####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_reu131 _database_code_depnum_ccdc_archive 'CCDC 1845975' _audit_update_record ; 2018-05-29 deposited with the CCDC. 2018-10-28 downloaded from the CCDC. ; _audit_creation_date 2018-05-28 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.18 svn.r3508 for OlexSys, GUI svn.r5497) ; _shelx_SHELXL_version_number 2018/3 _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C17 H15 N3 O2' _chemical_formula_sum 'C17 H15 N3 O2' _chemical_formula_weight 293.32 _chemical_absolute_configuration unk _chemical_melting_point ? _chemical_oxdiff_formula 'C17 H15 N3 O2' loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system orthorhombic _space_group_IT_number 19 _space_group_name_H-M_alt 'P 21 21 21' _space_group_name_Hall 'P 2ac 2ab' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' _cell_length_a 9.1912(3) _cell_length_b 11.3929(5) _cell_length_c 13.7464(6) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 1439.45(10) _cell_formula_units_Z 4 _cell_measurement_reflns_used 5920 _cell_measurement_temperature 100(10) _cell_measurement_theta_max 71.7690 _cell_measurement_theta_min 4.9790 _shelx_estimated_absorpt_T_max ? _shelx_estimated_absorpt_T_min ? _exptl_absorpt_coefficient_mu 0.741 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.47666 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.35a (Rigaku Oxford Diffraction, 2017) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _exptl_crystal_colour 'clear light white' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier light _exptl_crystal_colour_primary white _exptl_crystal_density_diffrn 1.353 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description prism _exptl_crystal_F_000 616 _exptl_crystal_size_max 0.7 _exptl_crystal_size_mid 0.6 _exptl_crystal_size_min 0.4 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0474 _diffrn_reflns_av_unetI/netI 0.0444 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.994 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -6 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_limit_l_min -16 _diffrn_reflns_number 7780 _diffrn_reflns_point_group_measured_fraction_full 0.997 _diffrn_reflns_point_group_measured_fraction_max 0.990 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 71.958 _diffrn_reflns_theta_min 5.042 _diffrn_ambient_temperature 100(10) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean ? _diffrn_detector_type HyPix3000 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.994 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -93.00 -65.00 0.50 0.20 -- -41.22 164.00 -82.00 56 2 \w -47.00 -21.00 0.50 0.20 -- -41.22 109.00 40.00 52 3 \w -24.00 28.00 0.50 0.20 -- -41.22 20.00 -67.00 104 4 \w -61.00 -35.00 0.50 0.20 -- -41.22 164.00 -82.00 52 5 \w -94.00 -56.00 0.50 0.20 -- -41.22 -20.00 125.00 76 6 \w 53.00 78.00 0.50 0.20 -- 41.22 164.00 -82.00 50 7 \w 21.00 46.00 0.50 0.20 -- 41.22-109.00 -55.00 50 8 \w 50.00 76.00 0.50 0.20 -- 41.22 20.00 -67.00 52 9 \w 91.00 128.00 0.50 0.25 -- 101.00 109.00 40.00 74 10 \w 112.00 137.00 0.50 0.25 -- 101.00 20.00 -67.00 50 11 \w 33.00 108.00 0.50 0.25 -- 101.00 -20.00 125.00 150 12 \w 101.00 127.00 0.50 0.25 -- 101.00 116.00 129.00 52 13 \w 78.00 103.00 0.50 0.25 -- 101.00 164.00 -82.00 50 14 \w 75.00 113.00 0.50 0.25 -- 101.00-116.00 40.00 76 15 \w 82.00 113.00 0.50 0.25 -- 101.00-109.00 -55.00 62 16 \w -11.00 17.00 0.50 0.20 -- -41.22 104.00 -90.00 56 17 \w -76.00 -19.00 0.50 0.20 -- -41.22 104.00 -90.00 114 18 \w 37.00 63.00 0.50 0.20 -- 41.22 32.00 30.00 52 19 \w -12.00 53.00 0.50 0.20 -- 41.22 -43.00 90.00 130 20 \w -1.00 24.00 0.50 0.20 -- 41.22 -20.00 125.00 50 21 \w 51.00 114.00 0.50 0.25 -- 101.00-111.00-180.00 126 22 \w 54.00 114.00 0.50 0.25 -- 101.00 -42.00 -30.00 120 23 \w 84.00 110.00 0.50 0.25 -- 101.00-111.00 -90.00 52 24 \w 36.00 74.00 0.50 0.25 -- 101.00-111.00 -90.00 76 25 \w 108.00 152.00 0.50 0.25 -- 101.00 33.00 -30.00 88 26 \w 37.00 89.00 0.50 0.25 -- 101.00 -33.00-120.00 104 27 \w 88.00 113.00 0.50 0.20 -- 41.22-164.00-107.00 50 28 \w 12.00 39.00 0.50 0.20 -- 41.22 -32.00 150.00 54 29 \w 41.00 97.00 0.50 0.25 -- 101.00-111.00 120.00 112 30 \w 33.00 59.00 0.50 0.25 -- 101.00 -17.00 -90.00 52 31 \w 69.00 106.00 0.50 0.25 -- 101.00 -17.00 -90.00 74 32 \w 82.00 108.00 0.50 0.25 -- 101.00 93.00-150.00 52 33 \w 114.00 140.00 0.50 0.25 -- 101.00 93.00-150.00 52 34 \w 84.00 110.00 0.50 0.25 -- 101.00 59.00-150.00 52 35 \w 49.00 75.00 0.50 0.25 -- 101.00 -77.00 120.00 52 36 \w 86.00 124.00 0.50 0.25 -- 101.00 -77.00 120.00 76 37 \w 132.00 157.00 0.50 0.25 -- 101.00 33.00 -90.00 50 38 \w 47.00 83.00 0.50 0.25 -- 101.00 -77.00 90.00 72 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Single source at offset/far, HyPix3000' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0396042000 _diffrn_orient_matrix_UB_12 -0.1309567000 _diffrn_orient_matrix_UB_13 -0.0094406000 _diffrn_orient_matrix_UB_21 0.0213955000 _diffrn_orient_matrix_UB_22 0.0157946000 _diffrn_orient_matrix_UB_23 -0.1103059000 _diffrn_orient_matrix_UB_31 0.1614965000 _diffrn_orient_matrix_UB_32 0.0299865000 _diffrn_orient_matrix_UB_33 0.0169671000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Cu) X-ray Source' _reflns_Friedel_coverage 0.723 _reflns_Friedel_fraction_full 0.995 _reflns_Friedel_fraction_max 0.985 _reflns_number_gt 2720 _reflns_number_total 2797 _reflns_odcompleteness_completeness 100.00 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 70.93 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'CrysAlisPro 1.171.39.35a (Rigaku OD, 2017)' _computing_data_collection 'CrysAlisPro 1.171.39.35a (Rigaku OD, 2017)' _computing_data_reduction 'CrysAlisPro 1.171.39.35a (Rigaku OD, 2017)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _refine_diff_density_max 0.458 _refine_diff_density_min -0.376 _refine_diff_density_rms 0.058 _refine_ls_abs_structure_details ; Flack x determined using 1118 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.05(15) _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.039 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 199 _refine_ls_number_reflns 2797 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0422 _refine_ls_R_factor_gt 0.0412 _refine_ls_restrained_S_all 1.039 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0635P)^2^+0.4370P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1078 _refine_ls_wR_factor_ref 0.1089 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups, All N(H) groups 2.a Secondary CH2 refined with riding coordinates: C8(H8A,H8B), C10(H10A,H10B), C9(H9A,H9B) 2.b Aromatic/amide H refined with riding coordinates: N2(H2), N1(H1), C5(H5), C14(H14), C15(H15), C13(H13), C4(H4), C2(H2A), C3(H3) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.86817(18) 0.28651(14) 0.32819(12) 0.0141(4) Uani 1 1 d . . . . . O2 O 0.61740(18) 0.17441(15) 0.53808(13) 0.0176(4) Uani 1 1 d . . . . . N2 N 0.8555(2) 0.48732(17) 0.43270(14) 0.0146(4) Uani 1 1 d . . . . . H2 H 0.940755 0.481322 0.407429 0.017 Uiso 1 1 calc R . . . . N1 N 0.8388(2) 0.26165(17) 0.54474(15) 0.0132(4) Uani 1 1 d . . . . . H1 H 0.924899 0.264256 0.520289 0.016 Uiso 1 1 calc R . . . . C7 C 0.7428(3) 0.1877(2) 0.50610(17) 0.0129(5) Uani 1 1 d . . . . . N3 N 0.5768(3) 0.7243(2) 0.4547(2) 0.0301(6) Uani 1 1 d . . . . . C16 C 0.7388(3) 0.3491(2) 0.32344(17) 0.0132(5) Uani 1 1 d . . . . . C1 C 0.8557(3) 0.1646(2) 0.33735(17) 0.0133(5) Uani 1 1 d . . . . . C12 C 0.6059(3) 0.5212(2) 0.37125(18) 0.0167(5) Uani 1 1 d . . . . . C5 C 0.7904(3) -0.0072(2) 0.42920(18) 0.0161(5) Uani 1 1 d . . . . . H5 H 0.749789 -0.041772 0.484171 0.019 Uiso 1 1 calc R . . . . C8 C 0.8050(3) 0.3389(2) 0.62699(18) 0.0169(5) Uani 1 1 d . . . . . H8A H 0.893274 0.352285 0.664008 0.020 Uiso 1 1 calc R . . . . H8B H 0.736279 0.299268 0.669313 0.020 Uiso 1 1 calc R . . . . C10 C 0.8410(3) 0.5317(2) 0.53278(18) 0.0165(5) Uani 1 1 d . . . . . H10A H 0.803338 0.611194 0.530404 0.020 Uiso 1 1 calc R . . . . H10B H 0.936793 0.534889 0.562287 0.020 Uiso 1 1 calc R . . . . C14 C 0.4973(3) 0.3805(2) 0.26078(19) 0.0190(5) Uani 1 1 d . . . . . H14 H 0.419900 0.356022 0.222251 0.023 Uiso 1 1 calc R . . . . C11 C 0.7353(3) 0.4550(2) 0.37821(17) 0.0140(5) Uani 1 1 d . . . . . C6 C 0.7975(2) 0.1153(2) 0.42227(18) 0.0133(5) Uani 1 1 d . . . . . C9 C 0.7412(3) 0.4574(2) 0.59740(16) 0.0158(5) Uani 1 1 d . . . . . H9A H 0.718900 0.501655 0.655824 0.019 Uiso 1 1 calc R . . . . H9B H 0.650502 0.444029 0.563106 0.019 Uiso 1 1 calc R . . . . C15 C 0.6247(3) 0.3143(2) 0.26531(17) 0.0162(5) Uani 1 1 d . . . . . H15 H 0.632697 0.245918 0.228723 0.019 Uiso 1 1 calc R . . . . C13 C 0.4874(3) 0.4831(2) 0.31426(19) 0.0205(6) Uani 1 1 d . . . . . H13 H 0.402260 0.527158 0.312590 0.025 Uiso 1 1 calc R . . . . C4 C 0.8433(3) -0.0775(2) 0.3548(2) 0.0196(5) Uani 1 1 d . . . . . H4 H 0.840939 -0.158793 0.361100 0.024 Uiso 1 1 calc R . . . . C2 C 0.9059(3) 0.0949(2) 0.26167(19) 0.0182(5) Uani 1 1 d . . . . . H2A H 0.943056 0.128976 0.205462 0.022 Uiso 1 1 calc R . . . . C17 C 0.5912(3) 0.6334(2) 0.4195(2) 0.0207(6) Uani 1 1 d . . . . . C3 C 0.8999(3) -0.0272(2) 0.27090(19) 0.0200(5) Uani 1 1 d . . . . . H3 H 0.933863 -0.074715 0.220815 0.024 Uiso 1 1 calc R . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0102(8) 0.0125(8) 0.0195(8) 0.0008(6) 0.0007(7) -0.0013(7) O2 0.0085(8) 0.0205(8) 0.0237(8) -0.0006(7) 0.0021(7) -0.0009(7) N2 0.0089(10) 0.0162(9) 0.0185(9) -0.0008(8) 0.0003(8) -0.0013(8) N1 0.0086(9) 0.0138(9) 0.0171(9) -0.0016(8) 0.0004(8) 0.0008(7) C7 0.0086(10) 0.0128(11) 0.0174(10) 0.0040(8) -0.0018(9) 0.0011(9) N3 0.0299(13) 0.0187(11) 0.0418(14) 0.0003(11) -0.0032(11) 0.0071(10) C16 0.0115(11) 0.0128(11) 0.0152(10) 0.0052(9) 0.0015(9) -0.0015(9) C1 0.0068(10) 0.0127(11) 0.0205(11) -0.0012(9) -0.0020(9) -0.0008(9) C12 0.0154(12) 0.0147(11) 0.0200(11) 0.0056(10) -0.0004(10) -0.0008(10) C5 0.0104(11) 0.0146(11) 0.0234(11) 0.0015(9) -0.0023(10) 0.0002(9) C8 0.0187(12) 0.0163(12) 0.0157(11) -0.0026(10) -0.0014(9) 0.0006(10) C10 0.0151(12) 0.0125(11) 0.0219(11) -0.0011(9) -0.0017(10) 0.0001(9) C14 0.0153(12) 0.0185(12) 0.0231(12) 0.0062(10) -0.0061(10) -0.0073(10) C11 0.0119(11) 0.0142(10) 0.0158(10) 0.0038(9) 0.0004(9) -0.0038(10) C6 0.0060(10) 0.0143(11) 0.0196(11) -0.0012(9) -0.0007(9) -0.0001(8) C9 0.0149(12) 0.0163(11) 0.0163(10) -0.0029(9) 0.0002(9) 0.0009(10) C15 0.0185(12) 0.0140(10) 0.0162(11) 0.0025(8) -0.0026(9) -0.0050(9) C13 0.0139(12) 0.0200(12) 0.0276(13) 0.0104(11) -0.0034(11) 0.0001(10) C4 0.0137(11) 0.0126(11) 0.0325(14) -0.0037(10) -0.0045(10) 0.0017(9) C2 0.0117(11) 0.0223(12) 0.0205(12) -0.0032(10) 0.0017(10) -0.0018(10) C17 0.0158(12) 0.0193(13) 0.0272(13) 0.0063(11) -0.0019(11) 0.0027(10) C3 0.0113(11) 0.0209(12) 0.0277(12) -0.0100(10) -0.0003(10) 0.0017(10) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C16 1.388(3) . ? O1 C1 1.399(3) . ? O2 C7 1.243(3) . ? N2 C10 1.472(3) . ? N2 C11 1.384(3) . ? N1 C7 1.331(3) . ? N1 C8 1.466(3) . ? C7 C6 1.504(3) . ? N3 C17 1.150(4) . ? C16 C11 1.422(3) . ? C16 C15 1.377(3) . ? C1 C6 1.402(3) . ? C1 C2 1.388(3) . ? C12 C11 1.412(3) . ? C12 C13 1.409(4) . ? C12 C17 1.446(4) . ? C5 C6 1.400(3) . ? C5 C4 1.387(4) . ? C8 C9 1.527(3) . ? C10 C9 1.532(3) . ? C14 C15 1.394(4) . ? C14 C13 1.384(4) . ? C4 C3 1.389(4) . ? C2 C3 1.397(4) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C16 O1 C1 116.35(18) . . ? C11 N2 C10 121.7(2) . . ? C7 N1 C8 123.2(2) . . ? O2 C7 N1 123.4(2) . . ? O2 C7 C6 120.9(2) . . ? N1 C7 C6 115.6(2) . . ? O1 C16 C11 115.5(2) . . ? C15 C16 O1 122.1(2) . . ? C15 C16 C11 122.3(2) . . ? O1 C1 C6 120.3(2) . . ? C2 C1 O1 118.3(2) . . ? C2 C1 C6 121.4(2) . . ? C11 C12 C17 121.3(2) . . ? C13 C12 C11 121.6(2) . . ? C13 C12 C17 117.0(2) . . ? C4 C5 C6 120.6(2) . . ? N1 C8 C9 114.00(19) . . ? N2 C10 C9 113.97(19) . . ? C13 C14 C15 119.3(2) . . ? N2 C11 C16 119.6(2) . . ? N2 C11 C12 124.5(2) . . ? C12 C11 C16 115.9(2) . . ? C1 C6 C7 123.1(2) . . ? C5 C6 C7 118.6(2) . . ? C5 C6 C1 118.3(2) . . ? C8 C9 C10 114.4(2) . . ? C16 C15 C14 120.6(2) . . ? C14 C13 C12 120.3(2) . . ? C5 C4 C3 120.3(2) . . ? C1 C2 C3 119.3(2) . . ? N3 C17 C12 177.4(3) . . ? C4 C3 C2 120.1(2) . . ? _shelx_res_file ; TITL reu131_a.res in P2(1)2(1)2(1) reu131.res created by SHELXL-2018/3 at 19:37:03 on 28-May-2018 REM Old TITL 8722-9530-reu131_a.res in P2(1)2(1)2(1) REM SHELXT solution in P2(1)2(1)2(1): R1 0.087, Rweak 0.021, Alpha 0.000 REM 0.744 for 21 systematic absences, Orientation as input REM Flack x = 0.153 ( 0.147 ) from 1135 Parsons' quotients REM Formula found by SHELXT: C17 N3 O2 CELL 1.54184 9.1912 11.3929 13.7464 90 90 90 ZERR 4 0.0003 0.0005 0.0006 0 0 0 LATT -1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H N O UNIT 68 60 12 8 L.S. 20 PLAN 5 list 4 fmap 2 acta OMIT -4 145 OMIT 1 3 6 OMIT 5 4 0 OMIT 4 5 3 OMIT 1 2 0 OMIT -1 7 1 OMIT 3 4 4 REM REM REM WGHT 0.063500 0.437000 FVAR 0.97756 O1 4 0.868168 0.286512 0.328190 11.00000 0.01025 0.01253 = 0.01948 0.00078 0.00065 -0.00131 O2 4 0.617396 0.174414 0.538077 11.00000 0.00851 0.02048 = 0.02371 -0.00058 0.00211 -0.00088 N2 3 0.855485 0.487317 0.432702 11.00000 0.00894 0.01620 = 0.01854 -0.00079 0.00033 -0.00133 AFIX 43 H2 2 0.940755 0.481322 0.407429 11.00000 -1.20000 AFIX 0 N1 3 0.838835 0.261648 0.544741 11.00000 0.00858 0.01379 = 0.01714 -0.00158 0.00039 0.00077 AFIX 43 H1 2 0.924899 0.264256 0.520289 11.00000 -1.20000 AFIX 0 C7 1 0.742811 0.187706 0.506103 11.00000 0.00862 0.01281 = 0.01738 0.00403 -0.00182 0.00109 N3 3 0.576764 0.724297 0.454667 11.00000 0.02990 0.01867 = 0.04178 0.00029 -0.00317 0.00709 C16 1 0.738784 0.349112 0.323439 11.00000 0.01155 0.01275 = 0.01521 0.00516 0.00153 -0.00152 C1 1 0.855669 0.164624 0.337345 11.00000 0.00682 0.01269 = 0.02045 -0.00115 -0.00197 -0.00083 C12 1 0.605861 0.521195 0.371249 11.00000 0.01539 0.01474 = 0.01999 0.00559 -0.00038 -0.00082 C5 1 0.790369 -0.007239 0.429201 11.00000 0.01036 0.01462 = 0.02338 0.00145 -0.00227 0.00022 AFIX 43 H5 2 0.749789 -0.041772 0.484171 11.00000 -1.20000 AFIX 0 C8 1 0.804977 0.338884 0.626988 11.00000 0.01865 0.01629 = 0.01574 -0.00256 -0.00142 0.00064 AFIX 23 H8A 2 0.893274 0.352285 0.664008 11.00000 -1.20000 H8B 2 0.736279 0.299268 0.669313 11.00000 -1.20000 AFIX 0 C10 1 0.841006 0.531713 0.532783 11.00000 0.01505 0.01247 = 0.02194 -0.00115 -0.00175 0.00009 AFIX 23 H10A 2 0.803338 0.611194 0.530404 11.00000 -1.20000 H10B 2 0.936793 0.534889 0.562287 11.00000 -1.20000 AFIX 0 C14 1 0.497334 0.380517 0.260779 11.00000 0.01535 0.01851 = 0.02314 0.00623 -0.00613 -0.00727 AFIX 43 H14 2 0.419900 0.356022 0.222251 11.00000 -1.20000 AFIX 0 C11 1 0.735322 0.454960 0.378213 11.00000 0.01193 0.01424 = 0.01576 0.00383 0.00041 -0.00381 C6 1 0.797471 0.115257 0.422274 11.00000 0.00601 0.01431 = 0.01957 -0.00124 -0.00069 -0.00011 C9 1 0.741227 0.457439 0.597399 11.00000 0.01487 0.01630 = 0.01629 -0.00293 0.00024 0.00088 AFIX 23 H9A 2 0.718900 0.501655 0.655824 11.00000 -1.20000 H9B 2 0.650502 0.444029 0.563106 11.00000 -1.20000 AFIX 0 C15 1 0.624718 0.314277 0.265312 11.00000 0.01846 0.01403 = 0.01620 0.00251 -0.00256 -0.00499 AFIX 43 H15 2 0.632697 0.245918 0.228723 11.00000 -1.20000 AFIX 0 C13 1 0.487428 0.483131 0.314261 11.00000 0.01390 0.02004 = 0.02761 0.01040 -0.00337 0.00012 AFIX 43 H13 2 0.402260 0.527158 0.312590 11.00000 -1.20000 AFIX 0 C4 1 0.843328 -0.077542 0.354789 11.00000 0.01374 0.01260 = 0.03248 -0.00365 -0.00449 0.00174 AFIX 43 H4 2 0.840939 -0.158793 0.361100 11.00000 -1.20000 AFIX 0 C2 1 0.905870 0.094868 0.261674 11.00000 0.01169 0.02227 = 0.02050 -0.00318 0.00172 -0.00178 AFIX 43 H2A 2 0.943056 0.128976 0.205462 11.00000 -1.20000 AFIX 0 C17 1 0.591203 0.633431 0.419452 11.00000 0.01576 0.01932 = 0.02717 0.00632 -0.00192 0.00272 C3 1 0.899911 -0.027158 0.270896 11.00000 0.01129 0.02090 = 0.02768 -0.01005 -0.00025 0.00173 AFIX 43 H3 2 0.933863 -0.074715 0.220815 11.00000 -1.20000 AFIX 0 HKLF 4 REM reu131_a.res in P2(1)2(1)2(1) REM wR2 = 0.1089, GooF = S = 1.039, Restrained GooF = 1.039 for all data REM R1 = 0.0412 for 2720 Fo > 4sig(Fo) and 0.0422 for all 2797 data REM 199 parameters refined using 0 restraints END WGHT 0.0635 0.4370 REM Highest difference peak 0.458, deepest hole -0.376, 1-sigma level 0.058 Q1 1 0.9311 0.4315 0.4345 11.00000 0.05 0.46 Q2 1 0.9446 0.1749 0.4366 11.00000 0.05 0.20 Q3 1 0.6094 0.1980 0.6046 11.00000 0.05 0.19 Q4 1 0.7429 0.4377 0.4404 11.00000 0.05 0.18 Q5 1 0.9519 0.1556 0.5764 11.00000 0.05 0.17 ; _shelx_res_checksum 32975 _shelx_hkl_file ; 0 0 -1 0.81 0.37 0 0 -2 469.05 24.95 0 0 2 545.73 24.75 0 0 -3 -0.17 0.90 0 0 3 0.13 0.71 0 0 -4 29.83 3.68 0 0 4 37.04 3.48 0 0 -5 0.67 1.59 0 0 5 7.63 1.84 0 0 -6 408.88 24.49 0 0 -7 -0.55 1.88 0 0 7 0.43 1.47 0 0 -8 241.85 18.46 0 0 8 237.18 17.00 0 0 9 2.66 1.91 0 0 9 0.62 2.02 0 0 10 1656.00 84.65 0 0 10 1731.76 87.92 0 0 11 -0.81 1.86 0 0 11 -0.55 1.41 0 0 11 0.44 1.43 0 0 12 121.28 10.60 0 0 12 111.03 10.94 0 0 13 -0.52 1.70 0 0 14 170.96 13.61 0 0 15 -0.95 1.80 0 0 16 106.05 9.00 0 1 0 0.10 0.30 0 1 0 -0.06 0.32 0 1 1 7964.93 337.25 0 -1 1 7192.94 338.28 0 1 1 7538.05 337.82 0 1 2 13.00 1.41 0 1 2 14.74 1.59 0 1 -3 1589.32 71.37 0 1 3 1461.95 72.46 0 1 3 1441.61 73.05 0 1 4 504.95 26.36 0 -1 5 1874.64 88.24 0 -1 -5 1888.80 88.94 0 1 5 1736.99 88.01 0 -1 -6 8.91 2.79 0 1 6 8.98 2.43 0 -1 -7 116.60 10.43 0 1 7 109.43 9.57 0 -1 -8 12.14 3.70 0 1 8 10.53 3.08 0 -1 -9 84.62 10.25 0 -1 -9 90.80 7.21 0 1 9 83.13 8.06 0 1 9 79.93 9.12 0 -1 9 93.81 8.87 0 -1 9 81.77 9.73 0 -1 -10 32.28 4.27 0 -1 10 38.53 5.77 0 1 10 40.25 5.09 0 1 10 36.46 5.41 0 1 10 36.59 6.46 0 -1 10 43.50 5.24 0 -1 10 32.95 6.50 0 1 11 5.51 3.00 0 1 11 3.78 2.56 0 -1 11 5.14 2.46 0 -1 11 2.59 2.43 0 1 11 4.38 2.02 0 -1 11 4.02 1.93 0 1 12 109.16 10.12 0 -1 12 125.09 10.71 0 1 12 104.85 10.58 0 -1 13 16.47 3.94 0 1 13 11.82 3.28 0 1 13 10.46 3.31 0 -1 14 344.18 22.30 0 1 14 341.80 22.14 0 1 15 267.63 18.37 0 -1 15 299.01 19.06 0 -1 16 10.77 2.71 0 1 16 11.42 2.78 0 1 -16 10.75 3.12 0 2 0 1587.54 75.89 0 2 0 1652.97 76.18 0 2 1 656.73 31.53 0 2 -1 630.13 31.24 0 -2 1 644.98 32.00 0 2 2 255.07 14.86 0 -2 2 271.81 15.85 0 2 2 294.56 14.16 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2197.47 103.40 0 4 -1 1.09 1.25 0 4 -1 2.03 1.10 0 4 1 0.55 1.10 0 4 1 2.50 1.28 0 4 -2 2431.20 115.67 0 -4 2 2521.78 118.00 0 4 2 2385.17 116.32 0 -4 3 757.78 42.92 0 4 -3 807.08 41.24 0 4 3 872.10 42.21 0 -4 4 0.94 1.62 0 4 4 0.37 1.35 0 4 -4 0.61 0.98 0 4 4 1.22 1.31 0 4 5 242.89 15.56 0 4 5 264.51 16.85 0 4 -5 241.56 15.66 0 4 -6 40.10 5.14 0 4 6 44.14 5.24 0 4 6 37.11 5.38 0 4 -7 10.24 2.88 0 4 7 16.57 3.70 0 -4 -8 545.39 31.83 0 4 8 606.69 33.07 0 4 -8 566.87 33.91 0 4 8 623.53 34.80 0 -4 8 585.30 35.59 0 -4 -9 49.95 7.76 0 -4 -9 53.10 6.42 0 -4 9 64.06 8.97 0 4 9 59.91 7.13 0 4 9 73.86 8.70 0 -4 -10 9.10 3.61 0 4 -10 16.30 4.96 0 4 10 12.63 3.46 0 4 10 18.94 4.62 0 -4 -10 20.62 4.06 0 4 -11 4.59 3.64 0 4 11 2.93 2.12 0 -4 -11 1.60 1.65 0 -4 -12 367.48 22.89 0 4 12 393.42 25.25 0 4 -12 430.81 29.29 0 4 13 570.90 33.89 0 4 -13 600.68 37.30 0 4 -13 589.26 35.71 0 -4 -13 562.23 31.72 0 4 14 12.67 3.43 0 -4 -14 10.95 2.62 0 4 -14 12.24 3.58 0 4 -14 13.71 4.12 0 4 -15 2.00 1.90 0 4 15 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4 -9 604.14 38.52 -2 4 9 768.21 37.89 -2 4 9 757.46 40.13 2 4 -9 621.56 37.16 -2 -4 -9 570.92 38.15 2 4 -8 237.19 17.65 2 -4 8 219.23 18.79 2 4 -8 232.45 16.52 -2 4 8 244.86 17.85 2 4 -8 226.51 17.37 -2 -4 -8 210.91 17.10 2 4 -7 1097.06 61.21 2 -4 7 1148.26 63.82 2 4 -7 1193.19 60.30 -2 4 7 1263.87 62.09 2 -4 6 1035.03 57.29 2 4 -6 1018.52 55.10 -2 4 6 1102.65 55.35 2 -4 5 438.86 26.95 -2 4 5 425.93 24.99 2 4 -5 412.74 25.27 2 4 -4 553.56 29.56 2 -4 4 497.72 30.01 2 -4 4 487.70 29.63 2 4 -3 681.23 34.19 2 -4 3 583.78 33.94 2 -4 3 599.91 34.30 -2 4 2 1285.68 63.48 2 4 -2 1285.18 64.06 2 -4 2 1286.04 64.95 2 -4 2 1295.44 64.54 -2 4 1 942.72 45.28 2 4 -1 950.52 45.55 2 -4 1 918.60 46.35 2 4 0 59.46 6.08 -2 4 0 63.68 6.39 2 4 0 69.27 5.94 2 4 1 918.41 45.38 2 4 1 864.45 45.78 -2 -4 1 866.33 46.29 2 4 1 937.35 45.47 -2 4 -1 905.15 46.81 2 4 2 1361.90 66.01 -2 -4 2 1311.32 67.42 2 4 3 614.00 32.78 -2 -4 3 637.16 34.73 2 4 4 531.69 28.82 -2 -4 4 520.60 30.67 2 4 5 388.62 23.49 2 4 5 438.19 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4.88 5 3 -9 38.32 6.12 5 -3 8 764.93 50.41 5 -3 8 816.39 44.22 5 3 -8 908.08 46.72 5 -3 7 39.93 7.72 5 -3 7 30.25 4.61 5 3 -7 33.47 5.47 5 -3 6 146.62 15.25 5 -3 5 851.27 49.61 5 -3 4 214.46 17.56 5 3 -4 219.73 14.75 5 -3 3 100.00 11.20 5 3 -3 98.42 10.00 5 -3 2 164.55 14.87 5 3 -2 156.18 13.42 5 -3 1 383.64 25.36 5 3 -1 331.06 22.74 5 3 0 248.78 18.32 5 -3 0 285.58 20.56 5 -3 -1 330.48 23.60 5 3 1 340.28 22.18 5 -3 -2 131.89 13.14 5 3 2 149.88 12.82 5 3 2 137.23 12.09 5 -3 -3 100.95 11.27 5 3 3 109.00 10.70 5 3 3 79.08 9.16 5 3 4 199.82 16.53 5 3 4 188.67 16.34 5 3 4 225.04 15.46 5 3 5 884.19 49.14 5 3 5 785.43 48.53 5 3 5 958.66 46.93 5 3 6 157.08 11.65 5 3 6 161.01 11.24 5 3 6 122.42 12.50 5 3 6 129.27 13.11 5 3 7 31.28 4.57 5 3 7 37.95 6.41 5 3 7 27.07 5.90 5 -3 -7 33.24 5.09 5 3 8 905.97 46.19 5 -3 -8 815.81 46.77 5 3 8 845.99 50.41 5 -3 -8 939.13 47.65 5 -3 -9 40.39 5.91 5 3 9 37.36 5.22 5 3 9 33.21 6.66 5 -3 -9 37.70 5.74 5 -3 -10 322.18 21.02 5 3 10 335.61 24.19 5 3 10 315.41 20.13 5 -3 -10 316.72 20.91 5 3 11 98.96 9.29 5 -3 -11 121.79 10.41 5 3 11 125.66 12.73 5 -3 -11 113.28 10.24 5 -3 -12 21.02 3.80 5 3 12 23.59 4.97 5 -3 -12 22.17 4.08 5 -3 -13 14.67 2.94 5 -3 -14 8.02 1.86 5 -4 14 67.56 5.40 5 -4 13 40.23 4.48 5 -4 12 37.81 4.81 5 -4 11 7.68 2.31 5 4 -11 13.66 3.62 5 -4 10 411.30 24.95 5 4 -10 429.28 27.06 5 -4 9 752.17 42.12 5 4 -9 827.99 44.43 5 -4 8 347.05 21.84 5 4 -8 350.00 23.10 5 -4 7 90.59 12.41 5 -4 7 95.12 8.87 5 -4 6 52.69 9.06 5 -4 6 62.43 6.78 5 4 -5 15.52 3.38 5 -4 5 13.08 2.96 5 4 -4 220.48 14.66 5 -4 4 191.94 13.76 5 -4 3 187.18 17.25 5 4 -3 217.09 14.43 5 4 -3 184.21 15.92 5 -4 3 222.34 15.27 5 4 -2 269.96 16.97 5 4 -2 324.31 16.26 5 -4 2 271.97 18.10 5 4 -1 386.06 21.85 5 4 -1 394.45 20.67 5 4 -1 349.50 21.53 5 -4 1 331.96 22.60 5 4 0 73.08 8.06 5 4 0 93.43 7.80 5 4 0 88.10 6.91 5 -4 0 83.14 8.63 5 4 1 354.10 22.23 5 4 1 330.98 20.20 5 4 1 312.71 20.35 5 4 1 396.82 19.82 5 -4 -1 359.19 22.39 5 4 2 278.64 18.24 5 4 2 246.24 16.46 5 4 2 276.51 16.42 5 4 2 282.00 16.46 5 4 2 307.69 15.78 5 -4 -2 276.42 18.17 5 4 3 204.06 15.00 5 4 3 264.30 15.27 5 4 3 173.95 16.23 5 4 3 288.11 14.46 5 4 3 222.68 16.34 5 4 3 209.70 17.03 5 4 3 238.72 15.09 5 -4 -3 263.85 20.40 5 4 4 182.96 16.43 5 4 4 202.74 15.14 5 4 4 190.03 16.35 5 4 5 11.64 3.10 5 4 5 6.94 3.01 5 4 5 9.26 3.39 5 4 6 69.37 6.76 5 4 6 58.61 8.56 5 4 7 73.70 7.48 5 -4 -7 89.66 9.45 5 4 7 67.54 9.72 5 4 8 319.01 20.64 5 -4 -8 320.67 22.81 5 4 8 332.44 25.36 5 -4 -8 372.70 22.24 5 4 9 771.93 41.96 5 4 9 795.02 47.29 5 -4 -9 788.89 42.93 5 4 10 390.01 24.48 5 -4 -10 410.68 24.99 5 4 10 411.34 28.96 5 -4 -10 455.25 25.92 5 4 11 8.74 2.52 5 -4 -11 9.87 2.73 5 4 11 14.17 4.12 5 -4 -11 9.25 2.89 5 -4 -12 30.13 4.36 5 4 12 34.14 6.02 5 -4 -13 41.14 4.61 5 4 13 39.99 5.80 5 -4 -14 60.63 5.05 5 -5 13 132.11 9.12 5 -5 12 75.51 6.86 5 -5 11 184.34 13.15 5 -5 10 25.79 4.37 5 -5 9 328.70 20.96 5 5 -9 317.11 21.68 5 -5 8 10.38 3.14 5 -5 7 119.57 10.60 5 -5 6 42.46 5.73 5 -5 5 106.22 9.61 5 -5 4 5.63 2.12 5 5 -3 4.44 2.05 5 -5 3 7.90 2.30 5 5 -3 4.69 1.88 5 -5 3 3.19 2.03 5 5 -2 26.53 4.36 5 -5 2 22.35 6.19 5 5 -2 29.32 4.52 5 -5 2 22.93 3.91 5 5 -2 40.56 4.31 5 -5 2 25.91 4.86 5 5 -1 21.66 3.80 5 5 -1 17.27 3.33 5 -5 1 11.58 2.93 5 5 -1 25.90 3.37 5 -5 1 18.86 5.56 5 -5 1 12.42 3.52 5 5 0 1106.13 56.01 5 -5 0 890.32 55.36 5 -5 0 1076.20 64.43 5 5 0 1006.58 55.87 5 -5 0 1070.77 58.45 5 -5 -1 13.82 5.08 5 5 1 14.93 3.69 5 5 1 12.51 2.91 -5 5 -1 11.24 3.76 5 5 1 27.22 3.86 5 -5 -1 12.26 2.93 5 5 1 20.32 3.56 5 5 1 20.89 2.98 5 -5 -1 15.27 3.91 5 -5 -2 21.95 6.36 5 5 2 29.51 4.43 -5 5 -2 27.81 5.86 5 5 2 28.50 4.02 5 5 2 40.69 4.06 5 5 2 27.38 4.94 5 5 2 21.25 3.71 5 -5 -2 27.17 5.06 5 5 3 4.79 2.29 5 5 3 6.81 2.35 -5 5 -3 4.87 2.64 5 5 3 4.70 1.86 5 5 3 5.41 1.82 5 5 3 2.26 1.45 5 5 4 7.51 2.50 -5 5 -4 8.78 3.91 5 5 4 6.75 2.55 5 -5 -5 99.47 9.84 -5 5 -5 89.52 11.93 5 5 5 100.96 11.33 5 5 6 49.17 5.97 5 -5 -6 48.86 6.90 -5 5 -6 42.52 8.03 5 5 6 38.72 7.19 5 5 7 139.10 10.89 5 -5 -7 122.25 11.88 -5 5 -7 103.84 13.51 5 5 7 119.68 13.44 5 5 8 11.02 2.99 5 -5 -8 11.69 3.90 5 5 8 8.92 4.12 5 -5 -8 10.84 3.17 5 -5 -9 314.72 22.99 5 5 9 337.10 25.50 5 5 9 352.50 21.44 5 -5 -9 353.69 22.17 5 5 10 22.49 4.13 5 5 10 28.20 6.15 5 -5 -10 23.11 4.34 5 5 11 199.25 13.95 5 5 11 203.01 16.76 5 5 12 63.16 7.88 5 5 13 145.99 11.52 5 -6 13 56.27 4.89 5 -6 12 273.43 16.36 5 -6 11 103.01 8.72 5 -6 10 2.17 1.72 5 -6 9 241.26 16.91 5 -6 8 26.76 4.80 5 -6 7 205.55 15.50 5 -6 6 334.73 21.86 5 -6 5 507.47 30.01 5 6 -5 510.95 29.48 5 6 -4 109.91 9.94 5 -6 4 112.59 10.08 5 -6 3 116.28 10.45 5 6 -3 128.60 10.80 5 -6 3 125.82 11.71 5 -6 2 75.70 11.89 5 -6 2 58.96 7.03 5 6 -2 78.88 7.82 5 -6 2 62.40 8.04 5 6 -1 16.50 3.54 5 -6 1 16.83 6.05 5 -6 1 15.56 3.47 5 -6 1 13.34 3.98 5 -6 0 121.39 16.06 5 6 0 151.02 11.88 5 -6 0 140.60 11.57 5 6 0 146.57 11.58 5 -6 0 155.63 13.52 5 -6 -1 14.56 5.59 5 6 1 12.06 3.41 5 6 1 12.65 3.29 5 -6 -1 11.56 3.16 5 -6 -1 11.30 2.94 5 6 1 19.01 3.57 5 -6 -1 10.12 3.45 5 6 2 81.36 8.86 5 -6 -2 57.06 10.58 -5 6 -2 62.42 9.68 5 6 2 77.27 7.85 5 6 2 75.89 7.59 5 -6 -2 83.80 9.33 5 6 3 115.61 11.06 5 6 3 113.63 10.26 -5 6 -3 108.59 13.12 5 6 3 140.78 10.02 5 -6 -3 108.29 14.64 5 -6 -3 125.84 11.77 -5 6 -4 79.60 11.13 5 -6 -4 76.80 8.62 -5 6 -5 484.84 34.83 5 -6 -5 527.22 31.30 5 6 6 321.37 20.40 -5 6 -6 314.80 25.94 5 6 6 350.74 24.93 5 -6 -6 309.70 22.12 5 6 7 211.41 14.96 5 -6 -7 193.52 16.35 5 6 7 222.62 19.07 5 6 8 26.18 4.30 5 -6 -8 16.60 4.39 5 6 8 19.95 5.42 5 -6 -8 14.48 3.75 5 -6 -9 244.95 18.75 5 6 9 246.40 16.56 5 6 9 234.34 19.96 5 -6 -9 261.00 17.52 5 6 10 4.73 2.03 5 6 10 5.15 3.05 5 6 11 91.00 7.98 5 6 11 99.68 10.31 5 6 12 327.60 21.13 5 6 13 60.56 6.28 5 -7 12 191.63 11.89 5 -7 11 36.51 4.57 5 -7 10 72.89 7.32 5 -7 9 57.12 6.79 5 -7 8 155.64 12.72 5 7 -7 269.35 17.51 5 -7 7 278.66 19.20 5 7 -6 405.39 24.24 5 -7 6 410.06 25.78 5 -7 5 197.67 15.23 5 7 -5 190.98 14.05 5 -7 4 137.27 12.41 5 -7 4 113.77 10.77 5 7 -4 113.77 10.23 5 7 -3 159.04 12.72 5 -7 3 172.45 14.34 5 -7 3 178.84 13.66 5 -7 3 154.55 14.05 5 -7 2 378.53 32.12 5 -7 2 431.28 26.78 5 -7 2 380.18 25.23 5 7 -2 446.21 25.63 5 -7 2 432.78 27.51 5 -7 1 122.45 11.71 5 7 -1 123.85 11.17 5 -7 1 149.74 11.97 5 7 -1 141.34 11.39 5 -7 1 122.48 12.39 5 -7 1 135.23 17.11 5 -7 0 1.32 3.39 5 7 0 3.56 2.19 5 -7 0 0.56 1.83 5 -7 0 2.52 1.83 5 7 0 1.86 1.85 5 -7 0 1.35 2.19 5 7 1 144.00 12.60 5 7 1 147.27 11.77 5 -7 -1 122.03 11.58 5 7 1 144.88 11.37 5 -7 -1 131.56 12.67 5 -7 -2 435.46 34.13 5 7 2 398.73 24.94 5 7 2 417.27 26.63 5 -7 -2 438.10 27.68 5 7 2 418.03 25.63 5 7 3 164.33 13.49 5 7 3 169.16 12.95 -5 7 -3 158.13 16.54 5 -7 -3 175.74 14.28 -5 7 -4 119.97 13.93 5 -7 -4 91.51 10.19 5 -7 -5 168.13 14.40 5 7 6 374.52 22.75 5 -7 -6 361.26 24.85 5 7 7 247.65 16.95 5 -7 -7 259.24 19.53 5 7 7 270.12 20.86 5 7 8 121.68 10.50 5 -7 -8 124.79 12.49 5 7 8 159.00 14.64 5 -7 -8 158.72 12.27 5 7 9 41.87 5.35 5 -7 -9 58.36 7.65 5 7 9 41.97 7.14 5 7 10 69.83 6.69 5 7 10 67.54 8.49 5 7 11 41.65 4.59 5 7 11 33.08 5.41 5 7 12 205.47 14.16 5 -8 11 7.71 1.92 5 -8 10 0.34 1.18 5 -8 9 180.51 13.26 5 -8 8 67.15 7.58 5 -8 7 100.98 10.34 5 -8 7 107.10 10.15 5 -8 6 32.79 5.83 5 -8 6 32.51 5.53 5 -8 5 63.02 8.25 5 8 -5 63.65 6.77 5 -8 5 54.61 7.34 5 -8 4 88.01 9.97 5 -8 4 83.17 9.17 5 8 -4 93.07 8.56 5 -8 3 1128.42 58.05 5 8 -3 1028.04 55.06 5 -8 3 995.98 56.25 5 -8 3 1142.77 58.23 5 8 -2 126.03 11.51 5 -8 2 120.68 11.81 5 -8 2 117.75 11.26 5 8 -2 134.67 11.07 5 -8 2 133.38 12.48 5 8 -1 896.15 45.65 5 -8 1 767.69 45.21 5 -8 1 744.32 44.35 5 8 -1 872.69 44.31 5 -8 1 791.24 46.10 5 8 0 179.81 15.16 5 8 0 192.99 14.71 5 -8 0 172.31 14.73 5 8 0 191.14 14.08 5 -8 0 180.02 15.62 5 8 1 840.43 45.00 5 8 1 833.13 46.52 5 8 1 867.39 45.86 5 -8 -1 778.65 46.65 5 8 2 132.77 11.98 5 8 2 119.93 11.04 5 -8 -2 114.94 11.83 5 8 3 1101.86 58.76 5 -8 -3 1146.31 60.55 5 -8 -4 76.30 9.20 5 -8 -5 49.95 7.39 5 8 6 24.36 4.21 5 -8 -6 27.82 5.55 5 8 7 96.95 8.61 5 -8 -7 94.25 10.46 5 8 8 50.88 5.74 5 -8 -8 52.21 7.26 5 -8 -9 154.10 13.06 5 8 9 135.97 10.55 5 8 9 177.39 13.73 5 8 10 1.73 1.28 5 8 10 0.95 1.55 5 8 11 6.85 2.33 5 -9 10 47.71 4.80 5 -9 9 6.54 2.18 5 -9 9 5.51 2.07 5 -9 8 157.61 11.88 5 -9 8 143.10 11.50 5 -9 7 26.86 4.80 5 -9 7 34.51 5.25 5 -9 6 49.09 6.74 5 -9 6 48.43 6.48 5 -9 5 19.90 4.35 5 -9 5 12.36 3.45 5 9 -4 249.31 17.70 5 -9 4 277.16 19.33 5 -9 4 258.04 18.47 5 9 -3 262.95 17.02 5 9 -3 304.76 19.06 5 -9 3 243.28 18.67 5 -9 3 224.05 17.67 5 -9 3 269.07 19.03 5 9 -2 153.45 11.80 5 9 -2 167.78 13.21 5 -9 2 144.35 13.15 5 -9 2 126.22 12.06 5 -9 2 163.71 13.74 5 9 -1 14.18 3.66 5 -9 1 7.39 3.10 5 9 -1 4.87 2.36 5 -9 1 12.51 3.81 5 9 0 970.46 51.11 5 9 0 989.67 50.26 5 -9 0 870.49 50.33 5 -9 0 852.10 50.30 5 9 1 8.97 3.10 5 9 1 12.35 3.46 5 -9 -1 8.82 3.10 5 9 2 170.11 13.33 5 -9 -2 145.44 13.41 5 -9 -3 238.86 19.02 5 -9 -3 315.32 20.59 5 -9 -4 236.89 18.06 5 9 5 19.28 3.64 5 -9 -5 9.48 3.54 5 9 6 48.39 5.58 5 -9 -6 42.01 6.64 5 9 7 24.85 3.78 5 -9 -7 21.02 4.71 5 9 8 125.01 9.47 5 -9 -8 142.03 12.02 5 9 9 3.72 1.50 5 9 10 49.59 4.55 5 -10 9 383.96 20.76 5 10 -8 153.13 10.40 5 10 -8 124.47 9.01 5 -10 8 143.09 10.21 5 -10 8 148.71 10.26 5 10 -7 93.12 7.65 5 -10 7 103.62 8.92 5 -10 7 111.28 9.02 5 10 -6 132.07 9.98 5 -10 6 143.97 11.48 5 -10 6 139.05 11.16 5 -10 5 14.96 3.63 5 -10 5 16.14 3.52 5 10 -4 9.32 2.72 5 -10 4 15.94 4.03 5 -10 4 11.04 3.06 5 10 -3 163.81 12.31 5 -10 3 152.51 13.02 5 -10 3 149.31 12.53 5 10 -2 391.74 25.10 5 10 -2 411.38 24.05 5 -10 2 362.32 24.58 5 -10 2 381.79 24.47 5 10 -1 18.81 4.24 5 10 -1 16.66 3.68 5 -10 1 17.31 4.29 5 -10 1 9.87 3.22 5 10 0 1361.41 72.60 5 10 0 1549.90 72.38 5 -10 0 1324.31 72.42 5 10 1 21.33 3.94 5 -10 -1 15.70 4.15 5 -10 -2 362.05 23.98 5 -10 -2 382.19 24.24 5 -10 -3 123.17 11.46 5 -10 -3 123.40 11.28 5 10 4 10.32 2.62 5 -10 -4 10.82 3.55 5 10 5 9.16 2.34 5 -10 -5 7.73 3.25 5 10 6 143.18 10.06 5 -10 -6 133.81 11.80 5 10 7 100.99 7.76 5 -10 -7 109.00 9.75 5 -10 -8 137.38 10.93 5 11 -7 228.98 13.71 5 -11 7 221.76 13.75 5 11 -6 124.48 9.45 5 -11 6 130.53 9.80 5 11 -5 72.21 7.03 5 -11 5 75.15 7.28 5 11 -4 50.25 5.94 5 -11 4 46.76 5.97 5 11 -3 225.80 15.70 5 -11 3 223.27 15.97 5 -11 3 235.90 15.49 5 11 -2 2.25 1.79 5 -11 2 2.56 1.77 5 11 -1 313.14 19.84 5 -11 1 298.21 19.52 5 -11 0 132.88 11.22 5 -11 -1 274.54 19.28 5 -11 -1 320.88 19.83 5 -11 -2 1.45 1.93 5 -11 -2 1.83 1.74 5 -11 -3 218.83 16.39 5 -11 -3 262.06 16.81 5 -11 -4 47.07 6.21 5 -11 -5 63.46 6.99 5 -11 -6 159.61 11.87 5 -11 -7 235.24 14.92 5 12 -4 23.84 3.19 5 12 -3 139.16 9.69 5 12 -2 12.53 2.51 5 -12 1 2.90 1.99 5 -12 1 0.33 1.26 5 -12 0 16.30 3.26 5 -12 0 19.76 3.36 5 -12 -1 1.86 1.71 5 -12 -1 2.79 1.70 5 -12 -2 18.21 3.44 5 -12 -3 155.53 11.26 5 -12 -4 31.50 4.12 6 0 0 207.40 15.20 6 0 -1 62.29 7.06 6 0 -1 61.90 7.17 6 0 2 10.09 2.60 6 0 2 8.82 2.88 6 0 -2 12.64 3.16 6 0 3 622.09 33.52 6 0 3 534.26 35.65 6 0 -3 588.57 33.19 6 0 -3 727.04 35.45 6 0 -3 748.57 35.73 6 0 -3 505.37 35.64 6 0 4 19.17 3.45 6 0 4 11.86 3.75 6 0 -4 19.08 3.50 6 0 -4 19.04 3.87 6 0 4 19.39 4.72 6 0 -4 14.73 4.30 6 0 5 386.69 28.11 6 0 -5 375.89 28.37 6 0 5 475.11 29.31 6 0 5 450.40 24.65 6 0 -6 137.12 11.24 6 0 6 130.96 14.25 6 0 -6 136.38 14.76 6 0 6 138.22 13.71 6 0 -6 153.22 12.07 6 0 6 161.37 11.27 6 0 -7 167.65 12.90 6 0 7 142.65 15.70 6 0 -7 138.23 15.86 6 0 7 165.62 15.21 6 0 -7 158.60 13.15 6 0 -8 284.23 19.24 6 0 -8 301.52 20.13 6 0 -9 113.14 10.20 6 0 -9 104.99 10.35 6 0 -10 400.85 23.65 6 0 -10 348.77 23.66 6 0 -11 98.91 9.63 6 0 -12 25.77 4.44 6 0 -13 8.09 2.31 6 0 -14 2.29 1.18 -6 0 14 1.69 1.03 6 0 -14 1.76 1.19 6 1 -14 84.99 6.53 -6 1 14 85.31 6.34 6 1 -13 67.80 6.27 6 1 -13 52.72 5.96 6 1 -12 254.11 17.04 6 1 -11 177.41 13.94 6 1 -10 64.35 7.83 6 1 -9 483.01 29.47 6 1 -8 677.33 38.53 6 -1 7 253.66 22.21 6 1 -7 255.78 22.85 6 1 -7 274.35 18.56 6 -1 6 682.94 44.87 6 1 -6 725.48 45.40 6 -1 6 790.78 39.73 6 -1 5 106.14 11.94 6 1 -5 83.05 10.82 6 -1 5 104.62 8.53 6 -1 4 203.26 18.13 6 1 -4 227.87 15.75 6 1 -4 195.53 17.74 6 -1 4 244.61 15.42 6 -1 3 667.39 33.51 6 -1 3 545.70 35.93 6 1 -3 551.73 32.88 6 1 -3 695.99 34.69 6 -1 3 616.68 39.15 6 1 -2 462.87 25.93 6 1 -2 475.39 27.12 6 -1 2 437.57 30.60 6 1 -1 140.63 10.71 6 -1 1 138.69 14.09 6 1 -1 153.30 11.99 6 1 -1 165.73 12.48 6 -1 1 163.49 12.88 6 1 0 24.12 3.59 6 -1 0 16.44 4.66 6 -1 0 28.65 4.86 6 1 1 155.94 11.77 6 1 1 159.41 11.01 6 1 1 125.15 12.35 6 -1 -1 146.24 14.20 6 -1 -1 166.48 12.67 6 -1 -1 186.38 13.23 6 1 2 440.96 25.94 6 1 2 483.89 25.28 6 1 2 392.77 27.48 6 -1 -2 495.41 27.40 6 -1 -2 347.81 28.05 6 -1 -2 530.55 27.82 6 1 3 581.92 32.41 6 1 3 691.71 31.97 6 1 3 495.35 33.89 6 -1 -3 737.40 34.65 6 1 3 583.26 35.93 6 -1 -3 399.12 33.95 6 1 4 245.45 16.32 6 1 4 192.58 17.46 6 -1 -4 201.23 18.38 6 1 4 227.22 18.91 6 1 5 105.37 8.81 6 1 5 81.03 10.19 6 -1 -5 71.69 10.18 6 1 5 95.68 10.99 6 -1 -5 115.13 9.59 6 -1 -6 676.86 37.34 6 1 6 571.12 40.05 6 -1 -6 622.71 41.69 6 1 6 721.11 41.56 6 -1 -6 722.67 38.33 6 1 6 754.94 37.31 6 -1 -7 244.50 17.69 6 1 7 247.65 20.84 6 -1 -7 236.79 21.51 6 1 7 255.39 20.32 6 -1 -7 275.22 18.52 6 1 7 315.25 17.83 6 -1 -8 725.33 39.89 6 1 8 676.22 42.20 6 -1 -8 686.78 39.89 6 1 8 753.76 38.55 6 -1 -9 471.89 28.53 6 1 9 475.19 30.97 6 -1 -9 481.34 28.91 6 -1 -10 58.28 7.03 6 -1 -10 63.28 7.59 6 -1 -11 188.59 13.29 6 -1 -11 151.58 12.80 6 -1 -12 208.57 14.65 6 -1 -13 43.76 5.15 6 -1 -14 82.61 6.07 -6 -1 14 79.00 5.83 6 2 -14 50.69 4.47 -6 2 14 46.96 4.22 6 2 -13 5.10 1.70 6 2 -13 5.43 2.00 6 2 -12 27.57 4.34 6 2 -12 25.62 4.45 6 2 -11 277.48 18.87 6 2 -10 69.63 8.20 6 2 -9 269.11 19.08 6 2 -8 236.94 17.31 6 -2 7 240.42 21.30 6 2 -7 217.08 19.99 6 2 -7 220.90 16.29 6 -2 6 468.58 33.15 6 2 -6 486.72 32.62 6 -2 5 293.27 23.38 6 2 -5 280.76 19.14 6 2 -5 265.81 21.83 6 -2 5 348.45 19.15 6 2 -4 245.24 17.74 6 2 -4 257.16 20.38 6 -2 4 302.59 17.87 6 -2 3 236.30 20.29 6 2 -3 225.76 15.59 6 2 -3 197.57 17.23 6 2 -3 238.49 16.09 6 -2 3 250.47 17.78 6 -2 3 276.72 15.83 6 -2 2 509.25 35.33 6 2 -2 543.57 30.69 6 2 -2 473.27 32.92 6 2 -2 574.08 31.66 6 2 -2 607.72 30.79 6 -2 2 633.57 33.65 6 2 -1 138.83 10.18 6 2 -1 104.63 11.37 6 2 -1 136.58 10.89 6 2 -1 153.63 10.34 6 -2 1 145.52 11.78 6 -2 1 84.17 11.58 6 -2 0 4.85 2.63 6 2 0 3.47 1.54 6 2 0 3.11 2.02 6 2 0 1.75 1.74 6 -2 0 0.48 1.99 6 2 0 2.71 2.01 6 2 0 3.02 1.54 6 -2 0 2.45 1.87 6 2 1 141.21 10.02 6 2 1 96.30 10.81 6 2 1 120.91 10.38 6 -2 -1 137.03 11.28 6 2 1 147.49 10.13 6 -2 -1 169.90 12.16 6 -2 -1 77.84 11.02 6 -2 -2 589.46 37.16 6 2 2 625.09 31.89 6 2 2 532.24 34.76 6 -2 -2 654.22 34.08 6 2 2 596.22 35.79 6 2 2 624.23 32.02 6 2 2 576.02 32.90 6 -2 -3 203.67 18.44 6 2 3 241.58 14.86 6 2 3 189.50 16.99 6 2 3 186.88 16.30 6 -2 -3 282.28 17.27 6 2 3 236.62 18.45 6 2 3 259.21 15.26 6 2 3 226.62 15.82 6 2 4 244.19 17.18 6 2 4 319.28 17.17 6 2 4 185.90 18.02 6 -2 -4 386.45 20.37 6 2 4 258.62 20.06 6 -2 -4 211.95 19.07 6 2 5 284.09 17.83 6 2 5 224.14 19.18 6 -2 -5 289.87 21.54 6 2 5 260.72 20.41 6 2 6 516.63 27.96 6 2 6 396.02 29.84 6 -2 -6 416.33 31.09 6 2 6 485.29 31.41 6 -2 -6 550.30 29.18 6 2 7 196.74 18.17 6 -2 -7 196.37 18.97 6 2 7 225.84 18.93 6 -2 -7 248.18 16.96 6 2 7 263.51 16.10 6 -2 -8 243.28 17.67 6 2 8 227.03 19.78 6 -2 -8 254.35 18.13 6 2 8 299.35 17.46 6 -2 -9 270.53 18.25 6 2 9 245.17 20.09 6 -2 -9 253.22 18.06 6 -2 -10 65.89 7.35 6 2 10 63.92 8.88 6 -2 -10 60.35 7.39 6 -2 -11 254.34 17.53 6 2 11 313.47 21.10 6 -2 -11 264.43 18.14 6 -2 -12 23.11 3.79 6 -2 -12 26.47 4.25 6 -2 -13 4.20 1.71 6 3 -13 144.72 9.83 6 3 -12 47.38 5.38 6 3 -12 45.41 5.74 6 3 -11 284.08 17.58 6 3 -11 241.22 17.53 6 3 -10 315.96 19.71 6 3 -10 271.91 19.57 6 3 -9 109.69 9.95 6 3 -9 84.95 9.30 6 3 -8 140.66 11.81 6 3 -8 124.16 11.49 6 3 -7 43.23 6.10 6 -3 6 318.33 25.84 6 3 -6 320.09 20.73 6 3 -5 815.34 43.82 6 3 -4 40.17 5.43 6 3 -3 96.06 8.64 6 3 -3 72.74 9.43 6 -3 3 66.83 10.39 6 3 -2 625.09 34.83 6 -3 2 691.84 42.07 6 3 -2 760.30 34.73 6 3 -1 424.28 26.00 6 3 -1 455.10 25.17 6 3 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91.77 7.87 6 4 3 58.14 8.43 6 4 3 100.96 7.39 6 4 3 76.40 9.77 6 4 3 81.76 8.84 6 -4 -3 59.02 10.35 6 4 4 265.04 16.10 6 4 4 246.42 17.32 6 4 5 29.80 4.99 6 4 5 20.18 5.20 6 4 6 115.06 10.17 6 4 6 118.35 9.76 6 4 6 89.75 11.62 6 4 7 112.60 9.73 6 4 7 105.65 12.67 6 -4 -7 120.98 10.90 6 4 8 625.44 34.45 6 4 8 552.79 38.69 6 -4 -8 678.25 36.22 6 4 9 61.41 9.19 6 4 9 61.82 6.61 6 -4 -9 52.81 6.92 6 4 10 167.75 12.31 6 4 10 179.97 16.00 6 -4 -10 166.36 13.01 6 4 11 5.94 2.14 6 4 11 8.60 3.40 6 -4 -11 5.41 2.21 6 4 12 111.65 10.27 6 -4 -12 92.99 8.19 6 4 13 86.74 7.90 6 5 -12 104.44 7.32 6 -5 12 86.70 6.97 6 -5 11 52.22 5.40 6 -5 10 368.58 21.69 6 5 -9 226.44 14.95 6 -5 9 213.67 14.91 6 5 -8 90.16 8.35 6 -5 8 79.91 8.04 6 5 -7 54.32 6.30 6 -5 7 39.39 5.67 6 5 -6 160.32 12.23 6 -5 6 138.13 11.77 6 5 -5 494.69 28.73 6 -5 5 487.35 28.79 6 5 -4 117.75 10.20 6 5 -4 93.42 9.19 6 5 -3 153.08 12.41 6 5 -3 139.49 12.21 6 5 -2 169.43 14.59 6 -5 2 143.02 17.49 6 5 -2 174.84 13.62 6 5 -2 198.95 13.97 6 5 -2 109.39 13.96 6 5 -2 261.84 13.29 6 -5 2 185.93 15.39 6 5 -1 2.29 1.89 6 5 -1 1.21 1.71 6 -5 1 1.19 2.73 6 5 -1 2.64 1.75 6 5 -1 0.79 1.29 6 5 -1 1.43 1.68 6 -5 1 3.32 2.64 6 5 0 299.28 21.21 6 -5 0 204.20 23.79 6 5 0 246.42 18.74 6 5 0 343.02 19.96 6 5 0 218.89 20.91 6 5 0 456.30 19.39 6 5 0 307.87 19.57 6 -5 0 327.26 22.55 6 5 1 0.42 1.37 6 5 1 -0.60 1.55 6 5 1 0.44 1.35 6 -5 -1 -1.20 3.38 6 5 1 2.03 1.74 6 5 1 2.35 2.37 6 5 1 4.95 2.07 6 -5 -1 -0.67 2.02 6 5 2 178.25 13.17 6 5 2 168.29 13.26 6 -5 -2 137.34 17.37 6 5 2 195.24 13.35 6 5 2 122.45 14.27 6 5 2 244.51 12.74 6 5 2 162.45 14.31 6 -5 -2 204.70 16.08 6 5 3 161.55 13.31 6 -5 -3 164.44 18.54 6 5 3 181.67 13.06 6 5 3 132.14 13.36 6 5 4 124.46 11.49 6 5 5 528.57 31.16 6 5 5 523.99 34.37 6 5 6 139.59 11.36 6 5 6 153.30 15.24 6 5 7 51.91 6.19 6 5 7 41.01 7.74 6 -5 -7 60.51 7.33 6 5 8 91.56 8.61 6 5 8 84.21 11.35 6 -5 -8 103.21 9.72 6 5 9 230.27 15.80 6 5 9 259.40 20.38 6 -5 -9 242.88 16.91 6 5 10 376.47 22.88 6 5 10 412.00 27.38 6 -5 -10 412.02 24.02 6 5 11 56.79 5.69 6 5 11 54.08 7.44 6 -5 -11 53.84 6.08 6 5 12 120.07 10.48 6 -6 12 2.06 1.03 6 -6 11 194.86 12.42 6 6 -10 23.92 3.56 6 -6 10 29.24 4.12 6 6 -9 70.28 6.79 6 -6 9 76.51 7.39 6 -6 8 68.96 7.37 6 6 -8 67.68 6.90 6 6 -7 289.07 17.78 6 -6 7 242.67 17.59 6 6 -6 79.50 7.89 6 -6 6 66.02 7.68 6 6 -5 150.48 12.03 6 -6 5 143.31 12.14 6 6 -4 253.56 17.61 6 -6 4 255.31 17.82 6 6 -3 196.02 14.35 6 -6 3 164.94 13.52 6 -6 3 177.36 15.26 6 6 -2 59.91 6.87 6 6 -2 41.42 6.77 6 -6 2 55.67 10.36 6 6 -2 29.40 6.78 6 -6 2 44.03 6.06 6 -6 2 45.92 7.29 6 6 -1 152.82 14.39 6 6 -1 163.84 13.18 6 6 -1 186.33 13.36 6 6 -1 111.65 14.35 6 -6 1 155.22 13.06 6 6 -1 163.63 13.35 6 -6 1 150.13 18.61 6 -6 1 174.40 15.50 6 6 0 34.35 6.02 6 6 0 34.12 5.20 6 -6 0 29.16 7.91 6 6 0 45.89 5.66 6 6 0 21.60 5.96 6 -6 0 29.12 5.00 6 6 0 28.35 4.90 6 -6 0 26.94 5.82 6 6 1 166.51 14.63 6 6 1 171.49 13.35 6 6 1 156.19 13.10 6 6 1 194.12 13.35 6 6 1 111.18 14.39 6 -6 -1 119.79 17.22 6 -6 -1 163.08 15.19 6 6 2 38.93 6.34 6 6 2 45.70 6.22 6 -6 -2 47.45 9.87 6 6 2 61.66 6.36 6 6 2 31.76 6.97 6 6 2 56.22 6.68 6 -6 -2 41.67 6.95 6 6 3 185.21 15.30 6 6 3 160.31 13.84 6 6 3 220.76 14.28 6 -6 -3 226.64 16.92 6 6 4 248.40 18.06 6 6 5 148.09 12.41 6 6 6 70.49 7.51 6 6 6 90.93 10.97 6 6 7 270.47 18.17 6 6 7 308.49 23.05 6 -6 -7 287.32 19.50 6 6 8 72.64 7.24 6 -6 -8 67.68 8.39 6 6 8 68.42 9.56 6 -6 -8 80.63 8.23 6 6 9 68.34 6.92 6 6 9 75.54 9.68 6 -6 -9 73.25 7.67 6 6 10 23.12 3.67 6 6 10 24.70 5.21 6 -6 -10 26.43 4.22 6 6 11 191.84 12.72 6 6 11 230.63 15.77 6 6 12 4.07 1.81 6 -7 11 23.01 3.02 6 -7 10 101.02 7.99 6 7 -9 13.79 2.70 6 -7 9 16.98 3.30 6 7 -8 54.78 5.67 6 -7 8 41.90 5.67 6 7 -7 97.61 8.68 6 -7 7 121.21 10.22 6 -7 6 64.00 7.51 6 7 -6 64.35 6.86 6 -7 5 166.84 13.82 6 7 -5 193.95 13.73 6 -7 4 467.71 29.67 6 7 -4 537.74 29.71 6 7 -3 659.25 34.10 6 -7 3 600.28 35.65 6 7 -2 51.31 6.54 6 7 -2 34.85 6.53 6 7 -2 43.06 6.11 6 -7 2 34.80 5.68 6 -7 2 51.73 7.65 6 7 -1 452.37 28.85 6 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158.10 13.79 6 9 -3 168.82 12.79 6 -9 3 163.85 13.11 6 -9 3 138.25 12.29 6 -9 3 177.27 13.80 6 9 -2 140.18 12.43 6 9 -2 135.73 11.28 6 -9 2 128.96 11.47 6 9 -2 134.17 10.66 6 -9 2 103.36 10.95 6 9 -1 270.34 20.67 6 -9 1 311.09 21.44 6 9 0 104.49 10.40 6 9 0 116.70 10.33 6 -9 0 99.26 10.57 6 9 1 316.25 20.26 6 9 1 292.27 20.33 6 -9 -1 295.11 21.02 6 9 2 123.06 10.93 6 -9 -2 109.84 10.90 6 -9 -2 131.10 11.82 6 -9 -3 144.44 12.57 6 9 4 341.94 20.06 6 -9 -4 290.20 20.96 6 9 5 169.42 11.94 6 -9 -5 154.05 13.23 6 9 6 58.77 5.98 6 -9 -6 62.36 7.39 6 9 7 167.98 11.12 6 -9 -7 181.21 13.17 6 -9 -7 146.39 11.33 6 9 8 15.62 2.67 6 9 9 98.31 6.98 6 10 -7 71.69 6.33 6 10 -7 78.35 5.95 6 10 -6 68.91 6.61 6 10 -6 62.60 5.64 6 10 -5 48.20 5.74 6 10 -5 39.47 4.55 6 -10 5 38.41 4.93 6 10 -4 207.90 14.83 6 10 -4 209.92 13.60 6 -10 4 195.24 13.99 6 10 -3 95.70 9.28 6 10 -3 97.76 8.40 6 10 -2 180.54 13.97 6 10 -2 179.76 12.97 6 10 -1 115.38 10.51 6 10 -1 128.64 10.30 6 -10 1 113.72 10.37 6 10 0 48.14 6.14 6 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0 5 1362.65 63.23 7 0 -6 24.01 4.59 7 0 6 28.71 4.36 7 0 -7 347.72 23.45 7 0 -7 341.11 23.11 7 0 -8 1.63 2.25 7 0 -8 7.38 2.90 7 0 -9 5.21 2.25 7 0 -9 5.19 2.53 7 0 -10 129.78 10.89 7 0 -10 118.73 10.72 7 0 -11 11.09 2.79 7 0 -11 7.59 2.55 7 0 -12 64.85 5.96 7 0 -12 47.06 5.56 7 0 -13 34.94 3.68 7 0 -13 31.26 3.87 7 1 -13 8.17 1.79 7 1 -13 6.61 1.76 7 1 -12 111.03 8.42 7 1 -12 92.45 8.14 7 1 -11 38.53 5.17 7 1 -11 34.62 5.04 7 1 -10 162.60 12.13 7 1 -10 115.80 10.77 7 1 -9 66.97 7.72 7 1 -9 54.70 7.09 7 1 -8 236.04 16.77 7 1 -8 198.85 15.55 7 1 -7 421.41 26.36 7 1 -6 147.51 12.31 7 -1 6 139.11 10.97 7 -1 5 370.57 29.43 7 1 -5 424.61 26.51 7 1 -4 1840.03 98.40 7 1 -4 2165.67 100.29 7 -1 4 2054.56 98.14 7 1 -3 471.21 29.77 7 1 -3 538.68 29.96 7 -1 3 552.90 33.47 7 -1 3 537.94 30.02 7 1 -2 34.34 4.82 7 1 -2 35.63 5.50 7 1 -2 29.87 4.50 7 1 -2 32.81 5.28 7 -1 2 36.57 6.20 7 1 -1 863.00 46.00 7 1 -1 899.18 47.99 7 1 -1 845.48 46.02 7 1 -1 903.24 48.27 7 -1 1 955.79 49.30 7 1 0 160.57 11.94 7 -1 0 163.58 13.65 7 1 0 170.31 13.62 7 1 0 159.62 12.18 7 -1 0 169.79 14.03 7 1 0 193.65 14.82 7 1 1 857.77 46.94 7 1 1 926.91 46.35 7 -1 -1 938.25 48.91 7 1 1 856.71 46.45 7 -1 -1 906.44 48.56 7 1 1 877.88 49.42 7 1 2 30.26 4.76 7 1 2 34.63 4.59 7 -1 -2 43.01 6.12 7 1 2 36.72 5.14 7 -1 -2 36.88 5.72 7 1 3 465.04 29.32 7 1 3 449.31 32.39 7 1 4 1903.45 96.97 7 1 4 1694.36 100.47 7 1 5 435.31 25.26 7 1 5 403.75 28.98 7 1 6 133.27 13.98 7 -1 -6 138.41 11.73 7 1 6 138.76 10.97 7 1 7 383.66 28.05 7 -1 -7 395.80 25.47 7 1 7 451.11 24.86 7 1 8 201.25 17.87 7 -1 -8 204.94 15.91 7 1 8 244.65 15.41 7 -1 -9 46.85 6.17 7 -1 -9 55.41 6.92 7 -1 -10 130.40 10.77 7 -1 -10 135.94 11.34 7 -1 -11 41.59 5.07 7 -1 -11 31.57 4.84 7 -1 -12 113.18 8.39 7 -1 -12 101.86 8.56 7 -1 -13 10.32 2.14 7 2 -13 112.04 7.58 7 2 -12 4.66 1.71 7 2 -12 4.48 1.81 7 2 -11 85.41 7.59 7 2 -11 65.77 7.09 7 2 -10 309.52 19.47 7 2 -10 279.93 18.94 7 2 -9 36.19 5.87 7 2 -9 39.26 5.75 7 2 -8 104.67 10.19 7 2 -7 320.43 21.39 7 2 -6 14.58 3.59 7 2 -5 15.33 3.61 7 2 -4 92.88 9.26 7 -2 4 107.51 11.16 7 -2 4 124.63 9.76 7 2 -3 207.04 15.89 7 2 -3 253.80 17.23 7 2 -3 256.51 15.93 7 -2 3 278.13 19.26 7 2 -2 31.16 4.65 7 2 -2 35.52 5.39 7 -2 2 31.12 7.31 7 2 -2 37.47 4.95 7 -2 2 35.36 6.06 7 2 -1 329.64 20.69 7 2 -1 352.51 22.30 7 -2 1 352.09 23.00 7 2 -1 397.93 21.13 7 -2 1 374.17 23.44 7 2 0 0.95 1.45 7 2 0 0.39 1.19 7 -2 0 1.13 1.95 7 2 0 -0.54 2.21 7 -2 0 1.01 2.59 7 2 0 0.74 1.48 7 -2 0 -0.56 1.43 7 2 0 1.15 1.87 7 2 1 342.80 22.41 7 2 1 379.93 21.78 7 -2 -1 360.36 23.43 7 2 1 328.77 22.97 7 -2 -1 292.05 26.08 7 2 1 381.91 21.75 7 -2 -1 425.56 24.36 7 2 2 31.25 5.02 7 2 2 34.38 4.66 7 -2 -2 40.45 5.98 7 -2 -2 29.01 6.78 7 2 2 40.55 5.11 7 2 3 221.60 16.55 7 -2 -3 185.67 19.49 7 2 3 270.73 16.26 7 2 3 208.74 19.12 7 -2 -3 277.94 18.24 7 2 3 270.14 16.39 7 2 4 94.60 9.45 7 2 4 101.32 12.05 7 2 5 18.84 3.79 7 2 5 23.54 5.76 7 -2 -5 14.93 3.57 7 2 6 11.93 3.12 7 2 6 8.39 3.88 7 -2 -6 9.84 3.06 7 2 7 342.37 25.30 7 -2 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12.80 7 3 3 160.22 11.98 7 -3 -3 159.36 17.38 7 3 3 186.35 12.03 7 3 4 341.38 21.88 7 3 4 321.05 24.78 7 3 5 163.39 13.17 7 3 5 162.05 15.93 7 -3 -5 172.21 13.52 7 3 6 86.32 8.44 7 3 6 60.00 9.59 7 -3 -6 88.85 8.98 7 3 7 7.36 2.59 7 3 7 3.45 3.28 7 -3 -7 2.10 2.01 7 3 8 316.51 24.33 7 -3 -8 312.95 21.18 7 3 8 345.95 20.33 7 3 9 158.87 14.96 7 -3 -9 152.96 12.44 7 3 10 129.30 12.31 7 -3 -10 105.17 9.66 7 -3 -11 110.93 9.19 7 -3 -12 195.18 12.61 7 4 -12 13.77 2.27 7 4 -12 15.33 2.31 7 4 -11 42.74 4.72 7 4 -11 51.54 5.05 7 4 -10 101.43 8.44 7 4 -9 68.18 7.06 7 4 -8 383.77 23.34 7 4 -7 101.62 9.53 7 4 -6 83.80 8.51 7 4 -5 92.20 8.97 7 4 -5 86.50 8.69 7 4 -4 98.32 9.36 7 4 -4 105.13 9.51 7 4 -3 478.07 29.38 7 4 -3 454.67 29.22 7 4 -2 57.00 7.33 7 4 -2 53.24 6.42 7 4 -2 50.92 6.38 7 4 -2 48.88 8.04 7 -4 2 46.85 9.78 7 4 -2 67.57 6.18 7 4 -1 577.11 34.20 7 4 -1 605.48 32.92 7 4 -1 596.71 32.61 7 4 -1 716.33 32.06 7 -4 1 572.67 41.18 7 4 0 103.79 10.44 7 4 0 107.47 9.34 7 4 0 74.13 10.25 7 4 0 127.96 8.85 7 -4 0 88.35 13.64 7 4 1 590.88 34.70 7 4 1 617.25 32.95 7 4 1 704.74 32.17 7 -4 -1 610.98 42.30 7 4 2 52.73 6.97 7 4 2 65.33 6.51 7 4 2 22.18 5.60 7 -4 -2 23.27 7.06 7 4 2 74.09 6.15 7 4 3 580.53 31.37 7 4 3 616.87 30.20 7 4 4 114.82 10.58 7 4 4 95.01 11.96 7 4 5 92.54 9.32 7 4 5 89.36 11.60 7 4 6 111.37 9.71 7 4 6 83.66 11.22 7 -4 -6 91.71 9.41 7 4 7 104.84 13.00 7 -4 -7 134.04 11.43 7 4 7 134.88 10.65 7 4 8 312.14 24.64 7 -4 -8 359.81 22.13 7 4 9 78.93 10.01 7 -4 -9 77.72 8.05 7 4 10 97.28 10.53 7 -4 -10 92.80 8.51 7 4 11 51.21 6.71 7 -4 -11 45.45 5.25 7 -4 -12 14.49 2.54 7 5 -11 95.92 7.11 7 5 -10 2.58 1.44 7 5 -10 1.36 1.09 7 5 -9 168.95 11.80 7 5 -9 168.74 11.69 7 5 -8 192.19 13.35 7 5 -8 190.44 13.31 7 5 -7 106.75 9.13 7 5 -7 90.35 8.61 7 5 -6 6.68 2.63 7 5 -6 8.36 2.69 7 5 -5 33.07 5.11 7 5 -5 39.78 5.52 7 5 -4 111.69 9.98 7 5 -4 107.34 9.80 7 5 -3 109.43 10.07 7 5 -3 82.25 10.01 7 5 -3 108.16 9.90 7 5 -2 632.59 35.74 7 5 -2 555.03 36.61 7 5 -2 515.04 34.54 7 5 -2 625.12 35.56 7 5 -1 335.49 21.93 7 5 -1 313.79 23.26 7 5 -1 299.57 21.39 7 5 -1 360.46 22.23 7 5 0 41.53 6.66 7 5 0 37.61 5.48 7 5 0 42.34 5.66 7 5 0 49.87 5.18 7 5 0 39.73 5.50 7 5 1 279.57 20.70 7 5 1 320.35 23.18 7 5 1 304.16 21.34 7 5 2 557.93 35.57 7 5 2 617.84 35.50 7 5 2 569.04 37.16 7 5 3 97.02 10.84 7 5 3 123.63 10.40 7 5 4 112.57 10.76 7 5 5 49.59 6.40 7 5 5 31.55 4.93 7 5 5 42.92 7.83 7 5 6 7.88 2.73 7 5 6 7.67 2.34 7 5 6 8.72 4.02 7 -5 -6 6.81 2.77 7 5 7 100.14 8.64 7 5 7 90.80 11.68 7 -5 -7 102.18 9.71 7 5 8 179.53 12.62 7 5 8 177.57 16.38 7 -5 -8 190.90 13.91 7 5 9 165.56 11.81 7 5 9 176.50 15.60 7 -5 -9 192.14 13.30 7 5 10 1.67 1.28 7 5 10 1.18 2.14 7 -5 -10 1.81 1.56 7 -5 -11 78.19 6.78 7 6 -11 15.96 2.17 7 6 -10 7.90 1.88 7 6 -9 49.03 5.06 7 6 -8 43.45 5.04 7 6 -7 56.81 6.20 7 6 -6 207.32 14.53 7 6 -6 214.20 14.33 7 6 -5 32.79 5.13 7 6 -5 33.76 4.77 7 6 -4 364.95 22.85 7 6 -4 317.45 23.69 7 6 -3 167.95 14.48 7 6 -3 164.87 12.97 7 6 -3 156.63 12.78 7 6 -3 167.03 12.68 7 6 -2 110.92 9.92 7 6 -2 105.48 11.08 7 6 -2 88.43 9.12 7 6 -2 107.70 9.54 7 6 -1 26.62 4.69 7 6 -1 19.92 4.83 7 6 -1 22.39 4.28 7 6 -1 33.94 4.99 7 6 0 4.28 2.25 7 6 0 4.55 2.48 7 6 0 2.37 1.81 7 6 0 4.00 2.11 7 6 1 26.82 4.71 7 6 1 21.45 4.94 7 6 1 24.76 4.50 7 6 1 31.27 4.74 7 6 2 89.09 9.95 7 6 2 93.81 9.23 7 6 2 118.33 9.65 7 6 3 163.57 13.73 7 6 4 370.93 23.75 7 6 5 25.96 4.58 7 6 5 27.96 4.36 7 6 6 229.12 14.89 7 6 6 177.41 13.59 7 6 6 214.61 17.99 7 -6 -6 219.50 15.67 7 6 7 65.86 6.50 7 6 7 66.33 9.17 7 -6 -7 66.15 7.47 7 6 8 51.64 5.57 7 6 8 57.29 8.14 7 -6 -8 60.52 6.60 7 6 9 43.26 4.75 7 6 9 48.65 7.01 7 -6 -9 51.44 5.82 7 6 10 7.85 1.92 7 6 10 7.18 2.65 7 -6 -10 7.36 2.11 7 -6 -11 16.07 2.53 7 7 -10 11.73 1.87 7 7 -10 12.97 2.18 7 7 -9 169.65 10.38 7 -7 9 155.83 10.44 7 7 -8 111.81 8.08 7 -7 8 96.42 8.05 7 7 -7 104.76 8.57 7 -7 7 126.22 9.49 7 7 -6 60.96 6.32 7 -7 6 65.99 6.89 7 7 -5 350.05 21.25 7 7 -5 354.29 21.81 7 -7 5 350.81 21.75 7 7 -4 256.84 16.37 7 7 -4 238.10 17.90 7 7 -4 224.90 16.04 7 -7 4 212.96 15.85 7 7 -3 110.60 9.68 7 7 -3 114.20 11.27 7 7 -3 96.58 9.26 7 -7 3 89.65 9.13 7 7 -2 490.80 28.44 7 7 -2 484.50 30.55 7 7 -2 468.37 28.24 7 7 -1 57.09 6.76 7 7 -1 46.46 7.02 7 7 -1 41.57 5.95 7 7 0 11.56 3.30 7 7 0 6.32 3.02 7 7 0 11.48 3.27 7 7 1 45.77 6.92 7 7 1 43.35 6.03 7 7 1 56.38 6.21 7 7 2 468.20 28.85 7 7 3 84.15 8.91 7 7 4 222.34 15.85 7 7 5 320.09 19.98 7 7 5 320.03 19.61 7 7 6 57.89 6.07 7 -7 -6 60.95 7.23 7 7 7 131.47 9.81 7 -7 -7 133.42 10.81 7 7 8 104.31 8.07 7 -7 -8 110.34 9.06 7 7 9 186.84 11.76 7 -7 -9 195.91 12.68 7 7 10 14.92 2.20 7 -7 -10 12.34 2.27 7 8 -9 19.02 2.59 7 8 -8 82.13 6.44 7 -8 8 67.78 5.99 7 8 -8 74.88 5.78 7 8 -7 68.73 5.94 7 8 -7 71.11 6.42 7 -8 7 71.53 6.49 7 8 -6 142.90 10.56 7 -8 6 149.06 10.74 7 8 -6 134.79 9.79 7 8 -5 67.82 6.44 7 8 -5 61.29 7.49 7 8 -5 74.54 7.11 7 -8 5 62.81 6.73 7 8 -4 50.70 5.68 7 8 -4 50.83 7.02 7 8 -4 55.87 6.22 7 -8 4 42.03 5.66 7 8 -3 22.50 4.08 7 8 -3 29.40 5.33 7 8 -3 16.07 3.62 7 8 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135.62 11.53 8 1 -6 268.69 18.54 8 -1 6 281.42 19.80 8 1 -5 731.70 41.06 8 -1 5 781.22 43.52 8 -1 4 18.17 3.62 8 1 -4 12.65 3.25 8 -1 4 14.46 4.12 8 1 -3 49.91 6.31 8 1 -3 68.94 7.95 8 1 -3 62.41 6.46 8 -1 3 50.49 7.57 8 1 -2 427.08 26.68 8 1 -2 530.66 29.34 8 -1 2 451.72 29.51 8 1 -2 446.15 26.60 8 1 -2 509.82 28.95 8 -1 2 473.00 29.95 8 1 -1 981.33 51.44 8 1 -1 1089.64 54.29 8 -1 1 1035.02 54.72 8 1 -1 959.73 51.27 8 1 -1 942.03 53.26 8 -1 1 1000.67 54.39 8 1 0 29.08 4.42 8 -1 0 28.42 5.45 8 1 0 29.94 5.38 8 1 0 22.49 4.05 8 -1 0 30.70 5.68 8 1 0 26.47 5.24 8 -1 -1 1104.32 56.67 8 1 1 1037.29 56.47 8 1 1 995.76 53.71 8 -1 -1 1150.35 56.91 8 1 1 973.02 56.35 8 1 2 456.75 26.82 8 1 2 404.25 28.24 8 1 2 468.90 26.74 8 1 2 412.77 28.86 8 1 3 43.95 5.98 8 -1 -3 67.72 7.91 8 1 3 57.89 6.43 8 1 3 48.33 7.69 8 1 4 16.58 3.55 8 1 4 18.56 4.86 8 1 5 789.78 42.14 8 1 6 301.42 19.03 8 1 7 159.65 11.86 8 -1 -8 56.02 6.69 8 -1 -9 127.17 10.43 8 -1 -10 2.19 1.73 8 -1 -11 68.16 6.25 8 2 -11 10.02 2.11 8 2 -11 9.60 2.12 8 2 -10 71.27 6.72 8 2 -9 112.85 9.60 8 2 -8 38.92 5.50 8 2 -7 191.24 14.39 8 2 -6 169.05 13.33 8 2 -5 243.50 17.03 8 2 -4 194.61 14.28 8 -2 4 184.69 15.42 8 2 -3 82.74 8.25 8 2 -3 92.30 9.19 8 -2 3 74.19 9.40 8 2 -3 76.92 7.27 8 -2 3 89.16 9.87 8 2 -2 71.53 7.52 8 2 -2 82.54 8.66 8 -2 2 66.48 8.64 8 2 -2 73.67 7.06 8 -2 2 80.64 9.29 8 2 -1 497.81 29.47 8 2 -1 528.09 31.22 8 -2 1 508.77 32.01 8 2 -1 524.62 29.07 8 -2 1 576.04 32.70 8 2 0 1.64 1.82 8 -2 0 5.48 2.88 8 2 0 4.03 2.56 8 2 0 1.89 1.94 8 -2 0 3.61 2.76 8 2 0 3.59 2.28 8 2 1 514.75 30.80 8 2 1 527.61 29.97 8 -2 -1 555.62 32.44 8 2 1 513.77 32.11 8 2 1 564.62 30.10 8 2 1 550.57 33.18 8 2 2 64.51 7.53 8 2 2 72.96 7.33 8 -2 -2 86.02 9.08 8 2 2 84.51 9.38 8 2 2 73.84 7.21 8 2 2 80.57 9.62 8 2 3 81.43 8.31 8 2 3 90.54 8.08 8 -2 -3 98.69 9.85 8 2 3 58.15 8.43 8 2 3 101.55 8.31 8 2 3 64.80 9.15 8 2 4 208.64 15.05 8 2 5 271.54 17.96 8 -2 -6 151.66 12.73 8 2 6 186.05 12.99 8 -2 -7 165.33 14.10 8 2 7 256.44 15.15 8 -2 -8 27.84 4.61 8 -2 -9 82.28 8.02 8 -2 -10 55.62 5.99 8 -2 -11 9.61 2.29 8 3 -11 63.32 5.30 8 3 -11 63.82 5.36 8 3 -10 184.36 11.88 8 3 -10 175.79 11.97 8 3 -9 35.44 4.61 8 3 -9 41.36 5.09 8 3 -8 -0.39 1.54 8 3 -8 -0.42 1.36 8 3 -7 33.40 4.88 8 3 -7 32.76 5.15 8 3 -6 42.39 5.56 8 3 -6 40.93 5.70 8 3 -5 59.51 6.77 8 3 -5 56.71 6.77 8 3 -4 4.67 2.28 8 3 -3 5.91 2.47 8 3 -3 11.47 2.54 8 -3 3 7.20 3.02 8 3 -2 60.04 7.08 8 3 -2 72.69 8.18 8 3 -2 83.27 7.16 8 -3 2 82.79 9.26 8 3 -1 52.58 6.56 8 3 -1 66.00 7.68 8 3 -1 75.73 6.78 8 -3 1 78.82 8.83 8 3 0 305.13 21.89 8 3 0 346.07 21.47 8 3 0 356.80 22.95 8 3 0 398.02 21.27 8 3 1 73.13 7.37 8 3 1 71.14 8.25 8 3 1 65.22 7.72 8 3 1 75.08 6.96 8 3 1 70.55 8.63 8 3 2 64.67 7.58 8 3 2 72.58 7.17 8 3 2 81.43 8.88 8 3 2 78.49 7.03 8 3 3 8.12 2.76 8 3 3 8.94 2.66 8 3 3 5.89 2.89 8 3 3 9.59 2.69 8 3 4 2.47 1.80 8 3 5 60.73 7.12 8 -3 -5 63.08 7.27 8 -3 -6 40.42 5.82 8 3 6 45.44 5.77 8 -3 -7 29.93 4.96 8 3 7 33.87 4.62 8 3 8 -0.67 1.28 8 -3 -8 -0.43 1.65 8 -3 -9 31.81 4.60 8 -3 -10 156.16 11.13 8 3 11 49.30 5.29 8 -3 -11 54.38 5.11 8 4 -11 47.86 4.19 8 4 -10 96.14 7.45 8 4 -10 113.20 7.83 8 4 -9 73.43 6.63 8 4 -9 80.43 6.88 8 4 -8 51.65 5.62 8 4 -8 49.95 5.65 8 4 -7 38.23 5.12 8 4 -7 43.57 5.44 8 4 -6 2.06 1.64 8 4 -6 6.01 2.37 8 4 -5 65.92 7.04 8 4 -5 65.60 7.26 8 4 -4 278.00 18.29 8 4 -4 292.93 18.81 8 4 -3 99.64 9.50 8 4 -3 108.19 10.04 8 4 -2 66.31 7.28 8 4 -2 79.49 6.76 8 4 -1 333.81 23.62 8 4 -1 373.67 23.17 8 4 0 61.23 7.72 8 4 0 68.49 7.27 8 4 1 336.82 23.95 8 4 1 378.57 23.06 8 4 2 52.58 7.13 8 4 2 71.69 7.08 8 4 2 71.45 6.42 8 4 3 92.38 10.42 8 4 3 173.03 10.49 8 4 4 266.48 18.34 8 -4 -4 267.76 18.38 8 4 5 56.28 6.67 8 -4 -5 57.15 7.04 8 4 6 2.86 1.69 8 -4 -6 2.86 2.05 8 -4 -7 39.94 5.50 8 4 7 44.48 5.23 8 -4 -8 48.19 6.08 8 4 8 72.20 6.22 8 -4 -9 75.25 7.11 8 -4 -10 85.70 7.19 8 -4 -11 59.27 5.18 8 5 -10 37.31 3.62 8 5 -10 32.67 3.32 8 5 -9 19.01 2.93 8 5 -9 18.01 2.71 8 5 -8 71.04 6.54 8 5 -8 78.97 6.64 8 5 -7 25.80 3.96 8 5 -7 19.84 3.49 8 5 -6 377.92 22.26 8 5 -6 372.77 22.05 8 5 -5 355.23 21.44 8 5 -5 350.10 21.30 8 5 -4 17.94 3.68 8 5 -4 19.82 3.71 8 5 -3 97.26 9.66 8 5 -3 107.90 9.92 8 5 -2 157.73 13.28 8 5 -2 160.67 14.32 8 5 -2 186.63 13.92 8 5 -1 39.55 5.67 8 5 -1 56.57 7.31 8 5 -1 53.27 6.33 8 5 0 21.13 4.49 8 5 0 22.61 4.13 8 5 0 30.94 4.16 8 5 1 44.50 6.80 8 5 1 62.76 6.70 8 5 2 169.28 15.37 8 5 2 201.61 14.78 8 5 3 104.70 11.19 8 5 3 195.56 11.40 8 5 4 20.65 4.16 8 5 5 345.40 21.48 8 -5 -5 347.76 21.97 8 5 6 424.57 24.06 8 -5 -6 397.46 24.59 8 -5 -7 26.36 4.33 8 5 7 27.26 3.84 8 -5 -8 71.02 7.03 8 -5 -9 18.79 3.28 8 -5 -10 30.57 3.69 8 6 -9 30.33 3.31 8 6 -8 126.21 8.77 8 6 -7 184.73 12.19 8 6 -7 190.35 11.93 8 6 -6 40.22 4.81 8 6 -6 36.89 4.40 8 6 -5 33.00 4.53 8 6 -5 33.71 4.36 8 6 -4 128.04 10.13 8 6 -4 122.50 9.67 8 6 -3 30.66 4.60 8 6 -3 34.09 5.44 8 6 -3 35.53 4.73 8 6 -2 32.87 4.79 8 6 -2 29.16 5.28 8 6 -2 36.26 4.84 8 6 -1 21.78 3.94 8 6 -1 19.41 4.42 8 6 -1 25.04 4.15 8 6 -1 25.45 4.13 8 6 0 497.61 30.02 8 6 0 507.61 31.79 8 6 0 511.83 30.22 8 6 1 25.79 4.83 8 6 1 21.62 3.88 8 6 2 23.72 4.48 8 6 3 32.15 5.17 8 6 4 111.28 9.59 8 6 4 105.20 8.65 8 6 5 27.90 4.31 8 6 5 37.26 4.50 8 -6 -5 30.80 4.94 8 6 6 41.99 4.67 8 6 6 28.94 3.90 8 -6 -6 37.41 5.09 8 -6 -7 175.35 12.50 8 -6 -8 117.40 9.11 8 -6 -9 27.94 3.61 8 7 -8 12.82 2.12 8 7 -7 18.61 2.74 8 7 -7 20.18 3.02 8 7 -6 60.66 5.66 8 7 -6 65.90 6.15 8 7 -5 31.21 4.15 8 7 -5 40.17 4.85 8 7 -4 71.50 6.81 8 7 -4 75.72 7.17 8 7 -3 273.69 17.18 8 7 -3 258.99 18.38 8 7 -3 285.82 17.59 8 7 -2 131.86 10.47 8 7 -2 124.00 11.49 8 7 -2 135.42 10.64 8 7 -2 147.94 10.21 8 7 -1 560.94 30.75 8 7 -1 528.17 32.03 8 7 -1 485.48 30.12 8 7 0 411.56 27.57 8 7 0 433.69 26.53 8 7 1 535.54 31.09 8 7 2 123.91 10.55 8 7 3 258.56 17.04 8 7 4 79.50 7.31 8 7 4 73.82 6.69 8 7 5 27.40 3.88 8 7 5 29.07 3.84 8 -7 -5 35.70 4.84 8 7 6 58.65 5.40 8 -7 -6 67.62 6.58 8 7 7 16.34 2.47 8 -7 -7 14.80 2.95 8 7 8 10.90 1.88 8 -7 -8 17.86 2.85 8 8 -7 33.80 3.23 8 8 -6 72.60 5.84 8 8 -6 87.37 6.49 8 8 -5 -0.24 0.98 8 8 -5 1.09 1.12 8 8 -4 110.35 8.39 8 8 -4 132.99 9.93 8 8 -4 110.06 8.68 8 8 -3 18.51 3.14 8 8 -3 20.22 3.91 8 8 -3 22.41 3.52 8 8 -2 190.13 13.72 8 8 -2 176.37 12.41 8 8 -1 2.69 1.85 8 8 -1 1.73 1.44 8 8 0 221.01 15.42 8 8 1 1.62 1.54 8 8 2 180.35 12.70 8 8 3 17.91 3.13 8 8 3 16.48 2.86 8 8 4 112.13 8.07 8 8 4 94.10 7.48 8 -8 -4 97.89 8.42 8 8 5 0.69 0.91 8 -8 -5 1.63 1.50 8 8 6 80.05 5.80 8 -8 -6 62.73 6.09 8 -8 -7 28.03 3.47 8 9 -4 16.27 2.73 8 9 -4 14.92 2.43 8 9 -3 85.51 7.13 8 9 -3 76.84 6.39 8 9 -2 198.78 13.19 8 9 -1 150.39 10.87 8 9 0 87.66 7.48 8 9 1 138.99 9.92 8 9 2 170.63 10.66 8 9 2 142.15 9.88 8 9 3 80.77 6.11 8 9 3 63.75 5.58 8 9 4 13.93 2.22 8 -9 -4 12.92 2.56 8 9 5 39.59 3.52 8 -9 -5 30.96 3.74 9 0 0 0.58 1.99 9 0 0 1.70 1.75 9 0 0 1.15 2.19 9 0 -1 104.74 10.27 9 0 1 106.23 10.61 9 0 -1 99.29 8.86 9 0 1 89.16 8.65 9 0 1 95.81 10.13 9 0 -2 21.49 4.76 9 0 2 19.08 4.65 9 0 -2 16.75 3.61 9 0 2 15.66 3.37 9 0 2 19.22 4.48 9 0 3 211.62 16.34 9 0 -3 195.35 13.45 9 0 3 195.31 13.68 9 0 3 197.34 15.74 9 0 3 198.77 13.47 9 0 4 785.96 45.97 9 0 4 761.38 45.23 9 0 4 903.24 43.48 9 0 5 905.32 50.44 9 0 5 939.53 49.93 9 0 6 304.49 20.98 9 0 6 312.18 20.30 9 0 7 285.42 18.41 9 0 8 256.40 16.23 9 0 9 3.79 2.05 9 0 10 29.21 3.81 9 -1 10 1.05 1.04 9 1 -9 59.03 5.34 9 -1 9 50.80 5.81 9 1 -8 103.44 8.28 9 1 -7 200.63 13.62 9 1 -6 458.00 26.34 9 -1 6 468.56 28.23 9 -1 6 458.34 27.07 9 1 -5 199.79 13.53 9 -1 5 159.86 14.31 9 -1 5 193.33 14.40 9 1 -4 221.88 14.77 9 -1 4 196.81 16.07 9 -1 4 212.65 15.99 9 1 -3 60.38 6.57 9 -1 3 58.59 7.94 9 1 -3 73.18 6.58 9 -1 3 64.44 6.88 9 -1 3 61.22 7.77 9 -1 2 52.74 7.80 9 1 -2 71.25 6.78 9 -1 2 59.24 7.02 9 -1 2 72.69 8.58 9 1 -1 691.39 36.72 9 -1 1 585.17 36.32 9 1 -1 613.66 33.87 9 -1 1 579.47 34.77 9 1 -1 685.87 36.72 9 -1 1 656.07 37.07 9 -1 0 254.94 18.63 9 1 0 252.48 18.39 9 1 0 272.42 16.81 9 -1 0 243.95 17.37 9 1 0 268.51 18.69 9 -1 -1 683.18 36.47 9 1 1 549.31 35.31 9 1 1 608.03 33.44 9 -1 -1 642.41 34.74 9 1 1 610.68 36.03 9 -1 -2 80.03 8.54 9 1 2 61.12 8.14 9 1 2 68.55 6.74 9 -1 -2 57.69 6.83 9 1 2 67.14 8.32 9 1 3 65.51 8.46 9 1 3 85.02 7.39 9 -1 -3 81.99 7.72 9 1 3 68.03 8.51 9 1 3 71.80 7.10 9 1 4 215.87 16.59 9 1 4 196.44 16.02 9 1 4 213.45 14.11 9 1 5 197.03 15.70 9 1 5 173.91 14.76 9 1 5 211.82 13.64 9 1 6 467.87 28.18 9 1 6 432.44 27.14 9 1 7 238.24 16.49 9 1 8 97.17 8.58 9 1 9 52.47 5.99 9 1 9 53.69 5.45 9 1 10 2.17 1.39 9 2 -9 56.27 5.17 9 -2 9 48.58 5.20 9 2 -8 70.64 6.33 9 -2 8 51.55 6.07 9 2 -7 342.09 19.90 9 -2 7 309.05 20.26 9 2 -6 98.73 8.40 9 -2 6 72.10 8.13 9 2 -5 175.77 12.70 9 -2 5 159.85 13.36 9 -2 5 172.82 13.06 9 2 -4 328.28 21.09 9 -2 4 350.07 23.00 9 -2 4 382.40 22.92 9 2 -3 216.18 14.91 9 -2 3 190.82 16.04 9 2 -3 233.82 14.00 9 -2 3 222.69 15.37 9 -2 3 231.45 16.63 9 2 -2 409.40 24.85 9 2 -2 454.76 26.55 9 -2 2 415.04 27.04 9 2 -2 435.81 24.10 9 -2 2 456.34 27.38 9 2 -1 71.01 7.17 9 2 -1 78.52 8.33 9 -2 1 79.55 8.87 9 2 -1 79.15 7.01 9 2 0 74.96 7.11 9 -2 0 70.68 8.29 9 2 0 77.13 8.25 9 2 0 67.20 6.59 9 2 0 71.93 8.13 9 2 1 81.39 7.29 9 -2 -1 91.02 9.10 9 2 1 61.45 7.76 9 2 1 71.60 6.81 9 2 1 74.92 8.53 9 2 2 363.95 24.21 9 2 2 486.73 25.01 9 -2 -2 466.63 27.04 9 2 2 418.24 26.72 9 2 2 463.29 24.53 9 2 2 384.37 26.41 9 2 3 206.35 16.15 9 -2 -3 197.18 14.64 9 2 3 190.28 16.02 9 2 3 201.32 14.37 9 2 4 329.23 22.05 9 2 4 307.20 21.99 9 2 4 344.03 20.23 9 2 5 187.92 14.68 9 2 5 197.86 12.92 9 2 6 80.51 8.79 9 2 6 74.26 8.47 9 2 6 95.92 7.84 9 2 7 320.77 20.37 9 2 7 293.41 19.81 9 2 8 58.22 6.56 9 2 8 53.58 6.28 9 2 9 46.05 5.26 9 2 9 50.05 5.38 9 3 -9 6.53 1.67 9 3 -9 12.95 2.29 9 3 -8 62.44 5.84 9 3 -8 76.77 6.43 9 3 -7 16.92 3.15 9 3 -6 244.84 15.88 9 3 -5 3.10 1.73 9 3 -4 11.88 2.92 9 3 -3 15.29 3.16 9 3 -3 21.77 3.26 9 3 -2 493.67 30.45 9 3 -2 618.77 29.92 9 3 -1 794.11 39.47 9 3 -1 734.91 36.59 9 3 0 587.02 31.06 9 3 0 546.72 28.43 9 3 1 706.59 36.30 9 3 1 698.25 37.91 9 3 1 766.70 35.78 9 3 2 497.54 30.53 9 3 2 564.87 30.27 9 3 2 542.70 31.80 9 3 2 490.82 31.83 9 3 3 20.92 3.83 9 3 3 21.77 4.31 9 3 3 19.10 3.27 9 3 3 14.24 3.90 9 3 4 14.07 3.10 9 3 4 8.56 2.85 9 3 4 4.60 2.49 9 3 5 5.73 2.14 9 3 5 3.42 2.25 9 3 5 4.48 2.41 9 3 6 230.03 15.88 9 3 6 282.07 15.35 9 3 7 14.65 3.65 9 3 8 63.66 6.67 9 -3 -8 51.17 5.52 9 3 9 10.48 2.49 9 -3 -9 9.80 2.19 9 4 -9 125.53 8.04 9 4 -8 119.37 8.26 9 4 -8 117.90 8.33 9 4 -7 161.70 11.01 9 4 -7 172.88 11.36 9 4 -6 26.41 3.81 9 4 -6 34.11 4.36 9 4 -5 254.69 16.11 9 4 -4 138.70 10.58 9 4 -3 1.82 1.45 9 4 -3 3.28 1.68 9 4 -2 25.70 4.10 9 4 -2 35.02 3.97 9 4 -1 250.65 17.61 9 4 -1 339.16 17.44 9 4 0 127.76 9.81 9 4 0 158.62 9.48 9 4 1 285.43 17.57 9 4 1 355.97 17.33 9 4 2 19.55 3.85 9 4 2 34.78 4.06 9 4 3 1.63 1.55 9 4 3 4.32 1.89 9 4 3 1.55 1.97 9 4 4 139.51 10.55 9 4 4 125.71 11.52 9 4 5 223.02 17.03 9 4 5 259.58 15.69 9 4 6 22.00 4.43 9 4 6 33.36 4.08 9 4 7 140.70 11.76 9 -4 -7 147.09 10.84 9 4 7 172.12 10.57 9 4 8 92.25 8.11 9 -4 -8 86.25 7.13 9 4 9 89.83 7.17 9 5 -8 75.50 5.68 9 5 -8 74.96 5.52 9 5 -7 1.65 1.22 9 5 -7 2.91 1.33 9 5 -6 113.20 8.32 9 5 -6 110.00 8.17 9 5 -5 177.29 11.53 9 5 -5 159.67 11.14 9 5 -4 104.16 8.43 9 5 -4 114.32 8.64 9 5 -3 53.48 5.64 9 5 -2 25.81 3.81 9 5 -1 73.86 7.51 9 5 -1 81.04 7.14 9 5 0 8.56 2.67 9 5 0 7.92 2.21 9 5 1 80.03 8.09 9 5 1 96.58 7.83 9 5 2 28.79 4.52 9 5 3 53.10 5.98 9 5 4 105.69 8.70 9 5 5 165.89 12.64 9 -5 -5 152.94 11.60 9 5 5 182.32 11.61 9 5 6 85.50 8.37 9 -5 -6 86.00 7.69 9 5 7 2.87 1.13 9 5 7 0.71 1.46 9 -5 -7 1.99 1.31 9 5 8 57.10 5.46 9 -5 -8 52.88 4.99 9 6 -7 28.41 3.06 9 6 -6 4.23 1.55 9 6 -6 5.53 1.48 9 6 -5 36.44 4.17 9 6 -5 41.45 4.10 9 6 -4 86.98 7.26 9 6 -4 98.97 7.26 9 6 -3 106.87 8.38 9 6 -3 118.09 8.43 9 6 -2 70.91 6.43 9 6 -2 73.60 6.38 9 6 -1 44.79 5.54 9 6 -1 50.16 5.12 9 6 0 87.17 8.43 9 6 0 110.30 8.20 9 6 1 38.43 5.09 9 6 2 75.08 7.20 9 6 3 106.29 8.65 9 6 4 84.87 6.99 9 -6 -4 78.65 7.20 9 -6 -5 27.86 3.91 9 6 5 34.26 3.83 9 6 6 3.35 1.23 9 -6 -6 2.48 1.45 9 -6 -7 16.82 2.63 9 7 -5 3.14 1.22 9 7 -4 40.94 4.23 9 7 -3 91.14 6.54 9 7 -2 173.98 12.81 9 7 -2 224.10 12.39 9 7 -1 358.35 20.99 9 7 0 13.04 2.79 9 7 1 358.39 20.82 9 7 2 206.23 13.32 9 7 3 84.26 6.82 9 7 4 48.81 4.32 9 -7 -4 28.09 3.79 9 7 5 5.19 1.31 9 -7 -5 1.98 1.28 9 8 -2 194.01 11.96 9 8 -1 66.60 5.82 9 8 0 249.22 14.84 9 8 1 78.58 6.31 9 8 2 207.71 12.41 9 8 3 41.60 3.82 10 0 0 2.71 1.94 10 0 0 2.23 1.42 10 0 -1 98.79 9.08 10 0 1 82.88 8.49 10 0 -1 95.41 7.60 10 0 1 80.79 7.22 10 0 2 257.07 17.45 10 0 -2 248.85 15.42 10 0 2 263.76 15.67 10 0 2 257.22 17.25 10 0 3 59.10 6.96 10 0 -3 61.30 5.52 10 0 3 60.39 5.47 10 0 3 57.61 6.64 10 0 4 58.27 6.86 10 0 4 55.48 6.24 10 0 5 -0.42 1.51 10 0 5 2.85 1.73 10 0 6 642.06 37.77 10 0 6 795.14 37.71 10 0 7 55.85 5.86 10 0 7 67.70 5.71 10 -1 7 18.49 3.01 10 -1 6 109.14 8.98 10 -1 6 117.09 8.51 10 -1 5 52.27 6.06 10 -1 5 58.88 5.86 10 -1 4 163.30 12.78 10 -1 4 194.78 13.02 10 -1 3 1.75 1.82 10 1 -3 3.67 1.69 10 -1 3 4.99 1.86 10 -1 2 146.92 11.84 10 1 -2 161.08 10.28 10 -1 2 144.35 10.53 10 -1 1 67.09 7.50 10 1 -1 69.90 6.33 10 -1 1 70.41 6.80 10 -1 0 340.87 20.09 10 1 0 315.57 19.48 10 1 0 291.76 17.31 10 -1 0 271.71 17.85 10 -1 -1 88.41 8.31 10 1 1 85.98 8.20 10 1 1 71.14 6.26 10 1 2 134.56 11.38 10 1 2 168.18 10.19 10 -1 -2 134.13 10.16 10 1 2 132.88 11.25 10 1 3 3.15 2.01 10 1 3 7.01 2.01 10 -1 -3 2.22 1.50 10 1 3 3.87 1.92 10 1 4 196.60 13.49 10 1 4 149.68 12.08 10 1 5 57.50 6.41 10 1 5 44.52 5.48 10 1 6 132.86 10.04 10 1 6 108.57 8.90 10 1 7 22.18 3.47 10 1 7 24.25 3.37 10 2 -7 96.36 6.86 10 -2 7 102.75 7.48 10 2 -6 55.24 5.02 10 -2 6 53.40 5.42 10 2 -5 44.79 4.65 10 -2 5 42.95 5.13 10 2 -4 102.00 7.75 10 -2 4 89.12 8.19 10 2 -3 244.58 16.47 10 -2 3 261.80 17.79 10 -2 3 291.37 17.02 10 2 -2 200.47 13.42 10 -2 2 204.23 14.77 10 2 -2 245.92 13.33 10 -2 2 214.89 14.11 10 2 -1 69.37 6.43 10 -2 1 91.95 8.31 10 2 -1 88.75 6.59 10 -2 1 70.34 7.15 10 2 0 132.57 9.55 10 -2 0 152.91 11.44 10 2 0 126.25 10.65 10 2 0 138.41 9.31 10 -2 0 132.78 10.44 10 2 1 84.23 7.93 10 2 1 84.06 6.56 10 -2 -1 74.29 7.23 10 2 1 68.46 7.40 10 2 2 217.54 15.12 10 2 2 244.72 13.59 10 -2 -2 226.03 14.51 10 2 2 191.77 14.69 10 2 3 292.08 18.57 10 -2 -3 291.96 17.19 10 2 3 263.41 18.12 10 2 3 245.32 16.41 10 2 4 114.30 9.50 10 2 4 100.61 9.10 10 2 4 115.64 8.26 10 2 5 43.50 5.23 10 2 5 33.15 4.71 10 2 6 63.20 6.15 10 2 6 54.24 5.76 10 2 7 102.61 7.70 10 2 7 90.38 7.39 10 3 -7 71.33 5.37 10 3 -6 110.73 7.74 10 3 -5 152.42 10.15 10 3 -4 187.96 12.06 10 3 -3 32.82 4.21 10 -3 3 40.27 4.70 10 3 -2 73.56 6.89 10 -3 2 77.68 7.48 10 3 -1 73.13 6.58 10 -3 1 70.71 7.26 10 3 0 9.85 2.24 10 3 0 12.84 2.47 10 -3 0 5.67 2.33 10 3 1 111.21 7.36 10 -3 -1 82.58 8.02 10 -3 -2 85.69 7.71 10 3 2 86.65 8.04 10 3 2 78.40 6.93 10 -3 -3 35.30 4.36 10 3 3 36.53 4.99 10 3 3 36.27 4.24 10 3 4 179.43 12.99 10 3 4 196.24 12.05 10 3 5 109.19 8.91 10 3 6 71.58 6.51 10 3 7 60.33 5.40 10 4 -6 525.87 26.79 10 4 -5 54.81 4.86 10 4 -4 62.26 5.48 10 4 -3 77.51 6.18 10 -4 3 62.08 5.86 10 4 -2 179.78 11.35 10 -4 2 167.48 11.72 10 4 -1 11.07 2.29 10 -4 1 8.68 2.68 10 -4 0 209.58 14.04 10 4 1 11.06 2.23 10 -4 -1 13.42 3.00 10 -4 -2 168.48 11.30 10 4 2 153.22 10.50 10 -4 -3 71.12 6.04 10 4 3 61.78 5.66 10 4 4 68.01 5.69 10 4 5 44.13 4.83 10 4 5 47.33 4.36 10 4 6 449.91 24.10 10 5 -5 245.93 13.60 10 5 -4 18.89 2.51 10 5 -3 11.74 2.13 10 -5 3 8.97 2.01 10 5 -2 12.14 2.18 10 -5 2 10.58 2.45 10 -5 1 55.71 5.69 10 -5 0 30.75 4.22 10 -5 -1 49.63 5.29 10 5 1 51.21 4.89 10 5 2 9.75 2.08 10 -5 -2 9.81 2.32 10 5 3 12.39 2.25 10 5 4 14.08 2.23 10 5 5 260.46 14.30 10 -6 2 40.44 4.04 10 -6 1 9.62 2.22 10 6 0 12.72 2.14 10 -6 0 9.44 2.09 10 6 1 10.08 1.93 10 -6 -1 9.24 2.13 10 -6 -2 43.63 4.21 10 6 2 45.66 4.17 10 6 3 23.30 2.72 11 0 0 1.97 1.16 11 0 -1 128.81 8.13 11 0 1 130.19 8.14 11 0 2 4.15 1.68 11 0 -2 2.59 1.10 11 0 2 4.39 1.22 11 0 3 400.14 21.93 11 0 4 225.42 13.48 11 -1 3 15.89 2.64 11 1 -2 143.05 7.94 11 -1 2 114.23 7.73 11 1 -1 14.69 2.15 11 -1 1 9.83 1.85 11 1 0 542.75 25.42 11 -1 0 456.05 25.33 11 1 1 12.95 1.99 11 -1 -1 12.92 2.10 11 1 2 143.62 7.99 11 -1 -2 117.63 7.90 11 1 3 15.96 2.76 11 2 -2 39.74 3.30 11 -2 2 30.49 3.18 11 2 -1 134.58 7.12 11 -2 1 83.02 6.72 11 2 0 27.26 2.82 11 -2 0 19.29 2.68 11 2 1 133.21 7.29 11 -2 -1 90.83 7.00 11 2 2 48.12 3.58 11 -2 -2 30.57 3.22 11 -3 1 19.54 2.42 11 -3 0 205.61 11.78 11 -3 -1 15.57 2.19 0 0 0 0.00 0.00 TITL 8722-9530-REU131 in P2(1)2(1)2(1) REM P2(1)2(1)2(1) (#19 in standard setting) CELL 1.54184 9.191215 11.392909 13.746419 90.0000 90.0000 90.0000 ZERR 4.00 0.000325 0.000451 0.000551 0.0000 0.0000 0.0000 LATT -1 SYMM -x+1/2,-y, z+1/2 SYMM -x, y+1/2,-z+1/2 SYMM x+1/2,-y+1/2,-z SFAC C H N O UNIT 68.00 60.00 12.00 8.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 25081 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.746 _oxdiff_exptl_absorpt_empirical_full_min 0.449