Carbon–Carbon
Bond-Forming Reductive Elimination
from Isolated Nickel(III) Complexes
Posted on 2016-12-02 - 19:04
This
manuscript describes the design, synthesis, characterization,
and reactivity studies of organometallic NiIII complexes
of general structure TpNiIII(R)(R1) (Tp = tris(pyrazolyl)borate).
With appropriate selection of the R and R1 ligands, the
complexes are stable at room temperature and can be characterized
by cyclic voltammetry, EPR spectroscopy, and X-ray crystallography.
Upon heating, many of these NiIII compounds undergo C(sp2)–C(sp2) or C(sp3)–C(sp2) bond-forming reactions that are challenging at lower oxidation
states of nickel.
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Bour, James
R.; Camasso, Nicole M.; Meucci, Elizabeth A.; Kampf, Jeff W.; Canty, Allan J.; Sanford, Melanie S. (2016). Carbon–Carbon
Bond-Forming Reductive Elimination
from Isolated Nickel(III) Complexes. ACS Publications. Collection. https://doi.org/10.1021/jacs.6b10350
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AUTHORS (6)
JB
James
R. Bour
NC
Nicole M. Camasso
EM
Elizabeth A. Meucci
JK
Jeff W. Kampf
AC
Allan J. Canty
MS
Melanie S. Sanford