Hydrogenation of
Sugar Enol-Ethers Using Pd/Et3SiH Reagent System: A Route
to Deoxy Sugars/Glycosides
Posted on 2024-12-16 - 19:37
We have developed a hydrogenation method using Pd(OAc)2/Et3SiH as a reagent system for sugar enol ethers
and
their glycosides. This approach is highly effective and applicable
to a wide range of glycals and glycosides, achieving yields up to
96% for the corresponding deoxy sugars. Applying standard conditions
to various O/C-glycosides resulted in excellent transformation to
2,3-dideoxy glycosides.
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Tiwari, Bindu; Pandey, Ram Pratap; Hussain, Nazar (2024). Hydrogenation of
Sugar Enol-Ethers Using Pd/Et3SiH Reagent System: A Route
to Deoxy Sugars/Glycosides. ACS Publications. Collection. https://doi.org/10.1021/acs.joc.4c02031
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AUTHORS (3)
- BTBindu TiwariRPRam Pratap PandeyNHNazar Hussain
