data_csmnsbcl
_audit_creation_date              2017-11-27
_audit_creation_method
;
Olex2 1.2-beta
(compiled 2017.08.10 svn.r3458 for OlexSys, GUI svn.r5381)
;
_shelx_SHELXL_version_number      '2014/7'
_publ_contact_author_address      ?
_publ_contact_author_email        ?
_publ_contact_author_id_orcid     ?
_publ_contact_author_name         ''
_publ_contact_author_phone        ?
_publ_section_references
;
Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H.
 (2009), J. Appl. Cryst. 42, 339-341.

Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8.
;
_chemical_name_common             ?
_chemical_name_systematic         ?
_chemical_formula_moiety          '2(Cl18 Cs6 Mn1.5 Sb3)'
_chemical_formula_sum             'Cl36 Cs12 Mn3 Sb6'
_chemical_formula_weight          3766.44
_chemical_melting_point           ?
loop_
  _atom_type_symbol
  _atom_type_description
  _atom_type_scat_dispersion_real
  _atom_type_scat_dispersion_imag
  _atom_type_scat_source
 'Cl' 'Cl' 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Cs' 'Cs' -0.3680 2.1192
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Mn' 'Mn' 0.3368 0.7283 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Sb' 'Sb' -0.5866 1.5461
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system       'trigonal'
_space_group_IT_number            166
_space_group_name_H-M_alt         'R -3 m'
_space_group_name_Hall            '-R 3 2"'
loop_
  _space_group_symop_operation_xyz
 'x, y, z'
 '-y, x-y, z'
 '-x+y, -x, z'
 'y, x, -z'
 'x-y, -y, -z'
 '-x, -x+y, -z'
 'x+2/3, y+1/3, z+1/3'
 '-y+2/3, x-y+1/3, z+1/3'
 '-x+y+2/3, -x+1/3, z+1/3'
 'y+2/3, x+1/3, -z+1/3'
 'x-y+2/3, -y+1/3, -z+1/3'
 '-x+2/3, -x+y+1/3, -z+1/3'
 'x+1/3, y+2/3, z+2/3'
 '-y+1/3, x-y+2/3, z+2/3'
 '-x+y+1/3, -x+2/3, z+2/3'
 'y+1/3, x+2/3, -z+2/3'
 'x-y+1/3, -y+2/3, -z+2/3'
 '-x+1/3, -x+y+2/3, -z+2/3'
 '-x, -y, -z'
 'y, -x+y, -z'
 'x-y, x, -z'
 '-y, -x, z'
 '-x+y, y, z'
 'x, x-y, z'
 '-x+2/3, -y+1/3, -z+1/3'
 'y+2/3, -x+y+1/3, -z+1/3'
 'x-y+2/3, x+1/3, -z+1/3'
 '-y+2/3, -x+1/3, z+1/3'
 '-x+y+2/3, y+1/3, z+1/3'
 'x+2/3, x-y+1/3, z+1/3'
 '-x+1/3, -y+2/3, -z+2/3'
 'y+1/3, -x+y+2/3, -z+2/3'
 'x-y+1/3, x+2/3, -z+2/3'
 '-y+1/3, -x+2/3, z+2/3'
 '-x+y+1/3, y+2/3, z+2/3'
 'x+1/3, x-y+2/3, z+2/3'

_cell_length_a                    7.4766(7)
_cell_length_b                    7.4766(7)
_cell_length_c                    36.302(4)
_cell_angle_alpha                 90
_cell_angle_beta                  90
_cell_angle_gamma                 120
_cell_volume                      1757.4(4)
_cell_formula_units_Z             1
_cell_measurement_reflns_used     3271
_cell_measurement_temperature     100(2)
_cell_measurement_theta_max       30.31
_cell_measurement_theta_min       3.20
_shelx_estimated_absorpt_T_max    0.783
_shelx_estimated_absorpt_T_min    0.554
_exptl_absorpt_coefficient_mu     10.296
_exptl_absorpt_correction_T_max   0.2657
_exptl_absorpt_correction_T_min   0.1940
_exptl_absorpt_correction_type    multi-scan
_exptl_absorpt_process_details
'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0635 before and 0.0394 after correction. The Ratio of minimum to maximum transmission is 0.7301. The λ/2 correction factor is Not present.'
_exptl_absorpt_special_details    ?
_exptl_crystal_colour             colorless
_exptl_crystal_colour_primary     colorless
_exptl_crystal_density_diffrn     3.559
_exptl_crystal_density_meas       ?
_exptl_crystal_density_method     ?
_exptl_crystal_description        irregular
_exptl_crystal_F_000              1653
_exptl_crystal_size_max           0.065
_exptl_crystal_size_mid           0.03
_exptl_crystal_size_min           0.025
_exptl_transmission_factor_max    ?
_exptl_transmission_factor_min    ?
_diffrn_reflns_av_R_equivalents   0.0217
_diffrn_reflns_av_unetI/netI      0.0110
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 1.000
_diffrn_reflns_limit_h_max        8
_diffrn_reflns_limit_h_min        -10
_diffrn_reflns_limit_k_max        10
_diffrn_reflns_limit_k_min        -6
_diffrn_reflns_limit_l_max        49
_diffrn_reflns_limit_l_min        -39
_diffrn_reflns_number             6648
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 1.000
_diffrn_reflns_theta_full         25.242
_diffrn_reflns_theta_max          29.092
_diffrn_reflns_theta_min          1.683
_diffrn_ambient_temperature       100.0
_diffrn_detector                  'Bruker APEX-II CCD'
_diffrn_detector_area_resol_mean  8.258
_diffrn_detector_type             'CCD Area Detector'
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device        'Kappa Four-Circle Diffractometer'
_diffrn_measurement_device_type   'Bruker APEX II Ultra'
_diffrn_measurement_method        'ω and φ scans'
_diffrn_radiation_monochromator   'Double Bounce Multilayer Mirrors'
_diffrn_radiation_probe           X-ray
_diffrn_radiation_type            MoK\a
_diffrn_radiation_wavelength      0.71073
_diffrn_source                    'Micro Focus Rotating Anode'
_diffrn_source_type               'Bruker TXS'
_diffrn_standards_number          0
_reflns_Friedel_coverage          0.000
_reflns_Friedel_fraction_full     .
_reflns_Friedel_fraction_max      .
_reflns_number_gt                 592
_reflns_number_total              647
_reflns_special_details
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression      'I > 2σ(I)'
_computing_cell_refinement        'SAINT v8.37A (Bruker, 2016)'
_computing_data_collection        'APEX3 v2016.1-0 (Bruker, 2016)'
_computing_data_reduction         'SAINT v8.37A (Bruker, 2016)'
_computing_molecular_graphics     'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material   'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement   'ShelXL (Sheldrick, 2015)'
_computing_structure_solution     'ShelXT (Sheldrick, 2015)'
_refine_diff_density_max          0.852
_refine_diff_density_min          -0.618
_refine_diff_density_rms          0.117
_refine_ls_extinction_coef        .
_refine_ls_extinction_method      none
_refine_ls_goodness_of_fit_ref    1.118
_refine_ls_hydrogen_treatment     undef
_refine_ls_matrix_type            full
_refine_ls_number_parameters      24
_refine_ls_number_reflns          647
_refine_ls_number_restraints      0
_refine_ls_R_factor_all           0.0178
_refine_ls_R_factor_gt            0.0144
_refine_ls_restrained_S_all       1.118
_refine_ls_shift/su_max           0.003
_refine_ls_shift/su_mean          0.000
_refine_ls_structure_factor_coef  Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0129P)²+2.6121P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme       calc
_refine_ls_wR_factor_gt           0.0311
_refine_ls_wR_factor_ref          0.0321
_refine_special_details           ?
_olex2_refinement_description
;
;
_atom_sites_solution_hydrogens    .
_atom_sites_solution_primary      ?
_atom_sites_solution_secondary    ?
loop_
  _atom_site_label
  _atom_site_type_symbol
  _atom_site_fract_x
  _atom_site_fract_y
  _atom_site_fract_z
  _atom_site_U_iso_or_equiv
  _atom_site_adp_type
  _atom_site_occupancy
  _atom_site_site_symmetry_order
  _atom_site_calc_flag
  _atom_site_refinement_flags_posn
  _atom_site_refinement_flags_adp
  _atom_site_refinement_flags_occupancy
  _atom_site_disorder_assembly
  _atom_site_disorder_group
 Cs1 Cs 0.6667 0.3333 0.46019(2) 0.01525(8) Uani 1 6 d S T P . .
 Cs2 Cs 0.0000 0.0000 0.62293(2) 0.01414(8) Uani 1 6 d S T P . .
 Sb1 Sb 0.6667 0.3333 0.58760(2) 0.00912(8) Uani 1 6 d S T P . .
 Mn1 Mn 0.0000 0.0000 0.5000 0.01038(19) Uani 1 12 d S T P . .
 Cl1 Cl 0.31595(9) 0.15797(5) 0.54061(2) 0.01729(15) Uani 1 2 d S T P . .
 Cl2 Cl 0.98239(9) 0.49120(5) 0.62559(2) 0.01555(14) Uani 1 2 d S T P . .


_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
  _geom_bond_atom_site_label_1
  _geom_bond_atom_site_label_2
  _geom_bond_distance
  _geom_bond_site_symmetry_2
  _geom_bond_publ_flag
 Cs1 Cl1 3.6986(7) . ?
 Cs1 Cl1 3.7401(4) 19_656 ?
 Cs1 Cl1 3.7401(4) 21_656 ?
 Cs1 Cl1 3.7401(4) 20_556 ?
 Cs1 Cl1 3.7401(4) 21_556 ?
 Cs1 Cl1 3.7401(3) 20_666 ?
 Cs1 Cl1 3.7401(4) 19_666 ?
 Cs1 Cl1 3.6986(7) 2_655 ?
 Cs1 Cl1 3.6986(7) 3_665 ?
 Cs1 Cl2 3.8546(7) 21_546 ?
 Cs1 Cl2 3.8546(7) 19_766 ?
 Cs1 Cl2 3.8546(7) 20_566 ?
 Cs2 Cl1 3.6215(7) 3 ?
 Cs2 Cl1 3.6215(7) 2 ?
 Cs2 Cl1 3.6215(7) . ?
 Cs2 Cl2 3.7413(4) 3_565 ?
 Cs2 Cl2 3.7413(4) 3_665 ?
 Cs2 Cl2 3.7413(4) 2_545 ?
 Cs2 Cl2 3.6961(7) 26_456 ?
 Cs2 Cl2 3.7413(4) 2_655 ?
 Cs2 Cl2 3.6961(7) 27_446 ?
 Cs2 Cl2 3.7413(4) 1_455 ?
 Cs2 Cl2 3.7413(4) 1_445 ?
 Cs2 Cl2 3.6961(7) 25_556 ?
 Sb1 Cs2 4.4581(6) 25_556 ?
 Sb1 Cs2 4.5031(4) 1_665 ?
 Sb1 Cs2 4.5031(4) 1_655 ?
 Sb1 Cl1 2.8402(6) 3_665 ?
 Sb1 Cl1 2.8403(6) . ?
 Sb1 Cl1 2.8402(6) 2_655 ?
 Sb1 Cl2 2.4659(6) . ?
 Sb1 Cl2 2.4659(6) 3_665 ?
 Sb1 Cl2 2.4659(6) 2_655 ?
 Mn1 Cs2 4.4625(5) 19_556 ?
 Mn1 Cl1 2.5215(6) 2 ?
 Mn1 Cl1 2.5215(6) 20_556 ?
 Mn1 Cl1 2.5215(6) 21_556 ?
 Mn1 Cl1 2.5215(6) 19_556 ?
 Mn1 Cl1 2.5215(6) 3 ?
 Mn1 Cl1 2.5215(6) . ?
 Cl1 Cs1 3.7401(4) 19_656 ?
 Cl1 Cs1 3.7401(4) 19_666 ?
 Cl2 Cs1 3.8546(7) 19_766 ?
 Cl2 Cs2 3.7413(4) 1_665 ?
 Cl2 Cs2 3.6960(7) 25_556 ?
 Cl2 Cs2 3.7413(4) 1_655 ?

loop_
  _geom_angle_atom_site_label_1
  _geom_angle_atom_site_label_2
  _geom_angle_atom_site_label_3
  _geom_angle
  _geom_angle_site_symmetry_1
  _geom_angle_site_symmetry_3
  _geom_angle_publ_flag
 Cl1 Cs1 Cl1 64.244(17) . 2_655 ?
 Cl1 Cs1 Cl1 57.681(16) 2_655 19_656 ?
 Cl1 Cs1 Cl1 176.440(19) 20_556 20_666 ?
 Cl1 Cs1 Cl1 63.447(19) 19_666 21_556 ?
 Cl1 Cs1 Cl1 121.891(8) . 20_666 ?
 Cl1 Cs1 Cl1 63.447(19) 21_656 20_666 ?
 Cl1 Cs1 Cl1 121.890(8) 2_655 21_556 ?
 Cl1 Cs1 Cl1 64.244(17) . 3_665 ?
 Cl1 Cs1 Cl1 63.447(19) 20_556 19_656 ?
 Cl1 Cs1 Cl1 176.44(2) 19_666 19_656 ?
 Cl1 Cs1 Cl1 57.681(16) 3_665 20_666 ?
 Cl1 Cs1 Cl1 64.244(16) 2_655 3_665 ?
 Cl1 Cs1 Cl1 120.0 19_656 20_666 ?
 Cl1 Cs1 Cl1 57.681(16) . 21_556 ?
 Cl1 Cs1 Cl1 176.440(19) 21_656 21_556 ?
 Cl1 Cs1 Cl1 121.891(8) . 21_656 ?
 Cl1 Cs1 Cl1 56.549(19) 20_556 21_556 ?
 Cl1 Cs1 Cl1 56.549(19) 21_656 19_656 ?
 Cl1 Cs1 Cl1 120.0 21_656 20_556 ?
 Cl1 Cs1 Cl1 57.681(16) 2_655 21_656 ?
 Cl1 Cs1 Cl1 91.407(10) . 19_666 ?
 Cl1 Cs1 Cl1 91.407(10) 2_655 20_666 ?
 Cl1 Cs1 Cl1 121.891(8) 2_655 19_666 ?
 Cl1 Cs1 Cl1 91.406(10) 3_665 21_656 ?
 Cl1 Cs1 Cl1 57.681(16) 3_665 19_666 ?
 Cl1 Cs1 Cl1 56.549(19) 19_666 20_666 ?
 Cl1 Cs1 Cl1 120.0 21_656 19_666 ?
 Cl1 Cs1 Cl1 57.681(16) . 20_556 ?
 Cl1 Cs1 Cl1 120.0 20_556 19_666 ?
 Cl1 Cs1 Cl1 91.407(10) 3_665 21_556 ?
 Cl1 Cs1 Cl1 91.407(10) . 19_656 ?
 Cl1 Cs1 Cl1 91.406(10) 2_655 20_556 ?
 Cl1 Cs1 Cl1 121.890(8) 3_665 19_656 ?
 Cl1 Cs1 Cl1 120.0 20_666 21_556 ?
 Cl1 Cs1 Cl1 121.891(8) 3_665 20_556 ?
 Cl1 Cs1 Cl1 119.994(1) 19_656 21_556 ?
 Cl1 Cs1 Cl2 117.168(12) . 21_546 ?
 Cl1 Cs1 Cl2 88.627(10) 21_556 21_546 ?
 Cl1 Cs1 Cl2 59.494(11) 21_656 19_766 ?
 Cl1 Cs1 Cl2 120.860(13) 21_556 19_766 ?
 Cl1 Cs1 Cl2 117.169(12) 2_655 19_766 ?
 Cl1 Cs1 Cl2 88.627(10) 20_666 20_566 ?
 Cl1 Cs1 Cl2 120.860(14) 20_666 21_546 ?
 Cl1 Cs1 Cl2 117.169(12) 2_655 21_546 ?
 Cl1 Cs1 Cl2 178.243(13) . 19_766 ?
 Cl1 Cs1 Cl2 120.859(13) 21_656 20_566 ?
 Cl1 Cs1 Cl2 117.169(13) 3_665 19_766 ?
 Cl1 Cs1 Cl2 178.244(13) 3_665 21_546 ?
 Cl1 Cs1 Cl2 59.495(11) 19_656 21_546 ?
 Cl1 Cs1 Cl2 88.627(10) 19_656 19_766 ?
 Cl1 Cs1 Cl2 117.169(12) . 20_566 ?
 Cl1 Cs1 Cl2 88.628(10) 21_656 21_546 ?
 Cl1 Cs1 Cl2 117.169(12) 3_665 20_566 ?
 Cl1 Cs1 Cl2 178.244(13) 2_655 20_566 ?
 Cl1 Cs1 Cl2 88.628(10) 20_556 20_566 ?
 Cl1 Cs1 Cl2 59.494(11) 20_556 21_546 ?
 Cl1 Cs1 Cl2 120.860(13) 19_656 20_566 ?
 Cl1 Cs1 Cl2 59.494(12) 19_666 20_566 ?
 Cl1 Cs1 Cl2 59.495(11) 21_556 20_566 ?
 Cl1 Cs1 Cl2 120.859(13) 19_666 21_546 ?
 Cl1 Cs1 Cl2 88.628(10) 19_666 19_766 ?
 Cl1 Cs1 Cl2 120.859(13) 20_556 19_766 ?
 Cl1 Cs1 Cl2 59.495(11) 20_666 19_766 ?
 Cl2 Cs1 Cl2 61.398(16) 21_546 20_566 ?
 Cl2 Cs1 Cl2 61.398(16) 21_546 19_766 ?
 Cl2 Cs1 Cl2 61.398(16) 19_766 20_566 ?
 Cl1 Cs2 Cl1 58.577(16) 3 2 ?
 Cl1 Cs2 Cl1 58.576(17) 3 . ?
 Cl1 Cs2 Cl1 58.577(17) 2 . ?
 Cl1 Cs2 Cl2 61.567(12) . 3_665 ?
 Cl1 Cs2 Cl2 61.567(13) 3 2_545 ?
 Cl1 Cs2 Cl2 120.099(13) . 3_565 ?
 Cl1 Cs2 Cl2 61.567(12) . 2_655 ?
 Cl1 Cs2 Cl2 92.206(10) 3 3_665 ?
 Cl1 Cs2 Cl2 120.099(13) 2 1_445 ?
 Cl1 Cs2 Cl2 92.206(10) . 1_445 ?
 Cl1 Cs2 Cl2 120.099(13) . 2_545 ?
 Cl1 Cs2 Cl2 61.566(12) 2 3_565 ?
 Cl1 Cs2 Cl2 61.567(12) 2 1_455 ?
 Cl1 Cs2 Cl2 92.206(10) . 1_455 ?
 Cl1 Cs2 Cl2 122.089(13) 2 27_446 ?
 Cl1 Cs2 Cl2 122.089(13) 3 26_456 ?
 Cl1 Cs2 Cl2 122.090(13) . 27_446 ?
 Cl1 Cs2 Cl2 61.566(12) 3 1_445 ?
 Cl1 Cs2 Cl2 122.089(13) 3 25_556 ?
 Cl1 Cs2 Cl2 179.185(13) 2 26_456 ?
 Cl1 Cs2 Cl2 122.089(13) 2 25_556 ?
 Cl1 Cs2 Cl2 92.206(10) 2 2_545 ?
 Cl1 Cs2 Cl2 179.186(14) . 25_556 ?
 Cl1 Cs2 Cl2 122.090(12) . 26_456 ?
 Cl1 Cs2 Cl2 120.099(13) 3 2_655 ?
 Cl1 Cs2 Cl2 120.099(13) 3 1_455 ?
 Cl1 Cs2 Cl2 92.207(10) 2 2_655 ?
 Cl1 Cs2 Cl2 179.186(13) 3 27_446 ?
 Cl1 Cs2 Cl2 92.207(10) 3 3_565 ?
 Cl1 Cs2 Cl2 120.099(13) 2 3_665 ?
 Cl2 Cs2 Cl2 117.746(9) 26_456 3_565 ?
 Cl2 Cs2 Cl2 87.802(10) 27_446 3_565 ?
 Cl2 Cs2 Cl2 175.42(2) 2_655 2_545 ?
 Cl2 Cs2 Cl2 119.934(1) 2_545 1_455 ?
 Cl2 Cs2 Cl2 117.746(9) 27_446 2_545 ?
 Cl2 Cs2 Cl2 60.549(16) 26_456 3_665 ?
 Cl2 Cs2 Cl2 56.486(19) 1_445 2_545 ?
 Cl2 Cs2 Cl2 60.549(16) 26_456 1_445 ?
 Cl2 Cs2 Cl2 87.803(10) 26_456 2_545 ?
 Cl2 Cs2 Cl2 56.486(18) 2_655 3_665 ?
 Cl2 Cs2 Cl2 60.549(16) 25_556 2_545 ?
 Cl2 Cs2 Cl2 119.934(1) 3_665 1_455 ?
 Cl2 Cs2 Cl2 63.470(19) 3_565 2_545 ?
 Cl2 Cs2 Cl2 60.548(15) 27_446 1_455 ?
 Cl2 Cs2 Cl2 57.240(16) 26_456 25_556 ?
 Cl2 Cs2 Cl2 87.803(10) 25_556 1_445 ?
 Cl2 Cs2 Cl2 57.240(16) 27_446 25_556 ?
 Cl2 Cs2 Cl2 87.803(10) 27_446 3_665 ?
 Cl2 Cs2 Cl2 175.42(2) 3_565 3_665 ?
 Cl2 Cs2 Cl2 119.934(1) 2_655 1_445 ?
 Cl2 Cs2 Cl2 119.934(1) 2_545 3_665 ?
 Cl2 Cs2 Cl2 63.470(18) 1_445 3_665 ?
 Cl2 Cs2 Cl2 119.934(1) 2_655 3_565 ?
 Cl2 Cs2 Cl2 119.934(1) 3_565 1_445 ?
 Cl2 Cs2 Cl2 117.746(9) 26_456 1_455 ?
 Cl2 Cs2 Cl2 87.802(10) 26_456 2_655 ?
 Cl2 Cs2 Cl2 87.802(10) 25_556 1_455 ?
 Cl2 Cs2 Cl2 57.240(17) 26_456 27_446 ?
 Cl2 Cs2 Cl2 56.486(19) 3_565 1_455 ?
 Cl2 Cs2 Cl2 63.470(19) 2_655 1_455 ?
 Cl2 Cs2 Cl2 60.549(16) 27_446 2_655 ?
 Cl2 Cs2 Cl2 117.746(9) 25_556 2_655 ?
 Cl2 Cs2 Cl2 117.747(9) 27_446 1_445 ?
 Cl2 Cs2 Cl2 175.42(2) 1_445 1_455 ?
 Cl2 Cs2 Cl2 60.548(15) 25_556 3_565 ?
 Cl2 Cs2 Cl2 117.746(9) 25_556 3_665 ?
 Cs2 Sb1 Cs2 112.230(5) . 1_665 ?
 Cs2 Sb1 Cs2 73.453(5) 25_556 . ?
 Cs2 Sb1 Cs2 112.230(5) 1_655 1_665 ?
 Cs2 Sb1 Cs2 73.452(5) 25_556 1_665 ?
 Cs2 Sb1 Cs2 112.230(5) 1_655 . ?
 Cs2 Sb1 Cs2 73.453(5) 25_556 1_655 ?
 Cl1 Sb1 Cs2 123.661(3) 3_665 . ?
 Cl1 Sb1 Cs2 53.462(14) 3_665 1_665 ?
 Cl1 Sb1 Cs2 126.914(14) 3_665 25_556 ?
 Cl1 Sb1 Cs2 123.661(3) 2_655 1_665 ?
 Cl1 Sb1 Cs2 126.915(14) . 25_556 ?
 Cl1 Sb1 Cs2 53.462(14) 2_655 1_655 ?
 Cl1 Sb1 Cs2 123.661(3) . 1_665 ?
 Cl1 Sb1 Cs2 126.914(14) 2_655 25_556 ?
 Cl1 Sb1 Cs2 123.661(3) . 1_655 ?
 Cl1 Sb1 Cs2 53.461(14) . . ?
 Cl1 Sb1 Cs2 123.660(3) 2_655 . ?
 Cl1 Sb1 Cs2 123.660(3) 3_665 1_655 ?
 Cl1 Sb1 Cl1 87.64(2) 2_655 3_665 ?
 Cl1 Sb1 Cl1 87.64(2) 2_655 . ?
 Cl1 Sb1 Cl1 87.64(2) 3_665 . ?
 Cl2 Sb1 Cs2 56.178(2) 2_655 . ?
 Cl2 Sb1 Cs2 55.999(15) . 25_556 ?
 Cl2 Sb1 Cs2 129.452(17) . . ?
 Cl2 Sb1 Cs2 56.178(2) 2_655 1_665 ?
 Cl2 Sb1 Cs2 129.451(17) 2_655 1_655 ?
 Cl2 Sb1 Cs2 56.178(2) . 1_665 ?
 Cl2 Sb1 Cs2 129.451(17) 3_665 1_665 ?
 Cl2 Sb1 Cs2 55.998(15) 2_655 25_556 ?
 Cl2 Sb1 Cs2 55.999(15) 3_665 25_556 ?
 Cl2 Sb1 Cs2 56.177(2) 3_665 1_655 ?
 Cl2 Sb1 Cs2 56.178(3) . 1_655 ?
 Cl2 Sb1 Cs2 56.179(3) 3_665 . ?
 Cl2 Sb1 Cl1 177.09(2) . . ?
 Cl2 Sb1 Cl1 90.254(14) 3_665 2_655 ?
 Cl2 Sb1 Cl1 177.09(2) 3_665 3_665 ?
 Cl2 Sb1 Cl1 90.255(14) . 2_655 ?
 Cl2 Sb1 Cl1 90.255(14) . 3_665 ?
 Cl2 Sb1 Cl1 177.09(2) 2_655 2_655 ?
 Cl2 Sb1 Cl1 90.256(14) 2_655 3_665 ?
 Cl2 Sb1 Cl1 90.256(14) 3_665 . ?
 Cl2 Sb1 Cl1 90.255(14) 2_655 . ?
 Cl2 Sb1 Cl2 91.77(2) . 3_665 ?
 Cl2 Sb1 Cl2 91.77(2) . 2_655 ?
 Cl2 Sb1 Cl2 91.77(2) 3_665 2_655 ?
 Cs2 Mn1 Cs2 180.0 . 19_556 ?
 Cl1 Mn1 Cs2 54.225(14) 20_556 19_556 ?
 Cl1 Mn1 Cs2 125.774(15) . 19_556 ?
 Cl1 Mn1 Cs2 125.775(14) 3 19_556 ?
 Cl1 Mn1 Cs2 125.775(14) 21_556 . ?
 Cl1 Mn1 Cs2 54.225(14) 19_556 19_556 ?
 Cl1 Mn1 Cs2 125.775(14) 20_556 . ?
 Cl1 Mn1 Cs2 54.226(15) . . ?
 Cl1 Mn1 Cs2 54.225(14) 21_556 19_556 ?
 Cl1 Mn1 Cs2 125.775(14) 2 19_556 ?
 Cl1 Mn1 Cs2 54.225(14) 2 . ?
 Cl1 Mn1 Cs2 125.775(14) 19_556 . ?
 Cl1 Mn1 Cs2 54.225(14) 3 . ?
 Cl1 Mn1 Cl1 179.999(16) . 19_556 ?
 Cl1 Mn1 Cl1 90.72(2) 19_556 3 ?
 Cl1 Mn1 Cl1 89.28(2) 20_556 21_556 ?
 Cl1 Mn1 Cl1 89.28(2) . 3 ?
 Cl1 Mn1 Cl1 89.28(2) 19_556 21_556 ?
 Cl1 Mn1 Cl1 90.72(2) . 20_556 ?
 Cl1 Mn1 Cl1 180.00(2) 20_556 2 ?
 Cl1 Mn1 Cl1 89.28(2) 19_556 20_556 ?
 Cl1 Mn1 Cl1 89.28(2) 2 3 ?
 Cl1 Mn1 Cl1 90.72(2) 20_556 3 ?
 Cl1 Mn1 Cl1 180.0 21_556 3 ?
 Cl1 Mn1 Cl1 90.72(2) 19_556 2 ?
 Cl1 Mn1 Cl1 89.28(2) . 2 ?
 Cl1 Mn1 Cl1 90.72(2) 2 21_556 ?
 Cl1 Mn1 Cl1 90.72(2) . 21_556 ?
 Cs1 Cl1 Cs1 176.441(19) 19_656 19_666 ?
 Cs1 Cl1 Cs1 88.594(10) . 19_666 ?
 Cs1 Cl1 Cs1 88.594(10) . 19_656 ?
 Cs2 Cl1 Cs1 91.337(10) . 19_656 ?
 Cs2 Cl1 Cs1 91.337(10) . 19_666 ?
 Cs2 Cl1 Cs1 176.516(18) . . ?
 Sb1 Cl1 Cs1 88.886(9) . 19_656 ?
 Sb1 Cl1 Cs1 89.036(18) . . ?
 Sb1 Cl1 Cs1 88.886(9) . 19_666 ?
 Sb1 Cl1 Cs2 87.479(17) . . ?
 Mn1 Cl1 Cs1 91.142(9) . 19_666 ?
 Mn1 Cl1 Cs1 92.104(18) . . ?
 Mn1 Cl1 Cs1 91.142(9) . 19_656 ?
 Mn1 Cl1 Cs2 91.380(19) . . ?
 Mn1 Cl1 Sb1 178.86(3) . . ?
 Cs2 Cl2 Cs1 87.778(10) 1_655 19_766 ?
 Cs2 Cl2 Cs1 87.777(10) 1_665 19_766 ?
 Cs2 Cl2 Cs1 177.459(18) 25_556 19_766 ?
 Cs2 Cl2 Cs2 92.197(10) 25_556 1_655 ?
 Cs2 Cl2 Cs2 175.43(2) 1_665 1_655 ?
 Cs2 Cl2 Cs2 92.196(10) 25_556 1_665 ?
 Sb1 Cl2 Cs1 92.120(19) . 19_766 ?
 Sb1 Cl2 Cs2 90.622(9) . 1_665 ?
 Sb1 Cl2 Cs2 90.42(2) . 25_556 ?
 Sb1 Cl2 Cs2 90.622(9) . 1_655 ?

_olex2_submission_special_instructions 'No special instructions were received'

