data_10
_audit_creation_date              2017-11-08
_audit_creation_method
;
Olex2 1.2
(compiled 2017.08.10 svn.r3458 for OlexSys, GUI svn.r5381)
;
_publ_contact_author_address      ?
_publ_contact_author_email        ?
_publ_contact_author_id_orcid     ?
_publ_contact_author_name         ''
_publ_contact_author_phone        ?
_publ_section_references
;
Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H.
 (2009), J. Appl. Cryst. 42, 339-341.

Palatinus, L. & Chapuis, G. (2007). J. Appl. Cryst., 40, 786-790;
Palatinus, L. & van der Lee, A. (2008). J. Appl. Cryst. 41, 975-984;
Palatinus, L., Prathapa, S. J. & van Smaalen, S. (2012). J. Appl. Cryst. 45,
 575-580.

Sheldrick, G.M. (2008). Acta Cryst. A64, 112-122.
;
_chemical_name_common             ?
_chemical_name_systematic
;
 ? 
;
_chemical_formula_moiety          'C30 H70 Cr I N2 O8 Si2, C3 H3'
_chemical_formula_sum             'C33 H73 Cr I N2 O8 Si2'
_chemical_formula_weight          861.01
_chemical_melting_point           ?
loop_
  _atom_type_symbol
  _atom_type_description
  _atom_type_scat_dispersion_real
  _atom_type_scat_dispersion_imag
  _atom_type_scat_source
 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Cr' 'Cr' 0.3209 0.6236 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'I' 'I' -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Si' 'Si' 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system       'triclinic'
_space_group_IT_number            2
_space_group_name_H-M_alt         'P -1'
_space_group_name_Hall            '-P 1'
loop_
  _space_group_symop_id
  _space_group_symop_operation_xyz
 1 'x, y, z'
 2 '-x, -y, -z'

_cell_length_a                    9.2746(13)
_cell_length_b                    14.813(2)
_cell_length_c                    17.529(2)
_cell_angle_alpha                 82.759(2)
_cell_angle_beta                  87.291(2)
_cell_angle_gamma                 73.148(2)
_cell_volume                      2286.3(5)
_cell_formula_units_Z             2
_cell_measurement_reflns_used     9881
_cell_measurement_temperature     150
_cell_measurement_theta_max       28.55
_cell_measurement_theta_min       2.295
_exptl_absorpt_coefficient_mu     1.020
_exptl_absorpt_correction_T_max   0.7458
_exptl_absorpt_correction_T_min   0.5828
_exptl_absorpt_correction_type    multi-scan
_exptl_absorpt_process_details
'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1392 before and 0.0666 after correction. The Ratio of minimum to maximum transmission is 0.7814. The λ/2 correction factor is Not present.'
_exptl_crystal_colour             'clear pinkish violet'
_exptl_crystal_colour_lustre      clear
_exptl_crystal_colour_modifier    pinkish
_exptl_crystal_colour_primary     violet
_exptl_crystal_density_diffrn     1.251
_exptl_crystal_density_meas       ?
_exptl_crystal_density_method     'not measured'
_exptl_crystal_description        block
_exptl_crystal_F_000              908
_exptl_crystal_size_max           0.4
_exptl_crystal_size_mid           0.2
_exptl_crystal_size_min           0.2
_exptl_special_details
;
 ? 
;
_diffrn_reflns_av_R_equivalents   0.0800
_diffrn_reflns_av_unetI/netI      0.0529
_diffrn_reflns_limit_h_max        12
_diffrn_reflns_limit_h_min        -12
_diffrn_reflns_limit_k_max        19
_diffrn_reflns_limit_k_min        -19
_diffrn_reflns_limit_l_max        23
_diffrn_reflns_limit_l_min        -23
_diffrn_reflns_number             71129
_diffrn_reflns_theta_full         28.67
_diffrn_reflns_theta_max          28.67
_diffrn_reflns_theta_min          1.45
_diffrn_ambient_temperature       150.0
_diffrn_detector_area_resol_mean  ?
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type   'Bruker APEX-II CCD'
_diffrn_measurement_method        'φ and ω scans'
_diffrn_radiation_monochromator   graphite
_diffrn_radiation_type            MoK\a
_diffrn_radiation_wavelength      0.71073
_diffrn_source                    'fine-focus sealed tube'
_diffrn_standards_number          0
_reflns_number_gt                 9008
_reflns_number_total              11751
_reflns_threshold_expression      >2sigma(I)
_computing_cell_refinement        'SAINT V8.38A (Bruker-AXS, 2016)'
_computing_data_collection        ?
_computing_data_reduction         'SAINT V8.38A (Bruker-AXS, 2016)'
_computing_molecular_graphics     'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material   'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement   'XL (Sheldrick, 2008)'
_computing_structure_solution
;
Superflip (Palatinus & Chapuis, 2007;Palatinus & van der Lee, 2008;
Palatinus et al., 2012)
;
_refine_diff_density_max          0.496
_refine_diff_density_min          -0.597
_refine_diff_density_rms          0.078
_refine_ls_extinction_coef        ?
_refine_ls_extinction_method      none
_refine_ls_goodness_of_fit_ref    1.044
_refine_ls_hydrogen_treatment     constr
_refine_ls_matrix_type            full
_refine_ls_number_parameters      446
_refine_ls_number_reflns          11751
_refine_ls_number_restraints      0
_refine_ls_R_factor_all           0.0537
_refine_ls_R_factor_gt            0.0309
_refine_ls_restrained_S_all       1.044
_refine_ls_shift/su_max           0.002
_refine_ls_shift/su_mean          0.000
_refine_ls_structure_factor_coef  Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0364P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme       calc
_refine_ls_wR_factor_gt           0.0680
_refine_ls_wR_factor_ref          0.0806
_refine_special_details
;
 Refinement of F² against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F², conventional R-factors R are based 
 on F, with F set to zero for negative F². The threshold expression of 
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F² are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. 
;
_olex2_refinement_description
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2.a Secondary CH2 refined with riding coordinates:
 C28(H28A,H28B), C27(H27A,H27B)
2.b Aromatic/amide H refined with riding coordinates:
 C33(H33), C31(H31), C32(H32)
2.c Idealised Me refined as rotating group:
 C15(H15A,H15B,H15C), C29(H29A,H29B,H29C), C4(H4A,H4B,H4C), C26(H26A,H26B,
 H26C), C20(H20A,H20B,H20C), C30(H30A,H30B,H30C), C7(H7A,H7B,H7C), C18(H18A,
 H18B,H18C), C12(H12A,H12B,H12C), C3(H3A,H3B,H3C), C6(H6A,H6B,H6C), C24(H24A,
 H24B,H24C), C16(H16A,H16B,H16C), C13(H13A,H13B,H13C), C25(H25A,H25B,H25C),
 C19(H19A,H19B,H19C), C10(H10A,H10B,H10C), C2(H2A,H2B,H2C), C8(H8A,H8B,H8C),
 C11(H11A,H11B,H11C), C23(H23A,H23B,H23C), C22(H22A,H22B,H22C)
;
_atom_sites_solution_hydrogens    geom
_atom_sites_solution_primary      iterative
_atom_sites_solution_secondary    difmap
loop_
  _atom_site_label
  _atom_site_type_symbol
  _atom_site_fract_x
  _atom_site_fract_y
  _atom_site_fract_z
  _atom_site_U_iso_or_equiv
  _atom_site_adp_type
  _atom_site_occupancy
  _atom_site_calc_flag
  _atom_site_disorder_assembly
  _atom_site_disorder_group
  _atom_site_refinement_flags_posn
 I1 I 1.092552(15) 0.309288(11) 0.358824(9) 0.02745(5) Uani 1 d . . .
 Cr1 Cr 0.81120(3) 0.30391(2) 0.323601(19) 0.01621(8) Uani 1 d . . .
 Si1 Si 0.88474(6) 0.14420(4) 0.19218(3) 0.01861(13) Uani 1 d . . .
 Si2 Si 0.69977(6) 0.54270(4) 0.26650(3) 0.01898(13) Uani 1 d . . .
 O5 O 0.75229(15) 0.43081(10) 0.29172(9) 0.0224(3) Uani 1 d . . .
 O2 O 0.86713(16) 0.04816(10) 0.24361(9) 0.0232(3) Uani 1 d . . .
 O1 O 0.87180(15) 0.21807(10) 0.25205(8) 0.0212(3) Uani 1 d . . .
 O6 O 0.73082(15) 0.57189(10) 0.17654(8) 0.0231(3) Uani 1 d . . .
 O4 O 0.74886(15) 0.17535(11) 0.13001(8) 0.0232(3) Uani 1 d . . .
 O7 O 0.78169(18) 0.59871(11) 0.31596(9) 0.0272(4) Uani 1 d . . .
 O3 O 1.03911(15) 0.12461(11) 0.14130(9) 0.0250(3) Uani 1 d . . .
 O8 O 0.51844(16) 0.57656(11) 0.28026(9) 0.0302(4) Uani 1 d . . .
 N1 N 0.8129(2) 0.19589(13) 0.42157(10) 0.0246(4) Uani 1 d . . .
 N2 N 0.58299(18) 0.30447(12) 0.32247(10) 0.0199(4) Uani 1 d . . .
 C14 C 0.8643(2) 0.58035(16) 0.13400(13) 0.0259(5) Uani 1 d . . .
 C1 C 0.8485(2) -0.03922(16) 0.22352(14) 0.0286(5) Uani 1 d . . .
 C15 C 0.8279(3) 0.5822(2) 0.05014(14) 0.0383(6) Uani 1 d . . .
 H15A H 0.8049 0.5233 0.0429 0.057 Uiso 1 calc . . GR
 H15B H 0.9148 0.5878 0.0178 0.057 Uiso 1 calc . . GR
 H15C H 0.7405 0.6366 0.0356 0.057 Uiso 1 calc . . GR
 C5 C 1.1943(2) 0.11263(18) 0.15804(14) 0.0306(6) Uani 1 d . . .
 C29 C 0.4903(2) 0.37351(16) 0.37289(14) 0.0259(5) Uani 1 d . . .
 H29A H 0.5411 0.3653 0.4221 0.039 Uiso 1 calc . . GR
 H29B H 0.3914 0.3624 0.3819 0.039 Uiso 1 calc . . GR
 H29C H 0.4773 0.4383 0.3478 0.039 Uiso 1 calc . . GR
 C4 C 0.6827(3) -0.0232(2) 0.20864(19) 0.0469(7) Uani 1 d . . .
 H4A H 0.6232 0.0001 0.2536 0.070 Uiso 1 calc . . GR
 H4B H 0.6659 -0.0831 0.1993 0.070 Uiso 1 calc . . GR
 H4C H 0.6519 0.0239 0.1635 0.070 Uiso 1 calc . . GR
 C28 C 0.5829(2) 0.20604(15) 0.35158(14) 0.0264(5) Uani 1 d . . .
 H28A H 0.6355 0.1621 0.3143 0.032 Uiso 1 calc . . R
 H28B H 0.4780 0.2024 0.3578 0.032 Uiso 1 calc . . R
 C26 C 0.9289(3) 0.10488(16) 0.41132(14) 0.0328(6) Uani 1 d . . .
 H26A H 0.9074 0.0809 0.3648 0.049 Uiso 1 calc . . GR
 H26B H 0.9271 0.0583 0.4560 0.049 Uiso 1 calc . . GR
 H26C H 1.0286 0.1155 0.4064 0.049 Uiso 1 calc . . GR
 C20 C 0.6700(3) 0.70241(18) 0.40984(17) 0.0456(7) Uani 1 d . . .
 H20A H 0.6950 0.7535 0.3756 0.068 Uiso 1 calc . . GR
 H20B H 0.6749 0.7137 0.4634 0.068 Uiso 1 calc . . GR
 H20C H 0.5680 0.7011 0.3990 0.068 Uiso 1 calc . . GR
 C33 C 0.4763(3) 0.04285(17) 0.56642(15) 0.0328(6) Uani 1 d . . .
 H33 H 0.4603 0.0726 0.6123 0.039 Uiso 1 calc . . R
 C30 C 0.5178(2) 0.32997(17) 0.24471(13) 0.0268(5) Uani 1 d . . .
 H30A H 0.5269 0.3925 0.2234 0.040 Uiso 1 calc . . GR
 H30B H 0.4112 0.3318 0.2477 0.040 Uiso 1 calc . . GR
 H30C H 0.5721 0.2825 0.2114 0.040 Uiso 1 calc . . GR
 C27 C 0.6613(3) 0.17783(17) 0.42747(14) 0.0309(5) Uani 1 d . . .
 H27A H 0.6739 0.1096 0.4439 0.037 Uiso 1 calc . . R
 H27B H 0.5989 0.2146 0.4668 0.037 Uiso 1 calc . . R
 C7 C 1.2853(3) 0.0535(2) 0.09727(17) 0.0487(8) Uani 1 d . . .
 H7A H 1.2667 -0.0089 0.1030 0.073 Uiso 1 calc . . GR
 H7B H 1.3929 0.0453 0.1039 0.073 Uiso 1 calc . . GR
 H7C H 1.2547 0.0861 0.0459 0.073 Uiso 1 calc . . GR
 C18 C 0.9411(3) 0.6071(2) 0.41395(16) 0.0419(7) Uani 1 d . . .
 H18A H 1.0124 0.5477 0.4010 0.063 Uiso 1 calc . . GR
 H18B H 0.9486 0.6121 0.4687 0.063 Uiso 1 calc . . GR
 H18C H 0.9649 0.6610 0.3833 0.063 Uiso 1 calc . . GR
 C9 C 0.7346(2) 0.23072(17) 0.05543(13) 0.0282(5) Uani 1 d . . .
 C17 C 0.7823(3) 0.60750(16) 0.39668(13) 0.0255(5) Uani 1 d . . .
 C12 C 0.5677(3) 0.2586(2) 0.03688(15) 0.0449(7) Uani 1 d . . .
 H12A H 0.5344 0.2013 0.0392 0.067 Uiso 1 calc . . GR
 H12B H 0.5512 0.2932 -0.0149 0.067 Uiso 1 calc . . GR
 H12C H 0.5102 0.2993 0.0744 0.067 Uiso 1 calc . . GR
 C31 C 0.3983(3) 0.03305(17) 0.44101(15) 0.0317(5) Uani 1 d . . .
 H31 H 0.3286 0.0558 0.4001 0.038 Uiso 1 calc . . R
 C3 C 0.9444(3) -0.07101(19) 0.15424(17) 0.0485(8) Uani 1 d . . .
 H3A H 0.9130 -0.0228 0.1099 0.073 Uiso 1 calc . . GR
 H3B H 0.9320 -0.1314 0.1428 0.073 Uiso 1 calc . . GR
 H3C H 1.0505 -0.0794 0.1652 0.073 Uiso 1 calc . . GR
 C6 C 1.2321(3) 0.0620(2) 0.23821(16) 0.0443(7) Uani 1 d . . .
 H6A H 1.1704 0.1005 0.2759 0.066 Uiso 1 calc . . GR
 H6B H 1.3390 0.0523 0.2481 0.066 Uiso 1 calc . . GR
 H6C H 1.2114 0.0003 0.2426 0.066 Uiso 1 calc . . GR
 C24 C 0.2659(3) 0.6627(3) 0.2993(2) 0.0782(12) Uani 1 d . . .
 H24A H 0.2417 0.6026 0.3138 0.117 Uiso 1 calc . . GR
 H24B H 0.1776 0.7104 0.2760 0.117 Uiso 1 calc . . GR
 H24C H 0.2945 0.6846 0.3452 0.117 Uiso 1 calc . . GR
 C16 C 0.8918(3) 0.67376(19) 0.14730(17) 0.0443(7) Uani 1 d . . .
 H16A H 0.8026 0.7265 0.1320 0.066 Uiso 1 calc . . GR
 H16B H 0.9790 0.6822 0.1166 0.066 Uiso 1 calc . . GR
 H16C H 0.9114 0.6726 0.2019 0.066 Uiso 1 calc . . GR
 C13 C 0.9979(3) 0.49647(19) 0.15928(16) 0.0398(6) Uani 1 d . . .
 H13A H 1.0194 0.4974 0.2133 0.060 Uiso 1 calc . . GR
 H13B H 1.0861 0.5004 0.1275 0.060 Uiso 1 calc . . GR
 H13C H 0.9746 0.4373 0.1534 0.060 Uiso 1 calc . . GR
 C25 C 0.8425(3) 0.2265(2) 0.49525(14) 0.0399(6) Uani 1 d . . .
 H25A H 0.9453 0.2321 0.4945 0.060 Uiso 1 calc . . GR
 H25B H 0.8312 0.1795 0.5379 0.060 Uiso 1 calc . . GR
 H25C H 0.7706 0.2882 0.5020 0.060 Uiso 1 calc . . GR
 C19 C 0.7396(3) 0.52719(17) 0.44660(14) 0.0325(6) Uani 1 d . . .
 H19A H 0.6370 0.5282 0.4345 0.049 Uiso 1 calc . . GR
 H19B H 0.7443 0.5354 0.5009 0.049 Uiso 1 calc . . GR
 H19C H 0.8099 0.4662 0.4365 0.049 Uiso 1 calc . . GR
 C32 C 0.3740(3) 0.07591(17) 0.50748(15) 0.0318(6) Uani 1 d . . .
 H32 H 0.2872 0.1280 0.5128 0.038 Uiso 1 calc . . R
 C10 C 0.8254(3) 0.1687(2) -0.00285(15) 0.0416(7) Uani 1 d . . .
 H10A H 0.9322 0.1491 0.0107 0.062 Uiso 1 calc . . GR
 H10B H 0.8123 0.2047 -0.0542 0.062 Uiso 1 calc . . GR
 H10C H 0.7903 0.1124 -0.0027 0.062 Uiso 1 calc . . GR
 C2 C 0.8981(3) -0.11100(18) 0.29372(17) 0.0455(7) Uani 1 d . . .
 H2A H 1.0049 -0.1198 0.3032 0.068 Uiso 1 calc . . GR
 H2B H 0.8836 -0.1718 0.2849 0.068 Uiso 1 calc . . GR
 H2C H 0.8380 -0.0878 0.3385 0.068 Uiso 1 calc . . GR
 C21 C 0.3952(3) 0.64782(18) 0.24221(16) 0.0385(6) Uani 1 d . . .
 C8 C 1.2202(3) 0.2096(2) 0.15044(17) 0.0471(7) Uani 1 d . . .
 H8A H 1.1935 0.2417 0.0985 0.071 Uiso 1 calc . . GR
 H8B H 1.3266 0.2024 0.1596 0.071 Uiso 1 calc . . GR
 H8C H 1.1574 0.2474 0.1882 0.071 Uiso 1 calc . . GR
 C11 C 0.7873(3) 0.31816(19) 0.05827(16) 0.0393(6) Uani 1 d . . .
 H11A H 0.7307 0.3549 0.0983 0.059 Uiso 1 calc . . GR
 H11B H 0.7703 0.3574 0.0084 0.059 Uiso 1 calc . . GR
 H11C H 0.8950 0.2986 0.0700 0.059 Uiso 1 calc . . GR
 C23 C 0.4354(3) 0.73932(19) 0.21717(19) 0.0515(8) Uani 1 d . . .
 H23A H 0.4657 0.7625 0.2621 0.077 Uiso 1 calc . . GR
 H23B H 0.3476 0.7871 0.1934 0.077 Uiso 1 calc . . GR
 H23C H 0.5188 0.7276 0.1798 0.077 Uiso 1 calc . . GR
 C22 C 0.3565(3) 0.6077(2) 0.17253(19) 0.0583(9) Uani 1 d . . .
 H22A H 0.4423 0.5967 0.1366 0.087 Uiso 1 calc . . GR
 H22B H 0.2683 0.6530 0.1470 0.087 Uiso 1 calc . . GR
 H22C H 0.3339 0.5475 0.1893 0.087 Uiso 1 calc . . GR


_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;
loop_
  _geom_bond_atom_site_label_1
  _geom_bond_atom_site_label_2
  _geom_bond_distance
  _geom_bond_site_symmetry_2
  _geom_bond_publ_flag
 I1 Cr1 2.7353(5) . ?
 Cr1 O5 1.8202(15) . ?
 Cr1 O1 1.8511(14) . ?
 Cr1 N1 2.1920(19) . ?
 Cr1 N2 2.1152(16) . ?
 Si1 O2 1.6311(16) . ?
 Si1 O1 1.5858(15) . ?
 Si1 O4 1.6293(15) . ?
 Si1 O3 1.6227(15) . ?
 Si2 O5 1.5961(15) . ?
 Si2 O6 1.6167(16) . ?
 Si2 O7 1.6206(16) . ?
 Si2 O8 1.6252(15) . ?
 O2 C1 1.442(3) . ?
 O6 C14 1.444(2) . ?
 O4 C9 1.443(3) . ?
 O7 C17 1.438(3) . ?
 O3 C5 1.438(2) . ?
 O8 C21 1.435(3) . ?
 N1 C26 1.486(3) . ?
 N1 C27 1.502(3) . ?
 N1 C25 1.484(3) . ?
 N2 C29 1.487(3) . ?
 N2 C28 1.483(3) . ?
 N2 C30 1.477(3) . ?
 C14 C15 1.519(3) . ?
 C14 C16 1.525(3) . ?
 C14 C13 1.515(3) . ?
 C1 C4 1.517(3) . ?
 C1 C3 1.512(3) . ?
 C1 C2 1.515(4) . ?
 C5 C7 1.528(3) . ?
 C5 C6 1.513(4) . ?
 C5 C8 1.512(4) . ?
 C28 C27 1.499(3) . ?
 C20 C17 1.524(3) . ?
 C33 C31 1.377(3) 2_656 ?
 C33 C32 1.380(4) . ?
 C18 C17 1.516(3) . ?
 C9 C12 1.521(3) . ?
 C9 C10 1.517(3) . ?
 C9 C11 1.518(3) . ?
 C17 C19 1.522(3) . ?
 C31 C33 1.377(3) 2_656 ?
 C31 C32 1.375(3) . ?
 C24 C21 1.509(4) . ?
 C21 C23 1.515(4) . ?
 C21 C22 1.524(4) . ?

loop_
  _geom_angle_atom_site_label_1
  _geom_angle_atom_site_label_2
  _geom_angle_atom_site_label_3
  _geom_angle
  _geom_angle_site_symmetry_1
  _geom_angle_site_symmetry_3
  _geom_angle_publ_flag
 O5 Cr1 I1 91.79(4) . . ?
 O5 Cr1 O1 119.89(7) . . ?
 O5 Cr1 N1 144.28(7) . . ?
 O5 Cr1 N2 88.82(6) . . ?
 O1 Cr1 I1 96.89(4) . . ?
 O1 Cr1 N1 95.01(7) . . ?
 O1 Cr1 N2 93.91(6) . . ?
 N1 Cr1 I1 91.26(5) . . ?
 N2 Cr1 I1 167.16(5) . . ?
 N2 Cr1 N1 80.87(7) . . ?
 O1 Si1 O2 105.03(8) . . ?
 O1 Si1 O4 113.95(8) . . ?
 O1 Si1 O3 113.99(8) . . ?
 O4 Si1 O2 106.00(8) . . ?
 O3 Si1 O2 112.36(8) . . ?
 O3 Si1 O4 105.38(8) . . ?
 O5 Si2 O6 113.47(8) . . ?
 O5 Si2 O7 111.99(8) . . ?
 O5 Si2 O8 106.05(8) . . ?
 O6 Si2 O7 107.49(8) . . ?
 O6 Si2 O8 107.15(8) . . ?
 O7 Si2 O8 110.60(9) . . ?
 Si2 O5 Cr1 178.22(10) . . ?
 C1 O2 Si1 132.74(15) . . ?
 Si1 O1 Cr1 166.87(9) . . ?
 C14 O6 Si2 132.75(14) . . ?
 C9 O4 Si1 131.20(13) . . ?
 C17 O7 Si2 132.77(14) . . ?
 C5 O3 Si1 134.11(14) . . ?
 C21 O8 Si2 134.65(15) . . ?
 C26 N1 Cr1 111.46(14) . . ?
 C26 N1 C27 108.24(18) . . ?
 C27 N1 Cr1 108.45(13) . . ?
 C25 N1 Cr1 112.24(15) . . ?
 C25 N1 C26 107.96(19) . . ?
 C25 N1 C27 108.37(18) . . ?
 C29 N2 Cr1 110.30(13) . . ?
 C28 N2 Cr1 105.29(12) . . ?
 C28 N2 C29 111.10(17) . . ?
 C30 N2 Cr1 112.81(12) . . ?
 C30 N2 C29 107.91(16) . . ?
 C30 N2 C28 109.47(17) . . ?
 O6 C14 C15 105.31(18) . . ?
 O6 C14 C16 108.52(18) . . ?
 O6 C14 C13 110.13(18) . . ?
 C15 C14 C16 110.3(2) . . ?
 C13 C14 C15 111.2(2) . . ?
 C13 C14 C16 111.2(2) . . ?
 O2 C1 C4 107.96(18) . . ?
 O2 C1 C3 111.18(18) . . ?
 O2 C1 C2 105.2(2) . . ?
 C3 C1 C4 111.4(2) . . ?
 C3 C1 C2 110.6(2) . . ?
 C2 C1 C4 110.3(2) . . ?
 O3 C5 C7 105.29(19) . . ?
 O3 C5 C6 110.45(19) . . ?
 O3 C5 C8 108.5(2) . . ?
 C6 C5 C7 111.1(2) . . ?
 C8 C5 C7 110.7(2) . . ?
 C8 C5 C6 110.6(2) . . ?
 N2 C28 C27 109.08(18) . . ?
 C31 C33 C32 120.3(2) 2_656 . ?
 C28 C27 N1 110.64(18) . . ?
 O4 C9 C12 105.34(18) . . ?
 O4 C9 C10 108.8(2) . . ?
 O4 C9 C11 110.30(19) . . ?
 C10 C9 C12 110.1(2) . . ?
 C10 C9 C11 111.3(2) . . ?
 C11 C9 C12 110.9(2) . . ?
 O7 C17 C20 107.3(2) . . ?
 O7 C17 C18 105.81(18) . . ?
 O7 C17 C19 112.58(18) . . ?
 C18 C17 C20 110.7(2) . . ?
 C18 C17 C19 110.5(2) . . ?
 C19 C17 C20 109.8(2) . . ?
 C32 C31 C33 120.1(2) . 2_656 ?
 C31 C32 C33 119.6(2) . . ?
 O8 C21 C24 105.9(2) . . ?
 O8 C21 C23 111.7(2) . . ?
 O8 C21 C22 107.3(2) . . ?
 C24 C21 C23 111.4(3) . . ?
 C24 C21 C22 110.2(3) . . ?
 C23 C21 C22 110.2(2) . . ?

_olex2_submission_special_instructions 'No special instructions were received'
