 -10 172.043 8.93655 6 15 -4 10 168.359 8.99620 8 15 4 10 148.220 8.66006 8 -16 4 -10 39.6622 7.60361 7 -16 -4 -10 46.1752 6.68914 7 16 -4 10 46.6694 6.64879 10 16 -4 10 38.0736 7.51018 3 -16 4 -10 30.0566 4.78886 6 16 -4 10 36.6080 5.20383 8 16 4 10 34.2369 4.97098 8 -17 4 -10 4.19543 6.24858 7 -17 -4 -10-5.92040 6.02903 7 17 -4 10-3.12698 6.68847 3 -17 4 -10 2.34312 4.00394 6 17 -4 10 0.81375 4.64486 8 17 4 10 4.39601 4.48269 8 -18 -4 -10 12.1148 6.26603 7 -18 4 -10 20.5363 7.52655 7 18 -4 10 17.1519 7.21020 3 -18 4 -10 2.01751 4.30897 6 18 -4 10 19.3905 5.32030 8 18 4 10 17.9585 4.96455 8 -19 4 -10 156.828 11.7163 7 19 -4 10 138.818 12.2033 3 19 -4 10 140.960 9.53604 8 19 4 10 136.699 9.09886 8 -20 4 -10 125.124 10.8820 7 20 -4 10 111.118 10.7874 3 20 -4 10 97.4459 8.43292 8 20 4 10 89.1861 8.01836 8 21 -4 10 35.2686 8.79798 3 21 4 10 31.2559 6.14792 8 22 -4 10 13.0807 7.59342 3 -28 -5 10 5.61643 7.10892 2 28 -5 -10 0.66517 6.88156 8 28 5 -10-1.66575 6.22992 8 -27 -5 10 2.46474 6.64953 2 -27 5 10-0.62620 7.28413 1 27 -5 -10-7.86504 6.45669 8 27 5 -10 8.12037 6.41233 8 -26 -5 10-0.60783 7.10026 2 -26 5 10 4.32571 7.42107 1 -26 -5 10 13.1831 8.90971 1 26 -5 -10-1.93667 6.67954 8 26 5 -10 6.29579 5.99033 8 -25 -5 10 9.60337 6.61195 2 -25 5 10 9.77555 7.14771 1 -25 -5 10 18.8452 8.05253 1 25 -5 -10 15.2498 6.62011 8 25 5 -10 8.14420 5.64975 8 -24 -5 10-5.91435 6.35308 2 -24 5 10 9.09742 7.01241 1 -24 -5 10 15.6073 7.64788 1 24 -5 -10 0.61463 5.98639 8 24 5 -10 3.44393 5.48469 8 -23 5 10 20.3355 7.25294 1 -23 -5 10 25.5272 7.58225 1 23 -5 -10 33.9922 6.79157 8 23 5 -10 32.8028 5.89419 8 22 5 -10 20.7823 7.39126 6 -22 5 10 1.78242 6.58750 1 -22 5 10 14.9658 5.44726 2 22 -5 -10 9.14130 5.26423 8 -22 -5 10 7.24583 6.81422 1 22 5 -10 9.60229 4.95953 8 21 5 -10 8.03597 6.95307 6 -21 5 10 9.95962 6.38472 1 -21 5 10 6.53027 5.23060 2 21 -5 -10 3.50972 5.28336 8 21 5 -10 4.53181 6.93863 5 21 5 -10 4.39562 4.70153 8 -21 -5 10 0.57320 6.11419 1 -20 -5 10 3.27004 5.78449 1 20 5 -10 0.58738 6.53370 6 -20 5 10-1.73898 6.21231 1 -20 5 10 9.57011 4.97926 2 20 -5 -10 12.5421 5.36107 8 20 5 -10 2.55697 6.11656 5 20 5 -10 0.84440 4.58024 8 -19 -5 10 2.07936 5.69029 1 19 5 -10 6.15113 6.13507 6 -19 5 10 2.21992 5.81625 1 -19 5 10 3.96531 4.67000 2 19 -5 -10-0.86061 4.65571 8 19 5 -10-5.05055 6.64940 5 19 5 -10 9.29927 4.62645 8 -18 -5 10 7.96600 5.33675 1 18 5 -10 7.46097 5.67063 6 -18 5 10 4.62424 5.79238 1 -18 5 10 2.62625 3.80357 2 18 -5 -10 2.38406 4.37185 8 18 5 -10 5.80775 4.17148 8 17 5 -10 0.19221 2.79874 7 -17 -5 10 4.76705 5.25401 1 17 5 -10-2.03214 5.44371 6 -17 5 10 0.95082 4.89341 1 -17 5 10 3.90120 3.61245 2 17 -5 -10 3.65447 4.01890 8 17 5 -10 5.16773 4.07789 8 16 5 -10 10.1390 2.89984 7 -16 -5 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3.31827 8 10 5 -10 14.7516 2.98235 7 10 5 -10 17.6990 4.67739 5 -10 5 10 14.3937 3.56159 1 10 -5 -10 15.6333 2.17028 4 10 5 -10 15.0178 3.28840 4 -10 -5 10 15.5797 4.28678 1 -10 5 10 15.3520 2.06661 9 10 -5 -10 15.8896 2.85377 8 9 5 -10 11.5563 2.88937 7 9 5 -10 6.46992 4.17249 5 -9 5 10 6.08372 3.17086 1 9 -5 -10 9.25198 1.72579 4 9 5 -10 5.20474 2.91976 4 -9 -5 10 1.44480 4.06206 1 9 -5 -10 8.91330 2.48745 8 8 5 -10 0.90791 2.58510 7 -8 -5 10 11.6535 3.99145 1 8 5 -10 11.8917 3.99639 5 8 -5 -10 4.44947 1.33707 4 -8 5 10 0.94950 3.09135 1 8 5 -10-0.73308 3.87315 6 8 -5 -10 7.57630 2.23388 8 7 5 -10 20.4323 3.06156 7 7 5 -10 16.7580 4.25283 5 -7 5 10 14.4943 3.06829 1 7 5 -10 19.2982 4.06616 6 -7 -5 10 9.66979 3.79505 1 7 5 -10 14.8949 2.00026 8 7 -5 -10 17.0286 2.36344 8 6 5 -10 1.66171 1.95472 7 6 5 -10-0.37099 3.57136 5 -6 5 10-0.33350 3.71809 5 -6 -5 10 3.39658 3.53325 1 -6 5 10 4.12898 2.43739 3 6 5 -10-0.69826 3.50867 6 -6 5 10 1.67283 2.68512 1 6 -5 -10 3.66345 1.88441 8 6 5 -10 3.76956 1.44845 8 5 5 -10 99.2673 6.66876 5 -5 5 10 104.045 6.43086 5 -5 -5 10 108.382 6.62984 1 -5 5 10 99.0975 5.40324 1 -5 5 10 99.6119 5.56682 3 5 5 -10 99.1286 6.58302 6 -5 5 10 92.0449 5.91562 6 5 -5 -10 98.2905 4.66475 8 5 5 -10 91.5305 3.96335 8 -4 5 10 41.8231 4.39827 5 4 5 -10 47.5100 4.72800 5 -4 -5 10 39.9350 5.00100 10 -4 5 10 41.9599 3.88969 3 -4 -5 10 47.4214 4.86556 1 4 5 -10 35.8885 4.54664 6 -4 5 10 37.6084 3.90524 6 -4 5 10 42.9502 3.61097 1 -4 5 10 42.0899 2.66734 8 -3 5 10 5.30518 1.92984 7 -3 5 10-1.25819 3.28828 5 3 5 -10 6.42054 3.39407 5 -3 -5 10 9.79028 2.79940 4 -3 -5 10-0.38655 3.77953 10 -3 5 10 6.42009 2.42720 1 3 5 -10 2.31389 3.32573 6 3 -5 -10 8.44260 3.70843 6 -3 5 10 3.81552 2.82807 3 -3 5 10 5.03738 2.96379 6 -3 5 10 5.94329 1.48749 8 -2 5 10 6.00079 2.12930 7 -2 5 10 4.05283 2.94072 5 2 5 -10-0.61148 3.21445 5 -2 -5 10 5.85478 2.75505 4 -2 -5 10-0.38337 3.73551 10 2 -5 -10 4.36175 3.50034 6 2 5 -10-0.65021 3.19616 6 -2 5 10 4.15185 2.90331 6 -2 5 10 5.14155 3.12462 3 -2 5 10 3.92881 2.33756 1 -2 5 10 4.04985 1.36349 8 1 5 -10 63.6122 4.95262 5 -1 5 10 57.9641 4.20813 5 -1 5 10 61.4520 3.96591 7 1 5 -10 59.3826 4.88082 7 -1 -5 10 52.1825 4.29296 4 -1 -5 10 58.8159 5.65810 10 1 -5 -10 50.4021 5.03506 6 -1 5 10 58.7561 3.99035 1 -1 5 10 60.5322 4.90220 3 -1 5 10 69.4092 4.45630 6 1 5 -10 53.3198 4.96361 6 -1 5 10 59.2276 2.88642 8 0 5 10 41.5045 3.60570 7 0 5 -10 42.8015 4.13572 5 0 5 10 38.8098 3.36342 1 0 5 10 41.1277 3.43185 5 0 5 -10 36.8563 4.32566 7 0 -5 10 42.6337 3.91510 4 0 -5 10 38.4138 4.97896 10 0 -5 -10 34.0492 4.20721 6 0 5 -10 39.0051 4.42432 6 0 5 10 45.1129 3.67052 6 0 5 10 38.1929 4.32784 3 0 5 10 41.1953 2.31815 8 1 5 10 5.32159 2.85761 7 -1 5 -10 6.03007 2.93557 5 -1 5 -10 9.07686 3.28085 7 1 -5 10 3.20893 2.83708 4 1 5 10 5.44823 2.94814 10 -1 -5 -10 3.52102 2.97886 6 1 -5 10 10.6491 4.00047 10 1 -5 10 2.79788 3.80550 3 -1 5 -10 4.71925 3.40121 6 1 5 10 4.59190 2.48280 6 1 5 10 6.84650 3.55739 3 1 5 10 6.75283 1.46444 8 -2 5 -10 90.2185 5.57168 5 2 5 10 100.740 5.82453 7 -2 5 -10 86.3602 6.15765 7 2 -5 10 88.9082 5.50564 4 2 5 10 93.4425 5.51220 10 -2 -5 -10 82.4484 5.51855 6 2 -5 10 96.6783 6.75648 10 2 -5 10 94.0424 6.77242 3 -2 5 -10 84.5062 5.96055 6 2 5 10 91.3582 4.88135 6 2 5 10 83.0362 3.97522 8 3 5 10 149.370 7.75269 7 -3 5 -10 128.878 8.05527 7 3 5 10 136.035 7.00538 10 3 -5 10 126.697 7.25504 4 3 -5 10 147.221 8.49612 10 3 -5 10 153.256 8.80891 3 -3 5 -10 144.840 7.72972 6 3 5 10 138.396 5.85687 8 3 5 10 142.313 6.44301 6 4 5 10 7.72733 3.63515 7 -4 5 -10 12.9209 3.95791 7 -4 -5 -10 13.9305 3.43050 7 4 5 10 9.23218 2.99952 10 4 -5 10 6.58731 4.06584 10 4 -5 10 6.07630 4.22927 3 -4 5 -10 16.4738 3.62590 6 4 5 10 11.9937 1.95827 8 4 5 10 6.99594 2.17962 6 5 5 10 40.0034 4.97936 7 -5 -5 -10 40.5030 4.62614 7 -5 5 -10 33.2938 4.81545 7 5 5 10 38.6715 3.79217 10 5 -5 10 37.7344 5.31307 3 5 -5 10 34.3666 4.95980 10 5 -5 10 33.1373 2.44622 8 -5 5 -10 37.8419 4.46406 6 5 5 10 36.7575 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57.9503 4.61332 6 5 6 -10 50.0934 5.09204 6 -5 -6 10 47.8628 5.13241 1 5 -6 -10 63.7966 3.60209 8 5 6 -10 48.1329 2.71712 8 -5 6 10 57.9270 3.29795 8 -5 -6 10 55.0166 5.58416 10 -4 6 10 298.736 11.2396 7 4 6 -10 302.637 13.4888 5 -4 -6 10 304.336 13.9630 10 -4 -6 10 304.468 13.5311 1 -4 6 10 302.992 12.1052 1 -4 6 10 316.428 12.6451 3 4 6 -10 296.776 13.5528 6 -4 6 10 302.207 12.6420 6 4 6 -10 275.947 10.9731 8 -4 6 10 312.363 11.5280 8 -4 6 10 325.612 13.4747 5 -3 6 10 492.200 17.6309 7 3 6 -10 487.577 19.1963 7 3 6 -10 495.067 19.4661 5 -3 -6 10 513.675 18.9712 4 -3 -6 10 533.324 20.4546 10 -3 6 10 503.122 18.8698 3 3 6 -10 508.938 19.7193 6 -3 6 10 495.808 18.6114 6 -3 6 10 489.786 18.1234 1 3 6 -10 411.274 16.9174 8 -3 6 10 514.891 17.5306 8 -3 6 10 516.684 19.2949 5 2 6 -10 198.400 9.55358 7 -2 6 10 183.927 8.19433 7 2 6 -10 191.081 9.52373 5 -2 -6 10 213.189 9.30188 4 -2 -6 10 189.661 10.2870 10 2 6 -10 208.705 9.96943 6 -2 6 10 197.693 8.85026 6 -2 6 10 198.502 9.28684 3 -2 6 10 194.862 8.37028 1 -2 6 10 187.058 7.69396 8 -2 6 10 199.464 9.31051 5 -1 6 10 7.75965 2.95662 5 1 6 -10 7.80283 3.30635 7 -1 6 10 5.20993 2.38955 7 -1 -6 10 13.7460 3.02912 4 -1 -6 10 4.36896 3.98844 10 1 6 -10 4.37870 3.41318 6 -1 6 10 9.46394 2.66593 6 -1 6 10 7.94729 3.23083 3 -1 6 10 9.77368 2.39245 1 -1 6 10 6.86643 1.66422 8 0 6 10 11.8162 2.79078 5 0 6 -10 14.3585 3.58785 7 0 6 10 15.9055 2.97020 7 0 -6 10 14.7801 3.32436 4 0 -6 10 14.6438 4.37853 10 0 6 10 18.2947 2.59678 1 0 6 -10 13.0361 3.58813 6 0 6 10 13.8658 2.72315 6 0 6 10 15.8194 3.74713 3 0 6 10 11.1068 1.80263 8 1 6 10 108.703 5.43670 5 -1 6 -10 97.9443 6.71905 7 1 6 10 99.6771 6.04030 7 1 6 10 100.726 5.26298 1 1 -6 10 97.7187 6.14560 4 1 6 10 104.113 5.88880 10 1 -6 10 113.153 7.46889 10 -1 6 -10 105.089 6.78287 6 1 6 10 104.747 5.44630 6 1 6 10 112.064 4.77569 8 2 6 10 142.496 6.50896 5 -2 6 -10 150.218 8.37513 7 2 6 10 150.103 7.75008 7 2 -6 10 159.858 7.79271 4 2 6 10 137.493 7.08165 10 2 -6 10 141.024 8.71899 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8 -10 94.9122 9.33256 6 21 -8 -10 69.8366 7.77023 8 -21 8 10 86.7304 8.30374 1 21 8 -10 87.8067 9.97325 5 -20 -8 10 11.2106 6.46659 1 -20 8 10 1.48273 5.50851 1 20 8 -10-7.90989 6.58560 6 20 -8 -10-0.47978 5.16520 8 20 8 -10-1.39144 6.95089 5 -19 -8 10 2.15327 5.90546 1 -19 8 10-4.36874 5.89576 1 19 8 -10-1.08419 5.78014 6 19 -8 -10 5.40279 4.93921 8 19 8 -10 5.34621 6.75066 5 18 8 -10 102.671 9.51034 5 -18 -8 10 80.3275 8.26070 1 -18 8 10 84.2187 8.07760 1 18 8 -10 81.3706 8.35235 6 18 -8 -10 89.2498 7.23244 8 -17 -8 10 152.136 10.1728 1 -17 8 10 151.816 10.0119 1 17 8 -10 150.240 10.3896 6 17 -8 -10 160.056 9.26426 8 -16 -8 10 122.483 9.12857 1 -16 8 10 124.391 8.87056 1 16 8 -10 112.371 8.93066 6 16 -8 -10 126.594 8.06612 8 -15 -8 10 123.523 8.97620 1 -15 8 10 134.673 8.81970 1 15 8 -10 133.731 9.18557 6 15 -8 -10 121.129 7.81195 8 14 8 -10 68.0120 7.14092 6 -14 8 10 51.8123 6.40248 1 14 -8 -10 77.6368 5.76716 8 -14 -8 10 70.1421 6.92552 1 13 8 -10 53.8886 6.28033 5 13 8 -10 50.5585 6.32858 6 -13 8 10 49.0472 5.77716 1 13 -8 -10 52.9631 4.89156 8 -13 -8 10 52.2677 6.25010 1 12 8 -10 168.308 10.3364 5 -12 8 10 177.948 9.73255 1 12 8 -10 177.582 10.3411 6 -12 -8 10 171.782 10.2834 1 12 -8 -10 189.220 8.98137 8 11 8 -10 367.203 16.7222 5 -11 8 10 365.420 15.7148 1 11 8 -10 360.382 16.4719 6 11 -8 -10 357.946 15.0894 8 -11 -8 10 351.111 16.3426 1 -10 -8 10 88.2897 6.94741 1 10 8 -10 97.9609 7.55702 5 -10 8 10 88.9247 6.26998 1 10 -8 -10 89.5891 5.66934 8 -10 8 10 93.6696 5.61187 8 -9 -8 10 1.98176 4.00933 1 9 -8 -10 5.54187 1.27768 4 9 8 -10 11.3935 2.38186 8 9 -8 -10 10.2938 2.96927 8 -9 8 10 5.92205 3.43655 1 -9 8 10 5.55153 2.92498 8 8 8 -10 0.40470 4.09979 5 -8 -8 10 3.12092 3.91996 1 8 8 -10 2.66246 2.35833 8 8 -8 -10 1.36432 2.71036 8 -8 8 10 2.07925 3.13569 1 -8 8 10 2.83417 2.67816 8 7 8 -10 70.9363 5.62362 7 7 8 -10 69.9447 6.32618 5 -7 -8 10 71.4505 6.15560 1 -7 8 10 84.6183 5.11245 1 7 -8 -10 80.0042 4.98930 8 7 8 -10 79.5895 4.36112 8 -7 8 10 81.9769 4.67600 8 6 8 -10 91.6660 6.05337 7 -6 8 10 78.1231 4.71871 3 6 -8 -10 84.2695 4.94442 8 6 8 -10 81.3285 4.32799 8 -6 8 10 84.8248 4.99028 1 -6 -8 10 72.2959 6.23656 1 -6 8 10 86.0780 4.69004 8 -5 8 10 25.3856 1.85223 7 5 8 -10 19.7407 3.79874 7 -5 8 10 20.6286 2.94000 1 -5 -8 10 33.7119 4.89581 1 -5 -8 10 28.0671 5.28921 10 -5 8 10 26.9238 3.15911 3 5 8 -10 19.9717 4.35228 6 5 -8 -10 27.9813 3.07149 8 5 8 -10 25.0927 2.43944 8 -5 8 10 27.3947 2.83315 8 4 8 -10 122.408 7.17724 7 -4 8 10 109.314 5.12836 7 -4 -8 10 121.791 6.97556 4 -4 -8 10 115.040 7.91950 10 -4 8 10 120.369 6.54988 6 -4 8 10 117.754 6.25733 3 4 8 -10 116.781 7.66285 6 4 8 -10 116.703 5.18879 8 -4 8 10 121.250 5.59058 8 -4 8 10 98.9233 7.40973 5 -4 8 10 115.253 5.68438 1 3 8 -10 165.513 9.09746 7 -3 8 10 174.938 7.53625 1 -3 8 10 180.038 7.45137 7 -3 -8 10 174.372 8.91394 4 -3 -8 10 176.548 10.1068 10 -3 8 10 168.500 8.21964 6 3 8 -10 176.719 9.60165 6 -3 8 10 172.550 8.29847 3 3 8 -10 169.730 7.05576 8 -3 8 10 177.917 7.51295 8 -3 8 10 174.705 9.52165 5 2 8 -10 207.462 10.6019 7 -2 8 10 221.143 9.25498 7 -2 -8 10 209.258 10.4079 4 -2 8 10 210.040 8.86145 1 -2 -8 10 208.703 11.2539 10 -2 8 10 220.984 9.63577 6 2 8 -10 237.307 11.2511 6 -2 8 10 217.899 10.0157 3 2 8 -10 215.682 8.51658 8 -2 8 10 227.808 8.97910 8 -2 8 10 214.335 10.7622 5 1 8 -10 271.014 13.0158 7 -1 8 10 300.198 11.9081 7 -1 -8 10 269.038 12.6640 4 -1 8 10 292.403 11.1370 1 -1 -8 10 272.037 13.7010 10 -1 8 10 281.925 11.7566 6 1 8 -10 270.567 13.2095 6 -1 8 10 290.295 11.2897 8 1 8 -10 286.462 10.8236 8 -1 8 10 285.943 12.7281 5 0 8 -10 183.018 9.55730 7 0 8 10 184.226 8.56351 7 0 -8 10 180.187 9.22785 4 0 -8 10 186.627 10.3570 10 0 8 10 176.787 8.05972 6 0 8 10 171.614 7.42034 1 0 8 -10 197.655 9.90133 6 0 8 10 191.124 7.73915 8 0 8 -10 179.345 7.24250 8 0 8 10 185.721 8.93758 5 1 8 10 0.22683 2.98067 5 -1 8 -10-1.89084 3.72687 7 1 8 10 3.15815 3.26349 7 1 8 10 4.60197 2.59144 10 1 -8 10 8.55728 3.47830 4 1 -8 10 6.04982 4.33061 10 1 8 10 2.46654 1.88465 1 1 8 10 3.09253 2.38055 6 -1 8 -10-1.11615 3.90979 6 1 8 10 3.89367 2.10151 8 -1 8 -10 3.11448 1.71830 8 2 8 10 5.42629 2.87746 5 -2 8 -10 6.28176 3.72837 7 2 8 10 5.60269 3.61558 7 2 8 10 8.97519 2.14434 1 2 8 10 6.37757 2.56699 10 2 -8 10 6.44518 3.37615 4 2 -8 10 13.0492 4.64349 10 2 8 10 8.41815 2.33402 6 -2 8 -10 3.36922 3.87974 6 2 8 10 5.39765 2.17726 8 -2 8 -10 5.17325 1.83060 8 3 8 10 190.463 7.58798 1 -3 8 -10 183.765 9.99920 7 3 8 10 165.091 9.38777 7 3 -8 10 183.931 9.41411 4 3 8 10 173.106 8.00401 10 3 -8 10 190.761 10.4714 10 -3 8 -10 189.077 9.86572 6 3 8 10 182.226 7.67112 6 3 8 10 194.045 7.96167 8 3 8 10 169.910 7.94899 5 -4 8 -10 352.159 15.7227 7 4 8 10 331.169 15.2510 7 4 8 10 332.190 13.5003 10 4 -8 10 358.114 15.0933 4 4 -8 10 341.148 15.8451 10 -4 8 -10 337.647 15.3589 6 4 8 10 350.811 13.5507 8 4 8 10 337.541 12.9880 6 4 8 10 345.397 13.2354 5 5 8 10 99.8566 4.51981 5 -5 8 -10 113.174 7.68384 7 5 8 10 116.738 5.10598 1 5 8 10 86.6449 3.73327 4 5 8 10 104.273 5.19425 10 5 -8 10 106.467 7.74242 10 5 -8 10 97.8834 7.68583 3 5 -8 10 104.036 5.18809 8 -5 8 -10 120.034 7.38774 6 5 8 10 105.662 5.41537 8 5 8 10 94.3685 4.26549 6 6 8 10 48.8317 2.65427 4 -6 8 -10 46.0872 5.68981 7 6 8 10 39.6112 3.44521 1 6 8 10 40.3560 3.48213 10 6 -8 10 36.4652 5.77463 10 6 -8 10 45.1124 3.53421 8 6 8 10 56.0403 3.98282 8 -6 8 -10 51.4968 5.43405 6 7 8 10 41.2507 2.86756 4 -7 8 -10 42.8255 5.92496 7 7 8 10 37.7301 3.62818 1 7 8 10 38.8246 3.39986 10 7 -8 10 43.2347 6.04972 10 7 -8 10 40.3327 3.53881 8 7 8 10 45.4169 3.90715 8 -7 8 -10 46.6681 5.30721 6 -8 8 -10 25.8395 5.46945 7 8 -8 10 20.3228 5.44933 10 8 8 10 13.4640 2.58309 10 8 8 10 11.9049 3.17295 8 8 -8 10 19.6294 3.10990 8 -8 8 -10 20.9563 4.56058 6 -9 8 -10 117.831 8.92406 7 9 -8 10 138.500 9.10769 10 9 8 10 113.236 5.82275 10 -9 8 -10 137.940 8.34198 6 9 -8 10 131.303 6.59783 8 -10 8 -10 215.699 11.9819 7 10 -8 10 185.206 11.1343 10 10 -8 10 172.979 11.3626 3 -10 8 -10 218.259 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4 6 -12 1160.90 43.4439 7 -4 -6 12 1130.15 44.7628 10 -4 6 12 1194.85 43.3135 3 -4 6 12 1132.34 42.5557 1 4 6 -12 1170.76 44.2568 6 -4 -6 12 1146.58 44.2368 1 4 6 -12 1204.87 44.5074 5 -3 6 12 521.630 19.5718 7 3 6 -12 531.774 21.3760 7 -3 -6 12 475.074 22.3555 10 -3 6 12 525.259 21.2107 3 3 6 -12 514.563 21.9542 6 -3 6 12 526.684 20.3136 1 3 6 -12 578.878 22.3115 5 -2 6 12 39.3805 3.42905 7 2 6 -12 34.4171 5.17704 5 2 6 -12 45.6511 4.97754 7 -2 -6 12 30.4836 4.22304 4 -2 -6 12 28.3727 5.73616 10 2 6 -12 38.6470 5.38803 6 -2 6 12 38.0921 4.74616 3 -2 6 12 44.3199 3.96699 1 -1 6 12 0.76093 2.77133 7 1 6 -12 4.12185 3.88843 5 1 6 -12 2.50337 3.86113 7 -1 -6 12 3.92270 3.41790 4 -1 6 12 7.01432 3.78849 10 -1 -6 12 4.69775 4.91158 10 1 6 -12-0.78071 4.35227 6 -1 6 12 7.01408 4.01383 3 -1 6 12 3.23535 3.26287 6 -1 6 12 3.80061 2.88322 1 0 6 -12 205.045 10.3883 5 0 6 12 201.702 9.36016 7 0 6 -12 198.380 10.5857 7 0 -6 12 204.006 9.87801 4 0 6 12 209.187 10.0916 10 0 6 12 202.158 9.20158 1 0 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8 16 13 -12 92.0006 9.58671 5 -16 -13 12 79.6022 9.20306 10 16 13 -12 61.5198 8.75254 6 16 -13 -12 75.3324 7.11853 8 15 13 -12 19.8338 7.32477 5 -15 -13 12 44.9780 8.06817 10 15 13 -12 28.0111 7.03643 6 15 -13 -12 51.4157 6.27400 8 14 13 -12 6.18466 6.84758 5 -14 -13 12 1.86515 6.12564 10 14 13 -12 1.12894 6.06337 6 14 -13 -12 3.61903 4.65958 8 13 13 -12 37.6978 7.10635 5 -13 -13 12 31.1951 7.01193 10 13 13 -12 34.4501 6.95671 6 13 -13 -12 40.8951 5.51578 8 12 13 -12-1.73643 6.11129 5 -12 -13 12 1.81172 6.23186 10 12 13 -12 10.9843 6.30994 6 12 -13 -12 0.37565 4.22452 8 11 13 -12 53.8578 7.50770 5 -11 -13 12 56.0220 7.52145 10 11 13 -12 66.9884 7.93092 6 -11 -13 12 55.3990 7.74985 1 11 -13 -12 59.4283 5.77020 8 10 13 -12 58.5025 6.57323 7 10 13 -12 53.4555 7.28186 5 -10 -13 12 48.3712 7.45280 10 10 13 -12 58.7989 7.27442 6 10 -13 -12 66.1043 5.74352 8 -10 -13 12 51.7158 7.10487 1 9 13 -12-0.46304 4.90189 7 9 13 -12 2.11629 5.31627 5 -9 -13 12 4.66687 5.80603 1 -9 -13 12 0.58779 5.79135 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37.4768 6.68800 6 -1 13 -12 22.6036 5.90259 7 1 -13 12-1.85332 4.94580 4 1 -13 12 15.3905 6.45282 10 -1 13 -12-1.56246 5.66537 6 -2 13 -12 69.3725 7.34772 7 2 -13 12 56.3481 6.77040 4 2 -13 12 63.1470 8.04856 10 -2 13 -12 61.4881 7.25904 6 -3 13 -12 102.529 8.73685 7 3 -13 12 106.045 8.18160 4 3 -13 12 103.324 9.51234 10 -3 13 -12 94.0998 8.52151 6 -4 13 -12 20.9011 6.36284 7 4 -13 12 29.6116 6.16112 4 4 -13 12 23.6797 6.90384 10 -4 13 -12 30.3154 6.40338 6 -5 13 -12 15.0528 6.33339 7 5 -13 12 11.8497 5.31667 4 5 -13 12 15.9614 7.01871 10 -5 13 -12 3.75190 5.58695 6 -6 13 -12 9.55113 6.44938 7 6 -13 12 10.0234 5.60678 4 6 -13 12 8.67563 6.63059 10 -6 13 -12 7.06842 6.01367 6 -7 13 -12 49.5635 7.54049 7 7 -13 12 69.4425 7.15609 4 7 -13 12 45.0007 7.95530 10 -7 13 -12 47.3742 7.20845 6 -8 13 -12 45.8455 7.64882 7 8 -13 12 33.3771 6.49689 4 8 -13 12 30.3267 7.41526 10 -8 13 -12 37.8570 6.73006 6 -9 13 -12 1.29505 6.59726 7 9 -13 12 6.41538 5.88182 4 9 -13 12 2.54763 6.94143 10 -9 13 -12 13.0039 6.48504 6 -10 13 -12 12.6504 7.12659 7 10 -13 12 19.2809 7.33125 10 -10 13 -12 3.45779 6.30435 6 -11 13 -12 2.07082 7.37796 7 11 -13 12-0.64879 6.96818 10 -11 13 -12-5.29412 6.62910 6 -12 13 -12 63.4120 8.91785 7 12 -13 12 46.4223 8.60076 10 -12 13 -12 57.5218 8.22862 6 -13 13 -12 81.2020 10.1516 7 13 -13 12 63.5392 9.36346 10 -13 13 -12 67.9872 8.80998 6 -14 13 -12 1.52645 7.77281 7 14 -13 12 2.00585 7.40257 10 -14 13 -12 4.35959 6.47716 6 -15 13 -12 22.9966 8.47810 7 15 -13 12 25.7774 8.03345 10 -15 13 -12 24.7247 7.05508 6 -16 13 -12 8.36600 6.78367 6 -17 13 -12-5.21522 7.00377 6 23 -14 -12 8.38721 6.56329 8 22 -14 -12-4.02387 6.43686 8 21 -14 -12 18.7237 6.26728 8 20 14 -12 44.6976 8.72360 6 20 -14 -12 30.6341 6.96203 8 -19 -14 12 62.4465 9.32231 10 19 14 -12 51.3091 8.71036 6 19 -14 -12 33.4771 6.77637 8 -18 -14 12 15.7182 7.56544 10 18 14 -12 21.2523 7.35056 6 18 -14 -12 9.78566 5.65563 8 17 14 -12 1.37921 7.85928 5 -17 -14 12 6.67662 7.05309 10 17 14 -12 13.7357 6.74894 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130.182 10.2274 6 -2 14 -12 58.1144 7.33217 7 2 -14 12 61.1746 6.88960 4 2 -14 12 52.1460 8.10997 10 -2 14 -12 67.1424 7.54707 6 -3 14 -12 3.42938 5.56979 7 3 -14 12 4.50458 5.35362 4 3 -14 12 8.68739 6.28866 10 -3 14 -12 8.26656 5.89402 6 -4 14 -12 5.83448 5.79731 7 4 -14 12 2.03597 5.38776 4 4 -14 12-8.16589 7.03257 10 -4 14 -12 9.43720 5.91948 6 -5 14 -12 32.3709 6.88077 7 5 -14 12 27.4783 6.18294 4 5 -14 12 45.6805 7.98984 10 -5 14 -12 20.7367 6.52448 6 -6 14 -12 141.763 11.0370 7 6 -14 12 185.752 11.0235 4 6 -14 12 139.346 11.2994 10 -6 14 -12 172.140 11.2477 6 -7 14 -12 124.554 10.1690 7 7 -14 12 107.441 9.27991 4 7 -14 12 130.352 10.9602 10 -7 14 -12 124.592 10.0137 6 -8 14 -12 5.15487 6.42223 7 8 -14 12 3.26835 5.95050 4 8 -14 12 5.21216 6.75996 10 -8 14 -12 6.41024 6.20068 6 -9 14 -12-4.62635 6.58502 7 9 -14 12 4.45549 6.02477 4 9 -14 12 1.96938 7.01665 10 -9 14 -12 4.73982 6.34817 6 -10 14 -12 18.4431 7.17659 7 10 -14 12 20.5496 6.82690 4 10 -14 12 11.9189 7.43220 10 -10 14 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6 -14 85.4571 7.55801 6 -3 -6 14 86.8255 7.60713 1 -3 6 14 93.3109 5.83897 1 3 6 -14 84.4067 7.75435 5 2 6 -14 14.4144 5.37282 5 2 6 -14 17.8661 4.82882 7 -2 6 14 25.1435 3.91352 1 -2 6 14 21.2803 4.97725 10 -2 -6 14 26.7680 6.17005 10 -2 6 14 24.0537 5.07616 3 2 6 -14 13.0678 5.21435 6 -2 -6 14 16.5517 5.59756 1 1 6 -14 23.3038 5.37256 5 -1 -6 14 17.9872 4.10707 4 1 6 -14 18.7861 5.08035 7 -1 6 14 18.6545 4.62319 10 -1 -6 14 20.6847 6.07200 10 -1 6 14 11.7021 3.62900 1 1 6 -14 18.3129 5.12640 6 -1 6 14 21.1760 5.33854 3 0 6 -14 36.1037 5.59708 5 0 6 -14 34.2514 5.71344 7 0 -6 14 44.8018 4.71730 4 0 6 14 37.0872 5.10067 10 0 -6 14 26.0230 6.47245 10 0 6 -14 28.6563 5.64981 6 0 6 14 41.9268 5.84906 3 0 6 14 36.6114 4.29331 1 1 -6 14 94.0229 6.23236 4 -1 6 -14 82.5122 7.32833 7 1 6 14 75.0956 5.69481 1 1 6 14 81.0217 6.48807 10 1 -6 14 88.4540 8.51396 10 -1 6 -14 106.922 7.83710 6 1 6 14 83.8518 7.38701 3 -1 6 -14 81.5926 6.94626 5 2 -6 14 83.1986 6.07006 4 -2 6 -14 74.9731 7.45369 7 2 6 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7 -14 40.7197 6.44569 6 -13 7 -14 39.0195 9.07247 7 13 -7 14 21.2011 7.09222 10 -14 7 -14 8.95137 8.50552 7 14 -7 14-4.60118 7.06375 10 -15 7 -14 4.08897 8.17932 7 15 -7 14 16.8713 7.66178 10 16 -7 14 14.0657 7.57532 10 -22 8 14 42.2805 8.30099 1 -21 8 14 29.5410 7.60452 1 -20 -8 14-0.62280 7.27424 1 20 8 -14 16.2121 8.54489 6 -20 8 14 0.54117 6.69510 1 20 8 -14-10.0106 8.10964 5 -19 -8 14 13.3418 7.35271 1 19 8 -14-4.08465 7.53752 6 -19 8 14 0.53930 6.57576 1 19 8 -14 6.12483 7.83899 5 -18 -8 14 60.8412 8.34982 1 18 8 -14 65.8913 9.41462 6 -18 8 14 55.3502 8.04720 1 18 8 -14 49.4605 9.77944 5 17 8 -14 117.008 10.4545 6 -17 -8 14 92.9096 9.44494 1 -17 8 14 89.8593 9.01922 1 17 8 -14 78.6493 10.7057 5 -16 8 14 47.7194 7.33967 1 -16 -8 14 59.6685 8.18645 1 16 8 -14 51.7961 9.45210 5 -15 8 14 42.6713 6.82894 1 -15 -8 14 50.5767 7.72034 1 15 8 -14 46.5430 8.83093 5 -14 8 14 57.4047 6.73112 1 -14 -8 14 52.8582 7.61483 1 14 8 -14 42.2734 8.13703 5 -13 -8 14 48.1809 7.31847 1 13 8 -14 36.8526 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10.2201 5 6 8 -14 91.3117 8.23480 5 6 8 -14 73.8436 6.46112 7 -6 -8 14 64.9280 8.40687 10 6 8 -14 78.5639 7.77393 6 -6 -8 14 97.1726 8.13425 1 -6 8 14 76.4475 5.60705 1 5 8 -14 30.0875 6.37844 5 5 8 -14 31.5985 5.08921 7 -5 8 14 28.6139 4.08691 1 -5 -8 14 32.3108 6.93069 10 -5 8 14 29.7189 4.66555 3 -5 -8 14 23.7033 6.24575 1 5 8 -14 41.6799 6.42536 6 4 8 -14 22.8515 5.95401 5 4 8 -14 29.6171 5.22847 7 -4 -8 14 20.6708 5.89602 1 -4 8 14 30.6806 4.06724 1 -4 -8 14 33.8604 7.30764 10 -4 8 14 28.4003 4.70727 3 4 8 -14 39.8105 6.23085 6 3 8 -14 22.6590 5.77432 5 3 8 -14 18.3320 5.05679 7 -3 -8 14 13.3631 6.40080 10 -3 -8 14 31.9891 6.28801 1 -3 8 14 29.6088 4.87847 3 3 8 -14 28.6163 5.85235 6 2 8 -14 25.7604 5.88863 5 2 8 -14 28.9052 5.40963 7 -2 8 14 29.0616 4.94354 10 -2 -8 14 26.0801 6.74722 10 2 8 -14 27.3570 5.83884 6 -2 8 14 32.6802 5.16839 3 -1 -8 14 95.8649 6.73336 4 1 8 -14 79.3039 7.09317 7 -1 8 14 81.5133 6.36417 10 -1 -8 14 88.5135 8.66773 10 -1 8 14 82.3684 7.03038 3 1 8 -14 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14 11.6602 4.76957 4 5 -8 14 11.4999 6.63573 10 -5 8 -14 25.2593 5.90899 6 5 8 14 10.5734 6.10808 3 -6 8 -14 0.59100 6.22746 7 6 -8 14 4.40156 4.76279 4 6 -8 14 6.35513 6.42803 10 -6 8 -14 7.02267 5.38255 6 6 8 14 12.3572 6.26211 3 -7 8 -14 22.2697 6.78635 7 7 -8 14 29.5329 5.60635 4 7 -8 14 21.4514 6.85971 10 -7 8 -14 23.9527 5.84450 6 7 8 14 14.3247 6.50945 3 -8 8 -14 79.7731 9.19731 7 8 -8 14 97.9375 7.58528 4 8 -8 14 84.2941 8.89417 10 8 -8 14 72.1706 9.28407 3 -8 8 -14 88.9337 8.06879 6 8 8 14 82.9495 9.38541 3 -9 8 -14 176.576 12.6399 7 9 -8 14 184.617 10.3997 4 9 -8 14 151.564 11.4321 10 -9 8 -14 149.262 10.4310 6 9 8 14 167.333 12.5953 3 -10 8 -14 81.1443 9.80952 7 10 -8 14 77.8273 8.72217 10 10 -8 14 89.0119 10.1309 3 -10 8 -14 82.3745 7.75962 6 -11 8 -14 8.98766 7.75277 7 11 -8 14 2.93980 6.83020 10 -11 8 -14 9.54785 5.47906 6 -12 8 -14 12.5482 7.58432 7 12 -8 14 10.6084 6.99654 10 -12 8 -14 15.7654 5.77759 6 -13 8 -14 45.7633 9.22450 7 13 -8 14 38.5907 8.15138 10 -14 8 -14 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7.79215 7 10 -11 14 6.22659 5.88958 4 10 -11 14 1.29631 7.30741 10 -10 11 -14 6.62492 6.37283 6 -11 11 -14-8.17892 8.02440 7 11 -11 14 10.1359 6.46767 4 11 -11 14-1.95050 7.54801 10 -11 11 -14 6.69195 6.44757 6 -12 11 -14 16.2760 8.18774 7 12 -11 14 5.20745 7.60823 10 -12 11 -14 5.61002 6.27312 6 -13 11 -14 32.2766 6.90560 6 17 12 -14 66.4531 10.1018 5 -17 -12 14 74.8135 9.94013 10 17 12 -14 63.1672 9.67485 6 -17 -12 14 82.2299 9.30297 1 16 12 -14 54.6576 9.50647 5 -16 -12 14 46.8910 9.02691 10 16 12 -14 68.2972 8.94913 6 -16 -12 14 56.6479 8.48645 1 15 12 -14 5.78787 7.53476 5 -15 -12 14 14.6501 7.48583 10 15 12 -14 6.88720 7.45688 6 -15 -12 14 18.9916 7.09716 1 -14 -12 14 11.1086 7.10949 1 14 12 -14 11.8614 7.17045 5 -14 -12 14 6.17909 7.25687 10 14 12 -14 10.4687 7.17169 6 13 12 -14 22.7468 5.82395 7 13 12 -14 26.2980 7.93967 5 -13 -12 14 20.2447 7.43674 1 -13 -12 14 32.5280 7.88243 10 12 12 -14 69.5125 7.24853 7 12 12 -14 74.9975 9.16763 5 -12 -12 14 69.3212 8.66114 1 -12 -12 14 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63.7855 9.70330 10 13 8 -16 73.1450 9.20842 6 -13 -8 16 74.5918 8.99881 1 13 8 -16 56.0059 9.79142 5 -12 -8 16 141.856 11.6935 10 12 8 -16 132.031 10.6522 6 -12 -8 16 112.630 10.0639 1 12 8 -16 117.487 11.8713 5 -11 -8 16 53.9759 7.78138 1 -11 -8 16 58.6718 8.83669 10 11 8 -16 44.9387 8.18145 6 11 8 -16 41.1852 8.96861 5 -10 -8 16 5.46546 7.54607 10 -10 -8 16-1.11912 6.83432 1 10 8 -16-2.40906 7.07719 6 10 8 -16-4.38231 7.59525 5 -9 -8 16 2.02949 7.36959 10 9 8 -16-6.49613 6.71292 6 -9 -8 16 1.11094 6.39489 1 9 8 -16 2.17159 7.21199 5 -8 -8 16 143.522 11.0027 1 -8 -8 16 177.059 12.4891 10 8 8 -16 155.887 11.1756 6 8 8 -16 140.039 12.1763 5 -7 -8 16 323.952 16.3547 1 -7 -8 16 317.443 17.2553 10 7 8 -16 308.360 16.1416 6 6 8 -16 95.3749 7.70927 7 -6 -8 16 102.154 10.0830 10 -6 -8 16 84.6356 9.01935 1 6 8 -16 117.964 9.71237 6 5 8 -16 3.79956 5.24344 7 -5 8 16 7.95019 5.95820 10 -5 -8 16 7.90391 7.35851 10 5 8 -16 3.32296 6.10470 6 -5 -8 16 9.32394 6.35505 1 5 8 -16-9.33216 7.10843 5 4 8 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7.94527 6 2 8 16 70.5704 7.91033 3 -3 8 -16 217.833 13.8825 7 3 -8 16 235.946 14.4833 10 -3 8 -16 239.892 13.3713 6 3 8 16 225.173 13.5545 3 -4 8 -16 131.320 10.8807 7 4 -8 16 108.187 10.5181 10 -4 8 -16 114.706 9.66191 6 4 8 16 137.123 10.6691 3 -5 8 -16-2.60379 6.78646 7 5 -8 16 4.43353 6.86736 10 -5 8 -16 0.51427 6.09151 6 5 8 16-3.06923 7.18419 3 -6 8 -16-7.47932 7.59697 7 6 -8 16-8.21738 7.54811 10 -6 8 -16-0.51426 5.93527 6 6 8 16-5.15114 7.44572 3 -7 8 -16 16.3484 7.95649 7 7 -8 16 16.4054 7.85133 10 -7 8 -16 12.7774 5.93099 6 7 8 16 14.8517 7.86960 3 -8 8 -16 112.260 11.2705 7 8 -8 16 129.930 11.1216 10 -8 8 -16 94.5270 9.18759 6 8 8 16 102.090 10.7299 3 -9 8 -16 131.325 11.9973 7 9 -8 16 117.165 11.1606 10 9 8 16 142.301 12.3013 3 -10 8 -16 11.2058 8.37036 7 10 -8 16 4.99250 7.39688 10 15 9 -16 9.32978 8.43634 5 -14 -9 16-1.78116 7.06562 1 14 9 -16 20.1286 7.99310 5 -13 -9 16 0.71708 7.68289 10 13 9 -16 0.64705 7.14696 6 13 9 -16-2.31187 8.15625 5 -13 -9 16 2.92970 6.63181 1 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9.15400 6.92008 6 -5 -2 18 16.0490 6.49240 1 -4 2 18 44.5044 7.71516 10 4 -2 -18 15.9729 7.09159 6 -4 -2 18 28.1678 7.56267 10 4 2 -18 23.2668 7.14498 6 -4 -2 18 27.6352 7.02915 1 -3 -2 18 9.71334 6.36866 1 3 -2 -18 2.59863 6.85967 6 -3 2 18-1.65072 6.89391 10 -3 -2 18-2.47247 7.30779 10 3 2 -18 5.25846 6.26083 6 -2 -2 18-6.80599 5.97221 1 2 -2 -18-0.63491 7.03018 6 -2 2 18-6.47419 6.59093 10 -2 -2 18-4.27923 7.53679 10 2 2 -18-1.14336 6.48585 6 -1 2 18 13.7285 6.75033 10 -1 -2 18 8.43069 7.43052 10 1 2 -18 6.69688 6.04597 6 -1 -2 18 9.75534 6.18395 1 0 -2 18 23.5177 6.76019 1 0 2 18 16.5006 6.70583 10 0 -2 18 18.3865 7.30107 10 0 2 -18 17.4386 6.30869 6 1 2 18 19.6884 6.73589 10 1 -2 18 20.4645 7.72800 10 -1 2 -18 20.2322 6.47418 6 1 -2 18 26.0386 6.96347 1 2 -2 18 20.7562 6.97312 1 2 -2 18 19.5237 7.31607 10 2 2 18 31.6946 7.84294 3 3 -2 18 6.78157 6.91483 10 3 2 18 19.6537 7.77100 3 3 -2 18 10.9280 6.50507 1 4 -2 18 2.79109 7.29498 10 4 -2 18 8.50864 6.43627 1 5 -2 18 28.7673 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-18 2.19679 7.75058 5 7 9 -18 5.78162 6.93695 5 2 9 -18 3.60372 6.82844 6 1 9 -18 3.57751 6.74963 6 0 9 -18 6.51914 6.99578 6 -1 9 -18-4.69718 7.14641 6 -2 9 -18-14.0346 7.71995 6 -3 9 -18 8.13249 7.12684 6 9 10 -18 12.1522 8.82701 5 8 10 -18 13.6059 8.40045 5 7 10 -18 13.4228 8.43489 5 8 11 -18-4.69559 7.66710 5 7 11 -18 10.8227 7.73282 5 8 0 -19 1.46968 7.19775 6 7 0 -19 15.0475 7.46993 6 6 0 -19-0.70278 7.52966 6 5 0 -19-4.11825 7.54812 6 -4 0 19 11.7346 7.64220 10 4 0 -19-1.34399 6.80800 6 -3 0 19-9.71889 7.84218 10 -2 0 19-17.9004 8.32454 10 -1 0 19 5.84858 7.40688 10 0 0 19 1.14991 7.10031 10 8 1 -19-6.41534 7.49151 6 7 -1 -19-1.48152 7.00005 6 7 1 -19-4.19776 7.62218 6 6 -1 -19-7.22547 7.64963 6 6 1 -19-3.41009 7.62056 6 5 -1 -19-12.7505 8.30776 6 -5 1 19-4.28060 7.41382 10 5 1 -19 9.37746 7.41592 6 4 -1 -19-5.54569 6.71254 6 -4 1 19-0.60051 7.55087 10 4 1 -19-5.87171 7.30530 6 -3 1 19-1.76626 7.40163 10 3 1 -19 0.63754 6.79756 6 -2 1 19-8.67222 7.43840 10 -1 1 19-0.56586 7.22531 10 -9 -2 19 4.60093 6.82255 1 -8 -2 19 14.6792 6.62454 1 -7 -2 19 6.53927 6.54379 1 7 2 -19-15.6993 8.55238 6 -6 -2 19 11.5427 6.32197 1 -6 2 19 7.90436 7.54658 10 6 2 -19 14.7025 7.27432 6 -5 2 19-5.95550 7.34131 10 -5 -2 19 4.51056 6.58190 1 5 2 -19 5.23290 6.80224 6 -4 2 19-2.91409 7.18531 10 4 2 -19 10.8914 7.33032 6 -3 2 19-1.14259 7.35638 10 3 2 -19 0.62949 6.67892 6 -7 -3 19 12.0110 7.04483 1 -6 -3 19 2.08560 6.66901 1 -6 3 19-0.59240 7.47367 10 6 3 -19 1.97466 7.06936 6 -5 3 19-0.57862 7.47563 10 5 3 -19-9.01538 7.35124 6 -5 -3 19 10.9143 6.84731 1 -4 3 19-5.64247 7.31583 10 4 3 -19-2.52978 6.81059 6 -4 -3 19-5.71577 6.82576 1 3 3 -19 8.67329 6.81198 6 -3 -3 19-4.15784 6.78167 1 -2 -3 19 4.16653 6.98189 1 2 3 -19 1.82187 6.52304 6 -1 -3 19 5.75010 7.09573 1 -7 4 19 8.81218 7.16856 10 -6 4 19 6.90610 7.61020 10 5 4 -19 14.0398 7.36338 6 4 4 -19-3.75436 7.33922 6 3 4 -19 3.07608 7.25910 6 2 4 -19 0.60382 7.13805 6 1 4 -19 4.15237 6.83071 6 3 5 -19 1.84141 7.29937 6 2 5 -19 10.8929 7.24858 6 1 5 -19 5.34554 6.78295 6 1 6 -19-4.80915 7.46589 6 0 6 -19-2.95485 7.24544 6 0 0 0 0.00 0.00 0 TITL MHT-III-53 in P2(1)/c REM P2(1)/c (#14 in standard setting) CELL 0.71073 21.097616 19.825465 12.614931 90.0000 98.2252 90.0000 ZERR 1.00 0.000427 0.000343 0.000197 0.0000 0.0017 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C N O I Pb UNIT 180.00 12.00 8.00 32.00 8.00 TREF HKLF 4 END ; _shelx_hkl_checksum 18132 _olex2_diffrn_ambient_temperature_device 'Oxford Cryosystems' _olex2_exptl_crystal_mounting_method 'The crystal was mounted on a loop with paratone oil' _olex2_submission_original_sample_id MHT-III-53 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.235 _oxdiff_exptl_absorpt_empirical_full_min 0.860