data_6b
_audit_creation_date              2017-12-14
_audit_creation_method
;
Olex2 1.2
(compiled 2017.08.10 svn.r3458 for OlexSys, GUI svn.r5381)
;
_publ_contact_author_address      ?
_publ_contact_author_email        ?
_publ_contact_author_id_orcid     ?
_publ_contact_author_name         ''
_publ_contact_author_phone        ?
_publ_section_references
;
Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H.
 (2009), J. Appl. Cryst. 42, 339-341.

Palatinus, L. & Chapuis, G. (2007). J. Appl. Cryst., 40, 786-790;
Palatinus, L. & van der Lee, A. (2008). J. Appl. Cryst. 41, 975-984;
Palatinus, L., Prathapa, S. J. & van Smaalen, S. (2012). J. Appl. Cryst. 45,
 575-580.

Sheldrick, G.M. (2008). Acta Cryst. A64, 112-122.
;
_chemical_name_common             ?
_chemical_name_systematic
;
 ? 
;
_chemical_formula_moiety          '2(C12 H27 Cr I O4 Si)'
_chemical_formula_sum             'C24 H54 Cr2 I2 O8 Si2'
_chemical_formula_weight          884.65
_chemical_melting_point           ?
loop_
  _atom_type_symbol
  _atom_type_description
  _atom_type_scat_dispersion_real
  _atom_type_scat_dispersion_imag
  _atom_type_scat_source
 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Cr' 'Cr' 0.3209 0.6236 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'I' 'I' -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Si' 'Si' 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system       'monoclinic'
_space_group_IT_number            14
_space_group_name_H-M_alt         'P 1 21/n 1'
_space_group_name_Hall            '-P 2yn'
loop_
  _space_group_symop_id
  _space_group_symop_operation_xyz
 1 'x, y, z'
 2 '-x+1/2, y+1/2, -z+1/2'
 3 '-x, -y, -z'
 4 'x-1/2, -y-1/2, z-1/2'

_cell_length_a                    17.8832(19)
_cell_length_b                    9.1254(10)
_cell_length_c                    23.860(3)
_cell_angle_alpha                 90.00
_cell_angle_beta                  104.6588(19)
_cell_angle_gamma                 90.00
_cell_volume                      3767.0(7)
_cell_formula_units_Z             4
_cell_measurement_reflns_used     8342
_cell_measurement_temperature     100
_cell_measurement_theta_max       26.720
_cell_measurement_theta_min       2.52
_exptl_absorpt_coefficient_mu     2.316
_exptl_absorpt_correction_T_max   0.7454
_exptl_absorpt_correction_T_min   0.6056
_exptl_absorpt_correction_type    multi-scan
_exptl_absorpt_process_details
'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1181 before and 0.0517 after correction. The Ratio of minimum to maximum transmission is 0.8124. The λ/2 correction factor is Not present.'
_exptl_crystal_colour             'clear colourless'
_exptl_crystal_colour_lustre      clear
_exptl_crystal_colour_primary     colourless
_exptl_crystal_density_diffrn     1.560
_exptl_crystal_density_meas       ?
_exptl_crystal_density_method     'not measured'
_exptl_crystal_description        block
_exptl_crystal_F_000              1776
_exptl_crystal_size_max           0.1
_exptl_crystal_size_mid           0.05
_exptl_crystal_size_min           0.05
_exptl_special_details
;
 ? 
;
_diffrn_reflns_av_R_equivalents   0.0897
_diffrn_reflns_av_unetI/netI      0.0556
_diffrn_reflns_limit_h_max        22
_diffrn_reflns_limit_h_min        -22
_diffrn_reflns_limit_k_max        11
_diffrn_reflns_limit_k_min        -11
_diffrn_reflns_limit_l_max        28
_diffrn_reflns_limit_l_min        -30
_diffrn_reflns_number             46122
_diffrn_reflns_theta_full         26.80
_diffrn_reflns_theta_max          26.80
_diffrn_reflns_theta_min          1.28
_diffrn_ambient_temperature       100
_diffrn_detector_area_resol_mean  ?
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type   'Bruker APEX-II CCD'
_diffrn_measurement_method        'φ and ω scans'
_diffrn_radiation_monochromator   graphite
_diffrn_radiation_type            MoK\a
_diffrn_radiation_wavelength      0.71073
_diffrn_source                    'fine-focus sealed tube'
_diffrn_special_details           ?
_diffrn_standards_number          0
_reflns_number_gt                 6007
_reflns_number_total              8049
_reflns_threshold_expression      >2sigma(I)
_computing_cell_refinement        'SAINT v8.37A (Bruker, 2015)'
_computing_data_collection        ?
_computing_data_reduction         'SAINT v8.37A (Bruker, 2015)'
_computing_molecular_graphics     'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material   'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement   'XL (Sheldrick, 2008)'
_computing_structure_solution
;
Superflip (Palatinus & Chapuis, 2007;Palatinus & van der Lee, 2008;
Palatinus et al., 2012)
;
_refine_diff_density_max          1.311
_refine_diff_density_min          -0.874
_refine_diff_density_rms          0.117
_refine_ls_extinction_coef        ?
_refine_ls_extinction_method      none
_refine_ls_goodness_of_fit_ref    1.054
_refine_ls_hydrogen_treatment     constr
_refine_ls_matrix_type            full
_refine_ls_number_parameters      381
_refine_ls_number_reflns          8049
_refine_ls_number_restraints      24
_refine_ls_R_factor_all           0.0661
_refine_ls_R_factor_gt            0.0398
_refine_ls_restrained_S_all       1.053
_refine_ls_shift/su_max           0.001
_refine_ls_shift/su_mean          0.000
_refine_ls_structure_factor_coef  Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0356P)²+2.8172P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme       calc
_refine_ls_wR_factor_gt           0.0793
_refine_ls_wR_factor_ref          0.0880
_refine_special_details
'ISOR command used to restrain disordered tBu group.'
_olex2_refinement_description
;
1. Fixed Uiso
 At 1.5 times of:
  All C(H,H,H) groups
2. Uiso/Uaniso restraints and constraints
Uanis(C25) \\sim Ueq: with sigma of 0.001 and sigma for terminal atoms of 0.001
Uanis(C24) \\sim Ueq: with sigma of 0.001 and sigma for terminal atoms of 0.001
Uanis(C22) \\sim Ueq: with sigma of 0.001 and sigma for terminal atoms of 0.001
Uanis(C26) \\sim Ueq: with sigma of 0.001 and sigma for terminal atoms of 0.001
3. Others
 Fixed Sof: C22(0.5) H22A(0.5) H22B(0.5) H22C(0.5) C25(0.5) H25A(0.5)
 H25B(0.5) H25C(0.5) C26(0.5) H26A(0.5) H26B(0.5) H26C(0.5) C24(0.5) H24A(0.5)
 H24B(0.5) H24C(0.5)
4.a Idealised Me refined as rotating group:
 C20(H20A,H20B,H20C), C4(H4A,H4B,H4C), C10(H10A,H10B,H10C), C8(H8A,H8B,H8C),
 C2(H2A,H2B,H2C), C7(H7A,H7B,H7C), C18(H18A,H18B,H18C), C3(H3A,H3B,H3C),
 C15(H15A,H15B,H15C), C14(H14A,H14B,H14C), C16(H16A,H16B,H16C), C11(H11A,H11B,
 H11C), C6(H6A,H6B,H6C), C12(H12A,H12B,H12C), C19(H19A,H19B,H19C), C23(H23A,
 H23B,H23C), C22(H22A,H22B,H22C), C25(H25A,H25B,H25C), C26(H26A,H26B,H26C),
 C24(H24A,H24B,H24C)
;
_atom_sites_solution_hydrogens    geom
_atom_sites_solution_primary      iterative
_atom_sites_solution_secondary    difmap
loop_
  _atom_site_label
  _atom_site_type_symbol
  _atom_site_fract_x
  _atom_site_fract_y
  _atom_site_fract_z
  _atom_site_U_iso_or_equiv
  _atom_site_adp_type
  _atom_site_occupancy
  _atom_site_calc_flag
  _atom_site_disorder_assembly
  _atom_site_disorder_group
  _atom_site_refinement_flags_posn
  _atom_site_refinement_flags_adp
 I1 I 0.592987(17) 0.29688(3) 0.390525(12) 0.03010(9) Uani 1 d . . . .
 I2 I 0.091547(18) 0.14608(3) 0.378475(13) 0.03493(10) Uani 1 d . . . .
 Cr1 Cr 0.55356(4) 0.39113(6) 0.48349(3) 0.01717(14) Uani 1 d . . . .
 Cr2 Cr 0.05530(4) 0.09446(7) 0.47741(3) 0.01984(15) Uani 1 d . . . .
 Si1 Si 0.59626(6) 0.39419(11) 0.60383(4) 0.0155(2) Uani 1 d . . . .
 Si2 Si 0.08598(6) 0.15600(12) 0.59562(5) 0.0189(2) Uani 1 d . . . .
 O5 O -0.02769(16) -0.0489(3) 0.44784(11) 0.0237(6) Uani 1 d . . . .
 O1 O 0.46796(15) 0.5213(3) 0.44466(11) 0.0205(6) Uani 1 d . . . .
 O2 O 0.62483(15) 0.2883(3) 0.55542(11) 0.0188(6) Uani 1 d . . . .
 O4 O 0.56594(15) 0.3042(3) 0.65102(11) 0.0208(6) Uani 1 d . . . .
 O7 O 0.04691(16) 0.2926(3) 0.61843(12) 0.0242(6) Uani 1 d . . . .
 O6 O 0.12682(16) 0.2195(3) 0.54388(12) 0.0230(6) Uani 1 d . . . .
 O3 O 0.67020(15) 0.4879(3) 0.63544(11) 0.0212(6) Uani 1 d . . . .
 O8 O 0.14671(16) 0.0797(3) 0.64771(12) 0.0257(7) Uani 1 d A . . .
 C17 C 0.0189(3) 0.3329(5) 0.66819(18) 0.0268(10) Uani 1 d . . . .
 C20 C 0.0506(4) 0.4863(5) 0.6845(2) 0.0560(16) Uani 1 d . . . .
 H20A H 0.1071 0.4821 0.6976 0.084 Uiso 1 calc . . GR .
 H20B H 0.0295 0.5248 0.7156 0.084 Uiso 1 calc . . GR .
 H20C H 0.0355 0.5506 0.6506 0.084 Uiso 1 calc . . GR .
 C4 C 0.7221(2) 0.1553(5) 0.62890(17) 0.0269(10) Uani 1 d . . . .
 H4A H 0.7401 0.2476 0.6488 0.040 Uiso 1 calc . . GR .
 H4B H 0.7653 0.0862 0.6348 0.040 Uiso 1 calc . . GR .
 H4C H 0.6812 0.1136 0.6446 0.040 Uiso 1 calc . . GR .
 C10 C 0.5309(3) 0.0693(5) 0.6780(2) 0.0415(13) Uani 1 d . . . .
 H10A H 0.5560 0.0194 0.6513 0.062 Uiso 1 calc . . GR .
 H10B H 0.4885 0.0084 0.6842 0.062 Uiso 1 calc . . GR .
 H10C H 0.5687 0.0855 0.7152 0.062 Uiso 1 calc . . GR .
 C8 C 0.7703(3) 0.5914(5) 0.7081(2) 0.0383(12) Uani 1 d . . . .
 H8A H 0.7797 0.4966 0.7280 0.057 Uiso 1 calc . . GR .
 H8B H 0.7850 0.6705 0.7366 0.057 Uiso 1 calc . . GR .
 H8C H 0.8012 0.5982 0.6796 0.057 Uiso 1 calc . . GR .
 C9 C 0.4992(2) 0.2150(4) 0.65257(18) 0.0245(9) Uani 1 d . . . .
 C5 C 0.6859(2) 0.6050(4) 0.67777(18) 0.0228(9) Uani 1 d . . . .
 C13 C 0.1753(2) 0.3530(4) 0.54579(19) 0.0264(10) Uani 1 d . . . .
 C1 C 0.6910(2) 0.1839(4) 0.56508(17) 0.0214(9) Uani 1 d . . . .
 C2 C 0.7519(2) 0.2561(5) 0.5397(2) 0.0347(11) Uani 1 d . . . .
 H2A H 0.7298 0.2767 0.4985 0.052 Uiso 1 calc . . GR .
 H2B H 0.7962 0.1900 0.5440 0.052 Uiso 1 calc . . GR .
 H2C H 0.7689 0.3479 0.5603 0.052 Uiso 1 calc . . GR .
 C7 C 0.6702(3) 0.7477(5) 0.6445(2) 0.0492(14) Uani 1 d . . . .
 H7A H 0.6999 0.7504 0.6152 0.074 Uiso 1 calc . . GR .
 H7B H 0.6856 0.8301 0.6713 0.074 Uiso 1 calc . . GR .
 H7C H 0.6149 0.7551 0.6255 0.074 Uiso 1 calc . . GR .
 C18 C 0.0462(3) 0.2272(6) 0.7174(2) 0.0458(13) Uani 1 d . . . .
 H18A H 0.0263 0.1290 0.7053 0.069 Uiso 1 calc . . GR .
 H18B H 0.0273 0.2586 0.7506 0.069 Uiso 1 calc . . GR .
 H18C H 0.1028 0.2249 0.7285 0.069 Uiso 1 calc . . GR .
 C21 C 0.1934(3) -0.0529(5) 0.6574(2) 0.0343(11) Uani 1 d . . . .
 C3 C 0.6592(3) 0.0460(4) 0.5325(2) 0.0339(11) Uani 1 d . . . .
 H3A H 0.6177 0.0065 0.5481 0.051 Uiso 1 calc . . GR .
 H3B H 0.7006 -0.0268 0.5370 0.051 Uiso 1 calc . . GR .
 H3C H 0.6389 0.0689 0.4913 0.051 Uiso 1 calc . . GR .
 C15 C 0.2341(3) 0.3172(5) 0.5124(2) 0.0405(13) Uani 1 d . . . .
 H15A H 0.2627 0.2290 0.5286 0.061 Uiso 1 calc . . GR .
 H15B H 0.2701 0.3994 0.5151 0.061 Uiso 1 calc . . GR .
 H15C H 0.2076 0.3001 0.4716 0.061 Uiso 1 calc . . GR .
 C14 C 0.2158(3) 0.3898(5) 0.6080(2) 0.0397(12) Uani 1 d . . . .
 H14A H 0.1772 0.4150 0.6292 0.060 Uiso 1 calc . . GR .
 H14B H 0.2505 0.4733 0.6088 0.060 Uiso 1 calc . . GR .
 H14C H 0.2458 0.3049 0.6263 0.060 Uiso 1 calc . . GR .
 C16 C 0.1212(3) 0.4730(5) 0.5178(2) 0.0414(12) Uani 1 d . . . .
 H16A H 0.0967 0.4464 0.4776 0.062 Uiso 1 calc . . GR .
 H16B H 0.1502 0.5644 0.5186 0.062 Uiso 1 calc . . GR .
 H16C H 0.0814 0.4865 0.5390 0.062 Uiso 1 calc . . GR .
 C11 C 0.4577(3) 0.2928(5) 0.6918(2) 0.0434(13) Uani 1 d . . . .
 H11A H 0.4929 0.3048 0.7303 0.065 Uiso 1 calc . . GR .
 H11B H 0.4128 0.2348 0.6949 0.065 Uiso 1 calc . . GR .
 H11C H 0.4404 0.3894 0.6755 0.065 Uiso 1 calc . . GR .
 C6 C 0.6353(3) 0.5901(6) 0.7196(2) 0.0456(14) Uani 1 d . . . .
 H6A H 0.5809 0.5985 0.6984 0.068 Uiso 1 calc . . GR .
 H6B H 0.6481 0.6679 0.7488 0.068 Uiso 1 calc . . GR .
 H6C H 0.6442 0.4943 0.7387 0.068 Uiso 1 calc . . GR .
 C12 C 0.4468(3) 0.1947(6) 0.5927(2) 0.0543(15) Uani 1 d . . . .
 H12A H 0.4253 0.2898 0.5775 0.081 Uiso 1 calc . . GR .
 H12B H 0.4047 0.1278 0.5946 0.081 Uiso 1 calc . . GR .
 H12C H 0.4765 0.1536 0.5671 0.081 Uiso 1 calc . . GR .
 C19 C -0.0671(3) 0.3365(6) 0.6485(2) 0.0483(14) Uani 1 d . . . .
 H19A H -0.0830 0.4058 0.6163 0.072 Uiso 1 calc . . GR .
 H19B H -0.0884 0.3675 0.6806 0.072 Uiso 1 calc . . GR .
 H19C H -0.0865 0.2385 0.6356 0.072 Uiso 1 calc . . GR .
 C23 C 0.2750(3) -0.0059(6) 0.6739(3) 0.071(2) Uani 1 d A . . .
 H23A H 0.2873 0.0458 0.6413 0.107 Uiso 1 calc . . GR .
 H23B H 0.3084 -0.0920 0.6839 0.107 Uiso 1 calc . . GR .
 H23C H 0.2834 0.0598 0.7074 0.107 Uiso 1 calc . . GR .
 C22 C 0.1687(6) -0.1626(11) 0.6132(5) 0.041(3) Uani 0.50 d A 1 . U
 H22A H 0.1140 -0.1853 0.6091 0.062 Uiso 0.50 calc A 1 GR .
 H22B H 0.1996 -0.2516 0.6241 0.062 Uiso 0.50 calc A 1 GR .
 H22C H 0.1756 -0.1256 0.5763 0.062 Uiso 0.50 calc A 1 GR .
 C25 C 0.1591(8) -0.1514(15) 0.6907(6) 0.070(4) Uani 0.50 d A 2 . U
 H25A H 0.1541 -0.1021 0.7260 0.104 Uiso 0.50 calc A 2 GR .
 H25B H 0.1919 -0.2382 0.7010 0.104 Uiso 0.50 calc A 2 GR .
 H25C H 0.1078 -0.1812 0.6676 0.104 Uiso 0.50 calc A 2 GR .
 C26 C 0.1899(8) -0.1259(15) 0.5956(6) 0.062(4) Uani 0.50 d A 2 . U
 H26A H 0.1364 -0.1528 0.5767 0.094 Uiso 0.50 calc A 2 GR .
 H26B H 0.2224 -0.2138 0.6011 0.094 Uiso 0.50 calc A 2 GR .
 H26C H 0.2088 -0.0557 0.5713 0.094 Uiso 0.50 calc A 2 GR .
 C24 C 0.1861(7) -0.1116(13) 0.7177(5) 0.050(3) Uani 0.50 d A 1 . U
 H24A H 0.2031 -0.0356 0.7472 0.076 Uiso 0.50 calc A 1 GR .
 H24B H 0.2185 -0.1989 0.7284 0.076 Uiso 0.50 calc A 1 GR .
 H24C H 0.1321 -0.1368 0.7152 0.076 Uiso 0.50 calc A 1 GR .


_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;
loop_
  _geom_bond_atom_site_label_1
  _geom_bond_atom_site_label_2
  _geom_bond_distance
  _geom_bond_site_symmetry_2
  _geom_bond_publ_flag
 I1 Cr1 2.6361(6) . ?
 I2 Cr2 2.6437(7) . ?
 Cr1 Si1 2.7782(12) . ?
 Cr1 O1 2.015(2) 3_666 ?
 Cr1 O1 1.974(3) . ?
 Cr1 O2 2.084(3) . ?
 Cr2 Si2 2.7907(13) . ?
 Cr2 O5 1.970(3) . ?
 Cr2 O5 2.011(3) 3_556 ?
 Cr2 O6 2.104(3) . ?
 Si1 O1 1.606(3) 3_666 ?
 Si1 O2 1.682(3) . ?
 Si1 O4 1.596(3) . ?
 Si1 O3 1.595(3) . ?
 Si2 O5 1.603(3) 3_556 ?
 Si2 O7 1.591(3) . ?
 Si2 O6 1.688(3) . ?
 Si2 O8 1.589(3) . ?
 O5 Cr2 2.011(3) 3_556 ?
 O5 Si2 1.603(3) 3_556 ?
 O1 Cr1 2.015(2) 3_666 ?
 O1 Si1 1.606(3) 3_666 ?
 O2 C1 1.491(4) . ?
 O4 C9 1.453(4) . ?
 O7 C17 1.448(4) . ?
 O6 C13 1.490(4) . ?
 O3 C5 1.448(5) . ?
 O8 C21 1.455(5) . ?
 C17 C20 1.523(6) . ?
 C17 C18 1.503(6) . ?
 C17 C19 1.490(6) . ?
 C4 C1 1.506(5) . ?
 C10 C9 1.511(6) . ?
 C8 C5 1.506(6) . ?
 C9 C11 1.511(6) . ?
 C9 C12 1.509(7) . ?
 C5 C7 1.515(6) . ?
 C5 C6 1.512(6) . ?
 C13 C15 1.507(6) . ?
 C13 C14 1.516(6) . ?
 C13 C16 1.501(6) . ?
 C1 C2 1.524(6) . ?
 C1 C3 1.512(6) . ?
 C21 C23 1.475(7) . ?
 C21 C22 1.440(11) . ?
 C21 C25 1.436(14) . ?
 C21 C26 1.605(13) . ?
 C21 C24 1.572(12) . ?

loop_
  _geom_angle_atom_site_label_1
  _geom_angle_atom_site_label_2
  _geom_angle_atom_site_label_3
  _geom_angle
  _geom_angle_site_symmetry_1
  _geom_angle_site_symmetry_3
  _geom_angle_publ_flag
 I1 Cr1 Si1 144.18(3) . . ?
 O1 Cr1 I1 98.18(7) . . ?
 O1 Cr1 I1 174.12(8) 3_666 . ?
 O1 Cr1 Si1 34.75(8) 3_666 . ?
 O1 Cr1 Si1 117.18(8) . . ?
 O1 Cr1 O1 82.43(11) . 3_666 ?
 O1 Cr1 O2 153.85(10) . . ?
 O1 Cr1 O2 71.73(10) 3_666 . ?
 O2 Cr1 I1 107.94(7) . . ?
 O2 Cr1 Si1 37.11(7) . . ?
 I2 Cr2 Si2 146.79(3) . . ?
 O5 Cr2 I2 97.54(8) . . ?
 O5 Cr2 I2 178.33(8) 3_556 . ?
 O5 Cr2 Si2 34.39(8) 3_556 . ?
 O5 Cr2 Si2 115.67(8) . . ?
 O5 Cr2 O5 81.29(12) . 3_556 ?
 O5 Cr2 O6 152.77(10) . . ?
 O5 Cr2 O6 71.48(10) 3_556 . ?
 O6 Cr2 I2 109.68(7) . . ?
 O6 Cr2 Si2 37.11(7) . . ?
 O1 Si1 Cr1 45.65(9) 3_666 . ?
 O1 Si1 O2 93.86(13) 3_666 . ?
 O2 Si1 Cr1 48.41(9) . . ?
 O4 Si1 Cr1 132.11(11) . . ?
 O4 Si1 O1 116.54(15) . 3_666 ?
 O4 Si1 O2 113.92(14) . . ?
 O3 Si1 Cr1 118.18(10) . . ?
 O3 Si1 O1 116.07(15) . 3_666 ?
 O3 Si1 O2 105.85(14) . . ?
 O3 Si1 O4 109.36(15) . . ?
 O5 Si2 Cr2 45.11(9) 3_556 . ?
 O5 Si2 O6 93.85(14) 3_556 . ?
 O7 Si2 Cr2 120.82(11) . . ?
 O7 Si2 O5 115.41(16) . 3_556 ?
 O7 Si2 O6 106.85(14) . . ?
 O6 Si2 Cr2 48.76(9) . . ?
 O8 Si2 Cr2 128.53(11) . . ?
 O8 Si2 O5 116.28(15) . 3_556 ?
 O8 Si2 O7 110.37(15) . . ?
 O8 Si2 O6 112.69(15) . . ?
 Cr2 O5 Cr2 98.71(12) . 3_556 ?
 Si2 O5 Cr2 160.74(16) 3_556 . ?
 Si2 O5 Cr2 100.51(13) 3_556 3_556 ?
 Cr1 O1 Cr1 97.57(11) . 3_666 ?
 Si1 O1 Cr1 99.61(12) 3_666 3_666 ?
 Si1 O1 Cr1 162.83(16) 3_666 . ?
 Si1 O2 Cr1 94.48(12) . . ?
 C1 O2 Cr1 135.3(2) . . ?
 C1 O2 Si1 128.9(2) . . ?
 C9 O4 Si1 137.3(3) . . ?
 C17 O7 Si2 138.8(3) . . ?
 Si2 O6 Cr2 94.13(12) . . ?
 C13 O6 Cr2 134.8(2) . . ?
 C13 O6 Si2 127.9(2) . . ?
 C5 O3 Si1 135.7(2) . . ?
 C21 O8 Si2 137.7(3) . . ?
 O7 C17 C20 105.0(3) . . ?
 O7 C17 C18 111.5(3) . . ?
 O7 C17 C19 106.9(4) . . ?
 C18 C17 C20 111.4(4) . . ?
 C19 C17 C20 110.4(4) . . ?
 C19 C17 C18 111.5(4) . . ?
 O4 C9 C10 106.1(3) . . ?
 O4 C9 C11 106.7(3) . . ?
 O4 C9 C12 111.2(3) . . ?
 C11 C9 C10 111.0(4) . . ?
 C12 C9 C10 110.7(4) . . ?
 C12 C9 C11 111.0(4) . . ?
 O3 C5 C8 105.6(3) . . ?
 O3 C5 C7 106.9(3) . . ?
 O3 C5 C6 110.6(3) . . ?
 C8 C5 C7 110.7(4) . . ?
 C8 C5 C6 111.7(4) . . ?
 C6 C5 C7 111.1(4) . . ?
 O6 C13 C15 106.6(3) . . ?
 O6 C13 C14 109.9(3) . . ?
 O6 C13 C16 106.2(3) . . ?
 C15 C13 C14 110.0(4) . . ?
 C16 C13 C15 112.3(4) . . ?
 C16 C13 C14 111.6(4) . . ?
 O2 C1 C4 110.1(3) . . ?
 O2 C1 C2 106.3(3) . . ?
 O2 C1 C3 105.8(3) . . ?
 C4 C1 C2 111.0(4) . . ?
 C4 C1 C3 111.7(3) . . ?
 C3 C1 C2 111.6(4) . . ?
 O8 C21 C23 106.8(4) . . ?
 O8 C21 C26 108.2(6) . . ?
 O8 C21 C24 104.5(5) . . ?
 C23 C21 C26 99.9(6) . . ?
 C23 C21 C24 99.2(6) . . ?
 C22 C21 O8 113.9(6) . . ?
 C22 C21 C23 119.8(6) . . ?
 C22 C21 C26 26.5(6) . . ?
 C22 C21 C24 110.6(7) . . ?
 C25 C21 O8 107.5(6) . . ?
 C25 C21 C23 124.5(8) . . ?
 C25 C21 C22 82.8(8) . . ?
 C25 C21 C26 109.0(8) . . ?
 C25 C21 C24 30.0(6) . . ?
 C24 C21 C26 135.0(7) . . ?

_olex2_submission_special_instructions 'No special instructions were received'
