Family of Conglomerate-Forming Systems Composed of
Chlocyphos and Alkyl-amine. Assessment of Their Resolution Performances
by Using Various Modes of Preferential Crystallization
Version 2 2019-08-22, 14:38
Version 1 2019-08-22, 14:35
Posted on 2019-08-22 - 14:38
The present study
aimed at screening conglomerate derivatives of racemic chlocyphos
(4-(2-chlorophenyl)-5,5-dimethyl-2-hydroxy-1,3,2-dioxaphosphorinane
2-oxide) and to perform enantiomeric separation by preferential crystallization.
A list of more than 20 chlocyphos salt derivatives were characterized
by various techniques (SHG, DSC, and X-ray powder diffraction). A
family of salts formed with various alkyl amines crystallizing as
conglomerates is evidenced. The first attempts to resolve these conglomerates
by preferential crystallization at small scale were successful. The
mitigated performances of these entrainments are discussed.
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Mbodji, Aliou; Gbabode, Gabin; Sanselme, Morgane; Couvrat, Nicolas; Leeman, Michel; Dupray, Valérie; et al. (2019). Family of Conglomerate-Forming Systems Composed of
Chlocyphos and Alkyl-amine. Assessment of Their Resolution Performances
by Using Various Modes of Preferential Crystallization. ACS Publications. Collection. https://doi.org/10.1021/acs.cgd.9b00568
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AUTHORS (8)
AM
Aliou Mbodji
GG
Gabin Gbabode
MS
Morgane Sanselme
NC
Nicolas Couvrat
ML
Michel Leeman
VD
Valérie Dupray
RK
Richard M. Kellogg
GC
Gérard Coquerel